ICPTest_FLM pdf

ICP Test Report Certification Packet
Company name :
Littelfuse, Inc.
Product Series:
Midget Fuse
Product #:
FLM Series
Issue Date:
June 29, 2012
It is hereby certified by Littelfuse, Inc. that there is neither RoHS (EU Directive 2002/95/EC,
2011/65/EU)-restricted substance nor such use, for materials to be used for unit parts, for
packing/packaging materials, and for additives and the like in the manufacturing processes.
In addition, it is hereby reported to you that the parts and sub-materials, the materials to be used
for unit parts, the packing/packaging materials, and the additives and the like in the manufacturing
processes, are all composed of the following components.
Issued by:
<Global EHS Engineer>
(1) Parts, sub-materials and unit parts
This document covers the
FLM Slo Blo Military Fuse
products manufactured by Littelfuse, Inc.
< Raw Materials Used
Please see Table 1
(2) The ICP data on all measurable substances
Please see appropriate pages as identifed in Table 1
Remarks:
1
RoHS-Compliant series
Table 1: List of Raw Materials covered by this report
Total Parts
1
2
3
4
5
6
7
8
9
10
11
13
Form 585-047 Rev. A
Raw Material Part Number
Raw Material Description
082xxx
Wire-CuNi
082xxx
Wire-99% Copper
082xxx
Wire-Ag plated Copper
082xxx
Wire-2% by Weight Ag Clad Cu (082684)
923-001
Cap
079xxx
Cu 110 Strip w/ Center Sn Overlay
909-410
Midget Paper Body
927-027
Solder Pellet
692532
Solder
090169
Silica Sand
648102
Yarn
955xxx
Zinc Strip Alloy
2
Page(s)
3-12
13-22
23-32
33-37
38-42
43-46
47-53
54-58
59-63
64-70
71-79
80-84
2/21/06
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ET.SCHIJKOM
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87, D.98669 VEILSDORF,GEL\LAIY
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perlorned by ICP-AIS.
,5
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A{*AA44I{*&A:.1.
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perforf,ed by ICP-nnS.
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2
reference to IEc 62321: 2008 and
pe.forn€d by ICP-A!S.
++tgc 6232r.2oo9fit, r/)k,Y"4
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62321: ?008and perfor0€d by
BoiI inE water extraction Merhod,#
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sulfonat€s
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( P F O S - A ci d , M e r a l S a l t
/ Iilh referen.e 16 us EPA 3540C:
1 9 9 6 n e t h o d f o r P F o SC o n t e n t .
Analysis sas perforned by LCINS,
ift+d.(14)
/ PFoA(cAsNo.: 33s-6?-
4+US EPA35a0c:l996tii,
,)(t{
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1)
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1 9 9 6n e t h o d f o r P F O AC o n t e n t .
Analysis vas perforned by tClMS.
c o m o a n+vj l 1 / n r l , r r , f ' | , 1 , i : 1 f i l r ,
r.I ltri{::
ny ssbled io b GeneG cond[dns d se
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lE*r(No-) : CE/2012/108s6
ES(Dare) : 2012101/11 F&(pase)
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5
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!o.: 22537-15-1)
(;i) / Halos€.-Bronine(Br) (cAs
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ag/(t
50
/ I[ith .efe.ence io Bs EN
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1 4 5 8 |22 0 0 ? .A n a l y s i s{ a s
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50
No.: 14362-44-8)
c o m D a n; "v, r 1 r i | l , f _ a { l , r . r r , , Jnt i j l r : r ] . 2 j i
ii!.fli,
r . 1rr rrlJLl.
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TestReport
frq(No-) : cE/201?/10836 g i ! ( D a i e ) : 2 0 r 2 l o r l r l F * . ( P a r e ) ; 4 o f l o
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ELEKTROSCHUTZKO\{PONEI\'TENBAU
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fiii(Note):
1. nglkg = ppni 0.lwt% = 100oppn
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3 . M D L= M e t t r o dD € r e c t i o n L i n i r ( t t i l F x l E f B l & )
' : Nor Resulated (**ei'.ii.)
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.
.
=
5.
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on rhe
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areas
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The d€tected concentration in boiling-water-ext.action solutibn is equal or sreate. th:n 0.02 bglkg with
50 cm, tested areas. / lii)*i{,i,8=0.02
malks sith 50 cm, (tested areas)
7. *l s 0t,nl?i,t.
A+ + if ^*,i,E 6tFl:lt' *r+ f ftliEe;il*,3*
+rri.a4f&r!
+-titr 616s.
(The satuples sas/{€re anaiyzed on b e h a l f o f l h e a f p l i c a n t a s n i x i n s s a m p l €i n o n e t e s t i n g . T h € a b o v e
r e s u l i s w a s / w e r eo n l y g i v e n a s t h e i n f o r n a l i l y v a l u € . )
PrOs++itfi.(Refer."ce Inforiatior)
(Directive 2006/122lEc)
. lE+ 2006/122/FL
(1) :**r( 6irE,ai4-Ld..n,s :ar+*lrf d.Ec.Er\rl**r*a++{.i'i+o. 00s%.
(Maynot be placed on ihe oarket or used as a srbstanceor constituent of preparations in a €onc€ntratioi
€qu,l io or !igher lhan 0.005 % by nass.)
(2,t hY4q&*fr*rii+d.sd.fi"%4.*#r{+r 1kr5e+rExfirt4ApFosltti€,*+6-La&.rElt€_LitSPFlsg&
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(May.ot be placed on th€ narke! in seni finished products or a.ticles, or paris rh€reof, if the
concentration of PIOS is equal to or hiab€r than 0.1 % by nass calculated *ith r€ference to the nass of
s t r u c t u . a l l y o . n i c r o s t r u c t u r a 1 Ly d i s t i n c t p a r r s r h a t c o n t a i n P F 0 6 o r , f o ! t € x t i l e s o r o t h e . c o a t e d
naterials,
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E&(Date):20I2l0r/11
FjR(P:se):5ofro
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( c - 5 ) 1 0 1 . 0 1 3 2 -. ( c - 6 ) 1 0 1 . 0 1 3 1 . 0(c-?) 101.01?1.0
( c - 8 ) 1 0 1 . 0 1 3 s -. ( c - 9 ) r 0 1 . 0 1 5 7 .0 ( c - 1 0 ) 1 0 1 . 0 1 3 6 -. (c-11) 101-- 064. ( c - r 2 ) 1 0 1 . 0 1 6 6 -. ( c - 1 3 ) 1 0 1 . 0 1 s 8 -. ( c - 1 4 ) 1 0 1 . 0 1 6 1 -. ( c - 1 5 ) 1 0 1 . 0 1 5 5O
.
( c - 1 6 ) 1 0 1 . 0 1 2 8 0. -
cdpaiy:
copper tin alloy wire CuSn6
copper cLad{ire - Elcon 30
coppcr cLad steel wire - Elcon F
copper clad iron-nick€l-alloy si.e
Elcon D
silve. copper alloy wire
AgC!50
silver copper alLoy wi.e Agcugo
.opper vire
Cu99.9%
silver copper alloy wire Ag72Cu28
copper-zinc-alloy
wire C u 8 0Z n 2 0
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-
copper plared, brass plared sp.ing-steel wire silver copperalloy sire
A 8 c u 7 0( E l c u 7 0 )
silv€r coppe. alloy vire
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oxyaenfr€€ copper vire
OF Cu
copper-,in.-alloy
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tungsten Furiry uire
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++ lEx.62321
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reference to IEC 62321: ?008 and
perforned by tCP-r{XS,
,i.flJ'
/ Heaav,lent chroni!n c.(vI)
++ \F: 62321.2OO8li*, t)a.,fr
*+
/ with fefe.€n€e ro IEc
RliAtll.
6 2 3 2 1 . 2 i A B a n d p e r f o r m e db y
B o iI i n s s a t e r e x t . a c t i o n M € t h o d . #
}fr.+B**
sulfonates
/ Perrruo.oocrane
nglka
(PF!S-Acid. Uetal salt
t+us
EPA3540C:1996tii, 'lil
IO
iE,9*f1[-r*&}f,4
an+,t,4*69'
/ t r i t h r e f e r e n c e t o u s E P A3 5 4 0 c
1 9 9 6n € t h o d f o r P F o SC o . l e . l .
