ICPTest_216XEP_04 11 2013 pdf

ICP Test Report Certification Packet
Company name :
Littelfuse, Inc.
Product Series:
216 series Axial Leaded Fuse
Product #:
216XEP
Issue Date:
April 11, 2013
It is hereby certified by Littelfuse, Inc. that there is neither RoHS (EU Directive 2011/65/EU,
recasting 2002/95/EC)-restricted substance nor such use, for materials to be used for unit parts,
for packing/packaging materials, and for additives and the like in the manufacturing processes.
In addition, it is hereby reported to you that the parts and sub-materials, the materials to be used
for unit parts, the packing/packaging materials, and the additives and the like in the manufacturing
processes, are all composed of the following components.
Issued by:
<Global EHS Specialist >
(1) Parts, sub-materials and unit parts
This document covers the 5x20 Fuse RoHS-Compliant series products manufactured by
Littelfuse, Inc.
< Raw Materials Used
Please see Table 1
(2) The ICP data on all measurable substances
Please see appropriate pages as identifed in Table 1
Remarks:
Form 585-047 Rev. A
1
2/21/06
Table 1: List of Raw Materials covered by this report
Total Parts
1
2
3
4
5
6
Raw Material Part Number
910-005
692539-002
909-444
091251
082xxx
C030210
Raw Material Description
Cap
Solder
Body
Sand Filler (RoHs & Halogens)
Wire-AgCu
Overcap
2
Page(s)
3-6
7-11
12-18
19-25
26-30
31-34
nov^
TESTREPORT
NO.4002R12050740-1R02
Daie:May.09,2012
Cu8tomer:SuzhouFuHongElectrcnic
IndustrialCo.,
Ltd.
AddT€€3:NO,69\ryEIDUROAD,WANGTING
TO\M{,XIANGCHENG
OISTRICISUZHOU.
CHINA
R€pot on the submitt€d sample sald to b€
Samplenah€: Copp€rsh€ll
Supplier:/
Samplerocolv€ddate:lvlay.07, 2012
T6tf ng pedod: Frcmluay.07,29l2toMay.A9,2012
T€€tino R€ou€6tod
As specifiedby clienl,lo delerminethe Lead,Cadmium,
l\,telcury
& Hexavalent
Chrcmiummntentin the submitledsamplein
.ccodancewilh Dircctive200295/EC(RoHS).
T€stino method:
I\l1QL
IEC62321:2008,seclionI
cadmium(Cd)
IEC62321:2008,seclion9
Mercury(Hs)
(CrVI)
chrcmium
IEC62321 2008,s€ction7
tcP-oEs
rcP-oEs
tcP-oEs
IEC62321i200EAnn€xB
2mg/kg
2 mg/kg
2 mSeS
0.02mg/kg'
Ieq
r 0.02mgl(g efers to the MQLofsampbenractiontiquid.
Concll|3ion:
-Whenlestedas specifiedlhe submitledsampl€€ompliedwith the requircments
of commission
Decisionof 18 Aug 2005
amendingDirecnve
2002r95/Ecnotifiedunderdocument
2005/61E/Ec.
*'*FOR FURTHERDETAILS.
PLEASEREFERTOTHEFOLLOWING
PAGE{S).*'"
Sigmdior andon behalfof
Shenzhen
AOVTeslingTechnology
Co.,Lld,KunshanBranch
/uI?'
,.r.ou.o.,,
oro.'n,44.
Li nngtng, lMaggie
Ch€micalTestDi€ctor
S}I€I\IZIIENAOV TESTINGTECHNOLOGY
CO.,ITD.(UI{SHAN ERANCH
ol:9Jllis,.*""
nov'
TESTREPORT
NO. A002R12050740-1R02
Add lhe digeslion€olution;lhe
vesselis heal€dunlilthe sample
f*;;1.,-
Coolinglhe vessel,fiteri washedand
T6st€dby tCP-OEs
filledto the man(withdislilledwater
Th8sampleis digesredin the
micrcwave
ov€niollowinga specific
decompositionprogram
Coolinglhevessol,filtsr;wasi€d and
filledlo lhe markwilhdistilled
water.
(boitingChromium
Content
warerext€crion)r
subsrrare)
{Mstat
Removetnesample,snd cool
Heal50 mL ofDlwalerin the
beakerto boilingfor 'l 0 min
-j.f*--*
lhe beakerto rcomtemp€€turc,
anddo the colorr€action
Testlhe samplesolutionandlhe 0.02
mg/kgstandardsolutionby W-VIS.
ToDsbmine d,C4lmiumandMercury
Conbnt(Plating)
Cooling,filter;washed
andfjll€d
lo lhe markwithDl water.
-------------l
-r€st€d by
________'
l__rl nupo,r I
Instumenl |
SHENZHEI\I
AOV T€STII{OTECHI{OLOGY
CO.,!TO.XUNSTIA BNA CH
|
|
Hotllne
nov'
TESTREPORT
NO
Dats:iray 09,2012
Page3ot4
5. To DetemineH€xavalent
Ch.omiumContenlin colorlessand coloredchromatecoalingon metals:(Plaling)
",ffii'Q*a*
lf lh€ tast r€sult is positive,
lhe samplels considered
lo
hav€hexavalenl
chromium
lfthe l€st tesull
and lhe 0.0?mg/kg
Boiling- waler- enraclion
proc€dureshall be used to
lfthe|eis interierence
oritis hardlodecidewhether
the samplehavelhe ho(avalent
chromium
5.2 Boiling-waleFexlraclion
Takethe (5015)cm'z
Remov€lhe sample,andcool
Heats0 mloforwalerin lhe
beaker
!o boiling
for10min
the b€akorlo roomtsmp€ralute,
anddo the colorreaction
Teslthe samplesolution
andthe 0.02
mg/kgslandaritsolutionby UV-VIS.
