ICPTest_451Sn_02 28 2013 pdf

ICP Test Report Certification Packet
Company name :
Littelfuse, Inc.
Product Series:
Nano2 Fuse
Product #:
451-Sn Series
Issue Date:
February 28, 2013
It is hereby certified by Littelfuse, Inc. that there is neither RoHS (EU Directive 2011/65/EU,
recasting 2002/95/EC)-restricted substance nor such use, for materials to be used for unit parts,
for packing/packaging materials, and for additives and the like in the manufacturing processes.
In addition, it is hereby reported to you that the parts and sub-materials, the materials to be used
for unit parts, the packing/packaging materials, and the additives and the like in the manufacturing
processes, are all composed of the following components.
Issued by:
<Global EHS Engineer>
(1) Parts, sub-materials and unit parts
This document covers the Nano2 Fuse - FA RoHS-Compliant series products
manufactured by Littelfuse, Inc.
＜ Raw Materials Used
Please see Table 1
(2) The ICP data on all measurable substances
Please see appropriate pages as identifed in Table 1
Remarks：
Pb (lead) contained in the high temperature melting solder > 85% and is categorized as
exempt under section 7a of the RoHS Annex.
Form 585-047 Rev. A
1
2/21/06
Table 1: List of Raw Materials covered by this report
Total Parts
1
2
3
4
5
6
7
Raw Material Part Number
910-238
Frequenta C221 (909-434)
082xxx
692321
087266
425809
082803
Raw Material Description
Cap
Body – Ceramic Tube
Element- 5% by weight Ag clad Cu
Solder
Adhesive - RoHS
Ink-Black - RoHS
Tin
2
Page(s)
3-10
11-39
40-44
45-50
51-60
61-69
70-78
Signature
ForQueqlion
Please
withSGS
m
3/13196 Date: 2013/01122Page:1 of 29
Test Report
GIVBH
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SampleDescription
No.
Style/ltem
Date
SampleReceiving
Period
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Te6t Result(s)
thetestresultsof Cadmium'Leacl'
samples,
ontheperfomedtestson submitted
complywiththe limitsas setby
PBDES
and
r. i""i*i"nt cnrotirln Cr(Vl),PBBS
2002/95/EC
recasting
Annexll;
directive2011/65/EU
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PARTl,lAMENo.l
CERAIVIC
Result
Uni
lrethod
MDL
Cadmium(Cd)
mg/r
2
Lead(Pb)
mg/l
2
n.d.
1000
(Hg)
Mercury
mg/|
2
n.d.
1000
Chromium
Cr(Vl)
Hexavalent
mgA
Withreference
to IEC62321:2008and
perfomedby ICP-AES.
Withreference
to IEC62321:2008and
performed
by |CP4ES.
to IEC62321:2008and
Withreference
perfomedby ICP-AES.
Withreference
to IEC62321:2008and
perfomedby UV-VIS.
to EN 14372.Analysis
Withreference
wasperformedby GC/MS.
Withreference
to EN 14372.Analysis
wEsperfomedby GC/MS.
Withreference
to EN14372.Analysis
wasperfomedby GC/MS.
to EN14372.Analysis
Withreferenc€
wasperfomedby GC/MS.
to EN 14372.Analysis
Witfrreference
performed
by GC/MS.
was
to EN14372.Analysis
with referenc€
wasperfomedby GC/MS.
With referenceto tJSEPA3550C:
bY
waspedormed
2007.Analysis
LC/MS.
No.l
n.d.
2
n.d.
1000
Test ltem(s)
o/.
(CAS
BBP(Bonzylbutylphthalate)
No.r85$8-7)
DEHP(Di-(2-ethylheryl)
phthalate)
(CASNo.r'117-81-7)
"/"
phthalate)
(CAS Yo
DIDP(Di-isodecyl
No.:26761-40-0)
phthalate)
(CAS %
DINP(Di-isononyl
No.:28553-12-0)
DNOP(Di-n-octylphthalate)(CAS
No-:117-84-0)
(CASNo.:
OBP(Dibuglphthalate)
84-74-2)
mg/ s
PerfIuorooctanesulfonates
(PFOS-Acid,
MetalSalt,Amide)
m9
PFOA(CAS No: 33547l)
to USePA3ssoOr
Wr1fr-i66rence
bY
wasPer{ormed
Analysis
2007.
0.003
n.d.
0.003
n.d.
0.01
n.d.
0.01
n.o.
0.003
n.d.
0.003
n-d.
10
n.d.
10
n.d-
0.5
n.o.
LC/MS.
to USEPA3540C
(PCBS) mg]]Kg Withreference
Biphenyls
Polychlorinated
bY
wasPerformed
Analysis
method.
(cAS No.:133s3S3)
GC/MS.
lnFsoheNsen4ktkresu|'s3h
9ffjli'J;"X,
,;'!i* ,i ;" #,";, l;6';j';; lr"
qhtddsl0*o3
Como.n! My unalhd zed anadbn
]itr.,;
Limit
'100
No.
Test Report
3t/13196Date:2013/01122
Page|3of 29
CERAI,,ITEC
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MULTIFUNKTI
Test ltem(e)
]
Unil
Polychlorinated
Terphenyls
(PCTS)
tl]
tI|||[|l
TAMIK.LUITPOLDSTMBE
15.9'1207
LAUF
Mothod
MDL
mg/k
Withreferenceto US EPA3t40C
0.5
method.
Analysis
waspedormed
by
GC/MS.
Polychlodnated
Naphthalene
mg/K With refefenc€io US EPA3540C
5
(PCNs)
method.
Analysis
wasperformed
by
GC/|MS.
Alkanes,C10-13,chloro(Sho
100
mgi/r( Withreference
to USEPA3540C
ChainChlorinatedParaffins)(CAS
method.Analysiswasperformedby
GC/MS.
No.:8553tr 1-8)
PVC
An€lysis
wasperformed
by FTIRand
FLAMETest.
Formaldehyde(CAS No.: 5040{)
mg/x Withreference
to ISO17226-1(2008).
3
Analysis
waspertormed
by HPLC/DAD.
mgil
Withreference
0.5
Monomethyl
dibromodiphenyl
to USEPA8270D
method.
Analysis
wasperformed
by
methane(DBBT)
GC/MS.
0.5
mg/r With referenceto US EPA8270D
Monomethyl
dichlorodiphenyl
Analysis
wEsperformed
by
method.
methane(Ugilec121)
GC/MS.
0.5
mg/l
With referenceto US EPA8270D
tetrachlorodiphenyl
Monomethyl
performed
by
(Ugilec141)
method.
Analysis
was
methane
GC/MS.
Halogen
50
(F) (CAS No.i
mg/l
Halogen-Fluodne
Result
No.1
n.d.
Limit
n.o.
n.d.
Negative
n.d.
n.d.
n.d.
n.o.
n.d.
14762-94-8)
(Cl)(CASNo.:
Halogen4hlorine
-15-'t\
22537
(Br)(CAsNo.:
Halogen-Bromine
100€7-32-2)
m9l
(l) (CAS No.:
Halogen-lodine
14 244-8)
mg/ s
mg/l
.
With referenceto BS EN 14582:2007
wasperfomedby lc.
J Analysis
organic-tincompounds
Tdbutyl
TinOBT)
mg/
rriphenylTin(TphT)
mg/
owi ! 'hLs13$rep9d d
rhe tftd
anys!0taEEG.!.
bred b remsamLq
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lidl!n4don
M.mnrfatoi
6 dmnl'on ont rid w
gh63ndoblg,llonsun'
ltl,/ithreferenceto DIN38407-13.
bYGC/FPD
wasperformed
Analysis
'r + i,
rl
50
n.d.
50
n.d.
50
n-o.
0.03
0.03
n.d.
n.o.
I ]r,--r
ltlv;'":'nrr.";m'.:'i.":f.l:'-tr;;'":*vi.'j
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13/13196 Date:2013/01122Page| 4of 29
ttff[t||l
MDL
Mothod
Unil
Asbestos
(CASNo.:77536-66-4) Yo
Aclinolite
(CAS
Amosite
No.: 12172-73-5\
(CASNo.:77536S7- o/o
Anthophyllite
5)
(CASNo.:12001-29-5) %
Chrysotile
(CASNo.:12001-28-4) %
Crocidolite
o/o
(CAS
Tremolite
No.:77536€8€)
EO
Withreference
to EPA600/R-93/116
method.
Analysis
waspedormed
by
(SM),Dispersion
StereoMicroscope
PolaizedLightllicroscope
Staining
(DS-PLM)andX-rayDiffraotion
(XRD).
