e03ba2376900a2d4c02b158fac2ef2c1

Test Report
No.: CQTC1101326/CHEM
Date: April 13, 2011
Page 1 of 15
CHONGQING PINGWEI ENTERPRISE CO., LTD
SHUANGGUI INDUSTRIAL PARK, ZAOJIAO CUN, LIANGSHAN TOWN, LIANGPING COUNTY, CHONGQING
THIS REPORT IS TO SUPERSEDE TEST REPORT NO. CQTC1100656/CHEM
The following sample(s) was/were submitted and identified on behalf of the applicant as: DO-41
SGS Job No.
Client Reference Information
: 13065108
: Test Model No : DO-41; Client Reference Model No: SOD-923,SOD-723,
SC-89,SOT-416,SOT-23,SOT-323,SOT-252,SOT-223,A-405,
DO-41,D0-204AL),DO-15, (D0-204AC),DO-27(D0-201AD),HVM,HV,
R-1,R-3,R-6,TO-220,TO-220AC AB,WOB,RB-1,MBS,BR-15,
RC-2,BRW,DB,DBS,GBJ,GBL,GBP,GBU,KBPC,KBP,KBU,KBL,
MB,MBR,MBUR,MM,RS,SMA(DO-214AC),SMB(DO-214AA),
SMC(DO-214AB),SOT-23,SOT-123,SOT-523,SOD-123,SOD-323,SOD-523 ,
TO-92 ,TO-126,SOD-126,ITO220AB,ABS,KBJ,,LL-34,DO-35,DO-41,LL-41
Date of Sample Received
: March 7, 2011
Testing Period
: March 7, 2011 to March 14, 2011
Test Requested
: Selected tests as requested by client.
Test Method (Reference)
: Please refer to next pages.
Test Results
: Please refer to next pages.
Conclusion
: Specimen 2: Based on the performed tests on submitted samples, the results
comply with the RoHS Directive 2002/95/EC and its subsequent amendments.
Signed for and on behalf of
SGS-CSTC Ltd.
______________________
Rain Qiao
Approved Signatory
Test Report
No.: CQTC1101326/CHEM
Date: April 13, 2011
Page 2 of 15
Test Results:
Description for specimen 1
: Black body with grey printing
A: RoHS Directive 2002/95/EC
Test Item(s)
Cadmium (Cd)
Lead (Pb)
Mercury (Hg)
Hexavalent Chromium (CrVI) by
alkaline extraction
Sum of PBBs
Monobromobiphenyl
Dibromobiphenyl
Tribromobiphenyl
Tetrabromobiphenyl
Pentabromobiphenyl
Hexabromobiphenyl
Heptabromobiphenyl
Octabromobiphenyl
Nonabromobiphenyl
Decabromobiphenyl
Sum of PBDEs
Monobromodiphenyl ether
Dibromodiphenyl ether
Tribromodiphenyl ether
Tetrabromodiphenyl ether
Pentabromodiphenyl ether
Hexabromodiphenyl ether
Heptabromodiphenyl ether
Octabromodiphenyl ether
Nonabromodiphenyl ether
Decabromodiphenyl ether
Note:
1. mg/kg = ppm
2. N.D. = Not Detected (< MDL)
3. MDL = Method Detection Limit
4. "-" = Not regulated
Unit
mg/kg
mg/kg
mg/kg
Test Method (Reference)
IEC 62321: 2008, ICP-OES
IEC 62321: 2008, ICP-OES
IEC 62321: 2008, ICP-OES
Result
N.D.
[1]
30982
N.D.
MDL
2
2
2
Limit
100
1000
1000
mg/kg
IEC 62321: 2008, UV-Vis
N.D.