Pl€ring
Lead(Pb)
(cd)
cadmium
(Hg)
Mercury
(Cr\,I)
chromium
Unil
RoHSLimil
mg/xg
1000
100
1000
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
1000
Negalive
Negalive
mg/Kg
mg/xg
mg/xg
SHENZHENAOV TISTII{G IECHNOfOGYCO.,!TO.XUNSIIATINA CH
Hotline
36.512-55100000
novTESTREPORT
NO.:4002R12050740-1R02
-Tnen€w RoHSdi€ctive2011/65/EU,
on Jul.21, 2011 com€inloiorce,on Jan 03,2013 thefomat imptemenlaton,
Dircctrve
2002/95/EC
sh.ll be rcp€aledsimultaneousty.
-Specimens,
whichrequesred
to detemineLead,Cadmiumand MercuryConrent,
haveboendissotved
compt€r€ty.
-N.D.=not
detecGd(<rUaL)
]\,lQL=lvlethod
Quantilation
Limit
-Negative=Absene
or cr (VI):
'Positive=Presence
of Cr (VI)l
Uncedain=
can nolv€dfywhetherthe samplehav€Hexavalent
Chromium
by spot-test.
(The lerled sampleshouldbe tunherveified by boiting,wal€r+xtraclion
methodif lhe spot test resuttis uncedainol
sThe tesl is basedon the followi.gassumplion:
The sampteptaringis a singlelayerandeachpa( is unifom The testresult
maybecannotsrandior lh€ physicalttuth
ofsampteptating.
Photographof Sample
SHINZIIENAOVTESIINGTFCHNOLOGYCO.,LTO-KUNSHABRAI{CH
Ollo.tll.?,.""""
TestR€port
No.SHAEC1216714750
Date:25 Sep2012
Page'l ofs
ZHEJIANGASIAGENERALSOLDERING&BRAZING
MATERIALCO.,LTD
XIHU INDUSTRIALPARK,SANDUN,HANGZHOUCITY,ZHEJIANG,PROVINCE,
CHINA
Thgfollowing
sample(s)
was/were
submitted
andidentifed
on beharf
of thedientsas : LEAD-FREE
soLDER
WIRE
SGSJobNo.:
PartNo.(P/N):
Composition
:
Dateof SampleReceived:
TestingPeriod:
Te6tRequested:
- SH
sP12-028285
YTWl02 (692s39-002)
Sn2.0CuRE
21 9ep 2012
21 Sep2012- 25 Sep2012
Selectedtest(s)as requestedby dient.
TestMethod:
TestResults:
Pleasereferto nextpage(s).
Pleaseref€rto ne\4page(s).
Basedonthe performedtestson submittedsamples,lhe resultsof Lead,
polybrominated
Mercury,
Cadmium,
Hexavalent
cfiromium,
biphenyls
(pBB),
Polybrominated
diphenylethe6
(PBDE)
compty
withthetimibas setby RoHS
Direclive
2011/6yEU
Annexll; recasting
2OO2|95/EC.
Conclusion
:
Signedfor and on b€halfof
scs-cgTcLtd.
,z?r"'-
FanJinqjie,JJ
ApprovedSign€tory
rhb d@Dnr b rFr.c |r nr
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Man!6rorrh€sqs olo!! (scs sA)
TestReport
No.SHAEC1216714750
Date:25Sep2012
Page2 of 5
TestResults:
TestPartDesciiotion:
Sp€oim€nllo.
1
SGSSampl€lD
Dcc,ipdon
SHA12-167147.043Sitvery
wire
RemarlG:
(1)1 mgftg=1 PPm=0.0001%
(2)IVDL= MethodDetedionLimit
(3) ND= NotDetected( < l\4DL)
(4) "-" = NotRegulated
RoHSDir€divo2011/85/EU
Testl\rethod: Withreferenc€
to IEC6232'1:2008
(1)Determination
ofCadmium
by ICP-OES.
(2)Determination
of Leadby tCp-OES.
(3)Determination
of Mercury
by |CP-OES.
(4) Determination
of Hexavalent
Chromiumby Spottest/ Cotodmetric
MethodusingUV-Vis.
(5)Determination
of PBBS/ PBDES
by GC-MS.
Te6t ltem(s)
Cadmium(Cd)
Lead (Pb)
Mercury(Hg)
HexavalenlChromium(Cr(Vl))
Sumof PBBS
Monobromobiphenyl
Dibromobiphenyl
Tribromobiphenyl
Tetrabrcmobiphenyl
Pentabromobiphenyl
!!!it
Ud!