Spectometer
(CAS No.: mg/f
1): 4-AMINODIPHENYL
92-87-1)
With referenceto LFGB82.02-2.
Analysiswas performedby GC/MS.
(CASNo.:92-872):BENZIDINE
@m^fGtoi
R6€ult
No.'l
Negative
Negative
Negalive
Negative
Negative
Negative
with reference
to LFGB82.02-2.
Analysis
wasperformed
by GC/MS.
to LFGB82.02-2.
3);4-CHLORO-O-ToLUIDINE mg/| with reference
wa6performed
by GC/MS.
(CASNo.:95€9-2)
Analysi6
reference
to
LFGB
82.02-2.
(CAS
mg4
With
4):2-NAPHTHYLAMINE
performed
Analysis
u/as
by
Gc/Ms.
No.:9159{)
to LFGB82.02-2.
(cAS mg/l
Withrefefence
5):O-AMINOAZOTOLUENE
by GC/MS.
Analysis
wasperformed
No.:97-56-3)
to LFGB82.02-2.
mg/r with reference
6):2-AMINO-4-NITROTOLUENE
wasperformed
by GC/MSAnatysis
(cAs No.r99-55-8)
to
LFGB
82.02-2.
(CASNo.: mg/l l Withreference
7): P-CHLOROANILINE
'106-47-8)
Analysis
wasperfomedby GC/MS.
to LFGB82.02-2.
(cAS
m9ng with reference
8)r2,+DIAMINOANISOLE
performed
was
by GC/MS.
Analysis
No.r615{5-4)
to LFGB82.02-2.
m9 g Withreference
9)i 4,4L
by GC/lllS.
wasperformed
Analy6is
DIAMINODIPHENYLMETHANE
(CASNo.:101-77-9)
'10):3,3-OICHLOROBENZIDINEmg/ s Withreference
to LFGB82.02-2.
perfomed
by GC/MS.
was
Analysis
(CASNo.:91-9+1)
to LFGB82.02-2.
mg/s with rcference
11): 3,3'-DIMETHOXYBENZIDINE
performed
bYGC/MS.
was
Analysis
(CASNo.:119-904)
to LFGB82.02-2.
12):3,3'-DIMETHYLBENZIDINEmg/ s Withreference
performed
bYGC/MS.
was
Analysis
(CASNo.:119-93-7)
comoaN,rl ,i, !
rh s d@ftnr 's islusd bv ft comqant sqd
Iltt]ll
RAMIK.LUITPOLDSTRABE
15,91207LAUF
mg/l
o E !e!'
sndllnsnLoi 3sue5o€
qhGandobrsargnsu
I
i+e10r,et7e
r{e6ion24tt
vRjq'Iw
3
n.d.
3
n.d.
3
n.d.
3
n.d.
3
n.d.
3
n.d.
3
n.d.
3
n.d.
3
n.d-
3
n.d.
3
n.d.
3
n.d.
Limit
No
Test RePort
CERAMTECGMBH
MULTIFUNKT
GESCHAFTSBEREICH
Testltem(s)
3i/13196Date: 2013i/01122
Page:5 ol29
lr][tttl
Unil
13):3,3'-DIMETHYL-4,4'me/(
DIAIIINODIPHENYLMETHANE
(CASNo : 838€8{)
'14):P-CRESIDINE
(2-METHOXY-mg/k
(CASNo.:
s-METHYLANILINE)
120-71-8)
(215):4,4'-METFIYLENE-B|Smg/N
(CASNo.:
CHLOROANILINE)
't01-144)
(CAs
mgiX
16)i4,4'-OXYDANILINE
No.:101€04)
(CAS
mg/N
17) 4,4'-THiODtANtLtNE
No. 13965-1)
(CASNo.:95- mlyr
18):O-TOLUIDINE
s3-4)
19):2,4-TOLUYLENEDIAMINE mg/r
(CASNo.:95-80-7)
20):2,4,s-TRIMETHYLANILINEmgn
(CASNo.:13717-7)
(CASNo.:90- m(yr
21):O-ANISIDINE
04{)
22):P-AMINOMOBENZENE
(CASNo.:60-09-3)
(CASNo.:9523):2,4-XYLIDINE
68-1)
24):2.6-X/LlDlNE(CASNo.:8762-7)
CFC's{Chlorofluoiocarbons)
Method
Result
No.l
n.d.
Withreference
to LFGB82.02-2.
Analysiswasperformedby GC/lVlS.
3
.n . d .
Withreference
to LFGB82.02-2.
Analysis
wEsperformed
by GC/MS.
3
n.d.
Withreference
to LFGB82.02-2.
Analysis
u€s performed
by GC/lllS.
3
n.d.
Wiih referenc€to LFGB82.02-2.
Analysi6was performedby GC/MS.
3
n.o.
3
n.d.
3
n.o.
3
n.d.
3
n.d.
3
n.d.
3
n.d.
3
n.d.
1
n.d.
I
n.d.
GroupI
With referenceto US EPA502'1
bY
wasperformed
method.
Analysis
1 (CASNo.:
Chlo.ofluorocarbon-'1
75€94)
mg,/
(CAsNo.:
ehbrofluorocarbon-12
75-714)
to l-JSEPA5021
mg/s Withreference
rhetm. or 6 deiwntononvandd
MDL
Withreference
to LFGB82.02-2.
Analysis
wasperformed
by GC/MS.
Withreference
to LFGB82.02-2.
Analysis
waspedormed
by GC/l\rS.
Withreference
to LFGB82.02-2.
Analysis
waspe.fomedby GC/MS.
Withreference
to LFGB82.02-2.
Analysis
wasperfomedby GC/MS.
to LFGB82.02-2.
Withreference
by GC/l\rS.
Analysis
waspedormed
to LFGB82.02-2.
mg/r Withreferenc€
wasperfomedby GC/MS.
Analysis
to LFGB82.02-2.
mg/l ) Withreference
by GC/MS.
Analysis
wa6performed
to
LFGB
82.02-2.
with
reference
mg/ s
by GC/MS.
wasperformed
Analysi6
[rs.
GCi
o9nm5|e9rcpdrt
I i l
comoan{rrr
,'ebrd ro 6 c.!(
bv
bs
c
omp'nv
rhs ddneni '' Blued
ohts.nd obBaL4^3ur
t!]
IAIVIK.LUITPOLDSTMBE'15.
9'1207
LAUF
bY
wasPerformed
Analysis
method.
GC/tVS.
Limit
l
Test Report
No
CERAMTECGMBH
MULTIFUNKT
GESCHAFTSBEREICH
Test ltern(s)
t]|||tr]
mg/N
luorocarbon-1
15 (CASNo.: mgA
Chlorof
76-15-3)
Method
With referenc€to US EPA5021
wasperformed
by
method.
Analysis
GC/MS.
to Us EPA5021
Withreference
by
Analysis
\rasperformed
method.
GC/MS.
With referenceto US EPA5021
wasperformed
by
method.
Analysis
GC/[rS.
MDL
Re-Bult
No.1
1
n.o,
1
n.d.
I
n.d.
1
n.d.
1
n.d.
lll
Group
3 (CASNo.:
Chlorof
luorocarbon-1
75-724l,
lttlt|l]
15, 9'I207LAUF
RAMIK,LUITPOLDSTRABE
lJnil
113(CASNo.: mg/x
Chlorofluorocadon7613r )
luorocadcon-'1
14(CASNo.:
Chlorof
76-14:2)
13/13196 Date: 2013/01122 Page: 6 of 29
mgn With feferenceto US EPA5021
by
Analysis
wasperformed
methodGC/t!ts.
to USEPA5021
11(CASNo.: mgn Withreference
Chlorofluorocarbon-1
bY
wasperfoamed
method.
Analysis
354-5e3)
GC/l\rs.
(cAs No.: mg/l ) with refe.enceto us EPA5021
Chlorofluorocarbon-'l'12
bY
Analysis
wasperformed
method.
76-12-0)
GC/MS.
1 (CASNo.: mg/ s nrith referenc€to US EPA5021
Chlorofluorocarbon-21
bY
wEsperformed
method.
Analysis
422-78-6)
GC/MS.
to USEPA5021
(CAS No.: mg/ s Withreference
Chlorofluorocarbon-212
bY
Analysis
wasPertormed
method.
3142-26-1)
GC/tVS.
3 (CASNo.: mg/ s With referenceto US EPA5021
luorocarbon-21
Chlorof
bY
wasperformed
method.
Analysis
2354-06-5)
n.d.
n.d.
1
n.d-
1
n.d.
cc/Ms.
