ICPTest_220XP_11 10 12 pdf

ICP Test Report Certification Packet
Company name :
Littelfuse, Inc.
Product Series:
2AG Special
Product #:
220xxxXP Series
Issue Date:
November 10, 2012
It is hereby certified by Littelfuse, Inc. that there is neither RoHS (EU Directive 2002/95/EC,
2011/65/EU)-restricted substance nor such use, for materials to be used for unit parts, for
packing/packaging materials, and for additives and the like in the manufacturing processes.
In addition, it is hereby reported to you that the parts and sub-materials, the materials to be used
for unit parts, the packing/packaging materials, and the additives and the like in the manufacturing
processes, are all composed of the following components.
Issued by:
<Global EHS Engineer>
(1) Parts, sub-materials and unit parts
This document covers the 2AG Special RoHS-Compliant series products manufactured by
Littelfuse, Inc.
＜ Raw Materials Used
Please see Table 1
(2) The ICP data on all measurable substances
Please see appropriate pages as identifed in Table 1
Remarks：
Form 585-047 Rev. A
1
2/21/06
Table 1: List of Raw Materials covered by this report
Total Parts
Raw Material Part Number
Raw Material Description
Page(s)
1
082XXX
Wire - Ag plated Cu
3-12
2
082779
Lead Wire
13-17
3
087244
HMA - ROHS
18-26
4
087244
HMA - Halogen
18-26
5
497XXX-001
Wire – Cu Clad Fe58 Ni Ag by weight
27-33
6
YTW108 (692535-001)
Solder
34-38
7
910-222
Cap – base and plating
39-42
8
910-537-3
Cap - base
43-46
9
910-537-3
Cap - plating
47-50
10
082xxx-001
Wire - Cu CDA 102 Sn plated
51-56
11
648106-001
C909-367-001
C909-369-001
Yarn
57-62
Body
63-67
12
2
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No.SHAEC1119525001 Date:07 Dec2011
Page1of 5
3MCHINALII\4ITED
222#T|ANLtNROAD,SHANGHAT
(200233)
Thefollowing
sample(s)
was/were
submjtted
andidentified
on behatfof thectientsas j 3M3779-pc
SGS Job No. :
- SH
sP11-036760
Date of Sample Received :
TestingPedod:
03 Dec2011
03 Dec20'11- 07 Dec2011
Test Requested :
Selectedtest(s)as requestedby ctient.
Test llethod :
Pleasereferto nextpage(s).
Test Rosults :
Pleasereferto nextpage(s).
Signedforandon behalfof
scs-csTcLtd.
,.,1s
,rt*{
*
Fan Jingjie,JJ
ApprovedSignatory
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Monboroth. SGSgrup (SGgS )
TestReport
No.SH4EC1119525001
Date:07 Dec 201'1
Page 2 of 5
Test Results:
TestPanDescriotion
:
Spodm€nNo.
1
SGSSamplelD
D66cription
1-195250.001
SHA1
Ye ow sotid
Remarks
:
(1)1 mg/kg=I PPm=0.0001o/o
(2)MDL= l,tethodDetection
Limit
(3)ND = NotDetected
( < IIDL )
(4)"-"= NotRegulated
RoHSDir€dive201iA5/EU
Testl\rethod: with referenc€
to tEC62321i2008
(1)Delemination
ofCadmium
by tCP-OES.
(2)Determination
of Leadby tCp-OES.
(3)Determination
of Mercury
by lCp-OES.
(4)Determination
of Hexavatent
Chromium
by Cotodmetric
MethodusingIJV-Vis.
(5)Determination
of PBBS/ PBDES
contentby GC-MS.
Test ltem(s)
Cadmium(Cd)
Lead(Pb)
Mercury(Hg)
Hexavalent
Chrcmium(Cr(Vl))
Sumof PBBS
Monobromobiphenyl
Dibromobiphenyl
Tdbromobiphenyl
Tetrabromobiphenyl
Pentabromobiphenyl
Hexabromobiphenyl
Heptabromobiphenyl
Oclabromobiphenyl
Nonabrohobjphenyl
Decabromobiph6nyl
Sumof PBDES
Monobromodiphenyl
ether
$uB4t6-.Bdk,Hie
'aad*
ud!
udr
Ma!
100
1,000
1,000
1,000
1,000
-
mS/kS
mg/kg
mg/kg
mg/kg
mg/kg
mg/Kg
ng/Kg
mg/kg
mg/Kg
mgfl(g
mg/kg
mg/Kg
mgKg
mgKg
mg/Kg
mg/kg
mg/kg
2
2
2
2
-
N
N
N
N
N
D
D
D
D
D
5
5
5
5
5
5
5
5
5
5
,
N
N
N
N
N
N
N
N
N
N
N
D
D
D
D
D
D
D
D
D
D
D
5
N
D
1,000
-
b hr
rmr
hd
com'rk
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h. c@
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Membfi ol h6 SGS G.o{p (SqS S,A)
TestReport
No.SHAEC1119525001
Test ltemls)
Dibromodiphenyl
ether
Tribrcmodiphenyl
ether
Tetrabromodiphenylether
Pentabromodiphenyl
elh€r
Hexabromodiphenyl
ether
Heptabromodiphenyl
ether
Oclabromodiphenyl
elher
Nonabromodiphenyl
ether
Decabromodiphenyl
elher
tuni.!
Ulit
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mdkS
mg/kg
mdkS
Date:07 Dec 2011
Mgt
Page3 ofs
@l
5
5
5
5
5
5
5
5
5
ND
ND
ND
ND
ND
ND
ND
ND
ND
Notes:
(1)Themaximum
permissible
limitis quotedfromdirective
2011/65/EU,
Annexll
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TestReport
No.SHAEC1119525001 Date:07 Dec2011
Page4 of 5
ATTACIII,|ENTS
Rol-lsTestingFlo\ r Chart
1) Nameof the p€rsonwho madetesting:Jan S hi/yolo Wangr'Aen Xiaocary Xu
2) Nameofthe p€r6onin charg€ofteging: JeffZhang/George
Xu/ Etim Lin
3) Thesesamples wered issolvedt otatty by pre-cond
itioning methodacDordi
ng to betow ffow chan.
(Cr6+and PABs/PBDEst6st
methodexdudeO
SamplePreparalion
SampleMeasuremenl
Pb/Cd/Hg
PBBs/PBDES
Acid digestionwith
micrDwa\€/hohlate
Metallic
matedal
Concentratio
n/
Dilutaon
ofodradion
solution
Heatingto 90-95C
for extraclion
1)AlkaliFudon
/
OryAshing
2) Acjdtodissol\E
Filtrationand pH
adiustnent
Adding1,S
diphenY€arbazide
Adding'l,$
diphentcarbazide
de\elopment
indicatesthe
iro -drll!!tub
bd
&!m.tr6
Ebld
b thr
md cdhffi
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[email protected]
ry b rb ..FPr.(.)
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M3mb6rot rheSGSGroup(SGSSA)
TestReport
No.SHAECI'l19s25001
Date:07Dec2011
Page 5 of 5
Samplepholo:
sHA11n9s250.001
SGS authenticate
the photoon originalreportonly
""' Endof Report"*
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TastReport
No. SHAEC1119525002
Date:07 Dec 2011
Page 1 of4
3MCHINALIIVITED
222#T|ANLtNROAD,SHANGHAT
(200233)
Thefollowing
sample(6)
wasi/vere
submitted
andidentified
on behalfofthectientsas :3M 3779-pc
- SH
SGSJobNo.:
sP11-036760
Dateof SampleReceived 03Dec2011
TestingPedod:
03Dec2011-07Dec2O11
Tesl Requested:
Selectedtest(s)as requestedby client.