10O
1000
mS/kS
mSikg
1000
-
mdkg
mgKg
mgKg
mgKg
mgKg
mg/Kg
ms/Ks
mg/Kg
mg/Kg
mS/kS
mgKs
mdkS
meyKg
1To 'nT
-
Heptabromobiphenyl
Oclabromobiphenyl
Nonabromobiphenyl
Decabromobiphenyl
Sumof PBDES
Monobromodiphenyl
ether
1000
-
l\4DL
@3
2
N
D
2
168
2
N
D
O
Negative
N
D
5
5
5
5
5
5
5
5
5
5
-
N
N
N
N
N
N
N
N
N
N
N
D
D
D
D
D
D
D
D
D
D
D
5
N
D
rn .dothr,$rLbhdtuFl
c!dr-/.
dnr ncr.|'ld
& qi.r rdta dsn-r
m.rr.ddaDlhMllln.d'lddtl.'
i'drbdn'l''hcd'c'|i&dcmdr.
h dr hi rPd
Dt' cir b,h. rm,
t'inr$r$fedrdrr6nl,gEidaorr
+l..t.t.lr6ldrl33oClstn
.b, hro
.
2o@3]
ll:M
ndhl. .rtrrhd
Fdr b. hnr.dm
lElE{S-Al6ia02563lElEls-a!ffiIg
rL{6-nl6|102ra rrlr{6-?r)5ae3
9w.64a.m
.€.d't!0.tM
.mb.rol rh. scs Goup{8Gs€ }
TestReport
No.SHAEC1216714750
Test ltem(s)
Dibromodiphenyl
ether
Tribromodiphenyl
ether
Tetrabromodiphenyl
ether
Psntabromodiphenyl
elher
H€xabromodiphenyl
ether
Heptabromodiphenyl
ether
Octabomodiphenylether
Nonabromodiphenyl
elher
Decabromodiphenyl
ether
udt
Lldl
ms/Ks
mg/Kg
mg/rg
mS/kg
mg/Kg
mg/Kg
mg/Kg
m9Kg
mdkg
Datei25 Sep 2012
upt
5
5
5
5
5
5
5
5
5
Page3 of 5
a3
ND
ND
ND
ND
ND
ND
ND
ND
NO
Notes:
(1)Themaximum
permissible
limitis quotedfromdirective
2011/65/EU,
Annexll
(2)
"spottest:=
Negative Abs€nceof Cr(Vl)coating,Positive= Presenceof Cr(Vt)coating;
methodif the spottest result
Cfhetestedsampleshouldbefurthervedfiedby boiling-wateFextraction
is Negative
or cannotbeconfirmed,)
oBoiling-wateFextraction:
Negative= Absenceof Cf(Vl)coating
Posilive= Presenceof Cr(Vl)coating;the detectedconcenhation
in boiling-water-extraclion
solutionis
equalor greaterthan0.02mg/kgwith50 cm. samplesurtac€area.
For@rosionprotection
coalings
on metals:Infofmation
onsto€geconditions
andproduction
dateof
thetestedsampleis unavailable
andthusresultsof Cr(Vl)represent
statusofthesampleat thetime
of testing.
n6.hffi
hft
*4dntuorrbrh
rrh..(.)r-rd.
f 6illselb'b.dld$0|..dlirdtqrr
lFt.-Ll.*tr6ltl€o!l6r}|
@
l|:a@3
TEEFZT)tll66! IBEFA)6*$,D
Hr (a-at614qer Hj F-a)fl@l
w6|a.M
. ttdhl&s@
M.m!.t olrhsaGsololp (aagsA)
TestReDort
No. SHAEC1216714750
Date:25 Sep2012
Page 4 of 5
ATTACHMENTS
RoHSTesflngFtowChart
1) Nameof the personwhomadetesting:
JanShi^/oyoWangr'A
enXao,caryXu
z) N€meortnepersonin chargeof testing:JeffZhang/ceorge
Xu/LindaLi
r) Inesesampres
w€redissotved
tota v bv ore-conditioning
methodaccording
to belowflowchart.(Cr6'
andPBBS/PBDES
testmethodexctudedi
Pb/Cd/Hg
PBBs/PBDEs
Aciddigestion
with
microwave/hotplate
Nonmetallic
matedal
1)AlkaliFusion/
DryAshing
2) Acidto dissolve
Filtration
andpH
adjustment
Addang
1,5diphenylcarbazide
for color
development
rn. .@md
e -.,r!!5ffi
I h.!d
byri.6oF
/ E[i-r
tu
&mil&hFd
b r. ord
codl|dr
b rm. rn c.dtu
rd.r[f,t
n6.hffi
6dr
oi s
k d
Ddod@nFr!.
Adding1,5diphenylc€rb€zide
for color
development
A redcolor
indicatesthe
pre6enceof cr6*. lf
necess€ry,
confirmwith
r.{dMrffi.
Thb drsrud
d!.r
b.6rmdr..d
*ror
6 nrr,$,l.d
N.ris,.4jwr
d tn.c.ffiv
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EtB-?)6r102r1 iL(ri-?r)A!G3
Urmllr ol |h. AgAelou! (gGSSA)
TestReport
No.SHAEC1216714750 Date:25
Sep2012
Page5 of 5
Samplephoto:
sHA12-167147.043
reportonly
SGSauthenticate
thephotoonoriginal
"' Endof Report"*
tt-!,ruaYanbrrrr&id,$.'icti
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lrom!.r ol rh.8og Group(8G€S )
Test Report
Applicant:
Littelfuse Philippines Inc.