(CASNo.
luorocarbon-214
Chlorof
29255-31-0)
to USEPA5021
m9/ .s Wttr reference
bY
wasPerformed
Analysis
method.
GC/MS.
1
n.d.
5 (CASNo:
luoroca6on-21
Chlorcf
42s943-2)
m9
to USEPA5021
Withreference
bY
wasPertormed
Analysis
method.
GC/tVS.
1
n.d.
un,s$oseRE ra'd ihares!fshori 'n'hEb'repPd rt
suqelt ro is ert
rh'[email protected] bv rhecomparry
,e rme ot[s 'nreiredoi onrYandm
Comorn,hy unrllTnzed one€lon
|,.e0:p3,rp''e610,r2e"
Limit
Test Report
013/13196 Date:2013101122Page:7 ot 29
No.
CERAMTECGMBH
GESCHAFTSBEREICH
IVULTIFUN
:l
T€€t ltem(s)
Unit
Chlorofluoroca.bon-216
(CAS No.:
661-57-2]
mg/K
Chlorofluorocarbon-2'17
(CAS No.:
422-86-8)
m(yK
Method
MDL
With referenceto US EPA5021
method.
Analysis
wasper{ormed
by
GC/MS.
Withreference
to USEPA5021
method.
Analysis
wEsperformed
by
GC/MS.
R€5ult
No.1
n.d-
n.d.
HCFCs
(Hydrochlorofluorocalbons)
(CASNo.:7543-4)
HCFC-21
mg/k
With referenceto US EPA5021
method.
Analysis
wa6performed
by
GC/MS.
HCFC-22
{CASNo.:7545€)
mg/k With referenceto US EPA5021
method.
Analysis
wasperformed
by
GC/MS.
(CASNo.:593-704)
HCFC-31
mg/K With referenceto US EPA5021
methodAnalysis
\ €s pedormed
by
GCiMS.
(CASNo.:354-14-3) mg/K With referenceto US EPA5021
HCFC-121
method.
Analysis
wasperfomedby
GC/r\4S.
HCFCI22(CASNo.:354-21-2) mgik Withreference
to USEPA5021
method.
Analysis
wasper{ormed
by
GC/MS,
HCFC-123(CAS No.: 306-83-2)
mg/K Withrefefence
to uS EPA5021
method.
Analysis
wasperformed
by
GC/MS.
HCFCI24(CASNo.:2837-89-0) mg/k With referenceto US EPA5021
wasperformed
by
method.
Analysis
GC/tds.
(CASNo.:359-28{)
mg/( Withreference
to USEPA5021
HCFC-131
by
method.
Analysis
wasperformed
GC/[rS.
(CAS
to USEPA502'1
No.:1d49-08-7) mg/r Withreference
HCFC-132b
wa6performed
by
method.
Analysi6
GC/MS.
c o m a N . ,r l r , r
l L il r r ( , l r i
rhs doci,mnrs 'ssrsdbt he conoanysubi*r b iu censr
,b r me or tr! 'meiurton oni and {
Co@d
d iuidid on ss6tr
al'€'don
Anvunadhorized
t tlt|ltrrrr
ERAMIK,LUITPOLDSTMBE
15, 91207LAUF
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01 id
h. (mo.n'.
rtrdon'
iinr
h hn,rondoareft
ord"r'
t,o"
sa
edtJ
don{
n.d.
n.d.
n.d.
n.o.
n.d.
n.o.
n.d.
1
n.d.
1
n.d.
Limit
TestReport
CERAMTEC
GMBH
GESCHAFTSBEREICH
MULTIFUNfiIO
913'196 Date:2013i01122Page 8c'29
,lS,91207LAUF
KERAMIK,LUITPOLDSTMBE
t|| tIIl||rIlrtfll
Test ltem(s)
(CASNo.:75-88-7)
HCFC-133a
reference
to USEPA5021
method.Analysiswas perfomed by
GC/[,ilS.
HCFC-I41b(CASNo.:1717-00€)
Withreference
to USEPA502'1
method.
Analysis
wasperformed
by
GC/[rtS.
HCFC-142b(CAS No.: 75-68-3)
With refefenceto US EPA 5021
method.Analysiswas performedby
GC/r!ts.
FC-221(CASNo.: 422-264)
FC-222(CASNo.:422-49-1)
With referenc€to US EPA5021
methodAnalysis
waspedormed
by
GC/MS.
Withreference
to USEPA5021
method.
Analysis
M€spedormed
by
GC/trs.
FC-223(CASNo.:422-52-6)
(CASNo.i422-54-8)
HCFC-224
(CASNo.:422-56-0)
HCFC-225ca
Withreference
to USEPA5021
method.
Analysis
w€sperfomedby
GC/|VS.
reference
to LJSEPA5021
method.
Analysi6
wasperfomedby
GC/MS.
referenceto US EPA5021
method.
Analysis
waspedormed
by
GC/t\rs.
(CASNo.:507-55-1)
HCFC-22scb
(CASNo.:431-87-8)
HCFC-226
(CASNo.:421-94-3)
HCFC-231
Withreference
to IJSEPA502'1
method.
Analysis
wasperformed
by
GC/MS.
With referenceto uS EPA5021
method.
Analysis
wasperformed
by
GC/MS.
with refe€nceto us EPA5021
ethod.Analysiswas performedby
HCFC-232(CAS No.:460-89-9)
to us EPA5021
ith reference
wasperformed
by
method.
Analysis
GC/tVS.
I I i
c o m o a n { i r !l
} i r l :
n i
l i
ft s duftnr
B Bsded hy rhs company&bid b ls cenea
ubied b rems 3.d con( l ns rorE doih
LEnetun tom .^ercrno alrhern
t l
l
' ! :
Do;uneft arwW
r,floru1o1
te".o'
irrm, it'
F c o m m n ' ss e
_"r.*rdbe?D'ooL(ed
rF hn,artridoem.ns
li e do!
. i . , ; r r r t 1 . , 1l3 r
TestReport
No.
CERAMTEC
GMBH
GESCFI,AFTSBEREICH
IMULTIFUN
Testltem(s)
(CASNo.:7125€4{)
HCFC-233
13/13196Date:2013l01n2
Page9 of29
t[| ||Illml
RAMIK,LUITPOLDSTRABE
15,91207
LAUF
Unit
It ethod
HCFC-244
mg/K Withreference
to USEPA5021
method.
Analysis
wasperfomedby
GC/tVlS.
m9K Withreference
to USEPA5021
method.
Analysis
wEsperformed
by
GC/MS.
mg/K Withreference
to USEPA5021
method.
Analysis
wasperfomedby
GC/MS.
mg/K With referenceto US EPA5021
method.
Analysis
wasperformed
by
GC/MS.
mg/K With referenc€to US EPA502'1
method.
Analysis
wasperformed
by
GC/tVS.
m(yK Withreference
to USEPA5021
method.
Anaiysis
wasperformed
by
GC/MS.
mg/K with reference
to us EPA5021
(CASNo.r42141-0)
HCFC-251
mg/(
(CASNo.:819-00-1)
HCFC-252
mg/N
(CASNo.:425-94-5)
HCFC-234
(CASNo.:460-92-4)
HCFC-235
HCFC-241
{CASNo.:666-27-3)
(CASNo.:460-63-9)
HCFC-242
HCFC-243{CAS No.: 4606$5)
MDL
Result
No.t
n.o,
Limit
n.d.
n.d.
n.d.
n.d.
n.d.
method.
Analysis
wasperformed
by
GC/tds.
(CASNo.:,160-35-5) mlyf
HCFC-253
(CASNo.:42G97-3)
HCFC-261
m9r
HCFC-262ICAS No.: 421-02-03)
mg/r
1.
c o m D a t u i . I,
Jl
i,
l!-ir'rrL
rh's docinsd 's $ued by rtu cmeafr subieo ro ts Gn-q
Withreference
to USEPA5021
method.
Analysis
waspedormed
by
GC/MS.
With referenceto US EPA5021
by
method.
Analysis
wa6performed
GC/MS.
With referenceto uS EPA502'1
method.
Analysis
wasperformed
by
GC/MS.
With referenceto US EPA5021
by
method.
Analysis
wasperformed
GC/MS.
With referenceto US EPA5021
by
Analysis
waspedormed
method.
GC/MS,
r'
1
n.d.
1
n.d.
1
n.d.
1
n.d.
1
n.d.
nl r l l
lonsb'.borcflcfudmenbals
i 6.;i
ti,io&'
dMs@am1
.druopm 4,,,-"
rhe ime d b deiwdidn onryard *
shs andobrisa9ns un. ; | n n ; o r c ' i o d m f u - n . e d m " i ' € - o . € F p o d ' " o " c p |
d "dP#
b441o
a
Test Report
No.