Analysis was perlorned by tClMS.
an+6.(J+) / PFoA(cAsNo.: 3356?
r)
++US EPA3540c:l996tt!,
,Xtl
&Eif 1{r*{,*fl an+d(n) }f
/ w i t h r e f e t e n c € t o U S E P A3 5 4 0 C
1 9 9 6e e t h o d f o r P F O AC o n t e n t .
Analysis was perfofned by rc/MS.
i j :i :r l , ]. r : . a i i . ; ; r t i ]
c o n o a .t y r r , : 1 r 1 , ri!' _, r r l - J n
iy $qd rob cene6cdidroc d s
onlysndwibinlh.imlsoic€nls'ns
pelsr reded rhE bd rcpod Enid be
1, . r, rjr,!*.
l0
s*
(Resql t)
No,1
rfla+E+
ft4(No.) : cE/20I2lr0835
Test Report
E J q ( D a r :e2)0 t 2 l 0 t
E * . t e , B " ,/ 3 . r
ELSCHUKOM
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CMBq
GMERBESTRASSE
87, D-98669 !'EIISDORF, GERMAIr\
d{t
E
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+4o
,{fi,t*
( U n it )
( R e s u1 t )
(IDL)
No.l
/ uonobronobiphenyt
:;Ad*
qA#tri
/ Dib.onobipltenyl
/ T r i b r o n o b ip h e n y l
/ T e t r a b r 6 n o bLo h e n v l
I*#Xi
/ P e n t a b r o n o br o h e n ! I
/ Hexabronobiphenyl
?!4$it
+iASf
/ H e p r a b . o n o bpi h e . y 1
^itrfi A / o.rabronobipheDyl
/ Nonabromobipheryt
4)qS*
/ D e c a b r o n o bpih e n y t
+;ASf
*trEc
/ suo of PBDES
t*AS.t&t"
-;ASf!{
/ M o n o b r o n o dD
i hehvl ether
=-r[#*e
:;A#+a{
/ D i b r o n o d ip h e n y l e t h e r
/ ' l r i b r o d o d i p } e n v l er h e .
B,*SiFa*
/ Tet ra6.onodi phe.vl erher
i;*Sxad
'r*S*a*
/ P e . r a b r o m o dDi h € " v l e t h e r
/ H e a a b r o n o dpih e r v t e r h e r
-k;A#Xa{
/ H e p t a b r o m o d iD h € n v l e t h e r
,\;*SXa{
/ o c r a b r o n o dD
i he.vl ether
,L;i#*e
i henvl etler
i N o n a b r o m o dD
+&#ii4
/ D € c a b r o n o d i D h e n velt h e r
623211
zoo$iiF, ,tfu|aE
+8dlf :*d,&jrl. / $ith rererence
ro IEC 62321:?008 and perforned
by rc/MS.
5
5
5
5
5
5
5
5
5
5
5
5
5
5
a* / s"l.s."
(fr.) / Halogen-Floo.ine(F) (c{s
6*
No.: 14?6?_94-8)
(5.) / Haloeen-chlo.ine (cl) (cAs
6*
! o . : 2 2 5 3 71- 5 - r )
& * ( * ) / H a l o r e n - B r o n i n e( B r ) ( c A S
l{o.: 10097-32-2)
50
ng/18
vx&+8fr
ltBs vt r4s82:2007,
50
/ sirh reference to Bs EN
{r}*t.
I 4 5 8 2 r 2 0 0 7A. n a l y si s v a s
50
(I) (cAS
6fr (dU / Halocen-lodine
No.: 14362-44-8)
conFiv;"
r 1 llu.,[r'r,
l: i/irr.r I i.tl
lt!,lr'i
oyglbredbb6ai.'alcondloisds
50
hrr.(s) rssbd rh s resr €pon ennd
lLr Lt[]!.
iq
3pdJb't}6lobc€da^dhsdocu
b
r**
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t*t**'ts
:14#*
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(Iethod)
ro
l ]tl|
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,F{a+E+
ff6(No.)
Test Report
: CE/2012l10835
aBlJzr.)
. 20L2/ot/71 Ftk(pare) : 1 of r0
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4. '- = Not R"sulated (Sli,+&.6)
5 . r ' = Q u a t i t a t i v e a n a L y s i s( N o u n i t ) _ € , B r ) * f ( * + & )
6. #:
a . P o s i t i v e b e a ! s t l e p . e s e n c eo f C r V t o n t h e r € s t e d a r e a s
(po s i t i ve *,F rq,lit E q.tF jq r{ ,r{l rS)
b . N e g a t i v e n e a n s t h e a b s e n c eo f C i V I o n r h € r e s t e d a . e a s
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T h e d e t e c t e dc o h c e n r r a t i o ni n b o i l ] n a - e a r € r - e x r r a c t i o sno l u t i o n i s € q u a l o r g r € a r e r t h a b 0 . 0 2
m A l k gw i t h
50 cn: tested ar.a". / li6;i{XA>0.02
nslka *iih 50 cm, (tested
z. tte.i,tlS{r.'Af
;F./.**isArxl:{,, *E+titi,sA,tt:ri}:+.Tftt 4 +1Erll+-ttlt aiAE.
(The sanples sas/were analyzed on behalf of the atfricant
! e s u l t s w a s / w e r eo n l y g i v e n a s r t e i n f o . n a t i t y v a l u e , )
PFos++*d,(R"f
Inf orlation)'
"'.o"€
(1) riitrrf rTfi.'|tsld.&n,r+r+4rrf,
as mixing sanpre in one resrine.
The above
!A+ 2oo6trzztEa (Di rect iae 2006/t2ztw)
d.Ee,Ed,rlE*tla+,i6d.n,+0.
005%.
(May not be placed on the market o. used as a sDbstance o. consrituent
€qual io or nigh€r than 0.005 % by nass.)
of prepararrons
(2rtit{ttX4n&*fi&}.ei+d."%d.6s{.*{r1+;1!i*€1+}aX*Jt+ApFosi.4t?J*fi}.e.t&r€t6€};l4pFosEE
,i.&+,i!d.i,ifo.r%,6*r&€d.4{tti.4rf. {,RprrsaAt*f + 6E*;Ad.Ji;Aruc/.,.
(Maynot be placed on ihe na.k€t in seni-linisned prodocts or articles, or pa.ts rhereof, if
ure
c o n c e n t . a t i o n o f P F O Si s e q u a t r o o r h i g h e . t h a n 0 . 1 % b y n a s s c a l c ! l a t e d s i t h r e f e r e n c e t o t l e n a s s o f
s t . u c t u r a l i y o . f r i c . o s t r u c r u r a l l y d i s r i n . r p a r r s t ! a i c o n t a i n P F o . so r , f o . r e x r i t e s o r o t h e . c o a r e d
naterials,
if thc anoun! of PFOSis equal to o. hiahcr than Ug/nr of thc coated nateriat.)
c o m p a ityr : ; r , r ; : i r l , , ; - f i t . r l J r . n i r r , . r , , t i i
Ltlttr
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-:.r ;::rlnti,,;i+46iDr,ssr7
l
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TestReport
ft,q(No.) : cE/20r2lr0835
E S ( D a t e ) : 2 0 1 2 1 0 1 / 1 1F * . ( p a s € ) : 5 o r l 0
EI-SCHIXOi,I
ELEKTRO€CHUIZKNTPONENTENMU
CVBH
GEIIERBESTInSSE
87, D 98669 IEIT,SDORF.GERILUY
tl&4!t(styl./I
[t[t
t.' N".)