LIMA Technology Center, Lipa City,
Malvar, Batangas
Number
: TWNC00304282
Date
: Mar 29, 2013
Sample Description:
One (1) group of submitted samples said to be :
Part Description
: Ceramic Body
Part Number
: 909-444_909-157_909-438
Date Sample Received
: Mar 21, 2013
Date Test Started
: Mar 22, 2013
Test Conducted :
As requested by the applicant, for details please refer to attached pages.
Authorized by:
On Behalf of Intertek Testing Services
Taiwan Limited
K. Y. Liang
Director
*THJ0304282*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C.
全國公證檢驗股份有限公司
11492 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410
Page 1 of 7
Number
Test Conducted
: TWNC00304282
(Ⅰ) Test Result Summary:
Test Item
Result
White
ceramic
RL
ND
2
ND
2
ND
2
ND
1
ppm
ND
5
ppm
ND
5
ppm
ND
5
ND
5
ND
5
ND
5
ND
5
ppm
ND
5
ppm
ND
5
ppm
ND
5
Unit
Test Method
Heavy Metal
Cadmium (Cd) Content
ppm
Lead (Pb) Content
ppm
Mercury (Hg) Content
ppm
Chromium VI (Cr6+) Content
ppm
Polybrominated Biphenyls (PBBs)
Monobrominated Biphenyls
(MonoBB)
Dibrominated Biphenyls
(DiBB)
Tribrominated Biphenyls
(TriBB)
Tetrabrominated Biphenyls
(TetraBB)
Pentabrominated Biphenyls
(PentaBB)
Hexabrominated Biphenyls
(HexaBB)
Heptabrominated Biphenyls
(HeptaBB)
Octabrominated Biphenyls
(OctaBB)
Nonabrominated Biphenyls
(NonaBB)
Decabrominated Biphenyl
(DecaBB)
ppm
ppm
ppm
ppm
With reference to IEC
62321: 2008, by
microwave digestion and
determined by ICP-OES.
With reference to IEC
62321: 2008, by
microwave digestion and
determined by ICP-OES.
With reference to IEC
62321: 2008, by
microwave digestion and
determined by ICP-OES.
With reference to IEC
62321: 2008, by
alkaline digestion and
determined by UV-Vis
Spectrophotometer.
With reference to IEC
62321: 2008, by solvent
extraction and
determined by GC-MS and
further HPLC-DAD
confirmation when
necessary.
*THJ0304282*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C.
全國公證檢驗股份有限公司
11492 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410
Page 2 of 7
Number
Test Conducted
Test Item
Unit
Polybrominated Diphenyl Ethers (PBDEs)
Monobrominated Diphenyl Ethers
ppm
(MonoBDE)
Dibrominated Diphenyl Ethers
ppm
(DiBDE)
Tribrominated Diphenyl Ethers
ppm
(TriBDE)
Tetrabrominated Diphenyl
ppm
Ethers (TetraBDE)
Pentabrominated Diphenyl
ppm
Ethers (PentaBDE)
Hexabrominated Diphenyl Ethers
ppm
(HexaBDE)
Heptabrominated Diphenyl
ppm
Ethers (HeptaBDE)
Octabrominated Diphenyl Ethers
ppm
(OctaBDE)
Nonabrominated Diphenyl Ethers
ppm
(NonaBDE)
Decabrominated Diphenyl Ether
ppm
(DecaBDE)
Halogen Content
Fluorine (F)
ppm
Chlorine (Cl)
ppm
Bromine (Br)
ppm
Iodine (I)
ppm
Remarks:
ppm
ND
RL
: TWNC00304282
Test Method
With reference to IEC
62321: 2008, by solvent
extraction and
determined by GC-MS and
further HPLC-DAD
confirmation when
necessary.
With reference to EN
14582:2007 by
calorimetric bomb with
oxygen and determined
by Ion Chromatograph.
Result
White
ceramic
RL
ND
5
ND
5
ND
5
ND
5
ND
5
ND
5
ND
5
ND
5
ND
5
ND
5
ND
ND
ND
ND
50
50
50
50
= parts per million based on weight of tested sample = mg/kg
= Not detected
= Reporting Limit, Quantitation limit of analyte in sample
Responsibility of Chemist:
Date Sample Received
Test Period
Kevin Liu/ Irene Chiou/ Vico Lin
: Mar 21, 2013
: Mar 22, 2013 To Mar 29, 2013
*THJ0304282*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C.
全國公證檢驗股份有限公司
11492 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410
Page 3 of 7
Number
Test Conducted
(Ⅱ) Limit:
RoHS Limit
Restricted Substances
Cadmium (Cd) content
Lead (Pb) content
Mercury (Hg) content
Chromium VI (Cr6+) content
Polybrominated Biphenyls (PBBs)
Polybrominated Diphenyl Ehters (PBDEs)
: TWNC00304282
Limits
0.01% (100ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
The above limits were quoted from Annex II of 2011/65/EU for homogeneous material.
*THJ0304282*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C.