CERAMTECGMBH
GESCHAFTSBEREICH
IVULTIFUN
Testltem(s)
(CASNo.:430-55-7)
HCFC-271
13/13196 Date:2013/01122Page 10 of 29
t|| ||t]
.15.91207LAUF
RAMIK.LUITPOLDSTMBE
Unil
Method
MDL
msyK With referenceto US EPA5021
method.
Analysjs
w€sperfomedby
GC/MS.
Result
No.l
n.d.
Halona
Halon-1211
{CASNo.:353-59-3)
(CASNo.:7553-8)
Halon-1301
(CASNo.:124-73-2)
Halon-2402
CHCS(Chlorinatehvdrocarbon)
(CAS
1,1,1,2-Te'trachloroethane
No.:63G20$)
mg/K
(CASNo.:
1,1,1-Trichloroethane
71-55€)
mg/K
(CAS
1,1,2,2-Tetrachloroethane
No.:79-34-5)
m(y(
(CAS No.:
1,1,2-Tichloroethane
7940-5)
mg/N
(CASNo.:7$
1.1-Dichloroethane
34-3)
mgr
'1,1-Dichloroethene
(CAS No.: 7$
354)
(CASNo.:
1,1-Dichloropropene
5635&6)
(CASNo.:
1,2,3-Trichloropropane
96-184)
(cASNo.:
1,2-Dichloroethane
107-06-2)
mg/K
GC/frs.
n.o,
mg/K
Withreference
to USEPA5021
method.
Analysis
wasperformed
by
GC/MS.
With referenc€to US EPA5021
method.
Analysis
waspedormed
by
GC/tVS.
Withreference
to USEPA5021
Analysis
wasperformed
by
method.
GC/MS,
n.d.
With reference to US EPA 5021
method.Analysiswas perfomed by
GC/MS.
With referenceto US EPA5021
wasperformed
by
method.
Analysis
GC/MS.
to USEPA5021
mlyr Withreference
by
Analysis
wasperformed
method.
GC/MS.
to USEPA5021
mg/l
Withreference
by
Analysis
wasperformed
method.
GC/tMS.
mgn) With referenceto US EPA5021
bY
waspedormed
Analysis
method.
GC/MS.
to Us EPA5021
mg/ s Withreference
bY
wasPerformed
Analysis
method.
LrnesdheMs *bd riere5dnssfMrn h sle' dePdrcr
rh , d@manr 6 6!ued by d'e companvebr& b s aele
romar do.umirs !
and.for e &hft
ComFnv hY dnalriotredaileraion
n.d.
n.d.
With referenceto US EPA5021
mg/K method.
Analysis
wasperformed
by
GC/MS.
n.d.
1
n.d.
1
n.d.
1
n.d.
1
n,o.
1
n.d.
n.d.
n.d.
||ttl!l]
Limit
TestReport
No.
013/13196Date:2013101/22Page.11ol29
[ltl t tnm|l]l
CERAI,TTEC
G[,iBH
GESCHAFTSBEREICH
MULTIFU
Test ltem(s)
(CASNo-:
1,2-Dichloropropane
78€7-5)
'1,$Dichloropropane
(CASNo.:
A2-24-9')
ERAMIK.LUITPOLDSTRABE
15.91207LAUF
Uni
Method
mga
mg4
(CASNo.:
2,2-Dichloropropane
594-20-7)
mg/l
(CASNo.:
Carbontetrachloride
56-23-s)
m9r
(CAS No.: 7M0-3)
Chloroethane
mg/r
WithGference
to IJSEPA5021
method.
Analysi6
wasperfomedby
GC/MS.
With referenceto US EPA5021
method.
Analysis
wasperformed
by
GC/tlts.
Withrefefence
1oUSEPA5021
method.
Analysis
wasperformed
by
GC/tVS.
Withreference
to IJSEPA502'1
method.
Analysis
wasperfomedby
GC/MS.
With referenceto Us EPA5021
method.
Analysis
M€sperformed
by
I'DL
Result
1
No.l
n.d.
I
n.d.
1
n.o.
1
n.d.
'I
n.d.
1
n.d.
'I
n.o.
Limit
GC/t\rs.
(CASNo.:67€6-3)
Chloroform
m!yr
Withreference
to USEPA5021
method.
Analysis
wasperformed
by
GC/MS.
(CASNo.r74-87- mg/r Withreference
to USEPA5021
Chloromethane
wasperfomedby
method.
Analysis
3)
GC/MS,
(cAs No.: mg/l J With referenceto US EPA5021
cis.l,2-Dichlofoethene
Analysis
wEsperfomedby
method.
156-59-2)
GC/MS.
(CASNo.: mg/ I With referenceto US EPA5021
cis-1,3-Dichloropropene
Analysis
wasperfomedby
method.
10061-01-5)
GC/MS.
mg/ s With referenc€to US EPA5021
(CASNo.:
Hexachlorobutadiene
bY
wasperformed
method.
Analysis
87€8-3)
n.d.
n.d.
n-d.
GC/MS.
to USEPA5021
mg/ g Withreference
bY
wasperformed
Analysis
method.
GC/tutS.
to USEPA5021
(CAS
mg/
No.:
127letrachloroethene
s Withreference
bY
wasperformed
method.
Analysis
184)
GC/|V]S.
MethyleneChlodde(CAS No.: 75
09-2)
comanvnli I Ll lL I
Ths dornmnr s 'esuedby rh companysubid b coent
$. tme or {s 'nraten' on onlv and w
shs andoDroarlds!f
Anydna!ho';ed aiieraton
ComDanv
1
n.d.
1
n.d.
Ie"!]ri..,.i'lpl"l:,!":i:l:{:.ifi
, .".d;.-+"* -i- "-d;; :6 m"o es.d ""F-.oa #E;;?:.:!tTi.?;:J"1i".+
;l,i.i::";:ifl%".j
i:?;i':;
i:mr *i:a'*;il;'';*;i:u*,1't;';': :li "i";":%
r$1""1
lil:r'"fjlrri#::
J.:J
l;fJ*;;i:l;,:::,i.
";;;;"":::.r.'i.:lil*:',;3'#;;;"qj€'"':
TestReport
No.:
'f3/13196Date:2013/01
n2
c
CERAIVTEC
GMBH
GESCHAFTSBEREICH
I,TULTIFUN
Testltem(s)
Page:12ot29
ll|
|l[I|l
tttt||]
RAMIK.LUITPOLDSTMBE
15.9'I207LAUF
Unil
tulethod
MDL
(CAS
trans-1,2-Dichloroethene
No.r156€0-5)
mg/K
Withreference
to USEPA5021
\.'/as
performed
method.
Analysis
by
(CAS
trans-1,3-Dichloropropene
No.:10061-02€)
mg/K
Trichloroethylene
(CASNo.:79016)
mg/K
With referenceto US EPA5021
methodAnalysis
wasperformed
by
GC/MS.
With referenc€to US EPA5021
method.
Analysis
wasperformed
by
Result
No.1
n.d.
Limit
GC/l\rs.
n.d.
n.d.
GC/t\rs.
Sumof PBEI5
Monobromobiphenyl
Dibromobiphenyl
mg/K
mg/x
5
mgk
n.d.
n.d.
n.d.
n.d.
n.d.
n.d-
Tribromobiphenyl
Tetrabromobiphenyl
Pentabromobiphenyl
mgr(
m!/x
mgI(
5
Hexabromobiphenyl
mg/t(
mg/x
mg/x
5
5
5
n.d.
Heptabromobiphenyl
Octabromobiphenyl
Nonabromobiphenyl
Dec€bromobiphenyl
Sum of PBDE9
Monobromodiphenyl
ether
Dibromodiphenyl
ether
Tribromodiphenyl
ether
Tetrabromodiphenyl
ether
Pentabromodiphenyl
ether
Hexabromodiphenyl
ether
Heptabromodiphenyl
ether
Octabromodiphenyl
other
ether
Nonabromodiphenyl
ether
Decabromodjphenyl
5
n.o.
coft,nrtrlf
fts dclmnr
5
5
mg/N
mg/N
mg/x
Withreference
to IEC62321:2008and
performed
by GC/MS.
mg/r
5
5
5
mg/l
mg/N
mg/l
mgn
mg/|
mgn
mg/r
osnlh9|ejrcpdrc'
r
l;
l -ll \ 1
1,i
sBsued bv 'he aomoanv subid d is Genq
- 1
-md.ions or >eM- o,itu e{e.