(B-1) 101. 014
-silver
plated coFpe.{tre-Cu. Ag - - %
(B-2) 101. 0131. - - - - -pure silve. sire-Ag l()()()
( B - 3 ) 1 0 1 . 0 1 2 3 . 0- - - - s i l v e r
platcd purest nickct vire-Ni99.98%. AgI%
-silve.-copper alloy plated cotpe. clad vire-Elcon D,
(B-4) 10r,0182.0 - -silver
(B 5) 101.0120.0
p l a t e d c o n s t a n t a nw i i € - C u N i 4 4 , A A S %
( B - 6 ) 1 0 1 . 0 1 5 1 . 0- - - - c o p p e r - n i c k e t 4 4 a l l o y s v e r p l a r e d s i . e - c u N i 4 4 ,
c o D o a n tv l r I t ! . , r - N ' | , r " l : l , i l l l i
:. ! 1 1:;!1,1\
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ont 3nd*ii'n rh. hrs or c €nr s 'ns
ri.:l,;l-":Iq:j1
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Test Report
f i { 5 ( N o . ) : C E l 2 0 1 2 l l o s 3 s E S ( D a r e ): 2 o t z l 0 r / t t F # ( p a s € ) :
ELSCHUI{OM
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8?, D 98669 WILSDoII, CERMA\Y
6
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2) r.lri^l:
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3) ir'13{I i ^ : tl4* / Nameof the pe6on in chargeormeasu€m€nlrTroychans
tr*. {rtt*s
/curing. p€galaton
iqr{.&,cf ! / sdde MeasuEmenl
&lf;F n l*'.g6tt{ f, 6 }xn!trai&it,tirt /LoeTt
4rt/!inlt n.i'la{&,aib /
4,;) /Acid dig€slion by suitabte acid dependedon
dtrerenlsahdemaledat{asbetowiable)
MiorcMve digestion with HNO3/HC|/HF
,"rl4rOf jit& jt.li,lilt +
C( / H€i to appropriate
1)
2)
f [*a{*4+*it{rtc
/ AlkaliF6ion
/HCltod$d€
/ rcP,aEs
f!911L / samdeMatedal
51eel,@pper,allnirum, solder
&ltgti
ta{*tt
;filt&AJlfi / DiqesL|onAcd
-t+, 4la{,!lt, nn*, el,,k /
Aa@ reoia. HNO' HCl. HF. H,O,
rra{,Inc / HNoJftF
A, J6,€, nit /
Gold,olalinum,
Dalladium,
ceramic
,i(f rf 7h-ir,g t.rLrlf,.' I
irl#B*i{Aftrcnm 6id
rti!€ /HNOr
&E / Plaslic
4?,*i&8tt$ / coot,
fherdigestate
lhrough
liher
*d, t{"*,
s!t, td / H,so. Ho,. HNorhcl
,! \'efi*1eti*l+
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j i i r i r +
r i l , i ,
! . r 1 r . t p . l i , . 1 , i f i ' ! ! l .
rhcdddneiiAs€dbysgcompa^ys!b4d{ob6ai..a|condloi3ds
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t]n]l
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Test Report
iEIS(No.) : cE/2012l10835
E rr?(Dare) : 2012l01/11 F&(P,s")
ELSCHUKOMELEI$ROSCHUTZKOIIPONENTENB,qU
GMBH
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a }l{,/\l
I a_i9*, / Nameoftheperson
whomademeasuremenl:
RomanWonq
r,$Ji( frt ^ : &+le / Nam€of thepersonIn chargeof measurement
TrcyCha;g
n^ ld,ElF / Firstlestry proce.s------------f
....,---.
prccess
€*,E&*€F / OptionalscE€n
-. -,t
*{.€,S / Confimation
orccess
:l
Scre€n
analysis
/ ,, rfi+rt
I
I
sample
erlraclion
*s+*/
Soxhlet
melhod6i,+tx;*
Concentrale/Dilute
Enractedsoluiion
+tri{ rira/ifi#
Filter/ +S.i{'E.d
Analysis
byGC/MS
/ fr"ian&f ie*,+&
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c o m D a n +! " , I
rirr,,: i;
r. lJ: ?.lria 1.:-!i
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Test Report
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F&{prse)
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RitaChen
jrl:i,A ll, : #,*e / Nameof thepersonin cbargeof measurement:
TroyChang
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it
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it4(No. ) : cE/2012l10835 AS(Dare) : 201210r/tr
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r
r
i A/-F : ij!9*y / Nameofthe personwhomademeesuementRcmanWong
t4j:{, q i,\ : tF'.*4 / Nameof the personin chargeof measurement:
TroyChang
( rd8,{ a : Afi.+n*.n/Afi.+rt(*)
, **.:4i{bA4,
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Es(Date) : 2tr2/ar/r1
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trlt[tl
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ir's
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10835
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Test Report
Applicant:
Number : TWNC00249178
Littelfuse Philippines Inc.
LIMA Technology Center, Lipa City,
Malvar, Batangas
Date
: Mar 26, 2012
Sample Description:
One (1) group of submitted samples said to be :
Part Description
: Silver Clad Cu Wire with 2% Ag
Part Number
: 082xxx(082684)
Date Sample Received
: Mar 22, 2012
Date Test Started
: Mar 22, 2012
Test Conducted :
As requested by the applicant, for details please refer to attached pages.
Authorized By:
On Behalf Of Intertek Testing Services
Taiwan Limited
K. Y. Liang
Director
This report shall not be reproduced
except in full, without the written
approval of the laboratory.
Page 1 of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Number : TWNC00249178
Test Conducted
(Ⅰ) Test Result Summary :
Test Item
Heavy Metal
Cadmium (Cd) content
Lead (Pb) content
Mercury (Hg) content
Chromium VI (Cr6+) content (mg/kg with 50cm2)
Remarks: ppm =
ND =
<
=
mg/kg
Result (ppm)
Silvery Wire
ND
ND
ND
Negative (< 0.02)
Parts per million based on weight of tested sample = mg/kg
Not detected
Less than
with 50cm2 = milligram per kilogram with 50 square centimetre
Responsibility of Chemist : Irene Chiou / Kevin Liu / Cathy Chen
Date Sample Received
Test Period
: Mar 22, 2012
: Mar 22, 2012 To Mar 26, 2012
(Ⅱ) RoHS Requirement:
Restricted Substances
Cadmium (Cd) Content
Lead (Pb) Content
Mercury (Hg) Content
Chromium VI (Cr6+) Content
Limits
0.01% (100ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for
homogeneous material.
Page 2 of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Number : TWNC00249178
Test Conducted
(Ⅲ) Test Method:
Test Item
Cadmium (Cd)
content
Lead (Pb) content
Mercury (Hg)
content
Chromium VI (Cr6+)
content
Test Method
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 7, by microwave
digestion until the tested samples are
totally dissolved and determined by
ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in annex B, by boiling water
extraction and determined by UV-Vis
Spectrophotometer.
Reporting Limit
2 ppm
2 ppm
2 ppm
0.02
mg/kg with 50cm2
Remark: Reporting limit = Quantitation limit of analyte in sample
Page 3 of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Number : TWNC00249178
Test Conducted
(Ⅳ) Measurement Flowchart:
Test For Cd/Pb/Hg/Chromium (VI)
Reference Standard:IEC 62321 edition 1.0:2008
Sampling/grinding or cutting
Cd/Pb/Hg
Cr
Polymers /
Electronics
Metal
For different
material, digest
the sample with
*1
appropriate acid
By spot test
Negative
Confirm the tested
samples are
totally dissolved
Make up with
deionized water
6+
*2
Weigh sample
and add
alkaline
solution
Get 50cm2 sample
Definite temp.
extraction
Boiling water
extraction
Cool and filter
the extract
Analyzed by ICP-OES
Make up with deionized
water and add diphenylcarbazide solution
Remarks:
*1: List Of Appropriate Acid:
Material
Polymers
Metals
Electronics
Analyzed by UV-VIS
Acid Added For Digestion
HNO3,HCl,HF,H2O2,H3BO3
HNO3,HCl,HF
HNO3,HCl,H2O2,HBF4
*2: If the result of spot test is positive, Chromium VI would be determined as detected.
End of Report
Page 4 of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Number : TWNC00249178
Test Conducted
Photo
Page 5 of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Test Report
Applicant:
Number : TWNC00213348
Littelfuse, S.A. de C.V.
Blvd. Fausto Z. Martinez #1800
Col. Magisterio Seccion 38 C.P.