全國公證檢驗股份有限公司
11492 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410
Page 4 of 7
Number
Test Conducted
: TWNC00304282
(Ⅲ) Measurement Flowchart:
Test for Cd/Pb/Hg/Chromium (VI)/PBBS/PBDES Contents
Reference Standard: IEC 62321 edition 1.0:2008
Sample preparation
For non-metal part
For metal part
Take sample and immerse into Aqua Regia, start to strip plating layer
Stop the stripping procedure upon color change completely
Take the Aqua solution as plating component and stripped body as substrate component
PBBs/PBDEs
Weigh sample and
add organic solvent
By Soxhlet
extraction or
Solvent extraction
Concentrate the
extract and make up
with organic
solvent
Cr
6+
Substrate
Cd/Pb/Hg
Weigh sample
and add
alkaline
solution
For different
material, digest
the sample with
*1
appropriate acid
Plating
Cr
6+
By spot test
Definite temp.
extraction
Cool and filter
the extract
Confirm the tested
samples are
totally dissolved
Negative
Get 50cm2 sample
Make up with
deionized water
By boiling water
extraction
Analyzed by ICP-OES
Analyzed by GC-MSD
Remarks:
*1: List of Appropriate Acid:
Material
Polymers
Metals
Electronics
*2
Make up with deionized
water and add
diphenyl-carbazide
solution
Analyzed by UV-VIS
Acid Added for Digestion
HNO3,HCl,HF,H2O2,H3BO3
HNO3,HCl,HF
HNO3,HCl,H2O2,HBF4
*2: If the result of spot test is positive, Chromium VI would be determined as detected.
*THJ0304282*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C.
全國公證檢驗股份有限公司
11492 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410
Page 5 of 7
Number
Test Conducted
: TWNC00304282
Test for Halogen Content
Reference Standard:EN 14582
Sampling/grinding or
cutting
Add absorbent in a
combustion flask &
place weighed sample in
equipment
Fill oxygen into
calorimetric bomb
Ignite then leave the
bomb at room
temperature
Transfer the absorbent
into a volumetric flask
Make up with deionized
water
Analyzed by ion
chromatography
End of Report
This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a
recommendation for any particular course of action. Intertek does not accept a duty of care or any other responsibility to any person other than
the Client in respect of this report and only accepts liability to the Client insofar as is expressly contained in the terms and conditions
governing Intertek's provision of services to you. Intertek makes no warranties or representations either express or implied with respect to this
report save as provided for in those terms and conditions. We have aimed to conduct the Review on a diligent and careful basis and we do not
accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by statute or otherwise, except in
the event of our gross negligence or wilful misconduct.
*THJ0304282*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C.
全國公證檢驗股份有限公司
11492 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410
Page 6 of 7
Number
Test Conducted
: TWNC00304282
Photo
*THJ0304282*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C.
全國公證檢驗股份有限公司
11492 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410
Page 7 of 7
Test Report
Applicant:
Number : TWNC00282887
Littelfuse Philippines Inc.
LIMA Technology Center, Lipa City,
Malvar, Batangas
Date
: Oct 31, 2012
Sample Description:
One (1) group of submitted samples said to be :
Part Description
: Filler
Part Number
: 091251
Date Sample Received
: Oct 24, 2012
Date Test Started
: Oct 25, 2012
Test Conducted :
As requested by the applicant, for details please refer to attached pages.
Authorized By:
On Behalf Of Intertek Testing Services
Taiwan Limited
K. Y. Liang
Director
*THJ0282887*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410
Page 1 of 7
Number : TWNC00282887
Test Conducted
(Ⅰ) Test Result Summary :
Result (ppm)
Submitted Samples
Test Item
Heavy Metal
Cadmium (Cd) content
Lead (Pb) content
Mercury (Hg) content
Chromium VI (Cr6+) content
Polybrominated Biphenyls (PBBs)
Monobrominated Biphenyls (MonoBB)
Dibrominated Biphenyls (DiBB)
Tribrominated Biphenyls (TriBB)
Tetrabrominated Biphenyls (TetraBB)
Pentabrominated Biphenyls (PentaBB)
Hexabrominated Biphenyls (HexaBB)
Heptabrominated Biphenyls (HeptaBB)
Octabrominated Biphenyls (OctaBB)
Nonabrominated Biphenyls (NonaBB)
Decabrominated Biphenyl (DecaBB)
Polybrominated Diphenyl Ethers (PBDEs)
Monobrominated Diphenyl Ethers (MonoBDE)
Dibrominated Diphenyl Ethers (DiBDE)
Tribrominated Diphenyl Ethers (TriBDE)
Tetrabrominated Diphenyl Ethers (TetraBDE)
Pentabrominated Diphenyl Ethers (PentaBDE)
Hexabrominated Diphenyl Ethers (HexaBDE)
Heptabrominated Diphenyl Ethers (HeptaBDE)
Octabrominated Diphenyl Ethers (OctaBDE)
Nonabrominated Diphenyl Ethers (NonaBDE)
Decabrominated Diphenyl Ether (DecaBDE)
Halogen Content
Fluorine (F)
Chlorine (Cl)
Bromine (Br)
Iodine (I)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Remarks: ppm = Parts per million based on weight of tested sample = mg/kg
ND = Not detected
Responsibility of Chemist : Irene Chiou / Kevin Liu / Cathy Chen
Date Sample Received
Test Period
: Oct 24, 2012
: Oct 25, 2012 To Oct 30, 2012
*THJ0282887*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410
Page 2 of 7
Number : TWNC00282887
Test Conducted
(Ⅱ) RoHS Limits:
Restricted Substances
Cadmium (Cd) Content
Lead (Pb) Content
Mercury (Hg) Content
Chromium VI (Cr6+) Content
Polybrominated Biphenyls (PBBs)
Polybrominated Diphenyl Ehters (PBDEs)
Limits
0.01% (100ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
The above limits were quoted from Annex II of 2011/65/EU for homogeneous
material.