2
1000
2008, GC-MS
2008, GC-MS
2008, GC-MS
2008, GC-MS
2008, GC-MS
2008, GC-MS
2008, GC-MS
2008, GC-MS
2008, GC-MS
2008, GC-MS
2008, GC-MS
2008, GC-MS
2008, GC-MS
2008, GC-MS
2008, GC-MS
2008, GC-MS
2008, GC-MS
2008, GC-MS
2008, GC-MS
2008, GC-MS
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
1000
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
IEC 62321:
IEC 62321:
IEC 62321:
IEC 62321:
IEC 62321:
IEC 62321:
IEC 62321:
IEC 62321:
IEC 62321:
IEC 62321:
IEC 62321:
IEC 62321:
IEC 62321:
IEC 62321:
IEC 62321:
IEC 62321:
IEC 62321:
IEC 62321:
IEC 62321:
IEC 62321:
1000
Test Report
No.: CQTC1101326/CHEM
Date: April 13, 2011
Page 3 of 15
B: PAHs (Polynuclear Aromatic Hydrocarbons)
Test Item(s)
Unit
Test Method
Naphthalene (NAP)
mg/kg
ZEK 01.2-08, GC-MS
Acenaphthylene (ANY)
mg/kg
ZEK 01.2-08, GC-MS
Acenaphthene (ANA)
mg/kg
ZEK 01.2-08, GC-MS
Fluorene (FLU)
mg/kg
ZEK 01.2-08, GC-MS
Phenanthrene (PHE)
mg/kg
ZEK 01.2-08, GC-MS
Anthracene (ANT)
mg/kg
ZEK 01.2-08, GC-MS
Fluoranthene (FLT)
mg/kg
ZEK 01.2-08, GC-MS
Pyrene (PYR)
mg/kg
ZEK 01.2-08, GC-MS
Benzo(a)anthracene (BaA)
mg/kg
ZEK 01.2-08, GC-MS
Chrysene (CHR)
mg/kg
ZEK 01.2-08, GC-MS
Benzo(b)fluoranthene (BbF)
mg/kg
ZEK 01.2-08, GC-MS
Benzo(k)fluoranthene (BkF)
mg/kg
ZEK 01.2-08, GC-MS
Benzo(a)pyrene (BaP)
mg/kg
ZEK 01.2-08, GC-MS
Indeno(1-,2,3-c,d)pyrene (IPY)
mg/kg
ZEK 01.2-08, GC-MS
Dibenzo(a,h)anthracene (DBA)
mg/kg
ZEK 01.2-08, GC-MS
Benzo(g,h,i)perylene (BPE)
mg/kg
ZEK 01.2-08, GC-MS
Sum of 16 PAHs acc. US EPA
mg/kg
Note:
1. mg/kg = ppm
2. N.D. = Not Detected (< MDL)
3. MDL = Method Detection Limit
4. This test was subcontracted to SGS Guangzhou chemical lab(GZ1103021412/CHEM)
Results
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
MDL
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.2
-
ZEK 01.2-08 : Restraining maximum values for products
Parameter
Category 1
Category 2
Category 3
Material indented to be put in Materials those are not
Materials those are not
the mouth or material for
included in Category 1, with included in Category 1 or 2,
toys with normal skin contact predictable contact with the with predictable skin contact
for children aged < 36
skin longer than 30 s. (long- up to 30 s (short-term skin
months
term skin contact).
contact).
Benzo[a]pyrene (mg/kg)
<MDL (<0.2)***
1
20
Sum of 16 PAH (US
EPA)(mg/kg)**
<MDL (<0.2)***
10
200
Remark:
** = Only PAH substances >0.2 mg/kg are taken into account while calculating the sum of PAHs.
*** = In case that the maximum values exceed the limits of category 1, but are within the limits of category 2,
one may confirm the suitability of the tested material which indented to be put in the mouth by additional
specific migration tests of PAH components based on DIN EN 1186ff and §64 LFGB 80.30-1. The conclusion
of the migration test results must be made based on food law criteria.
