ICPTest_395_06 15 2013 pdf

ICP Test Report Certification Packet
Company name :
Littelfuse, Inc.
Product Series:
TE5
Product #:
395xxxxxxx Series
Issue Date:
June 15, 2013
It is hereby certified by Littelfuse, Inc. that there is neither RoHS (EU Directive 2002/95/E,
2011/65/EU)-restricted substance nor such use, for materials to be used for unit parts, for
packing/packaging materials, and for additives and the like in the manufacturing processes.
In addition, it is hereby reported to you that the parts and sub-materials, the materials to be used
for unit parts, the packing/packaging materials, and the additives and the like in the manufacturing
processes, are all composed of the following components.
Issued by:
<Global EHS Specialist>
(1) Parts, sub-materials and unit parts
This document covers the TE5 RoHS-Compliant series products manufactured by
Littelfuse, Inc.
< Raw Materials Used
Please see Table 1
(2) The ICP data on all measurable substances
Please see appropriate pages as identifed in Table 1
Remarks:
Form 585-047 Rev. A
1
2/21/06
Table 1: List of Raw Materials covered by this report
Total Parts
1
2
3
4
5
6
7
Raw Material Part Number
DRKOxxx
DRCUxxx
DRAGxxx
LOZZ194 (692213)
910-017
867-002
009116
Raw Material Description
Element
Element
Element
Wire-Solder
Cap
Socket with pin
Ceramic Paper
2
Page(s)
3-7
8-15
16-20
21-26
27-35
36-46
47-53
Test Report
Applicant:
Littelfuse Philippines Inc.
LIMA Technology Center, Lipa City,
Malvar, Batangas
Number
: TWNC00294416
Date
: Jan 17, 2013
Sample Description:
One (1) group of submitted samples said to be :
Part Description
: Copper Nickel Alloy wires
Part Number
: DRKO
Date Sample Received
: Jan 11, 2013
Date Test Started
: Jan 11, 2013
Test Conducted :
As requested by the applicant, for details please refer to attached pages.
Authorized by:
On Behalf of Intertek Testing Services
Taiwan Limited
K. Y. Liang
Director
*THJ0294416*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C.
全國公證檢驗股份有限公司
11492 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410
Page 1 of 5
Number
: TWNC00294416
Test Conducted
(Ⅰ) Test Result Summary:
Test Item
Unit
Test Method
Result
Submitted
samples
RL
ND
2
ND
2
ND
2
Negative
0.02
Heavy Metal
Cadmium (Cd) content
ppm
Lead (Pb) content
ppm
Mercury (Hg) content
ppm
Chromium VI (Cr6+) content
Remarks:
mg/kg
with
50 cm2
With reference to IEC
62321: 2008, by
microwave digestion and
determined by ICP-OES.
With reference to IEC
62321: 2008, by
microwave digestion and
determined by ICP-OES.
With reference to IEC
62321: 2008, by
microwave digestion and
determined by ICP-OES.
With reference to IEC
62321: 2008, by boiling
water extraction and
determined by UV-Vis
Spectrophotometer.
ppm = parts per million based on weight of tested sample = mg/kg
ND
= Not detected
RL
= Reporting Limit, Quantitation limit of analyte in sample
mg/kg with 50cm2 = milligram per kilogram with 50 square centimeter
Negative = A negative test result indicated positive observation was not
found at the time of Test. When the spot test showed a negative
result, the boiling water extraction procedure shall be used to
verify the result.
Responsibility of Chemist:
Date Sample Received
Test Period
Kevin Liu/ Irene Chiou
: Jan 11, 2013
: Jan 11, 2013 To Jan 15, 2013
(Ⅱ) RoHS Limits:
Restricted Substances
Limits
Cadmium (Cd) content
Lead (Pb) content
Mercury (Hg) content
Chromium VI (Cr6+) content
0.01% (100ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
The above limits were quoted from Annex II of 2011/65/EU for homogeneous material.
*THJ0294416*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C.
全國公證檢驗股份有限公司
11492 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410
Page 2 of 5
Number
: TWNC00294416
Test Conducted
(Ⅳ) Measurement Flowchart:
Test For Cd/Pb/Hg/Chromium (VI)
Reference Standard:IEC 62321 edition 1.0:2008
Sampling/grinding or cutting
Cd/Pb/Hg
Cr
6+
Polymers /
Electronics
Metal
For different
material, digest
the sample with
*1
appropriate acid
By spot test
Negative
Confirm the tested
samples are
totally dissolved
Make up with
deionized water
*2
Weigh sample
and add
alkaline
solution
Get 50cm2 sample
Definite temp.
extraction
Boiling water
extraction
Cool and filter
the extract
Analyzed by ICP-OES
Make up with deionized
water and add diphenylcarbazide solution
Analyzed by UV-VIS
*THJ0294416*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C.
全國公證檢驗股份有限公司
11492 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410
Page 3 of 5
Number
: TWNC00294416
Test Conducted
Remarks:
*1: List of Appropriate Acid:
Material
Acid Added for Digestion
Polymers
HNO3,HCl,HF,H2O2,H3BO3
Metals
HNO3,HCl,HF
Electronics
HNO3,HCl,H2O2,HBF4
*2: If the result of spot test is positive, Chromium VI would be determined as
detected.
End of Report
This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a
recommendation for any particular course of action. Intertek does not accept a duty of care or any other responsibility to any person other than
the Client in respect of this report and only accepts liability to the Client insofar as is expressly contained in the terms and conditions
governing Intertek's provision of services to you. Intertek makes no warranties or representations either express or implied with respect to this
report save as provided for in those terms and conditions. We have aimed to conduct the Review on a diligent and careful basis and we do not
accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by statute or otherwise, except in
the event of our gross negligence or wilful misconduct.
