Optima 8x00 Series ICP-OES Consumables Guide

Consumables and Supplies Reference Guide
Optima® 8x00 ICP-OES
Demountable Torches
Demountable design using one-piece quartz tubing for plasma and auxiliary
gas flow. Available in a wide range of styles from 0-3 slots, depending on
your application needs. Torches without slots are recommended for organic
solvents. 1-slot torches are the standard torch for aqueous solutions. 3-slot
torches are typically used for organic analysis.
Quartz Torches
# of Slots
0 1 3 Torch Cutout
Knurled Nut (Part No. N0776027)
Washer (Part No. N0776028)
O-Ring
(Part No. 09902223)
Part No.
N0781097
Torch O-Rings
Description
Qty
O-Ring Kit for Adjustable Torch
Includes:
O-Ring – 1.171 ID 0.139 WD
1
O-Ring – 0.799 ID 0.103 WD
2
O-Ring – 1.109 ID 0.139 WD
1
O-Ring – 1.046 ID 0.139 WD
1
Silicone O-Ring lube 2 grams
1
Copper Foil
(Part No. N0781097)
Part No.
N0780133
N0780130
N0780132
Ignitor Tape
Description
Copper Ignitor Tape – Qty. 50 pcs.
Flat Plate™ Torch
(see warning below)
(Part No. N0780130)
Part No.
N0780437
09902131
09902223
09921061
09921062
09200078
O-Ring
(Part No. 09921061)
Glass Holder
(Part No. N0776020)
Spacer (Part No. N0776029)
O-Ring
(Part No. 09921062)
O-Ring
(Part No. 09902131)
Torch
Coupler
WARNING: Only use PerkinElmer Flat Plate™
Torch Glassware in your Optima 8x00.
Use of other torches may damage your instrument
and may affect instrument performance.
HybridXLT™ Torch
The new ceramic/quartz hybrid design provides the highest performance for
your Optima® ICP-OES 8x00 spectrometer with an extended lifetime of up
to 10 x your current quartz torch. The HybridXLT Torch gives you a viewable
plasma compared to a full ceramic design, and is ideal for all sample types,
except organic solvents.
HybridXLT Torch
Description
HybridXLT 1-Slot Torch Part No.
N0780128
Nebulizers
PerkinElmer offers high-quality sample introduction components for a wide variety of applications.
MEINHARD® Nebulizers
Provide excellent sensitivity and precision for aqueous solutions and samples with few dissolved solids (less than 1%).
MEINHARD Nebulizers are self-aspirating and must not be used with solutions containing hydrofluoric acid. All require
an end cap for use with Ryton® Scott spray chambers.
Type
Type A Type K1 (standard)
Type K3 Application
General purpose Ar low-flow, High dissolved solids Reduced flow, and organics Part No.
00472020 N0777707 N0681574 MEINHARD Nebulizer Parts
Description Liquid-End Connector Kit, 4 mm Nebulizer Clip for MEINHARD Nebulizers Part No.
N0777414
N0777460
End Cap for Concentric Glass Nebulizers
Description
End Cap
Part No.
N0680504
MicroMist Nebulizers
Ar Flow Rate 0.7 L/min 0.7 L/min 0.7 L/min 0.7 L/min Uptake Rate 0.05 mL/min 0.1 mL/min 0.2 mL/min 0.6 mL/min Part No.
N0775349
N0775348
N0775347
N0775346
Requires Quick Disconnect Part No. N0770336.
SeaSpray Nebulizers
Air Flow Rate 0.7 L/min Uptake Rate 2 mL/min Part No.
N0775345
PEEK MiraMist® Nebulizer
The MiraMist fits regular spray chambers as a direct replacement for glass concentric nebulizers. Its features include
standard pressure (45 psi), low sample flow and enhanced parallel path design.
Description PEEK MiraMist
Uptake Rate 0.2 to 2.5 mL/min Part No.