Test Method:
Pleasereferto nextpage(s).
TestResults:
Pleasereferto nextpage(s).
Signedfor and on behalfof
scs-csTcLtd.
.--),-
,/t*(
Y*
Fan Jingjie,JJ
Approved Signatory
tiu dud
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(SGSaA)
lrombor
otth€SCSCloup
TestReport
No.SHAEC1119525002
Date:07Dec2011
Page2 of 4
Test Results:
T€st PartDescriotion:
Sp€dm6nNo.
SGSSamplolO
D€6cfiption
1
SHA1l-195250.001Yellowsolid
Remarks:
(1) 1 mg/kg=1 ppm=0.0001%
(2) MDL = MethodDetectionLimit
(3) ND = Not Detected( < MDL )
(4) "-" = Not Regulated
Haloo€n
Test lrethod : With reference
to EN 14582:2007,analysis
wasperformed
(lC).
by lonChromatograph
Testltem{s)
(F)
Fluorine
(Cl)
Chlorine
(Br)
Bromine
lodine(l)
Unit
mg/kg
mg/kg
mg/kg
mg/kg
ftldemd
b &.d by rh. c.rtse &q-i
hd
@,.,gEo*
d..4d,r4d
tudnc
l+ltffill{eq!l.dlgr9
t3ltzEnastql/l!l{i!.'gq
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b h. ofmrc&dlnld
!d
b rlm.ir
o6idri6 k EMor.
h'h
aryi"k.lhb
&ffitL
MDL
50
50
50
50
D.eMr
d mcoMrB.-dM'
rdrd!E
ffi;Eifiaii'*-iiiaii
OA
ND
ND
ND
ND
tu- abdli
d.trtr,rD.cmk_qL.
rEtetlgfdritud&rrirE
$I.5f.h[AlttStots+ll
dnfi.$aoh 2o@3
!l:2@o3
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tErE€6+l)el4!55! taE6-al)t405$?9
Bci.t{.com
r€sdirorF.@
!r!(6-rjl611@o4 H!lt6-zt)sa6K0
MehbrrotlheSGSOlouD(SGSSA)
TestReport
No.SHAEC1'119525002
Date:07 Dec201'1
Page3 of 4
ATTACHMENTS
HalogenTestingFlowChart
1) Nameof thepersonwhomadetesting:
DaisyGong
2) Nameof thepersonin chargeofte6ting:Alex
Jiang
Samplemeasurement
Combustion
in oxygenboftb
Dissolved
in an absorption
solution
Analyzed
by ion
chromatography.
Doubleconfkm
byotherinstruments,
if
rhbdtuiff
| 6rd !r rh conFry rhtd b dr oddr ftrdds3 ar5
hn
daclhublr 4- b r.nr tn! codfr
!l! rd,,!!!!r'*
b ddo.
|.sd.nndbrdi.^ryh&'dls
ddroit, tur. . rn.c@ryr
rn.c@rvr
dd.bl|'.||d.u.d.r|h.h
rdlon
Doo|Eb
trqld & |d|#
!t ,N
ffis.c.fr4.!4!d!hn
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Fr. r.d$
Fr.
t'etEl$&lbrsto dxniudtd,gt$aflonr 2@33
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a-h ic6nhlbii;i'r
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rE!E(S-2r)0t104!&
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N!(6.?16r102!04 -L {*-n)6460cs3
lwcr.3s"co6
. .ssd'mO69q
(SGgsr)
M6mb6rollheaqsGbup
T€st Report
No.SHAEC1119525002
Date:07Dec2011
Page4 ol4
Samplephoto:
sHA11-195250.001
SGS authenticate
the photoon odginatreportonty
"* End of Report'*'
tTr.t:ry::.
i:?aq!Ke.n:
D-? I'gT.
j!L
1cbj
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hrw.iMridrndnldrhrnrrr.ih..F
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lrl:2M3
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(scssa)
Mlmb€|
olrh.scsGoup
Validi
nown
ForQueEll
PleaseCo
Test Report
No.: CEl2011184955
Datet20'1111201
POLYFILAG
OBERALLMENDSTMSSE2OA,CH€3OOZUG / SWITZERLAND
ithscs
Page:'l of 7
ll]uttfi
[[m
Thefollowingsample(s)wa3/weresubmitledand identitiedby/onbehalfof the clientas:
SampleDesciption
Buyer/OrderNo.
SampleReceiving
Date
TestingPeriod
Ni42Fe58MCuMAgs%
11-0803
2011t11t25
2011t11t25'l O 2011I 1'J01
T€stResult(s)
Pleasereferto nextpage(s).
(NW4E
f,lmdiorrd
Or.rlcd l,.bor|b.t - Trlpd
ps(31i€ded rhs ied rcpod eiior be
cwpanye
!,
rt
rr-ri'f.,ri,il]ilntlli ir ].ri
iiil-:i I
ny tublsd b b Gene6 coideoB d se
1,.
|.lrrrr?!t!:.
dbis r aiy'Iha cohpantssoo r69onsbiI s b r ct'odaddrhs dodm
! hdsrLrzore.N4lrFr .o ri p,i /F L I I|t,
f: lFt
. ,;,i+ @610?)ree
14 | + 8610r)2ee
ry
(w ar.on
TestReport
No.: CE/201
1/84955
Page:2of 7
Dale: 2111/12t01
POLYFILAG
OBERALLI\4ENDSTMSSE
2OA,CH63OO
ZUG/ SWITZERLAND
lm[tmlrltttll
Test Reault{s}
PARTNAMENo.1
SILVERCOLOREDI'ETAL WIRE (INCLUDINGTHE PLATINGLAYER)
T66l ltem(s)
Unit
Cadmium(Cd)
Method
mSikS Witheferenceto tEC62321:2008and
perfom€dby lCPdES.
mgKg Withreference
to IEC62321:2008and
perfomedby ICP-AES.
mg/Kg Withreference
to IEC62321:2008and
pe.formed
by ICP-AES.
Withreferenc€
to IEC6232'1:
2008and
performed
by Boilingwaterextraction
M€thod.#
Lead (Pb)
(Hg)
Mercury
Hexavalent
Chromium
Cr(Vl)
Sumof PBB9
l\4onobromobiphenyl
Dibromobiphenyl
Tribromobiphenyl
Tetrabromobiphenyl
MDL
2
R6sult
No.l
n.o.
2
2
n.d.
Negative
n.d.
n.d.
n.d.
n.d.
n.d.
n.d.
n.d.
n.d.
n,d,
n.o.
5
5
5
Pentabromobiphenyl
Hexabromobiphenyl
Heptabromobiphenyl
Octabromobiphenyl
Nonabromobiphenyl
Decabromobiphenyl
Sumof PBOE3
Monobromodiphenyl
ether
5
mgikg
Withreference
to IEC62321:2008and
per{ormedby GC/lrS.
DibromodiDhenvl
ether
TribromodiDhenvl
ether
Tetrabromodiphenyl
ether
PentabromodiDh9nvl
ether
Hexabromodiohenvl
ether
Heplabro.nodiphenylether
5
5
n.d.
n,o.