*THJ0294416*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C.
全國公證檢驗股份有限公司
11492 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410
Page 4 of 5
Number
: TWNC00294416
Test Conducted
Photo
*THJ0294416*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C.
全國公證檢驗股份有限公司
11492 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410
Page 5 of 5
Number : TWNC00296620
Test Report
Applicant:
Elschukom Elektroschutzkomponentenbau
GmbH
Gewerbestrasse 87, D-98669 Veilsdorf,
Germany
Date
: Jan 30, 2013
Sample Description:
One (1) group of submitted samples said to be :
Sample Description
: Tin plated Wires
Style / Item No.
: Please see page two to three.
Country of Origin
: Germany
Date Sample Received : Jan 23, 2013
Date Test Started
: Jan 23, 2013
Test Conducted :
As requested by the applicant, for details please refer to attached pages.
Authorized by:
On Behalf of Intertek Testing Services
Taiwan Limited
K. Y. Liang
Director
*THJ0296620*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C.
全國公證檢驗股份有限公司
11492 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410
Page 1 of 8
Number : TWNC00296620
Test Report
Sample Description:
Style / Item No.
: (A-1)101--271.0--– tin plated copper wire – Cu, Sn--%
(A-2)101--283.0--– tin plated, copper plated copper nickel alloy wire
– Elcon30, Sn--%
(A-3)101--272.0--– tin plated, copper plated steel wire – ElconF, Sn--%
(A-4)101--281.0--– tin plated, copper plated iron nickel alloy wire
– ElconD, Sn--%
(A-5)101--221.0--– tin plated copper nickel alloy wire - CuNi44, Sn--%
(A-6)101--24-.0--– tin plated, silver plated copper wire – Cu, Ag--%, Sn--%
(A-7)101--257.0--– tin plated brass wire – Cu80Zn20, Sn--%
Authorized by:
On Behalf of Intertek Testing Services
Taiwan Limited
K. Y. Liang
Director
*THJ0296620*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C.
全國公證檢驗股份有限公司
11492 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410
Page 2 of 8
Number : TWNC00296620
Test Report
Sample Description:
Style / Item No.
: (A-9)101--234.0--- tin plated silver copper alloy wire
– AgCu90, Sn--% (ElCu90, Sn--%)
(A-10)101--255.---– tin plated copper zinc alloy wire – Cu70Zn30, Sn--%
(A-11)101--229.---– tin plated copper nickel alloy wire – CuNi12, Sn--%
(A-12)101--235.---– tin plated silver copper alloy wire – Ag72Cu28, Sn--%
(A-13)101--231.---– tin plated silver
wire – Ag1000, Sn--%
(A-14)101--236.---– tin plated silver copper alloy wire
– Ag45Cu55, Sn--%(AgCu55, Sn)
(A-15)101--266.---– tin plated silver copper alloy wire
– AgCu70, Sn--%(ElCu70, Sn)
(A-16)101--238.---– tin plated silver copper alloy wire
– AgCu80, Sn--%(Elcu80, Sn)
(A-17)101--228.0--– tin plated tungsten wire – W, Sn
Authorized by:
On Behalf of Intertek Testing Services
Taiwan Limited
K. Y. Liang
Director
*THJ0296620*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C.
全國公證檢驗股份有限公司
11492 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410
Page 3 of 8
Number : TWNC00296620
Test Conducted
(Ⅰ) Test Result Summary:
Test Item
Unit
Test Method
Result
Mixed all
kinds of
metal wire
RL
ND
2
37
2
ND
2
Negative
(#)
0.02
Heavy Metal
Cadmium (Cd) content
ppm
Lead (Pb) content
ppm
Mercury (Hg) content
ppm
Chromium VI (Cr6+) content
Remarks:
mg/kg
with
50 cm2
With reference to IEC
62321: 2008, by
microwave digestion and
determined by ICP-OES.
With reference to IEC
62321: 2008, by
microwave digestion and
determined by ICP-OES.
With reference to IEC
62321: 2008, by
microwave digestion and
determined by ICP-OES.
With reference to IEC
62321: 2008, by boiling
water extraction and
determined by UV-Vis
Spectrophotometer.
ppm = parts per million based on weight of tested sample = mg/kg
ND
= Not detected
RL
= Reporting Limit, Quantitation limit of analyte in sample
mg/kg with 50cm2 = milligram per kilogram with 50 square centimeter
Negative = A negative test result indicated positive observation was not
found at the time of Test. When the spot test showed a negative
result, the boiling water extraction procedure shall be used to
verify the result.
#
= Due to the insufficient sample area, reduced total sample surface of
10 cm2 was used and the dilution factor was adjusted accordingly.
Responsibility of Chemist:
Date Sample Received
Test Period
Kevin Liu/ Irene Chiou
: Jan 23, 2013
: Jan 23, 2013 To Jan 29, 2013
*THJ0296620*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C.
全國公證檢驗股份有限公司
11492 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410
Page 4 of 8
Number : TWNC00296620
Test Conducted
(Ⅱ) RoHS Limits:
Restricted Substances
Cadmium (Cd) content
Lead (Pb) content
Mercury (Hg) content
Chromium VI (Cr6+) content
Limits
0.01% (100ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
The above limits were quoted from Annex II of 2011/65/EU for homogeneous material.
*THJ0296620*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C.