N0775330
MicroFlow Nebulizers
MicroFlow nebulizers are constructed entirely from chemically resistant fluoropolymers, ideal for strong acids, alkalis,
organics, high salt solutions and high solid concentrations. They are resistant to clogging, are reliably self-aspirated or
pumped and produce a fine aerosol for high transport efficiency and high sensitivity.
Description PolyPro ST Nebulizer
PFA-ST Nebulizer
PFA-ST3 Microflow Nebulizer
Part No.
N0777219
N0777049
N0777676
GemCone™ and GemTip Nebulizers
Low-flow GemCones permit lower nebulizer gas flow rates, useful for spectral lines with high excitation energies and for
providing a more robust plasma. GemCone Nebulizers require an end cap for use with Ryton Scott Spray Chambers.
Description Part No.
GemCone Low-Flow Nebulizer
N0770358
GemCone High Dissolved Solids
N0690670
GemCone Sample Capillary Adapter N0371505
End Cap for GemCone Nebulizers N0680504
Quick Disconnect Tubing
N0770336
2
Nebulizers, continued
GemTip Cross-Flow II Nebulizers
Excellent general purpose nebulizer for the analysis of strong mineral acids (including HF) and samples with less than
5% dissolved solids.
Description GemTip Cross-Flow II Nebulizer for Optima 8x00
GemTip Cross-Flow II Tip Kits for Optima 8x00 O-Ring Kit for GemTip Cross-Flow Nebulizers Part No.
N0780546
N0780676
N9300067
Spray Chambers
The spray chamber is an integral part of the sample introduction system responsible for filtering the sample mist to permit the appropriate
droplet size distribution to reach the plasma.
Cyclonic Spray Chambers
Description Standard O-Ring Free HF Resistant Part No.
N0776052 N0775351
N0777496 Unifit Drain Connectors with Tubing for Cyclonic Spray Chambers
Sample Tube Size
1⁄16 in. o.d. x 0.75 mm i.d. x 700 mm 1.3 mm o.d. x 0.75 mm i.d. x 700 mm Qty
3
3
Part No.
N0774080
N0774077
Baffled Cyclonic Spray Chambers
Description Standard O-Ring Free O-Ring free for Oil Analysis (4 mm baffle)
Standard for Oil Analysis (4 mm baffle)
Standard (7 mm baffle)
Part No.
N0776053 N0775352 N0775355 N0776090
N0777036
Scott Spray Chamber
The Scott Spray Chamber is corrosion-resistant and is inert to most mineral acids including HF, aqua regia and all
organic solvents normally used in ICP analyses.
Description Part No.
Scott Spray Chamber
N0770357
Injectors and Injector Support Adapters
Alumina Injectors
Alumina injectors are corrosion-resistant to all mineral acids including HF and aqua regia. They are also used with less
volatile organic solvents, e.g., xylene.
Dimensions 0.80 mm i.d. 1.2 mm i.d. 1.2 mm i.d. (1.2 mm entire length of tube)
2.0 mm i.d. (standard with Optima instrument)
www.perkinelmer.com/supplies
Part No.
N0781009 N0781015 N0781007
N0781014
3
Injectors and Injector Support Adapters, continued
Quartz Injectors
Quartz injectors are designed for organic solvents and non-HF matrices.
Dimensions 0.80 mm i.d. 1.2 mm i.d. 1.2 mm i.d. (1.2 mm entire length of tube) 1.6 mm i.d. 2.0 mm i.d. 3.0 mm i.d. Part No.
N0781018 N0781019 N0781013
N0781016 N0781050
N0781017
Sapphire Injectors
Sapphire injectors are ideal for silicon applications.
Dimensions 2.0 mm i.d. Part No.
N0781008
Injector Support Adapter and O-Ring
Description Injector Support Adapter
Injector Support Adapter O-Ring
Part No.
N0770603
N0770438
Sample Introduction Kits
Cyclonic/Concentric Kit
Cyclonic/Concentric Kit for Optima 8x00
Includes:
1 Slot Quartz Torch
2.0 mm i.d. Alumina Injector
Glass Cyclonic Spray Chamber
Meinhard® Type K1 Nebulizer
Quartz Torch Copper Ignitor Tape – Qty. 50 pcs.