5
5
5
n.d.
n.d.
n.d.
n.d.
5
n.o.
n.d.
5
5
5
Octabromodiphenvl
ether
NonabaomodiDhenvl
ether
n.d.
n.d.
n.d.
Decabromodiohenvl
ether
c o m o a n yi r r l ! /
tu.f-]i'
I rlirlltr] ntlrli
n,o,
I
:.i
i
^r!.l;li,
I r.. r.i. rriilA.
L@nnieroi
aidllr edd'on $@3 d
onry3id*ib'.lhormrrsorcenrsnsrld'on.f,'ryth6compaiyssecsponsurrysiobc,enraidhcdm!
iidbe€pduedexeptniur*6oq
!^r+s6(0nreenr
@! a!@n
M€f,be,or 'he 5616,@p (s6sr{)
TestReport
No.: CFJ2011184955
Page:3 of 7
Dale:2O11h21O1
POLYFIL
AG
OBEMLLMENDSTRASSE
2OA,CH-6300ZUG/ SWITZERLAND
Testltem(s)
Halogen
Halogen-Fluorine
(F)
(CASNo.:14762-9+8)
Halogen.chlorine
(Cl)
(CASNo.:22537-15-1)
Halogen-Bromine
(Br)
(CASNo.:10097-32-2)
Unit
lrethod
With refe.enc€to BS EN 14582].2007
.
mg/Kg
Analysis
wasperformod
by lC.
Halogen-lodine
(l)
(CAS No.: 14362-4,4-8)
|l]rl||l]
MDL
t[]||n
Result
No.1
50
n.d.
50
n.d-
50
n.d.
50
n.o.
NoteI
1. mg/kg= ppm; 0.1wt%= 1000ppm
2. n.d.= NotDetected
3. [4DL= MethodDetection
Limit
4."-"=NotRegulated
5. " = Qualitative
(NoUnit)
analysis
=
6. # a. Positivemeansthe presenceof CrVlon the testedareas
b. Negativemeansthe abgenceof CrVlon the testedareas
Thedetected
concentration
in boiling-wEter€xtraction
6olution
is equalor greaterthanO.O2
mg/kgwithS0cm,
testedareas.
7. The6ample(s)
was^rereanalyzed
on behalfoftheapplicant
as mixingsamplein onetesting.Theaboveresult(s)
was^^€re
onlygiv€nas theinformality
vaue.
c m e a i ya r | 1 l l r ' r d 1 1 ' t , r , i i l l , n r 4 L . i . r 1
iirl4li
r3G)rssrd rh I r€d'+on €nnd e '
ir'r'r Nlttll\.
tfi r:li {:/:rFi4,t;r+s6Frtreer7e r}s6Or)xerr
Ewar.on
Test Report
No.: CEl2011/84955
Paget 4 of 7
Dale:2011h2101
POLYFILAG
OBERALLMENDSTMSSE2OA,CH-6300ZUG / SWITZERLAND
t[| tl
rrr ]l
'1) Thesesamples
! €re dissolved
totallyby prcconditioning
methodaccording
to belowflowchart.
( Cf' test methode(cluded)
yang
2) Nameof the personwfiomademeasurement:
Climbgle€t
3) Nameof the personin chargeof measurement:
TroyChang
Cutling/ Preparation
Aciddigestion
by suitable
acid
dependedon differentsample
matedal(as belodtable)
Add appropriateamountof
digestion
reagent
Heatto eppropriate
temp€ratueto extract
Cool, filter digestate
1) AlkaliFusion
2) HCltodissolve
ICP-AES
throughfilter
AdddiphenyFcarbazide
for
SampleMaterial
colordevelopment
DigestionAcid
Steel,copper,aluminum,
solder
Aqua regia,HNO3,HCl,HF,HrO,
Glass
HNO/HF
measure the absorbance
Gold,platinum,palladium,ceramic
Aqua regia
at 540 nm by UV-VIS
Silver
HNOs
Plastic
H,SOI, H'O', HNO3,HCI
Others
Anyacidtototaldigestion
rlrlt
c f f i o . n yB : . 1
t-f
i,l'irl!
!,i
i,.t'l
lii]]irl)
! rd4krzE,
'r
1rItihl-
Nlwri @.ry.tuM{/}i.:
r ;r
+1 r rtLtri,ni+ s6 orrree
Test Report
No.: CE/2011/84955
POLYFILAG
OBEMLLMENDSTRASSE2OA,CH€3OO
ZUG/ SWITZERLAND
|t
PBB/PBDEanalyticalFLOW CHART
1) Name
of theperson
whorEdenEasurer€nt:
RormnWong
2) Mrneof theperson
incharge
of fipasurenEnt:
TroyChang
Firsttestingprocess----+
Optional
screenprocess---process - .>
Confifination
Scfeenanalysis
Sanpleextractiort
So*rlet nEthod
ConcedtratdDilute
Extractedsolution
Filter
Analysisby GCiMS
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TestReport
No.: CE/2011/84955
Page:6 of 7
Date 2011,1|:]01
POLYFILAG
OBERALLIVENDSTRASSE
2OA,CH$3OO
ZUG/ SWITZERLAND
rt][]|l
rtl[]ll
Analltical flow chart of halogen content
1) Narneofthe pe6on who rcde fiEasurenEnt:Rita Chen
2) Narneof the person in charge of rEasureient: Troy Chang
SaftplepretreatnEnt/ Separatbn
Weightiryandputting
sanplein cell
OrygenBombConbustion
/ Ahsorption
Dilution
to fixedvolunE
AnalysiswasperforfiEdby lC
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r l r r r j r J ,n j r l ; .
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Test Report
No.: CE/2011/84955
Page.7of 7
Dai.e| 2O11112J01
POLYFIL
AG
OBEMLLMENDSTMSSE
2OA,CH{3OOZUG/ SWITZERLAND
][|l
||ttl
' Thetsgtedsample,/pa is ma*ed by an
anow if ifs shownon the photo..
" Endof Repod*'
a o h p a n y, : j f r : | t r j , f _ i '
r , r i r r , , l :i l r l ) : i . . . ! , i
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l
TestReport
No.SHAECl216714748
Page 1 of 5
Date:25 Sep2012
CO''LTD
MATERIAL
SOLDERING&BRAZING
ASIAGENERAL
ZHEJIANG
CHINA
PROVINCE'
CITY,ZHEJIANG,
PARK,SANDUN,HANGZHOU
XIHUINDUSTRIAL
SOLOER
Thefollorvingsample(s)wasl/vercsubmittedandidentifiedon behalfof the clienb as : LEAD'FREE
WIRE
- SH
sP12-028285
sGSJobNo.:
)
YTW1o8(692535-001'692535-003
PartNo.(P/N):
Composition:
Dateol SampleReceived:
TestingPeriod:
TestReqlested:
TestMethod:
Test Resulb:
:
Condusion
Sn3.0CuRE
21 gep 2012
21 Sep2012- 25seq 2012
Selededtest(s)as requestedby client.
Pleasereferto nextpage(s).
Ple€sereferto nextPage(s)
testson submittedsamples,the resultsof Lead'
Basedonthe perfrcrmed
(PBB)'
biphenyls
Polybrominated
chromium,
cadmium,Hexavalent
Mercury,
RoHS
by
as
set
the
limits
with
(PBDE)
comply
diphenylethe6
Polybrominatecl
200295/EC.