全國公證檢驗股份有限公司
11492 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410
Page 5 of 8
Number : TWNC00296620
Test Conducted
(Ⅲ) Measurement Flowchart:
Test for Cd/Pb/Hg/Chromium (VI)
Reference Standard:IEC 62321 edition 1.0:2008
Sampling/grinding or cutting
Cd/Pb/Hg
Cr
6+
Polymers /
Electronics
Metal
For different
material, digest
the sample with
*1
appropriate acid
By spot test
Negative
Confirm the tested
samples are
totally dissolved
Make up with
deionized water
*2
Weigh sample
and add
alkaline
solution
Get 50cm2 sample
Definite temp.
extraction
Boiling water
extraction
Cool and filter
the extract
Analyzed by ICP-OES
Make up with deionized
water and add diphenylcarbazide solution
Analyzed by UV-VIS
*THJ0296620*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C.
全國公證檢驗股份有限公司
11492 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410
Page 6 of 8
Number : TWNC00296620
Test Conducted
Remarks:
*1: List of Appropriate Acid:
Acid Added for Digestion
Material
Polymers
HNO3,HCl,HF,H2O2,H3BO3
Metals
HNO3,HCl,HF
Electronics
HNO3,HCl,H2O2,HBF4
*2: If the result of spot test is positive, Chromium VI would be determined as
detected.
End of Report
This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a
recommendation for any particular course of action. Intertek does not accept a duty of care or any other responsibility to any person other than
the Client in respect of this report and only accepts liability to the Client insofar as is expressly contained in the terms and conditions
governing Intertek's provision of services to you. Intertek makes no warranties or representations either express or implied with respect to this
report save as provided for in those terms and conditions. We have aimed to conduct the Review on a diligent and careful basis and we do not
accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by statute or otherwise, except in
the event of our gross negligence or wilful misconduct.
*THJ0296620*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C.
全國公證檢驗股份有限公司
11492 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410
Page 7 of 8
Number : TWNC00296620
Test Conducted
Photo
*THJ0296620*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C.
全國公證檢驗股份有限公司
11492 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410
Page 8 of 8
Test Report
Applicant:
Number : TWNC00282894
Littelfuse Philippines Inc.
LIMA Technology Center, Lipa City,
Malvar, Batangas
Date
: Nov 01, 2012
Sample Description:
One (1) group of submitted samples said to be :
Part Description
: Solder wire
Part Number
: 692213
Date Sample Received
: Oct 24, 2012
Date Test Started
: Oct 25, 2012
Test Conducted :
As requested by the applicant, for details please refer to attached pages.
Authorized By:
On Behalf Of Intertek Testing Services
Taiwan Limited
K. Y. Liang
Director
*THJ0282894*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410
Page 1 of 6
Number : TWNC00282894
Test Conducted
(Ⅰ) Test Result Summary :
Result (ppm)
Silvery Metal Wire
Test Item
Heavy Metal
Cadmium (Cd) content
Lead (Pb) content
Mercury (Hg) content
Chromium VI (Cr6+) content (mg/kg with 50cm2)
ND
84
ND
Negative (< 0.02)
Remarks: ppm = Parts per million based on weight of tested sample = mg/kg
ND = Not detected
<
= Less than
mg/kg with 50cm2 = milligram per kilogram with 50 square centimetre
Negative = A negative test result indicated positive observation
was not found at the time of Test.
Responsibility of Chemist : Irene Chiou / Kevin Liu
Date Sample Received
Test Period
: Oct 24, 2012
: Oct 25, 2012 To Nov 01, 2012
(Ⅱ) RoHS Limits:
Restricted Substances
Cadmium (Cd) Content
Lead (Pb) Content
Mercury (Hg) Content
Chromium VI (Cr6+) Content
Limits
0.01% (100ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
The above limits were quoted from Annex II of 2011/65/EU for homogeneous
material.
*THJ0282894*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410
Page 2 of 6
Number : TWNC00282894
Test Conducted
(Ⅲ) Test Method:
Test Item
Cadmium (Cd)
content
Lead (Pb) content
Mercury (Hg)
content
Chromium VI (Cr6+)
content
Test Method
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 7, by microwave
digestion until the tested samples are
totally dissolved and determined by
ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in annex B, by boiling water
extraction and determined by UV-Vis
Spectrophotometer.
Reporting Limit
2 ppm
2 ppm
2 ppm
0.02
mg/kg with 50cm2
Remark: Reporting limit = Quantitation limit of analyte in sample
*THJ0282894*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410
Page 3 of 6
Number : TWNC00282894
Test Conducted
(Ⅳ) Measurement Flowchart:
Test for Cd/Pb/Hg/Chromium (VI)
Reference Standard:IEC 62321 edition 1.0:2008
Sample preparation
Take sample and immerse into Aqua Regia, start to strip plating layer
Stop the stripping procedure upon color change completely
Take the Aqua solution as plating component and stripped body as substrate component
Cd/Pb/Hg
Cr
6+
Polymers /
electronics
Metal
For different
material, digest
the sample with
*1
appropriate acid
By spot test
Negative
Confirm the tested
samples are
totally dissolved
Make up with
deionized water
*2
Weigh sample
and add
alkaline
solution
Get 50cm2 sample
Definite temp.
extraction
By boiling water
extraction
Cool and filter
the extract
Analyzed by ICP-OES
Make up with deionized water and add
diphenyl-carbazide solution
Analyzed by UV-VIS
*THJ0282894*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410
Page 4 of 6
Number : TWNC00282894
Test Conducted
Remarks:
*1: List of Appropriate Acid:
Material
Polymers
Metals
Electronics
Acid Added for Digestion
HNO3,HCl,HF,H2O2,H3BO3
HNO3,HCl,HF
HNO3,HCl,H2O2,HBF4
*2: If the result of spot test is positive, Chromium VI would be determined as detected.