;.dDrrdoB
i;n,
TheLomoa\<
{"
Pd td'
m
-/o
n.d.
n.d.
n.dn.d.
n.o,
n.d.
5
5
n.d.
5
5
5
mg4
n.d.
n.d.
5
mlyl
1000
n.d.
n.d.
n.d.
n.d.
n.d.
1000
Test Report
E/2013i/'1
3'196
CERAMTEC
GMBH
GESCFI,AFTSBEREICH
MULTIFUNKT
Date: 2013101122Paoe: 13 of 29
|r][ttl][||ta|ll
'15,9'1207
IK,LUITPOLDSTMBE
LAUF
Note :
'l- mgrkg= ppm;
0.1M%= 1o00ppm
2. n.d. = Not Detec{ed
3. MDL= MethodDetection
Limit
=
4. " " NotRegulated
(NoUnit)
analysis
5- *' = Qualitative
=
/ Positive Detectable
6. Negative Undetectable
qual
7. Testingrangeof asbestos
analysis
is fiom lessthan0.1%to '1000/6.
Thejudgment
critedon:
asbestos
fibe6
beingfound is shownas "Positive';
fibersnolbeingfoundis 6hownas "Negalive".
PFOSReferenceInformation: POPS- (
757t20.to
parationsin concentrations
products
(1oppm),
OutlawingPFOSas suo$ancesor
above0.0010/6
in semi-finished
or
in textilesor othercoatedmaterials
abovelpg/m'.
articles or pads at a levelabove0.1 1000ppm),
rhisdodme
6 sued bYthe compary subled ro b G
lbled b r4ms md
diunidon's<des
:iI. l.t ,i!!t.
t . i t. r- r" u
" s " , e p ' ep.dedowddar
-d"-;.,jdDho|'eod'o'Jor''0A'dss
c6d,irisorse
6{ errennld o oroio 5r"r'eDo-r
oi'rmqh d
dih;;"r
"-,s'
{^e:91: q'ilj19-r-:
I
,::;:'";,:3+:":",r:*":k*'tl.g;.':t*'",;t"t";;;".1ti;l"i:T,$I
inituclrons I any rh. compants s e
"1;is?r1""',119%ii
b pon\b,it !,o
;;'
l;::i;.t;.o;;:;;
r:i''..*oo"-".-n'i.doa-f.e1D'F'"ot!d@e
rc.r'd{r\do
.-.doP\ ol
TestReport
13/13't96Date| 2013101122Page: 14of 29
CERAMTEC
GMBH
15.91207IAUF
GESCHAFTSBEREICH
IVULTIFUNKTIOKERAMIK.LUITPOLDSTMBE
totallyby pre-conditioning
methodaccording
to belowflort/chart.
Thesesamplesu/€re
1)
I|| tII|[||lttlll
( Cre test method
uded)
Yang
2l Nameof the person mademeasurement:
Climbgreat
person
charge
of
measurement
Troy
Chang
Name
the
3)
of
SampleMeasurement
Addappropdate
amount
reagent
of digestion
Acid digestionby suitable
depended
on different
sam
(asbelowtable)
material
Heatto appropriate
temperatureto etfact
1) AlkaliFusion
2) HCltodissolve
Cool,filterdigestate
through
filter
AdddiphenyFcarbazide
for colordevelopment
solder
steel,copper,aluminum,
measure
theabsorbance
at 540 nm by UV-VIS
H,SO4,HrOr,HNO3,HCI
Addedappropriatereagentto total
digestion
add alkalinedigestionreagentand heatto 90-95 C.
( 1)For nonfi
licmaterial,
(2) For metall material,add purewaterand heatto boiling.
como.iY,rlf
r,'
I
;
l
bled b rem' !d
rhe tm
ot s meiwilononvaidw
c!
sh6 aid obrioatlonsd
lY i illl'f."li
i"Ii.i5,iiTl''il
LTiAru".#i[ffi31**"":f*fl"".:5?1tl"t!"#f*s]trffii"J:!?1'wir##]i'xli.il"
Bli':r**l*r*:.,*.":*lr*E::x#Jr$ffJiiir"tf'ff?i,i,ilfl,tffi*:x:"'s'"?*"":l1l1T
*i$##:#f:is#iiHi#$"?Ji.}qfi"r**d$$$:T
#f";*tft
No:
Test Report
CERAI'TEC GlllBH
GESCHAFTSBEREICH
MULTIFUNKTIO
PFOA/PFOS
I
r
Nameoft
Nameoft
Page:15of 29
3/13196 Date:2013/01122
t|| |l[]
RAMIK.LUITPOLDSTRABE
15,91207LAUF
procedur€
flow chartof Ultrasonicextraction(LCymS)
person
whomademeasurementr
Roman
Wong
person
incharge
of measurement
TrcyChang
ole extraction bv ljltrasonic extr€ction
method:USEPA3550C)
{Reference
Concentrate/Dilute
Extracted
solution
Analysiswas performedby LC/IIS
' , ' ] ' ! .
. 1 ' r r
"
bled'o r.m6 ad co
Memni(aionsidilnddon isue5 dei ;'ii;;:;;
;;;.i;N
he !m or E ireiuironoivand 0
!rt
shc rnd obriqargm
h;ld7t 6 a d;""*d
;fr rhe
tltttll
Test Report
0f3/13196 Dale:2013t01t22Page 16ot29
CERAMTECGI/|BH
GESCHAFTSBEREICH
MULTIFUNKTIO
ll|
|l [ttttll
RAMIK,LUITPOLDSTRABE
15. 91207LAUF
PCTSanalylical flow chart
ofthepersonwhomademeasurement:
BarryTseng
ofthepersonin chargeof measurement:
TfoyChang
Sampleprekealrnent
Sampleextraction
by organicsolveni
Concenhate/Dilute
theextracled
solution
AnalysiswEsperformedby GC/MS
rr / ,
c o m a N . rr !
I
rh s d@ftir : issEd byrhecompant>uqeqb s Geir
d iu' sd'd o^ 5q6
shEmd drs*lm(
(omoany
arreBlon
tuYunauhtrzed
de
q1rllff.:r'r(e
tie!
pemLsson
pnorwdten
oirhe
eeot i iuI witrour
eprcdu@d
Jliif..s)repon€motbe
gtr;""#.:ri.,i#?;:,liT;
S
i;:.1'Xgir' :l-.",":"'.::,3'i;f::1.?
1";;;";g;:1;."
:?;.?g'";;il[';'j
::i,::
:jT: $ri"ei:;5:l- : k*r:t',."r.Trtrl'%
ff ,"::;:#" ;;
Test Report
01A1Y
CERAI\4TEC
GlilBH
GESCHAFTSBEREICH
MULTIFU
I
I
Firsttestingprocess
Optionalscreenp
Confirmationproce6s
Oate.2013l01l22 Page:17ol 29
:I||||I[]
RAMIK,LUITPOLDSTRABE
15,91207LAUF
PBB/PBDE
analyticalFLOWCHART
of thepersonwhomademeasurement:
RomanWong
person
ofthe
in chargeof measurement:
TfoyChang
-_r-
fs"'pe---_-]
s""tr"p,"G#t-------r-----Screenanalysis
""""""'f
""""""
Sampleextraction/
Soxhletmethod
Concentrate/Dilute
Extractedsolution
Analysisby GC/MS
lssueReport
ft6
docnmd
sFEued byrhe(o@any
ubjed
oBG'
-.*riiad*dsd
fi";da.i;hhi,i
d iunid on kussd6h ;'i;;'
Dh{on, |i , 1PLomo4 3 se
-1'
' do*
rf
rF
hn*donooa
LdnEadrnhoms^€dtnq alrher n
ftmdor6d,nd
r
', r,
r f i N rl
ttt]t
TestReport
3/13196 Date: 2013/01122Page 18o129
CERAMTEC
GMBH
GESCHAFTSBEREICH
IVULTIFUN
r
ttl [tt]
RAMIK,LUITPOLDSTRABE
15,91207LAUF
PCBSanalyticalflow chart
I
N
r N
e of the perconwhomademeasurement
BarryTseng
e ofthe personin chafgeof measurement:
TroyChang
Samplepretreatment
Sampleextractionby organicso'vent
Concentrate/Dilute
the extrac{ed6olution
AnalysiswEs pedormedby GC/MS
:
i..
+r
-.1
T!'i!'!r!:!
r"l-';:iif*, "1":;1".";
i""i'r3"i'.t;t."