2011/6tEuAnnexlli recasting
Direciive
Signedfor andon behalfof
sc$csrc Ltd.
,zQv"-
Fan Jingjie,JJ
Approved Signatory
rhb@drb
&.d
tt tu cqryry
r4rg,.giffi:iii;
ftH,#'ffiffiffiffffififfi
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+t.rt.lE6lufte+eet
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2@
al:4
108{S.?r)61{!!a iElE6-?1Fa€m9
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wd{rm
. *!|h.e4(!ii
ri.rnb.lol0|. SosoollP (8oSS )
TeetReport
Date;25 Sep2012
No.SHAEC1216714748
Page2 of 5
TestResufts:
Test PartDesc.iption:
D*qiptlon
SpodmqrNo. SGSSandolD
Silvery
wire
SHA'12167147.041
1
Rema*€ :
( 1 )I m g / k g 1
=P P m = 0 0 0 0 1 %
(2) MDL= MethodDetedionLimit
(3) ND= NotDetected( < NIDL)
(4) = NotRegulated
""
RoHSDiradv€ 2011/65/EU
TestMethod: with referenceto lEc 62321i2008
by ICP-OES.
(1)Determination
of Cadmium
(2)Oetemination
of Leadby ICP-oES
of Merdirybv ICP'OES
(3) Determination
MethodusingUV-Vis
Chromiumby Spottest/ Colorimetric
(4) Determination
of Hexavalent
of PBBS/ PBDESby GC-MS'
(5) Determination
Test ltem(s)
Cadmium(Cd)
Lead (Pb)
Mercury(Hs)
HexavalentChromium(Cr(Vl))
Sumol PBBS
Monobrcmobiphenyl
Dibrcmobiphenyl
Tribromobiphenyl
TetrabromobiPhenyl
PentabromobiphenYl
Hexabromobtphenyl
HeptabromobiPhenyl
Octabromobiphenyl
Nonabromobiphonyl
DecabromobiPhenyl
Sumof PBDES
ether
Monobromodiphenyl
;i;a' ir*&{.d
Limit
ud!
100
1000
1000
mg/kS
mSftS
mS/kg
M0!
2
2
2
o
1000
-
mgkg
mSikS
mdkS
mS/kS
5
5
5
-
ms/ks
5
-
mdkS
mg/kg
mg/kg
mgftS
mdkg
mS/kg
mS/kg
mdkg
5
5
5
5
5
5
1000
-
n dnl.,.d/bb
tlrr'ttafi$bDd|rddna.{rofr
{l -I*.*trBlt!l8aea3+l
6rr.{.tt.d
5
@1
ND
55
ND
Negative
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
NO
ND
ND
'
!93
aI: 2@
rEE6+r)B1a@ IEE€GA)6|€Sdrg
nj{c-2rtauozg $i6GA)4|d063
M.n&r otfi. Soaor.r0 (8GssA)
sGq
TestReport
No.SHAEC1216714748
ud!
tird!
Test ltem{s)
Dibromodiphenylether
Tribromodiphenyl
ether
elher
Telrabromodiphenyl
Pentabrcmodiphenyl
ether
ether
Hexabromodiphenyl
elher
Heptabromodiphenyl
elher
Octabromodiphenyl
ethet
Nonabromodiphenyl
ether
Decabromodiphenyl
mg/kS
mS/kS
mdks
mSikS
mg/kS
mSftS
mdkS
mS/kS
mdkS
Date:25Sep2012
Mot
@1
5
5
5
5
5
5
5
5
5
ND
ND
ND
ND
ND
ND
ND
ND
ND
Page3 of 5
Notes:
Annexll
2011/65/EU'
(1)Themaximum
permissible
limitis quotedffomdireclive
(2) ospoltest:
Negative= Absenceof Cr(Vl)coating,Positive= Presenceof Cr(Vl)coating;
methodif the spottest result
Ohe testedsampleshouldbefurthervedfiedby boiling-wateFexlraction
is Negativeor cannotbe confimed-)
oBoiling-wateFextraction:
Negative= Absenceof Cr(Vl)coating
solutionis
positive= Presenceof Cr(Vl)coating;the detectedconcentration
in boiling-wateFextraction
area
surface
equalor greaterthanO.O2mg/kgwith50 crn"sample
Forcorosionprotectioncoatingsonmeta|s:|nformationonstorageconditionsandproducliondat
andthusresultsof Cr(Vl)representstatusof the sampleat the time
the testedsampleis unavailable
of testing.
iiiiir-r'ud-poa-t.ovbrk.md(.rrrd'
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d!| |lqsrflddctrr
+l -ll.*tr6lurlftaer+gttl
l|:
2@
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rii('-zl5r4&t4 f{! (6-er)6,La6t
(8GSSA)
€mD.rot!h. sGEGrcuP
TestR€port
No.SHAECl216714748
Date:25 Sep2012
Pag€ 4 of 5
ATTACHMENTS
RoHSTestingFlowChart
1)Nameof thepersonwhomadetesting:JanShi/Yoyo
Wangr'Allen
XiaolGaryXu
2) Nameof thepersonin chargeof testing:JeffZhanglceorge
Xu/LindaLi
3)Thesesampleswere
dissolved
lotallyby pre-conditioning
methodaccording
to betowflowchart.(Cf'
andPBB!,/PBDES
testmethodexcluded)
SamplePrepaEtion
Pb/CdHg
PBBs/PBDES
Heatingto 90-957
for extraction
1)AlkaliFusion
/
DryAshing
2)Acidtodissolve
1,5Adding
diphenylcarbaade
for color
development
t6&tttY|laf{dpdtrd,st{iatr
'Fr.-*.ltrEtdttidotsr+l
@
lr:2@3
Adding
1,5diphenylcalbaAde
for color
development
A rcd color
indicatesthe
presence
of cr8t.
necessary,
rErEF2!) 8r@53I€EF{|FMD
rll Fzl6lil&5aa rij F€i)i6063
lLint r otth.sos Gro{p(8GSs,l)
TeetReport
No.SHAEC1216714748
Oate:25 Sep2012
Page5 of 5
Samplephoto:
sHA12-167147.041
SGS authenticatethe photo on odginal report only
". Endof Report'_
ndd b rr oodr c.ddr
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[.tn!.rolfr. scaGr.{, {8GSA)
nov'
TESTREPORT
NO.jA002E11121307'1R02
page1of4
DaG:Dec.t5,2Oi1
Custom6iSuzhouFuHongEteclronic
IndustialCo.,
L6.
AddT€sg:
NO.89WEIDUROAD,WANGTINGTOWN.
XIANGCHENG
oIsTRIcT.sUzHoU.CHINA
Reporton tie subnitiedsamptes.idto be
Samplename:Coppershell
Modsl:/
Materlal:/
D€cripiion:/
Buyer:/
Supplier:/
SamPlercceiwd date:Elec.'13,2011
T€dng poriod:FromDec.13,2011
lo Dec.15,2o.l1
T€lino Reou6ted
As sp€cified
by client,to deteminethe L€ad,Cadmium,
Mercury
& Hexavat€nt
Chromilmcontentantheslbmifiedsamptein
accordancewilh Dircctive200295/EC(RoHS).