End of Report
This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a
recommendation for any particular course of action. Intertek does not accept a duty of care or any other responsibility to any person other than
the Client in respect of this report and only accepts liability to the Client insofar as is expressly contained in the terms and conditions
governing Intertek's provision of services to you. Intertek makes no warranties or representations either express or implied with respect to this
report save as provided for in those terms and conditions. We have aimed to conduct the Review on a diligent and careful basis and we do not
accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by statute or otherwise, except in
the event of our gross negligence or wilful misconduct.
*THJ0282894*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410
Page 5 of 6
Number : TWNC00282894
Test Conducted
Photo
*THJ0282894*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410
Page 6 of 6
Test Report
Applicant:
Number : TWNC00282891
Littelfuse Philippines Inc.
LIMA Technology Center, Lipa City,
Malvar, Batangas
Date
: Oct 31, 2012
Sample Description:
One (1) group of submitted samples said to be :
Part Description
: TRTE cap
Part Number
: 910-017
Date Sample Received
: Oct 24, 2012
Date Test Started
: Oct 25, 2012
Test Conducted :
As requested by the applicant, for details please refer to attached pages.
Authorized By:
On Behalf Of Intertek Testing Services
Taiwan Limited
K. Y. Liang
Director
*THJ0282891*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410
Page 1 of 9
Number : TWNC00282891
Test Conducted
(Ⅰ) Test Result Summary :
Result (ppm)
Brown Plastic
Test Item
Heavy Metal
Cadmium (Cd) content
Lead (Pb) content
Mercury (Hg) content
Chromium VI (Cr6+) content
Polybrominated Biphenyls (PBBs)
Monobrominated Biphenyls (MonoBB)
Dibrominated Biphenyls (DiBB)
Tribrominated Biphenyls (TriBB)
Tetrabrominated Biphenyls (TetraBB)
Pentabrominated Biphenyls (PentaBB)
Hexabrominated Biphenyls (HexaBB)
Heptabrominated Biphenyls (HeptaBB)
Octabrominated Biphenyls (OctaBB)
Nonabrominated Biphenyls (NonaBB)
Decabrominated Biphenyl (DecaBB)
Polybrominated Diphenyl Ethers (PBDEs)
Monobrominated Diphenyl Ethers (MonoBDE)
Dibrominated Diphenyl Ethers (DiBDE)
Tribrominated Diphenyl Ethers (TriBDE)
Tetrabrominated Diphenyl Ethers (TetraBDE)
Pentabrominated Diphenyl Ethers (PentaBDE)
Hexabrominated Diphenyl Ethers (HexaBDE)
Heptabrominated Diphenyl Ethers (HeptaBDE)
Octabrominated Diphenyl Ethers (OctaBDE)
Nonabrominated Diphenyl Ethers (NonaBDE)
Decabrominated Diphenyl Ether (DecaBDE)
Halogen Content
Fluorine (F)
Chlorine (Cl)
Bromine (Br)
Iodine (I)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
*THJ0282891*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410
Page 2 of 9
Number : TWNC00282891
Test Conducted
(Ⅰ) Test Result Summary :
Result (ppm)
Brown Plastic
Test Item
Phthalates
Di(2-ethylhexyl) Phthalate (DEHP)
Dibutyl Phthalate (DBP)
Benzyl Butyl Phthalate (BBP)
Others
Hexabromocyclododecane (HBCDD)
ND
ND
ND
ND
Remarks: ppm = Parts per million based on weight of tested sample = mg/kg
ND = Not detected
Responsibility of Chemist : Irene Chiou / Kevin Liu / Cathy Chen
Date Sample Received
Test Period
: Oct 24, 2012
: Oct 25, 2012 To Oct 30, 2012
(Ⅱ) RoHS Limits:
Restricted Substances
Cadmium (Cd) Content
Lead (Pb) Content
Mercury (Hg) Content
Chromium VI (Cr6+) Content
Polybrominated Biphenyls (PBBs)
Polybrominated Diphenyl Ehters (PBDEs)
Limits
0.01% (100ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
The above limits were quoted from Annex II of 2011/65/EU for homogeneous
material.
*THJ0282891*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410
Page 3 of 9
Number : TWNC00282891
Test Conducted
(Ⅲ) Test Method:
Test Item
Test Method
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
Cadmium (Cd) content
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
Lead (Pb) content
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 7, by microwave
digestion until the tested samples
Mercury (Hg) content
are totally dissolved and determined
by ICP-OES.
With reference to IEC 62321 edition
Chromium VI (Cr6+)
1.0:2008 in annex C, by alkaline
content
digestion and determined by UV-Vis
spectrophotometer.
With reference to IEC 62321 edition
1.0:2008 in annex A, by solvent
Polybrominated
extraction and determined by GC-MS
Biphenyls (PBBs)
and further HPLC-DAD confirmation
when necessary.
With reference to IEC 62321 edition
1.0:2008 in annex A, by solvent
Polybrominated
extraction and determined by GC-MS
Diphenyl Ethers
and further HPLC-DAD confirmation
(PBDEs)
when necessary.
With reference to EN 14582:2007 by
Halogen Content
calorimetric bomb with oxygen and
determined by Ion Chromatograph.
With reference to EN 14372: 2004, by
Phthalates
solvent extraction and determined by
GC-MS.