26070 Piedra Negras, Coahuila,
Mexico
Date
: Jul 01, 2011
Sample Description:
One (1) group of submitted samples said to be :
Part Description
: FUSE CAP-Plated
Part Number
: 923-001
Date Sample Received
: Jun 28, 2011
Date Test Started
: Jun 28, 2011
Test Conducted :
As requested by the applicant, for details please refer to attached pages.
Authorized By:
On Behalf Of Intertek Testing Services
Taiwan Limited
K. Y. Liang
Director
This report shall not be reproduced
except in full, without the written
approval of the laboratory.
Page 1 Of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Number : TWNC00213348
Test Conducted
(Ⅰ) Test Result Summary :
Result (ppm)
(1)
(2)
Test Item
Heavy Metal
Cadmium (Cd) content
Lead (Pb) content
Mercury (Hg) content
Chromium VI (Cr6+) content (mg/kg with 50cm2)
ND
ND
ND
Negative (<
0.02)(#)
ND
ND
ND
Negative (<
0.02)(#)
Remarks: ppm = Parts per million based on weight of tested sample = mg/kg
ND = Not detected
<
= Less than
mg/kg with 50cm2 = milligram per kilogram with 50 square centimetre
Negative = A negative test result indicated positive observation
was not found at the time of Test.
#
= Due to the insufficient sample area, reduced total sample
surface of 10 cm2 was used and the dilution factor was
adjusted accordingly.
Tested Components
(1) Silvery Plating Layer
(2) Silvery Metal Base Material
Responsibility Of Chemist : Irene Chiou / Kevin Liu / Cathy Chen
Date Sample Received
Test Period
: Jun 28, 2011
: Jun 28, 2011 To Jul 01, 2011
(Ⅱ) RoHS Requirement:
Restricted Substances
Cadmium (Cd) Content
Lead (Pb) Content
Mercury (Hg) Content
Chromium VI (Cr6+) Content
Limits
0.01% (100ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for
homogeneous material.
Page 2 Of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Number : TWNC00213348
Test Conducted
(Ⅲ) Test Method:
Test Item
Cadmium (Cd)
content
Lead (Pb) content
Mercury (Hg)
content
Chromium VI (Cr6+)
content
Test Method
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 7, by microwave
digestion until the tested samples are
totally dissolved and determined by
ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in annex B, by boiling water
extraction and determined by UV-Vis
spectrophotometer.
Reporting Limit
2 ppm
2 ppm
2 ppm
0.02
mg/kg with 50cm2
Remark: Reporting limit = Quantitation limit of analyte in sample
Page 3 Of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Number : TWNC00213348
Test Conducted
(Ⅳ) Measurement Flowchart:
Test For Cd/Pb/Hg/Chromium (VI)
Reference Standard:IEC 62321 edition 1.0:2008
Sample preparation
Take sample and immerse into Aqua Regia, start to strip plating layer
Stop the stripping procedure upon color change completely
Take the Aqua solution as plating component and stripped body as substrate component
Cd/Pb/Hg
Cr
Polymers /
electronics
Metal
For different
material, digest
the sample with
*1
appropriate acid
By spot test
Negative
Confirm the tested
samples are
totally dissolved
Make up with
deionized water
6+
*2
Weigh sample
and add
alkaline
solution
Get 50cm2 sample
Definite temp.
extraction
By boiling water
extraction
Cool and filter
the extract
Analyzed by ICP-OES
Make up with deionized water and add
diphenyl-carbazide solution
Remarks:
*1: List Of Appropriate Acid:
Material
Polymers
Metals
Electronics
Analyzed by UV-VIS
Acid Added For Digestion
HNO3,HCl,HF,H2O2,H3BO3
HNO3,HCl,HF
HNO3,HCl,H2O2,HBF4
*2: If the result of spot test is positive, Chromium VI would be determined as detected.
End Of Report
Page 4 Of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Number : TWNC00213348
Test Conducted
Photo
Page 5 Of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
PENY
PonyTcstingInaernalional
Group
T€atReport
NO.: W020320112MD
Ddet 2012.02.07
Page1 of4
Applicant:
Address:
SUZHOUXINWUOPTRONICTTECHNOLOGY
CO,.LTD
368 YOUYIRD,YOUYIDEVELOPMENT
AREA,SONGLING
TOWNWUJIANG
SUZHOU,CHINA
Thefollowingsample(s)
waslderesubmittedandidentified
on behalfof the clientas:
SampleName:
BRASS
i/lanufacfurer,
SUZHOU
XINWUOPTRONICTTECHNOLOGY
CO.,LTD
SampleDescription, SOLDER
COATING
ONCu
Testing
PadDescription:l\4lxTESTED
SampleReceived
Date: 2012.O2.03
TestPeriod:
2012.02.03 Io 2012.02.07
TestRequested
.
ln accordance
withthe RoHSDirective2011/65/EU
AnnexII
TestMethod:
Withreference
to 1EC62321
Edition1.0:2008method: RegulatedSubstances
Contentof testprooesswithElectrical
& Electronic
Products
(1) LeadAnalysis
performed
is
byMS
(2) CadmiumAnalysisis performed
byAAS
(3) MercuryAnalysis
is performed
by ICP-OES
(4) Hexavalent
Chromium
Analysisis performedBy Spot-test/Boiling-waterextractionMethod
(5) PBBSand PBDESAnalysis
is performedby GC-|\4S
TestResult:
Pleasereferto nextpage(s)
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Personin chargeofthe lab: Zhangdaiqin
TheseSamplesWere DissolvedToblly By Pre-conditioning
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And PBBS,/PBDES
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Test Report
Applicant:
Number : TWNC00213350
Littelfuse, S.A. de C.V.
Blvd. Fausto Z. Martinez #1800
Col. Magisterio Seccion 38 C.P.
26070 Piedra Negras, Coahuila,
Mexico
Date
: Jun 30, 2011
Sample Description:
One (1) group of submitted samples said to be :
Part Description
: MIDGET PAPER BODY
Part Number
: 909-410
Date Sample Received
: Jun 28, 2011
Date Test Started
: Jun 28, 2011
Test Conducted :
As requested by the applicant, for details please refer to attached pages.
Authorized By:
On Behalf Of Intertek Testing Services
Taiwan Limited
K. Y. Liang
Director
This report shall not be reproduced
except in full, without the written
approval of the laboratory.
Page 1 Of 7
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Number : TWNC00213350
Test Conducted
(Ⅰ) Test Result Summary :
Test Item
Result (ppm)
Black Material
Heavy Metal
Cadmium (Cd) content
Lead (Pb) content
Mercury (Hg) content
Chromium VI (Cr6+) content
Polybrominated Biphenyls (PBBs)
Monobrominated Biphenyls (MonoBB)
Dibrominated Biphenyls (DiBB)
Tribrominated Biphenyls (TriBB)
Tetrabrominated Biphenyls (TetraBB)
Pentabrominated Biphenyls (PentaBB)
Hexabrominated Biphenyls (HexaBB)
Heptabrominated Biphenyls (HeptaBB)
Octabrominated Biphenyls (OctaBB)
Nonabrominated Biphenyls (NonaBB)
Decabrominated Biphenyl (DecaBB)
Polybrominated Diphenyl Ethers (PBDEs)
Monobrominated Diphenyl Ethers (MonoBDE)
Dibrominated Diphenyl Ethers (DiBDE)
Tribrominated Diphenyl Ethers (TriBDE)
Tetrabrominated Diphenyl Ethers (TetraBDE)
Pentabrominated Diphenyl Ethers (PentaBDE)
Hexabrominated Diphenyl Ethers (HexaBDE)
Heptabrominated Diphenyl Ethers (HeptaBDE)
Octabrominated Diphenyl Ethers (OctaBDE)
Nonabrominated Diphenyl Ethers (NonaBDE)
Decabrominated Diphenyl Ether (DecaBDE)
Halogen Content
Fluorine (F)
Chlorine (Cl)
Bromine (Br)
Iodine (I)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Remarks: ppm = Parts per million based on weight of tested sample = mg/kg
ND = Not detected
Responsibility Of Chemist : Irene Chiou / Kevin Liu / Cathy Chen
Date Sample Received
Test Period
: Jun 28, 2011
: Jun 28, 2011 to Jun 30, 2011
Page 2 Of 7
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Number : TWNC00213350
Test Conducted
(Ⅱ) RoHS Requirement:
Restricted Substances
Cadmium (Cd) Content
Lead (Pb) Content
Mercury (Hg) Content
Chromium VI (Cr6+) Content
Polybrominated Biphenyls (PBBs)
Polybrominated Diphenyl Ehters (PBDEs)
Limits
0.01% (100ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for
homogeneous material.