Test Report
No.: CQTC1101326/CHEM
Date: April 13, 2011
Page 4 of 15
C: PFOA & PFOS (Perfluorooctanoic acid & Perfluorooctane sulfonates)
Test Item(s)
Unit
Test Method (Reference)
Perfluorooctanoic acid (PFOA)
mg/kg
EPA 3550C: 2007, LC-MS
Perfluorooctane sulfonates (PFOS)
PFOS – Acid
mg/kg
EPA 3550C: 2007, LC-MS
PFOS – Metal Salt
PFOS – Amide
Note:
1. mg/kg = ppm
2. N.D. = Not Detected (< MDL)
3. MDL = Method Detection Limit
4. This test was subcontracted to SGS Guangzhou chemical lab(GZ1103021412/CHEM)
Result
MDL
N.D.
10
N.D.
10
For reference: Entry 53 of Regulation (EC) No 552/2009 amending Annex XVII of REACH Regulation (EC) No
1907/2006 (previously restricted under Directive 2006/122/EC):
(1) May not be placed on the market or used as a substance or constituent of preparations in a concentration equal to
or higher than 0,005 % by mass.
(2) May not be placed on the market in semi-finished products or articles, or parts thereof, if the concentration of PFOS
is equal to or higher than 0,1% by mass calculated with reference to the mass of structurally or microstructurally distinct
parts that contain PFOS or, for textiles or other coated materials, if the amount of PFOS is equal to or higher than 1µg
2
/m of the coated material.
D: TBBP-A (Tetrabromobisphenol A)
Test Item(s)
Unit
Test Method (Reference)
Tetrabromobisphenol A (TBBP-A)
mg/kg
EPA 3550C: 2007, GC-MS
Note:
1. mg/kg = ppm
2. N.D. = Not Detected (< MDL)
3. MDL = Method Detection Limit
4. This test was subcontracted to SGS Guangzhou chemical lab(GZ1103021412/CHEM)
Result
N.D.
MDL
10
E: SCCP (Short chained chlorinated paraffins)
Test Item(s)
Unit
Test Method (Reference)
Result
Short Chained Chlorinated
mg/kg
N.D.
EPA 3550C:2007,GC-ECD
Paraffins (C10-C13)
Note:
1. mg/kg = ppm
2. N.D. = Not Detected (< MDL)
3. MDL = Method Detection Limit
4. This test was subcontracted to SGS Guangzhou chemical lab(GZ1103021412/CHEM)
MDL
50
Test Report
No.: CQTC1101326/CHEM
Date: April 13, 2011
Page 5 of 15
F: Dimethyl Fumarate
Test Item(s)
Dimethyl Fumarate
Unit
Test Method (Reference)
Result
MDL
Limit
mg/kg
SGS In-house method(GZTC
CHEM-TOP-095), GC-MS
N.D.
0.1
0.1
Comment
PASS
Note:
1. mg/kg = ppm
2. N.D. = Not Detected (< MDL)
3. MDL = Method Detection Limit
4. This test was subcontracted to SGS Guangzhou chemical lab(GZ1103021412/CHEM)
Reference Information (2011/135/EU requirement):
The presence of DMF in products should be determined against the maximum limit of 0.1 mg DMF per kg of product or
part of the product.
G: Nonylphenol
Test Item(s)
Unit
Test Method (Reference)
Nonylphenol (NP)
mg/kg
EPA 3550C: 2007, LC-MS
Note:
1. mg/kg = ppm
2. N.D. = Not Detected (< MDL)
3. MDL = Method Detection Limit
4. This test was subcontracted to SGS Guangzhou chemical lab(GZ1103021412/CHEM)
Result
N.D.