(Ⅲ) Test Method:
Test Item
Cadmium (Cd)
content
Lead (Pb) content
Mercury (Hg)
content
Chromium VI (Cr6+)
content
Test Method
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 7, by microwave
digestion until the tested samples
are totally dissolved and determined
by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in annex C, by alkaline
digestion and determined by UV-Vis
spectrophotometer.
Reporting Limit
*THJ0282887*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410
2 ppm
2 ppm
2 ppm
1 ppm
Page 3 of 7
Number : TWNC00282887
Test Conducted
(Ⅲ) Test Method:
Test Item
Polybrominated
Biphenyls (PBBs)
Polybrominated
Diphenyl Ethers
(PBDEs)
Halogen Content
Test Method
With reference to IEC 62321 edition
1.0:2008 in annex A, by solvent
extraction and determined by GC-MS
and further HPLC-DAD confirmation
when necessary.
With reference to IEC 62321 edition
1.0:2008 in annex A, by solvent
extraction and determined by GC-MS
and further HPLC-DAD confirmation
when necessary.
With reference to EN 14582:2007 by
calorimetric bomb with oxygen and
determined by Ion Chromatograph.
Reporting Limit
5 ppm
5 ppm
50 ppm
Remark: Reporting limit = Quantitation limit of analyte in sample
*THJ0282887*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410
Page 4 of 7
Number : TWNC00282887
Test Conducted
(Ⅳ) Measurement Flowchart:
Test for Cd/Pb/Hg/Chromium (VI)/PBBS/PBDES Contents
Reference Standard: IEC 62321 edition 1.0:2008
Sample preparation
For non-metal part
For metal part
Take sample and immerse into Aqua Regia, start to strip plating layer
Stop the stripping procedure upon color change completely
Take the Aqua solution as plating component and stripped body as substrate component
Cd/Pb/Hg
Cr
Weigh sample and
add organic solvent
By spot test
Negative
Confirm the tested
samples are
totally dissolved
Make up with
deionized water
PBBs/PBDEs
Polymers /
electronics
Metal
For different
material, digest
the sample with
*1
appropriate acid
6+
Get 50cm2 sample
By boiling water
extraction
*2
Weigh sample
and add
alkaline
solution
By Soxhlet
extraction or
Solvent extraction
Definite temp.
extraction
Cool and filter
the extract
Analyzed by ICP-OES
Concentrate the
extract and make up
with organic
solvent
Analyzed by GC-MSD
Make up with deionized
water and add diphenylcarbazide solution
Remarks:
*1: List of Appropriate Acid:
Material
Polymers
Metals
Electronics
Analyzed by UV-VIS
Acid Added for Digestion
HNO3,HCl,HF,H2O2,H3BO3
HNO3,HCl,HF
HNO3,HCl,H2O2,HBF4
*2: If the result of spot test is positive, Chromium VI would be determined as detected.
*THJ0282887*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410
Page 5 of 7
Number : TWNC00282887
Test Conducted
(Ⅳ) Measurement Flowchart:
Test for Halogen Content
Reference Standard:EN 14582
Sampling/grinding or
cutting
Add absorbent in a
combustion flask &
place weighed sample in
equipment
Fill oxygen into
calorimetric bomb
Ignite then leave the
bomb at room
temperature
Transfer the absorbent
into a volumetric flask
Make up with deionized
water
Analyzed by ion
chromatography
End of Report
This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a
recommendation for any particular course of action. Intertek does not accept a duty of care or any other responsibility to any person other than
the Client in respect of this report and only accepts liability to the Client insofar as is expressly contained in the terms and conditions
governing Intertek's provision of services to you. Intertek makes no warranties or representations either express or implied with respect to this
report save as provided for in those terms and conditions. We have aimed to conduct the Review on a diligent and careful basis and we do not
accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by
statute or otherwise, except in the event of our gross negligence or wilful misconduct.
*THJ0282887*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410
Page 6 of 7
Number : TWNC00282887
Test Conducted
Photo
*THJ0282887*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410
Page 7 of 7
Test Report
Applicant:
Number:
ELSCHUKOM ELEKTROSCHUTZKOMPONENTENBAU
GMBH
GEWERBESTRASSE 87,D-98669 VEILSDORF,
GERMANY
Date:
SHAH0036227401
JAN 18, 2013
Sample Description:
Two(2) pieces of submitted samples said to be :
(1) Mixed all kinds of metal substrates.
(2) Mixed all kinds of plating layers.
Item Name
: Silver Plated & Pure Silver Wires.
Item No.
: (B-1) 101.014 -. ---– silver plated copper wire – Cu, Ag--%
(B-2) 101.0131.---– pure silver wire – Ag 1000
(B-3) 101.0123.0--– silver plated purest nickel wire – Ni99.98%, Ag1%
(B-4) 101.0182.0--– silver-copper alloy plated copper plated iron nickel alloy wire
– ElconD, AgCu5%
(B-5) 101.0120.0--– silver plated constantan wire – CuNi44, Ag5%
(B-6) 101.0151.0--– silver plated copper - nickel 44 alloy wire
– CuNi44, Ag10%
(B-7) 1050--31.-------– pure silver strips – Ag 1000 pure
Country Of Origin
: Germany.
************************************************************************************************************************************************************
Tests Conducted:
As requested by the applicant, for details refer to attached page(s).