(Ⅲ) Test Method:
Test Item
Cadmium (Cd)
content
Lead (Pb) content
Mercury (Hg)
content
Chromium VI (Cr6+)
content
Test Method
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 7, by microwave
digestion until the tested samples are
totally dissolved and determined by
ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in annex C, by alkaline
digestion and determined by UV-Vis
spectrophotometer.
Reporting Limit
2 ppm
2 ppm
2 ppm
1 ppm
Page 3 Of 7
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Number : TWNC00213350
Test Conducted
(Ⅲ) Test Method:
Test Item
Polybrominated
Biphenyls (PBBs)
Polybrominated
Diphenyl Ethers
(PBDEs)
Halogen Content
Test Method
With reference to IEC 62321 edition
1.0:2008 in annex A, by solvent
extraction and determined by GC-MSD
and further HPLC confirmation when
necessary.
With reference to IEC 62321 edition
1.0:2008 in annex A, by solvent
extraction and determined by GC-MSD
and further HPLC confirmation when
necessary.
With reference to EN 14582:2007 by
calorimetric bomb with oxygen and
determined by ion chromatography
Reporting Limit
5 ppm
5 ppm
50 ppm
Remark: Reporting limit = Quantitation limit of analyte in sample
Page 4 Of 7
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Number : TWNC00213350
Test Conducted
(Ⅳ) Measurement Flowchart:
Test For Cd/Pb/Hg/Chromium (VI)/PBBS/PBDES Contents
Reference Standard: IEC 62321 edition 1.0:2008
Sample preparation
For non-metal part
For metal part
Take sample and immerse into Aqua Regia, start to strip plating layer
Stop the stripping procedure upon color change completely
Take the Aqua solution as plating component and stripped body as substrate component
Cd/Pb/Hg
Cr
Weigh sample and
add organic solvent
By spot test
Negative
Confirm the tested
samples are
totally dissolved
Make up with
deionized water
PBBs/PBDEs
Polymers /
electronics
Metal
For different
material, digest
the sample with
*1
appropriate acid
6+
Get 50cm2 sample
By boiling water
extraction
*2
Weigh sample
and add
alkaline
solution
By Soxhlet
extraction or
Solvent extraction
Definite temp.
extraction
Cool and filter
the extract
Analyzed by ICP-OES
Concentrate the
extract and make up
with organic
solvent
Analyzed by GC-MSD
Make up with deionized
water and add diphenylcarbazide solution
Remarks:
*1: List Of Appropriate Acid:
Material
Polymers
Metals
Electronics
Analyzed by UV-VIS
Acid Added For Digestion
HNO3,HCl,HF,H2O2,H3BO3
HNO3,HCl,HF
HNO3,HCl,H2O2,HBF4
*2: If the result of spot test is positive, Chromium VI would be determined as detected.
Page 5 Of 7
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Number : TWNC00213350
Test Conducted
(Ⅳ) Measurement Flowchart:
Test For Halogen Content
Reference Standard:EN 14582
Sampling/grinding or
cutting
Add absorbent in a
combustion flask &
place weighed sample in
equipment
Fill oxygen into
calorimetric bomb
Ignite then leave the
flask at room
temperature
Transfer the absorbent
into a volumetric flask
Make up with deionized
water
Analyzed by ion
chromatography
End Of Report
Page 6 Of 7
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Number : TWNC00213350
Test Conducted
Photo
Page 7 Of 7
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Test Report
Applicant:
Number : TWNC00213353
Littelfuse, S.A. de C.V.
Blvd. Fausto Z. Martinez #1800
Col. Magisterio Seccion 38 C.P.
26070 Piedra Negras, Coahuila,
Mexico
Date
: Jul 01, 2011
Sample Description:
One (1) group of submitted samples said to be :
Part Description
: SOLDER PELLET
Part Number
: 927-027
Date Sample Received
: Jun 28, 2011
Date Test Started
: Jun 28, 2011
Test Conducted :
As requested by the applicant, for details please refer to attached pages.
Authorized By:
On Behalf Of Intertek Testing Services
Taiwan Limited
K. Y. Liang
Director
This report shall not be reproduced
except in full, without the written
approval of the laboratory.
Page 1 Of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Number : TWNC00213353
Test Conducted
(Ⅰ) Test Result Summary :
Result (ppm)
Silvery Metal
Test Item
Heavy Metal
Cadmium (Cd) content
Lead (Pb) content
Mercury (Hg) content
Chromium VI (Cr6+) content (mg/kg with 50cm2)
ND
335
ND
Negative (< 0.02)
Remarks: ppm = Parts per million based on weight of tested sample = mg/kg
ND = Not detected
<
= Less than
mg/kg with 50cm2 = milligram per kilogram with 50 square centimetre
Negative = A negative test result indicated positive observation
was not found at the time of Test.
Responsibility Of Chemist : Irene Chiou / Kevin Liu / Cathy Chen
Date Sample Received
Test Period
: Jun 28, 2011
: Jun 28, 2011 To Jul 01, 2011
(Ⅱ) RoHS Requirement:
Restricted Substances
Cadmium (Cd) Content
Lead (Pb) Content
Mercury (Hg) Content
Chromium VI (Cr6+) Content
Limits
0.01% (100ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for
homogeneous material.
Page 2 Of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Number : TWNC00213353
Test Conducted
(Ⅲ) Test Method:
Test Item
Cadmium (Cd)
content
Lead (Pb) content
Mercury (Hg)
content
Chromium VI (Cr6+)
content
Test Method
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 7, by microwave
digestion until the tested samples are
totally dissolved and determined by
ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in annex B, by boiling water
extraction and determined by UV-Vis
spectrophotometer.
Reporting Limit
2 ppm
2 ppm
2 ppm
0.02
mg/kg with 50cm2
Remark: Reporting limit = Quantitation limit of analyte in sample
Page 3 Of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Number : TWNC00213353
Test Conducted
(Ⅳ) Measurement Flowchart:
Test For Cd/Pb/Hg/Chromium (VI)
Reference Standard:IEC 62321 edition 1.0:2008
Sample preparation
Take sample and immerse into Aqua Regia, start to strip plating layer
Stop the stripping procedure upon color change completely
Take the Aqua solution as plating component and stripped body as substrate component
Cd/Pb/Hg
Cr
Polymers /
electronics
Metal
For different
material, digest
the sample with
*1
appropriate acid
By spot test
Negative
Confirm the tested
samples are
totally dissolved
Make up with
deionized water
6+
*2
Weigh sample
and add
alkaline
solution
Get 50cm2 sample
Definite temp.
extraction
By boiling water
extraction
Cool and filter
the extract
Analyzed by ICP-OES
Make up with deionized water and add
diphenyl-carbazide solution
Remarks:
*1: List Of Appropriate Acid:
Material
Polymers
Metals
Electronics
Analyzed by UV-VIS
Acid Added For Digestion
HNO3,HCl,HF,H2O2,H3BO3
HNO3,HCl,HF
HNO3,HCl,H2O2,HBF4
*2: If the result of spot test is positive, Chromium VI would be determined as detected
End Of Report
Page 4 Of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Number : TWNC00213353
Test Conducted
Photo
Page 5 Of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Test Report
Applicant:
Number : TWNC00213351
Littelfuse, S.A. de C.V.
Blvd. Fausto Z. Martinez #1800
Col. Magisterio Seccion 38 C.P.
26070 Piedra Negras, Coahuila,
Mexico
Date
: Jul 01, 2011
Sample Description:
One (1) group of submitted samples said to be :
Part Description
: WIRE SOLDER .100 DIA - ROHS
Part Number
: 692532
Date Sample Received
: Jun 28, 2011
Date Test Started
: Jun 28, 2011
Test Conducted :
As requested by the applicant, for details please refer to attached pages.