MDL
10
Result
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
MDL
0.02
0.02
0.02
0.02
0.02
0.02
0.02
0.02
H: Organotin
Test Item(s)
Monobutyltin (MBT)
Dibutyltin (DBT)
Tributyltin (TBT)
Tetrabutyltin (TTBT)
Triphenyltin (TPhT)
Monooctyltin (MOT)
Dioctyltin (DOT)
Tricyclohexyltin (TCyT)
Unit
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
Test Method (Reference)
ISO 17353:2004, GC-MS
ISO 17353:2004, GC-MS
ISO 17353:2004, GC-MS
ISO 17353:2004, GC-MS
ISO 17353:2004, GC-MS
ISO 17353:2004, GC-MS
ISO 17353:2004, GC-MS
ISO 17353:2004, GC-MS
Note:
1. mg/kg = ppm
2. N.D. = Not Detected (< MDL)
3. MDL = Method Detection Limit
4. This test was subcontracted to SGS Guangzhou chemical lab(GZ1103021412/CHEM)
Test Report
No.: CQTC1101326/CHEM
Date: April 13, 2011
Page 6 of 15
I: Phthalate(s)
Test Item(s)
Dibutyl Phthalate (DBP)
Benzylbutyl Phthalate (BBP)
Di-(2-ethylhexyl) Phthalate (DEHP)
Diisononyl Phthalate (DINP)
Di-n-octyl Phthalate (DNOP)
Diisodecyl Phthalate (DIDP)
Di-n-hexyl phthalate (DnHP)
Diisobutyl Phthalate (DIBP)
Unit
%(w/w)
%(w/w)
%(w/w)
%(w/w)
%(w/w)
%(w/w)
%(w/w)
%(w/w)
Test Method (Reference)
EN14372: 2004, GC-MS
EN14372: 2004, GC-MS
EN14372: 2004, GC-MS
EN14372: 2004, GC-MS
EN14372: 2004, GC-MS
EN14372: 2004, GC-MS
EN14372: 2004, GC-MS
EN14372: 2004, GC-MS
Note :
1. mg/kg = ppm; 0.1% = 1000ppm
2. MDL = Method Detection Limit
3. N.D. = Not detected (< MDL)
4. This test was subcontracted to SGS Guangzhou chemical lab (GZ1103024759/CHEM)
Result
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
MDL
0.003
0.003
0.003
0.01
0.003
0.01
0.003
0.003
Test Report
No.: CQTC1101326/CHEM
Description for specimen 2
RoHS Directive 2002/95/EC
Test Item(s)
Cadmium (Cd)
Lead (Pb)
Mercury (Hg)
Hexavalent Chromium (CrVI) by
boiling water extraction
:
Date: April 13, 2011
Page 7 of 15
Silvery metal pin
Unit
mg/kg
mg/kg
mg/kg
-
Test Method (Reference)
IEC 62321: 2008, ICP-OES
IEC 62321: 2008, ICP-OES
IEC 62321: 2008, ICP-OES
IEC 62321: 2008, UV-Vis
Result
N.D.
10
N.D.
Negative
MDL
2
2
2
◇
Limit
100
1000
1000
#
Note:
1. mg/kg = ppm
2. N.D. = Not Detected (< MDL)
3. MDL = Method Detection Limit
4. ◇ = Spot test:
Negative = Absence of CrVI coating, Positive = Presence of CrVI coating;
(The tested sample should be further verified by boiling water extraction method if the spot test result is negative
or cannot be confirmed.)
Boiling water extraction:
Negative = Absence of CrVI coating
Positive = Presence of CrVI coating; the detected concentration in boiling water extraction solution is equal or
2
greater than 0.02 mg/kg with 50 cm sample surface area.
Storage conditions and production date of the tested sample are unavailable and thus results of Cr(VI) represent
status of the sample at the time of testing.
5. # = Positive indicates the presence of CrVI on the tested area.
Negative indicates the absence of CrVI on the tested area.