Part No.
N0780617
N0780130
N0781014
N0776052
N0777707
N0781097
Scott/Cross-Flow II Kit
Scott/Cross-Flow II Kit for Optima 8x00
Includes:
1 Slot Quartz Torch
2.0 mm i.d. Alumina Injector
Scott Spray Chamber
GemTip™ Cross-Flow II Nebulizer
Quartz Torch Copper Ignitor Tape – Qty. 50 pcs.
Part No.
N0780616
N0780130
N0781014
N0770357
N0780546
N0781097
Organics Kit
Qty.
Organics Kit for Optima 8x00
Includes:
3 Slot Quartz Torch 2
1.2 mm i.d. Alumina Injector
2
Baffled Cyclonic Spray Chamber 4mm
1
Gemcone Low-Flow Nebulizer
1
Cyclonic Spray Chamber Adapter
1
Injector Adapter Washer
1
Injector Adapter
1
Injector Adapter Nut
1
O-Ring
1
O-Ring 8.74 ID 1.78 WD
2
4
Part No.
N0780608
N0780132
N0781007
N0776090
N0770358
N0770614
N0776014
N0776091
N0776025
09902207
09921028
Purge Windows
Purge Extension Windows
ICP Model Optima 2x00/7000/8000 Optima 2x00/7000/8000 Optima 4x00/5x00/7100/7200/7300/8300 Optima 5x00/7100/7200/7300/8300 View
DV Axial DV Radial DV Axial DV Radial Part No.
09992731
N0690672
N0771116
N0770944
Pump Tubing
i.d. (mm)
Stop Colors
Standard PVC (Pkg 12)
Flared PVC Solvent Flex Viton® (Pkg 12)
(Pkg 12)
(Pkg 12)
0.19orange
red
N0695476
N0773111
orange
blue
N0773117
N0773112
green
N0777110
N0777042
0.25
0.38 orange
green
yellow
0.44
white
0.76
black
black
N0777874
N0773113
orange
yellow
0.51
0.64 orange
Santoprene® Silicone
(Pkg 12)
(Pkg 6)
N0777476
N0777711
09908587
N0777043
00473550
N0777446
N0773118
00473552
white
white
1.02N0777442N0777441
1.14
red
red
09908585
09923037
gray
gray
1.30
1.42
yellow
yellow
N0777521
1.52
yellow
blue
09923536
blue
blue
1.65
1.85
N0773115
N0773119
N0691595
N0777445
N0777444
N0777443
N0777447
green
green
N0777518
2.06 purple
purple
N0777561
purple
white
2.79
3.18
black
white
N0773116
02508080
09923448
N8122012
Autosampler Tubes
Autosampler Graduated Tubes with Red Caps
Capacity
Size
Type
Qty
Part No.
15 mL*
17 mm x 120 mm
Conical Bottom
500/50 per bag
B0193233
50 mL*
28 mm x 115 mm
Conical/Freestanding
500/25 per bag
B0193234
Autosampler Tubes
Capacity
Size
Type
Qty
Part No.
8 mL
13 mm x 100 mm
Round Bottom
1,200 bulk
N0777156
8 mL
13 mm x 100 mm
Round Bottom
1,000/250 per bag
N0777159
15 mL
17 mm x 100 mm
Round Bottom
1,200 bulk
N0777167
14 mL
Plug for 15 mL N0777167 Tubes
17 mm x 100 mm
Round Bottom
1,200 bulk
1,000/125 per bag
N0777599
N0777168
16 mL
17 mm x 100 mm
Round Bottom
1,000/125 per bag
N9301205
50 mL*
30 mm x 115 mm
Conical
500 bulk with teal flat caps N0777693
50 mL*
30 mm x 115 mm
Conical
500/50 per bag with
teal flat caps
N0777691
*Graduated
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5
PerkinElmer Pure Standards
Single-Element Standards – 1,000 mg/L
Whatever your application, you can depend on PerkinElmer Pure Standards to yield reliable, accurate results.