Authorized By:
On Behalf Of Intertek Testing Services
Taiwan Limited
K. Y. Liang
Director
This report shall not be reproduced
except in full, without the written
approval of the laboratory.
Page 1 Of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Number : TWNC00213351
Test Conducted
(Ⅰ) Test Result Summary :
Result (ppm)
Silvery Metal
Test Item
Heavy Metal
Cadmium (Cd) content
Lead (Pb) content
Mercury (Hg) content
Chromium VI (Cr6+) content (mg/kg with 50cm2)
ND
221
ND
Negative (< 0.02)
Remarks: ppm = Parts per million based on weight of tested sample = mg/kg
ND = Not detected
<
= Less than
mg/kg with 50cm2 = milligram per kilogram with 50 square centimetre
Negative = A negative test result indicated positive observation
was not found at the time of Test.
Responsibility Of Chemist : Irene Chiou / Kevin Liu / Cathy Chen
Date Sample Received
Test Period
: Jun 28, 2011
: Jun 28, 2011 To Jul 01, 2011
(Ⅱ) RoHS Requirement:
Restricted Substances
Cadmium (Cd) Content
Lead (Pb) Content
Mercury (Hg) Content
Chromium VI (Cr6+) Content
Limits
0.01% (100ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for
homogeneous material.
Page 2 Of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Number : TWNC00213351
Test Conducted
(Ⅲ) Test Method:
Test Item
Cadmium (Cd)
content
Lead (Pb) content
Mercury (Hg)
content
Chromium VI (Cr6+)
content
Test Method
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 7, by microwave
digestion until the tested samples are
totally dissolved and determined by
ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in annex B, by boiling water
extraction and determined by UV-Vis
spectrophotometer.
Reporting Limit
2 ppm
2 ppm
2 ppm
0.02
mg/kg with 50cm2
Remark: Reporting limit = Quantitation limit of analyte in sample
Page 3 Of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Number : TWNC00213351
Test Conducted
(Ⅳ) Measurement Flowchart:
Test For Cd/Pb/Hg/Chromium (VI)
Reference Standard:IEC 62321 edition 1.0:2008
Sample preparation
Take sample and immerse into Aqua Regia, start to strip plating layer
Stop the stripping procedure upon color change completely
Take the Aqua solution as plating component and stripped body as substrate component
Cd/Pb/Hg
Cr
Polymers /
electronics
Metal
For different
material, digest
the sample with
*1
appropriate acid
By spot test
Negative
Confirm the tested
samples are
totally dissolved
Make up with
deionized water
6+
*2
Weigh sample
and add
alkaline
solution
Get 50cm2 sample
Definite temp.
extraction
By boiling water
extraction
Cool and filter
the extract
Analyzed by ICP-OES
Make up with deionized water and add
diphenyl-carbazide solution
Remarks:
*1: List Of Appropriate Acid:
Material
Polymers
Metals
Electronics
Analyzed by UV-VIS
Acid Added For Digestion
HNO3,HCl,HF,H2O2,H3BO3
HNO3,HCl,HF
HNO3,HCl,H2O2,HBF4
*2: If the result of spot test is positive, Chromium VI would be determined as detected.
End Of Report
Page 4 Of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Number : TWNC00213351
Test Conducted
Photo
Page 5 Of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Test Report
Applicant:
Number : TWNC00213352
Littelfuse, S.A. de C.V.
Blvd. Fausto Z. Martinez #1800
Col. Magisterio Seccion 38 C.P.
26070 Piedra Negras, Coahuila,
Mexico
Date
: Jun 30, 2011
Sample Description:
One (1) group of submitted samples said to be :
Part Description
: SILICA SAND #2
Part Number
: 090169
Date Sample Received
: Jun 28, 2011
Date Test Started
: Jun 28, 2011
Test Conducted :
As requested by the applicant, for details please refer to attached pages.
Authorized By:
On Behalf Of Intertek Testing Services
Taiwan Limited
K. Y. Liang
Director
This report shall not be reproduced
except in full, without the written
approval of the laboratory.
Page 1 Of 7
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Number : TWNC00213352
Test Conducted
(Ⅰ) Test Result Summary :
Test Item
Result (ppm)
Beige Powder
Heavy Metal
Cadmium (Cd) content
Lead (Pb) content
Mercury (Hg) content
Chromium VI (Cr6+) content
Polybrominated Biphenyls (PBBs)
Monobrominated Biphenyls (MonoBB)
Dibrominated Biphenyls (DiBB)
Tribrominated Biphenyls (TriBB)
Tetrabrominated Biphenyls (TetraBB)
Pentabrominated Biphenyls (PentaBB)
Hexabrominated Biphenyls (HexaBB)
Heptabrominated Biphenyls (HeptaBB)
Octabrominated Biphenyls (OctaBB)
Nonabrominated Biphenyls (NonaBB)
Decabrominated Biphenyl (DecaBB)
Polybrominated Diphenyl Ethers (PBDEs)
Monobrominated Diphenyl Ethers (MonoBDE)
Dibrominated Diphenyl Ethers (DiBDE)
Tribrominated Diphenyl Ethers (TriBDE)
Tetrabrominated Diphenyl Ethers (TetraBDE)
Pentabrominated Diphenyl Ethers (PentaBDE)
Hexabrominated Diphenyl Ethers (HexaBDE)
Heptabrominated Diphenyl Ethers (HeptaBDE)
Octabrominated Diphenyl Ethers (OctaBDE)
Nonabrominated Diphenyl Ethers (NonaBDE)
Decabrominated Diphenyl Ether (DecaBDE)
Halogen Content
Fluorine (F)
Chlorine (Cl)
Bromine (Br)
Iodine (I)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Remarks: ppm = Parts per million based on weight of tested sample = mg/kg
ND = Not detected
Responsibility Of Chemist : Irene Chiou / Kevin Liu / Cathy Chen
Date Sample Received
Test Period
: Jun 28, 2011
: Jun 28, 2011 to Jun 30, 2011
Page 2 Of 7
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Number : TWNC00213352
Test Conducted
(Ⅱ) RoHS Requirement:
Restricted Substances
Cadmium (Cd) Content
Lead (Pb) Content
Mercury (Hg) Content
Chromium VI (Cr6+) Content
Polybrominated Biphenyls (PBBs)
Polybrominated Diphenyl Ehters (PBDEs)
Limits
0.01% (100ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for
homogeneous material.
(Ⅲ) Test Method:
Test Item
Cadmium (Cd)
content
Lead (Pb) content
Mercury (Hg)
content
Chromium VI (Cr6+)
content
Test Method
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 7, by microwave
digestion until the tested samples are
totally dissolved and determined by
ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in annex C, by alkaline
digestion and determined by UV-Vis
spectrophotometer.
Reporting Limit
2 ppm
2 ppm
2 ppm
1 ppm
Page 3 Of 7
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Number : TWNC00213352
Test Conducted
(Ⅲ) Test Method:
Test Item
Polybrominated
Biphenyls (PBBs)
Polybrominated
Diphenyl Ethers
(PBDEs)
Halogen Content
Test Method
With reference to IEC 62321 edition
1.0:2008 in annex A, by solvent
extraction and determined by GC-MSD
and further HPLC confirmation when
necessary.
With reference to IEC 62321 edition
1.0:2008 in annex A, by solvent
extraction and determined by GC-MSD
and further HPLC confirmation when
necessary.