Te.Unomethod:
T€slingliem
Lead(Pb)
IEC62321:2008,
sectionI
IEC62321:20t,3,
s€clion9
cadmium(cd)
llercury(Hg)
(Crl'1)
Chromrum
IEC62321:2008,
section7
IEC62321:2008,
AnnexB
Measuring
instrument MQL
rcP-oEs
2mg/kg
tcPoEs
lcPoEs
2 mg/kg
2 mg/kg
0 o2mgkg'
leg
-' 0.02mg/kgreGrclo theMQLof sampte
extraction
tiquid.
99!9!cis!i
-When
tesledas specined
thesubmi(ed
sample
compli€d
wilhthercquirements
of commission
Decision
of 18Aug2005
amendingDirective2002/95/ECnotiliedundefdocument2005/618/EC.
---FOR
Pro,ect
Leader
(Engine€r)
FURTHERDETAILS,PLEASEREFERTOTHEFOLLOWNGPAGE(ST**'
/{bjA-L
J4
,ffi:::j:,,44
lnsoected
bv
,**'*''*,n-, [,[rlg-,iti-Y\
BRANCIi
SHENZHEnlAOVTESTINC TECHNO!OGY CO..L.TD,KUI\ISIIAI\I
Holline
8 6 . 5 1 2 . 5 5 1800 0 0
nov.
TESTREPORT
NO,:A002E11121307-1
R02
Weighthesampleinto
Add the digestionsotutionithe
vesselis healeduntilthe sampl€
hasb€€ndissolved
F*_-lTo
Tesledby ICP-OES
Content(MelalsubstEle)
Add the digeslionsolutjon,ctose
The sampleis digesredin the
the micfowaveves:€|.
mrcrowave
oveniollowinga sp€citic
program.
decomposilion
+
Coolingthe vessel,fltet washedand
filled to the ma* with distilled wat€r.
To Detenn
exavalenl
Chromium
(bojtingContent
(Metatsubstrate)
wateFextraction):
Heat50 mL of Dl walerin the
samplein the beaker.
beakerto boilingior 10 min
F;;1.To Delemine
Remove
thesample,
andcool
thebeakerto roomlemperature,
anddothecolorleadion
Tesllh€s€mplesolution
andthe0.02
mg/kgstandardsolutionby UV-VIS.
andl\Iercury
Content(Plaling)
andlilled
___+l coorins.rirteiwashed
l_-_----|lresteo oy l+fl_*l
t ot h em a * w i tD
ht w a t e r .
l r n " r , u r n " nI , l " * '
I
I
SHENZHsN AOV TG6TINGICCHITOI"OGYCO.,L'O.KUNAHAN BRANCH
a
I
Hotline
86-512-551
80 0 0
nov'
TESTREPORT
NO.i4002E11121307-rR02
oste:oec15,2011
5. ToO€temineHexavalent
Chromium
Contentincolorlessand cotorcdcnromaEcoatingon metats(Plaljng)
,':"j":::i
v^02
lf the tesl rcsultis posilive,
the sampleis considercdto
havehexavalenl
chromilm
Place
1-5
Compare
the
Eoiling- wateF ext€ctjon
prccedurcshall be usedto
andlhe 0.02mg/(q
standa.d
solution
lfthereis int€rference
or it is hardto decidewhether
thesampl€havetie h€xavatent
chromium
5 2 Eoilingwat6Fextraction
Tako the (50+5) cm'?
Heat50 mlof Dlwaier in the
samplein the beaker.
beakerlo boilingfor 10 min
Removetie sample,and cool
lhe beaksrto roomtempeEture,
and do the colorreaolion
Testthesamplesolution
andthe0.02
mg/kgstandard
solution
by UV,VIS.
T€t Re6ult3:
Unit
Limil
Substrate
Plating'
N.O.
N.O.
N.D.
Negalive
Lead(Pb)
(cd)
Cadmium
mg/Kg
(Hg)
lvercury
mgn(]s
1000
100
1000
chromium(Crl'I)
mg/Kg
1000
mg/Kg
Result
RoHS
N.D,
N.D.
N.D.
Negative
S!IENZHENAOV'CSTING IECIINOIOGY CO..ITD,KUNSHAN gNANCH
Hotline
a6-512-551
80 0 0
novTESTREPORT
NO 4002E11121307.rR02
'The new RoHSdirective2011/65/EU,on Jul. 21 2011 comeintolorce
,
on Jan.03, 2013 the fomat imptementation.
Direclive
2002,95/ECshallbe rcpeatedsimuttaneousty.
-specimens,whichrequestedto determineLead,cadmiumand l,rercury
conteni,havebeendissorvedcomprererv
-N.D.=notdetected(<tltoL)
-MOL=ntethodOuantitation
Limit
-Negative=Absenceof Cr (VIir
PositivFPresenceofCr (\ll)i
Unc€rlain=can not verifywhetlerthe samptehaveHexavatent
Chromiumby spoltest.
(The test€d sample should be fufthet verifiedby boiling-waler-€nraction
method if the spot test resutt |s uncertainor
negalive.)
-'The tesl is basedon lhe followingassumption:Thesampteptatingis a singtetayefand
each paft is uniform.The tesr resutt
maybecannotslandbr lhe physicaltruthofsampteptating.
Photograph
ofSample
Coppershell
ARANCTI
SHENZHEN
AOVT€STINGTECHNOLOGYCO.,IID,XUNSHAN
e!:-"Jllls,.*
TestRgport
No.SHAEC1119466001
Date:13Dec2011
Page I of4
DONGGUAN
CITYXINHA]
METALPRODUCTS
CO,,LTD
fST WEIMINGROADHENGZENG
AV.XINANCOMMUNITY
CHANGAN
TOWNDONGGUAN
CIry
GUANGDONG
PROVINCE
The following sample(s)was/lvere submittedand identifiedon behalf of the clientEas : FUSE CAp
SGS Job No. :
Compositjon:
Date of Sample Receiv€d :
Testing Poriod :
Test Requested:
Test l\rethod :
Test Results :
- SH
sPl'1-036355
H65
02 Dec201l
02Dec2011-06Dec2011
Selecl€dtest(s)as requestedby ctient.
Pleasereferto nextpage(s).
Pleasercferto nextpage(s).
Basedonthe per{ormed
testson submittedsamples,the resultsof Lead,
lvercury,
Cadmium,
Ho/€valent
dlromiumcomply
withthelimitsas setby RoHS
Diredive2011/6tEUAnnexll; recasting
2002/95/EC.
Condusion:
Signedfor and on behalfof
scs-csrc Ltd.
7Qv
FanJinqjie,JJ
ApprovedSignatory
rhtr dqj|Jd
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rdd r|h.n.ore.r .l$. Coq
r.ndd.id.{ i.v b. rF.Ei.d 'orh. Mai.nd
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swcnl..m
..Fd'FO!@
Mombo.orths SGSGrotl! (SGS8A)
TestReport
No.SHAEC1119466001 Dale:13Dec2011
P€ge 2 of 4
TestResults:
TestPad Descriotion:
S@mfi
1
No.
SGSSgmptqlD
D€cription
SHA11"194660.001
Sitvermetatbasepart
Rema*6:
(1) l mgftg=1 ppm=0.0001%
(2) MDL= tdethodDet€ctionLimit
(3) ND= NotDeteded( < t DL )
(4) '-" = NotRegulated
RoHSOir€.tiv€20t t/AtEU
TestMethod: Wth reference
to IEC62321:2008
(1)Detennination
ofCadmium
by tCp-OES.
(2)Determination
of Leadby tCp_OES.
