Appendix E.pdf

Appendix E
Groundwater Well Construction
and Development Logs, Sampling
Logs, and Laboratory Analytical
Reports
ANALYTICAL REPORT
Job Number: 660-27893-1
Job Description: Raytheon
For:
ARCADIS U.S., Inc.
14055 Riveredge Drive
Suite 400
Tampa, FL 33637
Attention: Mr. Gus Suarez
_____________________________________________
Approved for release.
Nancy Robertson
Project Manager II
4/6/2009 2:17 PM
Designee for
Natalie Tafuni
Project Manager I
[email protected]
04/06/2009
Revision: 1
cc:
Ms. Jane Kennedy
Mr. Melvin Rivera
Albert Zumbuhl
Methods: FDEP, DOH Certification #: TestAmerica Tampa E84282
TestAmerica Tallahassee E81005
These test results meet all the requirements of NELAC unless specified in the case narrative. All questions regarding
this test report should be directed to the TestAmerica Project Manager who signed this test report. The estimated
uncertainty associated with these reported results is available upon request. The results contained in this test report
relate only to these samples included herein.
TestAmerica Laboratories, Inc.
TestAmerica Tampa 6712 Benjamin Road, Suite 100, Tampa, FL 33634
Tel (813) 885-7427 Fax (813) 885-7049 www.testamericainc.com
Page 1 of 221
04/06/2009
Job Narrative
660-J27893-1
Comments
No additional comments.
Receipt
All samples were received in good condition within temperature requirements.
8260B
The batch sample duplicate(job 660-27916) %RPD for batch 660-75683 has a result of NC for all analytes. The sample result and the
sample duplicate result are both Non-detect for these compounds. The Laboratory LIMs system flags the %RPD in this scenario as NC,
or "not calculated".
This report was revised on 4/6/09. A peak was misidentified as Chloroethane for sample
DMW-N_022509. Upon review of the data, per client request, it was noticed this was matrix interference causing background noise. This
revised report has the corrected results for this sample.
6010B
The matrix spike / matrix spike duplicate (MS/MSD) recoveries for batch 660-75517 were outside of control limits for calcium and iron.
The spike concentration of 1.0 mg/l is significantly less than 4X the sample concentration for Calcium. Therefore, the MS/MSD recovery
calculations are not applicable. The associated laboratory control standard (LCS) met acceptance criteria. The data are flagged with J3
qualifiers.
353.2
The matrix spike duplicate (MSD) recovery for batch 660-75644 was outside of control limits for NOX. The associated laboratory control
standard (LCS) and matrix spike (MS) met acceptance criteria. The data are flagged with J3 qualifiers.
2320B
The sample duplicate %RPD for batch 660-75553 has a result of NC for alkalinity. The sample result and the sample duplicate result are
both Non-detect for this compound. The Laboratory LIMs system flags the %RPD in this scenario as NC, or "not calculated".
The sample duplicate %RPD for batch 660-75622 has a result of NC for alkalinity. The sample result and the sample duplicate result are
both Non-detect for this compound. The Laboratory LIMs system flags the %RPD in this scenario as NC, or "not calculated".
300.0
The matrix spike / matrix spike duplicate (MS/MSD) recoveries for batch 660-75752 were outside of control limits for chloride and sulfate
only, possibly due to matrix interference from sample. The associated laboratory control standard (LCS) met acceptance criteria. The
data are flagged with J3 qualifiers.
Page 2 of 221
04/06/2009
EXECUTIVE SUMMARY - Detections
Client: ARCADIS U.S., Inc.
Lab Sample ID
Analyte
660-27893-1
Client Sample ID
Result / Qualifier
Chloromethane
20
ug/L
8260B
16
1.0
ug/L
8260C SIM/ID
5.2
1.0
ug/L
8260C SIM/ID
4.3
78
1.0
1.0
ug/L
ug/L
8260B
8260C SIM/ID
1.9
20
1.0
1.0
ug/L
ug/L
8260B
8260C SIM/ID
9.5
1.0
ug/L
8260C SIM/ID
1.4
1.0
ug/L
8260C SIM/ID
SMW-H_022509
1,4-Dioxane
660-27893-14
45
SMW-E_022509
1,4-Dioxane
660-27893-13
8260B
IDPT-9_022509
1,4-Dioxane
660-27893-12
ug/L
IDPT-8_022509
1,1-Dichloroethane
1,4-Dioxane
660-27893-11
1.0
IDPT-15_022509
1,1-Dichloroethane
1,4-Dioxane
660-27893-10
2.8
IMW-D_022509
1,4-Dioxane
660-27893-7
Method
DMW-C_022509
1,4-Dioxane
660-27893-5
Units
DMW-Q_022509
Acetone
660-27893-4
Reporting
Limit
DMW-P_022509
Chloroform
660-27893-3
Job Number: 660-27893-1
0.80
I
1.0
ug/L
8260C SIM/ID
1.1
I
4.0
ug/L
8260B
DMW-N_022509
TestAmerica Tampa
Page 3 of 221
04/06/2009
EXECUTIVE SUMMARY - Detections
Client: ARCADIS U.S., Inc.
Lab Sample ID
Analyte
660-27893-17
Client Sample ID
Result / Qualifier
ug/L
8260C SIM/ID
27
1.0
ug/L
8260C SIM/ID
1300
40
ug/L
8260B
0.83
I
1.0
ug/L
8260B
1.1
0.51
14
I
1.0
1.0
1.0
ug/L
ug/L
ug/L
8260B
8260B
8260C SIM/ID
1.0
2.0
ug/L
ug/L
8260B
8260B
1.0
ug/L
8260C SIM/ID
1.0
1.0
1.0
5.0
5.0
ug/L
ug/L
ug/L
ug/L
ug/L
8260B
8260B
8260B
8260B
8260C SIM/ID
IDPT-1_022509
IDPT-2_022509
13
1.8
I
IDPT-5_022509
1,4-Dioxane
660-27893-29
1.0
I
H-1_022509
Toluene
m-Xylene & p-Xylene
660-27893-28
8260B
8260C SIM/ID
IMW-J_022509
1,1-Dichloroethane
Vinyl chloride
1,4-Dioxane
660-27893-27
ug/L
ug/L
IDPT-12_022509
Benzene
660-27893-26
40
1.0
0.95
Acetone
660-27893-23
Method
SMW-N_022509
1,4-Dioxane
660-27893-20
Units
920
5.1
1,4-Dioxane
660-27893-19
Reporting
Limit
DMW-I_022509
Acetone
1,4-Dioxane
660-27893-18
Job Number: 660-27893-1
24
IDPT-6_022509
1,1-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
Vinyl chloride
1,4-Dioxane
16
0.59
4.0
330
100
I
TestAmerica Tampa
Page 4 of 221
04/06/2009
EXECUTIVE SUMMARY - Detections
Client: ARCADIS U.S., Inc.
Lab Sample ID
Analyte
660-27893-30
Client Sample ID
Result / Qualifier
1,4-Dioxane
1.0
ug/L
8260C SIM/ID
470
3800
160
50
50
50
ug/L
ug/L
ug/L
8260B
8260B
8260C SIM/ID
160
1.0
7.9
20
1.0
1.0
ug/L
ug/L
ug/L
8260B
8260B
8260C SIM/ID
3.4
110
2.0
2.0
ug/L
ug/L
8260B
8260C SIM/ID
36
14
2.7
1.5
6.2
1.0
1.0
1.0
1.0
1.0
ug/L
ug/L
ug/L
ug/L
ug/L
8260B
8260B
8260B
8260B
8260C SIM/ID
9800
55
400
20
ug/L
ug/L
8260B
8260C SIM/ID
88
2.0
ug/L
8260C SIM/ID
I
DMW-F_022509
DMW-J_022509
DMW-K_022509
Acetone
1,4-Dioxane
660-27893-37
8260B
IMW-F_022509
cis-1,2-Dichloroethene
Trichloroethene
Vinyl chloride
Carbon disulfide
1,4-Dioxane
660-27893-36
ug/L
IDPT-14_022509
Carbon disulfide
1,4-Dioxane
660-27893-35
1.0
0.77
Acetone
Carbon disulfide
1,4-Dioxane
660-27893-34
Method
IDPT-13_022509
cis-1,2-Dichloroethene
Trichloroethene
1,4-Dioxane
660-27893-33
Units
5.5
1,4-Dioxane
660-27893-32
Reporting
Limit
IDPT-10_022509
Toluene
660-27893-31
Job Number: 660-27893-1
DMW-L_022509
TestAmerica Tampa
Page 5 of 221
04/06/2009
EXECUTIVE SUMMARY - Detections
Client: ARCADIS U.S., Inc.
Lab Sample ID
Analyte
660-27893-38
Client Sample ID
Result / Qualifier
Units
Method
1.0
ug/L
8260C SIM/ID
8800
59
1000
50
ug/L
ug/L
8260B
8260C SIM/ID
310
290
12
0.54
170
36
150
150
580
65
23
8.7
3.3
1.2
2.1
0.050
1.0
0.50
1.0
1.0
10
5.0
20
2.0
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
SM 2340B
SM 2340B
SM 2340B
300.0
300.0
300.0
SM 2320B
SM 2320B
SM 2540C
SM 2540D
SM 5220D
SM 5310C
0.20
0.0040
mg/L
mg/L
6010B
6010B
0.50
0.20
1.0
0.080
0.0040
0.50
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
6010B
6010B
6010B
6010B
6010B
6010B
0.97
I
DUPE H_022509
Acetone
1,4-Dioxane
660-27893-41
Reporting
Limit
DUPE D_022509
1,4-Dioxane
660-27893-39
Job Number: 660-27893-1
IDPT-14_022509
Hardness as calcium carbonate
Calcium hardness as calcium carbonate
Magnesium hardness as calcium carbonate
Bromide
Chloride
Sulfate
Alkalinity
Bicarbonate Alkalinity as CaCO3
Total Dissolved Solids
Total Suspended Solids
Chemical Oxygen Demand
Total Organic Carbon
J3
J3
Dissolved
Iron, Dissolved
Manganese, Dissolved
9.0
0.0065
Total Recoverable
Calcium
Iron
Potassium
Magnesium
Manganese
Sodium
120
9.7
1.2
2.8
0.0072
45
J3
J3
TestAmerica Tampa
Page 6 of 221
04/06/2009
EXECUTIVE SUMMARY - Detections
Client: ARCADIS U.S., Inc.
Lab Sample ID
Analyte
660-27893-42
Job Number: 660-27893-1
Client Sample ID
Reporting
Limit
Units
Method
3.3
1.2
2.1
0.050
0.50
0.50
1.0
1.0
10
1.0
20
1.0
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
SM 2340B
SM 2340B
SM 2340B
300.0
300.0
300.0
SM 2320B
SM 2320B
SM 2540C
SM 2540D
SM 5220D
SM 5310C
2.6
0.0066
0.20
0.0040
mg/L
mg/L
6010B
6010B
99
2.6
0.45
2.5
0.0065
17
0.50
0.20
1.0
0.080
0.0040
0.50
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
6010B
6010B
6010B
6010B
6010B
6010B
Result / Qualifier
DMW-F_022509
Hardness as calcium carbonate
Calcium hardness as calcium carbonate
Magnesium hardness as calcium carbonate
Bromide
Chloride
Sulfate
Alkalinity
Bicarbonate Alkalinity as CaCO3
Total Dissolved Solids
Total Suspended Solids
Chemical Oxygen Demand
Total Organic Carbon
260
250
10
0.13
40
19
230
230
360
12
14
5.8
I
Dissolved
Iron, Dissolved
Manganese, Dissolved
Total Recoverable
Calcium
Iron
Potassium
Magnesium
Manganese
Sodium
I
TestAmerica Tampa
Page 7 of 221
04/06/2009
EXECUTIVE SUMMARY - Detections
Client: ARCADIS U.S., Inc.
Lab Sample ID
Analyte
660-27893-43
Job Number: 660-27893-1
Client Sample ID
Reporting
Limit
Units
Method
3.3
1.2
2.1
0.050
2.0
0.50
1.0
1.0
10
1.1
20
1.0
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
SM 2340B
SM 2340B
SM 2340B
300.0
300.0
300.0
SM 2320B
SM 2320B
SM 2540C
SM 2540D
SM 5220D
SM 5310C
12
0.0083
0.20
0.0040
mg/L
mg/L
6010B
6010B
160
13
0.70
3.6
0.0084
64
0.50
0.20
1.0
0.080
0.0040
0.50
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
6010B
6010B
6010B
6010B
6010B
6010B
Result / Qualifier
DMW-J_022509
Hardness as calcium carbonate
Calcium hardness as calcium carbonate
Magnesium hardness as calcium carbonate
Bromide
Chloride
Sulfate
Alkalinity
Bicarbonate Alkalinity as CaCO3
Total Dissolved Solids
Total Suspended Solids
Chemical Oxygen Demand
Total Organic Carbon
420
400
15
0.47
270
54
180
180
780
27
14
5.5
I
Dissolved
Iron, Dissolved
Manganese, Dissolved
Total Recoverable
Calcium
Iron
Potassium
Magnesium
Manganese
Sodium
I
TestAmerica Tampa
Page 8 of 221
04/06/2009
EXECUTIVE SUMMARY - Detections
Client: ARCADIS U.S., Inc.
Lab Sample ID
Analyte
660-27893-44
Job Number: 660-27893-1
Client Sample ID
Reporting
Limit
Units
Method
200
190
7.9
35
8.6
200
200
270
26
3.0
3.3
1.2
2.1
0.50
0.50
1.0
1.0
5.0
1.7
1.0
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
SM 2340B
SM 2340B
SM 2340B
300.0
300.0
SM 2320B
SM 2320B
SM 2540C
SM 2540D
SM 5310C
4.0
0.0051
0.20
0.0040
mg/L
mg/L
6010B
6010B
78
4.2
0.35
1.9
0.0052
17
0.50
0.20
1.0
0.080
0.0040
0.50
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
6010B
6010B
6010B
6010B
6010B
6010B
Result / Qualifier
DMW-L_022509
Hardness as calcium carbonate
Calcium hardness as calcium carbonate
Magnesium hardness as calcium carbonate
Chloride
Sulfate
Alkalinity
Bicarbonate Alkalinity as CaCO3
Total Dissolved Solids
Total Suspended Solids
Total Organic Carbon
Dissolved
Iron, Dissolved
Manganese, Dissolved
Total Recoverable
Calcium
Iron
Potassium
Magnesium
Manganese
Sodium
I
TestAmerica Tampa
Page 9 of 221
04/06/2009
EXECUTIVE SUMMARY - Detections
Client: ARCADIS U.S., Inc.
Lab Sample ID
Analyte
660-27893-45
Job Number: 660-27893-1
Client Sample ID
Reporting
Limit
Units
Method
240
230
11
0.22
75
2.0
180
180
340
32
26
8.7
3.3
1.2
2.1
0.050
0.50
0.50
1.0
1.0
10
1.7
20
1.0
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
SM 2340B
SM 2340B
SM 2340B
300.0
300.0
300.0
SM 2320B
SM 2320B
SM 2540C
SM 2540D
SM 5220D
SM 5310C
2.2
0.0068
0.20
0.0040
mg/L
mg/L
6010B
6010B
93
2.5
0.50
2.8
0.0051
14
0.50
0.20
1.0
0.080
0.0040
0.50
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
6010B
6010B
6010B
6010B
6010B
6010B
Result / Qualifier
DMW-I_022509
Hardness as calcium carbonate
Calcium hardness as calcium carbonate
Magnesium hardness as calcium carbonate
Bromide
Chloride
Sulfate
Alkalinity
Bicarbonate Alkalinity as CaCO3
Total Dissolved Solids
Total Suspended Solids
Chemical Oxygen Demand
Total Organic Carbon
Dissolved
Iron, Dissolved
Manganese, Dissolved
Total Recoverable
Calcium
Iron
Potassium
Magnesium
Manganese
Sodium
I
TestAmerica Tampa
Page 10 of 221
04/06/2009
EXECUTIVE SUMMARY - Detections
Client: ARCADIS U.S., Inc.
Lab Sample ID
Analyte
660-27893-46
Job Number: 660-27893-1
Client Sample ID
Reporting
Limit
Units
Method
260
250
8.7
41
71
130
130
320
3.9
6.8
3.3
1.2
2.1
0.50
0.50
1.0
1.0
10
1.0
1.0
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
SM 2340B
SM 2340B
SM 2340B
300.0
300.0
SM 2320B
SM 2320B
SM 2540C
SM 2540D
SM 5310C
3.4
0.023
0.20
0.0040
mg/L
mg/L
6010B
6010B
100
3.5
0.54
2.1
0.025
13
0.50
0.20
1.0
0.080
0.0040
0.50
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
6010B
6010B
6010B
6010B
6010B
6010B
Result / Qualifier
DMW-C_022609
Hardness as calcium carbonate
Calcium hardness as calcium carbonate
Magnesium hardness as calcium carbonate
Chloride
Sulfate
Alkalinity
Bicarbonate Alkalinity as CaCO3
Total Dissolved Solids
Total Suspended Solids
Total Organic Carbon
Dissolved
Iron, Dissolved
Manganese, Dissolved
Total Recoverable
Calcium
Iron
Potassium
Magnesium
Manganese
Sodium
I
TestAmerica Tampa
Page 11 of 221
04/06/2009
EXECUTIVE SUMMARY - Detections
Client: ARCADIS U.S., Inc.
Lab Sample ID
Analyte
660-27893-47
Job Number: 660-27893-1
Client Sample ID
Reporting
Limit
Units
Method
140
110
23
0.29
83
8.5
1.4
61
61
380
500
45
5.8
3.3
1.2
2.1
0.050
0.50
0.50
0.50
1.0
1.0
5.0
20
20
4.0
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
SM 2340B
SM 2340B
SM 2340B
300.0
300.0
300.0
353.2
SM 2320B
SM 2320B
SM 2540C
SM 2540D
SM 5220D
SM 5310C
3.3
0.0060
0.20
0.0040
mg/L
mg/L
6010B
6010B
46
7.2
1.4
5.6
0.0089
19
0.50
0.20
1.0
0.080
0.0040
0.50
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
6010B
6010B
6010B
6010B
6010B
6010B
Result / Qualifier
IDPT-9_022609
Hardness as calcium carbonate
Calcium hardness as calcium carbonate
Magnesium hardness as calcium carbonate
Bromide
Chloride
Sulfate
Nitrite as N
Alkalinity
Bicarbonate Alkalinity as CaCO3
Total Dissolved Solids
Total Suspended Solids
Chemical Oxygen Demand
Total Organic Carbon
Dissolved
Iron, Dissolved
Manganese, Dissolved
Total Recoverable
Calcium
Iron
Potassium
Magnesium
Manganese
Sodium
TestAmerica Tampa
Page 12 of 221
04/06/2009
EXECUTIVE SUMMARY - Detections
Client: ARCADIS U.S., Inc.
Lab Sample ID
Analyte
660-27893-48
Job Number: 660-27893-1
Client Sample ID
Reporting
Limit
Units
Method
3.3
1.2
2.1
0.050
2.0
0.50
1.0
1.0
10
1.7
20
1.0
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
SM 2340B
SM 2340B
SM 2340B
300.0
300.0
300.0
SM 2320B
SM 2320B
SM 2540C
SM 2540D
SM 5220D
SM 5310C
11
0.012
0.20
0.0040
mg/L
mg/L
6010B
6010B
61
9.6
1.0
2.5
0.011
27
0.50
0.20
1.0
0.080
0.0040
0.50
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
6010B
6010B
6010B
6010B
6010B
6010B
Result / Qualifier
IDPT-15_022609
Hardness as calcium carbonate
Calcium hardness as calcium carbonate
Magnesium hardness as calcium carbonate
Bromide
Chloride
Sulfate
Alkalinity
Bicarbonate Alkalinity as CaCO3
Total Dissolved Solids
Total Suspended Solids
Chemical Oxygen Demand
Total Organic Carbon
160
150
10
0.52
170
6.1
37
37
410
22
11
5.2
I
Dissolved
Iron, Dissolved
Manganese, Dissolved
Total Recoverable
Calcium
Iron
Potassium
Magnesium
Manganese
Sodium
TestAmerica Tampa
Page 13 of 221
04/06/2009
METHOD SUMMARY
Client: ARCADIS U.S., Inc.
Job Number: 660-27893-1
Description
Lab Location Method
Preparation Method
Volatile Organic Compounds (GC/MS)
Purge and Trap
TAL TAM
TAL TAM
SW846 8260B
SW846 5030B
1,4-Dioxane by SIM/Isotopic Dilution
Purge and Trap
TAL TAM
TAL TAM
SW846 8260C SIM/ID
SW846 5030B
Metals (ICP)
Sample Filtration, Field
Preparation, Total Recoverable or Dissolved Metals
TAL TAM
TAL TAM
TAL TAM
SW846 6010B
Hardness, Calculation
TAL TAM
SM SM 2340B
Anions, Ion Chromatography
TAL TAM
MCAWW 300.0
Nitrogen, Nitrate-Nitrite
Nitrogen, Nitrate-Nitrite
TAL TAM
TAL TAM
MCAWW 353.2
Alkalinity
TAL TAM
SM SM 2320B
Solids, Total Dissolved (TDS)
TAL TAL
SM SM 2540C
Solids, Total Suspended (TSS)
TAL TAL
SM SM 2540D
COD
TAL TAM
TAL TAM
SM SM 5220D
TAL TAM
SM SM 5310C
Matrix
Water
COD
TOC
FIELD_FLTRD
SW846 3005A
MCAWW 353.2
SM SM 5220
Lab References:
TAL TAL = TestAmerica Tallahassee
TAL TAM = TestAmerica Tampa
Method References:
MCAWW = "Methods For Chemical Analysis Of Water And Wastes", EPA-600/4-79-020, March 1983 And Subsequent Revisions.
SM = "Standard Methods For The Examination Of Water And Wastewater",
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its
Updates.
TestAmerica Tampa
Page 14 of 221
04/06/2009
METHOD / ANALYST SUMMARY
Client: ARCADIS U.S., Inc.
Job Number: 660-27893-1
Method
Analyst
Analyst ID
SW846 8260B
SW846 8260B
Carlson, Robyn
Mathew, Pinky
RC
PM
SW846 8260C SIM/ID
SW846 8260C SIM/ID
Carlson, Robyn
Mathew, Pinky
RC
PM
SW846 6010B
Fox, Greg
GF
SM SM 2340B
Fox, Greg
GF
MCAWW 300.0
Alvarez, Luz
LA
MCAWW 353.2
Steward, Tiffany
TS
SM SM 2320B
Steward, Tiffany
TS
SM SM 2540C
Frank, Michelle
MF
SM SM 2540D
Frank, Michelle
MF
SM SM 5220D
Martin, Randolph
RM
SM SM 5310C
Martin, Randolph
RM
TestAmerica Tampa
Page 15 of 221
04/06/2009
SAMPLE SUMMARY
Client: ARCADIS U.S., Inc.
Job Number: 660-27893-1
Lab Sample ID
Client Sample ID
Client Matrix
660-27893-1
660-27893-2
660-27893-3
660-27893-4
660-27893-5
660-27893-6
660-27893-7
660-27893-8
660-27893-9
660-27893-10
660-27893-11
660-27893-12
660-27893-13
660-27893-14
660-27893-15
660-27893-16
660-27893-17
660-27893-18
660-27893-19
660-27893-20
660-27893-21
660-27893-22
660-27893-23
660-27893-24
660-27893-25
660-27893-26
660-27893-27
660-27893-28
660-27893-29
660-27893-30
660-27893-31
660-27893-32
660-27893-33
660-27893-34
660-27893-35
660-27893-36
660-27893-37
660-27893-38
660-27893-39
660-27893-40
660-27893-41
660-27893-42
660-27893-43
660-27893-44
660-27893-45
660-27893-46
DMW-P_022509
DMW-O_022509
DMW-Q_022509
DMW-C_022509
IMW-D_022509
DMW-B_022509
IDPT-15_022509
DMW-8_022509
SMW-D_022509
IDPT-8_022509
IDPT-9_022509
SMW-E_022509
SMW-H_022509
DMW-N_022509
DUPE E_022509
SMW-I_022509
DMW-I_022509
SMW-N_022509
IDPT-12_022509
IMW-J_022509
DMW-A_022509
DMW-W_022509
H-1_022509
SMW-A_022509
Trip Blank 3_022509
IDPT-1_022509
IDPT-2_022509
IDPT-5_022509
IDPT-6_022509
IDPT-10_022509
IDPT-13_022509
IDPT-14_022509
IMW-F_022509
DMW-F_022509
DMW-J_022509
DMW-K_022509
DMW-L_022509
DUPE D_022509
DUPE H_022509
Trip Blank_022509
IDPT-14_022509
DMW-F_022509
DMW-J_022509
DMW-L_022509
DMW-I_022509
DMW-C_022609
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Date/Time
Sampled
02/25/2009
02/25/2009
02/25/2009
02/25/2009
02/25/2009
02/25/2009
02/25/2009
02/25/2009
02/25/2009
02/25/2009
02/25/2009
02/25/2009
02/25/2009
02/25/2009
02/25/2009
02/25/2009
02/25/2009
02/25/2009
02/25/2009
02/25/2009
02/25/2009
02/25/2009
02/25/2009
02/25/2009
02/25/2009
02/25/2009
02/25/2009
02/25/2009
02/25/2009
02/25/2009
02/25/2009
02/25/2009
02/25/2009
02/25/2009
02/25/2009
02/25/2009
02/25/2009
02/25/2009
02/25/2009
02/25/2009
02/25/2009
02/25/2009
02/25/2009
02/25/2009
02/25/2009
02/26/2009
0857
0944
1013
1112
1154
1238
1425
1553
1614
1648
1730
1814
1405
1055
0000
1130
1440
1020
1640
1540
1200
0946
1300
1235
0000
1555
1654
1422
1725
1626
1455
1317
0918
0828
1216
0954
1105
0000
0000
0000
1317
0828
1216
1105
1440
0755
Date/Time
Received
02/26/2009
02/26/2009
02/26/2009
02/26/2009
02/26/2009
02/26/2009
02/26/2009
02/26/2009
02/26/2009
02/26/2009
02/26/2009
02/26/2009
02/26/2009
02/26/2009
02/26/2009
02/26/2009
02/26/2009
02/26/2009
02/26/2009
02/26/2009
02/26/2009
02/26/2009
02/26/2009
02/26/2009
02/26/2009
02/26/2009
02/26/2009
02/26/2009
02/26/2009
02/26/2009
02/26/2009
02/26/2009
02/26/2009
02/26/2009
02/26/2009
02/26/2009
02/26/2009
02/26/2009
02/26/2009
02/26/2009
02/26/2009
02/26/2009
02/26/2009
02/26/2009
02/26/2009
02/26/2009
1030
1030
1030
1030
1030
1030
1030
1030
1030
1030
1030
1030
1030
1030
1030
1030
1030
1030
1030
1030
1030
1030
1030
1030
1030
1030
1030
1030
1030
1030
1030
1030
1030
1030
1030
1030
1030
1030
1030
1030
1030
1030
1030
1030
1030
1030
TestAmerica Tampa
Page 16 of 221
04/06/2009
SAMPLE SUMMARY
Client: ARCADIS U.S., Inc.
Job Number: 660-27893-1
Lab Sample ID
Client Sample ID
Client Matrix
660-27893-47
660-27893-48
IDPT-9_022609
IDPT-15_022609
Water
Water
Date/Time
Sampled
Date/Time
Received
02/26/2009 0745
02/26/2009 0805
02/26/2009 1030
02/26/2009 1030
TestAmerica Tampa
Page 17 of 221
04/06/2009
SAMPLE RESULTS
TestAmerica Tampa
Page 18 of 221
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Client Sample ID:
DMW-P_022509
Lab Sample ID:
Client Matrix:
660-27893-1
Water
Job Number: 660-27893-1
Date Sampled:
Date Received:
02/25/2009 0857
02/26/2009 1030
8260B Volatile Organic Compounds (GC/MS)
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260B
5030B
1.0
02/27/2009 1634
02/27/2009 1634
Analysis Batch: 660-75524
Analyte
Benzene
Bromobenzene
Chlorobromomethane
Dichlorobromomethane
Bromoform
Bromomethane
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
Chlorodibromomethane
1,2-Dibromo-3-Chloropropane
Ethylene Dibromide
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
Hexachlorobutadiene
Isopropylbenzene
4-Isopropyltoluene
Methylene Chloride
Naphthalene
N-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
Result (ug/L)
0.50
0.58
0.58
0.35
0.58
2.5
0.67
0.63
0.84
0.42
0.63
2.5
2.8
1.0
0.65
0.52
0.34
2.5
0.50
0.41
0.44
0.64
0.52
2.5
0.52
0.57
0.45
0.65
0.44
0.52
0.39
0.36
0.31
0.14
0.14
0.44
0.40
0.19
0.69
4.0
2.5
0.59
0.98
0.63
TestAmerica Tampa
Page 19 of 221
Instrument ID:
BVMH GC/MS
Lab File ID:
1HB2729.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
MDL
0.50
0.58
0.58
0.35
0.58
2.5
0.67
0.63
0.84
0.42
0.63
2.5
0.90
1.0
0.65
0.52
0.34
2.5
0.50
0.41
0.44
0.64
0.52
2.5
0.52
0.57
0.45
0.65
0.44
0.52
0.39
0.36
0.31
0.14
0.14
0.44
0.40
0.19
0.69
4.0
2.5
0.59
0.98
0.63
PQL
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
4.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
5.0
1.0
2.0
1.0
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Client Sample ID:
DMW-P_022509
Lab Sample ID:
Client Matrix:
660-27893-1
Water
Job Number: 660-27893-1
Date Sampled:
Date Received:
02/25/2009 0857
02/26/2009 1030
8260B Volatile Organic Compounds (GC/MS)
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260B
5030B
1.0
02/27/2009 1634
02/27/2009 1634
Analyte
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
o-Xylene
Acetone
2-Butanone (MEK)
4-Methyl-2-pentanone (MIBK)
Carbon disulfide
2-Hexanone
Methyl tert-butyl ether
m-Xylene & p-Xylene
Surrogate
Toluene-d8 (Surr)
4-Bromofluorobenzene
Dibromofluoromethane
TestAmerica Tampa
Analysis Batch: 660-75524
Result (ug/L)
0.15
0.50
0.51
0.77
0.58
0.46
0.47
0.50
2.5
0.18
0.86
0.54
0.50
0.50
9.9
8.4
3.8
0.85
4.4
0.44
0.60
%Rec
101
78
98
Page 20 of 221
Instrument ID:
BVMH GC/MS
Lab File ID:
1HB2729.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
MDL
0.15
0.50
0.51
0.77
0.58
0.46
0.47
0.50
2.5
0.18
0.86
0.54
0.50
0.50
9.9
8.4
3.8
0.85
4.4
0.44
0.60
PQL
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
20
10
10
1.0
10
1.0
2.0
Acceptance Limits
77 - 122
74 - 126
70 - 130
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Client Sample ID:
DMW-O_022509
Lab Sample ID:
Client Matrix:
660-27893-2
Water
Job Number: 660-27893-1
Date Sampled:
Date Received:
02/25/2009 0944
02/26/2009 1030
8260B Volatile Organic Compounds (GC/MS)
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260B
5030B
1.0
02/27/2009 1651
02/27/2009 1651
Analysis Batch: 660-75524
Analyte
Benzene
Bromobenzene
Chlorobromomethane
Dichlorobromomethane
Bromoform
Bromomethane
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
Chlorodibromomethane
1,2-Dibromo-3-Chloropropane
Ethylene Dibromide
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
Hexachlorobutadiene
Isopropylbenzene
4-Isopropyltoluene
Methylene Chloride
Naphthalene
N-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
Result (ug/L)
0.50
0.58
0.58
0.35
0.58
2.5
0.67
0.63
0.84
0.42
0.63
2.5
0.90
1.0
0.65
0.52
0.34
2.5
0.50
0.41
0.44
0.64
0.52
2.5
0.52
0.57
0.45
0.65
0.44
0.52
0.39
0.36
0.31
0.14
0.14
0.44
0.40
0.19
0.69
4.0
2.5
0.59
0.98
0.63
TestAmerica Tampa
Page 21 of 221
Instrument ID:
BVMH GC/MS
Lab File ID:
1HB2730.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
MDL
0.50
0.58
0.58
0.35
0.58
2.5
0.67
0.63
0.84
0.42
0.63
2.5
0.90
1.0
0.65
0.52
0.34
2.5
0.50
0.41
0.44
0.64
0.52
2.5
0.52
0.57
0.45
0.65
0.44
0.52
0.39
0.36
0.31
0.14
0.14
0.44
0.40
0.19
0.69
4.0
2.5
0.59
0.98
0.63
PQL
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
4.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
5.0
1.0
2.0
1.0
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Client Sample ID:
DMW-O_022509
Lab Sample ID:
Client Matrix:
660-27893-2
Water
Job Number: 660-27893-1
Date Sampled:
Date Received:
02/25/2009 0944
02/26/2009 1030
8260B Volatile Organic Compounds (GC/MS)
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260B
5030B
1.0
02/27/2009 1651
02/27/2009 1651
Analyte
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
o-Xylene
Acetone
2-Butanone (MEK)
4-Methyl-2-pentanone (MIBK)
Carbon disulfide
2-Hexanone
Methyl tert-butyl ether
m-Xylene & p-Xylene
Surrogate
Toluene-d8 (Surr)
4-Bromofluorobenzene
Dibromofluoromethane
TestAmerica Tampa
Analysis Batch: 660-75524
Result (ug/L)
0.15
0.50
0.51
0.77
0.58
0.46
0.47
0.50
2.5
0.18
0.86
0.54
0.50
0.50
9.9
8.4
3.8
0.85
4.4
0.44
0.60
%Rec
98
77
101
Page 22 of 221
Instrument ID:
BVMH GC/MS
Lab File ID:
1HB2730.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
MDL
0.15
0.50
0.51
0.77
0.58
0.46
0.47
0.50
2.5
0.18
0.86
0.54
0.50
0.50
9.9
8.4
3.8
0.85
4.4
0.44
0.60
PQL
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
20
10
10
1.0
10
1.0
2.0
Acceptance Limits
77 - 122
74 - 126
70 - 130
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Client Sample ID:
DMW-Q_022509
Lab Sample ID:
Client Matrix:
660-27893-3
Water
Job Number: 660-27893-1
Date Sampled:
Date Received:
02/25/2009 1013
02/26/2009 1030
8260B Volatile Organic Compounds (GC/MS)
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260B
5030B
1.0
02/27/2009 1708
02/27/2009 1708
Analysis Batch: 660-75524
Analyte
Benzene
Bromobenzene
Chlorobromomethane
Dichlorobromomethane
Bromoform
Bromomethane
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
Chlorodibromomethane
1,2-Dibromo-3-Chloropropane
Ethylene Dibromide
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
Hexachlorobutadiene
Isopropylbenzene
4-Isopropyltoluene
Methylene Chloride
Naphthalene
N-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
Result (ug/L)
0.50
0.58
0.58
0.35
0.58
2.5
0.67
0.63
0.84
0.42
0.63
2.5
0.90
1.0
0.65
0.52
0.34
2.5
0.50
0.41
0.44
0.64
0.52
2.5
0.52
0.57
0.45
0.65
0.44
0.52
0.39
0.36
0.31
0.14
0.14
0.44
0.40
0.19
0.69
4.0
2.5
0.59
0.98
0.63
TestAmerica Tampa
Page 23 of 221
Instrument ID:
BVMH GC/MS
Lab File ID:
1HB2731.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
MDL
0.50
0.58
0.58
0.35
0.58
2.5
0.67
0.63
0.84
0.42
0.63
2.5
0.90
1.0
0.65
0.52
0.34
2.5
0.50
0.41
0.44
0.64
0.52
2.5
0.52
0.57
0.45
0.65
0.44
0.52
0.39
0.36
0.31
0.14
0.14
0.44
0.40
0.19
0.69
4.0
2.5
0.59
0.98
0.63
PQL
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
4.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
5.0
1.0
2.0
1.0
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Client Sample ID:
DMW-Q_022509
Lab Sample ID:
Client Matrix:
660-27893-3
Water
Job Number: 660-27893-1
Date Sampled:
Date Received:
02/25/2009 1013
02/26/2009 1030
8260B Volatile Organic Compounds (GC/MS)
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260B
5030B
1.0
02/27/2009 1708
02/27/2009 1708
Analyte
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
o-Xylene
Acetone
2-Butanone (MEK)
4-Methyl-2-pentanone (MIBK)
Carbon disulfide
2-Hexanone
Methyl tert-butyl ether
m-Xylene & p-Xylene
Surrogate
Toluene-d8 (Surr)
4-Bromofluorobenzene
Dibromofluoromethane
TestAmerica Tampa
Analysis Batch: 660-75524
Result (ug/L)
0.15
0.50
0.51
0.77
0.58
0.46
0.47
0.50
2.5
0.18
0.86
0.54
0.50
0.50
45
8.4
3.8
0.85
4.4
0.44
0.60
%Rec
116
82
100
Page 24 of 221
Instrument ID:
BVMH GC/MS
Lab File ID:
1HB2731.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
MDL
0.15
0.50
0.51
0.77
0.58
0.46
0.47
0.50
2.5
0.18
0.86
0.54
0.50
0.50
9.9
8.4
3.8
0.85
4.4
0.44
0.60
PQL
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
20
10
10
1.0
10
1.0
2.0
Acceptance Limits
77 - 122
74 - 126
70 - 130
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Client Sample ID:
DMW-C_022509
Lab Sample ID:
Client Matrix:
660-27893-4
Water
Job Number: 660-27893-1
Date Sampled:
Date Received:
02/25/2009 1112
02/26/2009 1030
8260B Volatile Organic Compounds (GC/MS)
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260B
5030B
1.0
02/27/2009 1725
02/27/2009 1725
Analysis Batch: 660-75524
Analyte
Benzene
Bromobenzene
Chlorobromomethane
Dichlorobromomethane
Bromoform
Bromomethane
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
Chlorodibromomethane
1,2-Dibromo-3-Chloropropane
Ethylene Dibromide
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
Hexachlorobutadiene
Isopropylbenzene
4-Isopropyltoluene
Methylene Chloride
Naphthalene
N-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
Result (ug/L)
0.50
0.58
0.58
0.35
0.58
2.5
0.67
0.63
0.84
0.42
0.63
2.5
0.90
1.0
0.65
0.52
0.34
2.5
0.50
0.41
0.44
0.64
0.52
2.5
0.52
0.57
0.45
0.65
0.44
0.52
0.39
0.36
0.31
0.14
0.14
0.44
0.40
0.19
0.69
4.0
2.5
0.59
0.98
0.63
TestAmerica Tampa
Page 25 of 221
Instrument ID:
BVMH GC/MS
Lab File ID:
1HB2732.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
MDL
0.50
0.58
0.58
0.35
0.58
2.5
0.67
0.63
0.84
0.42
0.63
2.5
0.90
1.0
0.65
0.52
0.34
2.5
0.50
0.41
0.44
0.64
0.52
2.5
0.52
0.57
0.45
0.65
0.44
0.52
0.39
0.36
0.31
0.14
0.14
0.44
0.40
0.19
0.69
4.0
2.5
0.59
0.98
0.63
PQL
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
4.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
5.0
1.0
2.0
1.0
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Client Sample ID:
DMW-C_022509
Lab Sample ID:
Client Matrix:
660-27893-4
Water
Job Number: 660-27893-1
Date Sampled:
Date Received:
02/25/2009 1112
02/26/2009 1030
8260B Volatile Organic Compounds (GC/MS)
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260B
5030B
1.0
02/27/2009 1725
02/27/2009 1725
Analyte
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
o-Xylene
Acetone
2-Butanone (MEK)
4-Methyl-2-pentanone (MIBK)
Carbon disulfide
2-Hexanone
Methyl tert-butyl ether
m-Xylene & p-Xylene
Surrogate
Toluene-d8 (Surr)
4-Bromofluorobenzene
Dibromofluoromethane
TestAmerica Tampa
Analysis Batch: 660-75524
Result (ug/L)
0.15
0.50
0.51
0.77
0.58
0.46
0.47
0.50
2.5
0.18
0.86
0.54
0.50
0.50
9.9
8.4
3.8
0.85
4.4
0.44
0.60
%Rec
105
89
106
Page 26 of 221
Instrument ID:
BVMH GC/MS
Lab File ID:
1HB2732.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
MDL
0.15
0.50
0.51
0.77
0.58
0.46
0.47
0.50
2.5
0.18
0.86
0.54
0.50
0.50
9.9
8.4
3.8
0.85
4.4
0.44
0.60
PQL
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
20
10
10
1.0
10
1.0
2.0
Acceptance Limits
77 - 122
74 - 126
70 - 130
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Client Sample ID:
IMW-D_022509
Lab Sample ID:
Client Matrix:
660-27893-5
Water
Job Number: 660-27893-1
Date Sampled:
Date Received:
02/25/2009 1154
02/26/2009 1030
8260B Volatile Organic Compounds (GC/MS)
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260B
5030B
1.0
02/27/2009 1743
02/27/2009 1743
Analysis Batch: 660-75524
Analyte
Benzene
Bromobenzene
Chlorobromomethane
Dichlorobromomethane
Bromoform
Bromomethane
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
Chlorodibromomethane
1,2-Dibromo-3-Chloropropane
Ethylene Dibromide
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
Hexachlorobutadiene
Isopropylbenzene
4-Isopropyltoluene
Methylene Chloride
Naphthalene
N-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
Result (ug/L)
0.50
0.58
0.58
0.35
0.58
2.5
0.67
0.63
0.84
0.42
0.63
2.5
0.90
1.0
0.65
0.52
0.34
2.5
0.50
0.41
0.44
0.64
0.52
2.5
0.52
0.57
0.45
0.65
0.44
0.52
0.39
0.36
0.31
0.14
0.14
0.44
0.40
0.19
0.69
4.0
2.5
0.59
0.98
0.63
TestAmerica Tampa
Page 27 of 221
Instrument ID:
BVMH GC/MS
Lab File ID:
1HB2733.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
MDL
0.50
0.58
0.58
0.35
0.58
2.5
0.67
0.63
0.84
0.42
0.63
2.5
0.90
1.0
0.65
0.52
0.34
2.5
0.50
0.41
0.44
0.64
0.52
2.5
0.52
0.57
0.45
0.65
0.44
0.52
0.39
0.36
0.31
0.14
0.14
0.44
0.40
0.19
0.69
4.0
2.5
0.59
0.98
0.63
PQL
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
4.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
5.0
1.0
2.0
1.0
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Client Sample ID:
IMW-D_022509
Lab Sample ID:
Client Matrix:
660-27893-5
Water
Job Number: 660-27893-1
Date Sampled:
Date Received:
02/25/2009 1154
02/26/2009 1030
8260B Volatile Organic Compounds (GC/MS)
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260B
5030B
1.0
02/27/2009 1743
02/27/2009 1743
Analyte
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
o-Xylene
Acetone
2-Butanone (MEK)
4-Methyl-2-pentanone (MIBK)
Carbon disulfide
2-Hexanone
Methyl tert-butyl ether
m-Xylene & p-Xylene
Surrogate
Toluene-d8 (Surr)
4-Bromofluorobenzene
Dibromofluoromethane
TestAmerica Tampa
Analysis Batch: 660-75524
Result (ug/L)
0.15
0.50
0.51
0.77
0.58
0.46
0.47
0.50
2.5
0.18
0.86
0.54
0.50
0.50
9.9
8.4
3.8
0.85
4.4
0.44
0.60
%Rec
101
84
95
Page 28 of 221
Instrument ID:
BVMH GC/MS
Lab File ID:
1HB2733.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
MDL
0.15
0.50
0.51
0.77
0.58
0.46
0.47
0.50
2.5
0.18
0.86
0.54
0.50
0.50
9.9
8.4
3.8
0.85
4.4
0.44
0.60
PQL
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
20
10
10
1.0
10
1.0
2.0
Acceptance Limits
77 - 122
74 - 126
70 - 130
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Client Sample ID:
DMW-B_022509
Lab Sample ID:
Client Matrix:
660-27893-6
Water
Job Number: 660-27893-1
Date Sampled:
Date Received:
02/25/2009 1238
02/26/2009 1030
8260B Volatile Organic Compounds (GC/MS)
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260B
5030B
1.0
02/27/2009 1800
02/27/2009 1800
Analysis Batch: 660-75524
Analyte
Benzene
Bromobenzene
Chlorobromomethane
Dichlorobromomethane
Bromoform
Bromomethane
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
Chlorodibromomethane
1,2-Dibromo-3-Chloropropane
Ethylene Dibromide
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
Hexachlorobutadiene
Isopropylbenzene
4-Isopropyltoluene
Methylene Chloride
Naphthalene
N-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
Result (ug/L)
0.50
0.58
0.58
0.35
0.58
2.5
0.67
0.63
0.84
0.42
0.63
2.5
0.90
1.0
0.65
0.52
0.34
2.5
0.50
0.41
0.44
0.64
0.52
2.5
0.52
0.57
0.45
0.65
0.44
0.52
0.39
0.36
0.31
0.14
0.14
0.44
0.40
0.19
0.69
4.0
2.5
0.59
0.98
0.63
TestAmerica Tampa
Page 29 of 221
Instrument ID:
BVMH GC/MS
Lab File ID:
1HB2734.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
MDL
0.50
0.58
0.58
0.35
0.58
2.5
0.67
0.63
0.84
0.42
0.63
2.5
0.90
1.0
0.65
0.52
0.34
2.5
0.50
0.41
0.44
0.64
0.52
2.5
0.52
0.57
0.45
0.65
0.44
0.52
0.39
0.36
0.31
0.14
0.14
0.44
0.40
0.19
0.69
4.0
2.5
0.59
0.98
0.63
PQL
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
4.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
5.0
1.0
2.0
1.0
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Client Sample ID:
DMW-B_022509
Lab Sample ID:
Client Matrix:
660-27893-6
Water
Job Number: 660-27893-1
Date Sampled:
Date Received:
02/25/2009 1238
02/26/2009 1030
8260B Volatile Organic Compounds (GC/MS)
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260B
5030B
1.0
02/27/2009 1800
02/27/2009 1800
Analyte
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
o-Xylene
Acetone
2-Butanone (MEK)
4-Methyl-2-pentanone (MIBK)
Carbon disulfide
2-Hexanone
Methyl tert-butyl ether
m-Xylene & p-Xylene
Surrogate
Toluene-d8 (Surr)
4-Bromofluorobenzene
Dibromofluoromethane
TestAmerica Tampa
Analysis Batch: 660-75524
Result (ug/L)
0.15
0.50
0.51
0.77
0.58
0.46
0.47
0.50
2.5
0.18
0.86
0.54
0.50
0.50
9.9
8.4
3.8
0.85
4.4
0.44
0.60
%Rec
105
81
101
Page 30 of 221
Instrument ID:
BVMH GC/MS
Lab File ID:
1HB2734.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
MDL
0.15
0.50
0.51
0.77
0.58
0.46
0.47
0.50
2.5
0.18
0.86
0.54
0.50
0.50
9.9
8.4
3.8
0.85
4.4
0.44
0.60
PQL
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
20
10
10
1.0
10
1.0
2.0
Acceptance Limits
77 - 122
74 - 126
70 - 130
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Client Sample ID:
IDPT-15_022509
Lab Sample ID:
Client Matrix:
660-27893-7
Water
Job Number: 660-27893-1
Date Sampled:
Date Received:
02/25/2009 1425
02/26/2009 1030
8260B Volatile Organic Compounds (GC/MS)
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260B
5030B
1.0
02/27/2009 1817
02/27/2009 1817
Analysis Batch: 660-75524
Analyte
Benzene
Bromobenzene
Chlorobromomethane
Dichlorobromomethane
Bromoform
Bromomethane
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
Chlorodibromomethane
1,2-Dibromo-3-Chloropropane
Ethylene Dibromide
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
Hexachlorobutadiene
Isopropylbenzene
4-Isopropyltoluene
Methylene Chloride
Naphthalene
N-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
Result (ug/L)
0.50
0.58
0.58
0.35
0.58
2.5
0.67
0.63
0.84
0.42
0.63
2.5
0.90
1.0
0.65
0.52
0.34
2.5
0.50
0.41
0.44
0.64
0.52
2.5
4.3
0.57
0.45
0.65
0.44
0.52
0.39
0.36
0.31
0.14
0.14
0.44
0.40
0.19
0.69
4.0
2.5
0.59
0.98
0.63
TestAmerica Tampa
Page 31 of 221
Instrument ID:
BVMH GC/MS
Lab File ID:
1HB2735.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
MDL
0.50
0.58
0.58
0.35
0.58
2.5
0.67
0.63
0.84
0.42
0.63
2.5
0.90
1.0
0.65
0.52
0.34
2.5
0.50
0.41
0.44
0.64
0.52
2.5
0.52
0.57
0.45
0.65
0.44
0.52
0.39
0.36
0.31
0.14
0.14
0.44
0.40
0.19
0.69
4.0
2.5
0.59
0.98
0.63
PQL
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
4.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
5.0
1.0
2.0
1.0
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Client Sample ID:
IDPT-15_022509
Lab Sample ID:
Client Matrix:
660-27893-7
Water
Job Number: 660-27893-1
Date Sampled:
Date Received:
02/25/2009 1425
02/26/2009 1030
8260B Volatile Organic Compounds (GC/MS)
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260B
5030B
1.0
02/27/2009 1817
02/27/2009 1817
Analyte
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
o-Xylene
Acetone
2-Butanone (MEK)
4-Methyl-2-pentanone (MIBK)
Carbon disulfide
2-Hexanone
Methyl tert-butyl ether
m-Xylene & p-Xylene
Surrogate
Toluene-d8 (Surr)
4-Bromofluorobenzene
Dibromofluoromethane
TestAmerica Tampa
Analysis Batch: 660-75524
Result (ug/L)
0.15
0.50
0.51
0.77
0.58
0.46
0.47
0.50
2.5
0.18
0.86
0.54
0.50
0.50
9.9
8.4
3.8
0.85
4.4
0.44
0.60
%Rec
107
86
103
Page 32 of 221
Instrument ID:
BVMH GC/MS
Lab File ID:
1HB2735.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
MDL
0.15
0.50
0.51
0.77
0.58
0.46
0.47
0.50
2.5
0.18
0.86
0.54
0.50
0.50
9.9
8.4
3.8
0.85
4.4
0.44
0.60
PQL
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
20
10
10
1.0
10
1.0
2.0
Acceptance Limits
77 - 122
74 - 126
70 - 130
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Client Sample ID:
DMW-8_022509
Lab Sample ID:
Client Matrix:
660-27893-8
Water
Job Number: 660-27893-1
Date Sampled:
Date Received:
02/25/2009 1553
02/26/2009 1030
8260B Volatile Organic Compounds (GC/MS)
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260B
5030B
1.0
02/27/2009 1834
02/27/2009 1834
Analysis Batch: 660-75524
Analyte
Benzene
Bromobenzene
Chlorobromomethane
Dichlorobromomethane
Bromoform
Bromomethane
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
Chlorodibromomethane
1,2-Dibromo-3-Chloropropane
Ethylene Dibromide
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
Hexachlorobutadiene
Isopropylbenzene
4-Isopropyltoluene
Methylene Chloride
Naphthalene
N-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
Result (ug/L)
0.50
0.58
0.58
0.35
0.58
2.5
0.67
0.63
0.84
0.42
0.63
2.5
0.90
1.0
0.65
0.52
0.34
2.5
0.50
0.41
0.44
0.64
0.52
2.5
0.52
0.57
0.45
0.65
0.44
0.52
0.39
0.36
0.31
0.14
0.14
0.44
0.40
0.19
0.69
4.0
2.5
0.59
0.98
0.63
TestAmerica Tampa
Page 33 of 221
Instrument ID:
BVMH GC/MS
Lab File ID:
1HB2736.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
MDL
0.50
0.58
0.58
0.35
0.58
2.5
0.67
0.63
0.84
0.42
0.63
2.5
0.90
1.0
0.65
0.52
0.34
2.5
0.50
0.41
0.44
0.64
0.52
2.5
0.52
0.57
0.45
0.65
0.44
0.52
0.39
0.36
0.31
0.14
0.14
0.44
0.40
0.19
0.69
4.0
2.5
0.59
0.98
0.63
PQL
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
4.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
5.0
1.0
2.0
1.0
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Client Sample ID:
DMW-8_022509
Lab Sample ID:
Client Matrix:
660-27893-8
Water
Job Number: 660-27893-1
Date Sampled:
Date Received:
02/25/2009 1553
02/26/2009 1030
8260B Volatile Organic Compounds (GC/MS)
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260B
5030B
1.0
02/27/2009 1834
02/27/2009 1834
Analyte
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
o-Xylene
Acetone
2-Butanone (MEK)
4-Methyl-2-pentanone (MIBK)
Carbon disulfide
2-Hexanone
Methyl tert-butyl ether
m-Xylene & p-Xylene
Surrogate
Toluene-d8 (Surr)
4-Bromofluorobenzene
Dibromofluoromethane
TestAmerica Tampa
Analysis Batch: 660-75524
Result (ug/L)
0.15
0.50
0.51
0.77
0.58
0.46
0.47
0.50
2.5
0.18
0.86
0.54
0.50
0.50
9.9
8.4
3.8
0.85
4.4
0.44
0.60
%Rec
104
88
101
Page 34 of 221
Instrument ID:
BVMH GC/MS
Lab File ID:
1HB2736.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
MDL
0.15
0.50
0.51
0.77
0.58
0.46
0.47
0.50
2.5
0.18
0.86
0.54
0.50
0.50
9.9
8.4
3.8
0.85
4.4
0.44
0.60
PQL
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
20
10
10
1.0
10
1.0
2.0
Acceptance Limits
77 - 122
74 - 126
70 - 130
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Client Sample ID:
SMW-D_022509
Lab Sample ID:
Client Matrix:
660-27893-9
Water
Job Number: 660-27893-1
Date Sampled:
Date Received:
02/25/2009 1614
02/26/2009 1030
8260B Volatile Organic Compounds (GC/MS)
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260B
5030B
1.0
03/02/2009 1229
03/02/2009 1229
Analysis Batch: 660-75614
Analyte
Benzene
Bromobenzene
Chlorobromomethane
Dichlorobromomethane
Bromoform
Bromomethane
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
Chlorodibromomethane
1,2-Dibromo-3-Chloropropane
Ethylene Dibromide
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
Hexachlorobutadiene
Isopropylbenzene
4-Isopropyltoluene
Methylene Chloride
Naphthalene
N-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
Result (ug/L)
0.50
0.58
0.58
0.35
0.58
2.5
0.67
0.63
0.84
0.42
0.63
2.5
0.90
1.0
0.65
0.52
0.34
2.5
0.50
0.41
0.44
0.64
0.52
2.5
0.52
0.57
0.45
0.65
0.44
0.52
0.39
0.36
0.31
0.14
0.14
0.44
0.40
0.19
0.69
4.0
2.5
0.59
0.98
0.63
TestAmerica Tampa
Page 35 of 221
Instrument ID:
BVMH GC/MS
Lab File ID:
1HC0215.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
MDL
0.50
0.58
0.58
0.35
0.58
2.5
0.67
0.63
0.84
0.42
0.63
2.5
0.90
1.0
0.65
0.52
0.34
2.5
0.50
0.41
0.44
0.64
0.52
2.5
0.52
0.57
0.45
0.65
0.44
0.52
0.39
0.36
0.31
0.14
0.14
0.44
0.40
0.19
0.69
4.0
2.5
0.59
0.98
0.63
PQL
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
4.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
5.0
1.0
2.0
1.0
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Client Sample ID:
SMW-D_022509
Lab Sample ID:
Client Matrix:
660-27893-9
Water
Job Number: 660-27893-1
Date Sampled:
Date Received:
02/25/2009 1614
02/26/2009 1030
8260B Volatile Organic Compounds (GC/MS)
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260B
5030B
1.0
03/02/2009 1229
03/02/2009 1229
Analyte
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
o-Xylene
Acetone
2-Butanone (MEK)
4-Methyl-2-pentanone (MIBK)
Carbon disulfide
2-Hexanone
Methyl tert-butyl ether
m-Xylene & p-Xylene
Surrogate
Toluene-d8 (Surr)
4-Bromofluorobenzene
Dibromofluoromethane
TestAmerica Tampa
Analysis Batch: 660-75614
Result (ug/L)
0.15
0.50
0.51
0.77
0.58
0.46
0.47
0.50
2.5
0.18
0.86
0.54
0.50
0.50
9.9
8.4
3.8
0.85
4.4
0.44
0.60
%Rec
101
79
105
Page 36 of 221
Instrument ID:
BVMH GC/MS
Lab File ID:
1HC0215.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
MDL
0.15
0.50
0.51
0.77
0.58
0.46
0.47
0.50
2.5
0.18
0.86
0.54
0.50
0.50
9.9
8.4
3.8
0.85
4.4
0.44
0.60
PQL
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
20
10
10
1.0
10
1.0
2.0
Acceptance Limits
77 - 122
74 - 126
70 - 130
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Client Sample ID:
IDPT-8_022509
Lab Sample ID:
Client Matrix:
660-27893-10
Water
Job Number: 660-27893-1
Date Sampled:
Date Received:
02/25/2009 1648
02/26/2009 1030
8260B Volatile Organic Compounds (GC/MS)
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260B
5030B
1.0
03/02/2009 1212
03/02/2009 1212
Analysis Batch: 660-75614
Analyte
Benzene
Bromobenzene
Chlorobromomethane
Dichlorobromomethane
Bromoform
Bromomethane
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
Chlorodibromomethane
1,2-Dibromo-3-Chloropropane
Ethylene Dibromide
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
Hexachlorobutadiene
Isopropylbenzene
4-Isopropyltoluene
Methylene Chloride
Naphthalene
N-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
Result (ug/L)
0.50
0.58
0.58
0.35
0.58
2.5
0.67
0.63
0.84
0.42
0.63
2.5
0.90
1.0
0.65
0.52
0.34
2.5
0.50
0.41
0.44
0.64
0.52
2.5
1.9
0.57
0.45
0.65
0.44
0.52
0.39
0.36
0.31
0.14
0.14
0.44
0.40
0.19
0.69
4.0
2.5
0.59
0.98
0.63
TestAmerica Tampa
Page 37 of 221
Instrument ID:
BVMH GC/MS
Lab File ID:
1HC0214.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
MDL
0.50
0.58
0.58
0.35
0.58
2.5
0.67
0.63
0.84
0.42
0.63
2.5
0.90
1.0
0.65
0.52
0.34
2.5
0.50
0.41
0.44
0.64
0.52
2.5
0.52
0.57
0.45
0.65
0.44
0.52
0.39
0.36
0.31
0.14
0.14
0.44
0.40
0.19
0.69
4.0
2.5
0.59
0.98
0.63
PQL
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
4.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
5.0
1.0
2.0
1.0
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Client Sample ID:
IDPT-8_022509
Lab Sample ID:
Client Matrix:
660-27893-10
Water
Job Number: 660-27893-1
Date Sampled:
Date Received:
02/25/2009 1648
02/26/2009 1030
8260B Volatile Organic Compounds (GC/MS)
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260B
5030B
1.0
03/02/2009 1212
03/02/2009 1212
Analyte
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
o-Xylene
Acetone
2-Butanone (MEK)
4-Methyl-2-pentanone (MIBK)
Carbon disulfide
2-Hexanone
Methyl tert-butyl ether
m-Xylene & p-Xylene
Surrogate
Toluene-d8 (Surr)
4-Bromofluorobenzene
Dibromofluoromethane
TestAmerica Tampa
Analysis Batch: 660-75614
Result (ug/L)
0.15
0.50
0.51
0.77
0.58
0.46
0.47
0.50
2.5
0.18
0.86
0.54
0.50
0.50
9.9
8.4
3.8
0.85
4.4
0.44
0.60
%Rec
92
82
107
Page 38 of 221
Instrument ID:
BVMH GC/MS
Lab File ID:
1HC0214.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
MDL
0.15
0.50
0.51
0.77
0.58
0.46
0.47
0.50
2.5
0.18
0.86
0.54
0.50
0.50
9.9
8.4
3.8
0.85
4.4
0.44
0.60
PQL
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
20
10
10
1.0
10
1.0
2.0
Acceptance Limits
77 - 122
74 - 126
70 - 130
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Client Sample ID:
IDPT-9_022509
Lab Sample ID:
Client Matrix:
660-27893-11
Water
Job Number: 660-27893-1
Date Sampled:
Date Received:
02/25/2009 1730
02/26/2009 1030
8260B Volatile Organic Compounds (GC/MS)
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260B
5030B
1.0
03/02/2009 1247
03/02/2009 1247
Analysis Batch: 660-75614
Analyte
Benzene
Bromobenzene
Chlorobromomethane
Dichlorobromomethane
Bromoform
Bromomethane
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
Chlorodibromomethane
1,2-Dibromo-3-Chloropropane
Ethylene Dibromide
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
Hexachlorobutadiene
Isopropylbenzene
4-Isopropyltoluene
Methylene Chloride
Naphthalene
N-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
Result (ug/L)
0.50
0.58
0.58
0.35
0.58
2.5
0.67
0.63
0.84
0.42
0.63
2.5
0.90
1.0
0.65
0.52
0.34
2.5
0.50
0.41
0.44
0.64
0.52
2.5
0.52
0.57
0.45
0.65
0.44
0.52
0.39
0.36
0.31
0.14
0.14
0.44
0.40
0.19
0.69
4.0
2.5
0.59
0.98
0.63
TestAmerica Tampa
Page 39 of 221
Instrument ID:
BVMH GC/MS
Lab File ID:
1HC0216.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
MDL
0.50
0.58
0.58
0.35
0.58
2.5
0.67
0.63
0.84
0.42
0.63
2.5
0.90
1.0
0.65
0.52
0.34
2.5
0.50
0.41
0.44
0.64
0.52
2.5
0.52
0.57
0.45
0.65
0.44
0.52
0.39
0.36
0.31
0.14
0.14
0.44
0.40
0.19
0.69
4.0
2.5
0.59
0.98
0.63
PQL
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
4.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
5.0
1.0
2.0
1.0
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Client Sample ID:
IDPT-9_022509
Lab Sample ID:
Client Matrix:
660-27893-11
Water
Job Number: 660-27893-1
Date Sampled:
Date Received:
02/25/2009 1730
02/26/2009 1030
8260B Volatile Organic Compounds (GC/MS)
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260B
5030B
1.0
03/02/2009 1247
03/02/2009 1247
Analyte
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
o-Xylene
Acetone
2-Butanone (MEK)
4-Methyl-2-pentanone (MIBK)
Carbon disulfide
2-Hexanone
Methyl tert-butyl ether
m-Xylene & p-Xylene
Surrogate
Toluene-d8 (Surr)
4-Bromofluorobenzene
Dibromofluoromethane
TestAmerica Tampa
Analysis Batch: 660-75614
Result (ug/L)
0.15
0.50
0.51
0.77
0.58
0.46
0.47
0.50
2.5
0.18
0.86
0.54
0.50
0.50
9.9
8.4
3.8
0.85
4.4
0.44
0.60
%Rec
101
86
108
Page 40 of 221
Instrument ID:
BVMH GC/MS
Lab File ID:
1HC0216.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
MDL
0.15
0.50
0.51
0.77
0.58
0.46
0.47
0.50
2.5
0.18
0.86
0.54
0.50
0.50
9.9
8.4
3.8
0.85
4.4
0.44
0.60
PQL
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
20
10
10
1.0
10
1.0
2.0
Acceptance Limits
77 - 122
74 - 126
70 - 130
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Client Sample ID:
SMW-E_022509
Lab Sample ID:
Client Matrix:
660-27893-12
Water
Job Number: 660-27893-1
Date Sampled:
Date Received:
02/25/2009 1814
02/26/2009 1030
8260B Volatile Organic Compounds (GC/MS)
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260B
5030B
1.0
03/02/2009 1304
03/02/2009 1304
Analysis Batch: 660-75614
Analyte
Benzene
Bromobenzene
Chlorobromomethane
Dichlorobromomethane
Bromoform
Bromomethane
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
Chlorodibromomethane
1,2-Dibromo-3-Chloropropane
Ethylene Dibromide
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
Hexachlorobutadiene
Isopropylbenzene
4-Isopropyltoluene
Methylene Chloride
Naphthalene
N-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
Result (ug/L)
0.50
0.58
0.58
0.35
0.58
2.5
0.67
0.63
0.84
0.42
0.63
2.5
0.90
1.0
0.65
0.52
0.34
2.5
0.50
0.41
0.44
0.64
0.52
2.5
0.52
0.57
0.45
0.65
0.44
0.52
0.39
0.36
0.31
0.14
0.14
0.44
0.40
0.19
0.69
4.0
2.5
0.59
0.98
0.63
TestAmerica Tampa
Page 41 of 221
Instrument ID:
BVMH GC/MS
Lab File ID:
1HC0217.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
MDL
0.50
0.58
0.58
0.35
0.58
2.5
0.67
0.63
0.84
0.42
0.63
2.5
0.90
1.0
0.65
0.52
0.34
2.5
0.50
0.41
0.44
0.64
0.52
2.5
0.52
0.57
0.45
0.65
0.44
0.52
0.39
0.36
0.31
0.14
0.14
0.44
0.40
0.19
0.69
4.0
2.5
0.59
0.98
0.63
PQL
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
4.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
5.0
1.0
2.0
1.0
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Client Sample ID:
SMW-E_022509
Lab Sample ID:
Client Matrix:
660-27893-12
Water
Job Number: 660-27893-1
Date Sampled:
Date Received:
02/25/2009 1814
02/26/2009 1030
8260B Volatile Organic Compounds (GC/MS)
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260B
5030B
1.0
03/02/2009 1304
03/02/2009 1304
Analyte
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
o-Xylene
Acetone
2-Butanone (MEK)
4-Methyl-2-pentanone (MIBK)
Carbon disulfide
2-Hexanone
Methyl tert-butyl ether
m-Xylene & p-Xylene
Surrogate
Toluene-d8 (Surr)
4-Bromofluorobenzene
Dibromofluoromethane
TestAmerica Tampa
Analysis Batch: 660-75614
Result (ug/L)
0.15
0.50
0.51
0.77
0.58
0.46
0.47
0.50
2.5
0.18
0.86
0.54
0.50
0.50
9.9
8.4
3.8
0.85
4.4
0.44
0.60
%Rec
99
87
108
Page 42 of 221
Instrument ID:
BVMH GC/MS
Lab File ID:
1HC0217.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
MDL
0.15
0.50
0.51
0.77
0.58
0.46
0.47
0.50
2.5
0.18
0.86
0.54
0.50
0.50
9.9
8.4
3.8
0.85
4.4
0.44
0.60
PQL
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
20
10
10
1.0
10
1.0
2.0
Acceptance Limits
77 - 122
74 - 126
70 - 130
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Client Sample ID:
SMW-H_022509
Lab Sample ID:
Client Matrix:
660-27893-13
Water
Job Number: 660-27893-1
Date Sampled:
Date Received:
02/25/2009 1405
02/26/2009 1030
8260B Volatile Organic Compounds (GC/MS)
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260B
5030B
1.0
03/02/2009 1739
03/02/2009 1739
Analysis Batch: 660-75614
Analyte
Benzene
Bromobenzene
Chlorobromomethane
Dichlorobromomethane
Bromoform
Bromomethane
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
Chlorodibromomethane
1,2-Dibromo-3-Chloropropane
Ethylene Dibromide
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
Hexachlorobutadiene
Isopropylbenzene
4-Isopropyltoluene
Methylene Chloride
Naphthalene
N-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
Result (ug/L)
0.50
0.58
0.58
0.35
0.58
2.5
0.67
0.63
0.84
0.42
0.63
2.5
0.90
1.0
0.65
0.52
0.34
2.5
0.50
0.41
0.44
0.64
0.52
2.5
0.52
0.57
0.45
0.65
0.44
0.52
0.39
0.36
0.31
0.14
0.14
0.44
0.40
0.19
0.69
4.0
2.5
0.59
0.98
0.63
TestAmerica Tampa
Page 43 of 221
Instrument ID:
BVMH GC/MS
Lab File ID:
1HC0233.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
MDL
0.50
0.58
0.58
0.35
0.58
2.5
0.67
0.63
0.84
0.42
0.63
2.5
0.90
1.0
0.65
0.52
0.34
2.5
0.50
0.41
0.44
0.64
0.52
2.5
0.52
0.57
0.45
0.65
0.44
0.52
0.39
0.36
0.31
0.14
0.14
0.44
0.40
0.19
0.69
4.0
2.5
0.59
0.98
0.63
PQL
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
4.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
5.0
1.0
2.0
1.0
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Client Sample ID:
SMW-H_022509
Lab Sample ID:
Client Matrix:
660-27893-13
Water
Job Number: 660-27893-1
Date Sampled:
Date Received:
02/25/2009 1405
02/26/2009 1030
8260B Volatile Organic Compounds (GC/MS)
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260B
5030B
1.0
03/02/2009 1739
03/02/2009 1739
Analyte
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
o-Xylene
Acetone
2-Butanone (MEK)
4-Methyl-2-pentanone (MIBK)
Carbon disulfide
2-Hexanone
Methyl tert-butyl ether
m-Xylene & p-Xylene
Surrogate
Toluene-d8 (Surr)
4-Bromofluorobenzene
Dibromofluoromethane
TestAmerica Tampa
Analysis Batch: 660-75614
Result (ug/L)
0.15
0.50
0.51
0.77
0.58
0.46
0.47
0.50
2.5
0.18
0.86
0.54
0.50
0.50
9.9
8.4
3.8
0.85
4.4
0.44
0.60
%Rec
95
86
107
Page 44 of 221
Instrument ID:
BVMH GC/MS
Lab File ID:
1HC0233.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
MDL
0.15
0.50
0.51
0.77
0.58
0.46
0.47
0.50
2.5
0.18
0.86
0.54
0.50
0.50
9.9
8.4
3.8
0.85
4.4
0.44
0.60
PQL
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
20
10
10
1.0
10
1.0
2.0
Acceptance Limits
77 - 122
74 - 126
70 - 130
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Client Sample ID:
DMW-N_022509
Lab Sample ID:
Client Matrix:
660-27893-14
Water
Job Number: 660-27893-1
Date Sampled:
Date Received:
02/25/2009 1055
02/26/2009 1030
8260B Volatile Organic Compounds (GC/MS)
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260B
5030B
1.0
03/02/2009 1321
03/02/2009 1321
Analysis Batch: 660-75614
Analyte
Benzene
Bromobenzene
Chlorobromomethane
Dichlorobromomethane
Bromoform
Bromomethane
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
Chlorodibromomethane
1,2-Dibromo-3-Chloropropane
Ethylene Dibromide
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
Hexachlorobutadiene
Isopropylbenzene
4-Isopropyltoluene
Methylene Chloride
Naphthalene
N-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
Result (ug/L)
0.50
0.58
0.58
0.35
0.58
2.5
0.67
0.63
0.84
0.42
0.63
2.5
0.90
1.1
0.65
0.52
0.34
2.5
0.50
0.41
0.44
0.64
0.52
2.5
0.52
0.57
0.45
0.65
0.44
0.52
0.39
0.36
0.31
0.14
0.14
0.44
0.40
0.19
0.69
4.0
2.5
0.59
0.98
0.63
TestAmerica Tampa
Page 45 of 221
Instrument ID:
BVMH GC/MS
Lab File ID:
1HC0218.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
U
U
U
U
U
U
U
U
U
U
U
U
U
I
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
MDL
0.50
0.58
0.58
0.35
0.58
2.5
0.67
0.63
0.84
0.42
0.63
2.5
0.90
1.0
0.65
0.52
0.34
2.5
0.50
0.41
0.44
0.64
0.52
2.5
0.52
0.57
0.45
0.65
0.44
0.52
0.39
0.36
0.31
0.14
0.14
0.44
0.40
0.19
0.69
4.0
2.5
0.59
0.98
0.63
PQL
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
4.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
5.0
1.0
2.0
1.0
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Client Sample ID:
DMW-N_022509
Lab Sample ID:
Client Matrix:
660-27893-14
Water
Job Number: 660-27893-1
Date Sampled:
Date Received:
02/25/2009 1055
02/26/2009 1030
8260B Volatile Organic Compounds (GC/MS)
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260B
5030B
1.0
03/02/2009 1321
03/02/2009 1321
Analyte
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
o-Xylene
Acetone
2-Butanone (MEK)
4-Methyl-2-pentanone (MIBK)
Carbon disulfide
2-Hexanone
Methyl tert-butyl ether
m-Xylene & p-Xylene
Surrogate
Toluene-d8 (Surr)
4-Bromofluorobenzene
Dibromofluoromethane
TestAmerica Tampa
Analysis Batch: 660-75614
Result (ug/L)
0.15
0.50
0.51
0.77
0.58
0.46
0.47
0.50
2.5
0.18
0.86
0.54
0.50
0.50
9.9
8.4
3.8
0.85
4.4
0.44
0.60
%Rec
94
84
110
Page 46 of 221
Instrument ID:
BVMH GC/MS
Lab File ID:
1HC0218.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
MDL
0.15
0.50
0.51
0.77
0.58
0.46
0.47
0.50
2.5
0.18
0.86
0.54
0.50
0.50
9.9
8.4
3.8
0.85
4.4
0.44
0.60
PQL
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
20
10
10
1.0
10
1.0
2.0
Acceptance Limits
77 - 122
74 - 126
70 - 130
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Client Sample ID:
DUPE E_022509
Lab Sample ID:
Client Matrix:
660-27893-15
Water
Job Number: 660-27893-1
Date Sampled:
Date Received:
02/25/2009 0000
02/26/2009 1030
8260B Volatile Organic Compounds (GC/MS)
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260B
5030B
1.0
03/02/2009 1447
03/02/2009 1447
Analysis Batch: 660-75614
Analyte
Benzene
Bromobenzene
Chlorobromomethane
Dichlorobromomethane
Bromoform
Bromomethane
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
Chlorodibromomethane
1,2-Dibromo-3-Chloropropane
Ethylene Dibromide
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
Hexachlorobutadiene
Isopropylbenzene
4-Isopropyltoluene
Methylene Chloride
Naphthalene
N-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
Result (ug/L)
0.50
0.58
0.58
0.35
0.58
2.5
0.67
0.63
0.84
0.42
0.63
2.5
0.90
1.0
0.65
0.52
0.34
2.5
0.50
0.41
0.44
0.64
0.52
2.5
0.52
0.57
0.45
0.65
0.44
0.52
0.39
0.36
0.31
0.14
0.14
0.44
0.40
0.19
0.69
4.0
2.5
0.59
0.98
0.63
TestAmerica Tampa
Page 47 of 221
Instrument ID:
BVMH GC/MS
Lab File ID:
1HC0223.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
MDL
0.50
0.58
0.58
0.35
0.58
2.5
0.67
0.63
0.84
0.42
0.63
2.5
0.90
1.0
0.65
0.52
0.34
2.5
0.50
0.41
0.44
0.64
0.52
2.5
0.52
0.57
0.45
0.65
0.44
0.52
0.39
0.36
0.31
0.14
0.14
0.44
0.40
0.19
0.69
4.0
2.5
0.59
0.98
0.63
PQL
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
4.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
5.0
1.0
2.0
1.0
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Client Sample ID:
DUPE E_022509
Lab Sample ID:
Client Matrix:
660-27893-15
Water
Job Number: 660-27893-1
Date Sampled:
Date Received:
02/25/2009 0000
02/26/2009 1030
8260B Volatile Organic Compounds (GC/MS)
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260B
5030B
1.0
03/02/2009 1447
03/02/2009 1447
Analyte
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
o-Xylene
Acetone
2-Butanone (MEK)
4-Methyl-2-pentanone (MIBK)
Carbon disulfide
2-Hexanone
Methyl tert-butyl ether
m-Xylene & p-Xylene
Surrogate
Toluene-d8 (Surr)
4-Bromofluorobenzene
Dibromofluoromethane
TestAmerica Tampa
Analysis Batch: 660-75614
Result (ug/L)
0.15
0.50
0.51
0.77
0.58
0.46
0.47
0.50
2.5
0.18
0.86
0.54
0.50
0.50
9.9
8.4
3.8
0.85
4.4
0.44
0.60
%Rec
103
90
106
Page 48 of 221
Instrument ID:
BVMH GC/MS
Lab File ID:
1HC0223.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
MDL
0.15
0.50
0.51
0.77
0.58
0.46
0.47
0.50
2.5
0.18
0.86
0.54
0.50
0.50
9.9
8.4
3.8
0.85
4.4
0.44
0.60
PQL
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
20
10
10
1.0
10
1.0
2.0
Acceptance Limits
77 - 122
74 - 126
70 - 130
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Client Sample ID:
SMW-I_022509
Lab Sample ID:
Client Matrix:
660-27893-16
Water
Job Number: 660-27893-1
Date Sampled:
Date Received:
02/25/2009 1130
02/26/2009 1030
8260B Volatile Organic Compounds (GC/MS)
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260B
5030B
1.0
03/02/2009 1430
03/02/2009 1430
Analysis Batch: 660-75614
Analyte
Benzene
Bromobenzene
Chlorobromomethane
Dichlorobromomethane
Bromoform
Bromomethane
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
Chlorodibromomethane
1,2-Dibromo-3-Chloropropane
Ethylene Dibromide
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
Hexachlorobutadiene
Isopropylbenzene
4-Isopropyltoluene
Methylene Chloride
Naphthalene
N-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
Result (ug/L)
0.50
0.58
0.58
0.35
0.58
2.5
0.67
0.63
0.84
0.42
0.63
2.5
0.90
1.0
0.65
0.52
0.34
2.5
0.50
0.41
0.44
0.64
0.52
2.5
0.52
0.57
0.45
0.65
0.44
0.52
0.39
0.36
0.31
0.14
0.14
0.44
0.40
0.19
0.69
4.0
2.5
0.59
0.98
0.63
TestAmerica Tampa
Page 49 of 221
Instrument ID:
BVMH GC/MS
Lab File ID:
1HC0222.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
MDL
0.50
0.58
0.58
0.35
0.58
2.5
0.67
0.63
0.84
0.42
0.63
2.5
0.90
1.0
0.65
0.52
0.34
2.5
0.50
0.41
0.44
0.64
0.52
2.5
0.52
0.57
0.45
0.65
0.44
0.52
0.39
0.36
0.31
0.14
0.14
0.44
0.40
0.19
0.69
4.0
2.5
0.59
0.98
0.63
PQL
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
4.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
5.0
1.0
2.0
1.0
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Client Sample ID:
SMW-I_022509
Lab Sample ID:
Client Matrix:
660-27893-16
Water
Job Number: 660-27893-1
Date Sampled:
Date Received:
02/25/2009 1130
02/26/2009 1030
8260B Volatile Organic Compounds (GC/MS)
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260B
5030B
1.0
03/02/2009 1430
03/02/2009 1430
Analyte
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
o-Xylene
Acetone
2-Butanone (MEK)
4-Methyl-2-pentanone (MIBK)
Carbon disulfide
2-Hexanone
Methyl tert-butyl ether
m-Xylene & p-Xylene
Surrogate
Toluene-d8 (Surr)
4-Bromofluorobenzene
Dibromofluoromethane
TestAmerica Tampa
Analysis Batch: 660-75614
Result (ug/L)
0.15
0.50
0.51
0.77
0.58
0.46
0.47
0.50
2.5
0.18
0.86
0.54
0.50
0.50
9.9
8.4
3.8
0.85
4.4
0.44
0.60
%Rec
103
87
106
Page 50 of 221
Instrument ID:
BVMH GC/MS
Lab File ID:
1HC0222.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
MDL
0.15
0.50
0.51
0.77
0.58
0.46
0.47
0.50
2.5
0.18
0.86
0.54
0.50
0.50
9.9
8.4
3.8
0.85
4.4
0.44
0.60
PQL
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
20
10
10
1.0
10
1.0
2.0
Acceptance Limits
77 - 122
74 - 126
70 - 130
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Client Sample ID:
DMW-I_022509
Lab Sample ID:
Client Matrix:
660-27893-17
Water
Job Number: 660-27893-1
Date Sampled:
Date Received:
02/25/2009 1440
02/26/2009 1030
8260B Volatile Organic Compounds (GC/MS)
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260B
5030B
1.0
03/02/2009 1338
03/02/2009 1338
Analysis Batch: 660-75614
Analyte
Benzene
Bromobenzene
Chlorobromomethane
Dichlorobromomethane
Bromoform
Bromomethane
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
Chlorodibromomethane
1,2-Dibromo-3-Chloropropane
Ethylene Dibromide
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
Hexachlorobutadiene
Isopropylbenzene
4-Isopropyltoluene
Methylene Chloride
Naphthalene
N-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
Result (ug/L)
0.50
0.58
0.58
0.35
0.58
2.5
0.67
0.63
0.84
0.42
0.63
2.5
0.90
1.0
0.65
0.52
0.34
2.5
0.50
0.41
0.44
0.64
0.52
2.5
0.52
0.57
0.45
0.65
0.44
0.52
0.39
0.36
0.31
0.14
0.14
0.44
0.40
0.19
0.69
4.0
2.5
0.59
0.98
0.63
TestAmerica Tampa
Page 51 of 221
Instrument ID:
BVMH GC/MS
Lab File ID:
1HC0219.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
MDL
0.50
0.58
0.58
0.35
0.58
2.5
0.67
0.63
0.84
0.42
0.63
2.5
0.90
1.0
0.65
0.52
0.34
2.5
0.50
0.41
0.44
0.64
0.52
2.5
0.52
0.57
0.45
0.65
0.44
0.52
0.39
0.36
0.31
0.14
0.14
0.44
0.40
0.19
0.69
4.0
2.5
0.59
0.98
0.63
PQL
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
4.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
5.0
1.0
2.0
1.0
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Client Sample ID:
DMW-I_022509
Lab Sample ID:
Client Matrix:
660-27893-17
Water
Job Number: 660-27893-1
Date Sampled:
Date Received:
02/25/2009 1440
02/26/2009 1030
8260B Volatile Organic Compounds (GC/MS)
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260B
5030B
1.0
03/02/2009 1338
03/02/2009 1338
Analyte
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
o-Xylene
2-Butanone (MEK)
4-Methyl-2-pentanone (MIBK)
Carbon disulfide
2-Hexanone
Methyl tert-butyl ether
m-Xylene & p-Xylene
Surrogate
Toluene-d8 (Surr)
4-Bromofluorobenzene
Dibromofluoromethane
TestAmerica Tampa
Analysis Batch: 660-75614
Result (ug/L)
0.15
0.50
0.51
0.77
0.58
0.46
0.47
0.50
2.5
0.18
0.86
0.54
0.50
0.50
8.4
3.8
0.85
4.4
0.44
0.60
%Rec
118
84
107
Page 52 of 221
Instrument ID:
BVMH GC/MS
Lab File ID:
1HC0219.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
MDL
0.15
0.50
0.51
0.77
0.58
0.46
0.47
0.50
2.5
0.18
0.86
0.54
0.50
0.50
8.4
3.8
0.85
4.4
0.44
0.60
PQL
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
10
10
1.0
10
1.0
2.0
Acceptance Limits
77 - 122
74 - 126
70 - 130
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Client Sample ID:
DMW-I_022509
Lab Sample ID:
Client Matrix:
660-27893-17
Water
Job Number: 660-27893-1
Date Sampled:
Date Received:
02/25/2009 1440
02/26/2009 1030
8260B Volatile Organic Compounds (GC/MS)
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260B
5030B
2.0
03/03/2009 1303
03/03/2009 1303
Analysis Batch: 660-75683
Run Type: DL
Analyte
Acetone
Result (ug/L)
920
TestAmerica Tampa
Page 53 of 221
Instrument ID:
BVMH GC/MS
Lab File ID:
1HC0316.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
MDL
20
PQL
40
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Client Sample ID:
SMW-N_022509
Lab Sample ID:
Client Matrix:
660-27893-18
Water
Job Number: 660-27893-1
Date Sampled:
Date Received:
02/25/2009 1020
02/26/2009 1030
8260B Volatile Organic Compounds (GC/MS)
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260B
5030B
1.0
03/02/2009 1412
03/02/2009 1412
Analysis Batch: 660-75614
Analyte
Benzene
Bromobenzene
Chlorobromomethane
Dichlorobromomethane
Bromoform
Bromomethane
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
Chlorodibromomethane
1,2-Dibromo-3-Chloropropane
Ethylene Dibromide
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
Hexachlorobutadiene
Isopropylbenzene
4-Isopropyltoluene
Methylene Chloride
Naphthalene
N-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
Result (ug/L)
0.50
0.58
0.58
0.35
0.58
2.5
0.67
0.63
0.84
0.42
0.63
2.5
0.90
1.0
0.65
0.52
0.34
2.5
0.50
0.41
0.44
0.64
0.52
2.5
0.52
0.57
0.45
0.65
0.44
0.52
0.39
0.36
0.31
0.14
0.14
0.44
0.40
0.19
0.69
4.0
2.5
0.59
0.98
0.63
TestAmerica Tampa
Page 54 of 221
Instrument ID:
BVMH GC/MS
Lab File ID:
1HC0221.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
MDL
0.50
0.58
0.58
0.35
0.58
2.5
0.67
0.63
0.84
0.42
0.63
2.5
0.90
1.0
0.65
0.52
0.34
2.5
0.50
0.41
0.44
0.64
0.52
2.5
0.52
0.57
0.45
0.65
0.44
0.52
0.39
0.36
0.31
0.14
0.14
0.44
0.40
0.19
0.69
4.0
2.5
0.59
0.98
0.63
PQL
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
4.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
5.0
1.0
2.0
1.0
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Client Sample ID:
SMW-N_022509
Lab Sample ID:
Client Matrix:
660-27893-18
Water
Job Number: 660-27893-1
Date Sampled:
Date Received:
02/25/2009 1020
02/26/2009 1030
8260B Volatile Organic Compounds (GC/MS)
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260B
5030B
1.0
03/02/2009 1412
03/02/2009 1412
Analyte
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
o-Xylene
Acetone
2-Butanone (MEK)
4-Methyl-2-pentanone (MIBK)
Carbon disulfide
2-Hexanone
Methyl tert-butyl ether
m-Xylene & p-Xylene
Surrogate
Toluene-d8 (Surr)
4-Bromofluorobenzene
Dibromofluoromethane
TestAmerica Tampa
Analysis Batch: 660-75614
Result (ug/L)
0.15
0.50
0.51
0.77
0.58
0.46
0.47
0.50
2.5
0.18
0.86
0.54
0.50
0.50
9.9
8.4
3.8
0.85
4.4
0.44
0.60
%Rec
103
84
108
Page 55 of 221
Instrument ID:
BVMH GC/MS
Lab File ID:
1HC0221.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
MDL
0.15
0.50
0.51
0.77
0.58
0.46
0.47
0.50
2.5
0.18
0.86
0.54
0.50
0.50
9.9
8.4
3.8
0.85
4.4
0.44
0.60
PQL
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
20
10
10
1.0
10
1.0
2.0
Acceptance Limits
77 - 122
74 - 126
70 - 130
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Client Sample ID:
IDPT-12_022509
Lab Sample ID:
Client Matrix:
660-27893-19
Water
Job Number: 660-27893-1
Date Sampled:
Date Received:
02/25/2009 1640
02/26/2009 1030
8260B Volatile Organic Compounds (GC/MS)
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260B
5030B
1.0
03/02/2009 1355
03/02/2009 1355
Analysis Batch: 660-75614
Analyte
Benzene
Bromobenzene
Chlorobromomethane
Dichlorobromomethane
Bromoform
Bromomethane
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
Chlorodibromomethane
1,2-Dibromo-3-Chloropropane
Ethylene Dibromide
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
Hexachlorobutadiene
Isopropylbenzene
4-Isopropyltoluene
Methylene Chloride
Naphthalene
N-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
Result (ug/L)
0.50
0.58
0.58
0.35
0.58
2.5
0.67
0.63
0.84
0.42
0.63
2.5
0.90
1.0
0.65
0.52
0.34
2.5
0.50
0.41
0.44
0.64
0.52
2.5
0.52
0.57
0.45
0.65
0.44
0.52
0.39
0.36
0.31
0.14
0.14
0.44
0.40
0.19
0.69
4.0
2.5
0.59
0.98
0.63
TestAmerica Tampa
Page 56 of 221
Instrument ID:
BVMH GC/MS
Lab File ID:
1HC0220.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
MDL
0.50
0.58
0.58
0.35
0.58
2.5
0.67
0.63
0.84
0.42
0.63
2.5
0.90
1.0
0.65
0.52
0.34
2.5
0.50
0.41
0.44
0.64
0.52
2.5
0.52
0.57
0.45
0.65
0.44
0.52
0.39
0.36
0.31
0.14
0.14
0.44
0.40
0.19
0.69
4.0
2.5
0.59
0.98
0.63
PQL
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
4.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
5.0
1.0
2.0
1.0
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Client Sample ID:
IDPT-12_022509
Lab Sample ID:
Client Matrix:
660-27893-19
Water
Job Number: 660-27893-1
Date Sampled:
Date Received:
02/25/2009 1640
02/26/2009 1030
8260B Volatile Organic Compounds (GC/MS)
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260B
5030B
1.0
03/02/2009 1355
03/02/2009 1355
Analyte
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
o-Xylene
Acetone
2-Butanone (MEK)
4-Methyl-2-pentanone (MIBK)
Carbon disulfide
2-Hexanone
Methyl tert-butyl ether
m-Xylene & p-Xylene
Surrogate
Toluene-d8 (Surr)
4-Bromofluorobenzene
Dibromofluoromethane
TestAmerica Tampa
Analysis Batch: 660-75614
Result (ug/L)
0.15
0.50
0.51
0.77
0.58
0.46
0.47
0.50
2.5
0.18
0.86
0.54
0.50
0.50
9.9
8.4
3.8
0.85
4.4
0.44
0.60
%Rec
98
90
109
Page 57 of 221
Instrument ID:
BVMH GC/MS
Lab File ID:
1HC0220.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
MDL
0.15
0.50
0.51
0.77
0.58
0.46
0.47
0.50
2.5
0.18
0.86
0.54
0.50
0.50
9.9
8.4
3.8
0.85
4.4
0.44
0.60
PQL
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
20
10
10
1.0
10
1.0
2.0
Acceptance Limits
77 - 122
74 - 126
70 - 130
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Client Sample ID:
IMW-J_022509
Lab Sample ID:
Client Matrix:
660-27893-20
Water
Job Number: 660-27893-1
Date Sampled:
Date Received:
02/25/2009 1540
02/26/2009 1030
8260B Volatile Organic Compounds (GC/MS)
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260B
5030B
1.0
03/02/2009 1521
03/02/2009 1521
Analysis Batch: 660-75614
Analyte
Benzene
Bromobenzene
Chlorobromomethane
Dichlorobromomethane
Bromoform
Bromomethane
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
Chlorodibromomethane
1,2-Dibromo-3-Chloropropane
Ethylene Dibromide
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
Hexachlorobutadiene
Isopropylbenzene
4-Isopropyltoluene
Methylene Chloride
Naphthalene
N-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
Result (ug/L)
0.50
0.58
0.58
0.35
0.58
2.5
0.67
0.63
0.84
0.42
0.63
2.5
0.90
1.0
0.65
0.52
0.34
2.5
0.50
0.41
0.44
0.64
0.52
2.5
0.52
0.57
0.45
0.65
0.44
0.52
0.39
0.36
0.31
0.14
0.14
0.44
0.40
0.19
0.69
4.0
2.5
0.59
0.98
0.63
TestAmerica Tampa
Page 58 of 221
Instrument ID:
BVMH GC/MS
Lab File ID:
1HC0225.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
MDL
0.50
0.58
0.58
0.35
0.58
2.5
0.67
0.63
0.84
0.42
0.63
2.5
0.90
1.0
0.65
0.52
0.34
2.5
0.50
0.41
0.44
0.64
0.52
2.5
0.52
0.57
0.45
0.65
0.44
0.52
0.39
0.36
0.31
0.14
0.14
0.44
0.40
0.19
0.69
4.0
2.5
0.59
0.98
0.63
PQL
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
4.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
5.0
1.0
2.0
1.0
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Client Sample ID:
IMW-J_022509
Lab Sample ID:
Client Matrix:
660-27893-20
Water
Job Number: 660-27893-1
Date Sampled:
Date Received:
02/25/2009 1540
02/26/2009 1030
8260B Volatile Organic Compounds (GC/MS)
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260B
5030B
1.0
03/02/2009 1521
03/02/2009 1521
Analyte
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
o-Xylene
2-Butanone (MEK)
4-Methyl-2-pentanone (MIBK)
Carbon disulfide
2-Hexanone
Methyl tert-butyl ether
m-Xylene & p-Xylene
Surrogate
Toluene-d8 (Surr)
4-Bromofluorobenzene
Dibromofluoromethane
TestAmerica Tampa
Analysis Batch: 660-75614
Result (ug/L)
0.15
0.50
0.51
0.77
0.58
0.46
0.47
0.50
2.5
0.18
0.86
0.54
0.50
0.50
8.4
3.8
0.85
4.4
0.44
0.60
%Rec
101
91
110
Page 59 of 221
Instrument ID:
BVMH GC/MS
Lab File ID:
1HC0225.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
MDL
0.15
0.50
0.51
0.77
0.58
0.46
0.47
0.50
2.5
0.18
0.86
0.54
0.50
0.50
8.4
3.8
0.85
4.4
0.44
0.60
PQL
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
10
10
1.0
10
1.0
2.0
Acceptance Limits
77 - 122
74 - 126
70 - 130
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Client Sample ID:
IMW-J_022509
Lab Sample ID:
Client Matrix:
660-27893-20
Water
Job Number: 660-27893-1
Date Sampled:
Date Received:
02/25/2009 1540
02/26/2009 1030
8260B Volatile Organic Compounds (GC/MS)
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260B
5030B
2.0
03/03/2009 1321
03/03/2009 1321
Analysis Batch: 660-75683
Run Type: DL
Analyte
Acetone
Result (ug/L)
1300
TestAmerica Tampa
Page 60 of 221
Instrument ID:
BVMH GC/MS
Lab File ID:
1HC0317.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
MDL
20
PQL
40
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Client Sample ID:
DMW-A_022509
Lab Sample ID:
Client Matrix:
660-27893-21
Water
Job Number: 660-27893-1
Date Sampled:
Date Received:
02/25/2009 1200
02/26/2009 1030
8260B Volatile Organic Compounds (GC/MS)
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260B
5030B
1.0
02/28/2009 0140
02/28/2009 0140
Analysis Batch: 660-75698
Analyte
Benzene
Bromobenzene
Chlorobromomethane
Dichlorobromomethane
Bromoform
Bromomethane
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
Chlorodibromomethane
1,2-Dibromo-3-Chloropropane
Ethylene Dibromide
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
Hexachlorobutadiene
Isopropylbenzene
4-Isopropyltoluene
Methylene Chloride
Naphthalene
N-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
Result (ug/L)
0.50
0.58
0.58
0.35
0.58
2.5
0.67
0.63
0.84
0.42
0.63
2.5
0.90
1.0
0.65
0.52
0.34
2.5
0.50
0.41
0.44
0.64
0.52
2.5
0.52
0.57
0.45
0.65
0.44
0.52
0.39
0.36
0.31
0.14
0.14
0.44
0.40
0.19
0.69
4.0
2.5
0.59
0.98
0.63
TestAmerica Tampa
Page 61 of 221
Instrument ID:
BVMJ GC/MS
Lab File ID:
1JB2729.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
MDL
0.50
0.58
0.58
0.35
0.58
2.5
0.67
0.63
0.84
0.42
0.63
2.5
0.90
1.0
0.65
0.52
0.34
2.5
0.50
0.41
0.44
0.64
0.52
2.5
0.52
0.57
0.45
0.65
0.44
0.52
0.39
0.36
0.31
0.14
0.14
0.44
0.40
0.19
0.69
4.0
2.5
0.59
0.98
0.63
PQL
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
4.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
5.0
1.0
2.0
1.0
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Client Sample ID:
DMW-A_022509
Lab Sample ID:
Client Matrix:
660-27893-21
Water
Job Number: 660-27893-1
Date Sampled:
Date Received:
02/25/2009 1200
02/26/2009 1030
8260B Volatile Organic Compounds (GC/MS)
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260B
5030B
1.0
02/28/2009 0140
02/28/2009 0140
Analyte
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
o-Xylene
Acetone
2-Butanone (MEK)
4-Methyl-2-pentanone (MIBK)
Carbon disulfide
2-Hexanone
Methyl tert-butyl ether
m-Xylene & p-Xylene
Surrogate
Toluene-d8 (Surr)
4-Bromofluorobenzene
Dibromofluoromethane
TestAmerica Tampa
Analysis Batch: 660-75698
Result (ug/L)
0.15
0.50
0.51
0.77
0.58
0.46
0.47
0.50
2.5
0.18
0.86
0.54
0.50
0.50
9.9
8.4
3.8
0.85
4.4
0.44
0.60
%Rec
99
100
99
Page 62 of 221
Instrument ID:
BVMJ GC/MS
Lab File ID:
1JB2729.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
MDL
0.15
0.50
0.51
0.77
0.58
0.46
0.47
0.50
2.5
0.18
0.86
0.54
0.50
0.50
9.9
8.4
3.8
0.85
4.4
0.44
0.60
PQL
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
20
10
10
1.0
10
1.0
2.0
Acceptance Limits
77 - 122
74 - 126
70 - 130
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Client Sample ID:
DMW-W_022509
Lab Sample ID:
Client Matrix:
660-27893-22
Water
Job Number: 660-27893-1
Date Sampled:
Date Received:
02/25/2009 0946
02/26/2009 1030
8260B Volatile Organic Compounds (GC/MS)
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260B
5030B
1.0
03/02/2009 1538
03/02/2009 1538
Analysis Batch: 660-75700
Analyte
Benzene
Bromobenzene
Chlorobromomethane
Dichlorobromomethane
Bromoform
Bromomethane
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
Chlorodibromomethane
1,2-Dibromo-3-Chloropropane
Ethylene Dibromide
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
Hexachlorobutadiene
Isopropylbenzene
4-Isopropyltoluene
Methylene Chloride
Naphthalene
N-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
Result (ug/L)
0.50
0.58
0.58
0.35
0.58
2.5
0.67
0.63
0.84
0.42
0.63
2.5
0.90
1.0
0.65
0.52
0.34
2.5
0.50
0.41
0.44
0.64
0.52
2.5
0.52
0.57
0.45
0.65
0.44
0.52
0.39
0.36
0.31
0.14
0.14
0.44
0.40
0.19
0.69
4.0
2.5
0.59
0.98
0.63
TestAmerica Tampa
Page 63 of 221
Instrument ID:
BVMJ GC/MS
Lab File ID:
1JC0214.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
MDL
0.50
0.58
0.58
0.35
0.58
2.5
0.67
0.63
0.84
0.42
0.63
2.5
0.90
1.0
0.65
0.52
0.34
2.5
0.50
0.41
0.44
0.64
0.52
2.5
0.52
0.57
0.45
0.65
0.44
0.52
0.39
0.36
0.31
0.14
0.14
0.44
0.40
0.19
0.69
4.0
2.5
0.59
0.98
0.63
PQL
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
4.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
5.0
1.0
2.0
1.0
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Client Sample ID:
DMW-W_022509
Lab Sample ID:
Client Matrix:
660-27893-22
Water
Job Number: 660-27893-1
Date Sampled:
Date Received:
02/25/2009 0946
02/26/2009 1030
8260B Volatile Organic Compounds (GC/MS)
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260B
5030B
1.0
03/02/2009 1538
03/02/2009 1538
Analyte
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
o-Xylene
Acetone
2-Butanone (MEK)
4-Methyl-2-pentanone (MIBK)
Carbon disulfide
2-Hexanone
Methyl tert-butyl ether
m-Xylene & p-Xylene
Surrogate
Toluene-d8 (Surr)
4-Bromofluorobenzene
Dibromofluoromethane
TestAmerica Tampa
Analysis Batch: 660-75700
Result (ug/L)
0.15
0.50
0.51
0.77
0.58
0.46
0.47
0.50
2.5
0.18
0.86
0.54
0.50
0.50
9.9
8.4
3.8
0.85
4.4
0.44
0.60
%Rec
102
105
98
Page 64 of 221
Instrument ID:
BVMJ GC/MS
Lab File ID:
1JC0214.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
MDL
0.15
0.50
0.51
0.77
0.58
0.46
0.47
0.50
2.5
0.18
0.86
0.54
0.50
0.50
9.9
8.4
3.8
0.85
4.4
0.44
0.60
PQL