"":{i;3.""T'lli';* 3.1.v{f;il..i
,ii!'i, i.lla",i
a"-.n
j l'i i ;-.p
l .nnoi be *o,m
"d" ep r,
' s10
'o
"t"r
app'oilr or 0 P
l
Test Report
CERAIVTECGMBH
GESCHAFTSBEREICH
[,ilULTIFU
013'/13196Date: 2013t01t22 page: i9 of 29
IK,LUITPOLDSTMBE
15,91207LAUF
otinat€d PaEffins analyticalflow chart
e ofthe personwhomademeasurement
BarrvTseno
e ofthe personInchargeof measurement:
troy Cnaig
Samplepretreatment
Sampleedractionby organicsolvent
Concentrate/Dilute
theextracled
solution
Analysis
wasperfomedby cCYI\rS
:"|.tl::ii,t.{itl":ij,.ii:i li
;dhed
hd 'domrion conrainadh
rcspoisb]iyblobcislandlhsd
llfl||[l
[t
]rl
TestReport
13/13'196 Date:2013/01t22 page| 20 of 29
CERAIVTEC
GIVBH
GESCHAFTSBEREICH
IVULTIFUN
RAMIK.LUITPOLDSTMBE
15, 91207LAUF
tl||||l|||l
tlow chartfor determination
of Asb6tos
e of the personwhomademeasurefientVictorKao
e ofthe personin chargeof measuremer
: WendvWd
I
I
Refercn6e
EPA500/R-S3/fi61
Transportalion
andStoEge
Prcparalion
of pimaryanalyticat
sample
Examrnation
by stereorn
icrcscope(SM)
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013/'13'196Date:2013101122Page:21 oI 29
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3/13196 Date:2013/01n2 Page 22 of 29
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ofthe per6on
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ofthe personin chargeof measurement:
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13/13196Date:2013/01122
Page:26of 29
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1Y13196 Date:2013/01122
Page 28of 29
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Test Report
Applicant:
Number : TWNC00249177
Littelfuse Philippines Inc.
LIMA Technology Center, Lipa City,
Malvar, Batangas
Date
: Mar 26, 2012
Sample Description:
One (1) group of submitted samples said to be :
Part Description
: Silver Clad Cu Wire with 5% Ag
Part Number
: 082xxx(082375)
Date Sample Received
: Mar 22, 2012
Date Test Started
: Mar 22, 2012
Test Conducted :
As requested by the applicant, for details please refer to attached pages.
Authorized By:
On Behalf Of Intertek Testing Services
Taiwan Limited
K. Y. Liang
Director
This report shall not be reproduced
except in full, without the written
approval of the laboratory.
Page 1 of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00249177
Test Conducted
(Ⅰ) Test Result Summary :
Test Item
Heavy Metal
Cadmium (Cd) content
Lead (Pb) content
Mercury (Hg) content
Chromium VI (Cr6+) content (mg/kg with 50cm2)
Remarks: ppm =
ND =
<
=
mg/kg
Result (ppm)
Silvery Wire
ND
ND
ND
Negative (< 0.02)
Parts per million based on weight of tested sample = mg/kg
Not detected
Less than
with 50cm2 = milligram per kilogram with 50 square centimetre
Responsibility of Chemist : Irene Chiou / Kevin Liu / Cathy Chen
Date Sample Received
Test Period
: Mar 22, 2012
: Mar 22, 2012 To Mar 26, 2012
(Ⅱ) RoHS Requirement:
Restricted Substances
Cadmium (Cd) Content
Lead (Pb) Content
Mercury (Hg) Content
Chromium VI (Cr6+) Content
Limits
0.01% (100ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for
homogeneous material.
Page 2 of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00249177
Test Conducted
(Ⅲ) Test Method:
Test Item
Cadmium (Cd)
content
Lead (Pb) content
Mercury (Hg)
content
Chromium VI (Cr6+)
content
Test Method
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 7, by microwave
digestion until the tested samples are
totally dissolved and determined by
ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in annex B, by boiling water
extraction and determined by UV-Vis
Spectrophotometer.
Reporting Limit
2 ppm
2 ppm
2 ppm
0.02
mg/kg with 50cm2
Remark: Reporting limit = Quantitation limit of analyte in sample
Page 3 of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00249177
Test Conducted
(Ⅳ) Measurement Flowchart:
Test For Cd/Pb/Hg/Chromium (VI)
Reference Standard：IEC 62321 edition 1.0:2008
Sampling/grinding or cutting
Cd/Pb/Hg
Cr
Polymers /
Electronics
Metal
For different
material, digest
the sample with
*1
appropriate acid
By spot test
Negative
Confirm the tested
samples are
totally dissolved
Make up with
deionized water
6+
*2
Weigh sample
and add
alkaline
solution
Get 50cm2 sample
Definite temp.
extraction
Boiling water
extraction
Cool and filter
the extract
Analyzed by ICP-OES
Make up with deionized
water and add diphenylcarbazide solution
Remarks:
*1: List Of Appropriate Acid：
Material
Polymers
Metals
Electronics
Analyzed by UV-VIS
Acid Added For Digestion
HNO3,HCl,HF,H2O2,H3BO3
HNO3,HCl,HF
HNO3,HCl,H2O2,HBF4
*2: If the result of spot test is positive, Chromium VI would be determined as detected.
End of Report
Page 4 of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00249177
Test Conducted
Photo
Page 5 of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Test Report
Applicant:
Number : TWNC00285771
Littelfuse Philippines Inc.
LIMA Technology Center, Lipa City,
Malvar, Batangas
Date
: Nov 16, 2012
Sample Description:
One (1) group of submitted samples said to be :
Part Description
: Solder (Pb is ≥ 90%)
Part Number
: 692321
Date Sample Received
: Nov 12, 2012
Date Test Started
: Nov 13, 2012
Test Conducted :
As requested by the applicant, for details please refer to attached pages.
Authorized By:
On Behalf Of Intertek Testing Services
Taiwan Limited
K. Y. Liang
Director
*THJ0285771*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410
Page 1 of 6
Number : TWNC00285771
Test Conducted
(Ⅰ) Test Result Summary :
Result (ppm)
Silvery metal
Test Item
Heavy Metal
Cadmium (Cd) content
Lead (Pb) content
Mercury (Hg) content
Chromium VI (Cr6+) content (mg/kg with 50cm2)
ND
934557
ND
Negative (< 0.02)
Remarks: ppm = Parts per million based on weight of tested sample = mg/kg
ND = Not detected
<
= Less than
mg/kg with 50cm2 = milligram per kilogram with 50 square centimetre
Negative = A negative test result indicated positive observation
was not found at the time of Test.
Responsibility of Chemist : Irene Chiou / Kevin Liu
Date Sample Received
Test Period
: Nov 12, 2012
: Nov 13, 2012 to Nov 16, 2012
(Ⅱ) RoHS Limits:
Restricted Substances
Cadmium (Cd) Content
Lead (Pb) Content
Mercury (Hg) Content
Chromium VI (Cr6+) Content
Limits
0.01% (100ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
The above limits were quoted from Annex II of 2011/65/EU for homogeneous
material.
*THJ0285771*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410
Page 2 of 6
Number : TWNC00285771
Test Conducted
(Ⅲ) Test Method:
Test Item
Cadmium (Cd)
content
Lead (Pb) content
Mercury (Hg)
content
Chromium VI (Cr6+)
content
Test Method
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 7, by microwave
digestion until the tested samples are
totally dissolved and determined by
ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in annex B, by boiling water
extraction and determined by UV-Vis
Spectrophotometer.
Reporting Limit
2 ppm
2 ppm
2 ppm
0.02
mg/kg with 50cm2
Remark: Reporting limit = Quantitation limit of analyte in sample
*THJ0285771*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410
Page 3 of 6
Number : TWNC00285771
Test Conducted
(Ⅳ) Measurement Flowchart:
Test For Cd/Pb/Hg/Chromium (VI)
Reference Standard：IEC 62321 edition 1.0:2008
Sampling/grinding or cutting
Cd/Pb/Hg
Cr
6+
Polymers /
Electronics
Metal
For different
material, digest
the sample with
*1
appropriate acid
By spot test
Negative
Confirm the tested
samples are
totally dissolved
Make up with
deionized water
*2
Weigh sample
and add
alkaline
solution
Get 50cm2 sample
Definite temp.
extraction
Boiling water
extraction
Cool and filter
the extract
Analyzed by ICP-OES
Make up with deionized
water and add diphenylcarbazide solution
Analyzed by UV-VIS
*THJ0285771*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410
Page 4 of 6
Number : TWNC00285771
Test Conducted
Remarks:
*1: List of Appropriate Acid：
Acid Added for Digestion
Material
Polymers
HNO3,HCl,HF,H2O2,H3BO3
Metals
HNO3,HCl,HF
Electronics
HNO3,HCl,H2O2,HBF4
*2: If the result of spot test is positive, Chromium VI would be determined
as detected.