With reference to EN 14582:2007 by
calorimetric bomb with oxygen and
determined by ion chromatography
Reporting Limit
5 ppm
5 ppm
50 ppm
Remark: Reporting limit = Quantitation limit of analyte in sample
Page 4 Of 7
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Number : TWNC00213352
Test Conducted
(Ⅳ) Measurement Flowchart:
Test For Cd/Pb/Hg/Chromium (VI)/PBBS/PBDES Contents
Reference Standard: IEC 62321 edition 1.0:2008
Sample preparation
For non-metal part
For metal part
Take sample and immerse into Aqua Regia, start to strip plating layer
Stop the stripping procedure upon color change completely
Take the Aqua solution as plating component and stripped body as substrate component
Cd/Pb/Hg
Cr
Weigh sample and
add organic solvent
By spot test
Negative
Confirm the tested
samples are
totally dissolved
Make up with
deionized water
PBBs/PBDEs
Polymers /
electronics
Metal
For different
material, digest
the sample with
*1
appropriate acid
6+
Get 50cm2 sample
By boiling water
extraction
*2
Weigh sample
and add
alkaline
solution
By Soxhlet
extraction or
Solvent extraction
Definite temp.
extraction
Cool and filter
the extract
Analyzed by ICP-OES
Concentrate the
extract and make up
with organic
solvent
Analyzed by GC-MSD
Make up with deionized
water and add diphenylcarbazide solution
Remarks:
*1: List Of Appropriate Acid:
Material
Polymers
Metals
Electronics
Analyzed by UV-VIS
Acid Added For Digestion
HNO3,HCl,HF,H2O2,H3BO3
HNO3,HCl,HF
HNO3,HCl,H2O2,HBF4
*2: If the result of spot test is positive, Chromium VI would be determined as detected.
Page 5 Of 7
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Number : TWNC00213352
Test Conducted
(Ⅳ) Measurement Flowchart:
Test For Halogen Content
Reference Standard:EN 14582
Sampling/grinding or
cutting
Add absorbent in a
combustion flask &
place weighed sample in
equipment
Fill oxygen into
calorimetric bomb
Ignite then leave the
flask at room
temperature
Transfer the absorbent
into a volumetric flask
Make up with deionized
water
Analyzed by ion
chromatography
End Of Report
Page 6 Of 7
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Number : TWNC00213352
Test Conducted
Photo
Page 7 Of 7
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Intertek Testing Services Ltd., Shanghai
TFH Division
Block B, Jinling Business Square,No.801 Yi Shan Road,
Shanghai, China, 200233
Tel: +86 21 6120 6565
Fax: +86 21 6127 9740
www.intertek.com
www.intertek.com.cn
China Toll-Free: 800 999 1338
TEST REPORT
APPLICANT: LITTELFUSE,INC.
800 E. NORTHWEST HWY
ATTN: A. CESISTA/ K. BACILA
NUMBER: SHAH00276230
DATE: AUG 24, 2011
SAMPLE DESCRIPTION:
One(1) submitted sample said to be :White yarn.
Part Description
: Yarn.
Part Number
: 648102.
Date Sample Received
: Aug.18, 2011.
Date Test Started
: Aug.18, 2011.
***********************************************************************
TESTS CONDUCTED:
AS REQUESTED BY THE APPLICANT, FOR DETAILS REFER TO ATTACHED PAGE(S)
***********************************************************************
TO BE CONTINUED
PREPARED AND CHECKED BY:
FOR INTERTEK TESTING SERVICES
LTD., SHANGHAI
AUTHORIZED BY:
FOR INTERTEK TESTING SERVICES
LTD., SHANGHAI
MYRA LV
CHEMICAL LAB SENIOR MANAGER
STEPHEN TSANG
GENERAL MANAGER
PAGE 1 OF 9
Intertek Testing Services Ltd., Shanghai
TFH Division
Block B, Jinling Business Square,No.801 Yi Shan Road,
Shanghai, China, 200233
Tel: +86 21 6120 6565
Fax: +86 21 6127 9740
www.intertek.com
www.intertek.com.cn
China Toll-Free: 800 999 1338
TEST REPORT
NUMBER: SHAH00276230
TESTS CONDUCTED
1
(I) Test Result Summary :
Testing Item
Halogen Content
Fluorine (F)
Chlorine (Cl)
Bromine (Br)
Iodine (I)
Result (ppm)
ND
ND
ND
ND
Remarks: ppm = Parts per million = mg/kg
ND = Not detected
Responsibility Of Chemist : Ken He
(II) Test Method:
Testing Item
Testing Method
With reference to EN 14582:2007 by
Halogen
combustion flask with oxygen and
Content
determined by ion chromatography
Reporting Limit
50 ppm
Remark: Reporting limit = Quantitation limit of analyte in sample
***********************************************************************
TO BE CONTINUED
PAGE 2 OF 9
Intertek Testing Services Ltd., Shanghai
TFH Division
Block B, Jinling Business Square,No.801 Yi Shan Road,
Shanghai, China, 200233
Tel: +86 21 6120 6565
Fax: +86 21 6127 9740
www.intertek.com
www.intertek.com.cn
China Toll-Free: 800 999 1338
TEST REPORT
NUMBER: SHAH00276230
TESTS CONDUCTED
(III) Measurement Flowchart:
Test For Halogen Content
Reference Standard: EN 14582
sampling/grinding or
cutting
add absorbent in a
combustion flask &
place weighed sample in
equipment
fill the combustion
flask with oxygen
ignite then leave the
flask at room
temperature
transfer the absorbent
into a volumetric flask
make up with deionized
water
analyzed by ion
chromatography
***********************************************************************
TO BE CONTINUED
PAGE 3 OF 9
Intertek Testing Services Ltd., Shanghai
TFH Division
Block B, Jinling Business Square,No.801 Yi Shan Road,
Shanghai, China, 200233
Tel: +86 21 6120 6565
Fax: +86 21 6127 9740
www.intertek.com
www.intertek.com.cn
China Toll-Free: 800 999 1338
TEST REPORT
NUMBER: SHAH00276230
TESTS CONDUCTED
2
(I) Test Result Summary :
Testing Item
Heavy Metal
Cadmium (Cd) content
Lead (Pb) content
Mercury (Hg) content
Chromium VI (Cr6+) content
Polybrominated Biphenyls (PBBs)
Monobrominated Biphenyls (MonoBB)
Dibrominated Biphenyls (DiBB)
Tribrominated Biphenyls (TriBB)
Tetrabrominated Biphenyls (TetraBB)
Pentabrominated Biphenyls (PentaBB)
Hexabrominated Biphenyls (HexaBB)
Heptabrominated Biphenyls (HeptaBB)
Octabrominated Biphenyls (OctaBB)
Nonabrominated Biphenyls (NonaBB)
Decabrominated Biphenyl (DecaBB)
Polybrominated Diphenyl Ethers (PBDEs)
Monobrominated Diphenyl Ethers (MonoBDE)
Dibrominated Diphenyl Ethers (DiBDE)
Tribrominated Diphenyl Ethers (TriBDE)
Tetrabrominated Diphenyl Ethers (TetraBDE)
Pentabrominated Diphenyl Ethers (PentaBDE)
Hexabrominated Diphenyl Ethers (HexaBDE)
Heptabrominated Diphenyl Ethers (HeptaBDE)
Octabrominated Diphenyl Ethers (OctaBDE)
Nonabrominated Diphenyl Ethers (NonaBDE)
Decabrominated Diphenyl Ether (DecaBDE)
Result (ppm)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Remarks: ppm = Parts per million = mg/kg
ND = Not detected
Responsibility Of Chemist : Dent Fang / Ken He
***********************************************************************
TO BE CONTINUED
PAGE 4 OF 9
Intertek Testing Services Ltd., Shanghai
TFH Division
Block B, Jinling Business Square,No.801 Yi Shan Road,
Shanghai, China, 200233
Tel: +86 21 6120 6565
Fax: +86 21 6127 9740
www.intertek.com
www.intertek.com.cn
China Toll-Free: 800 999 1338
TEST REPORT
NUMBER: SHAH00276230
TESTS CONDUCTED
(II) RoHS Requirement:
Restricted Substances
Cadmium (Cd) Content
Lead (Pb) Content
Mercury (Hg) Content
Chromium VI (Cr6+) Content
Polybrominated Biphenyls (PBBs)
Polybrominated Diphenyl Ehters (PBDEs)
Limits
0.01% (100ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
The above limits were quoted from 2002/95/EC and amendment
2005/618/EC for homogeneous material.
(III) Test Method:
Testing Item
Testing Method
Reporting
Limit
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
Cadmium (Cd)
microwave digestion until the
2 ppm
content
tested samples are totally
dissolved and determined by ICPOES.
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the
Lead (Pb) content
2 ppm
tested samples are totally
dissolved and determined by ICPOES.