PerkinElmer offers a wide selection of atomic spectroscopy calibration standards. Each solution is supplied with a
comprehensive Certificate of Analysis that documents the quality and reliability. Please visit our website for a complete
listing of Atomic Spectroscopy Standards.
Element
Symbol Matrix
Pure Grade 125 mL
Part No. Aluminum Al
2% HNO3
Pure Grade 500 mL
Part No.
N9300184 N9300100
CadmiumCd 2% HNO3N9300176
N9300107
CalciumCa2% HNO3N9303763
N9300108
Chromium 2% HNO3N9300173
N9300112
CopperCu2% HNO3N9300183
Cr
N9300114
Iron Fe
2% HNO3N9303771
N9300126
Lead Pb
2% HNO3N9300175
N9300128
Mercury
Hg
10% HNO3N9300174
N9300133
Sodium
Na
2% HNO3N9303785
N9300152
Zinc
Zn
2% HNO3N9300178
N9300168
Universal Data Acquisition Standards Kit
Matrix
Contents
Vol.
Part No.
Solution Kit (Includes items listed below – 1 bottle of each) N9306225
5% HNO3
10 mg/L: Ce, Dy, Er, Eu, Gd, Ho, La, Lu, Nd, Pr, Sm, Sc, Tb, Th, Tm, Y, Yb
125 mL N9300232
5% HNO3
10 mg/L: Al, Ag, As, Ba, Be, Bi, Ca, Cd, Co, Cr, Cs, Cu, Fe, Ga, In, K, Li, Mg, Mn, Na, Ni, Pb, Rb, Se, Sr, Tl, V, U, Zn
125 mL N9300233
10% HCl/ 1% HNO3 10 mg/L: Au, Hf, Ir, Pd, Pt, Rh Ru, Te, Sb, Sn
125 mL N9300234
5% HNO3
10 mg/L: Hg 125 mL N9300253
H2O/tr HF
10 mg/L: B, Ge, Mo, Nb, P, Re, S, Si, Ta, Ti, W, Zr
125 mL N9300235
Vol.
Part No.
125 mL N9300231
125 mL N9300232
125 mL N9300233
Multi-Element Standards
Matrix
Contents
Multi-Element Solution 1
2% HNO3 10 mg/L: Be, Bi, Ce, Co, In, Mg, Ni, Pb, U
Multi-Element Solution 2
5% HNO3 10 mg/L: Ce, Dy, Er, Eu, Gd, Ho, La, Lu, Nd, Pr, Sc, Sm, Tb, Th, Tm, Y, Yb
Multi-Element Solution 3
5% HNO3 10 mg/L: Ag, Al, As, Ba, Be, Bi, Ca, Cd, Co, Cr, Cs, Cu, Fe, Ga, Hg*, In, K, Li, Mg, Mn, Na, Ni,
Pb, Rb, Se, Sr, Tl, U, V, Zn
*Supplied in separate bottle.
Multi-Element Solution 3 without MercuryN9301720
Multi-Element Solution 4
10% HCl/1% HNO3 10 mg/L: Au, Hf, Ir, Pd, Pt, Rh, Ru, Sb, Sn, Te
125 mL N9300234
125 mL N9300235
Multi-Element Solution 5
H2O/tr HF 6
10 mg/L: B, Ge, Mo, Nb, P, Re, S, Si, Ta, Ti, W, Zr
PerkinElmer Pure Standards, continued
Multi-Element Standards, continued
Matrix
Contents
Vol.
PerkinElmer Pure I
5% HNO3
400 mg/L: Tl
125 mL
200 mg/L: Bi, In, Pb
150 mg/L: Ga
100 mg/L: Al
50 mg/L: Ag, Ni
25 mg/L: Cr
20 mg/L: Cd, Co, Cu, Zn
15 mg/L: B, Fe
5 mg/L: Ba, Mn
1 mg/L: Be, Sr
Part No.