6. "-" = Not regulated
Remark [1]: According to the declaration from client, the source of Lead in Specimen 1 could be from the high melting
temperature type solder, while Lead in high melting temperature type solders is exempted by RoHS
reglatory (Directive 2002/95/EC of the European Parliament and of the council of 27 January 2003)
Remark [2]: Specimen 1, As requested by client, the testing was conducted as whole / part sample, for the sample
can’t be disjointed
Test Report
No.: CQTC1101326/CHEM
Date: April 13, 2011
Page 8 of 15
ATTACHMENTS
RoHS Testing Flow Chart
1) Name of the person who made testing: Tess Lv/Roger Yang/Leo Wang
2) Name of the person in charge of testing: Rain Qiao
Sample Preparation
Sample Measurement
Pb/Cd/Hg
Acid digestion with
microwave/ hotplate
Filtration
Sample solvent
extraction
Concentration/
Dilution of extraction
solution
Solution
Cr6+
PBBs/PBDEs
Nonmetallic
material
Adding digestion
reagent
Positive
Spot test
Negative
Residue
Filtration
1) Alkali Fusion
/ Dry Ashing
2) Acid to
dissolve
GC/MS
Heating to 90~95℃
for extraction
Filtration and pH
adjustment
DATA
ICP-OES/AAS
DATA
Metallic
material
Adding 1,5diphenylcarbazide
for color
development
Boiling water
extraction
Adding 1,5diphenylcarbazide for
color development
A red color indicates
6+
the presence of Cr .
If necessary, confirm
with UV-Vis.
UV-Vis
DATA
DATA
Test Report
No.: CQTC1101326/CHEM
ATTACHMENTS
PAHs Testing Flow Chart
1) Name of the person who made testing: Cutey Yu
2) Name of the person in charge of testing: Ryan Yang
Sample cutting / preparation
Sample Measurement
Solvent extraction
Concentration/Dilution
Filtration
GC-MS
DATA
Date: April 13, 2011
Page 9 of 15
Test Report
No.: CQTC1101326/CHEM
ATTACHMENTS
PFOA / PFOS Testing Flow Chart
1) Name of the person who made testing: Cindy Huang
2) Name of the person in charge of testing: Ryan Yang
Sample cutting / preparation
Sample Measurement
Solvent extraction
Concentration/Dilution
Filtration
LC-MS
DATA
Date: April 13, 2011
Page 10 of 15
Test Report
No.: CQTC1101326/CHEM
ATTACHMENTS
TBBPTBBP-A Testing Flow Chart
1) Name of the person who made testing: Cutey Yu
2) Name of the person in charge of testing: Ryan Yang
Sample cutting / preparation
Sample Measurement
Solvent extraction
Derivatization
Liquid-liquid extraction
Concentration/Dilution
Filtration
GC-MS
DATA
Date: April 13, 2011
Page 11 of 15
Test Report
No.: CQTC1101326/CHEM
ATTACHMENTS
SCCP/MCCP Testing Flow Chart
1) Name of the person who made testing: Tina Zhao
2) Name of the person in charge of testing: Ryan Yang
Sample cutting / preparation
Sample Measurement
Solvent extraction
Concentration
Clean-Up
Filtration
GC-ECD
DATA
Date: April 13, 2011
Page 12 of 15
Test Report
No.: CQTC1101326/CHEM
ATTACHMENTS
Dimethyl Fumarate Testing Flow Chart
1) Name of the person who made testing: Tina Zhao
2) Name of the person in charge of testing: Ryan Yang
Sample cutting / preparation
Sample Measurement
Solvent extraction
Concentration/Dilution
Filtration
GC-MS
DATA
Date: April 13, 2011
Page 13 of 15
Test Report
No.: CQTC1101326/CHEM
ATTACHMENTS
Phthalates Testing Flow Chart
1) Name of the person who made testing: Tina Zhao
2) Name of the person in charge of testing: Ryan Yang
Sample cutting / preparation
Sample Measurement
Solvent extraction
Concentration/Dilution
Filtration
GC-MS
DATA
Date: April 13, 2011
Page 14 of 15
Test Report
No.: CQTC1101326/CHEM
Date: April 13, 2011
Sample photo:
CQTC1101326/CHEM
Test part 1
Test part 2
SGS authenticate the photo on original report only
*** End of Report ***
Page 15 of 15
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