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
20
10
10
1.0
10
1.0
2.0
Acceptance Limits
77 - 122
74 - 126
70 - 130
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Client Sample ID:
H-1_022509
Lab Sample ID:
Client Matrix:
660-27893-23
Water
Job Number: 660-27893-1
Date Sampled:
Date Received:
02/25/2009 1300
02/26/2009 1030
8260B Volatile Organic Compounds (GC/MS)
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260B
5030B
1.0
03/02/2009 1651
03/02/2009 1651
Analysis Batch: 660-75700
Analyte
Benzene
Bromobenzene
Chlorobromomethane
Dichlorobromomethane
Bromoform
Bromomethane
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
Chlorodibromomethane
1,2-Dibromo-3-Chloropropane
Ethylene Dibromide
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
Hexachlorobutadiene
Isopropylbenzene
4-Isopropyltoluene
Methylene Chloride
Naphthalene
N-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
Result (ug/L)
0.83
0.58
0.58
0.35
0.58
2.5
0.67
0.63
0.84
0.42
0.63
2.5
0.90
1.0
0.65
0.52
0.34
2.5
0.50
0.41
0.44
0.64
0.52
2.5
0.52
0.57
0.45
0.65
0.44
0.52
0.39
0.36
0.31
0.14
0.14
0.44
0.40
0.19
0.69
4.0
2.5
0.59
0.98
0.63
TestAmerica Tampa
Page 65 of 221
Instrument ID:
BVMJ GC/MS
Lab File ID:
1JC0217.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
I
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
MDL
0.50
0.58
0.58
0.35
0.58
2.5
0.67
0.63
0.84
0.42
0.63
2.5
0.90
1.0
0.65
0.52
0.34
2.5
0.50
0.41
0.44
0.64
0.52
2.5
0.52
0.57
0.45
0.65
0.44
0.52
0.39
0.36
0.31
0.14
0.14
0.44
0.40
0.19
0.69
4.0
2.5
0.59
0.98
0.63
PQL
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
4.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
5.0
1.0
2.0
1.0
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Client Sample ID:
H-1_022509
Lab Sample ID:
Client Matrix:
660-27893-23
Water
Job Number: 660-27893-1
Date Sampled:
Date Received:
02/25/2009 1300
02/26/2009 1030
8260B Volatile Organic Compounds (GC/MS)
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260B
5030B
1.0
03/02/2009 1651
03/02/2009 1651
Analyte
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
o-Xylene
Acetone
2-Butanone (MEK)
4-Methyl-2-pentanone (MIBK)
Carbon disulfide
2-Hexanone
Methyl tert-butyl ether
m-Xylene & p-Xylene
Surrogate
Toluene-d8 (Surr)
4-Bromofluorobenzene
Dibromofluoromethane
TestAmerica Tampa
Analysis Batch: 660-75700
Result (ug/L)
0.15
0.50
0.51
0.77
0.58
0.46
0.47
0.50
2.5
0.18
0.86
0.54
0.50
0.50
9.9
8.4
3.8
0.85
4.4
0.44
0.60
%Rec
101
100
98
Page 66 of 221
Instrument ID:
BVMJ GC/MS
Lab File ID:
1JC0217.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
MDL
0.15
0.50
0.51
0.77
0.58
0.46
0.47
0.50
2.5
0.18
0.86
0.54
0.50
0.50
9.9
8.4
3.8
0.85
4.4
0.44
0.60
PQL
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
20
10
10
1.0
10
1.0
2.0
Acceptance Limits
77 - 122
74 - 126
70 - 130
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Client Sample ID:
SMW-A_022509
Lab Sample ID:
Client Matrix:
660-27893-24
Water
Job Number: 660-27893-1
Date Sampled:
Date Received:
02/25/2009 1235
02/26/2009 1030
8260B Volatile Organic Compounds (GC/MS)
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260B
5030B
1.0
03/02/2009 1715
03/02/2009 1715
Analysis Batch: 660-75700
Analyte
Benzene
Bromobenzene
Chlorobromomethane
Dichlorobromomethane
Bromoform
Bromomethane
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
Chlorodibromomethane
1,2-Dibromo-3-Chloropropane
Ethylene Dibromide
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
Hexachlorobutadiene
Isopropylbenzene
4-Isopropyltoluene
Methylene Chloride
Naphthalene
N-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
Result (ug/L)
0.50
0.58
0.58
0.35
0.58
2.5
0.67
0.63
0.84
0.42
0.63
2.5
0.90
1.0
0.65
0.52
0.34
2.5
0.50
0.41
0.44
0.64
0.52
2.5
0.52
0.57
0.45
0.65
0.44
0.52
0.39
0.36
0.31
0.14
0.14
0.44
0.40
0.19
0.69
4.0
2.5
0.59
0.98
0.63
TestAmerica Tampa
Page 67 of 221
Instrument ID:
BVMJ GC/MS
Lab File ID:
1JC0218.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
MDL
0.50
0.58
0.58
0.35
0.58
2.5
0.67
0.63
0.84
0.42
0.63
2.5
0.90
1.0
0.65
0.52
0.34
2.5
0.50
0.41
0.44
0.64
0.52
2.5
0.52
0.57
0.45
0.65
0.44
0.52
0.39
0.36
0.31
0.14
0.14
0.44
0.40
0.19
0.69
4.0
2.5
0.59
0.98
0.63
PQL
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
4.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
5.0
1.0
2.0
1.0
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Client Sample ID:
SMW-A_022509
Lab Sample ID:
Client Matrix:
660-27893-24
Water
Job Number: 660-27893-1
Date Sampled:
Date Received:
02/25/2009 1235
02/26/2009 1030
8260B Volatile Organic Compounds (GC/MS)
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260B
5030B
1.0
03/02/2009 1715
03/02/2009 1715
Analyte
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
o-Xylene
Acetone
2-Butanone (MEK)
4-Methyl-2-pentanone (MIBK)
Carbon disulfide
2-Hexanone
Methyl tert-butyl ether
m-Xylene & p-Xylene
Surrogate
Toluene-d8 (Surr)
4-Bromofluorobenzene
Dibromofluoromethane
TestAmerica Tampa
Analysis Batch: 660-75700
Result (ug/L)
0.15
0.50
0.51
0.77
0.58
0.46
0.47
0.50
2.5
0.18
0.86
0.54
0.50
0.50
9.9
8.4
3.8
0.85
4.4
0.44
0.60
%Rec
102
105
101
Page 68 of 221
Instrument ID:
BVMJ GC/MS
Lab File ID:
1JC0218.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
MDL
0.15
0.50
0.51
0.77
0.58
0.46
0.47
0.50
2.5
0.18
0.86
0.54
0.50
0.50
9.9
8.4
3.8
0.85
4.4
0.44
0.60
PQL
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
20
10
10
1.0
10
1.0
2.0
Acceptance Limits
77 - 122
74 - 126
70 - 130
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Job Number: 660-27893-1
Client Sample ID:
Trip Blank 3_022509
Lab Sample ID:
Client Matrix:
660-27893-25
Water
Date Sampled:
Date Received:
02/25/2009 0000
02/26/2009 1030
8260B Volatile Organic Compounds (GC/MS)
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260B
5030B
1.0
02/28/2009 0955
02/28/2009 0955
Analysis Batch: 660-75699
Analyte
Benzene
Bromobenzene
Chlorobromomethane
Dichlorobromomethane
Bromoform
Bromomethane
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
Chlorodibromomethane
1,2-Dibromo-3-Chloropropane
Ethylene Dibromide
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
Hexachlorobutadiene
Isopropylbenzene
4-Isopropyltoluene
Methylene Chloride
Naphthalene
N-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
Result (ug/L)
0.50
0.58
0.58
0.35
0.58
2.5
0.67
0.63
0.84
0.42
0.63
2.5
0.90
1.0
0.65
0.52
0.34
2.5
0.50
0.41
0.44
0.64
0.52
2.5
0.52
0.57
0.45
0.65
0.44
0.52
0.39
0.36
0.31
0.14
0.14
0.44
0.40
0.19
0.69
4.0
2.5
0.59
0.98
0.63
TestAmerica Tampa
Page 69 of 221
Instrument ID:
BVMJ GC/MS
Lab File ID:
1JB2749.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
MDL
0.50
0.58
0.58
0.35
0.58
2.5
0.67
0.63
0.84
0.42
0.63
2.5
0.90
1.0
0.65
0.52
0.34
2.5
0.50
0.41
0.44
0.64
0.52
2.5
0.52
0.57
0.45
0.65
0.44
0.52
0.39
0.36
0.31
0.14
0.14
0.44
0.40
0.19
0.69
4.0
2.5
0.59
0.98
0.63
PQL
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
4.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
5.0
1.0
2.0
1.0
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Job Number: 660-27893-1
Client Sample ID:
Trip Blank 3_022509
Lab Sample ID:
Client Matrix:
660-27893-25
Water
Date Sampled:
Date Received:
02/25/2009 0000
02/26/2009 1030
8260B Volatile Organic Compounds (GC/MS)
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260B
5030B
1.0
02/28/2009 0955
02/28/2009 0955
Analyte
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
o-Xylene
Acetone
2-Butanone (MEK)
4-Methyl-2-pentanone (MIBK)
Carbon disulfide
2-Hexanone
Methyl tert-butyl ether
m-Xylene & p-Xylene
Surrogate
Toluene-d8 (Surr)
4-Bromofluorobenzene
Dibromofluoromethane
TestAmerica Tampa
Analysis Batch: 660-75699
Result (ug/L)
0.15
0.50
0.51
0.77
0.58
0.46
0.47
0.50
2.5
0.18
0.86
0.54
0.50
0.50
9.9
8.4
3.8
0.85
4.4
0.44
0.60
%Rec
101
101
97
Page 70 of 221
Instrument ID:
BVMJ GC/MS
Lab File ID:
1JB2749.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
MDL
0.15
0.50
0.51
0.77
0.58
0.46
0.47
0.50
2.5
0.18
0.86
0.54
0.50
0.50
9.9
8.4
3.8
0.85
4.4
0.44
0.60
PQL
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
20
10
10
1.0
10
1.0
2.0
Acceptance Limits
77 - 122
74 - 126
70 - 130
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Client Sample ID:
IDPT-1_022509
Lab Sample ID:
Client Matrix:
660-27893-26
Water
Job Number: 660-27893-1
Date Sampled:
Date Received:
02/25/2009 1555
02/26/2009 1030
8260B Volatile Organic Compounds (GC/MS)
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260B
5030B
1.0
02/28/2009 1019
02/28/2009 1019
Analysis Batch: 660-75699
Analyte
Benzene
Bromobenzene
Chlorobromomethane
Dichlorobromomethane
Bromoform
Bromomethane
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
Chlorodibromomethane
1,2-Dibromo-3-Chloropropane
Ethylene Dibromide
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
Hexachlorobutadiene
Isopropylbenzene
4-Isopropyltoluene
Methylene Chloride
Naphthalene
N-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
Result (ug/L)
0.50
0.58
0.58
0.35
0.58
2.5
0.67
0.63
0.84
0.42
0.63
2.5
0.90
1.0
0.65
0.52
0.34
2.5
0.50
0.41
0.44
0.64
0.52
2.5
1.1
0.57
0.45
0.65
0.44
0.52
0.39
0.36
0.31
0.14
0.14
0.44
0.40
0.19
0.69
4.0
2.5
0.59
0.98
0.63
TestAmerica Tampa
Page 71 of 221
Instrument ID:
BVMJ GC/MS
Lab File ID:
1JB2750.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
MDL
0.50
0.58
0.58
0.35
0.58
2.5
0.67
0.63
0.84
0.42
0.63
2.5
0.90
1.0
0.65
0.52
0.34
2.5
0.50
0.41
0.44
0.64
0.52
2.5
0.52
0.57
0.45
0.65
0.44
0.52
0.39
0.36
0.31
0.14
0.14
0.44
0.40
0.19
0.69
4.0
2.5
0.59
0.98
0.63
PQL
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
4.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
5.0
1.0
2.0
1.0
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Client Sample ID:
IDPT-1_022509
Lab Sample ID:
Client Matrix:
660-27893-26
Water
Job Number: 660-27893-1
Date Sampled:
Date Received:
02/25/2009 1555
02/26/2009 1030
8260B Volatile Organic Compounds (GC/MS)
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260B
5030B
1.0
02/28/2009 1019
02/28/2009 1019
Analyte
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
o-Xylene
Acetone
2-Butanone (MEK)
4-Methyl-2-pentanone (MIBK)
Carbon disulfide
2-Hexanone
Methyl tert-butyl ether
m-Xylene & p-Xylene
Surrogate
Toluene-d8 (Surr)
4-Bromofluorobenzene
Dibromofluoromethane
TestAmerica Tampa
Analysis Batch: 660-75699
Result (ug/L)
0.15
0.50
0.51
0.77
0.58
0.46
0.47
0.50
2.5
0.18
0.86
0.54
0.51
0.50
9.9
8.4
3.8
0.85
4.4
0.44
0.60
%Rec
100
101
100
Page 72 of 221
Instrument ID:
BVMJ GC/MS
Lab File ID:
1JB2750.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
U
U
U
U
U
U
U
U
U
U
U
U
I
U
U
U
U
U
U
U
U
MDL
0.15
0.50
0.51
0.77
0.58
0.46
0.47
0.50
2.5
0.18
0.86
0.54
0.50
0.50
9.9
8.4
3.8
0.85
4.4
0.44
0.60
PQL
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
20
10
10
1.0
10
1.0
2.0
Acceptance Limits
77 - 122
74 - 126
70 - 130
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Client Sample ID:
IDPT-2_022509
Lab Sample ID:
Client Matrix:
660-27893-27
Water
Job Number: 660-27893-1
Date Sampled:
Date Received:
02/25/2009 1654
02/26/2009 1030
8260B Volatile Organic Compounds (GC/MS)
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260B
5030B
1.0
02/28/2009 1132
02/28/2009 1132
Analysis Batch: 660-75699
Analyte
Benzene
Bromobenzene
Chlorobromomethane
Dichlorobromomethane
Bromoform
Bromomethane
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
Chlorodibromomethane
1,2-Dibromo-3-Chloropropane
Ethylene Dibromide
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
Hexachlorobutadiene
Isopropylbenzene
4-Isopropyltoluene
Methylene Chloride
Naphthalene
N-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
Result (ug/L)
0.50
0.58
0.58
0.35
0.58
2.5
0.67
0.63
0.84
0.42
0.63
2.5
0.90
1.0
0.65
0.52
0.34
2.5
0.50
0.41
0.44
0.64
0.52
2.5
0.52
0.57
0.45
0.65
0.44
0.52
0.39
0.36
0.31
0.14
0.14
0.44
0.40
0.19
0.69
4.0
2.5
0.59
0.98
0.63
TestAmerica Tampa
Page 73 of 221
Instrument ID:
BVMJ GC/MS
Lab File ID:
1JB2753.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
MDL
0.50
0.58
0.58
0.35
0.58
2.5
0.67
0.63
0.84
0.42
0.63
2.5
0.90
1.0
0.65
0.52
0.34
2.5
0.50
0.41
0.44
0.64
0.52
2.5
0.52
0.57
0.45
0.65
0.44
0.52
0.39
0.36
0.31
0.14
0.14
0.44
0.40
0.19
0.69
4.0
2.5
0.59
0.98
0.63
PQL
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
4.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
5.0
1.0
2.0
1.0
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Client Sample ID:
IDPT-2_022509
Lab Sample ID:
Client Matrix:
660-27893-27
Water
Job Number: 660-27893-1
Date Sampled:
Date Received:
02/25/2009 1654
02/26/2009 1030
8260B Volatile Organic Compounds (GC/MS)
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260B
5030B
1.0
02/28/2009 1132
02/28/2009 1132
Analyte
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
o-Xylene
Acetone
2-Butanone (MEK)
4-Methyl-2-pentanone (MIBK)
Carbon disulfide
2-Hexanone
Methyl tert-butyl ether
m-Xylene & p-Xylene
Surrogate
Toluene-d8 (Surr)
4-Bromofluorobenzene
Dibromofluoromethane
TestAmerica Tampa
Analysis Batch: 660-75699
Result (ug/L)
0.15
0.50
13
0.77
0.58
0.46
0.47
0.50
2.5
0.18
0.86
0.54
0.50
0.50
9.9
8.4
3.8
0.85
4.4
0.44
1.8
%Rec
100
102
102
Page 74 of 221
Instrument ID:
BVMJ GC/MS
Lab File ID:
1JB2753.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
I
MDL
0.15
0.50
0.51
0.77
0.58
0.46
0.47
0.50
2.5
0.18
0.86
0.54
0.50
0.50
9.9
8.4
3.8
0.85
4.4
0.44
0.60
PQL
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
20
10
10
1.0
10
1.0
2.0
Acceptance Limits
77 - 122
74 - 126
70 - 130
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Client Sample ID:
IDPT-5_022509
Lab Sample ID:
Client Matrix:
660-27893-28
Water
Job Number: 660-27893-1
Date Sampled:
Date Received:
02/25/2009 1422
02/26/2009 1030
8260B Volatile Organic Compounds (GC/MS)
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260B
5030B
1.0
02/28/2009 1156
02/28/2009 1156
Analysis Batch: 660-75699
Analyte
Benzene
Bromobenzene
Chlorobromomethane
Dichlorobromomethane
Bromoform
Bromomethane
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
Chlorodibromomethane
1,2-Dibromo-3-Chloropropane
Ethylene Dibromide
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
Hexachlorobutadiene
Isopropylbenzene
4-Isopropyltoluene
Methylene Chloride
Naphthalene
N-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
Result (ug/L)
0.50
0.58
0.58
0.35
0.58
2.5
0.67
0.63
0.84
0.42
0.63
2.5
0.90
1.0
0.65
0.52
0.34
2.5
0.50
0.41
0.44
0.64
0.52
2.5
0.52
0.57
0.45
0.65
0.44
0.52
0.39
0.36
0.31
0.14
0.14
0.44
0.40
0.19
0.69
4.0
2.5
0.59
0.98
0.63
TestAmerica Tampa
Page 75 of 221
Instrument ID:
BVMJ GC/MS
Lab File ID:
1JB2754.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
MDL
0.50
0.58
0.58
0.35
0.58
2.5
0.67
0.63
0.84
0.42
0.63
2.5
0.90
1.0
0.65
0.52
0.34
2.5
0.50
0.41
0.44
0.64
0.52
2.5
0.52
0.57
0.45
0.65
0.44
0.52
0.39
0.36
0.31
0.14
0.14
0.44
0.40
0.19
0.69
4.0
2.5
0.59
0.98
0.63
PQL
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
4.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
5.0
1.0
2.0
1.0
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Client Sample ID:
IDPT-5_022509
Lab Sample ID:
Client Matrix:
660-27893-28
Water
Job Number: 660-27893-1
Date Sampled:
Date Received:
02/25/2009 1422
02/26/2009 1030
8260B Volatile Organic Compounds (GC/MS)
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260B
5030B
1.0
02/28/2009 1156
02/28/2009 1156
Analyte
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
o-Xylene
Acetone
2-Butanone (MEK)
4-Methyl-2-pentanone (MIBK)
Carbon disulfide
2-Hexanone
Methyl tert-butyl ether
m-Xylene & p-Xylene
Surrogate
Toluene-d8 (Surr)
4-Bromofluorobenzene
Dibromofluoromethane
TestAmerica Tampa
Analysis Batch: 660-75699
Result (ug/L)
0.15
0.50
0.51
0.77
0.58
0.46
0.47
0.50
2.5
0.18
0.86
0.54
0.50
0.50
9.9
8.4
3.8
0.85
4.4
0.44
0.60
%Rec
100
99
100
Page 76 of 221
Instrument ID:
BVMJ GC/MS
Lab File ID:
1JB2754.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
MDL
0.15
0.50
0.51
0.77
0.58
0.46
0.47
0.50
2.5
0.18
0.86
0.54
0.50
0.50
9.9
8.4
3.8
0.85
4.4
0.44
0.60
PQL
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
20
10
10
1.0
10
1.0
2.0
Acceptance Limits
77 - 122
74 - 126
70 - 130
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Client Sample ID:
IDPT-6_022509
Lab Sample ID:
Client Matrix:
660-27893-29
Water
Job Number: 660-27893-1
Date Sampled:
Date Received:
02/25/2009 1725
02/26/2009 1030
8260B Volatile Organic Compounds (GC/MS)
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260B
5030B
1.0
02/28/2009 1221
02/28/2009 1221
Analysis Batch: 660-75699
Analyte
Benzene
Bromobenzene
Chlorobromomethane
Dichlorobromomethane
Bromoform
Bromomethane
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
Chlorodibromomethane
1,2-Dibromo-3-Chloropropane
Ethylene Dibromide
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
Hexachlorobutadiene
Isopropylbenzene
4-Isopropyltoluene
Methylene Chloride
Naphthalene
N-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
Result (ug/L)
0.50
0.58
0.58
0.35
0.58
2.5
0.67
0.63
0.84
0.42
0.63
2.5
0.90
1.0
0.65
0.52
0.34
2.5
0.50
0.41
0.44
0.64
0.52
2.5
16
0.57
0.59
4.0
0.44
0.52
0.39
0.36
0.31
0.14
0.14
0.44
0.40
0.19
0.69
4.0
2.5
0.59
0.98
0.63
TestAmerica Tampa
Page 77 of 221
Instrument ID:
BVMJ GC/MS
Lab File ID:
1JB2755.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
I
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
MDL
0.50
0.58
0.58
0.35
0.58
2.5
0.67
0.63
0.84
0.42
0.63
2.5
0.90
1.0
0.65
0.52
0.34
2.5
0.50
0.41
0.44
0.64
0.52
2.5
0.52
0.57
0.45
0.65
0.44
0.52
0.39
0.36
0.31
0.14
0.14
0.44
0.40
0.19
0.69
4.0
2.5
0.59
0.98
0.63
PQL
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
4.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
5.0
1.0
2.0
1.0
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Client Sample ID:
IDPT-6_022509
Lab Sample ID:
Client Matrix:
660-27893-29
Water
Job Number: 660-27893-1
Date Sampled:
Date Received:
02/25/2009 1725
02/26/2009 1030
8260B Volatile Organic Compounds (GC/MS)
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260B
5030B
1.0
02/28/2009 1221
02/28/2009 1221
Analyte
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
o-Xylene
Acetone
2-Butanone (MEK)
4-Methyl-2-pentanone (MIBK)
Carbon disulfide
2-Hexanone
Methyl tert-butyl ether
m-Xylene & p-Xylene
Surrogate
Toluene-d8 (Surr)
4-Bromofluorobenzene
Dibromofluoromethane
TestAmerica Tampa
Analysis Batch: 660-75699
Result (ug/L)
0.15
0.50
0.51
0.77
0.58
0.46
0.47
0.50
2.5
0.18
0.86
0.54
0.50
9.9
8.4
3.8
0.85
4.4
0.44
0.60
%Rec
101
102
104
Page 78 of 221
Instrument ID:
BVMJ GC/MS
Lab File ID:
1JB2755.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
MDL
0.15
0.50
0.51
0.77
0.58
0.46
0.47
0.50
2.5
0.18
0.86
0.54
0.50
9.9
8.4
3.8
0.85
4.4
0.44
0.60
PQL
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
20
10
10
1.0
10
1.0
2.0
Acceptance Limits
77 - 122
74 - 126
70 - 130
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Client Sample ID:
IDPT-6_022509
Lab Sample ID:
Client Matrix:
660-27893-29
Water
Job Number: 660-27893-1
Date Sampled:
Date Received:
02/25/2009 1725
02/26/2009 1030
8260B Volatile Organic Compounds (GC/MS)
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260B
5030B
5.0
03/02/2009 2005
03/02/2009 2005
Analysis Batch: 660-75700
Run Type: DL
Analyte
Vinyl chloride
Result (ug/L)
330
TestAmerica Tampa
Page 79 of 221
Instrument ID:
BVMJ GC/MS
Lab File ID:
1JC0225.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
MDL
2.5
PQL
5.0
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Client Sample ID:
IDPT-10_022509
Lab Sample ID:
Client Matrix:
660-27893-30
Water
Job Number: 660-27893-1
Date Sampled:
Date Received:
02/25/2009 1626
02/26/2009 1030
8260B Volatile Organic Compounds (GC/MS)
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260B
5030B
1.0
03/02/2009 1804
03/02/2009 1804
Analysis Batch: 660-75700
Analyte
Benzene
Bromobenzene
Chlorobromomethane
Dichlorobromomethane
Bromoform
Bromomethane
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
Chlorodibromomethane
1,2-Dibromo-3-Chloropropane
Ethylene Dibromide
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
Hexachlorobutadiene
Isopropylbenzene
4-Isopropyltoluene
Methylene Chloride
Naphthalene
N-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
Result (ug/L)
0.50
0.58
0.58
0.35
0.58
2.5
0.67
0.63
0.84
0.42
0.63
2.5
0.90
1.0
0.65
0.52
0.34
2.5
0.50
0.41
0.44
0.64
0.52
2.5
0.52
0.57
0.45
0.65
0.44
0.52
0.39
0.36
0.31
0.14
0.14
0.44
0.40
0.19
0.69
4.0
2.5
0.59
0.98
0.63
TestAmerica Tampa
Page 80 of 221
Instrument ID:
BVMJ GC/MS
Lab File ID:
1JC0220.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
MDL
0.50
0.58
0.58
0.35
0.58
2.5
0.67
0.63
0.84
0.42
0.63
2.5
0.90
1.0
0.65
0.52
0.34
2.5
0.50
0.41
0.44
0.64
0.52
2.5
0.52
0.57
0.45
0.65
0.44
0.52
0.39
0.36
0.31
0.14
0.14
0.44
0.40
0.19
0.69
4.0
2.5
0.59
0.98
0.63
PQL
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
4.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
5.0
1.0
2.0
1.0
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Client Sample ID:
IDPT-10_022509
Lab Sample ID:
Client Matrix:
660-27893-30
Water
Job Number: 660-27893-1
Date Sampled:
Date Received:
02/25/2009 1626
02/26/2009 1030
8260B Volatile Organic Compounds (GC/MS)
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260B
5030B
1.0
03/02/2009 1804
03/02/2009 1804
Analyte
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
o-Xylene
Acetone
2-Butanone (MEK)
4-Methyl-2-pentanone (MIBK)
Carbon disulfide
2-Hexanone
Methyl tert-butyl ether
m-Xylene & p-Xylene
Surrogate
Toluene-d8 (Surr)
4-Bromofluorobenzene
Dibromofluoromethane
TestAmerica Tampa
Analysis Batch: 660-75700
Result (ug/L)
0.15
0.50
5.5
0.77
0.58
0.46
0.47
0.50
2.5
0.18
0.86
0.54
0.50
0.50
9.9
8.4
3.8
0.85
4.4
0.44
0.60
%Rec
103
104
102
Page 81 of 221
Instrument ID:
BVMJ GC/MS
Lab File ID:
1JC0220.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
MDL
0.15
0.50
0.51
0.77
0.58
0.46
0.47
0.50
2.5
0.18
0.86
0.54
0.50
0.50
9.9
8.4
3.8
0.85
4.4
0.44
0.60
PQL
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
20
10
10
1.0
10
1.0
2.0
Acceptance Limits
77 - 122
74 - 126
70 - 130
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Client Sample ID:
IDPT-13_022509
Lab Sample ID:
Client Matrix:
660-27893-31
Water
Job Number: 660-27893-1
Date Sampled:
Date Received:
02/25/2009 1455
02/26/2009 1030
8260B Volatile Organic Compounds (GC/MS)
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260B
5030B
1.0
02/28/2009 1310
02/28/2009 1310
Analysis Batch: 660-75699
Analyte
Benzene
Bromobenzene
Chlorobromomethane
Dichlorobromomethane
Bromoform
Bromomethane
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
Chlorodibromomethane
1,2-Dibromo-3-Chloropropane
Ethylene Dibromide
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
Hexachlorobutadiene
Isopropylbenzene
4-Isopropyltoluene
Methylene Chloride
Naphthalene
N-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
Result (ug/L)
0.50
0.58
0.58
0.35
0.58
2.5
0.67
0.63
0.84
0.42
0.63
2.5
0.90
1.0
0.65
0.52
0.34
2.5
0.50
0.41
0.44
0.64
0.52
2.5
0.52
0.57
0.45
0.65
0.44
0.52
0.39
0.36
0.31
0.14
0.14
0.44
0.40
0.19
0.69
4.0
2.5
0.59
0.98
0.63
TestAmerica Tampa
Page 82 of 221
Instrument ID:
BVMJ GC/MS
Lab File ID:
1JB2757.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
MDL
0.50
0.58
0.58
0.35
0.58
2.5
0.67
0.63
0.84
0.42
0.63
2.5
0.90
1.0
0.65
0.52
0.34
2.5
0.50
0.41
0.44
0.64
0.52
2.5
0.52
0.57
0.45
0.65
0.44
0.52
0.39
0.36
0.31
0.14
0.14
0.44
0.40
0.19
0.69
4.0
2.5
0.59
0.98
0.63
PQL
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
4.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
5.0
1.0
2.0
1.0
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Client Sample ID:
IDPT-13_022509
Lab Sample ID:
Client Matrix:
660-27893-31
Water
Job Number: 660-27893-1
Date Sampled:
Date Received:
02/25/2009 1455
02/26/2009 1030
8260B Volatile Organic Compounds (GC/MS)
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260B
5030B
1.0
02/28/2009 1310
02/28/2009 1310
Analyte
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
o-Xylene
Acetone
2-Butanone (MEK)
4-Methyl-2-pentanone (MIBK)
Carbon disulfide
2-Hexanone
Methyl tert-butyl ether
m-Xylene & p-Xylene
Surrogate
Toluene-d8 (Surr)
4-Bromofluorobenzene
Dibromofluoromethane
TestAmerica Tampa
Analysis Batch: 660-75699
Result (ug/L)
0.15
0.50
0.51
0.77
0.58
0.46
0.47
0.50
2.5
0.18
0.86
0.54
0.50
0.50
9.9
8.4
3.8
0.85
4.4
0.44
0.60
%Rec
101
103
101
Page 83 of 221
Instrument ID:
BVMJ GC/MS
Lab File ID:
1JB2757.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
MDL
0.15
0.50
0.51
0.77
0.58
0.46
0.47
0.50
2.5
0.18
0.86
0.54
0.50
0.50
9.9
8.4
3.8
0.85
4.4
0.44
0.60
PQL
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
20
10
10
1.0
10
1.0
2.0
Acceptance Limits
77 - 122
74 - 126
70 - 130
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Client Sample ID:
IDPT-14_022509
Lab Sample ID:
Client Matrix:
660-27893-32
Water
Job Number: 660-27893-1
Date Sampled:
Date Received:
02/25/2009 1317
02/26/2009 1030
8260B Volatile Organic Compounds (GC/MS)
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260B
5030B
50
03/02/2009 2030
03/02/2009 2030
Analysis Batch: 660-75700
Analyte
Benzene
Bromobenzene
Chlorobromomethane
Dichlorobromomethane
Bromoform
Bromomethane
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
Chlorodibromomethane
1,2-Dibromo-3-Chloropropane
Ethylene Dibromide
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
Hexachlorobutadiene
Isopropylbenzene
4-Isopropyltoluene
Methylene Chloride
Naphthalene
N-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
Result (ug/L)
25
29
29
18
29
120
34
32
42
21
32
120
45
50
32
26
17
120
25
20
22
32
26
120
26
28
22
470
22
26
20
18
16
7.0
7.0
22
20
9.5
34
200
120
30
49
32
TestAmerica Tampa
Page 84 of 221
Instrument ID:
BVMJ GC/MS
Lab File ID:
1JC0226.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
MDL
25
29
29
18
29
120
34
32
42
21
32
120
45
50
32
26
17
120
25
20
22
32
26
120
26
28
22
32
22
26
20
18
16
7.0
7.0
22
20
9.5
34
200
120
30
49
32
PQL
50
50
50
50
50
250
50
50
50
50
50
250
50
200
50
50
50
250
50
50
50
50
50
250
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
250
250
50
100
50
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Client Sample ID:
IDPT-14_022509
Lab Sample ID:
Client Matrix:
660-27893-32
Water
Job Number: 660-27893-1
Date Sampled:
Date Received:
02/25/2009 1317
02/26/2009 1030
8260B Volatile Organic Compounds (GC/MS)
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260B
5030B
50
03/02/2009 2030
03/02/2009 2030
Analyte
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
o-Xylene
Acetone
2-Butanone (MEK)
4-Methyl-2-pentanone (MIBK)
Carbon disulfide
2-Hexanone
Methyl tert-butyl ether
m-Xylene & p-Xylene
Surrogate
Toluene-d8 (Surr)
4-Bromofluorobenzene
Dibromofluoromethane
TestAmerica Tampa
Analysis Batch: 660-75700
Result (ug/L)
7.5
25
26
38
29
23
24
3800
120
9.0
43
27
25
25
500
420
190
42
220
22
30
%Rec
101
102
101
Page 85 of 221
Instrument ID:
BVMJ GC/MS
Lab File ID:
1JC0226.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
MDL
7.5
25
26
38
29
23
24
25
120
9.0
43
27
25
25
500
420
190
42
220
22
30
PQL
50
50
50
50
50
50
50
50
250
50
50
50
50
50
1000
500
500
50
500
50
100
Acceptance Limits
77 - 122
74 - 126
70 - 130
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Client Sample ID:
IMW-F_022509
Lab Sample ID:
Client Matrix:
660-27893-33
Water
Job Number: 660-27893-1
Date Sampled:
Date Received:
02/25/2009 0918
02/26/2009 1030
8260B Volatile Organic Compounds (GC/MS)
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260B
5030B
1.0
03/02/2009 1852
03/02/2009 1852
Analysis Batch: 660-75700
Analyte
Benzene
Bromobenzene
Chlorobromomethane
Dichlorobromomethane
Bromoform
Bromomethane
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
Chlorodibromomethane
1,2-Dibromo-3-Chloropropane
Ethylene Dibromide
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
Hexachlorobutadiene
Isopropylbenzene
4-Isopropyltoluene
Methylene Chloride
Naphthalene
N-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
Result (ug/L)
0.50
0.58
0.58
0.35
0.58
2.5
0.67
0.63
0.84
0.42
0.63
2.5
0.90
1.0
0.65
0.52
0.34
2.5
0.50
0.41
0.44
0.64
0.52
2.5
0.52
0.57
0.45
0.65
0.44
0.52
0.39
0.36
0.31
0.14
0.14
0.44
0.40
0.19
0.69
4.0
2.5
0.59
0.98
0.63
TestAmerica Tampa
Page 86 of 221
Instrument ID:
BVMJ GC/MS
Lab File ID:
1JC0222.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
MDL
0.50
0.58
0.58
0.35
0.58
2.5
0.67
0.63
0.84
0.42
0.63
2.5
0.90
1.0
0.65
0.52
0.34
2.5
0.50
0.41
0.44
0.64
0.52
2.5
0.52
0.57
0.45
0.65
0.44
0.52
0.39
0.36
0.31
0.14
0.14
0.44
0.40
0.19
0.69
4.0
2.5
0.59
0.98
0.63
PQL
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
4.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
5.0
1.0
2.0
1.0
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Client Sample ID:
IMW-F_022509
Lab Sample ID:
Client Matrix:
660-27893-33
Water
Job Number: 660-27893-1
Date Sampled:
Date Received:
02/25/2009 0918
02/26/2009 1030
8260B Volatile Organic Compounds (GC/MS)
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260B
5030B
1.0
03/02/2009 1852
03/02/2009 1852
Analyte
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
o-Xylene
Acetone
2-Butanone (MEK)
4-Methyl-2-pentanone (MIBK)
Carbon disulfide
2-Hexanone
Methyl tert-butyl ether
m-Xylene & p-Xylene
Surrogate
Toluene-d8 (Surr)
4-Bromofluorobenzene
Dibromofluoromethane
TestAmerica Tampa
Analysis Batch: 660-75700
Result (ug/L)
0.15
0.50
0.51
0.77
0.58
0.46
0.47
0.50
2.5
0.18
0.86
0.54
0.50
0.50
160
8.4
3.8
1.0
4.4
0.44
0.60
%Rec
101
104
102
Page 87 of 221
Instrument ID:
BVMJ GC/MS
Lab File ID:
1JC0222.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
MDL
0.15
0.50
0.51
0.77
0.58
0.46
0.47
0.50
2.5
0.18
0.86
0.54
0.50
0.50
9.9
8.4
3.8
0.85
4.4
0.44
0.60
PQL
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
20
10
10
1.0
10
1.0
2.0
Acceptance Limits
77 - 122
74 - 126
70 - 130
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Client Sample ID:
DMW-F_022509
Lab Sample ID:
Client Matrix:
660-27893-34
Water
Job Number: 660-27893-1
Date Sampled:
Date Received:
02/25/2009 0828
02/26/2009 1030
8260B Volatile Organic Compounds (GC/MS)
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260B
5030B
2.0
03/02/2009 2054
03/02/2009 2054
Analysis Batch: 660-75700
Analyte
Benzene
Bromobenzene
Chlorobromomethane
Dichlorobromomethane
Bromoform
Bromomethane
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
Chlorodibromomethane
1,2-Dibromo-3-Chloropropane
Ethylene Dibromide
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
Hexachlorobutadiene
Isopropylbenzene
4-Isopropyltoluene
Methylene Chloride
Naphthalene
N-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
Result (ug/L)
1.0
1.2
1.2
0.70
1.2
5.0
1.3
1.3
1.7
0.84
1.3
5.0
1.8
2.0
1.3
1.0
0.68
5.0
1.0
0.82
0.88
1.3
1.0
5.0
1.0
1.1
0.90
1.3
0.88
1.0
0.78
0.72
0.62
0.28
0.28
0.88
0.80
0.38
1.4
8.0
5.0
1.2
2.0
1.3
TestAmerica Tampa
Page 88 of 221
Instrument ID:
BVMJ GC/MS
Lab File ID:
1JC0227.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
MDL
1.0
1.2
1.2
0.70
1.2
5.0
1.3
1.3
1.7
0.84
1.3
5.0
1.8
2.0
1.3
1.0
0.68
5.0
1.0
0.82
0.88
1.3
1.0
5.0
1.0
1.1
0.90
1.3
0.88
1.0
0.78
0.72
0.62
0.28
0.28
0.88
0.80
0.38
1.4
8.0
5.0
1.2
2.0
1.3
PQL
2.0
2.0
2.0
2.0
2.0
10
2.0
2.0
2.0
2.0
2.0
10
2.0
8.0
2.0
2.0
2.0
10
2.0
2.0
2.0
2.0
2.0
10
2.0
2.0
2.0
2.0
2.0
2.0
2.0
2.0
2.0
2.0
2.0
2.0
2.0
2.0
2.0
10
10
2.0
4.0
2.0
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Client Sample ID:
DMW-F_022509
Lab Sample ID:
Client Matrix:
660-27893-34
Water
Job Number: 660-27893-1
Date Sampled:
Date Received:
02/25/2009 0828
02/26/2009 1030
8260B Volatile Organic Compounds (GC/MS)
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260B
5030B
2.0
03/02/2009 2054
03/02/2009 2054
Analyte
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
o-Xylene
Acetone
2-Butanone (MEK)
4-Methyl-2-pentanone (MIBK)
Carbon disulfide
2-Hexanone
Methyl tert-butyl ether
m-Xylene & p-Xylene
Surrogate
Toluene-d8 (Surr)
4-Bromofluorobenzene
Dibromofluoromethane
TestAmerica Tampa
Analysis Batch: 660-75700
Result (ug/L)
0.30
1.0
1.0
1.5
1.2
0.92
0.94
1.0
5.0
0.36
1.7
1.1
1.0
1.0
20
17
7.6
3.4
8.8
0.88
1.2
%Rec
103
101
104
Page 89 of 221
Instrument ID:
BVMJ GC/MS
Lab File ID:
1JC0227.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
MDL
0.30
1.0
1.0
1.5
1.2
0.92
0.94
1.0
5.0
0.36
1.7
1.1
1.0
1.0
20
17
7.6
1.7
8.8
0.88
1.2
PQL
2.0
2.0
2.0
2.0
2.0
2.0
2.0
2.0
10
2.0
2.0
2.0
2.0
2.0
40
20
20
2.0
20
2.0
4.0
Acceptance Limits
77 - 122
74 - 126
70 - 130
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Client Sample ID:
DMW-J_022509
Lab Sample ID:
Client Matrix:
660-27893-35
Water
Job Number: 660-27893-1
Date Sampled:
Date Received:
02/25/2009 1216
02/26/2009 1030
8260B Volatile Organic Compounds (GC/MS)
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260B
5030B
1.0
02/28/2009 1447
02/28/2009 1447
Analysis Batch: 660-75699
Analyte
Benzene
Bromobenzene
Chlorobromomethane
Dichlorobromomethane
Bromoform
Bromomethane
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
Chlorodibromomethane
1,2-Dibromo-3-Chloropropane
Ethylene Dibromide
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
Hexachlorobutadiene
Isopropylbenzene
4-Isopropyltoluene
Methylene Chloride
Naphthalene
N-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
Result (ug/L)
0.50
0.58
0.58
0.35
0.58
2.5
0.67
0.63
0.84
0.42
0.63
2.5
0.90
1.0
0.65
0.52
0.34
2.5
0.50
0.41
0.44
0.64
0.52
2.5
0.52
0.57
0.45
36
0.44
0.52
0.39
0.36
0.31
0.14
0.14
0.44
0.40
0.19
0.69
4.0
2.5
0.59
0.98
0.63
TestAmerica Tampa
Page 90 of 221
Instrument ID:
BVMJ GC/MS
Lab File ID:
1JB2761.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
MDL
0.50
0.58
0.58
0.35
0.58
2.5
0.67
0.63
0.84
0.42
0.63
2.5
0.90
1.0
0.65
0.52
0.34
2.5
0.50
0.41
0.44
0.64
0.52
2.5
0.52
0.57
0.45
0.65
0.44
0.52
0.39
0.36
0.31
0.14
0.14
0.44
0.40
0.19
0.69
4.0
2.5
0.59
0.98
0.63
PQL
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
4.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
5.0
1.0
2.0
1.0
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Client Sample ID:
DMW-J_022509
Lab Sample ID:
Client Matrix:
660-27893-35
Water
Job Number: 660-27893-1
Date Sampled:
Date Received:
02/25/2009 1216
02/26/2009 1030
8260B Volatile Organic Compounds (GC/MS)
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260B
5030B
1.0
02/28/2009 1447
02/28/2009 1447
Analyte
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
o-Xylene
Acetone
2-Butanone (MEK)
4-Methyl-2-pentanone (MIBK)
Carbon disulfide
2-Hexanone
Methyl tert-butyl ether
m-Xylene & p-Xylene
Surrogate
Toluene-d8 (Surr)
4-Bromofluorobenzene
Dibromofluoromethane
TestAmerica Tampa
Analysis Batch: 660-75699
Result (ug/L)
0.15
0.50
0.51
0.77
0.58
0.46
0.47
14
2.5
0.18
0.86
0.54
2.7
0.50
9.9
8.4
3.8
1.5
4.4
0.44
0.60
%Rec
99
101
98
Page 91 of 221
Instrument ID:
BVMJ GC/MS
Lab File ID:
1JB2761.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
MDL
0.15
0.50
0.51
0.77
0.58
0.46
0.47
0.50
2.5
0.18
0.86
0.54
0.50
0.50
9.9
8.4
3.8
0.85
4.4
0.44
0.60
PQL
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
20
10
10
1.0
10
1.0
2.0
Acceptance Limits
77 - 122
74 - 126
70 - 130
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Client Sample ID:
DMW-K_022509
Lab Sample ID:
Client Matrix:
660-27893-36
Water
Job Number: 660-27893-1
Date Sampled:
Date Received:
02/25/2009 0954
02/26/2009 1030
8260B Volatile Organic Compounds (GC/MS)
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260B
5030B
20
03/02/2009 2119
03/02/2009 2119
Analysis Batch: 660-75700
Analyte
Benzene
Bromobenzene
Chlorobromomethane
Dichlorobromomethane
Bromoform
Bromomethane
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
Chlorodibromomethane
1,2-Dibromo-3-Chloropropane
Ethylene Dibromide
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
Hexachlorobutadiene
Isopropylbenzene
4-Isopropyltoluene
Methylene Chloride
Naphthalene
N-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
Result (ug/L)
10
12
12
7.0
12
50
13
13
17
8.4
13
50
18
20
13
10
6.8
50
10
8.2
8.8
13
10
50
10
11
9.0
13
8.8
10
7.8
7.2
6.2
2.8
2.8
8.8
8.0
3.8
14
80
50
12
20
13
TestAmerica Tampa
Page 92 of 221
Instrument ID:
BVMJ GC/MS
Lab File ID:
1JC0228.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
MDL
10
12
12
7.0
12
50
13
13
17
8.4
13
50
18
20
13
10
6.8
50
10
8.2
8.8
13
10
50
10
11
9.0
13
8.8
10
7.8
7.2
6.2
2.8
2.8
8.8
8.0
3.8
14
80
50
12
20
13
PQL
20
20
20
20
20
100
20
20
20
20
20
100
20
80
20
20
20
100
20
20
20
20
20
100
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
100
100
20
40
20
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Client Sample ID:
DMW-K_022509
Lab Sample ID:
Client Matrix:
660-27893-36
Water
Job Number: 660-27893-1
Date Sampled:
Date Received:
02/25/2009 0954
02/26/2009 1030
8260B Volatile Organic Compounds (GC/MS)
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260B
5030B
20
03/02/2009 2119
03/02/2009 2119
Analyte
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
o-Xylene
Acetone
2-Butanone (MEK)
4-Methyl-2-pentanone (MIBK)
Carbon disulfide
2-Hexanone
Methyl tert-butyl ether
m-Xylene & p-Xylene
Surrogate
Toluene-d8 (Surr)
4-Bromofluorobenzene
Dibromofluoromethane
TestAmerica Tampa
Analysis Batch: 660-75700
Result (ug/L)
3.0
10
10
15
12
9.2
9.4
10
50
3.6
17
11
10
10
9800
170
76
17
88
8.8
12
%Rec
101
102
98
Page 93 of 221
Instrument ID:
BVMJ GC/MS
Lab File ID:
1JC0228.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
MDL
3.0
10
10
15
12
9.2
9.4
10
50
3.6
17
11
10
10
200
170
76
17
88
8.8
12
PQL
20
20
20
20
20
20
20
20
100
20
20
20
20
20
400
200
200
20
200
20
40
Acceptance Limits
77 - 122
74 - 126
70 - 130
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Client Sample ID:
DMW-L_022509
Lab Sample ID:
Client Matrix:
660-27893-37
Water
Job Number: 660-27893-1
Date Sampled:
Date Received:
02/25/2009 1105
02/26/2009 1030
8260B Volatile Organic Compounds (GC/MS)
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260B
5030B
2.0
03/02/2009 2144
03/02/2009 2144
Analysis Batch: 660-75700
Analyte
Benzene
Bromobenzene
Chlorobromomethane
Dichlorobromomethane
Bromoform
Bromomethane
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
Chlorodibromomethane
1,2-Dibromo-3-Chloropropane
Ethylene Dibromide
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
Hexachlorobutadiene
Isopropylbenzene
4-Isopropyltoluene
Methylene Chloride
Naphthalene
N-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
Result (ug/L)
1.0
1.2
1.2
0.70
1.2
5.0
1.3
1.3
1.7
0.84
1.3
5.0
1.8
2.0
1.3
1.0
0.68
5.0
1.0
0.82
0.88
1.3
1.0
5.0
1.0
1.1
0.90
1.3
0.88
1.0
0.78
0.72
0.62
0.28
0.28
0.88
0.80
0.38
1.4
8.0
5.0
1.2
2.0
1.3
TestAmerica Tampa
Page 94 of 221
Instrument ID:
BVMJ GC/MS
Lab File ID:
1JC0229.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
MDL
1.0
1.2
1.2
0.70
1.2
5.0
1.3
1.3
1.7
0.84
1.3
5.0
1.8
2.0
1.3
1.0
0.68
5.0
1.0
0.82
0.88
1.3
1.0
5.0
1.0
1.1
0.90
1.3
0.88
1.0
0.78
0.72
0.62
0.28
0.28
0.88
0.80
0.38
1.4
8.0
5.0
1.2
2.0
1.3
PQL
2.0
2.0
2.0
2.0
2.0
10
2.0
2.0
2.0
2.0
2.0
10
2.0
8.0
2.0
2.0
2.0
10
2.0
2.0
2.0
2.0
2.0
10
2.0
2.0
2.0
2.0
2.0
2.0
2.0
2.0
2.0
2.0
2.0
2.0
2.0
2.0
2.0
10
10
2.0
4.0
2.0
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Client Sample ID:
DMW-L_022509
Lab Sample ID:
Client Matrix:
660-27893-37
Water
Job Number: 660-27893-1
Date Sampled:
Date Received:
02/25/2009 1105
02/26/2009 1030
8260B Volatile Organic Compounds (GC/MS)
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260B
5030B
2.0
03/02/2009 2144
03/02/2009 2144
Analyte
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
o-Xylene
Acetone
2-Butanone (MEK)
4-Methyl-2-pentanone (MIBK)
Carbon disulfide
2-Hexanone
Methyl tert-butyl ether
m-Xylene & p-Xylene
Surrogate
Toluene-d8 (Surr)
4-Bromofluorobenzene
Dibromofluoromethane
TestAmerica Tampa
Analysis Batch: 660-75700