************************************************************************************************************************************************************
To Be Continued
Authorized by:
For intertek testing services Ltd., Shanghai
Jacob Lin
General Manager
Page 1 Of 5
Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233
Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
Test Report
Number:
SHAH0036227401
Tests Conducted
(A) Test result of RoHS Directive:
Result
Testing item
(1)
Cadmium (Cd) content (mg/kg)
ND
Lead (Pb) content (mg/kg)
ND
Mercury (Hg) content (mg/kg)
6+
Chromium2(VI)(Cr ) result (by boiling water extraction on metal) (mg/kg
with 50cm )
ND
ND
Result
Testing item
(2)
Cadmium (Cd) content (mg/kg) /Plating
ND
Lead (Pb) content (mg/kg) /Plating
ND
Mercury (Hg) content (mg/kg) /Plating
ND
6+
Chromium2(VI)(Cr ) result (by boiling water extraction on metal) (mg/kg
with 50cm ) /Plating
ND
2
Remark:mg/kg with 50cm = milligram per kilogram with 50 square centimeter
ND = not detected
(B) RoHS Requirement:
Restricted substances
Cadmium (Cd)
Lead (Pb)
Mercury (Hg)
6+
Chromium (VI) (Cr )
Limits
0.01% (100 mg/kg)
0.1% (1000 mg/kg)
0.1% (1000 mg/kg)
0.1% (1000 mg/kg)
The above limits were quoted from RoHS Directive 2011/65/EU for homogeneous material.
(C) Test method:
Testing item
Cadmium (Cd) content
Lead (Pb) content
Mercury (Hg) content
6+
Chromium (VI) (Cr ) content (for
metal)
Testing method
With reference to IEC 62321 Edition 1.0: 2008, by acid
digestion until the tested sample was totally dissolved, and
determined by ICP-OES.
With reference to IEC 62321 Edition 1.0: 2008, by acid
digestion until the tested sample was totally dissolved, and
determined by ICP-OES.
With reference to IEC 62321 Edition 1.0: 2008, by acid
digestion until the tested sample was totally dissolved, and
determined by ICP-OES.
With reference to IEC 62321 Edition 1.0: 2008, by boiling
water extraction and determined by UV-VIS
Spectrophotometer.
Reporting limit
2 mg/kg
2 mg/kg
2 mg/kg
2
0.02mg/kg with 50cm
(in testing solution)
Date sample received: Jan.14, 2013
Testing period: Jan.14, 2013 To Jan.17, 2013
************************************************************************************************************************************************************
To Be Continued
Page 2 Of 5
Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233
Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
Test Report
Number:
SHAH0036227401
Tests Conducted
(D) Measurement flowchart:
Test for Cd/Pb/Hg/Cr (VI)/PBBs/PBDEs contents
Reference standard: IEC 62321 Edition 1.0: 2008
Sampling/grinding or cutting
Cr
Cd/Pb/Hg
Metal
Weigh sample and for
different material, digest
the sample with
*1
appropriate acid
Positive
No
Confirm the tested
samples are totally
dissolved
Yes
Polymers /
electronics
PBBs/PBDEs
Weigh sample
and add alkaline
solution
Spot test
Get 50cm
samples
6+
Weigh sample and
add organic
solvent
*2
Definite temp.
Extraction
2
Boiling water
extraction
Soxhlet extraction
or
Solvent extraction
Cool and filter the
extract
Concentrate the
extract and make
up with organic
solvent
Make up with
deionized water
Analyzed by ICP-OES
Make up with deionized water
and add diphenyl-carbazide
solution
Analyzed by GC-MSD
Analyzed by UV-VIS
Remarks:
*1: list of appropriate acid:
Material
Polymers
Metals
Electronics
Acid added for digestion
HNO3,HCL,HF,H2O2,H3BO3
HNO3,HCL,HF
HNO3,HCL,H2O2,HBF4
*2: If the result of spot test is positive, Chromium VI would be determined as detected.
************************************************************************************************************************************************************
To Be Continued
Page 3 Of 5
Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233
Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
Test Report
Number:
SHAH0036227401
Tests Conducted
************************************************************************************************************************************************************
To Be Continued
Page 4 Of 5
Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233
Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
Test Report
Number:
SHAH0036227401
Tests Conducted
************************************************************************************************************************************************************
End Of Report
This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a recommendation for any particular
course of action. Intertek does not accept a duty of care or any other responsibility to any person other than the Client in respect of this report and only accepts liability
to the Client insofar as is expressly contained in the terms and conditions governing Intertek's provision of services to you. Intertek makes no warranties or
representations either express or implied with respect to this report save as provided for in those terms and conditions. We have aimed to conduct the Review on a
diligent and careful basis and we do not accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by statute or otherwise,
except in the event of our gross negligence or wilful misconduct.
Page 5 Of 5
Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233
Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
l\OV'BF.F.q,A
TESTREPORT
NO.:4002R121008024-2R02
Oate:Oct.1
0,2012
Cuslomer: SuzhouFuHongElectronicIndustriatCo.,
16.
Addr6s: NO.89 \/ElDU ROAD,WANGTINGTOVIN,XTANGCHENG
DISTR|CI SUZHOU.CHINA
Repod on the submltted samrl€ said to be
sample name: Leadwife coppershell
Modol:/
Itefi/Lot Io.: /
Matonal:/
Buyen/
Supplier:/,
lilanufacturE:/-f
.