(3) Determination
of Mercuryby lCp_OES.
(4) Determination
of Hexavatenl
Chromiumby Spottest/ Colorlmetric
l\rethodrjsinguv_Vis.
Testltem(s)
Cadmium
(Cd)
Leed(Pb)
Mercury
(Hg)
Hexavalent
Chromium
(Cr(Vj))
llllrt
ud!
100
mgks
1,000 mgKg
1,000 ms/ks
rrpl
2
2
2
@1
N
D
6
N
D
Negalive
Notes:
(1)Themaximum
pe.missible
limitis quotedfromdireciive
2011l65/EU,
Annexll
(2)o: a. Positive
meansthepresence
of CrVlonlhetest€dare€sl
b. Negativomean6theabGence
of CrVlonthe testedareas
Forcono.ionproteclioncoatingson morars:Information
on storageconditionsand productiondateof
the testedsampleis unavailable
andthusresuttsof Cr(Vl)representstatusof the sampleat the lime of
testing.
i
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TestReport
No.SMEC1119466001
Dato:13Dec2011
Page 3 of 4
ATTACHMENTS
RoHSTestingFlowChart
ol
whomade
testing:
eerson
JanShi/yoyo
wang/A
enXrao
lllj:T9
llte
z)
Nahe ot the,person
inchargeof teshng:
JeffZh€ng/ceorg;
Xu
";:iil"ff#rji:,ffi::,aissdved
totiay bypr+condiaionins-merhod
accordins
to betor/
fiowchart(Cr6.
Pb/Cd/Hg
Negative
1)AlkaliFusio./
DryAshing
2) Acjdto dissolve
Adding'1,5diphenylca.bazide
for
colordevelopment
Adding1,5diphenylcarbazide
for color
development
.h! domd
'r ud
br rD c.rts
m., &ffi.rdd
b r.m. hr cd.|@ & Ebdi'c Do6i.;it;;ii
raan.
rm n c@,.
d...on r
sthmw_rd.*r
,um_d srxrb.ddf,
rr t mco
u6.lm
hl*
M-rdDtrdr,bh
rDD.h
ka.dhnhdersl!tnl!44!@_!!!1ffi
;ni;;;
ii;:fi;ilffiii?ffifi#ffiffii
-rm,.n;;h*
;.-.^_
fr..o.iddr,br-**
ddmo..ryh@k_i.cbh.hdi*hddtrj,;.
j,!!d
f6ru$el|f
hdrt|, dam.'doi.
Fl 'Il.gi!Ai|lll839.te!t|t
t*
;-,
A red colorindicates
theprosence
of Cf*.
lf nec€ssary.confirm
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No.SHAECl119466001
Date:13 Dec2011
P a g e4 o f 4
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Date:13Oec2011
DONGGUAN
CITYXINHAI
METALPRODUCTS
CO.,LTD
fST WEIlrllNGROADHENGZENG
AV.X|NANCOtiMUNtTYCHANGAN
TOWNDONGGUAN
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PROVINCE
The following sample(s)wavu/ere submittedand identifiedon behatfof the dients as :
SGSJobNo.:
Composition:
Dateof S€mpleReceived
:
TestingPedod:
TestRequested:
Testlrothod :
TestResults:
Condusion
:
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sP11-03635s
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02 O€€,2011
- 08Dec2011
02oec2011
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Basedonthe perfo.medtestson selecledpartof submittedsample(s),th€
.esultsof Lead,Mero.ry,Cadmium,Hexavalent
chromiumcomplywiththe limits
in RoHSDireclive2011/65/EUAnnex ; recasting2002/95/EC.
Signedfor and on behalfof
scs-csTcLtd.
/Qv""'
Fan Jingjie,JJ
Approved Signatory
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No.SHAECl119466002
Page 2 of 4
TestResults:
TestPartDescdolion:
Sp€dn€nNo. SGSSemptetD Dssqipdon
1
SHAIt_194660.002 Sitvermetatptating
part
Rema*6:
(1)1 mgftg=1 ppm=0.0001%
(2) |VDL= tvethodDeteclionLimit
(3) ND = NotDetect€d( < MDL)
(4)"-' = NotRegulated
RoHSDl€ dva ZXIZ95/EC
Testllrgthod: IEC62321:2008
appticatjon
of modified
digestion
bysurtace
elchingforCadmrum,
Leact
ahd
l4erorry,anatysisby tCp-OES
Wth reference
to IEC6232i:2OOB
forHexavalent
Chrcmium
byspottest/ Coto.imetric
l\rethod.
Tesl ltem(s)
Lead (Pb)
Cadmium(Cd)
Mercury(Hg)
Hexaval€nt
(C l)
Chromium
lrpl
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Ud!
1,000
100
1,000
mg/kg
mdkg
mg/kg
10
10
10
C
0e
ND
ND
ND
Negative
Notes :
(1)Themaximum
pemissible
timitis quotedfromdirective
201.1/6tEU,
Annexll
o
(2) spot-test:
Negative= Absenceof CrVlcoating,Positive= pres€nceof CrVlcoating;
Thetestedsampleshouldbe furtherverifedby boiling-wateFexiraction
methodif the spottest resultis
Negativeor cannotb€confimed.
o Boiling-water-gxtraction:
Negalive= Absenc€of CrVlcoatingi Positive= Presenceof CrVlcoating
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in boiling-waleFextraclion
solutionis equalor greaterthan0.02mg/kgwith50
cm2samplesurfacearca.
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TestReport
'119466002
No.SHAEC1
Oate:13 Dec 2011
Page 3 of 4
ATTACHMENTS
PlatingPb/Cd/Hg/Cf TestingFtowChart
1)Nameof lhe personwhomadetesting:
YoyoWang/Allen
Xiao
2) Nameof lhe per€onin chargeof testing:
JetfZh€ng/Geo.ge
Xu
Acidwashingof
platinglayer
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mate.ial
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wasntng
Adding
1,$
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idefor
colordevelopmgnt
A red colorindicates
the pres€nceof Cfl.
lf ne@ssary,confirm
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TestReport
No.SHAECl119466002
Date:'13Dec 2011
Page 4 of 4
Samplephoto:
sHA11-194660.002
SGSauthenticate
thephotoonodginalreportonly
t" Endof Report*,*
ry e.jM b ir c.roDr cord{,oc o's
,dilrffiR<E,!{'.ddo.,@oidlirod'h!rn^rm.!'qa'r!G"!;.'{;;e;h;riiiii,ffi.;;.;'ja;;;o.conprr,,
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Test Report
Applicant:
Number : TWNC00282895
Littelfuse Philippines Inc.
LIMA Technology Center, Lipa City,
Malvar, Batangas
Date
: Oct 31, 2012
Sample Description:
One (1) group of submitted samples said to be :
Part Description
: Element (Cu CDA 102 Sn Plated)
Part Number
: 082418-001
Date Sample Received
: Oct 24, 2012
Date Test Started
: Oct 25, 2012
Test Conducted :
As requested by the applicant, for details please refer to attached pages.