Result (ug/L)
0.30
1.0
1.0
1.5
1.2
0.92
0.94
1.0
5.0
0.36
1.7
1.1
1.0
1.0
20
17
7.6
1.7
8.8
0.88
1.2
%Rec
103
104
100
Page 95 of 221
Instrument ID:
BVMJ GC/MS
Lab File ID:
1JC0229.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
MDL
0.30
1.0
1.0
1.5
1.2
0.92
0.94
1.0
5.0
0.36
1.7
1.1
1.0
1.0
20
17
7.6
1.7
8.8
0.88
1.2
PQL
2.0
2.0
2.0
2.0
2.0
2.0
2.0
2.0
10
2.0
2.0
2.0
2.0
2.0
40
20
20
2.0
20
2.0
4.0
Acceptance Limits
77 - 122
74 - 126
70 - 130
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Client Sample ID:
DUPE D_022509
Lab Sample ID:
Client Matrix:
660-27893-38
Water
Job Number: 660-27893-1
Date Sampled:
Date Received:
02/25/2009 0000
02/26/2009 1030
8260B Volatile Organic Compounds (GC/MS)
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260B
5030B
1.0
02/28/2009 1600
02/28/2009 1600
Analysis Batch: 660-75699
Analyte
Benzene
Bromobenzene
Chlorobromomethane
Dichlorobromomethane
Bromoform
Bromomethane
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
Chlorodibromomethane
1,2-Dibromo-3-Chloropropane
Ethylene Dibromide
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
Hexachlorobutadiene
Isopropylbenzene
4-Isopropyltoluene
Methylene Chloride
Naphthalene
N-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
Result (ug/L)
0.50
0.58
0.58
0.35
0.58
2.5
0.67
0.63
0.84
0.42
0.63
2.5
0.90
1.0
0.65
0.52
0.34
2.5
0.50
0.41
0.44
0.64
0.52
2.5
0.52
0.57
0.45
0.65
0.44
0.52
0.39
0.36
0.31
0.14
0.14
0.44
0.40
0.19
0.69
4.0
2.5
0.59
0.98
0.63
TestAmerica Tampa
Page 96 of 221
Instrument ID:
BVMJ GC/MS
Lab File ID:
1JB2764.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
MDL
0.50
0.58
0.58
0.35
0.58
2.5
0.67
0.63
0.84
0.42
0.63
2.5
0.90
1.0
0.65
0.52
0.34
2.5
0.50
0.41
0.44
0.64
0.52
2.5
0.52
0.57
0.45
0.65
0.44
0.52
0.39
0.36
0.31
0.14
0.14
0.44
0.40
0.19
0.69
4.0
2.5
0.59
0.98
0.63
PQL
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
4.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
5.0
1.0
2.0
1.0
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Client Sample ID:
DUPE D_022509
Lab Sample ID:
Client Matrix:
660-27893-38
Water
Job Number: 660-27893-1
Date Sampled:
Date Received:
02/25/2009 0000
02/26/2009 1030
8260B Volatile Organic Compounds (GC/MS)
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260B
5030B
1.0
02/28/2009 1600
02/28/2009 1600
Analyte
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
o-Xylene
Acetone
2-Butanone (MEK)
4-Methyl-2-pentanone (MIBK)
Carbon disulfide
2-Hexanone
Methyl tert-butyl ether
m-Xylene & p-Xylene
Surrogate
Toluene-d8 (Surr)
4-Bromofluorobenzene
Dibromofluoromethane
TestAmerica Tampa
Analysis Batch: 660-75699
Result (ug/L)
0.15
0.50
0.51
0.77
0.58
0.46
0.47
0.50
2.5
0.18
0.86
0.54
0.50
0.50
9.9
8.4
3.8
0.85
4.4
0.44
0.60
%Rec
100
101
100
Page 97 of 221
Instrument ID:
BVMJ GC/MS
Lab File ID:
1JB2764.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
MDL
0.15
0.50
0.51
0.77
0.58
0.46
0.47
0.50
2.5
0.18
0.86
0.54
0.50
0.50
9.9
8.4
3.8
0.85
4.4
0.44
0.60
PQL
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
20
10
10
1.0
10
1.0
2.0
Acceptance Limits
77 - 122
74 - 126
70 - 130
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Client Sample ID:
DUPE H_022509
Lab Sample ID:
Client Matrix:
660-27893-39
Water
Job Number: 660-27893-1
Date Sampled:
Date Received:
02/25/2009 0000
02/26/2009 1030
8260B Volatile Organic Compounds (GC/MS)
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260B
5030B
50
03/02/2009 2208
03/02/2009 2208
Analysis Batch: 660-75700
Analyte
Benzene
Bromobenzene
Chlorobromomethane
Dichlorobromomethane
Bromoform
Bromomethane
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
Chlorodibromomethane
1,2-Dibromo-3-Chloropropane
Ethylene Dibromide
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
Hexachlorobutadiene
Isopropylbenzene
4-Isopropyltoluene
Methylene Chloride
Naphthalene
N-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
Result (ug/L)
25
29
29
18
29
120
34
32
42
21
32
120
45
50
32
26
17
120
25
20
22
32
26
120
26
28
22
32
22
26
20
18
16
7.0
7.0
22
20
9.5
34
200
120
30
49
32
TestAmerica Tampa
Page 98 of 221
Instrument ID:
BVMJ GC/MS
Lab File ID:
1JC0230.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
MDL
25
29
29
18
29
120
34
32
42
21
32
120
45
50
32
26
17
120
25
20
22
32
26
120
26
28
22
32
22
26
20
18
16
7.0
7.0
22
20
9.5
34
200
120
30
49
32
PQL
50
50
50
50
50
250
50
50
50
50
50
250
50
200
50
50
50
250
50
50
50
50
50
250
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
250
250
50
100
50
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Client Sample ID:
DUPE H_022509
Lab Sample ID:
Client Matrix:
660-27893-39
Water
Job Number: 660-27893-1
Date Sampled:
Date Received:
02/25/2009 0000
02/26/2009 1030
8260B Volatile Organic Compounds (GC/MS)
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260B
5030B
50
03/02/2009 2208
03/02/2009 2208
Analyte
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
o-Xylene
Acetone
2-Butanone (MEK)
4-Methyl-2-pentanone (MIBK)
Carbon disulfide
2-Hexanone
Methyl tert-butyl ether
m-Xylene & p-Xylene
Surrogate
Toluene-d8 (Surr)
4-Bromofluorobenzene
Dibromofluoromethane
TestAmerica Tampa
Analysis Batch: 660-75700
Result (ug/L)
7.5
25
26
38
29
23
24
25
120
9.0
43
27
25
25
8800
420
190
42
220
22
30
%Rec
102
102
101
Page 99 of 221
Instrument ID:
BVMJ GC/MS
Lab File ID:
1JC0230.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
MDL
7.5
25
26
38
29
23
24
25
120
9.0
43
27
25
25
500
420
190
42
220
22
30
PQL
50
50
50
50
50
50
50
50
250
50
50
50
50
50
1000
500
500
50
500
50
100
Acceptance Limits
77 - 122
74 - 126
70 - 130
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Job Number: 660-27893-1
Client Sample ID:
Trip Blank_022509
Lab Sample ID:
Client Matrix:
660-27893-40
Water
Date Sampled:
Date Received:
02/25/2009 0000
02/26/2009 1030
8260B Volatile Organic Compounds (GC/MS)
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260B
5030B
1.0
03/02/2009 1513
03/02/2009 1513
Analyte
Benzene
Bromobenzene
Chlorobromomethane
Dichlorobromomethane
Bromoform
Bromomethane
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
Chlorodibromomethane
1,2-Dibromo-3-Chloropropane
Ethylene Dibromide
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
Hexachlorobutadiene
Isopropylbenzene
4-Isopropyltoluene
Methylene Chloride
Naphthalene
N-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
TestAmerica Tampa
Analysis Batch: 660-75700
Result (ug/L)
0.50
0.58
0.58
0.35
0.58
2.5
0.67
0.63
0.84
0.42
0.63
2.5
0.90
1.0
0.65
0.52
0.34
2.5
0.50
0.41
0.44
0.64
0.52
2.5
0.52
0.57
0.45
0.65
0.44
0.52
0.39
0.36
0.31
0.14
0.14
0.44
0.40
0.19
0.69
4.0
2.5
0.59
0.98
0.63
Page 100 of 221
Instrument ID:
BVMJ GC/MS
Lab File ID:
1JC0213.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
MDL
0.50
0.58
0.58
0.35
0.58
2.5
0.67
0.63
0.84
0.42
0.63
2.5
0.90
1.0
0.65
0.52
0.34
2.5
0.50
0.41
0.44
0.64
0.52
2.5
0.52
0.57
0.45
0.65
0.44
0.52
0.39
0.36
0.31
0.14
0.14
0.44
0.40
0.19
0.69
4.0
2.5
0.59
0.98
0.63
PQL
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
4.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
5.0
1.0
2.0
1.0
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Job Number: 660-27893-1
Client Sample ID:
Trip Blank_022509
Lab Sample ID:
Client Matrix:
660-27893-40
Water
Date Sampled:
Date Received:
02/25/2009 0000
02/26/2009 1030
8260B Volatile Organic Compounds (GC/MS)
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260B
5030B
1.0
03/02/2009 1513
03/02/2009 1513
Analyte
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
o-Xylene
Acetone
2-Butanone (MEK)
4-Methyl-2-pentanone (MIBK)
Carbon disulfide
2-Hexanone
Methyl tert-butyl ether
m-Xylene & p-Xylene
Surrogate
Toluene-d8 (Surr)
4-Bromofluorobenzene
Dibromofluoromethane
TestAmerica Tampa
Analysis Batch: 660-75700
Result (ug/L)
0.15
0.50
0.51
0.77
0.58
0.46
0.47
0.50
2.5
0.18
0.86
0.54
0.50
0.50
9.9
8.4
3.8
0.85
4.4
0.44
0.60
%Rec
102
106
98
Page 101 of 221
Instrument ID:
BVMJ GC/MS
Lab File ID:
1JC0213.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
MDL
0.15
0.50
0.51
0.77
0.58
0.46
0.47
0.50
2.5
0.18
0.86
0.54
0.50
0.50
9.9
8.4
3.8
0.85
4.4
0.44
0.60
PQL
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
20
10
10
1.0
10
1.0
2.0
Acceptance Limits
77 - 122
74 - 126
70 - 130
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Job Number: 660-27893-1
Client Sample ID:
DMW-P_022509
Lab Sample ID:
Client Matrix:
660-27893-1
Water
Date Sampled:
Date Received:
02/25/2009 0857
02/26/2009 1030
8260C SIM/ID 1,4-Dioxane by SIM/Isotopic Dilution
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260C SIM/ID
5030B
1.0
02/27/2009 1634
02/27/2009 1634
Analyte
1,4-Dioxane
TestAmerica Tampa
Analysis Batch: 660-75525
Result (ug/L)
0.54
Page 102 of 221
Instrument ID:
BVMH GC/MS
Lab File ID:
1HB2729.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
U
MDL
0.54
PQL
1.0
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Job Number: 660-27893-1
Client Sample ID:
DMW-O_022509
Lab Sample ID:
Client Matrix:
660-27893-2
Water
Date Sampled:
Date Received:
02/25/2009 0944
02/26/2009 1030
8260C SIM/ID 1,4-Dioxane by SIM/Isotopic Dilution
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260C SIM/ID
5030B
1.0
02/27/2009 1651
02/27/2009 1651
Analyte
1,4-Dioxane
TestAmerica Tampa
Analysis Batch: 660-75525
Result (ug/L)
0.54
Page 103 of 221
Instrument ID:
BVMH GC/MS
Lab File ID:
1HB2730.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
U
MDL
0.54
PQL
1.0
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Job Number: 660-27893-1
Client Sample ID:
DMW-Q_022509
Lab Sample ID:
Client Matrix:
660-27893-3
Water
Date Sampled:
Date Received:
02/25/2009 1013
02/26/2009 1030
8260C SIM/ID 1,4-Dioxane by SIM/Isotopic Dilution
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260C SIM/ID
5030B
1.0
02/27/2009 1708
02/27/2009 1708
Analyte
1,4-Dioxane
TestAmerica Tampa
Analysis Batch: 660-75525
Result (ug/L)
0.54
Page 104 of 221
Instrument ID:
BVMH GC/MS
Lab File ID:
1HB2731.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
U
MDL
0.54
PQL
1.0
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Job Number: 660-27893-1
Client Sample ID:
DMW-C_022509
Lab Sample ID:
Client Matrix:
660-27893-4
Water
Date Sampled:
Date Received:
02/25/2009 1112
02/26/2009 1030
8260C SIM/ID 1,4-Dioxane by SIM/Isotopic Dilution
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260C SIM/ID
5030B
1.0
02/27/2009 1725
02/27/2009 1725
Analyte
1,4-Dioxane
TestAmerica Tampa
Analysis Batch: 660-75525
Result (ug/L)
16
Page 105 of 221
Instrument ID:
BVMH GC/MS
Lab File ID:
1HB2732.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
MDL
0.54
PQL
1.0
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Job Number: 660-27893-1
Client Sample ID:
IMW-D_022509
Lab Sample ID:
Client Matrix:
660-27893-5
Water
Date Sampled:
Date Received:
02/25/2009 1154
02/26/2009 1030
8260C SIM/ID 1,4-Dioxane by SIM/Isotopic Dilution
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260C SIM/ID
5030B
1.0
02/27/2009 1743
02/27/2009 1743
Analyte
1,4-Dioxane
TestAmerica Tampa
Analysis Batch: 660-75525
Result (ug/L)
5.2
Page 106 of 221
Instrument ID:
BVMH GC/MS
Lab File ID:
1HB2733.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
MDL
0.54
PQL
1.0
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Job Number: 660-27893-1
Client Sample ID:
DMW-B_022509
Lab Sample ID:
Client Matrix:
660-27893-6
Water
Date Sampled:
Date Received:
02/25/2009 1238
02/26/2009 1030
8260C SIM/ID 1,4-Dioxane by SIM/Isotopic Dilution
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260C SIM/ID
5030B
1.0
02/27/2009 1800
02/27/2009 1800
Analyte
1,4-Dioxane
TestAmerica Tampa
Analysis Batch: 660-75525
Result (ug/L)
0.54
Page 107 of 221
Instrument ID:
BVMH GC/MS
Lab File ID:
1HB2734.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
U
MDL
0.54
PQL
1.0
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Job Number: 660-27893-1
Client Sample ID:
IDPT-15_022509
Lab Sample ID:
Client Matrix:
660-27893-7
Water
Date Sampled:
Date Received:
02/25/2009 1425
02/26/2009 1030
8260C SIM/ID 1,4-Dioxane by SIM/Isotopic Dilution
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260C SIM/ID
5030B
1.0
02/27/2009 1817
02/27/2009 1817
Analyte
1,4-Dioxane
TestAmerica Tampa
Analysis Batch: 660-75525
Result (ug/L)
78
Page 108 of 221
Instrument ID:
BVMH GC/MS
Lab File ID:
1HB2735.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
MDL
0.54
PQL
1.0
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Job Number: 660-27893-1
Client Sample ID:
DMW-8_022509
Lab Sample ID:
Client Matrix:
660-27893-8
Water
Date Sampled:
Date Received:
02/25/2009 1553
02/26/2009 1030
8260C SIM/ID 1,4-Dioxane by SIM/Isotopic Dilution
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260C SIM/ID
5030B
1.0
03/02/2009 1538
03/02/2009 1538
Analyte
1,4-Dioxane
TestAmerica Tampa
Analysis Batch: 660-75613
Result (ug/L)
0.54
Page 109 of 221
Instrument ID:
BVMH GC/MS
Lab File ID:
1HC0226.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
U
MDL
0.54
PQL
1.0
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Job Number: 660-27893-1
Client Sample ID:
SMW-D_022509
Lab Sample ID:
Client Matrix:
660-27893-9
Water
Date Sampled:
Date Received:
02/25/2009 1614
02/26/2009 1030
8260C SIM/ID 1,4-Dioxane by SIM/Isotopic Dilution
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260C SIM/ID
5030B
1.0
03/02/2009 1229
03/02/2009 1229
Analyte
1,4-Dioxane
TestAmerica Tampa
Analysis Batch: 660-75613
Result (ug/L)
0.54
Page 110 of 221
Instrument ID:
BVMH GC/MS
Lab File ID:
1HC0215.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
U
MDL
0.54
PQL
1.0
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Job Number: 660-27893-1
Client Sample ID:
IDPT-8_022509
Lab Sample ID:
Client Matrix:
660-27893-10
Water
Date Sampled:
Date Received:
02/25/2009 1648
02/26/2009 1030
8260C SIM/ID 1,4-Dioxane by SIM/Isotopic Dilution
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260C SIM/ID
5030B
1.0
03/02/2009 1212
03/02/2009 1212
Analyte
1,4-Dioxane
TestAmerica Tampa
Analysis Batch: 660-75613
Result (ug/L)
20
Page 111 of 221
Instrument ID:
BVMH GC/MS
Lab File ID:
1HC0214.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
MDL
0.54
PQL
1.0
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Job Number: 660-27893-1
Client Sample ID:
IDPT-9_022509
Lab Sample ID:
Client Matrix:
660-27893-11
Water
Date Sampled:
Date Received:
02/25/2009 1730
02/26/2009 1030
8260C SIM/ID 1,4-Dioxane by SIM/Isotopic Dilution
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260C SIM/ID
5030B
1.0
03/02/2009 1247
03/02/2009 1247
Analyte
1,4-Dioxane
TestAmerica Tampa
Analysis Batch: 660-75613
Result (ug/L)
9.5
Page 112 of 221
Instrument ID:
BVMH GC/MS
Lab File ID:
1HC0216.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
MDL
0.54
PQL
1.0
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Job Number: 660-27893-1
Client Sample ID:
SMW-E_022509
Lab Sample ID:
Client Matrix:
660-27893-12
Water
Date Sampled:
Date Received:
02/25/2009 1814
02/26/2009 1030
8260C SIM/ID 1,4-Dioxane by SIM/Isotopic Dilution
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260C SIM/ID
5030B
1.0
03/02/2009 1304
03/02/2009 1304
Analyte
1,4-Dioxane
TestAmerica Tampa
Analysis Batch: 660-75613
Result (ug/L)
1.4
Page 113 of 221
Instrument ID:
BVMH GC/MS
Lab File ID:
1HC0217.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
MDL
0.54
PQL
1.0
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Job Number: 660-27893-1
Client Sample ID:
SMW-H_022509
Lab Sample ID:
Client Matrix:
660-27893-13
Water
Date Sampled:
Date Received:
02/25/2009 1405
02/26/2009 1030
8260C SIM/ID 1,4-Dioxane by SIM/Isotopic Dilution
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260C SIM/ID
5030B
1.0
03/03/2009 1246
03/03/2009 1246
Analyte
1,4-Dioxane
TestAmerica Tampa
Analysis Batch: 660-75684
Result (ug/L)
0.80
Page 114 of 221
Instrument ID:
BVMH GC/MS
Lab File ID:
1HC0315.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
I
MDL
0.54
PQL
1.0
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Job Number: 660-27893-1
Client Sample ID:
DMW-N_022509
Lab Sample ID:
Client Matrix:
660-27893-14
Water
Date Sampled:
Date Received:
02/25/2009 1055
02/26/2009 1030
8260C SIM/ID 1,4-Dioxane by SIM/Isotopic Dilution
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260C SIM/ID
5030B
1.0
03/02/2009 1321
03/02/2009 1321
Analyte
1,4-Dioxane
TestAmerica Tampa
Analysis Batch: 660-75613
Result (ug/L)
0.54
Page 115 of 221
Instrument ID:
BVMH GC/MS
Lab File ID:
1HC0218.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
U
MDL
0.54
PQL
1.0
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Job Number: 660-27893-1
Client Sample ID:
DUPE E_022509
Lab Sample ID:
Client Matrix:
660-27893-15
Water
Date Sampled:
Date Received:
02/25/2009 0000
02/26/2009 1030
8260C SIM/ID 1,4-Dioxane by SIM/Isotopic Dilution
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260C SIM/ID
5030B
1.0
03/02/2009 1447
03/02/2009 1447
Analyte
1,4-Dioxane
TestAmerica Tampa
Analysis Batch: 660-75613
Result (ug/L)
0.54
Page 116 of 221
Instrument ID:
BVMH GC/MS
Lab File ID:
1HC0223.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
U
MDL
0.54
PQL
1.0
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Job Number: 660-27893-1
Client Sample ID:
SMW-I_022509
Lab Sample ID:
Client Matrix:
660-27893-16
Water
Date Sampled:
Date Received:
02/25/2009 1130
02/26/2009 1030
8260C SIM/ID 1,4-Dioxane by SIM/Isotopic Dilution
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260C SIM/ID
5030B
1.0
03/02/2009 1430
03/02/2009 1430
Analyte
1,4-Dioxane
TestAmerica Tampa
Analysis Batch: 660-75613
Result (ug/L)
0.54
Page 117 of 221
Instrument ID:
BVMH GC/MS
Lab File ID:
1HC0222.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
U
MDL
0.54
PQL
1.0
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Job Number: 660-27893-1
Client Sample ID:
DMW-I_022509
Lab Sample ID:
Client Matrix:
660-27893-17
Water
Date Sampled:
Date Received:
02/25/2009 1440
02/26/2009 1030
8260C SIM/ID 1,4-Dioxane by SIM/Isotopic Dilution
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260C SIM/ID
5030B
1.0
03/02/2009 1338
03/02/2009 1338
Analyte
1,4-Dioxane
TestAmerica Tampa
Analysis Batch: 660-75613
Result (ug/L)
5.1
Page 118 of 221
Instrument ID:
BVMH GC/MS
Lab File ID:
1HC0219.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
MDL
0.54
PQL
1.0
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Job Number: 660-27893-1
Client Sample ID:
SMW-N_022509
Lab Sample ID:
Client Matrix:
660-27893-18
Water
Date Sampled:
Date Received:
02/25/2009 1020
02/26/2009 1030
8260C SIM/ID 1,4-Dioxane by SIM/Isotopic Dilution
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260C SIM/ID
5030B
1.0
03/02/2009 1412
03/02/2009 1412
Analyte
1,4-Dioxane
TestAmerica Tampa
Analysis Batch: 660-75613
Result (ug/L)
0.95
Page 119 of 221
Instrument ID:
BVMH GC/MS
Lab File ID:
1HC0221.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
I
MDL
0.54
PQL
1.0
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Job Number: 660-27893-1
Client Sample ID:
IDPT-12_022509
Lab Sample ID:
Client Matrix:
660-27893-19
Water
Date Sampled:
Date Received:
02/25/2009 1640
02/26/2009 1030
8260C SIM/ID 1,4-Dioxane by SIM/Isotopic Dilution
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260C SIM/ID
5030B
1.0
03/02/2009 1355
03/02/2009 1355
Analyte
1,4-Dioxane
TestAmerica Tampa
Analysis Batch: 660-75613
Result (ug/L)
27
Page 120 of 221
Instrument ID:
BVMH GC/MS
Lab File ID:
1HC0220.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
MDL
0.54
PQL
1.0
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Job Number: 660-27893-1
Client Sample ID:
IMW-J_022509
Lab Sample ID:
Client Matrix:
660-27893-20
Water
Date Sampled:
Date Received:
02/25/2009 1540
02/26/2009 1030
8260C SIM/ID 1,4-Dioxane by SIM/Isotopic Dilution
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260C SIM/ID
5030B
1.0
03/02/2009 1521
03/02/2009 1521
Analyte
1,4-Dioxane
TestAmerica Tampa
Analysis Batch: 660-75613
Result (ug/L)
0.54
Page 121 of 221
Instrument ID:
BVMH GC/MS
Lab File ID:
1HC0225.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
U
MDL
0.54
PQL
1.0
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Job Number: 660-27893-1
Client Sample ID:
DMW-A_022509
Lab Sample ID:
Client Matrix:
660-27893-21
Water
Date Sampled:
Date Received:
02/25/2009 1200
02/26/2009 1030
8260C SIM/ID 1,4-Dioxane by SIM/Isotopic Dilution
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260C SIM/ID
5030B
1.0
02/28/2009 0140
02/28/2009 0140
Analyte
1,4-Dioxane
TestAmerica Tampa
Analysis Batch: 660-75694
Result (ug/L)
0.54
Page 122 of 221
Instrument ID:
BVMJ GC/MS
Lab File ID:
1JB2729.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
U
MDL
0.54
PQL
1.0
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Job Number: 660-27893-1
Client Sample ID:
DMW-W_022509
Lab Sample ID:
Client Matrix:
660-27893-22
Water
Date Sampled:
Date Received:
02/25/2009 0946
02/26/2009 1030
8260C SIM/ID 1,4-Dioxane by SIM/Isotopic Dilution
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260C SIM/ID
5030B
1.0
03/02/2009 1538
03/02/2009 1538
Analyte
1,4-Dioxane
TestAmerica Tampa
Analysis Batch: 660-75696
Result (ug/L)
0.54
Page 123 of 221
Instrument ID:
BVMJ GC/MS
Lab File ID:
1JC0214.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
U
MDL
0.54
PQL
1.0
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Client Sample ID:
H-1_022509
Lab Sample ID:
Client Matrix:
660-27893-23
Water
Job Number: 660-27893-1
Date Sampled:
Date Received:
02/25/2009 1300
02/26/2009 1030
8260C SIM/ID 1,4-Dioxane by SIM/Isotopic Dilution
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260C SIM/ID
5030B
1.0
03/02/2009 1651
03/02/2009 1651
Analyte
1,4-Dioxane
TestAmerica Tampa
Analysis Batch: 660-75696
Result (ug/L)
0.54
Page 124 of 221
Instrument ID:
BVMJ GC/MS
Lab File ID:
1JC0217.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
U
MDL
0.54
PQL
1.0
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Job Number: 660-27893-1
Client Sample ID:
SMW-A_022509
Lab Sample ID:
Client Matrix:
660-27893-24
Water
Date Sampled:
Date Received:
02/25/2009 1235
02/26/2009 1030
8260C SIM/ID 1,4-Dioxane by SIM/Isotopic Dilution
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260C SIM/ID
5030B
1.0
03/02/2009 1715
03/02/2009 1715
Analyte
1,4-Dioxane
TestAmerica Tampa
Analysis Batch: 660-75696
Result (ug/L)
0.54
Page 125 of 221
Instrument ID:
BVMJ GC/MS
Lab File ID:
1JC0218.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
U
MDL
0.54
PQL
1.0
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Job Number: 660-27893-1
Client Sample ID:
Trip Blank 3_022509
Lab Sample ID:
Client Matrix:
660-27893-25
Water
Date Sampled:
Date Received:
02/25/2009 0000
02/26/2009 1030
8260C SIM/ID 1,4-Dioxane by SIM/Isotopic Dilution
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260C SIM/ID
5030B
1.0
02/28/2009 0955
02/28/2009 0955
Analyte
1,4-Dioxane
TestAmerica Tampa
Analysis Batch: 660-75695
Result (ug/L)
0.54
Page 126 of 221
Instrument ID:
BVMJ GC/MS
Lab File ID:
1JB2749.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
U
MDL
0.54
PQL
1.0
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Job Number: 660-27893-1
Client Sample ID:
IDPT-1_022509
Lab Sample ID:
Client Matrix:
660-27893-26
Water
Date Sampled:
Date Received:
02/25/2009 1555
02/26/2009 1030
8260C SIM/ID 1,4-Dioxane by SIM/Isotopic Dilution
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260C SIM/ID
5030B
1.0
02/28/2009 1019
02/28/2009 1019
Analyte
1,4-Dioxane
TestAmerica Tampa
Analysis Batch: 660-75695
Result (ug/L)
14
Page 127 of 221
Instrument ID:
BVMJ GC/MS
Lab File ID:
1JB2750.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
MDL
0.54
PQL
1.0
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Job Number: 660-27893-1
Client Sample ID:
IDPT-2_022509
Lab Sample ID:
Client Matrix:
660-27893-27
Water
Date Sampled:
Date Received:
02/25/2009 1654
02/26/2009 1030
8260C SIM/ID 1,4-Dioxane by SIM/Isotopic Dilution
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260C SIM/ID
5030B
1.0
03/02/2009 1739
03/02/2009 1739
Analyte
1,4-Dioxane
TestAmerica Tampa
Analysis Batch: 660-75696
Result (ug/L)
0.54
Page 128 of 221
Instrument ID:
BVMJ GC/MS
Lab File ID:
1JC0219.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
U
MDL
0.54
PQL
1.0
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Job Number: 660-27893-1
Client Sample ID:
IDPT-5_022509
Lab Sample ID:
Client Matrix:
660-27893-28
Water
Date Sampled:
Date Received:
02/25/2009 1422
02/26/2009 1030
8260C SIM/ID 1,4-Dioxane by SIM/Isotopic Dilution
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260C SIM/ID
5030B
1.0
02/28/2009 1156
02/28/2009 1156
Analyte
1,4-Dioxane
TestAmerica Tampa
Analysis Batch: 660-75695
Result (ug/L)
24
Page 129 of 221
Instrument ID:
BVMJ GC/MS
Lab File ID:
1JB2754.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
MDL
0.54
PQL
1.0
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Job Number: 660-27893-1
Client Sample ID:
IDPT-6_022509
Lab Sample ID:
Client Matrix:
660-27893-29
Water
Date Sampled:
Date Received:
02/25/2009 1725
02/26/2009 1030
8260C SIM/ID 1,4-Dioxane by SIM/Isotopic Dilution
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260C SIM/ID
5030B
5.0
03/02/2009 2005
03/02/2009 2005
Analyte
1,4-Dioxane
TestAmerica Tampa
Analysis Batch: 660-75696
Result (ug/L)
100
Page 130 of 221
Instrument ID:
BVMJ GC/MS
Lab File ID:
1JC0225.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
MDL
2.7
PQL
5.0
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Job Number: 660-27893-1
Client Sample ID:
IDPT-10_022509
Lab Sample ID:
Client Matrix:
660-27893-30
Water
Date Sampled:
Date Received:
02/25/2009 1626
02/26/2009 1030
8260C SIM/ID 1,4-Dioxane by SIM/Isotopic Dilution
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260C SIM/ID
5030B
1.0
03/02/2009 1804
03/02/2009 1804
Analyte
1,4-Dioxane
TestAmerica Tampa
Analysis Batch: 660-75696
Result (ug/L)
0.54
Page 131 of 221
Instrument ID:
BVMJ GC/MS
Lab File ID:
1JC0220.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
U
MDL
0.54
PQL
1.0
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Job Number: 660-27893-1
Client Sample ID:
IDPT-13_022509
Lab Sample ID:
Client Matrix:
660-27893-31
Water
Date Sampled:
Date Received:
02/25/2009 1455
02/26/2009 1030
8260C SIM/ID 1,4-Dioxane by SIM/Isotopic Dilution
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260C SIM/ID
5030B
1.0
03/02/2009 1828
03/02/2009 1828
Analyte
1,4-Dioxane
TestAmerica Tampa
Analysis Batch: 660-75696
Result (ug/L)
0.77
Page 132 of 221
Instrument ID:
BVMJ GC/MS
Lab File ID:
1JC0221.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
I
MDL
0.54
PQL
1.0
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Job Number: 660-27893-1
Client Sample ID:
IDPT-14_022509
Lab Sample ID:
Client Matrix:
660-27893-32
Water
Date Sampled:
Date Received:
02/25/2009 1317
02/26/2009 1030
8260C SIM/ID 1,4-Dioxane by SIM/Isotopic Dilution
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260C SIM/ID
5030B
50
03/02/2009 2030
03/02/2009 2030
Analyte
1,4-Dioxane
TestAmerica Tampa
Analysis Batch: 660-75696
Result (ug/L)
160
Page 133 of 221
Instrument ID:
BVMJ GC/MS
Lab File ID:
1JC0226.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
MDL
27
PQL
50
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Job Number: 660-27893-1
Client Sample ID:
IMW-F_022509
Lab Sample ID:
Client Matrix:
660-27893-33
Water
Date Sampled:
Date Received:
02/25/2009 0918
02/26/2009 1030
8260C SIM/ID 1,4-Dioxane by SIM/Isotopic Dilution
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260C SIM/ID
5030B
1.0
03/02/2009 1852
03/02/2009 1852
Analyte
1,4-Dioxane
TestAmerica Tampa
Analysis Batch: 660-75696
Result (ug/L)
7.9
Page 134 of 221
Instrument ID:
BVMJ GC/MS
Lab File ID:
1JC0222.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
MDL
0.54
PQL
1.0
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Job Number: 660-27893-1
Client Sample ID:
DMW-F_022509
Lab Sample ID:
Client Matrix:
660-27893-34
Water
Date Sampled:
Date Received:
02/25/2009 0828
02/26/2009 1030
8260C SIM/ID 1,4-Dioxane by SIM/Isotopic Dilution
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260C SIM/ID
5030B
2.0
03/02/2009 2054
03/02/2009 2054
Analyte
1,4-Dioxane
TestAmerica Tampa
Analysis Batch: 660-75696
Result (ug/L)
110
Page 135 of 221
Instrument ID:
BVMJ GC/MS
Lab File ID:
1JC0227.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
MDL
1.1
PQL
2.0
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Job Number: 660-27893-1
Client Sample ID:
DMW-J_022509
Lab Sample ID:
Client Matrix:
660-27893-35
Water
Date Sampled:
Date Received:
02/25/2009 1216
02/26/2009 1030
8260C SIM/ID 1,4-Dioxane by SIM/Isotopic Dilution
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260C SIM/ID
5030B
1.0
03/02/2009 1917
03/02/2009 1917
Analyte
1,4-Dioxane
TestAmerica Tampa
Analysis Batch: 660-75696
Result (ug/L)
6.2
Page 136 of 221
Instrument ID:
BVMJ GC/MS
Lab File ID:
1JC0223.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
MDL
0.54
PQL
1.0
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Job Number: 660-27893-1
Client Sample ID:
DMW-K_022509
Lab Sample ID:
Client Matrix:
660-27893-36
Water
Date Sampled:
Date Received:
02/25/2009 0954
02/26/2009 1030
8260C SIM/ID 1,4-Dioxane by SIM/Isotopic Dilution
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260C SIM/ID
5030B
20
03/02/2009 2119
03/02/2009 2119
Analyte
1,4-Dioxane
TestAmerica Tampa
Analysis Batch: 660-75696
Result (ug/L)
55
Page 137 of 221
Instrument ID:
BVMJ GC/MS
Lab File ID:
1JC0228.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
MDL
11
PQL
20
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Job Number: 660-27893-1
Client Sample ID:
DMW-L_022509
Lab Sample ID:
Client Matrix:
660-27893-37
Water
Date Sampled:
Date Received:
02/25/2009 1105
02/26/2009 1030
8260C SIM/ID 1,4-Dioxane by SIM/Isotopic Dilution
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260C SIM/ID
5030B
2.0
03/02/2009 2144
03/02/2009 2144
Analyte
1,4-Dioxane
TestAmerica Tampa
Analysis Batch: 660-75696
Result (ug/L)
88
Page 138 of 221
Instrument ID:
BVMJ GC/MS
Lab File ID:
1JC0229.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
MDL
1.1
PQL
2.0
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Job Number: 660-27893-1
Client Sample ID:
DUPE D_022509
Lab Sample ID:
Client Matrix:
660-27893-38
Water
Date Sampled:
Date Received:
02/25/2009 0000
02/26/2009 1030
8260C SIM/ID 1,4-Dioxane by SIM/Isotopic Dilution
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260C SIM/ID
5030B
1.0
03/02/2009 1941
03/02/2009 1941
Analyte
1,4-Dioxane
TestAmerica Tampa
Analysis Batch: 660-75696
Result (ug/L)
0.97
Page 139 of 221
Instrument ID:
BVMJ GC/MS
Lab File ID:
1JC0224.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
I
MDL
0.54
PQL
1.0
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Job Number: 660-27893-1
Client Sample ID:
DUPE H_022509
Lab Sample ID:
Client Matrix:
660-27893-39
Water
Date Sampled:
Date Received:
02/25/2009 0000
02/26/2009 1030
8260C SIM/ID 1,4-Dioxane by SIM/Isotopic Dilution
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260C SIM/ID
5030B
50
03/02/2009 2208
03/02/2009 2208
Analyte
1,4-Dioxane
TestAmerica Tampa
Analysis Batch: 660-75696
Result (ug/L)
59
Page 140 of 221
Instrument ID:
BVMJ GC/MS
Lab File ID:
1JC0230.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
MDL
27
PQL
50
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Job Number: 660-27893-1
Client Sample ID:
Trip Blank_022509
Lab Sample ID:
Client Matrix:
660-27893-40
Water
Date Sampled:
Date Received:
02/25/2009 0000
02/26/2009 1030
8260C SIM/ID 1,4-Dioxane by SIM/Isotopic Dilution
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260C SIM/ID
5030B
1.0
02/28/2009 1648
02/28/2009 1648
Analyte
1,4-Dioxane
TestAmerica Tampa
Analysis Batch: 660-75695
Result (ug/L)
0.54
Page 141 of 221
Instrument ID:
BVMJ GC/MS
Lab File ID:
1JB2766.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
U
MDL
0.54
PQL
1.0
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Client Sample ID:
IDPT-14_022509
Lab Sample ID:
Client Matrix:
660-27893-41
Water
Job Number: 660-27893-1
Date Sampled:
Date Received:
02/25/2009 1317
02/26/2009 1030
6010B Metals (ICP)-Total Recoverable
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
6010B
3005A
1.0
03/03/2009 1324
02/27/2009 1027
Analysis Batch: 660-75689
Prep Batch: 660-75517
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
TJA ICP TRACE
9C03A
50 mL
50 mL
Analyte
Result (mg/L)
Qualifier
MDL
PQL
Calcium
Iron
Potassium
Magnesium
Manganese
Sodium
120
9.7
1.2
2.8
0.0072
45
J3
J3
0.10
0.050
0.19
0.020
0.0010
0.31
0.50
0.20
1.0
0.080
0.0040
0.50
6010B Metals (ICP)-Dissolved
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
6010B
3005A
1.0
03/03/2009 1351
02/27/2009 1027
Analysis Batch: 660-75689
Prep Batch: 660-75517
Analyte
Result (mg/L)
Iron, Dissolved
Manganese, Dissolved
9.0
0.0065
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Qualifier
TJA ICP TRACE
9C03A
50 mL
50 mL
MDL
PQL
0.050
0.0010
0.20
0.0040
SM 2340B Hardness, Calculation
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
SM 2340B
N/A
1.0
03/03/2009 1527
N/A
Analysis Batch: 660-75708
Analyte
Result (mg/L)
Hardness as calcium carbonate
Calcium hardness as calcium carbonate
Magnesium hardness as calcium carbonate
310
290
12
TestAmerica Tampa
Page 142 of 221
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Qualifier
No Equipment
N/A
1.0 mL
PQL
PQL
3.3
1.2
2.1
3.3
1.2
2.1
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Client Sample ID:
DMW-F_022509
Lab Sample ID:
Client Matrix:
660-27893-42
Water
Job Number: 660-27893-1
Date Sampled:
Date Received:
02/25/2009 0828
02/26/2009 1030
6010B Metals (ICP)-Total Recoverable
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
6010B
3005A
1.0
03/03/2009 1357
02/27/2009 1027
Analysis Batch: 660-75689
Prep Batch: 660-75517
Analyte
Result (mg/L)
Calcium
Iron
Potassium
Magnesium
Manganese
Sodium
99
2.6
0.45
2.5
0.0065
17
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Qualifier
I
TJA ICP TRACE
9C03A
50 mL
50 mL
MDL
PQL
0.10
0.050
0.19
0.020
0.0010
0.31
0.50
0.20
1.0
0.080
0.0040
0.50
6010B Metals (ICP)-Dissolved
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
6010B
3005A
1.0
03/03/2009 1403
02/27/2009 1027
Analysis Batch: 660-75689
Prep Batch: 660-75517
Analyte
Result (mg/L)
Iron, Dissolved
Manganese, Dissolved
2.6
0.0066
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Qualifier
TJA ICP TRACE
9C03A
50 mL
50 mL
MDL
PQL
0.050
0.0010
0.20
0.0040
SM 2340B Hardness, Calculation
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
SM 2340B
N/A
1.0
03/03/2009 1527
N/A
Analysis Batch: 660-75708
Analyte
Result (mg/L)
Hardness as calcium carbonate
Calcium hardness as calcium carbonate
Magnesium hardness as calcium carbonate
260
250
10
TestAmerica Tampa
Page 143 of 221
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Qualifier
No Equipment
N/A
1.0 mL
PQL
PQL
3.3
1.2
2.1
3.3
1.2
2.1
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Client Sample ID:
DMW-J_022509
Lab Sample ID:
Client Matrix:
660-27893-43
Water
Job Number: 660-27893-1
Date Sampled:
Date Received:
02/25/2009 1216
02/26/2009 1030
6010B Metals (ICP)-Total Recoverable
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
6010B
3005A
1.0
03/03/2009 1408
02/27/2009 1027
Analysis Batch: 660-75689
Prep Batch: 660-75517
Analyte
Result (mg/L)
Calcium
Iron
Potassium
Magnesium
Manganese
Sodium
160
13
0.70
3.6
0.0084
64
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Qualifier
I
TJA ICP TRACE
9C03A
50 mL
50 mL
MDL
PQL
0.10
0.050
0.19
0.020
0.0010
0.31
0.50
0.20
1.0
0.080
0.0040
0.50
6010B Metals (ICP)-Dissolved
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
6010B
3005A
1.0
03/03/2009 1414
02/27/2009 1027
Analysis Batch: 660-75689
Prep Batch: 660-75517
Analyte
Result (mg/L)
Iron, Dissolved
Manganese, Dissolved
12
0.0083
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Qualifier
TJA ICP TRACE
9C03A
50 mL
50 mL
MDL
PQL
0.050
0.0010
0.20
0.0040
SM 2340B Hardness, Calculation
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
SM 2340B
N/A
1.0
03/03/2009 1527
N/A
Analysis Batch: 660-75708
Analyte
Result (mg/L)
Hardness as calcium carbonate
Calcium hardness as calcium carbonate
Magnesium hardness as calcium carbonate
420
400
15
TestAmerica Tampa
Page 144 of 221
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Qualifier
No Equipment
N/A
1.0 mL
PQL
PQL
3.3
1.2
2.1
3.3
1.2
2.1
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Client Sample ID:
DMW-L_022509
Lab Sample ID:
Client Matrix:
660-27893-44
Water
Job Number: 660-27893-1
Date Sampled:
Date Received:
02/25/2009 1105
02/26/2009 1030
6010B Metals (ICP)-Total Recoverable
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
6010B
3005A
1.0
03/03/2009 1420
02/27/2009 1027
Analysis Batch: 660-75689
Prep Batch: 660-75517
Analyte
Result (mg/L)
Calcium
Iron
Potassium
Magnesium
Manganese
Sodium
78
4.2
0.35
1.9
0.0052
17
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Qualifier
I
TJA ICP TRACE
9C03A
50 mL
50 mL
MDL
PQL
0.10
0.050
0.19
0.020
0.0010
0.31
0.50
0.20
1.0
0.080
0.0040
0.50
6010B Metals (ICP)-Dissolved
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
6010B
3005A
1.0
03/03/2009 1437
02/27/2009 1027
Analysis Batch: 660-75689
Prep Batch: 660-75517
Analyte
Result (mg/L)
Iron, Dissolved
Manganese, Dissolved
4.0
0.0051
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Qualifier
TJA ICP TRACE
9C03A
50 mL
50 mL
MDL
PQL
0.050
0.0010
0.20
0.0040
SM 2340B Hardness, Calculation
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
SM 2340B
N/A
1.0
03/03/2009 1527
N/A
Analysis Batch: 660-75708
Analyte
Result (mg/L)
Hardness as calcium carbonate
Calcium hardness as calcium carbonate
Magnesium hardness as calcium carbonate
200
190
7.9
TestAmerica Tampa
Page 145 of 221
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Qualifier
No Equipment
N/A
1.0 mL
PQL
PQL
3.3
1.2
2.1
3.3
1.2
2.1
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Client Sample ID:
DMW-I_022509
Lab Sample ID:
Client Matrix:
660-27893-45
Water
Job Number: 660-27893-1
Date Sampled:
Date Received:
02/25/2009 1440
02/26/2009 1030
6010B Metals (ICP)-Total Recoverable
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
6010B
3005A
1.0
03/03/2009 1443
02/27/2009 1027
Analysis Batch: 660-75689
Prep Batch: 660-75517
Analyte
Result (mg/L)
Calcium
Iron
Potassium
Magnesium
Manganese
Sodium
93
2.5
0.50
2.8
0.0051
14
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Qualifier
I
TJA ICP TRACE
9C03A
50 mL
50 mL
MDL
PQL
0.10
0.050
0.19
0.020
0.0010
0.31
0.50
0.20
1.0
0.080
0.0040
0.50
6010B Metals (ICP)-Dissolved
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
6010B
3005A
1.0
03/03/2009 1448
02/27/2009 1027
Analysis Batch: 660-75689
Prep Batch: 660-75517
Analyte
Result (mg/L)
Iron, Dissolved
Manganese, Dissolved
2.2
0.0068
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Qualifier
TJA ICP TRACE
9C03A
50 mL
50 mL
MDL
PQL
0.050
0.0010
0.20
0.0040
SM 2340B Hardness, Calculation
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
SM 2340B
N/A
1.0
03/03/2009 1527
N/A
Analysis Batch: 660-75708
Analyte
Result (mg/L)
Hardness as calcium carbonate
Calcium hardness as calcium carbonate
Magnesium hardness as calcium carbonate
240
230
11
TestAmerica Tampa
Page 146 of 221
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Qualifier
No Equipment
N/A
1.0 mL
PQL
PQL
3.3
1.2
2.1
3.3
1.2
2.1
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Client Sample ID:
DMW-C_022609
Lab Sample ID:
Client Matrix:
660-27893-46
Water
Job Number: 660-27893-1
Date Sampled:
Date Received:
02/26/2009 0755
02/26/2009 1030
6010B Metals (ICP)-Total Recoverable
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
6010B
3005A
1.0
03/03/2009 1454
02/27/2009 1027