Hexabromocyclododecane With reference to USEPA 3540C, by
solvent extraction and determined by
(HBCDD)
GC-MSD.
Reporting Limit
2 ppm
2 ppm
2 ppm
1 ppm
5 ppm
5 ppm
50 ppm
50 ppm
10 ppm
Remark: Reporting limit = Quantitation limit of analyte in sample
*THJ0282891*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410
Page 4 of 9
Number : TWNC00282891
Test Conducted
(Ⅳ) Measurement Flowchart:
Test for Cd/Pb/Hg/Chromium (VI)/PBBS/PBDES Contents
Reference Standard: IEC 62321 edition 1.0:2008
Sample preparation
For non-metal part
For metal part
Take sample and immerse into Aqua Regia, start to strip plating layer
Stop the stripping procedure upon color change completely
Take the Aqua solution as plating component and stripped body as substrate component
Cd/Pb/Hg
Cr
Confirm the tested
samples are
totally dissolved
Make up with
deionized water
PBBs/PBDEs
Polymers /
electronics
Metal
For different
material, digest
the sample with
*1
appropriate acid
6+
Weigh sample and
add organic solvent
By spot test
Negative
Get 50cm2 sample
By boiling water
extraction
*2
Weigh sample
and add
alkaline
solution
By Soxhlet
extraction or
Solvent extraction
Definite temp.
extraction
Cool and filter
the extract
Analyzed by ICP-OES
Concentrate the
extract and make up
with organic
solvent
Analyzed by GC-MSD
Make up with deionized
water and add diphenylcarbazide solution
Remarks:
*1: List of Appropriate Acid:
Material
Polymers
Metals
Electronics
Analyzed by UV-VIS
Acid Added for Digestion
HNO3,HCl,HF,H2O2,H3BO3
HNO3,HCl,HF
HNO3,HCl,H2O2,HBF4
*2: If the result of spot test is positive, Chromium VI would be determined as detected.
*THJ0282891*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410
Page 5 of 9
Number : TWNC00282891
Test Conducted
(Ⅳ) Measurement Flowchart:
Test for Halogen Content
Reference Standard:EN 14582
Sampling/grinding or
cutting
Add absorbent in a
combustion flask &
place weighed sample in
equipment
Fill oxygen into
calorimetric bomb
Ignite then leave the
bomb at room
temperature
Transfer the absorbent
into a volumetric flask
Make up with deionized
water
Analyzed by ion
chromatography
*THJ0282891*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410
Page 6 of 9
Number : TWNC00282891
Test Conducted
(Ⅳ) Measurement Flowchart:
Test For Phthalates Contents
Reference Method: EN 14372: 2004
Sampling/grinding or
cutting
Weigh sample and add
organic solvent
By solvent extraction
Concentrate the extract
and make up with
organic solvent
Analyzed by GC-MSD
*THJ0282891*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410
Page 7 of 9
Number : TWNC00282891
Test Conducted
(Ⅳ) Measurement Flowchart:
Test For Hexabromocyclododecane (HBCDD)
Reference Standard:USEPA 3540C
Sampling/grinding or cutting
Weigh sample and add organic
solvent
By soxhlet extraction
Concentrate the extract and
make up with organic solvent
Analyzed by GC-MSD
End of Report
This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a
recommendation for any particular course of action. Intertek does not accept a duty of care or any other responsibility to any person other than
the Client in respect of this report and only accepts liability to the Client insofar as is expressly contained in the terms and conditions
governing Intertek's provision of services to you. Intertek makes no warranties or representations either express or implied with respect to this
report save as provided for in those terms and conditions. We have aimed to conduct the Review on a diligent and careful basis and we do not
accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by
statute or otherwise, except in the event of our gross negligence or wilful misconduct.
*THJ0282891*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410
Page 8 of 9
Number : TWNC00282891
Test Conducted
Photo
*THJ0282891*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410
Page 9 of 9
Test Report
Applicant:
Littelfuse Philippines Inc.
LIMA Technology Center, Lipa City,
Malvar, Batangas
Number
:
TWNC00316621
Date
:
Jun 13, 2013
Sample Description:
One (1) group of submitted samples said to be :
Part Description
: Socket with pin
Part Number
: 867-002
Date Sample Received
: Jun 05, 2013
Date Test Started
: Jun 06, 2013
Test Conducted :
As requested by the applicant, for details please refer to attached pages.
Tested Components
(1) Black plastic body
(2) Coppery metal substrate of pin
(3) Silvery plating layer of pin
Authorized by:
On Behalf of Intertek Testing Services
Taiwan Limited
K. Y. Liang
Director
*THJ0316621*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C.
全國公證檢驗股份有限公司
11492 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410
Page 1 of 13
Test Report
Number
Test Conducted
:
TWNC00316621
Test Result Summary:
Test Item
Unit
Test Method
(1)
Result
(2)
(3)
ND
ND
ND
2
ND
ND
ND
2
ND
ND
ND
2
ND
--
--
2
ND
--
--
1
--
Negative
Negative
0.02
RL
Heavy Metal
Cadmium (Cd) content
ppm
Lead (Pb) content
ppm
Mercury (Hg) content
ppm
Antimony (Sb) Content
ppm
Chromium VI (Cr6+) content
ppm
Chromium VI (Cr6+) content
mg/kg
with
50 cm2
With reference to IEC 62321:
2008, by microwave digestion
and determined by ICP-OES.
With reference to IEC 62321:
2008, by microwave digestion
and determined by ICP-OES.