_
- i
Samplerecelveddate:
Gq
2012 :
_08,
:
t*,tn o"n.o,t.. o".;;,,013
"."r.-,.,,613,
1
,]
i
&glirs-Bgsccsgq
As specifedby dienl,to determine
the L€ad,Cadrium,l,tercury
& tiexayabntChrcmium
conle in the6ubmitted
samptein
accodance
withDirective
2OO2I95/EC
{RoHS).
j
Testino method:
Testingltem
Lead(Pb)
IEC62321:2008.
sectionI
cadmium(Cd)
IEC62321:2008,
s€ction9
(Hg)
[,lercury
IEC62321r2008,
s€ction7
(CrM)
Chromium
IEC62321:2008,AnnexB
Measufing
instrument ,MQL
rcP-oEs
a!gag
tcP-oEs
rcP-oEs
2 mg/kg
2 mg/kg
0.02mg/kg*
lsq
j 0.02mg/tg rctursto the MQL olsampleexlractionliquid.
Conclu3ion:
-\ryhentested as specifiedlhe submiliedsamplecompriedwith th€ requircmentsof commissionD€cisionof 18 Aug 2005
amendingDircctive2002/95/ECnotiliedunderdocum€nt2005/618/EC.
."*FOR
FURTHERDETAILS,PLEASEREFERTOT
Sign€dior and on behallol
ShenzhenAOVTestingTechnology
Co., Ltd,Kunshan8ran6h
Walbn
A?1
ea"arc"a"r,
YuanQi, l,lickey
LiTingting,Maggie
Chemical Test Direclor
OrO."*0r44
Technical
Di€clor
LabManager
STIENZIIEN
AOVTE$Tl'{GI€CHI!OLOGYCO,.I.TD,KUNSHAN
BRANCI]
(,10",'ll,,u*
l\ov"BF,?sn
TESTREPORT
NO.:A0O2R12100802+2R02
D a t eO c i . 1 0 , 2 0 1 2
T63l Flow:
L
ToDetemine/lead,
CldmiumContent(Metalsubstrale)
lestedbY
L7.^otq,
Add the digestionsolulionjthe
vess€lis heateduntilthesample
Coolingthe vessel,fiitei washedand
fllledlo the mafKwith distilledwaler.
-*".irl,"*J
"r,to,"t|,
The sampleis digestedin the
Addlhe digestion
soluUon,
close
lhemicrowave
vessel.
micrcwaveoventollowinga specinc
progrcm.
deoomposilion
Coolingthe vessel,frller;washedand
filled to the maft wilh dislilled waler.
Remove
lhe sample,
andcool
thebeak€rlo roomtemperature,
anddo thecolorreaclion
-].f----
Testthe samplesolulionand ihe 0.02
mg/kgslandardsolutionby uv-vls.
(Plating)
nrte,.washedand
______-l
l_____*p;-r, f;;-1
"*rn
rilledlo$e markwithDlwaler
I
I
ON
EANCH
ShENZH€N
A O VI 6 S T I I { GT ' C N O I O G YC O . . I T D . X U N S H A
' Hotlrne
40a 7008600
/\OV"BF#,HN
TESTREPORT
NO.iA002R121008024-2R02
O a t e : O c l 1 02 0 1 2
coalingon metals:(Plating)
in colorless
andcolorcdchromate
Hexavalent
Chromium
Content
5. ToDeiermine
r e s t ebd'v : l )
^,
L/A^U,4.
(
5.1Spotlesl
lf thelestresultis posiiive,
lo
ihesampleis considered
chromium
havehexavalenl
Place
1-5
Boiling- water-
lf the testreslrlt
extracton
procedurcshall be us€d to
and the 0.02 mg/kg
lltherc is intederenceor it is had to decide
whetherlhesamplehavethe hexavalent
water-enractron
5.2Boilin9Removethe sample,and cool
Takethe (50i5)cm2
Heat50 ml ol Dl walerin the
samplein the beaker.
beak€rto boilinglof 10 min
the beakerto rcomtemperalu€,
and do the colorrcaolion
Sample Doscripilon:
Code
Sample Desc{iplion
Leadwire Plating
Unit
Code
coppershellsubslfate
CoppershellPlatng
24
Result
RoHSLimit
2-3
N.O
Lead{Pb)
(Cd)
Cadmium
mg/l(g
1000
N.D.
N.D.
N.D.
mg/k9
100
N.D.
N.D.
N.D,
N.D.
(Hg)
Meroury
mg/kg
1000
N.D.
N.D.
N.D,
ND.
Chromum(Crl'I)
mg/K9
1000
Negalive
Negalrve
Negaliv€
Negative
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TESTREPORT
oare:oct.10,2012
NO.:A0O2R12100802+2R02
-:fh€newRoHSdi€ctive2011/65/EU,
Direcliv€
on Jul.21,2011comeinloforce,on Jan.03,2013thsformalimplementation,
simultaneously200295/EC
ahallbe repeal€d
Sp€cimens,whichggqeted to d€temineLead,CadmiumandMercuryconient havebeendissolvedcompletelv.
-mg/Kg=ppm
ceofC_rl\,I)l
if"veiry/y6hetp ttef.li
v
meresr{.q!.be/rurTr
--The iest is bas€don the following
maybecannotstandfor the physicaltruth
-Photois included
ii'iffyiT-''
lhe spot test result is uncertainor
*'q:*
eachpadis unifom.Theteslrcsult
Leadwir€ coppershell
"'End of Repod""
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