Analysis Batch: 660-75689
Prep Batch: 660-75517
Analyte
Result (mg/L)
Calcium
Iron
Potassium
Magnesium
Manganese
Sodium
100
3.5
0.54
2.1
0.025
13
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Qualifier
I
TJA ICP TRACE
9C03A
50 mL
50 mL
MDL
PQL
0.10
0.050
0.19
0.020
0.0010
0.31
0.50
0.20
1.0
0.080
0.0040
0.50
6010B Metals (ICP)-Dissolved
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
6010B
3005A
1.0
03/03/2009 1500
02/27/2009 1027
Analysis Batch: 660-75689
Prep Batch: 660-75517
Analyte
Result (mg/L)
Iron, Dissolved
Manganese, Dissolved
3.4
0.023
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Qualifier
TJA ICP TRACE
9C03A
50 mL
50 mL
MDL
PQL
0.050
0.0010
0.20
0.0040
SM 2340B Hardness, Calculation
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
SM 2340B
N/A
1.0
03/03/2009 1527
N/A
Analysis Batch: 660-75708
Analyte
Result (mg/L)
Hardness as calcium carbonate
Calcium hardness as calcium carbonate
Magnesium hardness as calcium carbonate
260
250
8.7
TestAmerica Tampa
Page 147 of 221
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Qualifier
No Equipment
N/A
1.0 mL
PQL
PQL
3.3
1.2
2.1
3.3
1.2
2.1
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Client Sample ID:
IDPT-9_022609
Lab Sample ID:
Client Matrix:
660-27893-47
Water
Job Number: 660-27893-1
Date Sampled:
Date Received:
02/26/2009 0745
02/26/2009 1030
6010B Metals (ICP)-Total Recoverable
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
6010B
3005A
1.0
03/03/2009 1505
02/27/2009 1027
Analysis Batch: 660-75689
Prep Batch: 660-75517
Analyte
Result (mg/L)
Calcium
Iron
Potassium
Magnesium
Manganese
Sodium
46
7.2
1.4
5.6
0.0089
19
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Qualifier
TJA ICP TRACE
9C03A
50 mL
50 mL
MDL
PQL
0.10
0.050
0.19
0.020
0.0010
0.31
0.50
0.20
1.0
0.080
0.0040
0.50
6010B Metals (ICP)-Dissolved
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
6010B
3005A
1.0
03/03/2009 1511
02/27/2009 1027
Analysis Batch: 660-75689
Prep Batch: 660-75517
Analyte
Result (mg/L)
Iron, Dissolved
Manganese, Dissolved
3.3
0.0060
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Qualifier
TJA ICP TRACE
9C03A
50 mL
50 mL
MDL
PQL
0.050
0.0010
0.20
0.0040
SM 2340B Hardness, Calculation
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
SM 2340B
N/A
1.0
03/03/2009 1527
N/A
Analysis Batch: 660-75708
Analyte
Result (mg/L)
Hardness as calcium carbonate
Calcium hardness as calcium carbonate
Magnesium hardness as calcium carbonate
140
110
23
TestAmerica Tampa
Page 148 of 221
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Qualifier
No Equipment
N/A
1.0 mL
PQL
PQL
3.3
1.2
2.1
3.3
1.2
2.1
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Client Sample ID:
IDPT-15_022609
Lab Sample ID:
Client Matrix:
660-27893-48
Water
Job Number: 660-27893-1
Date Sampled:
Date Received:
02/26/2009 0805
02/26/2009 1030
6010B Metals (ICP)-Total Recoverable
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
6010B
3005A
1.0
03/03/2009 1517
02/27/2009 1027
Analysis Batch: 660-75689
Prep Batch: 660-75517
Analyte
Result (mg/L)
Calcium
Iron
Potassium
Magnesium
Manganese
Sodium
61
9.6
1.0
2.5
0.011
27
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Qualifier
TJA ICP TRACE
9C03A
50 mL
50 mL
MDL
PQL
0.10
0.050
0.19
0.020
0.0010
0.31
0.50
0.20
1.0
0.080
0.0040
0.50
6010B Metals (ICP)-Dissolved
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
6010B
3005A
1.0
03/03/2009 1523
02/27/2009 1027
Analysis Batch: 660-75689
Prep Batch: 660-75517
Analyte
Result (mg/L)
Iron, Dissolved
Manganese, Dissolved
11
0.012
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Qualifier
TJA ICP TRACE
9C03A
50 mL
50 mL
MDL
PQL
0.050
0.0010
0.20
0.0040
SM 2340B Hardness, Calculation
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
SM 2340B
N/A
1.0
03/03/2009 1527
N/A
Analysis Batch: 660-75708
Analyte
Result (mg/L)
Hardness as calcium carbonate
Calcium hardness as calcium carbonate
Magnesium hardness as calcium carbonate
160
150
10
TestAmerica Tampa
Page 149 of 221
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Qualifier
No Equipment
N/A
1.0 mL
PQL
PQL
3.3
1.2
2.1
3.3
1.2
2.1
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Job Number: 660-27893-1
General Chemistry
TestAmerica Tampa
Page 150 of 221
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Job Number: 660-27893-1
General Chemistry
Client Sample ID:
Lab Sample ID:
Client Matrix:
IDPT-14_022509
660-27893-41
Water
Analyte
Total Dissolved Solids
Date Sampled:
Date Received:
Result
580
Anly Batch: 640-54348
Units
mg/L
Date Analyzed
MDL
10
02/27/2009 1212
PQL
10
Dil
1.0
Method
SM 2540C
Total Suspended Solids
65
Anly Batch: 640-54352
mg/L
Date Analyzed
2.4
02/27/2009 1228
5.0
1.0
SM 2540D
Bromide
0.54
Anly Batch: 660-75752
mg/L
Date Analyzed
0.027
03/02/2009 1809
0.050
1.0
300.0
Sulfate
36
Anly Batch: 660-75752
J3
mg/L
Date Analyzed
0.20
03/04/2009 1425
0.50
1.0
300.0
Chloride
170
Anly Batch: 660-75752
J3
mg/L
Date Analyzed
0.40
03/04/2009 1437
1.0
2.0
300.0
Nitrite as N
0.10
Anly Batch: 660-75441
U
mg/L
Date Analyzed
0.10
02/26/2009 1531
0.50
1.0
353.2
Nitrate Nitrite as N
0.10
Anly Batch: 660-75644
1.0
353.2
0.10
Anly Batch: 660-75441
0.10
03/02/2009 1303
03/02/2009 1303
0.10
02/26/2009 1531
0.50
Nitrate as N
U
mg/L
Date Analyzed
Date Prepared:
U
mg/L
Date Analyzed
0.50
1.0
353.2
Chemical Oxygen Demand
23
Anly Batch: 660-75563
Prep Batch: 660-75561
Total Organic Carbon
8.7
Anly Batch: 660-75675
mg/L
Date Analyzed
Date Prepared:
mg/L
Date Analyzed
10
02/27/2009 1500
02/27/2009 1220
1.1
03/02/2009 2023
20
1.0
SM 5220D
2.0
2.0
SM 5310C
TestAmerica Tampa
Qual
02/25/2009 1317
02/26/2009 1030
Page 151 of 221
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Job Number: 660-27893-1
General Chemistry
Client Sample ID:
Lab Sample ID:
Client Matrix:
IDPT-14_022509
660-27893-41
Water
Analyte
Alkalinity
Date Sampled:
Date Received:
Result
150
Anly Batch: 660-75553
Units
mg/L
Date Analyzed
PQL
1.0
02/27/2009 1232
PQL
1.0
Dil
1.0
Method
SM 2320B
Bicarbonate Alkalinity as CaCO3
150
Anly Batch: 660-75553
mg/L
Date Analyzed
1.0
02/27/2009 1232
1.0
1.0
SM 2320B
Carbonate Alkalinity as CaCO3
1.0
Anly Batch: 660-75553
U
mg/L
Date Analyzed
1.0
02/27/2009 1232
1.0
1.0
SM 2320B
Hydroxide Alkalinity
1.0
Anly Batch: 660-75553
U
mg/L
Date Analyzed
1.0
02/27/2009 1232
1.0
1.0
SM 2320B
Phenolphthalein Alkalinity
1.0
Anly Batch: 660-75553
U
mg/L
Date Analyzed
1.0
02/27/2009 1232
1.0
1.0
SM 2320B
TestAmerica Tampa
Qual
02/25/2009 1317
02/26/2009 1030
Page 152 of 221
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Job Number: 660-27893-1
General Chemistry
Client Sample ID:
Lab Sample ID:
Client Matrix:
DMW-F_022509
660-27893-42
Water
Analyte
Total Dissolved Solids
Date Sampled:
Date Received:
Result
360
Anly Batch: 640-54348
Units
mg/L
Date Analyzed
MDL
10
02/27/2009 1212
PQL
10
Dil
1.0
Method
SM 2540C
Total Suspended Solids
12
Anly Batch: 640-54352
mg/L
Date Analyzed
0.49
02/27/2009 1228
1.0
1.0
SM 2540D
Bromide
0.13
Anly Batch: 660-75752
mg/L
Date Analyzed
0.027
03/02/2009 1926
0.050
1.0
300.0
Chloride
40
Anly Batch: 660-75752
mg/L
Date Analyzed
0.20
03/04/2009 1515
0.50
1.0
300.0
Sulfate
19
Anly Batch: 660-75752
mg/L
Date Analyzed
0.20
03/04/2009 1515
0.50
1.0
300.0
Nitrite as N
0.10
Anly Batch: 660-75441
U
mg/L
Date Analyzed
0.10
02/26/2009 1531
0.50
1.0
353.2
Nitrate Nitrite as N
0.10
Anly Batch: 660-75644
1.0
353.2
0.10
Anly Batch: 660-75441
0.10
03/02/2009 1303
03/02/2009 1303
0.10
02/26/2009 1531
0.50
Nitrate as N
U
mg/L
Date Analyzed
Date Prepared:
U
mg/L
Date Analyzed
0.50
1.0
353.2
Chemical Oxygen Demand
14
Anly Batch: 660-75563
Prep Batch: 660-75561
Total Organic Carbon
5.8
Anly Batch: 660-75675
I
mg/L
Date Analyzed
Date Prepared:
mg/L
Date Analyzed
10
02/27/2009 1500
02/27/2009 1220
0.53
03/02/2009 2046
20
1.0
SM 5220D
1.0
1.0
SM 5310C
TestAmerica Tampa
Qual
02/25/2009 0828
02/26/2009 1030
Page 153 of 221
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Job Number: 660-27893-1
General Chemistry
Client Sample ID:
Lab Sample ID:
Client Matrix:
DMW-F_022509
660-27893-42
Water
Analyte
Alkalinity
Date Sampled:
Date Received:
Result
230
Anly Batch: 660-75553
Units
mg/L
Date Analyzed
PQL
1.0
02/27/2009 1239
PQL
1.0
Dil
1.0
Method
SM 2320B
Bicarbonate Alkalinity as CaCO3
230
Anly Batch: 660-75553
mg/L
Date Analyzed
1.0
02/27/2009 1239
1.0
1.0
SM 2320B
Carbonate Alkalinity as CaCO3
1.0
Anly Batch: 660-75553
U
mg/L
Date Analyzed
1.0
02/27/2009 1239
1.0
1.0
SM 2320B
Hydroxide Alkalinity
1.0
Anly Batch: 660-75553
U
mg/L
Date Analyzed
1.0
02/27/2009 1239
1.0
1.0
SM 2320B
Phenolphthalein Alkalinity
1.0
Anly Batch: 660-75553
U
mg/L
Date Analyzed
1.0
02/27/2009 1239
1.0
1.0
SM 2320B
TestAmerica Tampa
Qual
02/25/2009 0828
02/26/2009 1030
Page 154 of 221
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Job Number: 660-27893-1
General Chemistry
Client Sample ID:
Lab Sample ID:
Client Matrix:
DMW-J_022509
660-27893-43
Water
Analyte
Total Dissolved Solids
Date Sampled:
Date Received:
Result
780
Anly Batch: 640-54348
Units
mg/L
Date Analyzed
MDL
10
02/27/2009 1212
PQL
10
Dil
1.0
Method
SM 2540C
Total Suspended Solids
27
Anly Batch: 640-54352
mg/L
Date Analyzed
0.53
02/27/2009 1228
1.1
1.0
SM 2540D
Bromide
0.47
Anly Batch: 660-75752
mg/L
Date Analyzed
0.027
03/02/2009 1952
0.050
1.0
300.0
Sulfate
54
Anly Batch: 660-75752
mg/L
Date Analyzed
0.20
03/04/2009 1527
0.50
1.0
300.0
Chloride
270
Anly Batch: 660-75752
mg/L
Date Analyzed
0.80
03/04/2009 1540
2.0
4.0
300.0
Nitrite as N
0.10
Anly Batch: 660-75441
U
mg/L
Date Analyzed
0.10
02/26/2009 1531
0.50
1.0
353.2
Nitrate Nitrite as N
0.10
Anly Batch: 660-75644
1.0
353.2
0.10
Anly Batch: 660-75441
0.10
03/02/2009 1303
03/02/2009 1303
0.10
02/26/2009 1531
0.50
Nitrate as N
U
mg/L
Date Analyzed
Date Prepared:
U
mg/L
Date Analyzed
0.50
1.0
353.2
Chemical Oxygen Demand
14
Anly Batch: 660-75563
Prep Batch: 660-75561
Total Organic Carbon
5.5
Anly Batch: 660-75675
I
mg/L
Date Analyzed
Date Prepared:
mg/L
Date Analyzed
10
02/27/2009 1500
02/27/2009 1220
0.53
03/02/2009 2113
20
1.0
SM 5220D
1.0
1.0
SM 5310C
TestAmerica Tampa
Qual
02/25/2009 1216
02/26/2009 1030
Page 155 of 221
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Job Number: 660-27893-1
General Chemistry
Client Sample ID:
Lab Sample ID:
Client Matrix:
DMW-J_022509
660-27893-43
Water
Analyte
Alkalinity
Date Sampled:
Date Received:
Result
180
Anly Batch: 660-75553
Units
mg/L
Date Analyzed
PQL
1.0
02/27/2009 1245
PQL
1.0
Dil
1.0
Method
SM 2320B
Bicarbonate Alkalinity as CaCO3
180
Anly Batch: 660-75553
mg/L
Date Analyzed
1.0
02/27/2009 1245
1.0
1.0
SM 2320B
Carbonate Alkalinity as CaCO3
1.0
Anly Batch: 660-75553
U
mg/L
Date Analyzed
1.0
02/27/2009 1245
1.0
1.0
SM 2320B
Hydroxide Alkalinity
1.0
Anly Batch: 660-75553
U
mg/L
Date Analyzed
1.0
02/27/2009 1245
1.0
1.0
SM 2320B
Phenolphthalein Alkalinity
1.0
Anly Batch: 660-75553
U
mg/L
Date Analyzed
1.0
02/27/2009 1245
1.0
1.0
SM 2320B
TestAmerica Tampa
Qual
02/25/2009 1216
02/26/2009 1030
Page 156 of 221
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Job Number: 660-27893-1
General Chemistry
Client Sample ID:
Lab Sample ID:
Client Matrix:
DMW-L_022509
660-27893-44
Water
Analyte
Total Dissolved Solids
Date Sampled:
Date Received:
Result
270
Anly Batch: 640-54348
Units
mg/L
Date Analyzed
MDL
5.0
02/27/2009 1212
PQL
5.0
Dil
1.0
Method
SM 2540C
Total Suspended Solids
26
Anly Batch: 640-54352
mg/L
Date Analyzed
0.80
02/27/2009 1228
1.7
1.0
SM 2540D
Bromide
0.027
Anly Batch: 660-75752
U
mg/L
Date Analyzed
0.027
03/02/2009 2018
0.050
1.0
300.0
Chloride
35
Anly Batch: 660-75752
mg/L
Date Analyzed
0.20
03/04/2009 1552
0.50
1.0
300.0
Sulfate
8.6
Anly Batch: 660-75752
mg/L
Date Analyzed
0.20
03/04/2009 1552
0.50
1.0
300.0
Nitrite as N
0.10
Anly Batch: 660-75441
U
mg/L
Date Analyzed
0.10
02/26/2009 1531
0.50
1.0
353.2
Nitrate Nitrite as N
0.10
Anly Batch: 660-75644
1.0
353.2
0.10
Anly Batch: 660-75441
0.10
03/02/2009 1303
03/02/2009 1303
0.10
02/26/2009 1531
0.50
Nitrate as N
U
mg/L
Date Analyzed
Date Prepared:
U
mg/L
Date Analyzed
0.50
1.0
353.2
Chemical Oxygen Demand
10
Anly Batch: 660-75563
Prep Batch: 660-75561
Total Organic Carbon
3.0
Anly Batch: 660-75675
U
mg/L
Date Analyzed
Date Prepared:
mg/L
Date Analyzed
10
02/27/2009 1500
02/27/2009 1220
0.53
03/02/2009 2231
20
1.0
SM 5220D
1.0
1.0
SM 5310C
TestAmerica Tampa
Qual
02/25/2009 1105
02/26/2009 1030
Page 157 of 221
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Job Number: 660-27893-1
General Chemistry
Client Sample ID:
Lab Sample ID:
Client Matrix:
DMW-L_022509
660-27893-44
Water
Analyte
Alkalinity
Date Sampled:
Date Received:
Result
200
Anly Batch: 660-75553
Units
mg/L
Date Analyzed
PQL
1.0
02/27/2009 1303
PQL
1.0
Dil
1.0
Method
SM 2320B
Bicarbonate Alkalinity as CaCO3
200
Anly Batch: 660-75553
mg/L
Date Analyzed
1.0
02/27/2009 1303
1.0
1.0
SM 2320B
Carbonate Alkalinity as CaCO3
1.0
Anly Batch: 660-75553
U
mg/L
Date Analyzed
1.0
02/27/2009 1303
1.0
1.0
SM 2320B
Hydroxide Alkalinity
1.0
Anly Batch: 660-75553
U
mg/L
Date Analyzed
1.0
02/27/2009 1303
1.0
1.0
SM 2320B
Phenolphthalein Alkalinity
1.0
Anly Batch: 660-75553
U
mg/L
Date Analyzed
1.0
02/27/2009 1303
1.0
1.0
SM 2320B
TestAmerica Tampa
Qual
02/25/2009 1105
02/26/2009 1030
Page 158 of 221
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Job Number: 660-27893-1
General Chemistry
Client Sample ID:
Lab Sample ID:
Client Matrix:
DMW-I_022509
660-27893-45
Water
Analyte
Total Dissolved Solids
Date Sampled:
Date Received:
Result
340
Anly Batch: 640-54348
Units
mg/L
Date Analyzed
MDL
10
02/27/2009 1212
PQL
10
Dil
1.0
Method
SM 2540C
Total Suspended Solids
32
Anly Batch: 640-54352
mg/L
Date Analyzed
0.80
02/27/2009 1228
1.7
1.0
SM 2540D
Bromide
0.22
Anly Batch: 660-75752
mg/L
Date Analyzed
0.027
03/02/2009 2044
0.050
1.0
300.0
Chloride
75
Anly Batch: 660-75752
mg/L
Date Analyzed
0.20
03/04/2009 1605
0.50
1.0
300.0
Sulfate
2.0
Anly Batch: 660-75752
mg/L
Date Analyzed
0.20
03/04/2009 1605
0.50
1.0
300.0
Nitrite as N
0.10
Anly Batch: 660-75441
U
mg/L
Date Analyzed
0.10
02/26/2009 1531
0.50
1.0
353.2
Nitrate Nitrite as N
0.10
Anly Batch: 660-75644
1.0
353.2
0.10
Anly Batch: 660-75441
0.10
03/02/2009 1303
03/02/2009 1303
0.10
02/26/2009 1531
0.50
Nitrate as N
U
mg/L
Date Analyzed
Date Prepared:
U
mg/L
Date Analyzed
0.50
1.0
353.2
Chemical Oxygen Demand
26
Anly Batch: 660-75563
Prep Batch: 660-75561
Total Organic Carbon
8.7
Anly Batch: 660-75675
mg/L
Date Analyzed
Date Prepared:
mg/L
Date Analyzed
10
02/27/2009 1500
02/27/2009 1220
0.53
03/02/2009 2255
20
1.0
SM 5220D
1.0
1.0
SM 5310C
TestAmerica Tampa
Qual
02/25/2009 1440
02/26/2009 1030
Page 159 of 221
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Job Number: 660-27893-1
General Chemistry
Client Sample ID:
Lab Sample ID:
Client Matrix:
DMW-I_022509
660-27893-45
Water
Analyte
Alkalinity
Date Sampled:
Date Received:
Result
180
Anly Batch: 660-75553
Units
mg/L
Date Analyzed
PQL
1.0
02/27/2009 1309
PQL
1.0
Dil
1.0
Method
SM 2320B
Bicarbonate Alkalinity as CaCO3
180
Anly Batch: 660-75553
mg/L
Date Analyzed
1.0
02/27/2009 1309
1.0
1.0
SM 2320B
Carbonate Alkalinity as CaCO3
1.0
Anly Batch: 660-75553
U
mg/L
Date Analyzed
1.0
02/27/2009 1309
1.0
1.0
SM 2320B
Hydroxide Alkalinity
1.0
Anly Batch: 660-75553
U
mg/L
Date Analyzed
1.0
02/27/2009 1309
1.0
1.0
SM 2320B
Phenolphthalein Alkalinity
1.0
Anly Batch: 660-75553
U
mg/L
Date Analyzed
1.0
02/27/2009 1309
1.0
1.0
SM 2320B
TestAmerica Tampa
Qual
02/25/2009 1440
02/26/2009 1030
Page 160 of 221
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Job Number: 660-27893-1
General Chemistry
Client Sample ID:
Lab Sample ID:
Client Matrix:
DMW-C_022609
660-27893-46
Water
Analyte
Total Dissolved Solids
Date Sampled:
Date Received:
Result
320
Anly Batch: 640-54348
Units
mg/L
Date Analyzed
MDL
10
02/27/2009 1212
PQL
10
Dil
1.0
Method
SM 2540C
Total Suspended Solids
3.9
Anly Batch: 640-54352
mg/L
Date Analyzed
0.48
02/27/2009 1228
1.0
1.0
SM 2540D
Bromide
0.027
Anly Batch: 660-75752
U
mg/L
Date Analyzed
0.027
03/02/2009 2110
0.050
1.0
300.0
Chloride
41
Anly Batch: 660-75752
mg/L
Date Analyzed
0.20
03/04/2009 1617
0.50
1.0
300.0
Sulfate
71
Anly Batch: 660-75752
mg/L
Date Analyzed
0.20
03/04/2009 1617
0.50
1.0
300.0
Nitrite as N
0.10
Anly Batch: 660-75441
U
mg/L
Date Analyzed
0.10
02/26/2009 1531
0.50
1.0
353.2
Nitrate Nitrite as N
0.10
Anly Batch: 660-75644
1.0
353.2
0.10
Anly Batch: 660-75441
0.10
03/02/2009 1303
03/02/2009 1303
0.10
02/26/2009 1531
0.50
Nitrate as N
U
mg/L
Date Analyzed
Date Prepared:
U
mg/L
Date Analyzed
0.50
1.0
353.2
Chemical Oxygen Demand
10
Anly Batch: 660-75563
Prep Batch: 660-75561
Total Organic Carbon
6.8
Anly Batch: 660-75675
U
mg/L
Date Analyzed
Date Prepared:
mg/L
Date Analyzed
10
02/27/2009 1500
02/27/2009 1220
0.53
03/02/2009 2318
20
1.0
SM 5220D
1.0
1.0
SM 5310C
TestAmerica Tampa
Qual
02/26/2009 0755
02/26/2009 1030
Page 161 of 221
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Job Number: 660-27893-1
General Chemistry
Client Sample ID:
Lab Sample ID:
Client Matrix:
DMW-C_022609
660-27893-46
Water
Analyte
Alkalinity
Date Sampled:
Date Received:
Result
130
Anly Batch: 660-75553
Units
mg/L
Date Analyzed
PQL
1.0
02/27/2009 1316
PQL
1.0
Dil
1.0
Method
SM 2320B
Bicarbonate Alkalinity as CaCO3
130
Anly Batch: 660-75553
mg/L
Date Analyzed
1.0
02/27/2009 1316
1.0
1.0
SM 2320B
Carbonate Alkalinity as CaCO3
1.0
Anly Batch: 660-75553
U
mg/L
Date Analyzed
1.0
02/27/2009 1316
1.0
1.0
SM 2320B
Hydroxide Alkalinity
1.0
Anly Batch: 660-75553
U
mg/L
Date Analyzed
1.0
02/27/2009 1316
1.0
1.0
SM 2320B
Phenolphthalein Alkalinity
1.0
Anly Batch: 660-75553
U
mg/L
Date Analyzed
1.0
02/27/2009 1316
1.0
1.0
SM 2320B
TestAmerica Tampa
Qual
02/26/2009 0755
02/26/2009 1030
Page 162 of 221
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Job Number: 660-27893-1
General Chemistry
Client Sample ID:
Lab Sample ID:
Client Matrix:
IDPT-9_022609
660-27893-47
Water
Analyte
Total Dissolved Solids
Date Sampled:
Date Received:
Result
380
Anly Batch: 640-54348
Units
mg/L
Date Analyzed
MDL
5.0
02/27/2009 1212
PQL
5.0
Dil
1.0
Method
SM 2540C
Total Suspended Solids
500
Anly Batch: 640-54352
mg/L
Date Analyzed
9.6
02/27/2009 1228
20
1.0
SM 2540D
Bromide
0.29
Anly Batch: 660-75752
mg/L
Date Analyzed
0.027
03/02/2009 2227
0.050
1.0
300.0
Chloride
83
Anly Batch: 660-75752
mg/L
Date Analyzed
0.20
03/04/2009 1655
0.50
1.0
300.0
Sulfate
8.5
Anly Batch: 660-75752
mg/L
Date Analyzed
0.20
03/04/2009 1655
0.50
1.0
300.0
Nitrite as N
1.4
Anly Batch: 660-75441
mg/L
Date Analyzed
0.10
02/26/2009 1531
0.50
1.0
353.2
Nitrate Nitrite as N
0.10
Anly Batch: 660-75644
1.0
353.2
0.10
Anly Batch: 660-75441
0.10
03/02/2009 1303
03/02/2009 1303
0.10
02/26/2009 1531
0.50
Nitrate as N
U
mg/L
Date Analyzed
Date Prepared:
U
mg/L
Date Analyzed
0.50
1.0
353.2
Chemical Oxygen Demand
45
Anly Batch: 660-75563
Prep Batch: 660-75561
Total Organic Carbon
5.8
Anly Batch: 660-75675
mg/L
Date Analyzed
Date Prepared:
mg/L
Date Analyzed
10
02/27/2009 1500
02/27/2009 1220
2.1
03/02/2009 2338
20
1.0
SM 5220D
4.0
4.0
SM 5310C
TestAmerica Tampa
Qual
02/26/2009 0745
02/26/2009 1030
Page 163 of 221
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Job Number: 660-27893-1
General Chemistry
Client Sample ID:
Lab Sample ID:
Client Matrix:
IDPT-9_022609
660-27893-47
Water
Analyte
Alkalinity
Date Sampled:
Date Received:
Result
61
Anly Batch: 660-75622
Units
mg/L
Date Analyzed
PQL
1.0
03/02/2009 0920
PQL
1.0
Dil
1.0
Method
SM 2320B
Bicarbonate Alkalinity as CaCO3
61
Anly Batch: 660-75622
mg/L
Date Analyzed
1.0
03/02/2009 0920
1.0
1.0
SM 2320B
Carbonate Alkalinity as CaCO3
1.0
Anly Batch: 660-75622
U
mg/L
Date Analyzed
1.0
03/02/2009 0920
1.0
1.0
SM 2320B
Hydroxide Alkalinity
1.0
Anly Batch: 660-75622
U
mg/L
Date Analyzed
1.0
03/02/2009 0920
1.0
1.0
SM 2320B
Phenolphthalein Alkalinity
1.0
Anly Batch: 660-75622
U
mg/L
Date Analyzed
1.0
03/02/2009 0920
1.0
1.0
SM 2320B
TestAmerica Tampa
Qual
02/26/2009 0745
02/26/2009 1030
Page 164 of 221
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Job Number: 660-27893-1
General Chemistry
Client Sample ID:
Lab Sample ID:
Client Matrix:
IDPT-15_022609
660-27893-48
Water
Analyte
Total Dissolved Solids
Date Sampled:
Date Received:
Result
410
Anly Batch: 640-54348
Units
mg/L
Date Analyzed
MDL
10
02/27/2009 1212
PQL
10
Dil
1.0
Method
SM 2540C
Total Suspended Solids
22
Anly Batch: 640-54352
mg/L
Date Analyzed
0.80
02/27/2009 1228
1.7
1.0
SM 2540D
Bromide
0.52
Anly Batch: 660-75752
mg/L
Date Analyzed
0.027
03/02/2009 2253
0.050
1.0
300.0
Sulfate
6.1
Anly Batch: 660-75752
mg/L
Date Analyzed
0.20
03/04/2009 1707
0.50
1.0
300.0
Chloride
170
Anly Batch: 660-75752
mg/L
Date Analyzed
0.80
03/05/2009 0926
2.0
4.0
300.0
Nitrite as N
0.10
Anly Batch: 660-75441
U
mg/L
Date Analyzed
0.10
02/26/2009 1531
0.50
1.0
353.2
Nitrate Nitrite as N
0.10
Anly Batch: 660-75644
1.0
353.2
0.10
Anly Batch: 660-75441
0.10
03/02/2009 1303
03/02/2009 1303
0.10
02/26/2009 1531
0.50
Nitrate as N
U J3 mg/L
Date Analyzed
Date Prepared:
U
mg/L
Date Analyzed
0.50
1.0
353.2
Chemical Oxygen Demand
11
Anly Batch: 660-75563
Prep Batch: 660-75561
Total Organic Carbon
5.2
Anly Batch: 660-75675
I
mg/L
Date Analyzed
Date Prepared:
mg/L
Date Analyzed
10
02/27/2009 1500
02/27/2009 1220
0.53
03/03/2009 0006
20
1.0
SM 5220D
1.0
1.0
SM 5310C
TestAmerica Tampa
Qual
02/26/2009 0805
02/26/2009 1030
Page 165 of 221
04/06/2009
Analytical Data
Client: ARCADIS U.S., Inc.
Job Number: 660-27893-1
General Chemistry
Client Sample ID:
Lab Sample ID:
Client Matrix:
IDPT-15_022609
660-27893-48
Water
Analyte
Alkalinity
Date Sampled:
Date Received:
Result
37
Anly Batch: 660-75622
Units
mg/L
Date Analyzed
PQL
1.0
03/02/2009 0929
PQL
1.0
Dil
1.0
Method
SM 2320B
Bicarbonate Alkalinity as CaCO3
37
Anly Batch: 660-75622
mg/L
Date Analyzed
1.0
03/02/2009 0929
1.0
1.0
SM 2320B
Carbonate Alkalinity as CaCO3
1.0
Anly Batch: 660-75622
U
mg/L
Date Analyzed
1.0
03/02/2009 0929
1.0
1.0
SM 2320B
Hydroxide Alkalinity
1.0
Anly Batch: 660-75622
U
mg/L
Date Analyzed
1.0
03/02/2009 0929
1.0
1.0
SM 2320B
Phenolphthalein Alkalinity
1.0
Anly Batch: 660-75622
U
mg/L
Date Analyzed
1.0
03/02/2009 0929
1.0
1.0
SM 2320B
TestAmerica Tampa
Qual
02/26/2009 0805
02/26/2009 1030
Page 166 of 221
04/06/2009
DATA REPORTING QUALIFIERS
Client: ARCADIS U.S., Inc.
Lab Section
Job Number: 660-27893-1
Qualifier
Description
U
Indicates that the compound was analyzed for but not
detected.
I
The reported value is between the laboratory method
detection limit and the laboratory practical quantitation limit.
J3
Estimated value; value may not be accurate. Spike recovery
or RPD outside of criteria.
U
Indicates that the compound was analyzed for but not
detected.
I
The reported value is between the laboratory method
detection limit and the laboratory practical quantitation limit.
J3
Estimated value; value may not be accurate. Spike recovery
or RPD outside of criteria.
U
Indicates that the compound was analyzed for but not
detected.
I
The reported value is between the laboratory method
detection limit and the laboratory practical quantitation limit.
GC/MS VOA
Metals
General Chemistry
TestAmerica Tampa
Page 167 of 221
04/06/2009
QUALITY CONTROL RESULTS
TestAmerica Tampa
Page 168 of 221
04/06/2009
Quality Control Results
Client: ARCADIS U.S., Inc.
Job Number: 660-27893-1
Surrogate Recovery Report
8260B Volatile Organic Compounds (GC/MS)
Client Matrix: Water
Lab Sample ID
Client Sample ID
TOL
%Rec
BFB
%Rec
660-27893-1
DMW-P_022509
101
78
98
660-27893-2
DMW-O_022509
98
77
101
660-27893-3
DMW-Q_022509
116
82
100
660-27893-4
DMW-C_022509
105
89
106
660-27893-5
IMW-D_022509
101
84
95
660-27893-6
DMW-B_022509
105
81
101
660-27893-7
IDPT-15_022509
107
86
103
660-27893-8
DMW-8_022509
104
88
101
660-27893-9
SMW-D_022509
101
79
105
660-27893-10
IDPT-8_022509
92
82
107
660-27893-11
IDPT-9_022509
101
86
108
660-27893-12
SMW-E_022509
99
87
108
660-27893-13
SMW-H_022509
95
86
107
660-27893-14
DMW-N_022509
94
84
110
660-27893-15
DUPE E_022509
103
90
106
660-27893-16
SMW-I_022509
103
87
106
660-27893-17
DMW-I_022509
118
84
107
660-27893-18
SMW-N_022509
103
84
108
660-27893-19
IDPT-12_022509
98
90
109
660-27893-20
IMW-J_022509
101
91
110
660-27893-21
DMW-A_022509
99
100
99
660-27893-22
DMW-W_022509
102
105
98
660-27893-23
H-1_022509
101
100
98
660-27893-24
SMW-A_022509
102
105
101
660-27893-25
Trip Blank 3_022509
101
101
97
660-27893-26
IDPT-1_022509
100
101
100
660-27893-27
IDPT-2_022509
100
102
102
660-27893-28
IDPT-5_022509
100
99
100
660-27893-29
IDPT-6_022509
101
102
104
Surrogate
TOL = Toluene-d8 (Surr)
BFB = 4-Bromofluorobenzene
DBFM = Dibromofluoromethane
DBFM
%Rec
Acceptance Limits
77-122
74-126
70-130
TestAmerica Tampa
Page 169 of 221
04/06/2009
Quality Control Results
Client: ARCADIS U.S., Inc.
Job Number: 660-27893-1
Surrogate Recovery Report
8260B Volatile Organic Compounds (GC/MS)
Client Matrix: Water
Lab Sample ID
660-27893-30
Client Sample ID
IDPT-10_022509
TOL
%Rec
103
BFB
%Rec
104
DBFM
%Rec
102
660-27893-31
IDPT-13_022509
101
103
101
660-27893-32
IDPT-14_022509
101
102
101
660-27893-33
IMW-F_022509
101
104
102
660-27893-34
DMW-F_022509
103
101
104
660-27893-35
DMW-J_022509
99
101
98
660-27893-36
DMW-K_022509
101
102
98
660-27893-37
DMW-L_022509
103
104
100
660-27893-38
DUPE D_022509
100
101
100
660-27893-39
DUPE H_022509
102
102
101
660-27893-40
Trip Blank_022509
102
106
98
MB 660-75524/2
93
87
102
MB 660-75614/2
94
83
107
MB 660-75683/2
114
87
107
MB 660-75698/2
98
101
95
MB 660-75699/2
99
102
96
MB 660-75700/2
102
106
100
LCS 660-75524/1
91
85
99
LCS 660-75614/1
92
85
108
LCS 660-75683/1
92
88
106
LCS 660-75698/1
100
100
96
LCS 660-75699/1
99
100
95
102
105
102
88
85
105
LCS 660-75700/1
660-27893-14 MS
DMW-N_022509 MS
660-27893-21 MS
DMW-A_022509 MS
98
100
97
660-27893-22 MS
DMW-W_022509 MS
101
103
100
660-27893-26 MS
IDPT-1_022509 MS
100
100
98
660-27890-C-3 MS
92
81
98
660-27916-D-15 MS
94
89
104
Surrogate
TOL = Toluene-d8 (Surr)
BFB = 4-Bromofluorobenzene
DBFM = Dibromofluoromethane
Acceptance Limits
77-122
74-126
70-130
TestAmerica Tampa
Page 170 of 221
04/06/2009
Quality Control Results
Client: ARCADIS U.S., Inc.
Job Number: 660-27893-1
Surrogate Recovery Report
8260B Volatile Organic Compounds (GC/MS)
Client Matrix: Water
Lab Sample ID
660-27893-14 MSD
660-27893-21 MSD
660-27893-22 MSD
660-27893-26 MSD
Client Sample ID
DMW-N_022509
MSD
DMW-A_022509 MSD
DMW-W_022509
MSD
IDPT-1_022509 MSD
TOL
%Rec
90
BFB
%Rec
82
DBFM
%Rec
104
98
103
96
102
104
101
100
101
100
660-27890-D-3 MSD
94
82
99
660-27916-B-13 DU
86
83
106
Surrogate
TOL = Toluene-d8 (Surr)
BFB = 4-Bromofluorobenzene
DBFM = Dibromofluoromethane
Acceptance Limits
77-122
74-126
70-130
TestAmerica Tampa
Page 171 of 221
04/06/2009
Quality Control Results
Client: ARCADIS U.S., Inc.
Job Number: 660-27893-1
Method Blank - Batch: 660-75524
Lab Sample ID:
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
MB 660-75524/2
Water
1.0
02/27/2009 1200
02/27/2009 1200
Method: 8260B
Preparation: 5030B
Analysis Batch: 660-75524
Prep Batch: N/A
Units: ug/L
Instrument ID: BVMH GC/MS
Lab File ID:
1HB2713.D
Initial Weight/Volume: 5 mL
Final Weight/Volume: 5 mL
Analyte
Result
Qual
MDL
PQL
Benzene
Bromobenzene
Chlorobromomethane
Dichlorobromomethane
Bromoform
Bromomethane
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
Chlorodibromomethane
1,2-Dibromo-3-Chloropropane
Ethylene Dibromide
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
Hexachlorobutadiene
Isopropylbenzene
4-Isopropyltoluene
Methylene Chloride
Naphthalene
0.50
0.58
0.58
0.35
0.58
2.5
0.67
0.63
0.84
0.42
0.63
2.5
0.90
1.0
0.65
0.52
0.34
2.5
0.50
0.41
0.44
0.64
0.52
2.5
0.52
0.57
0.45
0.65
0.44
0.52
0.39
0.36
0.31
0.14
0.14
0.44
0.40
0.19
0.69
4.0
2.5
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
0.50
0.58
0.58
0.35
0.58
2.5
0.67
0.63
0.84
0.42
0.63
2.5
0.90
1.0
0.65
0.52
0.34
2.5
0.50
0.41
0.44
0.64
0.52
2.5
0.52
0.57
0.45
0.65
0.44
0.52
0.39
0.36
0.31
0.14
0.14
0.44
0.40
0.19
0.69
4.0
2.5
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
4.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
5.0
Calculations are performed before rounding to avoid round-off errors in calculated results.
TestAmerica Tampa
Page 172 of 221
04/06/2009
Quality Control Results
Client: ARCADIS U.S., Inc.
Job Number: 660-27893-1
Method Blank - Batch: 660-75524
Lab Sample ID:
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
MB 660-75524/2
Water
1.0
02/27/2009 1200
02/27/2009 1200
Method: 8260B
Preparation: 5030B
Analysis Batch: 660-75524
Prep Batch: N/A
Units: ug/L
Instrument ID: BVMH GC/MS
Lab File ID:
1HB2713.D
Initial Weight/Volume: 5 mL
Final Weight/Volume: 5 mL
Analyte
Result
Qual
MDL
PQL
N-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
o-Xylene
Acetone
2-Butanone (MEK)
4-Methyl-2-pentanone (MIBK)
Carbon disulfide
2-Hexanone
Methyl tert-butyl ether
m-Xylene & p-Xylene
0.59
0.98
0.63
0.15
0.50
0.51
0.77
0.58
0.46
0.47
0.50
2.5
0.18
0.86
0.54
0.50
0.50
9.9
8.4
3.8
0.85
4.4
0.44
0.60
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
0.59
0.98
0.63
0.15
0.50
0.51
0.77
0.58
0.46
0.47
0.50
2.5
0.18
0.86
0.54
0.50
0.50
9.9
8.4
3.8
0.85
4.4
0.44
0.60
1.0
2.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
20
10
10
1.0
10
1.0
2.0
Surrogate
Toluene-d8 (Surr)
4-Bromofluorobenzene
Dibromofluoromethane
% Rec
Acceptance Limits
93
87
102
77 - 122
74 - 126
70 - 130
Calculations are performed before rounding to avoid round-off errors in calculated results.
TestAmerica Tampa
Page 173 of 221
04/06/2009
Quality Control Results
Client: ARCADIS U.S., Inc.
Job Number: 660-27893-1
Lab Control Spike - Batch: 660-75524
Lab Sample ID:
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
LCS 660-75524/1
Water
1.0
02/27/2009 1052
02/27/2009 1052
Method: 8260B
Preparation: 5030B
Analysis Batch: 660-75524
Prep Batch: N/A
Units: ug/L
Instrument ID: BVMH GC/MS
Lab File ID:
1HB2709.D
Initial Weight/Volume: 5 mL
Final Weight/Volume: 5 mL
Analyte
Spike Amount
Result
% Rec.
Limit
Qual
Benzene
Chlorobenzene
1,1-Dichloroethene
Toluene
Trichloroethene
50.0
50.0
50.0
50.0
50.0
52.0
46.8
68.8
47.5
51.7
104
94
138
95
103
62 - 135
72 - 127
46 - 147
68 - 131
56 - 143
Matrix Spike/
Matrix Spike Duplicate Recovery Report - Batch: 660-75524
Method: 8260B
Preparation: 5030B
MS Lab Sample ID:
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
660-27890-C-3 MS
Water
1.0
02/27/2009 1525
02/27/2009 1525
Analysis Batch: 660-75524
Prep Batch: N/A
Instrument ID: BVMH GC/MS
Lab File ID:
1HB2725.D
Initial Weight/Volume: 5 mL
Final Weight/Volume: 5 mL
MSD Lab Sample ID:
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
660-27890-D-3 MSD
Water
1.0
02/27/2009 1542
02/27/2009 1542
Analysis Batch: 660-75524
Prep Batch: N/A
Instrument ID: BVMH GC/MS
Lab File ID:
1HB2726.D
Initial Weight/Volume: 5 mL
Final Weight/Volume: 5 mL
Analyte
MS
Benzene
Chlorobenzene
1,1-Dichloroethene
Toluene
Trichloroethene
107
103
100
96
103
% Rec.
MSD
99
96
86
92
96
Limit
RPD
RPD Limit
62 - 135
72 - 127
46 - 147
68 - 131
56 - 143
8
7
15
4
8
37
22
30
33
35
MS Qual MSD Qual
Calculations are performed before rounding to avoid round-off errors in calculated results.
TestAmerica Tampa
Page 174 of 221
04/06/2009
Quality Control Results
Client: ARCADIS U.S., Inc.
Job Number: 660-27893-1
Method Blank - Batch: 660-75614
Lab Sample ID:
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
MB 660-75614/2
Water
1.0
03/02/2009 1138
03/02/2009 1138
Method: 8260B
Preparation: 5030B
Analysis Batch: 660-75614
Prep Batch: N/A
Units: ug/L
Instrument ID: BVMH GC/MS
Lab File ID:
1HC0212.D
Initial Weight/Volume: 5 mL
Final Weight/Volume: 5 mL
Analyte
Result
Qual
MDL
PQL
Benzene
Bromobenzene
Chlorobromomethane
Dichlorobromomethane
Bromoform
Bromomethane
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
Chlorodibromomethane
1,2-Dibromo-3-Chloropropane
Ethylene Dibromide
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
Hexachlorobutadiene
Isopropylbenzene
4-Isopropyltoluene
Methylene Chloride
Naphthalene
0.50
0.58
0.58
0.35
0.58
2.5
0.67
0.63
0.84
0.42
0.63
2.5
0.90
1.0
0.65
0.52
0.34
2.5
0.50
0.41
0.44
0.64
0.52
2.5
0.52
0.57
0.45
0.65
0.44
0.52
0.39
0.36
0.31
0.14
0.14
0.44
0.40
0.19
0.69
4.0
2.5
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
0.50
0.58
0.58
0.35
0.58
2.5
0.67
0.63
0.84
0.42
0.63
2.5
0.90
1.0
0.65
0.52
0.34
2.5
0.50
0.41
0.44
0.64
0.52
2.5
0.52
0.57
0.45
0.65
0.44
0.52
0.39
0.36
0.31
0.14
0.14
0.44
0.40
0.19
0.69
4.0
2.5
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
4.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
5.0
Calculations are performed before rounding to avoid round-off errors in calculated results.
TestAmerica Tampa
Page 175 of 221
04/06/2009
Quality Control Results
Client: ARCADIS U.S., Inc.
Job Number: 660-27893-1
Method Blank - Batch: 660-75614
Lab Sample ID:
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
MB 660-75614/2
Water
1.0
03/02/2009 1138
03/02/2009 1138
Method: 8260B
Preparation: 5030B
Analysis Batch: 660-75614
Prep Batch: N/A
Units: ug/L
Instrument ID: BVMH GC/MS
Lab File ID:
1HC0212.D
Initial Weight/Volume: 5 mL
Final Weight/Volume: 5 mL
Analyte
Result
Qual
MDL
PQL
N-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
o-Xylene
Acetone
2-Butanone (MEK)
4-Methyl-2-pentanone (MIBK)
Carbon disulfide
2-Hexanone
Methyl tert-butyl ether
m-Xylene & p-Xylene
0.59
0.98
0.63
0.15
0.50
0.51
0.77
0.58
0.46
0.47
0.50
2.5
0.18
0.86
0.54
0.50
0.50
9.9
8.4
3.8
0.85
4.4
0.44
0.60
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
0.59
0.98
0.63
0.15
0.50
0.51
0.77
0.58
0.46
0.47
0.50
2.5
0.18
0.86
0.54
0.50
0.50
9.9
8.4
3.8
0.85
4.4
0.44
0.60
1.0
2.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
20
10
10
1.0
10
1.0
2.0
Surrogate
Toluene-d8 (Surr)
4-Bromofluorobenzene
Dibromofluoromethane
% Rec
Acceptance Limits
94
83
107
77 - 122
74 - 126
70 - 130
Calculations are performed before rounding to avoid round-off errors in calculated results.
TestAmerica Tampa
Page 176 of 221
04/06/2009
Quality Control Results
Client: ARCADIS U.S., Inc.
Job Number: 660-27893-1
Lab Control Spike - Batch: 660-75614
Lab Sample ID:
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
LCS 660-75614/1
Water
1.0
03/02/2009 1046
03/02/2009 1046
Method: 8260B
Preparation: 5030B
Analysis Batch: 660-75614
Prep Batch: N/A
Units: ug/L
Instrument ID: BVMH GC/MS
Lab File ID:
1HC0209.D
Initial Weight/Volume: 5 mL
Final Weight/Volume: 5 mL
Analyte
Spike Amount
Result
% Rec.
Limit
Qual
Benzene
Chlorobenzene
1,1-Dichloroethene
Toluene
Trichloroethene
50.0
50.0
50.0
50.0
50.0
53.6
46.4
55.2
47.6
60.0
107
93
110
95
120
62 - 135
72 - 127
46 - 147
68 - 131
56 - 143
Matrix Spike/
Matrix Spike Duplicate Recovery Report - Batch: 660-75614
Method: 8260B
Preparation: 5030B
MS Lab Sample ID:
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
660-27893-14
Water
1.0
03/02/2009 1756
03/02/2009 1756
Analysis Batch: 660-75614
Prep Batch: N/A
Instrument ID: BVMH GC/MS
Lab File ID:
1HC0234.D
Initial Weight/Volume: 5 mL
Final Weight/Volume: 5 mL
MSD Lab Sample ID:
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
660-27893-14
Water
1.0
03/02/2009 1813
03/02/2009 1813
Analysis Batch: 660-75614
Prep Batch: N/A
Instrument ID: BVMH GC/MS
Lab File ID:
1HC0235.D
Initial Weight/Volume: 5 mL
Final Weight/Volume: 5 mL
Analyte
MS
Benzene
Chlorobenzene
1,1-Dichloroethene
Toluene
Trichloroethene
107
98
109
95
117
% Rec.
MSD
95
92
97
85
101
Limit
RPD
RPD Limit
62 - 135
72 - 127
46 - 147
68 - 131
56 - 143
12
6
11
11
14
37
22
30
33
35
MS Qual MSD Qual
Calculations are performed before rounding to avoid round-off errors in calculated results.
TestAmerica Tampa
Page 177 of 221
04/06/2009
Quality Control Results
Client: ARCADIS U.S., Inc.
Job Number: 660-27893-1
Method Blank - Batch: 660-75683
Lab Sample ID:
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
MB 660-75683/2
Water
1.0
03/03/2009 1212
03/03/2009 1212
Method: 8260B
Preparation: 5030B
Analysis Batch: 660-75683
Prep Batch: N/A
Units: ug/L
Instrument ID: BVMH GC/MS
Lab File ID:
1HC0313.D
Initial Weight/Volume: 5 mL
Final Weight/Volume: 5 mL
Analyte
Result
Qual
MDL
PQL
Benzene
Bromobenzene
Chlorobromomethane
Dichlorobromomethane
Bromoform
Bromomethane
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
Chlorodibromomethane
1,2-Dibromo-3-Chloropropane
Ethylene Dibromide
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
Hexachlorobutadiene
Isopropylbenzene
4-Isopropyltoluene
Methylene Chloride
Naphthalene
0.50
0.58
0.58
0.35
0.58
2.5
0.67
0.63
0.84
0.42
0.63
2.5
0.90
1.0
0.65
0.52
0.34
2.5
0.50
0.41
0.44
0.64
0.52
2.5
0.52
0.57
0.45
0.65
0.44
0.52
0.39
0.36
0.31
0.14
0.14
0.44
0.40
0.19
0.69
4.0
2.5
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
0.50
0.58
0.58
0.35
0.58
2.5
0.67
0.63
0.84
0.42
0.63
2.5
0.90
1.0
0.65
0.52
0.34
2.5
0.50
0.41
0.44
0.64
0.52
2.5
0.52
0.57
0.45
0.65
0.44
0.52
0.39
0.36
0.31
0.14
0.14
0.44
0.40
0.19
0.69
4.0
2.5
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
4.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
5.0
Calculations are performed before rounding to avoid round-off errors in calculated results.
TestAmerica Tampa
Page 178 of 221
04/06/2009
Quality Control Results
Client: ARCADIS U.S., Inc.
Job Number: 660-27893-1
Method Blank - Batch: 660-75683
Lab Sample ID:
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
MB 660-75683/2
Water
1.0
03/03/2009 1212
03/03/2009 1212
Method: 8260B
Preparation: 5030B
Analysis Batch: 660-75683
Prep Batch: N/A
Units: ug/L
Instrument ID: BVMH GC/MS
Lab File ID:
1HC0313.D
Initial Weight/Volume: 5 mL
Final Weight/Volume: 5 mL
Analyte
Result
Qual
MDL
PQL
N-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
o-Xylene
Acetone
2-Butanone (MEK)
4-Methyl-2-pentanone (MIBK)
Carbon disulfide
2-Hexanone
Methyl tert-butyl ether
m-Xylene & p-Xylene
0.59
0.98
0.63
0.15
0.50
0.51
0.77
0.58
0.46
0.47
0.50
2.5
0.18
0.86
0.54
0.50
0.50
9.9
8.4
3.8
0.85
4.4
0.44
0.60
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
0.59
0.98
0.63
0.15
0.50
0.51
0.77
0.58
0.46
0.47
0.50
2.5
0.18
0.86
0.54
0.50
0.50
9.9
8.4
3.8
0.85
4.4
0.44
0.60
1.0
2.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
20
10
10
1.0
10
1.0
2.0
Surrogate
Toluene-d8 (Surr)
4-Bromofluorobenzene
Dibromofluoromethane
% Rec
Acceptance Limits
114
87
107
77 - 122
74 - 126
70 - 130
Calculations are performed before rounding to avoid round-off errors in calculated results.
TestAmerica Tampa
Page 179 of 221
04/06/2009
Quality Control Results
Client: ARCADIS U.S., Inc.
Job Number: 660-27893-1
Lab Control Spike - Batch: 660-75683
Lab Sample ID:
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
LCS 660-75683/1
Water
1.0
03/03/2009 1103
03/03/2009 1103
Method: 8260B
Preparation: 5030B
Analysis Batch: 660-75683
Prep Batch: N/A
Units: ug/L
Instrument ID: BVMH GC/MS
Lab File ID:
1HC0309.D
Initial Weight/Volume: 5 mL
Final Weight/Volume: 5 mL
Analyte
Spike Amount
Result
% Rec.
Limit
Benzene
Chlorobenzene
1,1-Dichloroethene
Toluene
Trichloroethene
50.0
50.0
50.0
50.0
50.0
50.6
46.1
54.7
46.3
56.1
101
92
109
93
112
62 - 135
72 - 127
46 - 147
68 - 131
56 - 143
Matrix Spike - Batch: 660-75683
Lab Sample ID:
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
660-27916-D-15 MS
Water
1.0
03/03/2009 1429
03/03/2009 1429
Qual
Method: 8260B
Preparation: 5030B
Analysis Batch: 660-75683
Prep Batch: N/A
Units: ug/L
Instrument ID: BVMH GC/MS
Lab File ID:
1HC0321.D
Initial Weight/Volume: 5 mL
Final Weight/Volume: 5 mL
Analyte
Sample Result/Qual
Spike Amount
Result
% Rec.
Benzene
Chlorobenzene
1,1-Dichloroethene
Toluene
Trichloroethene
0.50
0.63
0.45
0.51
0.50
50.0
50.0
50.0
50.0
50.0
48.1
43.4
50.5
43.6
51.9
96
87
101
87
104
U
U
U
U
U
Limit
Qual
62 - 135
72 - 127
46 - 147
68 - 131
56 - 143
Calculations are performed before rounding to avoid round-off errors in calculated results.
TestAmerica Tampa
Page 180 of 221
04/06/2009
Quality Control Results
Client: ARCADIS U.S., Inc.