End of Report
This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a
recommendation for any particular course of action. Intertek does not accept a duty of care or any other responsibility to any person other than
the Client in respect of this report and only accepts liability to the Client insofar as is expressly contained in the terms and conditions
governing Intertek's provision of services to you. Intertek makes no warranties or representations either express or implied with respect to this
report save as provided for in those terms and conditions. We have aimed to conduct the Review on a diligent and careful basis and we do not
accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by statute or otherwise, except in
the event of our gross negligence or wilful misconduct.
*THJ0285771*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410
Page 5 of 6
Number : TWNC00285771
Test Conducted
Photo
*THJ0285771*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410
Page 6 of 6
Test Report
Applicant:
Number : TWNC00285781
Littelfuse Philippines Inc.
LIMA Technology Center, Lipa City,
Malvar, Batangas
Date
: Nov 19, 2012
Sample Description:
One (1) group of submitted samples said to be :
Part Description
: Anaerobic Adhesive
Part Number
: 087266
Date Sample Received
: Nov 12, 2012
Date Test Started
: Nov 13, 2012
Test Conducted :
As requested by the applicant, for details please refer to attached pages.
Authorized By:
On Behalf Of Intertek Testing Services
Taiwan Limited
K. Y. Liang
Director
*THJ0285781*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410
Page 1 of 10
Number : TWNC00285781
Test Conducted
(Ⅰ) Test Result Summary :
Result (ppm)
Green Liquid
Test Item
Heavy Metal
Cadmium (Cd) content
Lead (Pb) content
Mercury (Hg) content
Chromium VI (Cr6+) content
Polybrominated Biphenyls (PBBs)
Monobrominated Biphenyls (MonoBB)
Dibrominated Biphenyls (DiBB)
Tribrominated Biphenyls (TriBB)
Tetrabrominated Biphenyls (TetraBB)
Pentabrominated Biphenyls (PentaBB)
Hexabrominated Biphenyls (HexaBB)
Heptabrominated Biphenyls (HeptaBB)
Octabrominated Biphenyls (OctaBB)
Nonabrominated Biphenyls (NonaBB)
Decabrominated Biphenyl (DecaBB)
Polybrominated Diphenyl Ethers (PBDEs)
Monobrominated Diphenyl Ethers (MonoBDE)
Dibrominated Diphenyl Ethers (DiBDE)
Tribrominated Diphenyl Ethers (TriBDE)
Tetrabrominated Diphenyl Ethers (TetraBDE)
Pentabrominated Diphenyl Ethers (PentaBDE)
Hexabrominated Diphenyl Ethers (HexaBDE)
Heptabrominated Diphenyl Ethers (HeptaBDE)
Octabrominated Diphenyl Ethers (OctaBDE)
Nonabrominated Diphenyl Ethers (NonaBDE)
Decabrominated Diphenyl Ether (DecaBDE)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
*THJ0285781*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410
Page 2 of 10
Number : TWNC00285781
Test Conducted
(Ⅰ) Test Result Summary :
Result (ppm)
Green Liquid
Test Item
Halogen Content
Fluorine (F)
Chlorine (Cl)
Bromine (Br)
Iodine (I)
Phthalates
Di(2-ethylhexyl) Phthalate (DEHP)
Dibutyl Phthalate (DBP)
Benzyl Butyl Phthalate (BBP)
Others
Hexabromocyclododecane (HBCDD)
ND
ND
ND
ND
ND
77
ND
ND
Remarks: ppm = Parts per million based on wet weight of tested sample =
mg/kg
ND = Not detected
Responsibility of Chemist : Irene Chiou / Kevin Liu / Cathy Chen
Date Sample Received
Test Period
: Nov 12, 2012
: Nov 13, 2012 To Nov 15, 2012
(Ⅱ) RoHS Limits:
Restricted Substances
Cadmium (Cd) Content
Lead (Pb) Content
Mercury (Hg) Content
Chromium VI (Cr6+) Content
Polybrominated Biphenyls (PBBs)
Polybrominated Diphenyl Ehters (PBDEs)
Limits
0.01% (100ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
The above limits were quoted from Annex II of 2011/65/EU for homogeneous
material.
*THJ0285781*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410
Page 3 of 10
Number : TWNC00285781
Test Conducted
(Ⅲ) Test Method:
Test Item
Reporting Limit
Test Method
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the
Cadmium (Cd) content
2 ppm
tested samples are totally
dissolved and determined by ICPOES.
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the
Lead (Pb) content
2 ppm
tested samples are totally
dissolved and determined by ICPOES.
With reference to IEC 62321 edition
1.0:2008 in clause 7, by microwave
Mercury (Hg) content
digestion until the tested samples
2 ppm
are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
Chromium VI (Cr6+)
1.0:2008 in annex C, by alkaline
1 ppm
digestion and determined by UV-Vis
content
spectrophotometer.
With reference to IEC 62321 edition
1.0:2008 in annex A, by solvent
Polybrominated
extraction and determined by GC-MS
5 ppm
Biphenyls (PBBs)
and further HPLC-DAD confirmation
when necessary.
With reference to IEC 62321 edition
1.0:2008 in annex A, by solvent
Polybrominated
Diphenyl Ethers
extraction and determined by GC-MS
5 ppm
(PBDEs)
and further HPLC-DAD confirmation
when necessary.
With reference to EN 14582:2007 by
50 ppm
Halogen Content
calorimetric bomb with oxygen and
determined by Ion Chromatograph.
With reference to EN 14372: 2004, by
Phthalates
solvent extraction and determined by
50 ppm
GC-MS.
With reference to USEPA 3540C, by
Hexabromocyclododecane
10 ppm
solvent extraction and determined by
(HBCDD)
GC-MS.
Remark: Reporting limit = Quantitation limit of analyte in sample
*THJ0285781*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410
Page 4 of 10
Number : TWNC00285781
Test Conducted
(Ⅳ) Measurement Flowchart:
Test for Cd/Pb/Hg/Chromium (VI)/PBBS/PBDES Contents
Reference Standard: IEC 62321 edition 1.0:2008
Sample preparation
For non-metal part
For metal part
Take sample and immerse into Aqua Regia, start to strip plating layer
Stop the stripping procedure upon color change completely
Take the Aqua solution as plating component and stripped body as substrate component
PBBs/PBDEs
Weigh sample and
add organic solvent
By Soxhlet
extraction or
Solvent extraction
Concentrate the
extract and make up
with organic
solvent
Analyzed by GC-MSD
Cr
6+
Substrate
Cd/Pb/Hg
Weigh sample
and add
alkaline
solution
For different
material, digest
the sample with
*1
appropriate acid
Plating
Cr
6+
By spot test
Definite temp.
extraction
Cool and filter
the extract
Confirm the tested
samples are
totally dissolved
Negative
*2
Get 50cm2 sample
Make up with
deionized water
By boiling water
extraction
Analyzed by ICP-OES
Make up with deionized
water and add
diphenyl-carbazide
solution
Analyzed by UV-VIS
*THJ0285781*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410
Page 5 of 10
Number : TWNC00285781
Test Conducted
(Ⅳ) Measurement Flowchart:
Remarks:
*1: List of Appropriate Acid：
Material
Polymers
Metals
Electronics
Acid Added for Digestion
HNO3,HCl,HF,H2O2,H3BO3
HNO3,HCl,HF
HNO3,HCl,H2O2,HBF4
*2: If the result of spot test is positive, Chromium VI would be determined as detected.
*THJ0285781*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410
Page 6 of 10
Number : TWNC00285781
Test Conducted
(Ⅳ) Measurement Flowchart:
Test for Halogen Content
Reference Standard：EN 14582
Sampling/grinding or
cutting
Add absorbent in a
combustion flask &
place weighed sample in
equipment
Fill oxygen into
calorimetric bomb
Ignite then leave the
bomb at room
temperature
Transfer the absorbent
into a volumetric flask
Make up with deionized
water
Analyzed by ion
chromatography
*THJ0285781*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410
Page 7 of 10
Number : TWNC00285781
Test Conducted
(Ⅳ) Measurement Flowchart:
Test For Phthalates Contents
Reference Method: EN 14372: 2004
Sampling/grinding or
cutting
Weigh sample and add
organic solvent
By solvent extraction
Concentrate the extract
and make up with
organic solvent
Analyzed by GC-MSD
*THJ0285781*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410
Page 8 of 10
Number : TWNC00285781
Test Conducted
(Ⅳ) Measurement Flowchart:
Test For Hexabromocyclododecane (HBCDD)
Reference Standard：USEPA 3540C
Sampling/grinding or cutting
Weigh sample and add
organic solvent
By soxhlet extraction
Concentrate the extract and
make up with organic solvent
Analyzed by GC-MSD
End of Report
This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a
recommendation for any particular course of action. Intertek does not accept a duty of care or any other responsibility to any person other than
the Client in respect of this report and only accepts liability to the Client insofar as is expressly contained in the terms and conditions
governing Intertek's provision of services to you. Intertek makes no warranties or representations either express or implied with respect to this
report save as provided for in those terms and conditions. We have aimed to conduct the Review on a diligent and careful basis and we do not
accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by statute or otherwise, except in
the event of our gross negligence or wilful misconduct.