Authorized By:
On Behalf Of Intertek Testing Services
Taiwan Limited
K. Y. Liang
Director
*THJ0282895*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410
Page 1 of 6
Number : TWNC00282895
Test Conducted
(Ⅰ) Test Result Summary :
Result (ppm)
Silvery Metal
Test Item
Heavy Metal
Cadmium (Cd) content
Lead (Pb) content
Mercury (Hg) content
Chromium VI (Cr6+) content (mg/kg with 50cm2)
ND
ND
ND
Negative (< 0.02)
Remarks: ppm = Parts per million based on weight of tested sample = mg/kg
ND = Not detected
<
= Less than
mg/kg with 50cm2 = milligram per kilogram with 50 square centimetre
Negative = A negative test result indicated positive observation
was not found at the time of Test.
Responsibility of Chemist : Irene Chiou / Kevin Liu
Date Sample Received
Test Period
: Oct 24, 2012
: Oct 25, 2012 To Oct 31, 2012
(Ⅱ) RoHS Limits:
Restricted Substances
Cadmium (Cd) Content
Lead (Pb) Content
Mercury (Hg) Content
Chromium VI (Cr6+) Content
Limits
0.01% (100ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
The above limits were quoted from Annex II of 2011/65/EU for homogeneous
material.
*THJ0282895*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410
Page 2 of 6
Number : TWNC00282895
Test Conducted
(Ⅲ) Test Method:
Test Item
Cadmium (Cd)
content
Lead (Pb) content
Mercury (Hg)
content
Chromium VI (Cr6+)
content
Test Method
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 7, by microwave
digestion until the tested samples are
totally dissolved and determined by
ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in annex B, by boiling water
extraction and determined by UV-Vis
Spectrophotometer.
Reporting Limit
2 ppm
2 ppm
2 ppm
0.02
mg/kg with 50cm2
Remark: Reporting limit = Quantitation limit of analyte in sample
*THJ0282895*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410
Page 3 of 6
Number : TWNC00282895
Test Conducted
(Ⅳ) Measurement Flowchart:
Test for Cd/Pb/Hg/Chromium (VI)
Reference Standard：IEC 62321 edition 1.0:2008
Sample preparation
Take sample and immerse into Aqua Regia, start to strip plating layer
Stop the stripping procedure upon color change completely
Take the Aqua solution as plating component and stripped body as substrate component
Cd/Pb/Hg
Cr
6+
Polymers /
electronics
Metal
For different
material, digest
the sample with
*1
appropriate acid
By spot test
Negative
Confirm the tested
samples are
totally dissolved
Make up with
deionized water
*2
Weigh sample
and add
alkaline
solution
Get 50cm2 sample
Definite temp.
extraction
By boiling water
extraction
Cool and filter
the extract
Analyzed by ICP-OES
Make up with deionized water and add
diphenyl-carbazide solution
Analyzed by UV-VIS
*THJ0282895*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410
Page 4 of 6
Number : TWNC00282895
Test Conducted
Remarks:
*1: List of Appropriate Acid：
Material
Polymers
Metals
Electronics
Acid Added for Digestion
HNO3,HCl,HF,H2O2,H3BO3
HNO3,HCl,HF
HNO3,HCl,H2O2,HBF4
*2: If the result of spot test is positive, Chromium VI would be determined as detected.
End of Report
This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a
recommendation for any particular course of action. Intertek does not accept a duty of care or any other responsibility to any person other than
the Client in respect of this report and only accepts liability to the Client insofar as is expressly contained in the terms and conditions
governing Intertek's provision of services to you. Intertek makes no warranties or representations either express or implied with respect to this
report save as provided for in those terms and conditions. We have aimed to conduct the Review on a diligent and careful basis and we do not
accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by
statute or otherwise, except in the event of our gross negligence or wilful misconduct.
*THJ0282895*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410
Page 5 of 6
Number : TWNC00282895
Test Conducted
Photo
*THJ0282895*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410
Page 6 of 6
Test Report
Applicant:
Number : TWNC00233542
Littelfuse Philippines Inc.
LIMA Technology Center, Lipa City,
Malvar, Batangas
Date
: Nov 25, 2011
Sample Description:
One (1) group of submitted samples said to be :
Part Description
: Yarn
Part Number
: 648106-001
Date Sample Received
: Nov 21, 2011
Date Test Started
: Nov 22, 2011
Test Conducted :
As requested by the applicant, for details please refer to attached pages.
Authorized By:
On Behalf Of Intertek Testing Services
Taiwan Limited
K. Y. Liang
Director
This report shall not be reproduced
except in full, without the written
approval of the laboratory.
Page 1 of 6
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00233542
Test Conducted
(Ⅰ) Test Result Summary :
Test Item
Result (ppm)
White Yarn
Heavy Metal
Cadmium (Cd) content
Lead (Pb) content
Mercury (Hg) content
Chromium VI (Cr6+) content
Polybrominated Biphenyls (PBBs)
Monobrominated Biphenyls (MonoBB)
Dibrominated Biphenyls (DiBB)
Tribrominated Biphenyls (TriBB)
Tetrabrominated Biphenyls (TetraBB)
Pentabrominated Biphenyls (PentaBB)
Hexabrominated Biphenyls (HexaBB)
Heptabrominated Biphenyls (HeptaBB)
Octabrominated Biphenyls (OctaBB)
Nonabrominated Biphenyls (NonaBB)
Decabrominated Biphenyl (DecaBB)
Polybrominated Diphenyl Ethers (PBDEs)
Monobrominated Diphenyl Ethers (MonoBDE)
Dibrominated Diphenyl Ethers (DiBDE)
Tribrominated Diphenyl Ethers (TriBDE)
Tetrabrominated Diphenyl Ethers (TetraBDE)
Pentabrominated Diphenyl Ethers (PentaBDE)
Hexabrominated Diphenyl Ethers (HexaBDE)
Heptabrominated Diphenyl Ethers (HeptaBDE)
Octabrominated Diphenyl Ethers (OctaBDE)
Nonabrominated Diphenyl Ethers (NonaBDE)
Decabrominated Diphenyl Ether (DecaBDE)
Halogen Content
Fluorine (F)
Chlorine (Cl)
Bromine (Br)
Iodine (I)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
591
ND
ND
Remarks: ppm = Parts per million based on weight of tested sample = mg/kg
ND = Not detected
Responsibility of Chemist : Irene Chiou / Kevin Liu / Cathy Chen
Date Sample Received
Test Period
: Nov 21, 2011
: Nov 22, 2011 To Nov 25, 2011
Page 2 of 6
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00233542
Test Conducted
(Ⅱ) RoHS Requirement:
Restricted Substances
Cadmium (Cd) Content
Lead (Pb) Content
Mercury (Hg) Content
Chromium VI (Cr6+) Content
Polybrominated Biphenyls (PBBs)
Polybrominated Diphenyl Ehters (PBDEs)
Limits
0.01% (100ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for
homogeneous material.
(Ⅲ) Test Method:
Test Item
Cadmium (Cd)
content
Lead (Pb) content
Mercury (Hg)
content
Chromium VI (Cr6+)
content
Polybrominated
Biphenyls (PBBs)
Polybrominated
Diphenyl Ethers
(PBDEs)
Halogen Content
Test Method
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 7, by microwave
digestion until the tested samples are
totally dissolved and determined by
ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in annex C, by alkaline
digestion and determined by UV-Vis
spectrophotometer.
With reference to IEC 62321 edition
1.0:2008 in annex A, by solvent
extraction and determined by GC-MSD
and further HPLC confirmation when
necessary.
With reference to IEC 62321 edition
1.0:2008 in annex A, by solvent
extraction and determined by GC-MSD
and further HPLC confirmation when
necessary.