Job Number: 660-27893-1
Duplicate - Batch: 660-75683
Lab Sample ID:
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
660-27916-B-13 DU
Water
1.0
03/03/2009 1355
03/03/2009 1355
Method: 8260B
Preparation: 5030B
Analysis Batch: 660-75683
Prep Batch: N/A
Units: ug/L
Instrument ID: BVMH GC/MS
Lab File ID:
1HC0319.D
Initial Weight/Volume: 5 mL
Final Weight/Volume: 5 mL
Analyte
Sample Result/Qual
Result
RPD
Limit
Qual
Benzene
Bromobenzene
Chlorobromomethane
Dichlorobromomethane
Bromoform
Bromomethane
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
Chlorodibromomethane
1,2-Dibromo-3-Chloropropane
Ethylene Dibromide
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
Hexachlorobutadiene
Isopropylbenzene
4-Isopropyltoluene
0.50
0.58
0.58
0.35
0.58
2.5
0.67
0.63
0.84
0.42
0.63
2.5
0.90
1.0
0.65
0.52
0.34
2.5
0.50
0.41
0.44
0.64
0.52
2.5
0.52
0.57
0.45
0.65
0.44
0.52
0.39
0.36
0.31
0.14
0.14
0.44
0.40
0.19
0.69
0.50
0.58
0.58
0.35
0.58
2.5
0.67
0.63
0.84
0.42
0.63
2.5
0.90
1.0
0.65
0.52
0.34
2.5
0.50
0.41
0.44
0.64
0.52
2.5
0.52
0.57
0.45
0.65
0.44
0.52
0.39
0.36
0.31
0.14
0.14
0.44
0.40
0.19
0.69
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
37
35
33
28
31
33
33
34
34
38
22
34
20
44
39
25
31
30
40
40
39
29
31
34
47
23
30
28
22
24
40
21
37
21
24
18
29
36
34
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
Calculations are performed before rounding to avoid round-off errors in calculated results.
TestAmerica Tampa
Page 181 of 221
04/06/2009
Quality Control Results
Client: ARCADIS U.S., Inc.
Job Number: 660-27893-1
Duplicate - Batch: 660-75683
Lab Sample ID:
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
660-27916-B-13 DU
Water
1.0
03/03/2009 1355
03/03/2009 1355
Method: 8260B
Preparation: 5030B
Analysis Batch: 660-75683
Prep Batch: N/A
Units: ug/L
Instrument ID: BVMH GC/MS
Lab File ID:
1HC0319.D
Initial Weight/Volume: 5 mL
Final Weight/Volume: 5 mL
Analyte
Sample Result/Qual
Result
RPD
Limit
Qual
Methylene Chloride
Naphthalene
N-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
o-Xylene
Acetone
2-Butanone (MEK)
4-Methyl-2-pentanone (MIBK)
Carbon disulfide
2-Hexanone
Methyl tert-butyl ether
m-Xylene & p-Xylene
4.0
2.5
0.59
0.98
0.63
0.15
0.50
0.51
0.77
0.58
0.46
0.47
0.50
2.5
0.18
0.86
0.54
0.50
0.50
9.9
8.4
3.8
0.85
4.4
0.44
0.60
4.0
2.5
0.59
0.98
0.63
0.15
0.50
0.51
0.77
0.58
0.46
0.47
0.50
2.5
0.18
0.86
0.54
0.50
0.50
9.9
8.4
3.8
0.85
4.4
0.44
0.60
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
50
50
34
28
20
22
24
33
65
57
27
21
35
21
26
20
48
21
30
52
31
42
23
36
38
30
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
Surrogate
% Rec
Toluene-d8 (Surr)
4-Bromofluorobenzene
Dibromofluoromethane
86
83
106
Acceptance Limits
77 - 122
74 - 126
70 - 130
Calculations are performed before rounding to avoid round-off errors in calculated results.
TestAmerica Tampa
Page 182 of 221
04/06/2009
Quality Control Results
Client: ARCADIS U.S., Inc.
Job Number: 660-27893-1
Method Blank - Batch: 660-75698
Lab Sample ID:
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
MB 660-75698/2
Water
1.0
02/28/2009 0051
02/28/2009 0051
Method: 8260B
Preparation: 5030B
Analysis Batch: 660-75698
Prep Batch: N/A
Units: ug/L
Instrument ID: BVMJ GC/MS
Lab File ID:
1JB2727.D
Initial Weight/Volume: 5 mL
Final Weight/Volume: 5 mL
Analyte
Result
Qual
MDL
PQL
Benzene
Bromobenzene
Chlorobromomethane
Dichlorobromomethane
Bromoform
Bromomethane
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
Chlorodibromomethane
1,2-Dibromo-3-Chloropropane
Ethylene Dibromide
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
Hexachlorobutadiene
Isopropylbenzene
4-Isopropyltoluene
Methylene Chloride
Naphthalene
0.50
0.58
0.58
0.35
0.58
2.5
0.67
0.63
0.84
0.42
0.63
2.5
0.90
1.0
0.65
0.52
0.34
2.5
0.50
0.41
0.44
0.64
0.52
2.5
0.52
0.57
0.45
0.65
0.44
0.52
0.39
0.36
0.31
0.14
0.14
0.44
0.40
0.19
0.69
4.0
2.5
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
0.50
0.58
0.58
0.35
0.58
2.5
0.67
0.63
0.84
0.42
0.63
2.5
0.90
1.0
0.65
0.52
0.34
2.5
0.50
0.41
0.44
0.64
0.52
2.5
0.52
0.57
0.45
0.65
0.44
0.52
0.39
0.36
0.31
0.14
0.14
0.44
0.40
0.19
0.69
4.0
2.5
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
4.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
5.0
Calculations are performed before rounding to avoid round-off errors in calculated results.
TestAmerica Tampa
Page 183 of 221
04/06/2009
Quality Control Results
Client: ARCADIS U.S., Inc.
Job Number: 660-27893-1
Method Blank - Batch: 660-75698
Lab Sample ID:
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
MB 660-75698/2
Water
1.0
02/28/2009 0051
02/28/2009 0051
Method: 8260B
Preparation: 5030B
Analysis Batch: 660-75698
Prep Batch: N/A
Units: ug/L
Instrument ID: BVMJ GC/MS
Lab File ID:
1JB2727.D
Initial Weight/Volume: 5 mL
Final Weight/Volume: 5 mL
Analyte
Result
Qual
MDL
PQL
N-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
o-Xylene
Acetone
2-Butanone (MEK)
4-Methyl-2-pentanone (MIBK)
Carbon disulfide
2-Hexanone
Methyl tert-butyl ether
m-Xylene & p-Xylene
0.59
0.98
0.63
0.15
0.50
0.51
0.77
0.58
0.46
0.47
0.50
2.5
0.18
0.86
0.54
0.50
0.50
9.9
8.4
3.8
0.85
4.4
0.44
0.60
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
0.59
0.98
0.63
0.15
0.50
0.51
0.77
0.58
0.46
0.47
0.50
2.5
0.18
0.86
0.54
0.50
0.50
9.9
8.4
3.8
0.85
4.4
0.44
0.60
1.0
2.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
20
10
10
1.0
10
1.0
2.0
Surrogate
Toluene-d8 (Surr)
4-Bromofluorobenzene
Dibromofluoromethane
% Rec
Acceptance Limits
98
101
95
77 - 122
74 - 126
70 - 130
Calculations are performed before rounding to avoid round-off errors in calculated results.
TestAmerica Tampa
Page 184 of 221
04/06/2009
Quality Control Results
Client: ARCADIS U.S., Inc.
Job Number: 660-27893-1
Lab Control Spike - Batch: 660-75698
Lab Sample ID:
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
LCS 660-75698/1
Water
1.0
02/28/2009 0026
02/28/2009 0026
Method: 8260B
Preparation: 5030B
Analysis Batch: 660-75698
Prep Batch: N/A
Units: ug/L
Instrument ID: BVMJ GC/MS
Lab File ID:
1JB2726.D
Initial Weight/Volume: 5 mL
Final Weight/Volume: 5 mL
Analyte
Spike Amount
Result
% Rec.
Limit
Qual
Benzene
Chlorobenzene
1,1-Dichloroethene
Toluene
Trichloroethene
50.0
50.0
50.0
50.0
50.0
53.6
53.5
53.6
54.2
54.2
107
107
107
108
108
62 - 135
72 - 127
46 - 147
68 - 131
56 - 143
Matrix Spike/
Matrix Spike Duplicate Recovery Report - Batch: 660-75698
Method: 8260B
Preparation: 5030B
MS Lab Sample ID:
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
660-27893-21
Water
1.0
02/28/2009 0205
02/28/2009 0205
Analysis Batch: 660-75698
Prep Batch: N/A
Instrument ID: BVMJ GC/MS
Lab File ID:
1JB2730.D
Initial Weight/Volume: 5 mL
Final Weight/Volume: 5 mL
MSD Lab Sample ID:
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
660-27893-21
Water
1.0
02/28/2009 0230
02/28/2009 0230
Analysis Batch: 660-75698
Prep Batch: N/A
Instrument ID: BVMJ GC/MS
Lab File ID:
1JB2731.D
Initial Weight/Volume: 5 mL
Final Weight/Volume: 5 mL
Analyte
MS
Benzene
Chlorobenzene
1,1-Dichloroethene
Toluene
Trichloroethene
108
105
102
105
107
% Rec.
MSD
98
95
96
98
104
Limit
RPD
RPD Limit
62 - 135
72 - 127
46 - 147
68 - 131
56 - 143
10
10
6
8
3
37
22
30
33
35
MS Qual MSD Qual
Calculations are performed before rounding to avoid round-off errors in calculated results.
TestAmerica Tampa
Page 185 of 221
04/06/2009
Quality Control Results
Client: ARCADIS U.S., Inc.
Job Number: 660-27893-1
Method Blank - Batch: 660-75699
Lab Sample ID:
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
MB 660-75699/2
Water
1.0
02/28/2009 0906
02/28/2009 0906
Method: 8260B
Preparation: 5030B
Analysis Batch: 660-75699
Prep Batch: N/A
Units: ug/L
Instrument ID: BVMJ GC/MS
Lab File ID:
1JB2747.D
Initial Weight/Volume: 5 mL
Final Weight/Volume: 5 mL
Analyte
Result
Qual
MDL
PQL
Benzene
Bromobenzene
Chlorobromomethane
Dichlorobromomethane
Bromoform
Bromomethane
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
Chlorodibromomethane
1,2-Dibromo-3-Chloropropane
Ethylene Dibromide
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
Hexachlorobutadiene
Isopropylbenzene
4-Isopropyltoluene
Methylene Chloride
Naphthalene
0.50
0.58
0.58
0.35
0.58
2.5
0.67
0.63
0.84
0.42
0.63
2.5
0.90
1.0
0.65
0.52
0.34
2.5
0.50
0.41
0.44
0.64
0.52
2.5
0.52
0.57
0.45
0.65
0.44
0.52
0.39
0.36
0.31
0.14
0.14
0.44
0.40
0.19
0.69
4.0
2.5
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
0.50
0.58
0.58
0.35
0.58
2.5
0.67
0.63
0.84
0.42
0.63
2.5
0.90
1.0
0.65
0.52
0.34
2.5
0.50
0.41
0.44
0.64
0.52
2.5
0.52
0.57
0.45
0.65
0.44
0.52
0.39
0.36
0.31
0.14
0.14
0.44
0.40
0.19
0.69
4.0
2.5
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
4.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
5.0
Calculations are performed before rounding to avoid round-off errors in calculated results.
TestAmerica Tampa
Page 186 of 221
04/06/2009
Quality Control Results
Client: ARCADIS U.S., Inc.
Job Number: 660-27893-1
Method Blank - Batch: 660-75699
Lab Sample ID:
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
MB 660-75699/2
Water
1.0
02/28/2009 0906
02/28/2009 0906
Method: 8260B
Preparation: 5030B
Analysis Batch: 660-75699
Prep Batch: N/A
Units: ug/L
Instrument ID: BVMJ GC/MS
Lab File ID:
1JB2747.D
Initial Weight/Volume: 5 mL
Final Weight/Volume: 5 mL
Analyte
Result
Qual
MDL
PQL
N-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
o-Xylene
Acetone
2-Butanone (MEK)
4-Methyl-2-pentanone (MIBK)
Carbon disulfide
2-Hexanone
Methyl tert-butyl ether
m-Xylene & p-Xylene
0.59
0.98
0.63
0.15
0.50
0.51
0.77
0.58
0.46
0.47
0.50
2.5
0.18
0.86
0.54
0.50
0.50
9.9
8.4
3.8
0.85
4.4
0.44
0.60
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
0.59
0.98
0.63
0.15
0.50
0.51
0.77
0.58
0.46
0.47
0.50
2.5
0.18
0.86
0.54
0.50
0.50
9.9
8.4
3.8
0.85
4.4
0.44
0.60
1.0
2.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
20
10
10
1.0
10
1.0
2.0
Surrogate
Toluene-d8 (Surr)
4-Bromofluorobenzene
Dibromofluoromethane
% Rec
Acceptance Limits
99
102
96
77 - 122
74 - 126
70 - 130
Calculations are performed before rounding to avoid round-off errors in calculated results.
TestAmerica Tampa
Page 187 of 221
04/06/2009
Quality Control Results
Client: ARCADIS U.S., Inc.
Job Number: 660-27893-1
Lab Control Spike - Batch: 660-75699
Lab Sample ID:
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
LCS 660-75699/1
Water
1.0
02/28/2009 0816
02/28/2009 0816
Method: 8260B
Preparation: 5030B
Analysis Batch: 660-75699
Prep Batch: N/A
Units: ug/L
Instrument ID: BVMJ GC/MS
Lab File ID:
1JB2745.D
Initial Weight/Volume: 5 mL
Final Weight/Volume: 5 mL
Analyte
Spike Amount
Result
% Rec.
Limit
Qual
Benzene
Chlorobenzene
1,1-Dichloroethene
Toluene
Trichloroethene
50.0
50.0
50.0
50.0
50.0
55.6
55.1
54.1
55.6
56.4
111
110
108
111
113
62 - 135
72 - 127
46 - 147
68 - 131
56 - 143
Matrix Spike/
Matrix Spike Duplicate Recovery Report - Batch: 660-75699
Method: 8260B
Preparation: 5030B
MS Lab Sample ID:
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
660-27893-26
Water
1.0
02/28/2009 1044
02/28/2009 1044
Analysis Batch: 660-75699
Prep Batch: N/A
Instrument ID: BVMJ GC/MS
Lab File ID:
1JB2751.D
Initial Weight/Volume: 5 mL
Final Weight/Volume: 5 mL
MSD Lab Sample ID:
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
660-27893-26
Water
1.0
02/28/2009 1108
02/28/2009 1108
Analysis Batch: 660-75699
Prep Batch: N/A
Instrument ID: BVMJ GC/MS
Lab File ID:
1JB2752.D
Initial Weight/Volume: 5 mL
Final Weight/Volume: 5 mL
Analyte
MS
Benzene
Chlorobenzene
1,1-Dichloroethene
Toluene
Trichloroethene
100
97
97
100
101
% Rec.
MSD
103
99
99
101
101
Limit
RPD
RPD Limit
62 - 135
72 - 127
46 - 147
68 - 131
56 - 143
3
2
2
1
0
37
22
30
33
35
MS Qual MSD Qual
Calculations are performed before rounding to avoid round-off errors in calculated results.
TestAmerica Tampa
Page 188 of 221
04/06/2009
Quality Control Results
Client: ARCADIS U.S., Inc.
Job Number: 660-27893-1
Method Blank - Batch: 660-75700
Lab Sample ID:
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
MB 660-75700/2
Water
1.0
03/02/2009 1424
03/02/2009 1424
Method: 8260B
Preparation: 5030B
Analysis Batch: 660-75700
Prep Batch: N/A
Units: ug/L
Instrument ID: BVMJ GC/MS
Lab File ID:
1JC0211.D
Initial Weight/Volume: 5 mL
Final Weight/Volume: 5 mL
Analyte
Result
Qual
MDL
PQL
Benzene
Bromobenzene
Chlorobromomethane
Dichlorobromomethane
Bromoform
Bromomethane
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
Chlorodibromomethane
1,2-Dibromo-3-Chloropropane
Ethylene Dibromide
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
Hexachlorobutadiene
Isopropylbenzene
4-Isopropyltoluene
Methylene Chloride
Naphthalene
0.50
0.58
0.58
0.35
0.58
2.5
0.67
0.63
0.84
0.42
0.63
2.5
0.90
1.0
0.65
0.52
0.34
2.5
0.50
0.41
0.44
0.64
0.52
2.5
0.52
0.57
0.45
0.65
0.44
0.52
0.39
0.36
0.31
0.14
0.14
0.44
0.40
0.19
0.69
4.0
2.5
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
0.50
0.58
0.58
0.35
0.58
2.5
0.67
0.63
0.84
0.42
0.63
2.5
0.90
1.0
0.65
0.52
0.34
2.5
0.50
0.41
0.44
0.64
0.52
2.5
0.52
0.57
0.45
0.65
0.44
0.52
0.39
0.36
0.31
0.14
0.14
0.44
0.40
0.19
0.69
4.0
2.5
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
4.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
5.0
Calculations are performed before rounding to avoid round-off errors in calculated results.
TestAmerica Tampa
Page 189 of 221
04/06/2009
Quality Control Results
Client: ARCADIS U.S., Inc.
Job Number: 660-27893-1
Method Blank - Batch: 660-75700
Lab Sample ID:
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
MB 660-75700/2
Water
1.0
03/02/2009 1424
03/02/2009 1424
Method: 8260B
Preparation: 5030B
Analysis Batch: 660-75700
Prep Batch: N/A
Units: ug/L
Instrument ID: BVMJ GC/MS
Lab File ID:
1JC0211.D
Initial Weight/Volume: 5 mL
Final Weight/Volume: 5 mL
Analyte
Result
Qual
MDL
PQL
N-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
o-Xylene
Acetone
2-Butanone (MEK)
4-Methyl-2-pentanone (MIBK)
Carbon disulfide
2-Hexanone
Methyl tert-butyl ether
m-Xylene & p-Xylene
0.59
0.98
0.63
0.15
0.50
0.51
0.77
0.58
0.46
0.47
0.50
2.5
0.18
0.86
0.54
0.50
0.50
9.9
8.4
3.8
0.85
4.4
0.44
0.60
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
0.59
0.98
0.63
0.15
0.50
0.51
0.77
0.58
0.46
0.47
0.50
2.5
0.18
0.86
0.54
0.50
0.50
9.9
8.4
3.8
0.85
4.4
0.44
0.60
1.0
2.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
20
10
10
1.0
10
1.0
2.0
Surrogate
Toluene-d8 (Surr)
4-Bromofluorobenzene
Dibromofluoromethane
% Rec
Acceptance Limits
102
106
100
77 - 122
74 - 126
70 - 130
Calculations are performed before rounding to avoid round-off errors in calculated results.
TestAmerica Tampa
Page 190 of 221
04/06/2009
Quality Control Results
Client: ARCADIS U.S., Inc.
Job Number: 660-27893-1
Lab Control Spike - Batch: 660-75700
Lab Sample ID:
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
LCS 660-75700/1
Water
1.0
03/02/2009 1247
03/02/2009 1247
Method: 8260B
Preparation: 5030B
Analysis Batch: 660-75700
Prep Batch: N/A
Units: ug/L
Instrument ID: BVMJ GC/MS
Lab File ID:
1JC0207.D
Initial Weight/Volume: 5 mL
Final Weight/Volume: 5 mL
Analyte
Spike Amount
Result
% Rec.
Limit
Qual
Benzene
Chlorobenzene
1,1-Dichloroethene
Toluene
Trichloroethene
50.0
50.0
50.0
50.0
50.0
52.6
50.1
52.8
51.1
55.9
105
100
106
102
112
62 - 135
72 - 127
46 - 147
68 - 131
56 - 143
Matrix Spike/
Matrix Spike Duplicate Recovery Report - Batch: 660-75700
Method: 8260B
Preparation: 5030B
MS Lab Sample ID:
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
660-27893-22
Water
1.0
03/02/2009 1602
03/02/2009 1602
Analysis Batch: 660-75700
Prep Batch: N/A
Instrument ID: BVMJ GC/MS
Lab File ID:
1JC0215.D
Initial Weight/Volume: 5 mL
Final Weight/Volume: 5 mL
MSD Lab Sample ID:
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
660-27893-22
Water
1.0
03/02/2009 1626
03/02/2009 1626
Analysis Batch: 660-75700
Prep Batch: N/A
Instrument ID: BVMJ GC/MS
Lab File ID:
1JC0216.D
Initial Weight/Volume: 5 mL
Final Weight/Volume: 5 mL
Analyte
MS
Benzene
Chlorobenzene
1,1-Dichloroethene
Toluene
Trichloroethene
101
96
98
96
102
% Rec.
MSD
105
99
101
100
104
Limit
RPD
RPD Limit
62 - 135
72 - 127
46 - 147
68 - 131
56 - 143
4
2
3
4
2
37
22
30
33
35
MS Qual MSD Qual
Calculations are performed before rounding to avoid round-off errors in calculated results.
TestAmerica Tampa
Page 191 of 221
04/06/2009
Quality Control Results
Client: ARCADIS U.S., Inc.
Job Number: 660-27893-1
Method Blank - Batch: 660-75525
Lab Sample ID:
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
MB 660-75525/2
Water
1.0
02/27/2009 1200
02/27/2009 1200
Method: 8260C SIM/ID
Preparation: 5030B
Analysis Batch: 660-75525
Prep Batch: N/A
Units: ug/L
Instrument ID: BVMH GC/MS
Lab File ID:
1HB2713.D
Initial Weight/Volume: 5 mL
Final Weight/Volume: 5 mL
Analyte
Result
Qual
MDL
PQL
1,4-Dioxane
0.54
U
0.54
1.0
Lab Control Spike - Batch: 660-75525
Lab Sample ID:
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
LCS 660-75525/1
Water
1.0
02/27/2009 1052
02/27/2009 1052
Method: 8260C SIM/ID
Preparation: 5030B
Analysis Batch: 660-75525
Prep Batch: N/A
Units: ug/L
Instrument ID: BVMH GC/MS
Lab File ID:
1HB2709.D
Initial Weight/Volume: 5 mL
Final Weight/Volume: 5 mL
Analyte
Spike Amount
Result
% Rec.
Limit
Qual
1,4-Dioxane
25.0
25.5
102
50 - 150
Matrix Spike/
Matrix Spike Duplicate Recovery Report - Batch: 660-75525
Method: 8260C SIM/ID
Preparation: 5030B
MS Lab Sample ID:
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
660-27890-C-3 MS
Water
1.0
02/27/2009 1525
02/27/2009 1525
Analysis Batch: 660-75525
Prep Batch: N/A
Instrument ID: BVMH GC/MS
Lab File ID:
1HB2725.D
Initial Weight/Volume: 5 mL
Final Weight/Volume: 5 mL
MSD Lab Sample ID:
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
660-27890-D-3 MSD
Water
1.0
02/27/2009 1542
02/27/2009 1542
Analysis Batch: 660-75525
Prep Batch: N/A
Instrument ID: BVMH GC/MS
Lab File ID:
1HB2726.D
Initial Weight/Volume: 5 mL
Final Weight/Volume: 5 mL
Analyte
MS
1,4-Dioxane
100
% Rec.
MSD
90
Limit
RPD
RPD Limit
50 - 150
11
50
MS Qual MSD Qual
Calculations are performed before rounding to avoid round-off errors in calculated results.
TestAmerica Tampa
Page 192 of 221
04/06/2009
Quality Control Results
Client: ARCADIS U.S., Inc.
Job Number: 660-27893-1
Method Blank - Batch: 660-75613
Lab Sample ID:
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
MB 660-75613/2
Water
1.0
03/02/2009 1138
03/02/2009 1138
Method: 8260C SIM/ID
Preparation: 5030B
Analysis Batch: 660-75613
Prep Batch: N/A
Units: ug/L
Instrument ID: BVMH GC/MS
Lab File ID:
1HC0212.D
Initial Weight/Volume: 5 mL
Final Weight/Volume: 5 mL
Analyte
Result
Qual
MDL
PQL
1,4-Dioxane
0.54
U
0.54
1.0
Lab Control Spike - Batch: 660-75613
Lab Sample ID:
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
LCS 660-75613/1
Water
1.0
03/02/2009 1046
03/02/2009 1046
Method: 8260C SIM/ID
Preparation: 5030B
Analysis Batch: 660-75613
Prep Batch: N/A
Units: ug/L
Instrument ID: BVMH GC/MS
Lab File ID:
1HC0209.D
Initial Weight/Volume: 5 mL
Final Weight/Volume: 5 mL
Analyte
Spike Amount
Result
% Rec.
Limit
Qual
1,4-Dioxane
25.0
27.3
109
50 - 150
Matrix Spike/
Matrix Spike Duplicate Recovery Report - Batch: 660-75613
Method: 8260C SIM/ID
Preparation: 5030B
MS Lab Sample ID:
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
660-27893-14
Water
1.0
03/02/2009 1756
03/02/2009 1756
Analysis Batch: 660-75613
Prep Batch: N/A
Instrument ID: BVMH GC/MS
Lab File ID:
1HC0234.D
Initial Weight/Volume: 5 mL
Final Weight/Volume: 5 mL
MSD Lab Sample ID:
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
660-27893-14
Water
1.0
03/02/2009 1813
03/02/2009 1813
Analysis Batch: 660-75613
Prep Batch: N/A
Instrument ID: BVMH GC/MS
Lab File ID:
1HC0235.D
Initial Weight/Volume: 5 mL
Final Weight/Volume: 5 mL
Analyte
MS
1,4-Dioxane
102
% Rec.
MSD
101
Limit
RPD
RPD Limit
50 - 150
0
50
MS Qual MSD Qual
Calculations are performed before rounding to avoid round-off errors in calculated results.
TestAmerica Tampa
Page 193 of 221
04/06/2009
Quality Control Results
Client: ARCADIS U.S., Inc.
Job Number: 660-27893-1
Method Blank - Batch: 660-75684
Lab Sample ID:
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
MB 660-75684/3
Water
1.0
03/03/2009 1229
03/03/2009 1229
Method: 8260C SIM/ID
Preparation: 5030B
Analysis Batch: 660-75684
Prep Batch: N/A
Units: ug/L
Instrument ID: BVMH GC/MS
Lab File ID:
1HC0314.D
Initial Weight/Volume: 5 mL
Final Weight/Volume: 5 mL
Analyte
Result
Qual
MDL
PQL
1,4-Dioxane
0.54
U
0.54
1.0
Lab Control Spike - Batch: 660-75684
Lab Sample ID:
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
LCS 660-75684/1
Water
1.0
03/03/2009 1103
03/03/2009 1103
Method: 8260C SIM/ID
Preparation: 5030B
Analysis Batch: 660-75684
Prep Batch: N/A
Units: ug/L
Instrument ID: BVMH GC/MS
Lab File ID:
1HC0309.D
Initial Weight/Volume: 5 mL
Final Weight/Volume: 5 mL
Analyte
Spike Amount
Result
% Rec.
Limit
1,4-Dioxane
25.0
25.6
103
50 - 150
Matrix Spike - Batch: 660-75684
Lab Sample ID:
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
660-27916-D-15 MS
Water
1.0
03/03/2009 1429
03/03/2009 1429
Qual
Method: 8260C SIM/ID
Preparation: 5030B
Analysis Batch: 660-75684
Prep Batch: N/A
Units: ug/L
Instrument ID: BVMH GC/MS
Lab File ID:
1HC0321.D
Initial Weight/Volume: 5 mL
Final Weight/Volume: 5 mL
Analyte
Sample Result/Qual
Spike Amount
Result
% Rec.
1,4-Dioxane
0.89
25.0
23.3
90
I
Limit
Qual
50 - 150
Calculations are performed before rounding to avoid round-off errors in calculated results.
TestAmerica Tampa
Page 194 of 221
04/06/2009
Quality Control Results
Client: ARCADIS U.S., Inc.
Job Number: 660-27893-1
Duplicate - Batch: 660-75684
Lab Sample ID:
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
660-27916-B-13 DU
Water
1.0
03/03/2009 1355
03/03/2009 1355
Method: 8260C SIM/ID
Preparation: 5030B
Analysis Batch: 660-75684
Prep Batch: N/A
Units: ug/L
Instrument ID: BVMH GC/MS
Lab File ID:
1HC0319.D
Initial Weight/Volume: 5 mL
Final Weight/Volume: 5 mL
Analyte
Sample Result/Qual
Result
RPD
Limit
1,4-Dioxane
13
17.2
28
50
Qual
Calculations are performed before rounding to avoid round-off errors in calculated results.
TestAmerica Tampa
Page 195 of 221
04/06/2009
Quality Control Results
Client: ARCADIS U.S., Inc.
Job Number: 660-27893-1
Method Blank - Batch: 660-75694
Lab Sample ID:
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
MB 660-75694/2
Water
1.0
02/28/2009 0051
02/28/2009 0051
Method: 8260C SIM/ID
Preparation: 5030B
Analysis Batch: 660-75694
Prep Batch: N/A
Units: ug/L
Instrument ID: BVMJ GC/MS
Lab File ID:
1JB2727.D
Initial Weight/Volume: 5 mL
Final Weight/Volume: 5 mL
Analyte
Result
Qual
MDL
PQL
1,4-Dioxane
0.54
U
0.54
1.0
Lab Control Spike - Batch: 660-75694
Lab Sample ID:
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
LCS 660-75694/1
Water
1.0
02/28/2009 0026
02/28/2009 0026
Method: 8260C SIM/ID
Preparation: 5030B
Analysis Batch: 660-75694
Prep Batch: N/A
Units: ug/L
Instrument ID: BVMJ GC/MS
Lab File ID:
1JB2726.D
Initial Weight/Volume: 5 mL
Final Weight/Volume: 5 mL
Analyte
Spike Amount
Result
% Rec.
Limit
Qual
1,4-Dioxane
25.0
25.1
100
50 - 150
Matrix Spike/
Matrix Spike Duplicate Recovery Report - Batch: 660-75694
Method: 8260C SIM/ID
Preparation: 5030B
MS Lab Sample ID:
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
660-27893-21
Water
1.0
02/28/2009 0205
02/28/2009 0205
Analysis Batch: 660-75694
Prep Batch: N/A
Instrument ID: BVMJ GC/MS
Lab File ID:
1JB2730.D
Initial Weight/Volume: 5 mL
Final Weight/Volume: 5 mL
MSD Lab Sample ID:
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
660-27893-21
Water
1.0
02/28/2009 0230
02/28/2009 0230
Analysis Batch: 660-75694
Prep Batch: N/A
Instrument ID: BVMJ GC/MS
Lab File ID:
1JB2731.D
Initial Weight/Volume: 5 mL
Final Weight/Volume: 5 mL
Analyte
MS
1,4-Dioxane
115
% Rec.
MSD
91
Limit
RPD
RPD Limit
50 - 150
24
50
MS Qual MSD Qual
Calculations are performed before rounding to avoid round-off errors in calculated results.
TestAmerica Tampa
Page 196 of 221
04/06/2009
Quality Control Results
Client: ARCADIS U.S., Inc.
Job Number: 660-27893-1
Method Blank - Batch: 660-75695
Lab Sample ID:
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
MB 660-75695/2
Water
1.0
02/28/2009 0930
02/28/2009 0930
Method: 8260C SIM/ID
Preparation: 5030B
Analysis Batch: 660-75695
Prep Batch: N/A
Units: ug/L
Instrument ID: BVMJ GC/MS
Lab File ID:
1JB2748.D
Initial Weight/Volume: 5 mL
Final Weight/Volume: 5 mL
Analyte
Result
Qual
MDL
PQL
1,4-Dioxane
0.54
U
0.54
1.0
Lab Control Spike - Batch: 660-75695
Lab Sample ID:
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
LCS 660-75695/1
Water
1.0
02/28/2009 0816
02/28/2009 0816
Method: 8260C SIM/ID
Preparation: 5030B
Analysis Batch: 660-75695
Prep Batch: N/A
Units: ug/L
Instrument ID: BVMJ GC/MS
Lab File ID:
1JB2745.D
Initial Weight/Volume: 5 mL
Final Weight/Volume: 5 mL
Analyte
Spike Amount
Result
% Rec.
Limit
Qual
1,4-Dioxane
25.0
30.5
122
50 - 150
Matrix Spike/
Matrix Spike Duplicate Recovery Report - Batch: 660-75695
Method: 8260C SIM/ID
Preparation: 5030B
MS Lab Sample ID:
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
660-27893-26
Water
1.0
02/28/2009 1044
02/28/2009 1044
Analysis Batch: 660-75695
Prep Batch: N/A
Instrument ID: BVMJ GC/MS
Lab File ID:
1JB2751.D
Initial Weight/Volume: 5 mL
Final Weight/Volume: 5 mL
MSD Lab Sample ID:
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
660-27893-26
Water
1.0
02/28/2009 1108
02/28/2009 1108
Analysis Batch: 660-75695
Prep Batch: N/A
Instrument ID: BVMJ GC/MS
Lab File ID:
1JB2752.D
Initial Weight/Volume: 5 mL
Final Weight/Volume: 5 mL
Analyte
MS
1,4-Dioxane
104
% Rec.
MSD
107
Limit
RPD
RPD Limit
50 - 150
1
50
MS Qual MSD Qual
Calculations are performed before rounding to avoid round-off errors in calculated results.
TestAmerica Tampa
Page 197 of 221
04/06/2009
Quality Control Results
Client: ARCADIS U.S., Inc.
Job Number: 660-27893-1
Method Blank - Batch: 660-75696
Lab Sample ID:
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
MB 660-75696/1
Water
1.0
03/02/2009 1424
03/02/2009 1424
Method: 8260C SIM/ID
Preparation: 5030B
Analysis Batch: 660-75696
Prep Batch: N/A
Units: ug/L
Instrument ID: BVMJ GC/MS
Lab File ID:
1JC0211.D
Initial Weight/Volume: 5 mL
Final Weight/Volume: 5 mL
Analyte
Result
Qual
MDL
PQL
1,4-Dioxane
0.54
U
0.54
1.0
Lab Control Spike - Batch: 660-75696
Lab Sample ID:
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
LCS 660-75696/2
Water
1.0
03/02/2009 1449
03/02/2009 1449
Method: 8260C SIM/ID
Preparation: 5030B
Analysis Batch: 660-75696
Prep Batch: N/A
Units: ug/L
Instrument ID: BVMJ GC/MS
Lab File ID:
1JC0212.D
Initial Weight/Volume: 5 mL
Final Weight/Volume: 5 mL
Analyte
Spike Amount
Result
% Rec.
Limit
Qual
1,4-Dioxane
25.0
18.6
74
50 - 150
Matrix Spike/
Matrix Spike Duplicate Recovery Report - Batch: 660-75696
Method: 8260C SIM/ID
Preparation: 5030B
MS Lab Sample ID:
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
660-27893-22
Water
1.0
03/02/2009 1602
03/02/2009 1602
Analysis Batch: 660-75696
Prep Batch: N/A
Instrument ID: BVMJ GC/MS
Lab File ID:
1JC0215.D
Initial Weight/Volume: 5 mL
Final Weight/Volume: 5 mL
MSD Lab Sample ID:
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
660-27893-22
Water
1.0
03/02/2009 1626
03/02/2009 1626
Analysis Batch: 660-75696
Prep Batch: N/A
Instrument ID: BVMJ GC/MS
Lab File ID:
1JC0216.D
Initial Weight/Volume: 5 mL
Final Weight/Volume: 5 mL
Analyte
MS
1,4-Dioxane
94
% Rec.
MSD
94
Limit
RPD
RPD Limit
50 - 150
0
50
MS Qual MSD Qual
Calculations are performed before rounding to avoid round-off errors in calculated results.
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04/06/2009
Quality Control Results
Client: ARCADIS U.S., Inc.
Job Number: 660-27893-1
Method Blank - Batch: 660-75517
Lab Sample ID:
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
MB 660-75517/1-A
Water
1.0
03/03/2009 1254
02/27/2009 1027
Method: 6010B
Preparation: 3005A
Total Recoverable
Analysis Batch: 660-75689
Prep Batch: 660-75517
Units: mg/L
Instrument ID: TJA ICP TRACE
Lab File ID:
9C03A
Initial Weight/Volume: 50 mL
Final Weight/Volume: 50 mL
Analyte
Result
Qual
MDL
PQL
Calcium
Iron
Iron, Dissolved
Potassium
Magnesium
Manganese
Manganese, Dissolved
Sodium
0.10
0.050
0.050
0.19
0.020
0.0010
0.0010
0.31
U
U
U
U
U
U
U
U
0.10
0.050
0.050
0.19
0.020
0.0010
0.0010
0.31
0.50
0.20
0.20
1.0
0.080
0.0040
0.0040
0.50
Lab Control Spike - Batch: 660-75517
Lab Sample ID:
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
LCS 660-75517/2-A
Water
1.0
03/03/2009 1300
02/27/2009 1027
Method: 6010B
Preparation: 3005A
Total Recoverable
Analysis Batch: 660-75689
Prep Batch: 660-75517
Units: mg/L
Instrument ID: TJA ICP TRACE
Lab File ID:
9C03A
Initial Weight/Volume: 50 mL
Final Weight/Volume: 50 mL
Analyte
Spike Amount
Result
% Rec.
Limit
Calcium
Iron
Iron, Dissolved
Potassium
Magnesium
Manganese
Manganese, Dissolved
Sodium
1.00
1.00
1.00
10.0
1.00
1.00
1.00
10.0
0.962
0.969
0.969
8.81
0.929
0.966
0.966
9.71
96
97
97
88
93
97
97
97
75 - 125
75 - 125
75 - 125
75 - 125
75 - 125
75 - 125
75 - 125
75 - 125
Qual
Calculations are performed before rounding to avoid round-off errors in calculated results.
TestAmerica Tampa
Page 199 of 221
04/06/2009
Quality Control Results
Client: ARCADIS U.S., Inc.
Job Number: 660-27893-1
Matrix Spike/
Matrix Spike Duplicate Recovery Report - Batch: 660-75517
Method: 6010B
Preparation: 3005A
Total Recoverable
MS Lab Sample ID:
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
660-27893-41
Water
1.0
03/03/2009 1330
02/27/2009 1027
Analysis Batch: 660-75689
Prep Batch: 660-75517
Instrument ID: TJA ICP TRACE
Lab File ID:
9C03A
Initial Weight/Volume: 50 mL
Final Weight/Volume: 50 mL
MSD Lab Sample ID:
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
660-27893-41
Water
1.0
03/03/2009 1335
02/27/2009 1027
Analysis Batch: 660-75689
Prep Batch: 660-75517
Instrument ID: TJA ICP TRACE
Lab File ID:
9C03A
Initial Weight/Volume: 50 mL
Final Weight/Volume: 50 mL
Analyte
MS
Calcium
Iron
Iron, Dissolved
Potassium
Magnesium
Manganese
Manganese, Dissolved
Sodium
430
138
138
104
107
97
97
124
% Rec.
MSD
57
106
106
101
95
96
96
109
Limit
RPD
RPD Limit
MS Qual MSD Qual
75 - 125
75 - 125
75 - 125
75 - 125
75 - 125
75 - 125
75 - 125
75 - 125
3
3
3
3
3
1
1
3
20
20
20
20
20
20
20
20
J3
J3
J3
J3
Calculations are performed before rounding to avoid round-off errors in calculated results.
TestAmerica Tampa
Page 200 of 221
04/06/2009
Quality Control Results
Client: ARCADIS U.S., Inc.
Job Number: 660-27893-1
Method Blank - Batch: 660-75752
Lab Sample ID:
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
MB 660-75752/3
Water
1.0
03/02/2009 1717
N/A
Method: 300.0
Preparation: N/A
Analysis Batch: 660-75752
Prep Batch: N/A
Units: mg/L
Instrument ID: ICS 2000
Lab File ID:
N/A
Initial Weight/Volume:
Final Weight/Volume: 2 mL
Analyte
Result
Qual
MDL
PQL
Bromide
Chloride
0.027
0.20
U
U
0.027
0.20
0.050
0.50
Method Blank - Batch: 660-75752
Lab Sample ID:
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
MB 660-75752/19
Water
1.0
03/03/2009 1416
N/A
Method: 300.0
Preparation: N/A
Analysis Batch: 660-75752
Prep Batch: N/A
Units: mg/L
Instrument ID: ICS 2000
Lab File ID:
N/A
Initial Weight/Volume:
Final Weight/Volume: 2 mL
Analyte
Result
Qual
MDL
PQL
Sulfate
0.20
U
0.20
0.50
Calculations are performed before rounding to avoid round-off errors in calculated results.
TestAmerica Tampa
Page 201 of 221
04/06/2009
Quality Control Results
Client: ARCADIS U.S., Inc.
Job Number: 660-27893-1
Lab Control Spike - Batch: 660-75752
Lab Sample ID:
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
LCS 660-75752/4
Water
1.0
03/02/2009 1743
N/A
Method: 300.0
Preparation: N/A
Analysis Batch: 660-75752
Prep Batch: N/A
Units: mg/L
Instrument ID: ICS 2000
Lab File ID:
N/A
Initial Weight/Volume:
Final Weight/Volume: 2 mL
Analyte
Spike Amount
Result
% Rec.
Limit
Bromide
Chloride
1.00
10.0
0.994
10.1
99
101
90 - 110
90 - 110
Lab Control Spike - Batch: 660-75752
Lab Sample ID:
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
LCS 660-75752/20
Water
1.0
03/03/2009 1442
N/A
Qual
Method: 300.0
Preparation: N/A
Analysis Batch: 660-75752
Prep Batch: N/A
Units: mg/L
Instrument ID: ICS 2000
Lab File ID:
N/A
Initial Weight/Volume:
Final Weight/Volume: 2 mL
Analyte
Spike Amount
Result
% Rec.
Limit
Sulfate
10.0
10.2
102
90 - 110
Qual
Calculations are performed before rounding to avoid round-off errors in calculated results.
TestAmerica Tampa
Page 202 of 221
04/06/2009
Quality Control Results
Client: ARCADIS U.S., Inc.
Job Number: 660-27893-1
Matrix Spike/
Matrix Spike Duplicate Recovery Report - Batch: 660-75752
Method: 300.0
Preparation: N/A
MS Lab Sample ID:
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
660-27893-41
Water
2.0
03/02/2009 1835
N/A
Analysis Batch: 660-75752
Prep Batch: N/A
Instrument ID: ICS 2000
Lab File ID:
N/A
Initial Weight/Volume:
Final Weight/Volume: 2 mL
MSD Lab Sample ID:
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
660-27893-41
Water
2.0
03/02/2009 1900
N/A
Analysis Batch: 660-75752
Prep Batch: N/A
Instrument ID: ICS 2000
Lab File ID:
N/A
Initial Weight/Volume:
Final Weight/Volume: 2 mL
Analyte
MS
Bromide
100
% Rec.
MSD
102
Limit
RPD
RPD Limit
90 - 110
1
30
MS Qual MSD Qual
Matrix Spike/
Matrix Spike Duplicate Recovery Report - Batch: 660-75752
Method: 300.0
Preparation: N/A
MS Lab Sample ID:
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
660-27893-41
Water
2.0
03/04/2009 1450
N/A
Analysis Batch: 660-75752
Prep Batch: N/A
Instrument ID: ICS 2000
Lab File ID:
N/A
Initial Weight/Volume:
Final Weight/Volume: 5 mL
MSD Lab Sample ID:
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
660-27893-41
Water
2.0
03/04/2009 1502
N/A
Analysis Batch: 660-75752
Prep Batch: N/A
Instrument ID: ICS 2000
Lab File ID:
N/A
Initial Weight/Volume:
Final Weight/Volume: 5 mL
Analyte
MS
Chloride
Sulfate
656
178
% Rec.
MSD
664
179
Limit
RPD
RPD Limit
MS Qual MSD Qual
90 - 110
90 - 110
0
0
30
30
J3
J3
J3
J3
Calculations are performed before rounding to avoid round-off errors in calculated results.
TestAmerica Tampa
Page 203 of 221
04/06/2009
Quality Control Results
Client: ARCADIS U.S., Inc.
Job Number: 660-27893-1
Method Blank - Batch: 660-75441
Lab Sample ID:
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
MB 660-75441/1
Water
1.0
02/26/2009 0841
N/A
Method: 353.2
Preparation: N/A
Analysis Batch: 660-75441
Prep Batch: N/A
Units: mg/L
Instrument ID: No Equipment Assigned
Lab File ID:
N/A
Initial Weight/Volume: 50 mL
Final Weight/Volume: 50 mL
Analyte
Result
Qual
MDL
PQL
Nitrite as N
Nitrate as N
0.10
0.10
U
U
0.10
0.10
0.50
0.50
Lab Control Spike - Batch: 660-75441
Lab Sample ID:
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
LCS 660-75441/2
Water
1.0
02/26/2009 0841
N/A
Method: 353.2
Preparation: N/A
Analysis Batch: 660-75441
Prep Batch: N/A
Units: mg/L
Instrument ID: No Equipment Assigned
Lab File ID:
N/A
Initial Weight/Volume: 100 mL
Final Weight/Volume: 100 mL
Analyte
Spike Amount
Result
% Rec.
Limit
Nitrite as N
1.00
0.923
92
90 - 110
Qual
Calculations are performed before rounding to avoid round-off errors in calculated results.
TestAmerica Tampa
Page 204 of 221
04/06/2009
Quality Control Results
Client: ARCADIS U.S., Inc.
Job Number: 660-27893-1
Matrix Spike/
Matrix Spike Duplicate Recovery Report - Batch: 660-75441
Method: 353.2
Preparation: N/A
MS Lab Sample ID:
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
660-27852-Z-1 MS
Water
1.0
02/26/2009 0841
N/A
Analysis Batch: 660-75441
Prep Batch: N/A
Instrument ID: No Equipment Assigned
Lab File ID:
N/A
Initial Weight/Volume: 50 mL
Final Weight/Volume: 50 mL
MSD Lab Sample ID:
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
660-27852-Z-1 MSD
Water
1.0
02/26/2009 0841
N/A
Analysis Batch: 660-75441
Prep Batch: N/A
Instrument ID: No Equipment Assigned
Lab File ID:
N/A
Initial Weight/Volume: 50 mL
Final Weight/Volume: 50 mL
Analyte
MS
Nitrite as N
110
% Rec.
MSD
97
Limit
RPD
RPD Limit
90 - 110
12
30
MS Qual MSD Qual
Calculations are performed before rounding to avoid round-off errors in calculated results.
TestAmerica Tampa
Page 205 of 221
04/06/2009
Quality Control Results
Client: ARCADIS U.S., Inc.
Job Number: 660-27893-1
Method Blank - Batch: 660-75644
Lab Sample ID:
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
MB 660-75644/1
Water
1.0
03/02/2009 1303
03/02/2009 1303
Method: 353.2
Preparation: 353.2
Analysis Batch: 660-75644
Prep Batch: N/A
Units: mg/L
Instrument ID: No Equipment Assigned
Lab File ID:
N/A
Initial Weight/Volume: 50 mL
Final Weight/Volume: 50 mL
Analyte
Result
Qual
MDL
PQL
Nitrate Nitrite as N
0.10
U
0.10
0.50
Lab Control Spike - Batch: 660-75644
Lab Sample ID:
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
LCS 660-75644/2
Water
1.0
03/02/2009 1303
03/02/2009 1303
Method: 353.2
Preparation: 353.2
Analysis Batch: 660-75644
Prep Batch: N/A
Units: mg/L
Instrument ID: No Equipment Assigned
Lab File ID:
N/A
Initial Weight/Volume: 100 mL
Final Weight/Volume: 100 mL
Analyte
Spike Amount
Result
% Rec.
Limit
Qual
Nitrate Nitrite as N
1.00
0.972
97
90 - 110
Matrix Spike/
Matrix Spike Duplicate Recovery Report - Batch: 660-75644
Method: 353.2
Preparation: 353.2
MS Lab Sample ID:
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
660-27893-48
Water
1.0
03/02/2009 1303
03/02/2009 1303
Analysis Batch: 660-75644
Prep Batch: N/A
Instrument ID: No Equipment Assigned
Lab File ID:
N/A
Initial Weight/Volume: 50 mL
Final Weight/Volume: 50 mL
MSD Lab Sample ID:
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
660-27893-48
Water
1.0
03/02/2009 1303
03/02/2009 1303
Analysis Batch: 660-75644
Prep Batch: N/A
Instrument ID: No Equipment Assigned
Lab File ID:
N/A
Initial Weight/Volume: 50 mL
Final Weight/Volume: 50 mL
Analyte
MS
Nitrate Nitrite as N
96
% Rec.
MSD
88
Limit
RPD
RPD Limit
90 - 110
8
30
MS Qual MSD Qual
J3
Calculations are performed before rounding to avoid round-off errors in calculated results.
TestAmerica Tampa
Page 206 of 221
04/06/2009
Quality Control Results
Client: ARCADIS U.S., Inc.
Job Number: 660-27893-1
Method Blank - Batch: 660-75553
Lab Sample ID:
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
MB 660-75553/3
Water
1.0
02/27/2009 1037
N/A
Method: SM 2320B
Preparation: N/A
Analysis Batch: 660-75553
Prep Batch: N/A
Units: mg/L
Instrument ID: Titrator Instrument
Lab File ID:
N/A
Initial Weight/Volume: 50 mL
Final Weight/Volume: 50 mL
Analyte
Result
Qual
PQL
PQL
Alkalinity
Bicarbonate Alkalinity as CaCO3
Carbonate Alkalinity as CaCO3
Hydroxide Alkalinity
Phenolphthalein Alkalinity
1.0
1.0
1.0
1.0
1.0
U
U
U
U
U
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
Lab Control Spike - Batch: 660-75553
Lab Sample ID:
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
LCS 660-75553/4
Water
1.0
02/27/2009 1045
N/A
Method: SM 2320B
Preparation: N/A
Analysis Batch: 660-75553
Prep Batch: N/A
Units: mg/L
Instrument ID: Titrator Instrument
Lab File ID:
N/A
Initial Weight/Volume: 50 mL
Final Weight/Volume: 50 mL
Analyte
Spike Amount
Result
% Rec.
Limit
Alkalinity
118
124
105
80 - 120
Duplicate - Batch: 660-75553
Lab Sample ID:
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
660-27893-46
Water
1.0
02/27/2009 1322
N/A
Qual
Method: SM 2320B
Preparation: N/A
Analysis Batch: 660-75553
Prep Batch: N/A
Units: mg/L
Instrument ID: Titrator Instrument
Lab File ID:
N/A
Initial Weight/Volume: 50 mL
Final Weight/Volume: 50 mL
Analyte
Sample Result/Qual
Result
RPD
Alkalinity
Bicarbonate Alkalinity as CaCO3
Carbonate Alkalinity as CaCO3
Hydroxide Alkalinity
Phenolphthalein Alkalinity
130
130
1.0
1.0
1.0
138
138
1.0
1.0
1.0
2.36
2.36
NC
NC
NC
U
U
U
Limit
Qual
U
U
U
Calculations are performed before rounding to avoid round-off errors in calculated results.