*THJ0285781*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410
Page 9 of 10
Number : TWNC00285781
Test Conducted
Photo
*THJ0285781*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410
Page 10 of 10
Test Report
Applicant:
Number : TWNC00253636
Littelfuse Philippines Inc.
LIMA Technology Center, Lipa City,
Malvar, Batangas
Date
: Apr 24, 2012
Sample Description:
One (1) group of submitted samples said to be :
Part Description
: Black Ink
Part Number
: 425809
Date Sample Received
: Apr 19, 2012
Date Test Started
: Apr 19, 2012
Test Conducted :
As requested by the applicant, for details please refer to attached pages.
Authorized By:
On Behalf Of Intertek Testing Services
Taiwan Limited
K. Y. Liang
Director
This report shall not be reproduced
except in full, without the written
approval of the laboratory.
Page 1 of 9
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00253636
Test Conducted
(Ⅰ) Test Result Summary :
Test Item
Heavy Metal
Cadmium (Cd) content
Lead (Pb) content
Mercury (Hg) content
Chromium VI (Cr6+) content
Polybrominated Biphenyls (PBBs)
Monobrominated Biphenyls (MonoBB)
Dibrominated Biphenyls (DiBB)
Tribrominated Biphenyls (TriBB)
Tetrabrominated Biphenyls (TetraBB)
Pentabrominated Biphenyls (PentaBB)
Hexabrominated Biphenyls (HexaBB)
Heptabrominated Biphenyls (HeptaBB)
Octabrominated Biphenyls (OctaBB)
Nonabrominated Biphenyls (NonaBB)
Decabrominated Biphenyl (DecaBB)
Polybrominated Diphenyl Ethers (PBDEs)
Monobrominated Diphenyl Ethers (MonoBDE)
Dibrominated Diphenyl Ethers (DiBDE)
Tribrominated Diphenyl Ethers (TriBDE)
Tetrabrominated Diphenyl Ethers (TetraBDE)
Pentabrominated Diphenyl Ethers (PentaBDE)
Hexabrominated Diphenyl Ethers (HexaBDE)
Heptabrominated Diphenyl Ethers (HeptaBDE)
Octabrominated Diphenyl Ethers (OctaBDE)
Nonabrominated Diphenyl Ethers (NonaBDE)
Decabrominated Diphenyl Ether (DecaBDE)
Result (ppm)
Black Paste
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Page 2 of 9
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00253636
Test Conducted
(Ⅰ) Test Result Summary :
Test Item
Result (ppm)
Black Paste
Halogen Content
Fluorine (F)
Chlorine (Cl)
Bromine (Br)
Iodine (I)
Phthalates
Di(2-ethylhexyl) Phthalate (DEHP)
Dibutyl Phthalate (DBP)
Benzyl Butyl Phthalate (BBP)
Others
Hexabromocyclododecane (HBCDD)
ND
610
ND
ND
ND
ND
ND
ND
Remarks: ppm = Parts per million based on wet weight of tested sample =
mg/kg
ND = Not detected
Responsibility of Chemist : Irene Chiou / Kevin Liu / Cathy Chen
Date Sample Received
Test Period
: Apr 19, 2012
: Apr 19, 2012 To Apr 24, 2012
(Ⅱ) RoHS Requirement:
Restricted Substances
Cadmium (Cd) Content
Lead (Pb) Content
Mercury (Hg) Content
Chromium VI (Cr6+) Content
Polybrominated Biphenyls (PBBs)
Polybrominated Diphenyl Ehters (PBDEs)
Limits
0.01% (100ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for
homogeneous material.
Page 3 of 9
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00253636
Test Conducted
(Ⅲ) Test Method:
Test Item
Test Method
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
Cadmium (Cd) content
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
Lead (Pb) content
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 7, by microwave
Mercury (Hg) content
digestion until the tested samples
are totally dissolved and determined
by ICP-OES.
With reference to IEC 62321 edition
Chromium VI (Cr6+)
1.0:2008 in annex C, by alkaline
content
digestion and determined by UV-Vis
spectrophotometer.
With reference to IEC 62321 edition
1.0:2008 in annex A, by solvent
Polybrominated
extraction and determined by GC-MS
Biphenyls (PBBs)
and further HPLC-DAD confirmation
when necessary.
With reference to IEC 62321 edition
Polybrominated
1.0:2008 in annex A, by solvent
Diphenyl Ethers
extraction and determined by GC-MS
(PBDEs)
and further HPLC-DAD confirmation
when necessary.
With reference to EN 14582:2007 by
Halogen Content
calorimetric bomb with oxygen and
determined by Ion Chromatograph.
With reference to EN 14372: 2004, by
Phthalates
solvent extraction and determined by
GC-MS.
With reference to USEPA 3540C, by
Hexabromocyclododecane
solvent extraction and determined by
(HBCDD)
GC-MSD.
Reporting Limit
2 ppm
2 ppm
2 ppm
1 ppm
5 ppm
5 ppm
50 ppm
10 ppm
10 ppm
Remark: Reporting limit = Quantitation limit of analyte in sample
Page 4 of 9
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00253636
Test Conducted
(Ⅳ) Measurement Flowchart:
Test for Cd/Pb/Hg/Chromium (VI)/PBBS/PBDES Contents
Reference Standard: IEC 62321 edition 1.0:2008
Sample preparation
For non-metal part
For metal part
Take sample and immerse into Aqua Regia, start to strip plating layer
Stop the stripping procedure upon color change completely
Take the Aqua solution as plating component and stripped body as substrate component
Cd/Pb/Hg
Cr
Confirm the tested
samples are
totally dissolved
Make up with
deionized water
PBBs/PBDEs
Polymers /
electronics
Metal
For different
material, digest
the sample with
*1
appropriate acid
6+
Weigh sample and
add organic solvent
By spot test
Negative
Get 50cm2 sample
By boiling water
extraction
*2
Weigh sample
and add
alkaline
solution
By Soxhlet
extraction or
Solvent extraction
Definite temp.
extraction
Cool and filter
the extract
Analyzed by ICP-OES
Concentrate the
extract and make up
with organic
solvent
Analyzed by GC-MSD
Make up with deionized
water and add diphenylcarbazide solution
Analyzed by UV-VIS
Remarks:
*1: List of Appropriate Acid：
Acid Added for Digestion
Material
Polymers
HNO3,HCl,HF,H2O2,H3BO3
Metals
HNO3,HCl,HF
Electronics
HNO3,HCl,H2O2,HBF4
*2: If the result of spot test is positive, Chromium VI would be determined as detected.
Page 5 of 9
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00253636
Test Conducted
(Ⅳ) Measurement Flowchart:
Test for Halogen Content
Reference Standard：EN 14582
Sampling/grinding or
cutting
Add absorbent in a
combustion flask &
place weighed sample in
equipment
Fill oxygen into
calorimetric bomb
Ignite then leave the
bomb at room
temperature
Transfer the absorbent
into a volumetric flask
Make up with deionized
water
Analyzed by ion
chromatography
Page 6 of 9
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00253636
Test Conducted
(Ⅳ) Measurement Flowchart:
Test For Phthalates Contents
Reference Method: EN 14372: 2004
Sampling/grinding or
cutting
Weigh sample and add
organic solvent
By solvent extraction
Concentrate the extract
and make up with
organic solvent
Analyzed by GC-MSD
Page 7 of 9
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00253636
Test Conducted
(Ⅳ) Measurement Flowchart:
Test For Hexabromocyclododecane (HBCDD)
Reference Standard：USEPA 3540C
Sampling/grinding or cutting
Weigh sample and add organic
solvent
By soxhlet extraction
Concentrate the extract and
make up with organic solvent
Analyzed by GC-MSD
End of Report
Page 8 of 9
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00253636
Test Conducted
Photo
Page 9 of 9
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Signaturetid
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