With reference to IEC 62321:
2008, by microwave digestion
and determined by ICP-OES.
With reference to USEPA 3052,
by microwave digestion and
determined by ICP-OES.
With reference to IEC 62321:
2008, by alkaline digestion and
determined by UV-Vis
Spectrophotometer.
With reference to IEC 62321:
2008, by boiling water
extraction and determined by
UV-Vis Spectrophotometer.
*THJ0316621*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C.
全國公證檢驗股份有限公司
11492 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410
Page 2 of 13
Test Report
Number
Test Conducted
Test Item
Unit
Polybrominated Biphenyls (PBBs)
Monobrominated Biphenyls
ppm
(MonoBB)
Dibrominated Biphenyls
ppm
(DiBB)
Tribrominated Biphenyls
ppm
(TriBB)
Tetrabrominated Biphenyls
ppm
(TetraBB)
Pentabrominated Biphenyls
ppm
(PentaBB)
Hexabrominated Biphenyls
ppm
(HexaBB)
Heptabrominated Biphenyls
ppm
(HeptaBB)
Octabrominated Biphenyls
ppm
(OctaBB)
Nonabrominated Biphenyls
ppm
(NonaBB)
Decabrominated Biphenyl
ppm
(DecaBB)
Test Method
With reference to IEC 62321:
2008, by solvent extraction
and determined by GC-MS and
further HPLC-DAD confirmation
when necessary.
:
TWNC00316621
(1)
Result
(2)
(3)
ND
--
--
5
ND
--
--
5
ND
--
--
5
ND
--
--
5
ND
--
--
5
ND
--
--
5
ND
--
--
5
ND
--
--
5
ND
--
--
5
ND
--
--
5
*THJ0316621*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C.
全國公證檢驗股份有限公司
11492 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410
RL
Page 3 of 13
Test Report
Number
Test Conducted
Test Item
Unit
Test Method
Polybrominated Diphenyl Ethers (PBDEs)
Monobrominated Diphenyl Ethers
ppm
(MonoBDE)
Dibrominated Diphenyl Ethers
ppm
(DiBDE)
Tribrominated Diphenyl Ethers
ppm
(TriBDE)
Tetrabrominated Diphenyl Ethers
ppm
(TetraBDE)
With reference to IEC 62321:
Pentabrominated Diphenyl Ethers
2008, by solvent extraction
ppm
(PentaBDE)
and determined by GC-MS and
Hexabrominated Diphenyl Ethers
further HPLC-DAD confirmation
ppm
(HexaBDE)
when necessary.
Heptabrominated Diphenyl Ethers
ppm
(HeptaBDE)
Octabrominated Diphenyl Ethers
ppm
(OctaBDE)
Nonabrominated Diphenyl Ethers
ppm
(NonaBDE)
Decabrominated Diphenyl Ether
ppm
(DecaBDE)
Halogen Content
With reference to EN
Fluorine (F)
ppm
14582:2007 by calorimetric
Chlorine (Cl)
ppm
bomb with oxygen and
Bromine (Br)
ppm
determined by Ion
Iodine (I)
ppm
Chromatograph.
Phthalates
Di(2-ethylhexyl) Phthalate (DEHP)
ppm
With reference to EN 14372:
Dibutyl Phthalate (DBP)
ppm
2004, by solvent extraction
Benzyl Butyl Phthalate (BBP)
ppm
and determined by GC-MS.
Diisobutyl phthalate (DIBP)
ppm
Others
With reference to USEPA
Hexabromocyclododecane
ppm
3540C, by solvent extraction
(HBCDD)
and determined by GC-MS.
:
TWNC00316621
(1)
Result
(2)
(3)
ND
--
--
5
ND
--
--
5
ND
--
--
5
ND
--
--
5
ND
--
--
5
ND
--
--
5
ND
--
--
5
ND
--
--
5
ND
--
--
5
ND
--
--
5
ND
ND
ND
----
----
50
50
50
ND
--
--
50
ND
ND
ND
ND
-----
-----
50
50
50
50
ND
--
--
10
*THJ0316621*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C.
全國公證檢驗股份有限公司
11492 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410
RL
Page 4 of 13
Test Report
Number
Test Conducted
Remarks:
:
TWNC00316621
ppm = parts per million based on weight of tested sample = mg/kg
ND = Not detected
RL
= Reporting Limit, Quantitation limit of analyte in sample
mg/kg with 50cm2 = milligram per kilogram with 50 square centimeter
Negative = A negative test result indicated positive observation was not found at the time of test.
Responsibility of Chemist: Kevin Liu/ Irene Chiou/ Vico Lin
Date Sample Received
Test Period
:
:
Jun 05, 2013
Jun 06, 2013 to Jun 13, 2013
RoHS Limit
Limits
Restricted Substances
Cadmium (Cd) content
0.01% (100ppm)
Lead (Pb) content
0.1% (1000ppm)
Mercury (Hg) content
0.1% (1000ppm)
Chromium VI (Cr6+) content
0.1% (1000ppm)
Polybrominated Biphenyls (PBBs)
0.1% (1000ppm)
Polybrominated Diphenyl Ethers (PBDEs)
0.1% (1000ppm)
The above limits were quoted from Annex II of 2011/65/EU for homogeneous material.
*THJ0316621*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C.