With reference to IEC 62321 edition
1.0:2008 in clause 7, by microwave
Mercury (Hg)
digestion until the tested samples
2 ppm
content
are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
Chromium VI (Cr6+) 1.0:2008 in annex C, by alkaline
1 ppm
content
digestion and determined by UV-Vis
spectrophotometer.
***********************************************************************
TO BE CONTINUED
PAGE 5 OF 9
Intertek Testing Services Ltd., Shanghai
TFH Division
Block B, Jinling Business Square,No.801 Yi Shan Road,
Shanghai, China, 200233
Tel: +86 21 6120 6565
Fax: +86 21 6127 9740
www.intertek.com
www.intertek.com.cn
China Toll-Free: 800 999 1338
TEST REPORT
NUMBER: SHAH00276230
TESTS CONDUCTED
Testing Item
Polybrominated
Biphenyls (PBBs)
Polybrominated
Diphenyl Ethers
(PBDEs)
Testing Method
With reference to IEC 62321 edition
1.0:2008 in annex A, by solvent
extraction and determined by GC-MSD
and further HPLC confirmation when
necessary.
With reference to IEC 62321 edition
1.0:2008 in annex A, by solvent
extraction and determined by GC-MSD
and further HPLC confirmation when
necessary.
Reporting
Limit
5 ppm
5 ppm
Remark: Reporting limit = Quantitation limit of analyte in sample
Date Sample Received : AUG.18, 2011
Testing Period : AUG.18, 2011 TO AUG.23, 2011
***********************************************************************
TO BE CONTINUED
PAGE 6 OF 9
Intertek Testing Services Ltd., Shanghai
TFH Division
Block B, Jinling Business Square,No.801 Yi Shan Road,
Shanghai, China, 200233
Tel: +86 21 6120 6565
Fax: +86 21 6127 9740
www.intertek.com
www.intertek.com.cn
China Toll-Free: 800 999 1338
TEST REPORT
NUMBER: SHAH00276230
TESTS CONDUCTED
(IV) Measurement Flowchart:
Test For Cd/Pb/Hg/Chromium (VI)/PBBs/PBDEs Contents
Reference Standard: IEC 62321 edition 1.0:2008
sampling/grinding or cutting
Cr6+
Cd/Pb/Hg
metal
weigh sample and
for different
material, digest
the sample with
confirm the tested
samples are totally
dissolved
spot test
negative*2
No
polymers /
electronics
weigh sample
and add
alkaline
solution
get 50cm2
samples
definite
temp.
boiling water
extraction
cool and
filter the
extract
PBBs/PBDEs
weigh sample
and add
organic
soxhlet
extraction or
solvent
extraction
make up with
deionized water
analyzed by ICP-OES
make up with deionized
water and add diphenylcarbazide solution
concentrate
the extract
and make up
with organic
analyzed by GCMSD
analyzed by UV-VIS
***********************************************************************
TO BE CONTINUED
PAGE 7 OF 9
Intertek Testing Services Ltd., Shanghai
TFH Division
Block B, Jinling Business Square,No.801 Yi Shan Road,
Shanghai, China, 200233
Tel: +86 21 6120 6565
Fax: +86 21 6127 9740
www.intertek.com
www.intertek.com.cn
China Toll-Free: 800 999 1338
TEST REPORT
NUMBER: SHAH00276230
TESTS CONDUCTED
REMARKS:
*1: List of appropriate acid:
Material
Acid added for digestion
Polymers
HNO3,HCl,HF,H2O2,H3BO3
Metals
HNO3,HCl,HF
Electronics
HNO3,HCl,H2O2,HBF4
*2: If the result of spot test is positive, Chromium VI would be
determined as detected.
***********************************************************************
TO BE CONTINUED
PAGE 8 OF 9
Intertek Testing Services Ltd., Shanghai
TFH Division
Block B, Jinling Business Square,No.801 Yi Shan Road,
Shanghai, China, 200233
Tel: +86 21 6120 6565
Fax: +86 21 6127 9740
www.intertek.com
www.intertek.com.cn
China Toll-Free: 800 999 1338
TEST REPORT
NUMBER: SHAH00276230
TESTS CONDUCTED
***********************************************************************
END OF REPORT
PAGE 9 OF 9
Test Report
Applicant:
Number : TWNC00254946
Littelfuse, S.A. de C.V.
Blvd. Fausto Z. Martinez #1800
Col. Magisterio Seccion 38 C.P.
26070 Piedra Negras, Coahuila,
Mexico
Date
: May 04, 2012
Sample Description:
One (1) group of submitted samples said to be :
Part Description
: PLATED ZINC STRIP
Part Number
: 955412-001
Date Sample Received
: Apr 27, 2012
Date Test Started
: Apr 28, 2012
Test Conducted :
As requested by the applicant, for details please refer to attached pages.
Authorized By:
On Behalf Of Intertek Testing Services
Taiwan Limited
K. Y. Liang
Director
This report shall not be reproduced
except in full, without the written
approval of the laboratory.
Page 1 of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Number : TWNC00254946
Test Conducted
(Ⅰ) Test Result Summary :
Result (ppm)
(1)
(2)
Test Item
Heavy Metal
Cadmium (Cd) content
Lead (Pb) content
Mercury (Hg) content
Chromium VI (Cr6+) content (mg/kg with 50cm2)
ND
14
ND
Negative
(< 0.02)(#)
54
112
ND
Negative
(< 0.02)(#)
Remarks: ppm = Parts per million based on weight of tested sample = mg/kg
ND = Not detected
<
= Less than
mg/kg with 50cm2 = milligram per kilogram with 50 square centimetre
Negative = A negative test result indicated positive observation
was not found at the time of Test.
#
= Due to the insufficient sample area, reduced total sample
surface of 24 cm2 was used and the dilution factor was
adjusted accordingly.
Tested Components
(1) Silvery Metal Base Material
(2) Silvery Plating Layer
Responsibility of Chemist : Irene Chiou / Kevin Liu / Cathy Chen
Date Sample Received
Test Period
: Apr 27, 2012
: Apr 28, 2012 To May 03, 2012
(Ⅱ) RoHS Requirement:
Restricted Substances
Cadmium (Cd) Content
Lead (Pb) Content
Mercury (Hg) Content
Chromium VI (Cr6+) Content
Limits
0.01% (100ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for
homogeneous material.
Page 2 of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Number : TWNC00254946
Test Conducted
(Ⅲ) Test Method:
Test Item
Cadmium (Cd)
content
Lead (Pb) content
Mercury (Hg)
content
Chromium VI (Cr6+)
content
Test Method
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 7, by microwave
digestion until the tested samples are
totally dissolved and determined by
ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in annex B, by boiling water
extraction and determined by UV-Vis
Spectrophotometer.
Reporting Limit
2 ppm
2 ppm
2 ppm
0.02
mg/kg with 50cm2
Remark: Reporting limit = Quantitation limit of analyte in sample
Page 3 of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Number : TWNC00254946
Test Conducted
(Ⅳ) Measurement Flowchart:
Test for Cd/Pb/Hg/Chromium (VI)
Reference Standard:IEC 62321 edition 1.0:2008
Sample preparation
Take sample and immerse into Aqua Regia, start to strip plating layer
Stop the stripping procedure upon color change completely
Take the Aqua solution as plating component and stripped body as substrate component
Cd/Pb/Hg
Cr
Polymers /
electronics
Metal
For different
material, digest
the sample with
*1
appropriate acid
By spot test
Negative
Confirm the tested
samples are
totally dissolved
Make up with
deionized water
6+
*2
Weigh sample
and add
alkaline
solution
Get 50cm2 sample
Definite temp.
extraction
By boiling water
extraction
Cool and filter
the extract
Analyzed by ICP-OES
Make up with deionized water and add
diphenyl-carbazide solution
Remarks:
*1: List of Appropriate Acid:
Material
Polymers
Metals
Electronics
Analyzed by UV-VIS
Acid Added for Digestion
HNO3,HCl,HF,H2O2,H3BO3
HNO3,HCl,HF
HNO3,HCl,H2O2,HBF4
*2: If the result of spot test is positive, Chromium VI would be determined as detected.
End of Report
Page 4 of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Number : TWNC00254946
Test Conducted
Photo
Page 5 of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401