TestAmerica Tampa
Page 207 of 221
04/06/2009
Quality Control Results
Client: ARCADIS U.S., Inc.
Job Number: 660-27893-1
Method Blank - Batch: 660-75622
Lab Sample ID:
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
MB 660-75622/3
Water
1.0
03/02/2009 0907
N/A
Method: SM 2320B
Preparation: N/A
Analysis Batch: 660-75622
Prep Batch: N/A
Units: mg/L
Instrument ID: Titrator Instrument
Lab File ID:
N/A
Initial Weight/Volume: 50 mL
Final Weight/Volume: 50 mL
Analyte
Result
Qual
PQL
PQL
Alkalinity
Bicarbonate Alkalinity as CaCO3
Carbonate Alkalinity as CaCO3
Hydroxide Alkalinity
Phenolphthalein Alkalinity
1.0
1.0
1.0
1.0
1.0
U
U
U
U
U
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
Lab Control Spike - Batch: 660-75622
Lab Sample ID:
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
LCS 660-75622/4
Water
1.0
03/02/2009 0915
N/A
Method: SM 2320B
Preparation: N/A
Analysis Batch: 660-75622
Prep Batch: N/A
Units: mg/L
Instrument ID: Titrator Instrument
Lab File ID:
N/A
Initial Weight/Volume: 50 mL
Final Weight/Volume: 50 mL
Analyte
Spike Amount
Result
% Rec.
Limit
Alkalinity
118
127
108
80 - 120
Duplicate - Batch: 660-75622
Lab Sample ID:
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
660-27893-47
Water
1.0
03/02/2009 0925
N/A
Qual
Method: SM 2320B
Preparation: N/A
Analysis Batch: 660-75622
Prep Batch: N/A
Units: mg/L
Instrument ID: Titrator Instrument
Lab File ID:
N/A
Initial Weight/Volume: 50 mL
Final Weight/Volume: 50 mL
Analyte
Sample Result/Qual
Result
RPD
Alkalinity
Bicarbonate Alkalinity as CaCO3
Carbonate Alkalinity as CaCO3
Hydroxide Alkalinity
Phenolphthalein Alkalinity
61
61
1.0
1.0
1.0
60.5
60.5
1.0
1.0
1.0
0.0330
0.0330
NC
NC
NC
U
U
U
Limit
Qual
U
U
U
Calculations are performed before rounding to avoid round-off errors in calculated results.
TestAmerica Tampa
Page 208 of 221
04/06/2009
Quality Control Results
Client: ARCADIS U.S., Inc.
Job Number: 660-27893-1
Method Blank - Batch: 640-54348
Lab Sample ID:
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
MB 640-54348/1
Water
1.0
02/27/2009 1212
N/A
Method: SM 2540C
Preparation: N/A
Analysis Batch: 640-54348
Prep Batch: N/A
Units: mg/L
Instrument ID: No Equipment Assigned
Lab File ID:
N/A
Initial Weight/Volume: 200 mL
Final Weight/Volume: 200 mL
Analyte
Result
Qual
MDL
PQL
Total Dissolved Solids
5.0
U
5.0
5.0
Lab Control Spike/
Lab Control Spike Duplicate Recovery Report - Batch: 640-54348
Method: SM 2540C
Preparation: N/A
LCS Lab Sample ID: LCS 640-54348/2
Client Matrix:
Water
Dilution:
1.0
02/27/2009 1212
Date Analyzed:
Date Prepared:
N/A
Analysis Batch: 640-54348
Prep Batch: N/A
Units: mg/L
Instrument ID: No Equipment Assigned
Lab File ID: N/A
Initial Weight/Volume:
100 mL
Final Weight/Volume:
200 mL
LCSD Lab Sample ID: LCSD 640-54348/3
Client Matrix:
Water
Dilution:
1.0
02/27/2009 1212
Date Analyzed:
Date Prepared:
N/A
Analysis Batch: 640-54348
Prep Batch: N/A
Units: mg/L
Instrument ID:
No Equipment Assigned
Lab File ID:
N/A
Initial Weight/Volume: 100 mL
Final Weight/Volume: 200 mL
Analyte
LCS
Total Dissolved Solids
98
% Rec.
LCSD
102
Limit
RPD
RPD Limit
80 - 120
4
25
LCS Qual LCSD Qual
Calculations are performed before rounding to avoid round-off errors in calculated results.
TestAmerica Tampa
Page 209 of 221
04/06/2009
Quality Control Results
Client: ARCADIS U.S., Inc.
Job Number: 660-27893-1
Duplicate - Batch: 640-54348
Lab Sample ID:
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
660-27893-41
Water
1.0
02/27/2009 1212
N/A
Method: SM 2540C
Preparation: N/A
Analysis Batch: 640-54348
Prep Batch: N/A
Units: mg/L
Instrument ID: No Equipment Assigned
Lab File ID:
N/A
Initial Weight/Volume: 100 mL
Final Weight/Volume: 200 mL
Analyte
Sample Result/Qual
Result
RPD
Limit
Total Dissolved Solids
580
592
2
25
Qual
Calculations are performed before rounding to avoid round-off errors in calculated results.
TestAmerica Tampa
Page 210 of 221
04/06/2009
Quality Control Results
Client: ARCADIS U.S., Inc.
Job Number: 660-27893-1
Method Blank - Batch: 640-54352
Lab Sample ID:
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
MB 640-54352/1
Water
1.0
02/27/2009 1228
N/A
Method: SM 2540D
Preparation: N/A
Analysis Batch: 640-54352
Prep Batch: N/A
Units: mg/L
Instrument ID: No Equipment Assigned
Lab File ID:
N/A
Initial Weight/Volume: 1000 mL
Final Weight/Volume: 200 mL
Analyte
Result
Qual
MDL
PQL
Total Suspended Solids
0.48
U
0.48
1.0
Lab Control Spike/
Lab Control Spike Duplicate Recovery Report - Batch: 640-54352
Method: SM 2540D
Preparation: N/A
LCS Lab Sample ID: LCS 640-54352/2
Client Matrix:
Water
Dilution:
1.0
02/27/2009 1228
Date Analyzed:
Date Prepared:
N/A
Analysis Batch: 640-54352
Prep Batch: N/A
Units: mg/L
Instrument ID: No Equipment Assigned
Lab File ID: N/A
Initial Weight/Volume:
200 mL
Final Weight/Volume:
200 mL
LCSD Lab Sample ID: LCSD 640-54352/3
Client Matrix:
Water
Dilution:
1.0
02/27/2009 1228
Date Analyzed:
Date Prepared:
N/A
Analysis Batch: 640-54352
Prep Batch: N/A
Units: mg/L
Instrument ID:
No Equipment Assigned
Lab File ID:
N/A
Initial Weight/Volume: 200 mL
Final Weight/Volume: 200 mL
Analyte
LCS
Total Suspended Solids
90
% Rec.
LCSD
90
Limit
RPD
RPD Limit
80 - 120
0
25
LCS Qual LCSD Qual
Calculations are performed before rounding to avoid round-off errors in calculated results.
TestAmerica Tampa
Page 211 of 221
04/06/2009
Quality Control Results
Client: ARCADIS U.S., Inc.
Job Number: 660-27893-1
Duplicate - Batch: 640-54352
Lab Sample ID:
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
660-27893-41
Water
1.0
02/27/2009 1228
N/A
Method: SM 2540D
Preparation: N/A
Analysis Batch: 640-54352
Prep Batch: N/A
Units: mg/L
Instrument ID: No Equipment Assigned
Lab File ID:
N/A
Initial Weight/Volume: 200 mL
Final Weight/Volume: 200 mL
Analyte
Sample Result/Qual
Result
RPD
Limit
Total Suspended Solids
65
58.5
11
25
Qual
Calculations are performed before rounding to avoid round-off errors in calculated results.
TestAmerica Tampa
Page 212 of 221
04/06/2009
Quality Control Results
Client: ARCADIS U.S., Inc.
Job Number: 660-27893-1
Method Blank - Batch: 660-75561
Lab Sample ID:
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
MB 660-75561/1-A
Water
1.0
02/27/2009 1500
02/27/2009 1220
Method: SM 5220D
Preparation: SM 5220
Analysis Batch: 660-75563
Prep Batch: 660-75561
Units: mg/L
Instrument ID: No Equipment Assigned
Lab File ID:
N/A
Initial Weight/Volume: 2 mL
Final Weight/Volume: 2 mL
Analyte
Result
Qual
MDL
PQL
Chemical Oxygen Demand
10
U
10
20
Lab Control Spike - Batch: 660-75561
Lab Sample ID:
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
LCS 660-75561/2-A
Water
1.0
02/27/2009 1500
02/27/2009 1220
Method: SM 5220D
Preparation: SM 5220
Analysis Batch: 660-75563
Prep Batch: 660-75561
Units: mg/L
Instrument ID: No Equipment Assigned
Lab File ID:
N/A
Initial Weight/Volume: 2 mL
Final Weight/Volume: 2 mL
Analyte
Spike Amount
Result
% Rec.
Limit
Qual
Chemical Oxygen Demand
50.0
52.2
104
90 - 110
Matrix Spike/
Matrix Spike Duplicate Recovery Report - Batch: 660-75561
Method: SM 5220D
Preparation: SM 5220
MS Lab Sample ID:
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
660-27893-45
Water
1.0
02/27/2009 1500
02/27/2009 1220
Analysis Batch: 660-75563
Prep Batch: 660-75561
Instrument ID: No Equipment Assigned
Lab File ID:
N/A
Initial Weight/Volume: 2 mL
Final Weight/Volume: 2 mL
MSD Lab Sample ID:
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
660-27893-45
Water
1.0
02/27/2009 1500
02/27/2009 1220
Analysis Batch: 660-75563
Prep Batch: 660-75561
Instrument ID: No Equipment Assigned
Lab File ID:
N/A
Initial Weight/Volume: 2 mL
Final Weight/Volume: 2 mL
Analyte
MS
Chemical Oxygen Demand
94
% Rec.
MSD
92
Limit
RPD
RPD Limit
90 - 110
2
20
MS Qual MSD Qual
Calculations are performed before rounding to avoid round-off errors in calculated results.
TestAmerica Tampa
Page 213 of 221
04/06/2009
Quality Control Results
Client: ARCADIS U.S., Inc.
Job Number: 660-27893-1
Method Blank - Batch: 660-75675
Lab Sample ID:
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
MB 660-75675/5
Water
1.0
03/02/2009 1936
N/A
Method: SM 5310C
Preparation: N/A
Analysis Batch: 660-75675
Prep Batch: N/A
Units: mg/L
Instrument ID: Teledyne TOC Analyzer
Lab File ID:
03021812
Initial Weight/Volume:
Final Weight/Volume: 40 mL
Analyte
Result
Qual
MDL
PQL
Total Organic Carbon
0.53
U
0.53
1.0
Lab Control Spike - Batch: 660-75675
Lab Sample ID:
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
LCS 660-75675/6
Water
1.0
03/02/2009 1958
N/A
Method: SM 5310C
Preparation: N/A
Analysis Batch: 660-75675
Prep Batch: N/A
Units: mg/L
Instrument ID: Teledyne TOC Analyzer
Lab File ID:
03021812
Initial Weight/Volume:
Final Weight/Volume: 40 mL
Analyte
Spike Amount
Result
% Rec.
Limit
Qual
Total Organic Carbon
10.0
9.08
91
80 - 120
Matrix Spike/
Matrix Spike Duplicate Recovery Report - Batch: 660-75675
Method: SM 5310C
Preparation: N/A
MS Lab Sample ID:
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
660-27893-43
Water
1.0
03/02/2009 2141
N/A
Analysis Batch: 660-75675
Prep Batch: N/A
Instrument ID: Teledyne TOC Analyzer
Lab File ID:
03021812
Initial Weight/Volume:
Final Weight/Volume: 40 mL
MSD Lab Sample ID:
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
660-27893-43
Water
1.0
03/02/2009 2208
N/A
Analysis Batch: 660-75675
Prep Batch: N/A
Instrument ID: Teledyne TOC Analyzer
Lab File ID:
03021812
Initial Weight/Volume:
Final Weight/Volume: 40 mL
Analyte
MS
Total Organic Carbon
91
% Rec.
MSD
90
Limit
RPD
RPD Limit
80 - 120
0
25
MS Qual MSD Qual
Calculations are performed before rounding to avoid round-off errors in calculated results.
TestAmerica Tampa
Page 214 of 221
04/06/2009
Page 215 of 221
04/06/2009
Page 216 of 221
04/06/2009
Page 217 of 221
04/06/2009
Page 218 of 221
04/06/2009
Page 219 of 221
04/06/2009
Login Sample Receipt Check List
Client: ARCADIS U.S., Inc.
Job Number: 660-27893-1
Login Number: 27893
Creator: Harrison, Amanda
List Number: 1
List Source: TestAmerica Tampa
Question
T / F/ NA
Radioactivity either was not measured or, if measured, is at or below
background
The cooler's custody seal, if present, is intact.
N/A
The cooler or samples do not appear to have been compromised or
tampered with.
Samples were received on ice.
Cooler Temperature is acceptable.
True
Cooler Temperature is recorded.
COC is present.
COC is filled out in ink and legible.
COC is filled out with all pertinent information.
There are no discrepancies between the sample IDs on the containers and
the COC.
Samples are received within Holding Time.
Sample containers have legible labels.
Containers are not broken or leaking.
True
True
True
True
True
Sample collection date/times are provided.
Appropriate sample containers are used.
Sample bottles are completely filled.
There is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
VOA sample vials do not have headspace or bubble is <6mm (1/4") in
diameter.
If necessary, staff have been informed of any short hold time or quick TAT
needs
Multiphasic samples are not present.
Samples do not require splitting or compositing.
True
True
True
True
TestAmerica Tampa
Comment
N/A
True
True
2.9, 3.6, 3.1, and 4.0 degrees C CU-07
True
True
True
True
True
True
True
Page 220 of 221
04/06/2009
Login Sample Receipt Check List
Client: ARCADIS U.S., Inc.
Job Number: 660-27893-1
Login Number: 27893
Creator: Jones, Daniella
List Number: 1
List Source: TestAmerica Tallahassee
List Creation: 02/27/09 08:04 AM
Question
T / F/ NA
Radioactivity either was not measured or, if measured, is at or below
background
The cooler's custody seal, if present, is intact.
N/A
The cooler or samples do not appear to have been compromised or
tampered with.
Samples were received on ice.
Cooler Temperature is acceptable.
True
Cooler Temperature is recorded.
COC is present.
COC is filled out in ink and legible.
COC is filled out with all pertinent information.
There are no discrepancies between the sample IDs on the containers and
the COC.
Samples are received within Holding Time.
Sample containers have legible labels.
Containers are not broken or leaking.
True
True
True
True
True
Sample collection date/times are provided.
Appropriate sample containers are used.
Sample bottles are completely filled.
There is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
VOA sample vials do not have headspace or bubble is <6mm (1/4") in
diameter.
If necessary, staff have been informed of any short hold time or quick TAT
needs
Multiphasic samples are not present.
Samples do not require splitting or compositing.
True
True
True
True
TestAmerica Tampa
Comment
True
True
True
True
True
True
N/A
True
True
True
Page 221 of 221
04/06/2009
MONITOR WELL CONSTRUCTION SCHEMATIC DIAGRAM
Client
Raytheon
Site Location St. Petersburg Fl
Well Location Median of 68th St N, 490 ft south of 68th St N & Crosswind Dr, St. Petersburg FL
Project No.
TF00922.0043
Contractor
PDS
Driller(s) Jon, Sergio, Eucoio
Drilling Method(s)
Direct Push
Prepared By
M. Sedor
Date(s) Installed
11/13/2009
Monitor Well No.
DMW-CC
Survey
Datum
Ground
Elevation
Type of Protective Cover
8" Manhole
Type of Riser Pipe
1" Sch 40 PVC
Diameter of Borehole
1.5 inches
Type of Grout Around Riser Pipe
Portland Type I/II Cement Grout
Depth Top of Seal
44 feet
Type of Seal
Prepacked bentonite
Depth Bottom of Seal
47 feet
Depth Top of Screen
under 30/65
silica sand
47 feet
Screen Section Material
Screen Size
1" Sch 40 PVC
0.01
Type of Sand Pack Around Screen
20/30 silica prepacked sand
Depth Bottom of Screen
47 feet
Depth Bottom of Borehole/Sandpack
50 feet
REMARKS:
PROJ\FORMS\FIELD\DMW-CC Construction.xlsx
Florida Department of Environmental Protection - Division of Waste Management - Bureau of Petroleum Storage Systems
WELL CONSTRUCTION AND DEVELOPMENT LOG
WELL CONSTRUCTION DATA
Site Name:
Well Number:
DMW-CC
Well Location and Type (check appropriate boxes):
On-Site
FDEP Facility I.D. Number:
RAYTHEON
Well Purpose:
Right-of-Way
Perched Monitoring
Shallow (Water-T able ) Monitoring
Flush-to-Grade
Intermediate or Deep Monit
Monitoring
oring
Remediation or Other (describe)
Off-Site Private Property
Above Grade (AG)
Well Install Date(s):
11/13/09
Well Install Method:
Direct Push
Surface Casing Install Method:
N/A
If AG, list feet of riser above land surface:
Well Depth
Borehole Depth
55
(feet):
Borehole Diameter Manhole Diameter
52
(feet):
(inches):
2.5
Riser/Screen
Connections:
Riser Diameter and Material:
1" Schedule 40 PVC
Screen Diameter and Material:
Permanent
2 Surface Casing Material:
Permanent
Permanent
N/A
3 Surface Casing Material:
Permanent
Permanent
3 Surface Casing I.D. (inches):
Yes
Filter Pack Seal Material and
Size:
0
from
Surface Seal Material:
/ C
Portland type I/II
Cement G
Grout
feet to
5
52
feet to
3
Filter Pack Seal Length:
from
47
feet to
44
Surface Seal Length:
from
feet
feet
Filter Pack Length:
No
2' prepacked bentonite packer below 1' of 30/65
Silica Sand
feet to
3 Surface Casing Length:
from
Filter Pack Material and Size: Prepacked Filter Around Screen (check one):
20/30 Silica Sand
0
feet
feet
rd
T emporary
feet
47 feet
feet to
2 Surface Casing Length:
from
rd
0
feet
nd
T emporary
rd
also check:
2 Surface Casing I.D. (inches):
N/A
feet to
0
from
nd
feet
feet
52
1st Surface Casing Length:
T emporary
nd
also check:
1st Surface Casing I.D. (inches):
N/A
feet to
5
from
2
feet
47
Screen Length:
0.01
by
47
from
Other (describe)
Screen Slot Size:
1st Surface Casing Material:
feet
Riser Length:
Flush-T hreaded
1" Schedule 40 PVC
also check:
8
(inches):
Well Pad Size:
2
44
feet to
feet
feet
47 feet
feet
44 feet
feet
0 feet
WELL DEVELOPMENT DATA
Well Development Date:
Well Development Method (check one):
Development Pump Type (check):
Submersible
Centrifugal
Peristaltic
Pump
Compressed Air
Depth to Groundwater (before developing in feet):
Other (describe)
Pumping Rate (gallons per minute):
~0.7
Pumping Condition (check one):
Continuous
Surge/Pump
Other (describe)
11/16/09
Intermittent
Maximum Drawdown of Groundwater During
Development (feet):
N/A
Total Development Water
Removed (gallons):
Water Appearance (color and odor) At Start of Development:
Brown
25
3.70
Well Purged Dry (check one):
Yes
No
Development Duration Development Water Drummed
(check one):
(minutes):
Yes
35
Water Appearance (color and odor) At End of Development:
Clear
WELL CONSTRUCTION OR DEVELOPMENT REMARKS
No
MONITOR WELL CONSTRUCTION SCHEMATIC DIAGRAM
Client
Raytheon
Site Location St. Petersburg Fl
Well Location Median of 68th St N, 490 ft south of 68th St N & Crosswind Dr, St. Petersburg FL
Project No.
TF00922.0043
Contractor
PDS
Driller(s) Jon, Sergio, Eucoio
Drilling Method(s)
Direct Push
Prepared By
M. Sedor
Date(s) Installed
11/13/2009
Monitor Well No.
IMW-V
Survey
Datum
Ground
Elevation
Type of Protective Cover
8" Manhole
Type of Riser Pipe
1" Sch 40 PVC
Diameter of Borehole
1.5 inches
Type of Grout Around Riser Pipe
Portland Type I/II Cement Grout
Depth Top of Seal
31 feet
Type of Seal
30/65 silica sand
Depth Bottom of Seal
33 feet
Depth Top of Screen
34 feet
Screen Section Material
Screen Size
1" Sch 40 PVC
0.01
Type of Sand Pack Around Screen
20/30 silica prepacked sand+poured sand
Depth Bottom of Screen
39 feet
Depth Bottom of Borehole/Sandpack
39 feet
REMARKS:
PROJ\FORMS\FIELD\IMW-V Construction.xlsx
Florida Department of Environmental Protection - Division of Waste Management - Bureau of Petroleum Storage Systems
WELL CONSTRUCTION AND DEVELOPMENT LOG
WELL CONSTRUCTION DATA
Site Name:
Well Number:
IMW-V
Well Location and Type (check appropriate boxes):
On-Site
FDEP Facility I.D. Number:
RAYTHEON
Well Purpose:
Right-of-Way
Perched Monitoring
Shallow (Water-T able ) Monitoring
Flush-to-Grade
Intermediate or Deep Monit
Monitoring
oring
Remediation or Other (describe)
Off-Site Private Property
Above Grade (AG)
Well Install Date(s):
11/13/09
Well Install Method:
Direct Push
Surface Casing Install Method:
N/A
If AG, list feet of riser above land surface:
Well Depth
Borehole Depth
39
(feet):
Borehole Diameter Manhole Diameter
39
(feet):
(inches):
2.5
Riser/Screen
Connections:
Riser Diameter and Material:
1" Schedule 40 PVC
Screen Diameter and Material:
Permanent
2 Surface Casing Material:
Permanent
Permanent
N/A
3 Surface Casing Material:
Permanent
Permanent
3 Surface Casing I.D. (inches):
Yes
Filter Pack Seal Material and
Size:
feet to
0
feet to
6
Filter Pack Length:
No
from
39
feet to
2
Filter Pack Seal Length:
30/65 Silica Sand
from
Surface Seal Material:
/ C
Portland type I/II
Cement G
Grout
33
feet to
44
Surface Seal Length:
from
feet
feet
3 Surface Casing Length:
from
Filter Pack Material and Size: Prepacked Filter Around Screen (check one):
20/30 Silica Sand
0
feet
feet
rd
T emporary
feet
34 feet
feet to
2 Surface Casing Length:
from
rd
0
feet
nd
T emporary
rd
also check:
2 Surface Casing I.D. (inches):
N/A
feet to
0
from
nd
feet
feet
39
1st Surface Casing Length:
T emporary
nd
also check:
1st Surface Casing I.D. (inches):
N/A
feet to
5
from
2
feet
34
Screen Length:
0.01
by
34
from
Other (describe)
Screen Slot Size:
1st Surface Casing Material:
feet
Riser Length:
Flush-T hreaded
1" Schedule 40 PVC
also check:
8
(inches):
Well Pad Size:
2
31
feet to
feet
feet
33 feet
feet
31 feet
feet
0 feet
WELL DEVELOPMENT DATA
Well Development Date:
Well Development Method (check one):
Development Pump Type (check):
Submersible
Centrifugal
Peristaltic
Pump
Compressed Air
Depth to Groundwater (before developing in feet):
Other (describe)
Pumping Rate (gallons per minute):
~0.7
Pumping Condition (check one):
Continuous
Surge/Pump
Other (describe)
11/16/09
Intermittent
Maximum Drawdown of Groundwater During
Development (feet):
N/A
Total Development Water
Removed (gallons):
Water Appearance (color and odor) At Start of Development:
Brown
20
4.35
Well Purged Dry (check one):
Yes
No
Development Duration Development Water Drummed
(check one):
(minutes):
Yes
30
Water Appearance (color and odor) At End of Development:
Clear
WELL CONSTRUCTION OR DEVELOPMENT REMARKS
Note that the prepacked filter was 5 feet, but was surrounded by 6 feet of poured filter pack below the seal
No
ANALYTICAL REPORT
Job Number: 660-32642-1
Job Description: Raytheon
For:
ARCADIS U.S., Inc.
14055 Riveredge Drive
Suite 400
Tampa, FL 33637
Attention: Mr. Gus Suarez
_____________________________________________
Approved for release.
Natalie Tafuni
Project Manager I
11/30/2009 3:31 PM
Natalie Tafuni
Project Manager I
[email protected]
11/30/2009
cc:
Ms. Lyndi Mott
Mr. Melvin Rivera
Albert Zumbuhl
Methods: FDEP, DOH Certification #: TestAmerica Tampa E84282
These test results meet all the requirements of NELAC unless specified in the case narrative. All questions regarding
this test report should be directed to the TestAmerica Project Manager who signed this test report. The estimated
uncertainty associated with these reported results is available upon request. The results contained in this test report
relate only to these samples included herein.
TestAmerica Laboratories, Inc.
TestAmerica Tampa 6712 Benjamin Road, Suite 100, Tampa, FL 33634
Tel (813) 885-7427 Fax (813) 885-7049 www.testamericainc.com
Page 1 of 31
Job Narrative
660-32642-1
Comments
No additional comments.
Receipt
All samples were received in good condition within temperature requirements.
8260B
The laboratory control sample (LCS) for batch 660-87646 was outside of control limits for MIBK and 2-hexanone. These compounds are
biased high in the LCS and the samples are non detect for MIBK and 2-hexanone. The data are flagged with J3 qualifiers.
The batch matrix spike (MS) for batch 660-87646(job 660-32564) was outside of control limits for cis-1,3 dichloropropene, MIBK and
2-hexanone. The laboratory control sample (LCS) was withinn control criteria except as noted above. The data are flagged with J3
qualifiers.
The sample duplicate %RPD for batch 660-87646 has a result of NC for most compounds. The sample result and the sample duplicate
result are both Non-detect for these compounds. The Laboratory LIMs system flags the %RPD in this scenario as NC, or "not calculated".
8260C
The batch matrix spike (MS) for batch 660-87653(job 660-32643) was over calibration range for 1,4-dioxane. The data are flagged with L
qualifiers.
Page 2 of 31
EXECUTIVE SUMMARY - Detections
Client: ARCADIS U.S., Inc.
Lab Sample ID
Analyte
660-32642-1
Carbon disulfide
1,4-Dioxane
Job Number: 660-32642-1
Client Sample ID
Result / Qualifier
Reporting
Limit
Units
Method
ug/L
ug/L
8260B
8260C _SIM/ID
IMW-V_111909
0.93
5.7
I
TestAmerica Tampa
Page 3 of 31
1.0
2.0
METHOD SUMMARY
Client: ARCADIS U.S., Inc.
Description
Job Number: 660-32642-1
Lab Location Method
Preparation Method
Volatile Organic Compounds (GC/MS)
Purge and Trap
TAL TAM
TAL TAM
SW846 8260B
SW846 5030B
1,4-Dioxane by SIM/Isotopic Dilution
Purge and Trap
TAL TAM
TAL TAM
SW846 8260C _SIM/ID
SW846 5030C
Matrix
Water
Lab References:
TAL TAM = TestAmerica Tampa
Method References:
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its
Updates.
TestAmerica Tampa
Page 4 of 31
METHOD / ANALYST SUMMARY
Client: ARCADIS U.S., Inc.
Job Number: 660-32642-1
Method
Analyst
SW846 8260B
Perrin, Todd
TP
SW846 8260C _SIM/ID
Perrin, Todd
TP
TestAmerica Tampa
Page 5 of 31
Analyst ID
SAMPLE SUMMARY
Client: ARCADIS U.S., Inc.
Job Number: 660-32642-1
Lab Sample ID
Client Sample ID
Client Matrix
660-32642-1
660-32642-2
660-32642-3
IMW-V_111909
DMW-CC_111909
Trip Blank#4_111909
Water
Water
Water
TestAmerica Tampa
Page 6 of 31
Date/Time
Sampled
Date/Time
Received
11/19/2009 1638
11/19/2009 1715
11/19/2009 0000
11/20/2009 1045
11/20/2009 1045
11/20/2009 1045
SAMPLE RESULTS
TestAmerica Tampa
Page 7 of 31
Analytical Data
Client: ARCADIS U.S., Inc.
Client Sample ID:
IMW-V_111909
Lab Sample ID:
Client Matrix:
660-32642-1
Water
Job Number: 660-32642-1
Date Sampled: 11/19/2009 1638
Date Received: 11/20/2009 1045
8260B Volatile Organic Compounds (GC/MS)
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260B
5030B
1.0
11/20/2009 1832
11/20/2009 1832
Analyte
Benzene
Bromobenzene
1,2-Dichlorobenzene
Chlorobromomethane
Dichlorobromomethane
Bromoform
Bromomethane
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
Chlorodibromomethane
1,2-Dibromo-3-Chloropropane
Ethylene Dibromide
Dibromomethane
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
Hexachlorobutadiene
Isopropylbenzene
4-Isopropyltoluene
Methylene Chloride
Naphthalene
N-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
TestAmerica Tampa
Analysis Batch: 660-87646
Result (ug/L)
0.50
0.58
0.44
0.58
0.35
0.58
2.5
0.67
0.63
0.84
0.42
0.63
2.5
0.90
1.0
0.65
0.52
0.34
2.5
0.50
0.41
0.64
0.52
2.5
0.52
0.57
0.45
0.65
0.44
0.52
0.39
0.36
0.31
0.14
0.14
0.44
0.40
0.19
0.69
4.0
2.5
0.59
0.98
0.63
0.15
0.50
Page 8 of 31
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Qualifier
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
MDL
0.50
0.58
0.44
0.58
0.35
0.58
2.5
0.67
0.63
0.84
0.42
0.63
2.5
0.90
1.0
0.65
0.52
0.34
2.5
0.50
0.41
0.64
0.52
2.5
0.52
0.57
0.45
0.65
0.44
0.52
0.39
0.36
0.31
0.14
0.14
0.44
0.40
0.19
0.69
4.0
2.5
0.59
0.98
0.63
0.15
0.50
BVMH5973
1HK2024.D
5 mL
5 mL
PQL
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
4.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
5.0
1.0
2.0
1.0
1.0
1.0
Analytical Data
Client: ARCADIS U.S., Inc.
Client Sample ID:
IMW-V_111909
Lab Sample ID:
Client Matrix:
660-32642-1
Water
Job Number: 660-32642-1
Date Sampled: 11/19/2009 1638
Date Received: 11/20/2009 1045
8260B Volatile Organic Compounds (GC/MS)
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260B
5030B
1.0
11/20/2009 1832
11/20/2009 1832
Analysis Batch: 660-87646
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Analyte
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
o-Xylene
Acetone
2-Butanone (MEK)
4-Methyl-2-pentanone (MIBK)
Carbon disulfide
2-Hexanone
Methyl tert-butyl ether
m-Xylene & p-Xylene
Result (ug/L)
0.51
0.77
0.58
0.46
0.47
0.50
2.5
0.18
0.86
0.54
0.50
0.50
9.9
8.4
3.8
0.93
4.4
0.44
0.60
Qualifier
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U J3
I
U J3
U
U
Surrogate
Toluene-d8 (Surr)
4-Bromofluorobenzene
Dibromofluoromethane
%Rec
111
95
93
Qualifier
TestAmerica Tampa
Page 9 of 31
MDL
0.51
0.77
0.58
0.46
0.47
0.50
2.5
0.18
0.86
0.54
0.50
0.50
9.9
8.4
3.8
0.85
4.4
0.44
0.60
BVMH5973
1HK2024.D
5 mL
5 mL
PQL
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
20
10
10
1.0
10
1.0
2.0
Acceptance Limits
70 - 130
70 - 130
70 - 130
Analytical Data
Client: ARCADIS U.S., Inc.
Client Sample ID:
DMW-CC_111909
Lab Sample ID:
Client Matrix:
660-32642-2
Water
Job Number: 660-32642-1
Date Sampled: 11/19/2009 1715
Date Received: 11/20/2009 1045
8260B Volatile Organic Compounds (GC/MS)
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260B
5030B
1.0
11/20/2009 1917
11/20/2009 1917
Analyte
Benzene
Bromobenzene
1,2-Dichlorobenzene
Chlorobromomethane
Dichlorobromomethane
Bromoform
Bromomethane
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
Chlorodibromomethane
1,2-Dibromo-3-Chloropropane
Ethylene Dibromide
Dibromomethane
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
Hexachlorobutadiene
Isopropylbenzene
4-Isopropyltoluene
Methylene Chloride
Naphthalene
N-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
TestAmerica Tampa
Analysis Batch: 660-87646
Result (ug/L)
0.50
0.58
0.44
0.58
0.35
0.58
2.5
0.67
0.63
0.84
0.42
0.63
2.5
0.90
1.0
0.65
0.52
0.34
2.5
0.50
0.41
0.64
0.52
2.5
0.52
0.57
0.45
0.65
0.44
0.52
0.39
0.36
0.31
0.14
0.14
0.44
0.40
0.19
0.69
4.0
2.5
0.59
0.98
0.63
0.15
0.50
Page 10 of 31
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Qualifier
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
MDL
0.50
0.58
0.44
0.58
0.35
0.58
2.5
0.67
0.63
0.84
0.42
0.63
2.5
0.90
1.0
0.65
0.52
0.34
2.5
0.50
0.41
0.64
0.52
2.5
0.52
0.57
0.45
0.65
0.44
0.52
0.39
0.36
0.31
0.14
0.14
0.44
0.40
0.19
0.69
4.0
2.5
0.59
0.98
0.63
0.15
0.50
BVMH5973
1HK2026.D
5 mL
5 mL
PQL
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
4.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
5.0
1.0
2.0
1.0
1.0
1.0
Analytical Data
Client: ARCADIS U.S., Inc.
Client Sample ID:
DMW-CC_111909
Lab Sample ID:
Client Matrix:
660-32642-2
Water
Job Number: 660-32642-1
Date Sampled: 11/19/2009 1715
Date Received: 11/20/2009 1045
8260B Volatile Organic Compounds (GC/MS)
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260B
5030B
1.0
11/20/2009 1917
11/20/2009 1917
Analysis Batch: 660-87646
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Analyte
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
o-Xylene
Acetone
2-Butanone (MEK)
4-Methyl-2-pentanone (MIBK)
Carbon disulfide
2-Hexanone
Methyl tert-butyl ether
m-Xylene & p-Xylene
Result (ug/L)
0.51
0.77
0.58
0.46
0.47
0.50
2.5
0.18
0.86
0.54
0.50
0.50
9.9
8.4
3.8
0.85
4.4
0.44
0.60
Qualifier
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U J3
U
U J3
U
U
Surrogate
Toluene-d8 (Surr)
4-Bromofluorobenzene
Dibromofluoromethane
%Rec
100
97
92
Qualifier
TestAmerica Tampa
Page 11 of 31
MDL
0.51
0.77
0.58
0.46
0.47
0.50
2.5
0.18
0.86
0.54
0.50
0.50
9.9
8.4
3.8
0.85
4.4
0.44
0.60
BVMH5973
1HK2026.D
5 mL
5 mL
PQL
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
20
10
10
1.0
10
1.0
2.0
Acceptance Limits
70 - 130
70 - 130
70 - 130
Analytical Data
Client: ARCADIS U.S., Inc.
Job Number: 660-32642-1
Client Sample ID:
Trip Blank#4_111909
Lab Sample ID:
Client Matrix:
660-32642-3
Water
Date Sampled: 11/19/2009 0000
Date Received: 11/20/2009 1045
8260B Volatile Organic Compounds (GC/MS)
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260B
5030B
1.0
11/20/2009 1748
11/20/2009 1748
Analyte
Benzene
Bromobenzene
1,2-Dichlorobenzene
Chlorobromomethane
Dichlorobromomethane
Bromoform
Bromomethane
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
Chlorodibromomethane
1,2-Dibromo-3-Chloropropane
Ethylene Dibromide
Dibromomethane
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
Hexachlorobutadiene
Isopropylbenzene
4-Isopropyltoluene
Methylene Chloride
Naphthalene
N-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
TestAmerica Tampa
Analysis Batch: 660-87646
Result (ug/L)
0.50
0.58
0.44
0.58
0.35
0.58
2.5
0.67
0.63
0.84
0.42
0.63
2.5
0.90
1.0
0.65
0.52
0.34
2.5
0.50
0.41
0.64
0.52
2.5
0.52
0.57
0.45
0.65
0.44
0.52
0.39
0.36
0.31
0.14
0.14
0.44
0.40
0.19
0.69
4.0
2.5
0.59
0.98
0.63
0.15
0.50
Page 12 of 31
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Qualifier
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
MDL
0.50
0.58
0.44
0.58
0.35
0.58
2.5
0.67
0.63
0.84
0.42
0.63
2.5
0.90
1.0
0.65
0.52
0.34
2.5
0.50
0.41
0.64
0.52
2.5
0.52
0.57
0.45
0.65
0.44
0.52
0.39
0.36
0.31
0.14
0.14
0.44
0.40
0.19
0.69
4.0
2.5
0.59
0.98
0.63
0.15
0.50
BVMH5973
1HK2022.D
5 mL
5 mL
PQL
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
4.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
5.0
1.0
2.0
1.0
1.0
1.0
Analytical Data
Client: ARCADIS U.S., Inc.
Job Number: 660-32642-1
Client Sample ID:
Trip Blank#4_111909
Lab Sample ID:
Client Matrix:
660-32642-3
Water
Date Sampled: 11/19/2009 0000
Date Received: 11/20/2009 1045
8260B Volatile Organic Compounds (GC/MS)
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260B
5030B
1.0
11/20/2009 1748
11/20/2009 1748
Analysis Batch: 660-87646
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Analyte
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
o-Xylene
Acetone
2-Butanone (MEK)
4-Methyl-2-pentanone (MIBK)
Carbon disulfide
2-Hexanone
Methyl tert-butyl ether
m-Xylene & p-Xylene
Result (ug/L)
0.51
0.77
0.58
0.46
0.47
0.50
2.5
0.18
0.86
0.54
0.50
0.50
9.9
8.4
3.8
0.85
4.4
0.44
0.60
Qualifier
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U J3
U
U J3
U
U
Surrogate
Toluene-d8 (Surr)
4-Bromofluorobenzene
Dibromofluoromethane
%Rec
91
97
91
Qualifier
TestAmerica Tampa
Page 13 of 31
MDL
0.51
0.77
0.58
0.46
0.47
0.50
2.5
0.18
0.86
0.54
0.50
0.50
9.9
8.4
3.8
0.85
4.4
0.44
0.60
BVMH5973
1HK2022.D
5 mL
5 mL
PQL
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
20
10
10
1.0
10
1.0
2.0
Acceptance Limits
70 - 130
70 - 130
70 - 130
Analytical Data
Client: ARCADIS U.S., Inc.
Client Sample ID:
IMW-V_111909
Lab Sample ID:
Client Matrix:
660-32642-1
Water
Job Number: 660-32642-1
Date Sampled: 11/19/2009 1638
Date Received: 11/20/2009 1045
8260C _SIM/ID 1,4-Dioxane by SIM/Isotopic Dilution
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260C _SIM/ID
5030C
1.0
11/20/2009 1832
11/20/2009 1832
Analyte
1,4-Dioxane
TestAmerica Tampa
Analysis Batch: 660-87653
Result (ug/L)
5.7
Page 14 of 31
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Qualifier
MDL
1.0
BVMH5973
1HK2024.D
5 mL
5 mL
PQL
2.0
Analytical Data
Client: ARCADIS U.S., Inc.
Job Number: 660-32642-1
Client Sample ID:
DMW-CC_111909
Lab Sample ID:
Client Matrix:
660-32642-2
Water
Date Sampled: 11/19/2009 1715
Date Received: 11/20/2009 1045
8260C _SIM/ID 1,4-Dioxane by SIM/Isotopic Dilution
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260C _SIM/ID
5030C
1.0
11/20/2009 1917
11/20/2009 1917
Analyte
1,4-Dioxane
TestAmerica Tampa
Analysis Batch: 660-87653
Result (ug/L)
1.0
Page 15 of 31
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Qualifier
U
MDL
1.0
BVMH5973
1HK2026.D
5 mL
5 mL
PQL
2.0
Analytical Data
Client: ARCADIS U.S., Inc.
Job Number: 660-32642-1
Client Sample ID:
Trip Blank#4_111909
Lab Sample ID:
Client Matrix:
660-32642-3
Water
Date Sampled: 11/19/2009 0000
Date Received: 11/20/2009 1045
8260C _SIM/ID 1,4-Dioxane by SIM/Isotopic Dilution
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260C _SIM/ID
5030C
1.0
11/20/2009 1748
11/20/2009 1748
Analyte
1,4-Dioxane
TestAmerica Tampa
Analysis Batch: 660-87653
Result (ug/L)
1.0
Page 16 of 31
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Qualifier
U
MDL
1.0
BVMH5973
1HK2022.D
5 mL
5 mL
PQL
2.0
DATA REPORTING QUALIFIERS
Client: ARCADIS U.S., Inc.
Lab Section
Job Number: 660-32642-1
Qualifier
Description
J3
Estimated value; value may not be accurate. Spike recovery
or RPD outside of criteria.
U
Indicates that the compound was analyzed for but not
detected.
L
Off-scale high. Actual value is known to be greater than the
value given.
I
The reported value is between the laboratory method
detection limit and the laboratory practical quantitation limit.
GC/MS VOA
TestAmerica Tampa
Page 17 of 31
QUALITY CONTROL RESULTS
TestAmerica Tampa
Page 18 of 31
Quality Control Results
Client: ARCADIS U.S., Inc.
Job Number: 660-32642-1
Surrogate Recovery Report
8260B Volatile Organic Compounds (GC/MS)
Client Matrix: Water
TOL
%Rec
BFB
%Rec
DBFM
%Rec
Lab Sample ID
Client Sample ID
660-32642-1
IMW-V_111909
111
95
93
660-32642-2
DMW-CC_111909
100
97
92
660-32642-3
Trip Blank#4_111909
91
97
91
MB 660-87646/4
108
97
93
LCS 660-87646/3
110
97
93
111
95
94
108
98
94
660-32564-C-11 MS
660-32642-1 DU
IMW-V_111909 DU
Surrogate
TOL = Toluene-d8 (Surr)
BFB = 4-Bromofluorobenzene
DBFM = Dibromofluoromethane
Acceptance Limits
70-130
70-130
70-130
TestAmerica Tampa
Page 19 of 31
Quality Control Results
Client: ARCADIS U.S., Inc.
Job Number: 660-32642-1
Method Blank - Batch: 660-87646
Lab Sample ID:
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
MB 660-87646/4
Water
1.0
11/20/2009 1304
11/20/2009 1304
Method: 8260B
Preparation: 5030B
Analysis Batch: 660-87646
Prep Batch: N/A
Units: ug/L
Instrument ID: BVMH GC/MS
Lab File ID:
1HK2010.D
Initial Weight/Volume: 5 mL
Final Weight/Volume: 5 mL
Analyte
Result
Qual
MDL
PQL
Benzene
Bromobenzene
1,2-Dichlorobenzene
Chlorobromomethane
Dichlorobromomethane
Bromoform
Bromomethane
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
Chlorodibromomethane
1,2-Dibromo-3-Chloropropane
Ethylene Dibromide
Dibromomethane
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
Hexachlorobutadiene
Isopropylbenzene
4-Isopropyltoluene
Methylene Chloride
Naphthalene
0.50
0.58
0.44
0.58
0.35
0.58
2.5
0.67
0.63
0.84
0.42
0.63
2.5
0.90
1.0
0.65
0.52
0.34
2.5
0.50
0.41
0.64
0.52
2.5
0.52
0.57
0.45
0.65
0.44
0.52
0.39
0.36
0.31
0.14
0.14
0.44
0.40
0.19
0.69
4.0
2.5
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
0.50
0.58
0.44
0.58
0.35
0.58
2.5
0.67
0.63
0.84
0.42
0.63
2.5
0.90
1.0
0.65
0.52
0.34
2.5
0.50
0.41
0.64
0.52
2.5
0.52
0.57
0.45
0.65
0.44
0.52
0.39
0.36
0.31
0.14
0.14
0.44
0.40
0.19
0.69
4.0
2.5
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
4.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
5.0
Calculations are performed before rounding to avoid round-off errors in calculated results.
TestAmerica Tampa
Page 20 of 31
Quality Control Results
Client: ARCADIS U.S., Inc.
Job Number: 660-32642-1
Method Blank - Batch: 660-87646
Lab Sample ID:
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
MB 660-87646/4
Water
1.0
11/20/2009 1304
11/20/2009 1304
Method: 8260B
Preparation: 5030B
Analysis Batch: 660-87646
Prep Batch: N/A
Units: ug/L
Instrument ID: BVMH GC/MS
Lab File ID:
1HK2010.D
Initial Weight/Volume: 5 mL
Final Weight/Volume: 5 mL
Analyte
Result
Qual
MDL
PQL
N-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
o-Xylene
Acetone
2-Butanone (MEK)
4-Methyl-2-pentanone (MIBK)
Carbon disulfide
2-Hexanone
Methyl tert-butyl ether
m-Xylene & p-Xylene
0.59
0.98
0.63
0.15
0.50
0.51
0.77
0.58
0.46
0.47
0.50
2.5
0.18
0.86
0.54
0.50
0.50
9.9
8.4
3.8
0.85
4.4
0.44
0.60
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
0.59
0.98
0.63
0.15
0.50
0.51
0.77
0.58
0.46
0.47
0.50
2.5
0.18
0.86
0.54
0.50
0.50
9.9
8.4
3.8
0.85
4.4
0.44
0.60
1.0
2.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
20
10
10
1.0
10
1.0
2.0
Surrogate
Toluene-d8 (Surr)
4-Bromofluorobenzene
Dibromofluoromethane
% Rec
Acceptance Limits
108
97
93
70 - 130
70 - 130
70 - 130
Calculations are performed before rounding to avoid round-off errors in calculated results.
TestAmerica Tampa
Page 21 of 31
Quality Control Results
Client: ARCADIS U.S., Inc.
Job Number: 660-32642-1
Lab Control Sample - Batch: 660-87646
Lab Sample ID:
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
LCS 660-87646/3
Water
1.0
11/20/2009 1051
11/20/2009 1051
Method: 8260B
Preparation: 5030B
Analysis Batch: 660-87646
Prep Batch: N/A
Units: ug/L
Instrument ID: BVMH GC/MS
Lab File ID:
1HK2004.D
Initial Weight/Volume: 5 mL
Final Weight/Volume: 5 mL
Analyte
Spike Amount
Result
% Rec.
Limit
Benzene
Bromobenzene
1,2-Dichlorobenzene
Chlorobromomethane
Dichlorobromomethane
Bromoform
Bromomethane
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
Chlorodibromomethane
1,2-Dibromo-3-Chloropropane
Ethylene Dibromide
Dibromomethane
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
Hexachlorobutadiene
Isopropylbenzene
4-Isopropyltoluene
Methylene Chloride
Naphthalene
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.1
21.0
21.5
20.6
22.8
19.1
19.2
21.7
22.7
21.9
20.8
21.3
13.8
20.3
18.0
20.8
21.3
22.2
19.6
23.0
23.2
21.1
20.4
11.9
20.7
20.1
22.1
20.9
21.4
23.3
23.8
21.1
21.7
26.1
20.9
21.3
22.4
20.3
21.9
20.4
22.0
100
105
107
103
114
95
96
108
113
110
104
107
69
102
90
104
107
111
98
115
116
106
102
60
103
101
111
104
107
116
119
105
108
130
104
106
112
101
109
102
110
64 - 140
68 - 130
70 - 130
59 - 130
70 - 130
65 - 130
14 - 184
59 - 133
68 - 134
64 - 130
53 - 145
70 - 130
39 - 174
59 - 130
35 - 153
70 - 130
70 - 130
70 - 130
52 - 130
65 - 130
70 - 130
68 - 130
70 - 130
16 - 149
60 - 132
70 - 130
51 - 157
61 - 130
55 - 145
70 - 130
70 - 130
49 - 139
58 - 146
70 - 130
62 - 130
69 - 131
62 - 155
60 - 131
65 - 134
57 - 130
41 - 157
Calculations are performed before rounding to avoid round-off errors in calculated results.
TestAmerica Tampa
Page 22 of 31
Qual
Quality Control Results
Client: ARCADIS U.S., Inc.
Job Number: 660-32642-1
Lab Control Sample - Batch: 660-87646
Lab Sample ID:
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
LCS 660-87646/3
Water
1.0
11/20/2009 1051
11/20/2009 1051
Method: 8260B
Preparation: 5030B
Analysis Batch: 660-87646
Prep Batch: N/A
Units: ug/L
Instrument ID: BVMH GC/MS
Lab File ID:
1HK2004.D
Initial Weight/Volume: 5 mL
Final Weight/Volume: 5 mL
Analyte
Spike Amount
Result
% Rec.
Limit
N-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
o-Xylene
Acetone
2-Butanone (MEK)
4-Methyl-2-pentanone (MIBK)
Carbon disulfide
2-Hexanone
Methyl tert-butyl ether
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
100
100
100
10.0
100
10.0
21.8
22.1
21.0
21.1
24.1
23.0
20.1
21.5
20.4
23.5
21.8
19.7
21.2
21.9
21.4
17.9
21.6
122
131
154
12.7
149
11.5
109
111
105
105
120
115
100
107
102
118
109
99
106
109
107
89
108
122
131
154
127
149
115
66 - 130
62 - 136
70 - 130
67 - 130
47 - 143
70 - 131
46 - 148
54 - 136
57 - 135
69 - 130
59 - 142
62 - 147
62 - 130
66 - 138
65 - 134
48 - 147
66 - 133
62 - 142
63 - 140
64 - 137
30 - 184
57 - 148
67 - 130
Surrogate
Toluene-d8 (Surr)
4-Bromofluorobenzene
Dibromofluoromethane
% Rec
Acceptance Limits
110
97
93
70 - 130
70 - 130
70 - 130
Calculations are performed before rounding to avoid round-off errors in calculated results.