N9303940
PerkinElmer Pure IV
10% HNO3
1000 mg/L: Ag, Al, B, Ba, Bi, Ca, Cd, Co, Cr, Cu, Fe, Ga, In, 125 mL
K, Li, Mg, Mn, Na, Ni, Pb, Sr, Tl, Zn
N9303941
PerkinElmer Pure VIII
5% HNO3
100 mg/L: Al, B, Ba, Be, Bi, Ca, Cd, Co, Cr, Cu, Fe, Ga, K, 125 mL
Li, Mg, Mn, Na, Ni, Pb, Se, Sr, Te, Tl, Zn
N9303942
PerkinElmer Pure IX
5% HNO3
100 mg/L: As, Be, Pb, Cd, Cr, Ni, Se, Tl
125 mL
N9303943
Mercury
5% HNO3
125 mL
N9300223
100 mg/L
100 mg/L: Mercury in 5% HNO3
PerkinElmer Pure X
2% HNO3
35,000 ug/L: Ca
125 mL
15,000 ug/L: Mg
8,000 ug/L: Na
3,000 ug/L: K
100 ug/L: B, Fe, Mo, Sr
50 ug/L: As, Ba, Ni, V, Zn
30 ug/L: Mn
25 ug/L: Co, Pb
20 ug/L: Be, Cd, Cr, Cu
10 ug/L: Bi, Se, Tl
Mercury
5% HNO3
8 mg/L
8 mg/L: Mercury in 5% HNO3
125 mL
PerkinElmer Pure XI
5% HNO3
2500 mg/L: Zn
125 mL
900 mg/L: Cr, Pb
800 mg/L: Cu
200 mg/L: Ni
10 mg/L: Cd
Mercury
5% HNO3
5 mg/L
5 mg/L: Mercury in 5% HNO3
125 mL
PerkinElmer Pure XIII
5% HNO3
500 mg/L: Al
125 mL
250 mg/L: V
100 mg/L: As, Be, Co, Cr, Cu, Fe, Mn, Ni, Pb, Zn
25 mg/L: Cd, Se
PerkinElmer Pure XVII
15% HCL/trace HF
100 mg/L: Hf, Ir, Sb, Sn, Ta, Ti, Zr
125 mL
N9303944
N9303954
N9303945
N9303949
N9303946
N9303948
www.perkinelmer.com/supplies
7
PerkinElmer Pure Standards, continued
Interference Check Standards
Matrix
Contents
Vol.
Part No.
5,000 mg/L: Al, Ca, Mg 2,000 mg/L: Fe
500 mL N9300226
1,000 mg/L: Cr, Cu, Mn,
Ni, Ti, V
500 mL N9300228
125 mL N9300227
125 mL N9300229
Interferents A
5% HNO3 Alternate Interferents A
5% HNO3 Analytes B
5% HNO3/trTartaric Acid/tr HF 100 mg/L: Cd, Ni, Zn
60 mg/L: Sb
50 mg/L: Ba, Be, Co, Cr, Cu, Mn, V
20 mg/L: Ag
10 mg/L: As, Tl
Alternate Analytes B
5% HNO3/tr Tartaric Acid/tr HF 100 mg/L: Al, As, B, Mo, Na, Sb, Se, Tl
10 mg/L: Ca, Fe, Mg, Si
Instrument Setup Solutions
Matrix
Contents
Vol.
Part No.
Vis Wavecal Solution
2% HNO3 50 mg/L: K 10 mg/L: La, Li, Mn, Na, Sr
1 mg/L: Ba, Ca
250 mL N9302946
UV Wavecal Solution
5% HCl 100 mg/L: K, P, S 20 mg/L: As, La, Li, Mn, Mo, Na, Ni, Sc
125 mL N0681470
5% HCl 100 mg/L: K, P, S 20 mg/L: As, La, Li, Mn, Mo, Na, Ni, Sc
500 mL N0582152
Low UV Standard
2% HNO3 10 mg/L: Al, P, S 250 mL N0691580
Calcium Stray Light Standard
H 2O 10,000 mg/L: Ca 125 mL N0691581
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