With reference to EN 14582:2007 by
calorimetric bomb with oxygen and
determined by ion chromatography
Reporting Limit
2 ppm
2 ppm
2 ppm
1 ppm
5 ppm
5 ppm
50 ppm
Remark: Reporting limit = Quantitation limit of analyte in sample
Page 3 of 6
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00233542
Test Conducted
(Ⅳ) Measurement Flowchart:
Test for Cd/Pb/Hg/Chromium (VI)/PBBS/PBDES Contents
Reference Standard: IEC 62321 edition 1.0:2008
Sample preparation
For non-metal part
For metal part
Take sample and immerse into Aqua Regia, start to strip plating layer
Stop the stripping procedure upon color change completely
Take the Aqua solution as plating component and stripped body as substrate component
Cd/Pb/Hg
Cr
Confirm the tested
samples are
totally dissolved
Make up with
deionized water
PBBs/PBDEs
Polymers /
electronics
Metal
For different
material, digest
the sample with
*1
appropriate acid
6+
Weigh sample and
add organic solvent
By spot test
Negative
Get 50cm2 sample
By boiling water
extraction
*2
Weigh sample
and add
alkaline
solution
By Soxhlet
extraction or
Solvent extraction
Definite temp.
extraction
Cool and filter
the extract
Analyzed by ICP-OES
Concentrate the
extract and make up
with organic
solvent
Analyzed by GC-MSD
Make up with deionized
water and add diphenylcarbazide solution
Analyzed by UV-VIS
Remarks:
*1: List of Appropriate Acid：
Material
Polymers
Metals
Electronics
Acid Added for Digestion
HNO3,HCl,HF,H2O2,H3BO3
HNO3,HCl,HF
HNO3,HCl,H2O2,HBF4
*2: If the result of spot test is positive, Chromium VI would be determined as detected.
Page 4 of 6
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00233542
Test Conducted
(Ⅳ) Measurement Flowchart:
Test for Halogen Content
Reference Standard：EN 14582
Sampling/grinding or
cutting
Add absorbent in a
combustion flask &
place weighed sample in
equipment
Fill oxygen into
calorimetric bomb
Ignite then leave the
flask at room
temperature
Transfer the absorbent
into a volumetric flask
Make up with deionized
water
Analyzed by ion
chromatography
End of Report
Page 5 of 6
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00233542
Test Conducted
Photo
Page 6 of 6
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
TestReport
No. CANEC1207912202
Date:26Jun2012
Page 1 of 5
XIAMENLICHUNELECTRONICELEMENTCO.,LTD
DISTRICT,XIA['EN,,FUJIAN,P.R.C
42 2XINGLINWEST RD.,361O22,JIMEI
on behalfof theclientsas : BOSIGLASSTUBE
was^/vere
submitted
andidentified
Thefollowing
s€mple(s)
XM13901119EC-XM
SGSJobNo.:
: 18Jun2012
Dateof SampleReceived
18Jun2012'26 Jun2012
TestingPeriod:
Selectedtest(s)as requestedby client.
Test Requested:
Pleasefeferto nextpage(s)
Test Method:
Test Results:
Pleasereferto nextpage(s).
:
Conclusion
theresultsof Lead,
samples,
Basedontheoeformedtestson submitted
(PBB),
biphenyls
Polybrominated
chromium,
Hexavalent
Cadmium.
Mercury,
by
RoHS
limits
as
s€t
(PBDE)
with
the
comply
ethers
diphenyl
Polybrominated
2002/95/EC.
Annexll; recasting
2011/65/EU
Direclive
Signedfor and on behalfof
scs-csrc Ltd.
Luc'yWu
Signatory
Approved
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No.CANEC1207912202 oate:26Jun2012
TestReport
Page2 of5
Test Results:
Test Part Descriotion:
SpodmenNo.
1
O€6cfiption
SGSSamplelD
glasstube
Transparent
CAN12-079122.002
Remarks:
(1)1 mg/kg= 1 PPm= 0 0001%
Limit
(2)MDL= MethodDetection
( < l\rDL)
(3)ND= NotDetected
(4)"-" = NotRegulated
RoHSDlr€div62()l 1/85/EU
to lEc 62321:2008
TestMethod: with reference
by ICP-OES.
(1)Detemination
ofCadmium
of Leadby ICP-OES
(2)Determination
of lrerdiryby ICP-OES.
(3)Determination
MethodusinglJV_Vis'
by Colorimetdc
Chromium
of Hexavalent
(4)Determination
contentby GC-MS
(5)Determination
of PBBS/ PBDES
Testltem{s)
(Cd)
C.dmium
Lead(Pb)
[,lercury(Hg)
Chromium(crvl)
Hexavalent
Sumof PBBS
Monobromobiphenyl
Dibromobiphenyl
Tribromobiphenyl
TetrabromobiPhenyl
PentabromobiPhenyl
Hexabromobiphenyl
Heptabromobiphenyl
Octabromobiphenyl
Nonabromobiphenyl
Decabromobiphenyl
Sumof PBDES
ether
Monobromodiphenyl
MDL
Unit
Limit
2
mS/kS
100
2
1.000 mg/kg
2
1,000 mg/kg
2
1,000 mg/kg
mg/kg
1,000
5
mdkg
,
5
mg/kg
5
mdkS
5
mg/kg
5
mg/kg
5
mo/kg
5
mg/kg
5
ms/kg
5
msiks
5
mg/lq
1,000 mg/kg
5
mdkg
9u
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
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TestReport
No.CANEC1207912202
t!d!
Test ltem(sl
elhet
Dibrcmodiphenyl
ether
Tribromodiphenyl
ether
Tetrabromodiphenyl
ether
Pentabromodiphenyl
ether
Hexabromodiphenyl
ethe.
Heptabromodiphenyl
ether
Octabromodiphenyl
ethet
Nonabromodiphenyl
ether
Decabromodiphenyl
Notes :
Date:26Jun2012
ui!
IVDL
5
mgKg
5
mg/Kg
5
mg/Kg
5
mg/Kg
5
mgKg
5
mg/Kg
5
mg/Kg
5
mg/Kg
5
mg/Kg
Page3 ol 5
0!2
ND
ND
ND
ND
ND
ND
ND
ND
ND
(1) The maximumpermissiblelimitis quotedftom the directive2011/65/EU,Annexll
i
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TestReport
Date:26Jun2012
No. CANEC1207912202
Page 4 of 5
ATTACHMENTS
RoHSTestingFlowChart
'1) Nameof the peEon who madetesting:BellaWang/ CuteyYu
2) Nameof the personin chargeof testing:AdamsYu / RyanYang
methodaccordingto belowflowchart
tcEllyby pre-conditioning
3lThese
'(Cf* samolisweredissolved
test methodexcluded).
and PBBS/PBDES
Pbrcd/Hg
PBB3/PBDE8
Acid digestionwith
micrcwaveJhotplate
Positive
1) AlkaliFusion/
DryAshing
to
2)
Acid
dissolve
1,5Adding
diphenylcarbazide
color
for
development
1,t
Adding
diphenylcarbazide
color
for
development
red color
A
indicates the
presenceof CF*.
necessary,
f
with
confirm
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sGSGrouP
M6mberollho
SGS
TestReport
No. CANEC1207912202
Datet 26 Jun 2012
Page 5 of 5
Samplephoto:
cAN12-079122.002
thephotoononginalreportonly
SGSauthenticate
'** Endof Report*-
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