全國公證檢驗股份有限公司
11492 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410
Page 5 of 13
Test Report
Number
Test Conducted
Measurement Flowchart:
Test for Cd/Pb/Hg/Chromium (VI)/PBBs/PBDEs Contents
Reference Standard: IEC 62321 edition 1.0:2008
:
Sample preparation
For non-metal part
TWNC00316621
For metal part
Take sample and immerse into Aqua Regia, start to strip plating layer
Stop the stripping procedure upon color change completely
Take the Aqua solution as plating component and stripped body as substrate component
6+
Cr
Weigh sample and add
organic solvent
Weigh sample and
add alkaline solution
By Soxhlet extraction or
Solvent extraction
Concentrate the extract
and make up with organic
solvent
Substrate
Cd/Pb/Hg
PBBs/PBDEs
For different material,
digest the sample with
*1
appropriate acid
Plating
Cr
6+
By spot test
Confirm the tested
samples are totally
dissolved
Definite temp.
extraction
Cool and filter the
extract
Negative
Get 50cm2 sample
Make up with deionized
water
By boiling water
extraction
Analyzed by ICP-OES
Analyzed by GC-MS
*2
Make up with deionized water
and add diphenyl-carbazide
solution
Remarks:
*1: List of Appropriate Acid:
Material
Acid Added for Digestion
Polymers
HNO3,HCl,HF,H2O2,H3BO3
Metals
HNO3,HCl,HF
Electronics
HNO3,HCl,H2O2,HBF4
Analyzed by UV-VIS
*2: If the result of spot test is positive, Chromium VI would be determined as detected.
*THJ0316621*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C.
全國公證檢驗股份有限公司
11492 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410
Page 6 of 13
Test Report
Number
Test Conducted
Measurement Flowchart:
:
TWNC00316621
Test for Heavy Metal (Sb ) Contents
Reference Method:USEPA 3052
Sampling
Weigh sample and digest in microwave
digestion oven with suitable acid
Confirm the tested samples are totally
dissolved
Transfer the digested solution and make up
with deionized water
Analyzed by ICP-OES
*THJ0316621*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C.
全國公證檢驗股份有限公司
11492 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410
Page 7 of 13
Test Report
Number
Test Conducted
Measurement Flowchart:
:
TWNC00316621
Test for Halogen Content
Reference Method:EN 14582
Sampling
Add absorbent in a combustion flask & place
weighed sample in equipment
Fill oxygen into calorimetric bomb
Ignite then leave the bomb at room
temperature
Transfer the absorbent into a volumetric flask
Make up with deionized water
Analyzed by ion chromatography
*THJ0316621*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C.
全國公證檢驗股份有限公司
11492 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410
Page 8 of 13
Test Report
Number
Test Conducted
Measurement Flowchart:
:
TWNC00316621
Test for Phthalates Contents
Reference Method: EN 14372: 2004
Sampling
Weigh sample and add organic solvent
By solvent extraction
Concentrate the extract and make up with
organic solvent
Analyzed by GC-MS
*THJ0316621*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C.
全國公證檢驗股份有限公司
11492 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410
Page 9 of 13
Test Report
Number
Test Conducted
Measurement Flowchart:
:
TWNC00316621
Test for Hexabromocyclododecane (HBCDD)
Reference Method:USEPA 3540C
Sampling
Weigh sample and add organic solvent
By soxhlet extraction
Concentrate the extract and make up with
organic solvent
Analyzed by GC-MS
*THJ0316621*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C.
全國公證檢驗股份有限公司
11492 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410
Page 10 of 13
Test Report
Number
Test Conducted
:
TWNC00316621
(1)
(2)
(1)
(2)(3)
End of Report
This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a recommendation for any particular course of action. Intertek
does not accept a duty of care or any other responsibility to any person other than the Client in respect of this report and only accepts liability to the Client insofar as is expressly contained in the
terms and conditions governing Intertek's provision of services to you. Intertek makes no warranties or representations either express or implied with respect to this report save as provided for in
those terms and conditions. We have aimed to conduct the Review on a diligent and careful basis and we do not accept any liability to you for any loss arising out of or in connection with this
report, in contract, tort, by statute or otherwise, except in the event of our gross negligence or wilful misconduct.
*THJ0316621*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C.
全國公證檢驗股份有限公司
11492 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410
Page 11 of 13
Test Report
Applicant:
Number : TWNC00282889
Littelfuse Philippines Inc.
LIMA Technology Center, Lipa City,
Malvar, Batangas
Date
: Oct 31, 2012
Sample Description:
One (1) group of submitted samples said to be :
Part Description
: Ceramic paper
Part Number
: 009116
Date Sample Received
: Oct 24, 2012
Date Test Started
: Oct 25, 2012
Test Conducted :
As requested by the applicant, for details please refer to attached pages.
Authorized By:
On Behalf Of Intertek Testing Services
Taiwan Limited
K. Y. Liang
Director
*THJ0282889*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410
Page 1 of 7
Number : TWNC00282889
Test Conducted
(Ⅰ) Test Result Summary :
Result (ppm)
White Ceramic Paper
Test Item
Heavy Metal
Cadmium (Cd) content
Lead (Pb) content
Mercury (Hg) content
Chromium VI (Cr6+) content
Polybrominated Biphenyls (PBBs)
Monobrominated Biphenyls (MonoBB)
Dibrominated Biphenyls (DiBB)
Tribrominated Biphenyls (TriBB)
Tetrabrominated Biphenyls (TetraBB)
Pentabrominated Biphenyls (PentaBB)
Hexabrominated Biphenyls (HexaBB)
Heptabrominated Biphenyls (HeptaBB)
Octabrominated Biphenyls (OctaBB)
Nonabrominated Biphenyls (NonaBB)
Decabrominated Biphenyl (DecaBB)
Polybrominated Diphenyl Ethers (PBDEs)
Monobrominated Diphenyl Ethers (MonoBDE)
Dibrominated Diphenyl Ethers (DiBDE)
Tribrominated Diphenyl Ethers (TriBDE)
Tetrabrominated Diphenyl Ethers (TetraBDE)
Pentabrominated Diphenyl Ethers (PentaBDE)
Hexabrominated Diphenyl Ethers (HexaBDE)
Heptabrominated Diphenyl Ethers (HeptaBDE)
Octabrominated Diphenyl Ethers (OctaBDE)
Nonabrominated Diphenyl Ethers (NonaBDE)
Decabrominated Diphenyl Ether (DecaBDE)
Halogen Content
Fluorine (F)
Chlorine (Cl)
Bromine (Br)
Iodine (I)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Remarks: ppm = Parts per million based on weight of tested sample = mg/kg
ND = Not detected
Responsibility of Chemist : Irene Chiou / Kevin Liu / Cathy Chen
Date Sample Received
Test Period
: Oct 24, 2012
: Oct 25, 2012 To Oct 30, 2012
*THJ0282889*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410
Page 2 of 7
Number : TWNC00282889
Test Conducted
(Ⅱ) RoHS Limits:
Restricted Substances
Cadmium (Cd) Content
Lead (Pb) Content
Mercury (Hg) Content
Chromium VI (Cr6+) Content
Polybrominated Biphenyls (PBBs)
Polybrominated Diphenyl Ehters (PBDEs)
Limits
0.01% (100ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
The above limits were quoted from Annex II of 2011/65/EU for homogeneous
material.
(Ⅲ) Test Method:
Test Item
Cadmium (Cd)
content
Lead (Pb) content
Mercury (Hg)
content
Chromium VI (Cr6+)
content
Test Method
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 7, by microwave
digestion until the tested samples
are totally dissolved and determined
by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in annex C, by alkaline
digestion and determined by UV-Vis
spectrophotometer.
Reporting Limit
*THJ0282889*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410
2 ppm
2 ppm
2 ppm
1 ppm
Page 3 of 7
Number : TWNC00282889
Test Conducted
(Ⅲ) Test Method:
Test Item
Polybrominated
Biphenyls (PBBs)
Polybrominated
Diphenyl Ethers
(PBDEs)
Halogen Content
Test Method
With reference to IEC 62321 edition
1.0:2008 in annex A, by solvent
extraction and determined by GC-MS
and further HPLC-DAD confirmation
when necessary.
With reference to IEC 62321 edition
1.0:2008 in annex A, by solvent
extraction and determined by GC-MS
and further HPLC-DAD confirmation
when necessary.
With reference to EN 14582:2007 by
calorimetric bomb with oxygen and
determined by Ion Chromatograph.
Reporting Limit
5 ppm
5 ppm
50 ppm
Remark: Reporting limit = Quantitation limit of analyte in sample
*THJ0282889*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410
Page 4 of 7
Number : TWNC00282889
Test Conducted
(Ⅳ) Measurement Flowchart:
Test for Cd/Pb/Hg/Chromium (VI)/PBBS/PBDES Contents
Reference Standard: IEC 62321 edition 1.0:2008
Sample preparation
For non-metal part
For metal part
Take sample and immerse into Aqua Regia, start to strip plating layer
Stop the stripping procedure upon color change completely
Take the Aqua solution as plating component and stripped body as substrate component
Cd/Pb/Hg
Cr
Confirm the tested
samples are
totally dissolved
Make up with
deionized water
PBBs/PBDEs
Polymers /
electronics
Metal
For different
material, digest
the sample with
*1
appropriate acid
6+
Weigh sample and
add organic solvent
By spot test
Negative
Get 50cm2 sample
By boiling water
extraction
*2
Weigh sample
and add
alkaline
solution
By Soxhlet
extraction or
Solvent extraction
Definite temp.
extraction
Cool and filter
the extract
Analyzed by ICP-OES
Concentrate the
extract and make up
with organic
solvent
Analyzed by GC-MSD
Make up with deionized
water and add diphenylcarbazide solution
Remarks:
*1: List of Appropriate Acid:
Material
Polymers
Metals
Electronics
Analyzed by UV-VIS
Acid Added for Digestion
HNO3,HCl,HF,H2O2,H3BO3
HNO3,HCl,HF
HNO3,HCl,H2O2,HBF4
*2: If the result of spot test is positive, Chromium VI would be determined as detected.
*THJ0282889*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410
Page 5 of 7
Number : TWNC00282889
Test Conducted
(Ⅳ) Measurement Flowchart:
Test for Halogen Content
Reference Standard:EN 14582
Sampling/grinding or
cutting
Add absorbent in a
combustion flask &
place weighed sample in
equipment
Fill oxygen into
calorimetric bomb
Ignite then leave the
bomb at room
temperature
Transfer the absorbent
into a volumetric flask
Make up with deionized
water
Analyzed by ion
chromatography
End of Report
This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a
recommendation for any particular course of action. Intertek does not accept a duty of care or any other responsibility to any person other than
the Client in respect of this report and only accepts liability to the Client insofar as is expressly contained in the terms and conditions
governing Intertek's provision of services to you. Intertek makes no warranties or representations either express or implied with respect to this
report save as provided for in those terms and conditions. We have aimed to conduct the Review on a diligent and careful basis and we do not
accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by
statute or otherwise, except in the event of our gross negligence or wilful misconduct.
*THJ0282889*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410
Page 6 of 7
Number : TWNC00282889
Test Conducted
Photo
*THJ0282889*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410
Page 7 of 7