TestAmerica Tampa
Page 23 of 31
Qual
J3
J3
Quality Control Results
Client: ARCADIS U.S., Inc.
Job Number: 660-32642-1
Matrix Spike - Batch: 660-87646
Lab Sample ID:
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
660-32564-C-11 MS
Water
1.0
11/20/2009 1703
11/20/2009 1703
Method: 8260B
Preparation: 5030B
Analysis Batch: 660-87646
Prep Batch: N/A
Units: ug/L
Instrument ID: BVMH GC/MS
Lab File ID:
1HK2020.D
Initial Weight/Volume: 5 mL
Final Weight/Volume: 5 mL
Analyte
Sample Result/Qual
Spike Amount
Result
% Rec.
Benzene
Bromobenzene
1,2-Dichlorobenzene
Chlorobromomethane
Dichlorobromomethane
Bromoform
Bromomethane
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
Chlorodibromomethane
1,2-Dibromo-3-Chloropropane
Ethylene Dibromide
Dibromomethane
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
0.50
0.58
0.44
0.58
0.35
0.58
2.5
0.67
0.63
0.84
0.42
0.63
2.5
0.90
1.0
0.65
0.52
0.34
2.5
0.50
0.41
0.64
0.52
2.5
0.52
0.57
0.45
0.65
0.44
0.52
0.39
0.36
0.31
0.14
0.14
0.44
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
21.4
21.2
21.3
20.5
23.2
18.0
10.6
21.9
23.6
22.7
22.9
22.1
15.9
21.4
18.1
21.6
21.7
22.3
18.0
23.0
23.8
21.5
20.6
12.6
22.2
21.2
24.5
22.4
23.0
24.5
24.5
22.3
23.8
26.4
20.4
22.4
107
106
106
102
116
90
53
110
118
113
114
110
79
107
91
108
109
112
90
115
119
107
103
63
111
106
122
112
115
123
122
112
119
132
102
112
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
Calculations are performed before rounding to avoid round-off errors in calculated results.
TestAmerica Tampa
Page 24 of 31
Limit
64 - 140
68 - 130
70 - 130
59 - 130
70 - 130
65 - 130
14 - 184
59 - 133
68 - 134
64 - 130
53 - 145
70 - 130
39 - 174
59 - 130
35 - 153
70 - 130
70 - 130
70 - 130
52 - 130
65 - 130
70 - 130
68 - 130
70 - 130
16 - 149
60 - 132
70 - 130
51 - 157
61 - 130
55 - 145
70 - 130
70 - 130
49 - 139
58 - 146
70 - 130
62 - 130
69 - 131
Qual
J3
Quality Control Results
Client: ARCADIS U.S., Inc.
Job Number: 660-32642-1
Matrix Spike - Batch: 660-87646
Lab Sample ID:
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
660-32564-C-11 MS
Water
1.0
11/20/2009 1703
11/20/2009 1703
Method: 8260B
Preparation: 5030B
Analysis Batch: 660-87646
Prep Batch: N/A
Units: ug/L
Instrument ID: BVMH GC/MS
Lab File ID:
1HK2020.D
Initial Weight/Volume: 5 mL
Final Weight/Volume: 5 mL
Analyte
Sample Result/Qual
Spike Amount
Result
% Rec.
Hexachlorobutadiene
Isopropylbenzene
4-Isopropyltoluene
Methylene Chloride
Naphthalene
N-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
o-Xylene
Acetone
2-Butanone (MEK)
4-Methyl-2-pentanone (MIBK)
Carbon disulfide
2-Hexanone
Methyl tert-butyl ether
0.40
0.19
0.69
4.0
2.5
0.59
0.98
0.63
0.15
0.50
0.51
0.77
0.58
0.46
0.47
0.50
2.5
0.18
0.86
0.54
0.50
0.50
9.9
8.4
3.8
0.85
4.4
0.44
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
100
100
100
10.0
100
10.0
20.8
21.1
22.1
20.1
20.1
22.7
22.8
21.3
20.8
25.1
24.7
18.4
19.5
22.3
23.9
21.7
22.1
20.4
21.7
22.2
19.5
22.6
122
129
159
13.3
150
11.7
104
105
111
101
101
114
114
106
104
125
124
92
98
111
119
109
111
102
108
111
97
113
122
129
159
133
150
117
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
Surrogate
% Rec
Toluene-d8 (Surr)
4-Bromofluorobenzene
Dibromofluoromethane
111
95
94
Calculations are performed before rounding to avoid round-off errors in calculated results.
TestAmerica Tampa
Page 25 of 31
Acceptance Limits
70 - 130
70 - 130
70 - 130
Limit
62 - 155
60 - 131
65 - 134
57 - 130
41 - 157
66 - 130
62 - 136
70 - 130
67 - 130
47 - 143
70 - 131
46 - 148
54 - 136
57 - 135
69 - 130
59 - 142
62 - 147
62 - 130
66 - 138
65 - 134
48 - 147
66 - 133
62 - 142
63 - 140
64 - 137
30 - 184
57 - 148
67 - 130
Qual
J3
J3
Quality Control Results
Client: ARCADIS U.S., Inc.
Job Number: 660-32642-1
Duplicate - Batch: 660-87646
Lab Sample ID:
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
660-32642-1
Water
1.0
11/20/2009 1854
11/20/2009 1854
Method: 8260B
Preparation: 5030B
Analysis Batch: 660-87646
Prep Batch: N/A
Units: ug/L
Instrument ID: BVMH GC/MS
Lab File ID:
1HK2025.D
Initial Weight/Volume: 5 mL
Final Weight/Volume: 5 mL
Analyte
Sample Result/Qual
Result
RPD
Limit
Qual
Benzene
Bromobenzene
1,2-Dichlorobenzene
Chlorobromomethane
Dichlorobromomethane
Bromoform
Bromomethane
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
Chlorodibromomethane
1,2-Dibromo-3-Chloropropane
Ethylene Dibromide
Dibromomethane
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
Hexachlorobutadiene
Isopropylbenzene
4-Isopropyltoluene
0.50
0.58
0.44
0.58
0.35
0.58
2.5
0.67
0.63
0.84
0.42
0.63
2.5
0.90
1.0
0.65
0.52
0.34
2.5
0.50
0.41
0.64
0.52
2.5
0.52
0.57
0.45
0.65
0.44
0.52
0.39
0.36
0.31
0.14
0.14
0.44
0.40
0.19
0.69
0.50
0.58
0.44
0.58
0.35
0.58
2.5
0.67
0.63
0.84
0.42
0.63
2.5
0.90
1.0
0.65
0.52
0.34
2.5
0.50
0.41
0.64
0.52
2.5
0.52
0.57
0.45
0.65
0.44
0.52
0.39
0.36
0.31
0.14
0.14
0.44
0.40
0.19
0.69
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
Calculations are performed before rounding to avoid round-off errors in calculated results.
TestAmerica Tampa
Page 26 of 31
Quality Control Results
Client: ARCADIS U.S., Inc.
Job Number: 660-32642-1
Duplicate - Batch: 660-87646
Lab Sample ID:
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
660-32642-1
Water
1.0
11/20/2009 1854
11/20/2009 1854
Method: 8260B
Preparation: 5030B
Analysis Batch: 660-87646
Prep Batch: N/A
Units: ug/L
Instrument ID: BVMH GC/MS
Lab File ID:
1HK2025.D
Initial Weight/Volume: 5 mL
Final Weight/Volume: 5 mL
Analyte
Sample Result/Qual
Result
RPD
Limit
Qual
Methylene Chloride
Naphthalene
N-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
o-Xylene
Acetone
2-Butanone (MEK)
4-Methyl-2-pentanone (MIBK)
Carbon disulfide
2-Hexanone
Methyl tert-butyl ether
m-Xylene & p-Xylene
4.0
2.5
0.59
0.98
0.63
0.15
0.50
0.51
0.77
0.58
0.46
0.47
0.50
2.5
0.18
0.86
0.54
0.50
0.50
9.9
8.4
3.8
0.93
4.4
0.44
0.60
4.0
2.5
0.59
0.98
0.63
0.15
0.50
0.51
0.77
0.58
0.46
0.47
0.50
2.5
0.18
0.86
0.54
0.50
0.50
9.9
8.4
3.8
0.886
4.4
0.44
0.60
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
5
NC
NC
NC
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U J3
I
U J3
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
I
U
U
U
Surrogate
% Rec
Toluene-d8 (Surr)
4-Bromofluorobenzene
Dibromofluoromethane
108
98
94
Calculations are performed before rounding to avoid round-off errors in calculated results.
TestAmerica Tampa
Page 27 of 31
Acceptance Limits
70 - 130
70 - 130
70 - 130
Quality Control Results
Client: ARCADIS U.S., Inc.
Job Number: 660-32642-1
Method Blank - Batch: 660-87653
Lab Sample ID:
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
Method: 8260C _SIM/ID
Preparation: 5030C
MB 660-87653/4
Water
1.0
11/20/2009 1304
11/20/2009 1304
Analysis Batch: 660-87653
Prep Batch: N/A
Units: ug/L
Instrument ID: BVMH GC/MS
Lab File ID:
1HK2010.D
Initial Weight/Volume: 5 mL
Final Weight/Volume: 5 mL
Analyte
Result
Qual
MDL
PQL
1,4-Dioxane
1.0
U
1.0
2.0
Lab Control Sample - Batch: 660-87653
Lab Sample ID:
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
LCS 660-87653/3
Water
1.0
11/20/2009 1158
11/20/2009 1158
Method: 8260C _SIM/ID
Preparation: 5030C
Analysis Batch: 660-87653
Prep Batch: N/A
Units: ug/L
Instrument ID: BVMH GC/MS
Lab File ID:
1HK2007.D
Initial Weight/Volume: 5 mL
Final Weight/Volume: 5 mL
Analyte
Spike Amount
Result
% Rec.
Limit
1,4-Dioxane
25.0
21.9
88
50 - 150
Matrix Spike - Batch: 660-87653
Lab Sample ID:
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
660-32643-C-2 MS
Water
1.0
11/20/2009 2110
11/20/2009 2110
Method: 8260C _SIM/ID
Preparation: 5030C
Analysis Batch: 660-87653
Prep Batch: N/A
Units: ug/L
Instrument ID: BVMH GC/MS
Lab File ID:
1HK2031.D
Initial Weight/Volume: 5 mL
Final Weight/Volume: 5 mL
Analyte
Sample Result/Qual
Spike Amount
Result
% Rec.
1,4-Dioxane
130
25.0
159
103
Calculations are performed before rounding to avoid round-off errors in calculated results.
TestAmerica Tampa
Qual
Page 28 of 31
Limit
50 - 150
Qual
L
Quality Control Results
Client: ARCADIS U.S., Inc.
Job Number: 660-32642-1
Duplicate - Batch: 660-87653
Lab Sample ID:
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
660-32642-1
Water
1.0
11/20/2009 1854
11/20/2009 1854
Method: 8260C _SIM/ID
Preparation: 5030C
Analysis Batch: 660-87653
Prep Batch: N/A
Units: ug/L
Instrument ID: BVMH GC/MS
Lab File ID:
1HK2025.D
Initial Weight/Volume: 5 mL
Final Weight/Volume: 5 mL
Analyte
Sample Result/Qual
Result
RPD
Limit
1,4-Dioxane
5.7
5.93
4
50
Calculations are performed before rounding to avoid round-off errors in calculated results.
TestAmerica Tampa
Page 29 of 31
Qual
Page 30 of 31
Login Sample Receipt Check List
Client: ARCADIS U.S., Inc.
Job Number: 660-32642-1
Login Number: 32642
Creator: Harrison, Amanda
List Number: 1
List Source: TestAmerica Tampa
Question
T / F/ NA
Radioactivity either was not measured or, if measured, is at or below
background
The cooler's custody seal, if present, is intact.
N/A
The cooler or samples do not appear to have been compromised or
tampered with.
Samples were received on ice.
Cooler Temperature is acceptable.
True
Cooler Temperature is recorded.
COC is present.
COC is filled out in ink and legible.
COC is filled out with all pertinent information.
There are no discrepancies between the sample IDs on the containers and
the COC.
Samples are received within Holding Time.
Sample containers have legible labels.
Containers are not broken or leaking.
True
True
True
False
True
Sample collection date/times are provided.
Appropriate sample containers are used.
Sample bottles are completely filled.
There is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
VOA sample vials do not have headspace or bubble is <6mm (1/4") in
diameter.
If necessary, staff have been informed of any short hold time or quick TAT
needs
Multiphasic samples are not present.
Samples do not require splitting or compositing.
Is the Field Sampler's name present on COC?
Sample Preservation Verified
True
True
True
True
TestAmerica Tampa
Comment
True
True
True
True
True
True
True
True
True
True
True
True
Page 31 of 31
2.7 degrees C CU-07
only rec'd 1 vial for Trip Blank 11.19.09
ANALYTICAL REPORT
Job Number: 660-32804-1
Job Description: Raytheon
For:
ARCADIS U.S., Inc.
14055 Riveredge Drive
Suite 400
Tampa, FL 33637
Attention: Mr. Gus Suarez
_____________________________________________
Approved for release.
Natalie Tafuni
Project Manager I
12/8/2009 2:05 PM
Natalie Tafuni
Project Manager I
[email protected]
12/08/2009
cc:
Ms. Lyndi Mott
Mr. Melvin Rivera
Albert Zumbuhl
Methods: FDEP, DOH Certification #: TestAmerica Tampa E84282
These test results meet all the requirements of NELAC unless specified in the case narrative. All questions regarding
this test report should be directed to the TestAmerica Project Manager who signed this test report. The estimated
uncertainty associated with these reported results is available upon request. The results contained in this test report
relate only to these samples included herein.
TestAmerica Laboratories, Inc.
TestAmerica Tampa 6712 Benjamin Road, Suite 100, Tampa, FL 33634
Tel (813) 885-7427 Fax (813) 885-7049 www.testamericainc.com
Page 1 of 28
Job Narrative
660-32804-1
Comments
No additional comments.
Receipt
All samples were received in good condition within temperature requirements.
8260B
The laboratory control sample (LCS) for batch 660-88145 was outside of control limits for MTBE. MTBE recovered high with samples
non-detect for MTBE. The data are flagged with J3 qualifiers.
The batch matrix spike (MS) recoveries for batch 660-88145(660-32795) were outside of control limits. The associated laboratory control
sample (LCS) recovery met acceptance criteria except as noted above. The data are flagged with J3 qualifiers.
The batch sample duplicate %RPD for batch 660-88145(660-32794) has a result of NC for most compounds. The sample result and the
sample duplicate result are both Non-detect for these compounds. The Laboratory LIMs system flags the %RPD in this scenario as NC, or
"not calculated".
Page 2 of 28
EXECUTIVE SUMMARY - Detections
Client: ARCADIS U.S., Inc.
Lab Sample ID
Analyte
660-32804-1
1,4-Dioxane
Job Number: 660-32804-1
Client Sample ID
Result / Qualifier
Reporting
Limit
Units
Method
ug/L
8260C _SIM/ID
IMW-V_120209
4.0
2.0
TestAmerica Tampa
Page 3 of 28
METHOD SUMMARY
Client: ARCADIS U.S., Inc.
Description
Job Number: 660-32804-1
Lab Location Method
Preparation Method
Volatile Organic Compounds (GC/MS)
Purge and Trap
TAL TAM
TAL TAM
SW846 8260B
SW846 5030B
1,4-Dioxane by SIM/Isotopic Dilution
Purge and Trap
TAL TAM
TAL TAM
SW846 8260C _SIM/ID
SW846 5030C
Matrix
Water
Lab References:
TAL TAM = TestAmerica Tampa
Method References:
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its
Updates.
TestAmerica Tampa
Page 4 of 28
METHOD / ANALYST SUMMARY
Client: ARCADIS U.S., Inc.
Job Number: 660-32804-1
Method
Analyst
SW846 8260B
Harris, Chris
CH
SW846 8260C _SIM/ID
Harris, Chris
CH
TestAmerica Tampa
Page 5 of 28
Analyst ID
SAMPLE SUMMARY
Client: ARCADIS U.S., Inc.
Job Number: 660-32804-1
Lab Sample ID
Client Sample ID
Client Matrix
660-32804-1
660-32804-2
IMW-V_120209
Trip Blank_120209
Water
Water
TestAmerica Tampa
Page 6 of 28
Date/Time
Sampled
Date/Time
Received
12/02/2009 1030
12/02/2009 0000
12/03/2009 1420
12/03/2009 1420
SAMPLE RESULTS
TestAmerica Tampa
Page 7 of 28
Analytical Data
Client: ARCADIS U.S., Inc.
Client Sample ID:
IMW-V_120209
Lab Sample ID:
Client Matrix:
660-32804-1
Water
Job Number: 660-32804-1
Date Sampled: 12/02/2009 1030
Date Received: 12/03/2009 1420
8260B Volatile Organic Compounds (GC/MS)
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260B
5030B
1.0
12/04/2009 1738
12/04/2009 1738
Analyte
Benzene
Bromobenzene
1,2-Dichlorobenzene
Chlorobromomethane
Dichlorobromomethane
Bromoform
Bromomethane
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
Chlorodibromomethane
1,2-Dibromo-3-Chloropropane
Ethylene Dibromide
Dibromomethane
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
Hexachlorobutadiene
Isopropylbenzene
4-Isopropyltoluene
Methylene Chloride
Naphthalene
N-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
TestAmerica Tampa
Analysis Batch: 660-88145
Result (ug/L)
0.50
0.58
0.44
0.58
0.35
0.58
2.5
0.67
0.63
0.84
0.42
0.63
2.5
0.90
1.0
0.65
0.52
0.34
2.5
0.50
0.41
0.64
0.52
2.5
0.52
0.57
0.45
0.65
0.44
0.52
0.39
0.36
0.31
0.14
0.14
0.44
0.40
0.19
0.69
4.0
2.5
0.59
0.98
0.63
0.15
0.50
Page 8 of 28
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Qualifier
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
MDL
0.50
0.58
0.44
0.58
0.35
0.58
2.5
0.67
0.63
0.84
0.42
0.63
2.5
0.90
1.0
0.65
0.52
0.34
2.5
0.50
0.41
0.64
0.52
2.5
0.52
0.57
0.45
0.65
0.44
0.52
0.39
0.36
0.31
0.14
0.14
0.44
0.40
0.19
0.69
4.0
2.5
0.59
0.98
0.63
0.15
0.50
BVMJ5975
1JL0423.D
5 mL
5 mL
PQL
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
4.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
5.0
1.0
2.0
1.0
1.0
1.0
Analytical Data
Client: ARCADIS U.S., Inc.
Client Sample ID:
IMW-V_120209
Lab Sample ID:
Client Matrix:
660-32804-1
Water
Job Number: 660-32804-1
Date Sampled: 12/02/2009 1030
Date Received: 12/03/2009 1420
8260B Volatile Organic Compounds (GC/MS)
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260B
5030B
1.0
12/04/2009 1738
12/04/2009 1738
Analysis Batch: 660-88145
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Analyte
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
o-Xylene
Acetone
2-Butanone (MEK)
4-Methyl-2-pentanone (MIBK)
Carbon disulfide
2-Hexanone
Methyl tert-butyl ether
m-Xylene & p-Xylene
Result (ug/L)
0.51
0.77
0.58
0.46
0.47
0.50
2.5
0.18
0.86
0.54
0.50
0.50
9.9
8.4
3.8
0.85
4.4
0.44
0.60
Qualifier
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U J3
U
Surrogate
Toluene-d8 (Surr)
4-Bromofluorobenzene
Dibromofluoromethane
%Rec
94
95
102
Qualifier
TestAmerica Tampa
Page 9 of 28
MDL
0.51
0.77
0.58
0.46
0.47
0.50
2.5
0.18
0.86
0.54
0.50
0.50
9.9
8.4
3.8
0.85
4.4
0.44
0.60
BVMJ5975
1JL0423.D
5 mL
5 mL
PQL
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
20
10
10
1.0
10
1.0
2.0
Acceptance Limits
70 - 130
70 - 130
70 - 130
Analytical Data
Client: ARCADIS U.S., Inc.
Client Sample ID:
Trip Blank_120209
Lab Sample ID:
Client Matrix:
660-32804-2
Water
Job Number: 660-32804-1
Date Sampled: 12/02/2009 0000
Date Received: 12/03/2009 1420
8260B Volatile Organic Compounds (GC/MS)
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260B
5030B
1.0
12/04/2009 1410
12/04/2009 1410
Analyte
Benzene
Bromobenzene
1,2-Dichlorobenzene
Chlorobromomethane
Dichlorobromomethane
Bromoform
Bromomethane
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
Chlorodibromomethane
1,2-Dibromo-3-Chloropropane
Ethylene Dibromide
Dibromomethane
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
Hexachlorobutadiene
Isopropylbenzene
4-Isopropyltoluene
Methylene Chloride
Naphthalene
N-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
TestAmerica Tampa
Analysis Batch: 660-88145
Result (ug/L)
0.50
0.58
0.44
0.58
0.35
0.58
2.5
0.67
0.63
0.84
0.42
0.63
2.5
0.90
1.0
0.65
0.52
0.34
2.5
0.50
0.41
0.64
0.52
2.5
0.52
0.57
0.45
0.65
0.44
0.52
0.39
0.36
0.31
0.14
0.14
0.44
0.40
0.19
0.69
4.0
2.5
0.59
0.98
0.63
0.15
0.50
Page 10 of 28
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Qualifier
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
MDL
0.50
0.58
0.44
0.58
0.35
0.58
2.5
0.67
0.63
0.84
0.42
0.63
2.5
0.90
1.0
0.65
0.52
0.34
2.5
0.50
0.41
0.64
0.52
2.5
0.52
0.57
0.45
0.65
0.44
0.52
0.39
0.36
0.31
0.14
0.14
0.44
0.40
0.19
0.69
4.0
2.5
0.59
0.98
0.63
0.15
0.50
BVMJ5975
1JL0414.D
5 mL
5 mL
PQL
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
4.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
5.0
1.0
2.0
1.0
1.0
1.0
Analytical Data
Client: ARCADIS U.S., Inc.
Client Sample ID:
Trip Blank_120209
Lab Sample ID:
Client Matrix:
660-32804-2
Water
Job Number: 660-32804-1
Date Sampled: 12/02/2009 0000
Date Received: 12/03/2009 1420
8260B Volatile Organic Compounds (GC/MS)
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260B
5030B
1.0
12/04/2009 1410
12/04/2009 1410
Analysis Batch: 660-88145
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Analyte
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
o-Xylene
Acetone
2-Butanone (MEK)
4-Methyl-2-pentanone (MIBK)
Carbon disulfide
2-Hexanone
Methyl tert-butyl ether
m-Xylene & p-Xylene
Result (ug/L)
0.51
0.77
0.58
0.46
0.47
0.50
2.5
0.18
0.86
0.54
0.50
0.50
9.9
8.4
3.8
0.85
4.4
0.44
0.60
Qualifier
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U J3
U
Surrogate
Toluene-d8 (Surr)
4-Bromofluorobenzene
Dibromofluoromethane
%Rec
94
97
100
Qualifier
TestAmerica Tampa
Page 11 of 28
MDL
0.51
0.77
0.58
0.46
0.47
0.50
2.5
0.18
0.86
0.54
0.50
0.50
9.9
8.4
3.8
0.85
4.4
0.44
0.60
BVMJ5975
1JL0414.D
5 mL
5 mL
PQL
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
20
10
10
1.0
10
1.0
2.0
Acceptance Limits
70 - 130
70 - 130
70 - 130
Analytical Data
Client: ARCADIS U.S., Inc.
Client Sample ID:
IMW-V_120209
Lab Sample ID:
Client Matrix:
660-32804-1
Water
Job Number: 660-32804-1
Date Sampled: 12/02/2009 1030
Date Received: 12/03/2009 1420
8260C _SIM/ID 1,4-Dioxane by SIM/Isotopic Dilution
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260C _SIM/ID
5030C
1.0
12/04/2009 1738
12/04/2009 1738
Analyte
1,4-Dioxane
TestAmerica Tampa
Analysis Batch: 660-88144
Result (ug/L)
4.0
Page 12 of 28
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Qualifier
MDL
1.0
BVMJ5975
1JL0423.D
5 mL
5 mL
PQL
2.0
Analytical Data
Client: ARCADIS U.S., Inc.
Job Number: 660-32804-1
Client Sample ID:
Trip Blank_120209
Lab Sample ID:
Client Matrix:
660-32804-2
Water
Date Sampled: 12/02/2009 0000
Date Received: 12/03/2009 1420
8260C _SIM/ID 1,4-Dioxane by SIM/Isotopic Dilution
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260C _SIM/ID
5030C
1.0
12/04/2009 1410
12/04/2009 1410
Analyte
1,4-Dioxane
TestAmerica Tampa
Analysis Batch: 660-88144
Result (ug/L)
1.0
Page 13 of 28
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Qualifier
U
MDL
1.0
BVMJ5975
1JL0414.D
5 mL
5 mL
PQL
2.0
DATA REPORTING QUALIFIERS
Client: ARCADIS U.S., Inc.
Lab Section
Job Number: 660-32804-1
Qualifier
Description
J3
Estimated value; value may not be accurate. Spike recovery
or RPD outside of criteria.
U
Indicates that the compound was analyzed for but not
detected.
I
The reported value is between the laboratory method
detection limit and the laboratory practical quantitation limit.
GC/MS VOA
TestAmerica Tampa
Page 14 of 28
QUALITY CONTROL RESULTS
TestAmerica Tampa
Page 15 of 28
Quality Control Results
Client: ARCADIS U.S., Inc.
Job Number: 660-32804-1
Surrogate Recovery Report
8260B Volatile Organic Compounds (GC/MS)
Client Matrix: Water
Lab Sample ID
Client Sample ID
TOL
%Rec
BFB
%Rec
DBFM
%Rec
660-32804-1
IMW-V_120209
94
95
102
660-32804-2
Trip Blank_120209
94
97
100
MB 660-88145/3
94
97
101
LCS 660-88145/2
97
93
108
660-32795-A-5 MS
97
95
104
660-32794-A-1 DU
95
98
101
Surrogate
TOL = Toluene-d8 (Surr)
BFB = 4-Bromofluorobenzene
DBFM = Dibromofluoromethane
Acceptance Limits
70-130
70-130
70-130
TestAmerica Tampa
Page 16 of 28
Quality Control Results
Client: ARCADIS U.S., Inc.
Job Number: 660-32804-1
Method Blank - Batch: 660-88145
Lab Sample ID:
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
MB 660-88145/3
Water
1.0
12/04/2009 1258
12/04/2009 1258
Method: 8260B
Preparation: 5030B
Analysis Batch: 660-88145
Prep Batch: N/A
Units: ug/L
Instrument ID: BVMJ GC/MS
Lab File ID:
1JL0411.D
Initial Weight/Volume: 5 mL
Final Weight/Volume: 5 mL
Analyte
Result
Qual
MDL
PQL
Benzene
Bromobenzene
1,2-Dichlorobenzene
Chlorobromomethane
Dichlorobromomethane
Bromoform
Bromomethane
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
Chlorodibromomethane
1,2-Dibromo-3-Chloropropane
Ethylene Dibromide
Dibromomethane
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
Hexachlorobutadiene
Isopropylbenzene
4-Isopropyltoluene
Methylene Chloride
Naphthalene
0.50
0.58
0.44
0.58
0.35
0.58
2.5
0.67
0.63
0.84
0.42
0.63
2.5
0.90
1.0
0.65
0.52
0.34
2.5
0.50
0.41
0.64
0.52
2.5
0.52
0.57
0.45
0.65
0.44
0.52
0.39
0.36
0.31
0.14
0.14
0.44
0.40
0.19
0.69
4.0
2.5
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
0.50
0.58
0.44
0.58
0.35
0.58
2.5
0.67
0.63
0.84
0.42
0.63
2.5
0.90
1.0
0.65
0.52
0.34
2.5
0.50
0.41
0.64
0.52
2.5
0.52
0.57
0.45
0.65
0.44
0.52
0.39
0.36
0.31
0.14
0.14
0.44
0.40
0.19
0.69
4.0
2.5
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
4.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
5.0
Calculations are performed before rounding to avoid round-off errors in calculated results.
TestAmerica Tampa
Page 17 of 28
Quality Control Results
Client: ARCADIS U.S., Inc.
Job Number: 660-32804-1
Method Blank - Batch: 660-88145
Lab Sample ID:
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
MB 660-88145/3
Water
1.0
12/04/2009 1258
12/04/2009 1258
Method: 8260B
Preparation: 5030B
Analysis Batch: 660-88145
Prep Batch: N/A
Units: ug/L
Instrument ID: BVMJ GC/MS
Lab File ID:
1JL0411.D
Initial Weight/Volume: 5 mL
Final Weight/Volume: 5 mL
Analyte
Result
Qual
MDL
PQL
N-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
o-Xylene
Acetone
2-Butanone (MEK)
4-Methyl-2-pentanone (MIBK)
Carbon disulfide
2-Hexanone
Methyl tert-butyl ether
m-Xylene & p-Xylene
0.59
0.98
0.63
0.15
0.50
0.51
0.77
0.58
0.46
0.47
0.50
2.5
0.18
0.86
0.54
0.50
0.50
9.9
8.4
3.8
0.85
4.4
0.44
0.60
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
0.59
0.98
0.63
0.15
0.50
0.51
0.77
0.58
0.46
0.47
0.50
2.5
0.18
0.86
0.54
0.50
0.50
9.9
8.4
3.8
0.85
4.4
0.44
0.60
1.0
2.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
20
10
10
1.0
10
1.0
2.0
Surrogate
Toluene-d8 (Surr)
4-Bromofluorobenzene
Dibromofluoromethane
% Rec
Acceptance Limits
94
97
101
70 - 130
70 - 130
70 - 130
Calculations are performed before rounding to avoid round-off errors in calculated results.
TestAmerica Tampa
Page 18 of 28
Quality Control Results
Client: ARCADIS U.S., Inc.
Job Number: 660-32804-1
Lab Control Sample - Batch: 660-88145
Lab Sample ID:
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
LCS 660-88145/2
Water
1.0
12/04/2009 1151
12/04/2009 1151
Method: 8260B
Preparation: 5030B
Analysis Batch: 660-88145
Prep Batch: N/A
Units: ug/L
Instrument ID: BVMJ GC/MS
Lab File ID:
1JL0408.D
Initial Weight/Volume: 5 mL
Final Weight/Volume: 5 mL
Analyte
Spike Amount
Result
% Rec.
Limit
Benzene
Bromobenzene
1,2-Dichlorobenzene
Chlorobromomethane
Dichlorobromomethane
Bromoform
Bromomethane
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
Chlorodibromomethane
1,2-Dibromo-3-Chloropropane
Ethylene Dibromide
Dibromomethane
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
Hexachlorobutadiene
Isopropylbenzene
4-Isopropyltoluene
Methylene Chloride
Naphthalene
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.4
18.8
18.8
20.5
22.2
18.5
27.2
17.0
17.3
16.3
21.4
18.9
18.8
20.4
18.3
17.3
16.8
23.0
17.3
21.1
20.2
18.3
18.0
18.8
20.2
21.5
17.7
19.7
20.1
19.8
19.9
20.3
21.6
21.2
20.3
18.7
22.5
16.5
17.5
20.8
18.8
102
94
94
102
111
93
136
85
87
81
107
94
94
102
91
87
84
115
87
105
101
92
90
94
101
108
88
98
101
99
100
101
108
106
102
93
113
82
87
104
94
64 - 140
68 - 130
70 - 130
59 - 130
70 - 130
65 - 130
14 - 184
59 - 133
68 - 134
64 - 130
53 - 145
70 - 130
39 - 174
59 - 130
35 - 153
70 - 130
70 - 130
70 - 130
52 - 130
65 - 130
70 - 130
68 - 130
70 - 130
16 - 149
60 - 132
70 - 130
51 - 157
61 - 130
55 - 145
70 - 130
70 - 130
49 - 139
58 - 146
70 - 130
62 - 130
69 - 131
62 - 155
60 - 131
65 - 134
57 - 130
41 - 157
Calculations are performed before rounding to avoid round-off errors in calculated results.
TestAmerica Tampa
Page 19 of 28
Qual
Quality Control Results
Client: ARCADIS U.S., Inc.
Job Number: 660-32804-1
Lab Control Sample - Batch: 660-88145
Lab Sample ID:
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
LCS 660-88145/2
Water
1.0
12/04/2009 1151
12/04/2009 1151
Method: 8260B
Preparation: 5030B
Analysis Batch: 660-88145
Prep Batch: N/A
Units: ug/L
Instrument ID: BVMJ GC/MS
Lab File ID:
1JL0408.D
Initial Weight/Volume: 5 mL
Final Weight/Volume: 5 mL
Analyte
Spike Amount
Result
% Rec.
Limit
Qual
N-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
o-Xylene
Acetone
2-Butanone (MEK)
4-Methyl-2-pentanone (MIBK)
Carbon disulfide
2-Hexanone
Methyl tert-butyl ether
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
100
100
100
10.0
100
10.0
17.4
18.0
20.6
18.1
19.9
17.6
19.7
18.6
22.3
21.3
23.1
26.2
17.4
18.2
17.5
23.2
18.3
113
128
119
11.4
127
13.8
87
90
103
90
100
88
98
93
112
106
116
131
87
91
88
116
92
113
128
119
114
127
138
66 - 130
62 - 136
70 - 130
67 - 130
47 - 143
70 - 131
46 - 148
54 - 136
57 - 135
69 - 130
59 - 142
62 - 147
62 - 130
66 - 138
65 - 134
48 - 147
66 - 133
62 - 142
63 - 140
64 - 137
30 - 184
57 - 148
67 - 130
J3
Surrogate
Toluene-d8 (Surr)
4-Bromofluorobenzene
Dibromofluoromethane
% Rec
Acceptance Limits
97
93
108
70 - 130
70 - 130
70 - 130
Calculations are performed before rounding to avoid round-off errors in calculated results.
TestAmerica Tampa
Page 20 of 28
Quality Control Results
Client: ARCADIS U.S., Inc.
Job Number: 660-32804-1
Matrix Spike - Batch: 660-88145
Lab Sample ID:
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
660-32795-A-5 MS
Water
1.0
12/04/2009 2021
12/04/2009 2021
Method: 8260B
Preparation: 5030B
Analysis Batch: 660-88145
Prep Batch: N/A
Units: ug/L
Instrument ID: BVMJ GC/MS
Lab File ID:
1JL0430.D
Initial Weight/Volume: 5 mL
Final Weight/Volume: 5 mL
Analyte
Sample Result/Qual
Spike Amount
Result
% Rec.
Benzene
Bromobenzene
1,2-Dichlorobenzene
Chlorobromomethane
Dichlorobromomethane
Bromoform
Bromomethane
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
Chlorodibromomethane
1,2-Dibromo-3-Chloropropane
Ethylene Dibromide
Dibromomethane
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
0.50
0.58
0.44
0.58
0.35
0.58
2.5
0.67
0.63
0.84
0.42
0.63
2.5
0.90
1.0
0.65
0.52
0.34
2.5
0.50
0.41
0.64
0.52
2.5
10
0.57
0.45
0.65
0.44
0.52
0.39
0.36
0.31
0.14
0.14
0.44
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
21.0
19.0
18.6
23.1
23.1
20.4
28.3
14.5
15.6
16.2
21.9
18.5
16.8
21.3
22.9
17.0
14.6
24.6
20.0
23.5
21.6
18.0
17.1
14.2
29.7
22.3
15.7
21.2
19.0
22.3
21.4
19.6
20.2
20.6
18.7
16.2
105
95
93
115
116
102
142
73
78
81
110
93
84
106
114
85
73
123
100
118
108
90
86
71
97
111
78
106
95
111
107
98
101
103
94
81
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
Calculations are performed before rounding to avoid round-off errors in calculated results.
TestAmerica Tampa
Page 21 of 28
Limit
64 - 140
68 - 130
70 - 130
59 - 130
70 - 130
65 - 130
14 - 184
59 - 133
68 - 134
64 - 130
53 - 145
70 - 130
39 - 174
59 - 130
35 - 153
70 - 130
70 - 130
70 - 130
52 - 130
65 - 130
70 - 130
68 - 130
70 - 130
16 - 149
60 - 132
70 - 130
51 - 157
61 - 130
55 - 145
70 - 130
70 - 130
49 - 139
58 - 146
70 - 130
62 - 130
69 - 131
Qual
Quality Control Results
Client: ARCADIS U.S., Inc.
Job Number: 660-32804-1
Matrix Spike - Batch: 660-88145
Lab Sample ID:
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
660-32795-A-5 MS
Water
1.0
12/04/2009 2021
12/04/2009 2021
Method: 8260B
Preparation: 5030B
Analysis Batch: 660-88145
Prep Batch: N/A
Units: ug/L
Instrument ID: BVMJ GC/MS
Lab File ID:
1JL0430.D
Initial Weight/Volume: 5 mL
Final Weight/Volume: 5 mL
Analyte
Sample Result/Qual
Spike Amount
Result
% Rec.
Hexachlorobutadiene
Isopropylbenzene
4-Isopropyltoluene
Methylene Chloride
Naphthalene
N-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
o-Xylene
Acetone
2-Butanone (MEK)
4-Methyl-2-pentanone (MIBK)
Carbon disulfide
2-Hexanone
Methyl tert-butyl ether
0.40
0.19
0.69
4.0
2.5
0.59
0.98
0.63
0.15
0.50
0.51
0.77
0.58
0.46
0.47
0.65
2.5
0.18
0.86
0.54
0.50
0.50
37
8.4
3.8
0.85
4.4
0.44
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
100
100
100
10.0
100
10.0
20.2
14.6
12.7
19.4
3.43
15.8
4.12
20.7
20.3
20.5
16.7
19.0
16.3
22.2
23.8
24.3
27.7
21.1
3.46
6.15
22.2
12.7
179
151
152
11.1
160
14.4
101
73
64
97
17
79
21
103
101
103
83
95
82
111
119
118
138
106
17
31
111
63
142
151
152
111
160
144
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
I
U
U
U
U
U
U
U
U
U
U
U
Surrogate
% Rec
Toluene-d8 (Surr)
4-Bromofluorobenzene
Dibromofluoromethane
97
95
104
Calculations are performed before rounding to avoid round-off errors in calculated results.
TestAmerica Tampa
Page 22 of 28
Acceptance Limits
70 - 130
70 - 130
70 - 130
Limit
62 - 155
60 - 131
65 - 134
57 - 130
41 - 157
66 - 130
62 - 136
70 - 130
67 - 130
47 - 143
70 - 131
46 - 148
54 - 136
57 - 135
69 - 130
59 - 142
62 - 147
62 - 130
66 - 138
65 - 134
48 - 147
66 - 133
62 - 142
63 - 140
64 - 137
30 - 184
57 - 148
67 - 130
Qual
J3
I J3
J3
J3
J3
J3
J3
J3
J3
J3
Quality Control Results
Client: ARCADIS U.S., Inc.
Job Number: 660-32804-1
Duplicate - Batch: 660-88145
Lab Sample ID:
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
660-32794-A-1 DU
Water
10
12/04/2009 1822
12/04/2009 1822
Method: 8260B
Preparation: 5030B
Analysis Batch: 660-88145
Prep Batch: N/A
Units: ug/L
Instrument ID: BVMJ GC/MS
Lab File ID:
1JL0425.D
Initial Weight/Volume: 5 mL
Final Weight/Volume: 5 mL
Analyte
Sample Result/Qual
Result
RPD
Limit
Qual
Benzene
Bromobenzene
1,2-Dichlorobenzene
Chlorobromomethane
Dichlorobromomethane
Bromoform
Bromomethane
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
Chlorodibromomethane
1,2-Dibromo-3-Chloropropane
Ethylene Dibromide
Dibromomethane
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
Hexachlorobutadiene
Isopropylbenzene
4-Isopropyltoluene
5.0
5.8
4.4
5.8
3.5
5.8
25
6.7
6.3
8.4
4.2
6.3
25
9.0
10
6.5
5.2
3.4
25
5.0
4.1
6.4
5.2
25
23
5.7
19
200
4.4
5.2
3.9
3.6
3.1
1.4
1.4
4.4
4.0
1.9
6.9
5.0
5.8
4.4
5.8
3.5
5.8
25
6.7
6.3
8.4
4.2
6.3
25
9.0
10
6.5
5.2
3.4
25
5.0
4.1
6.4
5.2
25
21.2
5.7
17.1
191
4.4
5.2
3.9
3.6
3.1
1.4
1.4
4.4
4.0
1.9
6.9
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
7
NC
12
4
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
Calculations are performed before rounding to avoid round-off errors in calculated results.
TestAmerica Tampa
Page 23 of 28
U
U
U
U
U
U
U
U
U
U
U
U
Quality Control Results
Client: ARCADIS U.S., Inc.
Job Number: 660-32804-1
Duplicate - Batch: 660-88145
Lab Sample ID:
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
660-32794-A-1 DU
Water
10
12/04/2009 1822
12/04/2009 1822
Method: 8260B
Preparation: 5030B
Analysis Batch: 660-88145
Prep Batch: N/A
Units: ug/L
Instrument ID: BVMJ GC/MS
Lab File ID:
1JL0425.D
Initial Weight/Volume: 5 mL
Final Weight/Volume: 5 mL
Analyte
Sample Result/Qual
Result
RPD
Limit
Qual
Methylene Chloride
Naphthalene
N-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
o-Xylene
Acetone
2-Butanone (MEK)
4-Methyl-2-pentanone (MIBK)
Carbon disulfide
2-Hexanone
Methyl tert-butyl ether
m-Xylene & p-Xylene
40
25
5.9
9.8
6.3
1.5
5.0
5.1
7.7
5.8
4.6
4.7
1400
25
1.8
8.6
5.4
17
5.0
99
84
38
8.5
44
4.4
6.0
40
25
5.9
9.8
6.3
1.5
5.0
5.1
7.7
5.8
4.6
4.7
1320
25
1.8
8.6
5.4
15.8
5.0
99
84
38
8.5
44
4.4
6.0
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
5
NC
NC
NC
NC
5
NC
NC
NC
NC
NC
NC
NC
NC
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
Surrogate
% Rec
Toluene-d8 (Surr)
4-Bromofluorobenzene
Dibromofluoromethane
95
98
101
Calculations are performed before rounding to avoid round-off errors in calculated results.
TestAmerica Tampa
Page 24 of 28
Acceptance Limits
70 - 130
70 - 130
70 - 130
U
U
U
U
U
U
U
U
U
U
U J3
U
Quality Control Results
Client: ARCADIS U.S., Inc.
Job Number: 660-32804-1
Method Blank - Batch: 660-88144
Lab Sample ID:
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
Method: 8260C _SIM/ID
Preparation: 5030C
MB 660-88144/4
Water
1.0
12/04/2009 1258
12/04/2009 1258
Analysis Batch: 660-88144
Prep Batch: N/A
Units: ug/L
Instrument ID: BVMJ GC/MS
Lab File ID:
1JL0411.D
Initial Weight/Volume: 5 mL
Final Weight/Volume: 5 mL
Analyte
Result
Qual
MDL
PQL
1,4-Dioxane
1.0
U
1.0
2.0
Lab Control Sample - Batch: 660-88144
Lab Sample ID:
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
LCS 660-88144/3
Water
1.0
12/04/2009 1044
12/04/2009 1044
Method: 8260C _SIM/ID
Preparation: 5030C
Analysis Batch: 660-88144
Prep Batch: N/A
Units: ug/L
Instrument ID: BVMJ GC/MS
Lab File ID:
1JL0405.D
Initial Weight/Volume: 5 mL
Final Weight/Volume: 5 mL
Analyte
Spike Amount
Result
% Rec.
Limit
1,4-Dioxane
25.0
22.3
89
50 - 150
Matrix Spike - Batch: 660-88144
Lab Sample ID:
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
660-32795-A-5 MS
Water
1.0
12/04/2009 1956
12/04/2009 1956
Method: 8260C _SIM/ID
Preparation: 5030C
Analysis Batch: 660-88144
Prep Batch: N/A
Units: ug/L
Instrument ID: BVMJ GC/MS
Lab File ID:
1JL0429.D
Initial Weight/Volume: 5 mL
Final Weight/Volume: 5 mL
Analyte
Sample Result/Qual
Spike Amount
Result
% Rec.
1,4-Dioxane
1.0
25.0
22.9
92
U
Calculations are performed before rounding to avoid round-off errors in calculated results.
TestAmerica Tampa
Qual
Page 25 of 28
Limit
50 - 150
Qual
Quality Control Results
Client: ARCADIS U.S., Inc.
Job Number: 660-32804-1
Duplicate - Batch: 660-88144
Lab Sample ID:
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
660-32794-A-1 DU
Water
10
12/04/2009 1822
12/04/2009 1822
Method: 8260C _SIM/ID
Preparation: 5030C
Analysis Batch: 660-88144
Prep Batch: N/A
Units: ug/L
Instrument ID: BVMJ GC/MS
Lab File ID:
1JL0425.D
Initial Weight/Volume: 5 mL
Final Weight/Volume: 5 mL
Analyte
Sample Result/Qual
Result
RPD
Limit
1,4-Dioxane
260
376
37
50
Calculations are performed before rounding to avoid round-off errors in calculated results.
TestAmerica Tampa
Page 26 of 28
Qual
Page 27 of 28
Login Sample Receipt Check List
Client: ARCADIS U.S., Inc.
Job Number: 660-32804-1
Login Number: 32804
Creator: Harrison, Amanda
List Number: 1
List Source: TestAmerica Tampa
Question
T / F/ NA
Radioactivity either was not measured or, if measured, is at or below
background
The cooler's custody seal, if present, is intact.
N/A
The cooler or samples do not appear to have been compromised or
tampered with.
Samples were received on ice.
Cooler Temperature is acceptable.
True
Cooler Temperature is recorded.
COC is present.
COC is filled out in ink and legible.
COC is filled out with all pertinent information.
There are no discrepancies between the sample IDs on the containers and
the COC.
Samples are received within Holding Time.
Sample containers have legible labels.
Containers are not broken or leaking.
True
True
True
True
True
Sample collection date/times are provided.
Appropriate sample containers are used.
Sample bottles are completely filled.
There is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
VOA sample vials do not have headspace or bubble is <6mm (1/4") in
diameter.
If necessary, staff have been informed of any short hold time or quick TAT
needs
Multiphasic samples are not present.
Samples do not require splitting or compositing.
Is the Field Sampler's name present on COC?
Sample Preservation Verified
True
True
True
True
TestAmerica Tampa
Comment
True
True
True
True
True
True
True
True
True
True
True
True
Page 28 of 28
3.0 degrees C CU-07
ANALYTICAL REPORT
Job Number: 660-33568-1
Job Description: Raytheon
For:
ARCADIS U.S., Inc.
14055 Riveredge Drive
Suite 400
Tampa, FL 33637
Attention: Mr. Gus Suarez
_____________________________________________
Approved for release.
Natalie Tafuni
Project Manager I
2/1/2010 3:27 PM
Natalie Tafuni
Project Manager I
[email protected]
02/01/2010
cc:
Ms. Lyndi Mott
Mr. Melvin Rivera
Albert Zumbuhl
Methods: FDEP, DOH Certification #: TestAmerica Tampa E84282
These test results meet all the requirements of NELAC unless specified in the case narrative. All questions regarding
this test report should be directed to the TestAmerica Project Manager who signed this test report. The estimated
uncertainty associated with these reported results is available upon request. The results contained in this test report
relate only to these samples included herein.
TestAmerica Laboratories, Inc.
TestAmerica Tampa 6712 Benjamin Road, Suite 100, Tampa, FL 33634
Tel (813) 885-7427 Fax (813) 885-7049 www.testamericainc.com
Page 1 of 17
Job Narrative
660-33568-1
Comments
No additional comments.
Receipt
All samples were received in good condition within temperature requirements.
Page 2 of 17
EXECUTIVE SUMMARY - Detections
Client: ARCADIS U.S., Inc.
Lab Sample ID
Analyte
660-33568-1
Client Sample ID
Result / Qualifier
1,4-Dioxane
Units
Method
4.9
2.0
ug/L
8260C _SIM/ID
2.1
2.0
ug/L
8260C _SIM/ID
58
2.0
ug/L
8260C _SIM/ID
IMW-V_012910
1,4-Dioxane
660-33568-3
Reporting
Limit
IMW-21_012910
1,4-Dioxane
660-33568-2
Job Number: 660-33568-1
SMW-B_012910
TestAmerica Tampa
Page 3 of 17
METHOD SUMMARY
Client: ARCADIS U.S., Inc.
Description
Job Number: 660-33568-1
Lab Location Method
Preparation Method
Matrix: Water
1,4-Dioxane by SIM/Isotopic Dilution
Purge and Trap
TAL TAM
TAL TAM
SW846 8260C _SIM/ID
SW846 5030C
Lab References:
TAL TAM = TestAmerica Tampa
Method References:
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
TestAmerica Tampa
Page 4 of 17
METHOD / ANALYST SUMMARY
Client: ARCADIS U.S., Inc.
Job Number: 660-33568-1
Method
Analyst
SW846 8260C _SIM/ID
Harris, Chris
TestAmerica Tampa
Page 5 of 17
Analyst ID
CH
SAMPLE SUMMARY
Client: ARCADIS U.S., Inc.
Job Number: 660-33568-1
Lab Sample ID
Client Sample ID
Client Matrix
660-33568-1
660-33568-2
660-33568-3
660-33568-4
IMW-21_012910
IMW-V_012910
SMW-B_012910
Trip Blank_012910
Water
Water
Water
Water
TestAmerica Tampa
Page 6 of 17
Date/Time
Sampled
01/29/2010
01/29/2010
01/29/2010
01/29/2010
1008
1119
1230
1008
Date/Time
Received
01/29/2010
01/29/2010
01/29/2010
01/29/2010
1315
1315
1315
1315
SAMPLE RESULTS
TestAmerica Tampa
Page 7 of 17
Analytical Data
Client: ARCADIS U.S., Inc.
Job Number: 660-33568-1
Client Sample ID:
IMW-21_012910
Lab Sample ID:
Client Matrix:
660-33568-1
Water
Date Sampled: 01/29/2010 1008
Date Received: 01/29/2010 1315
8260C _SIM/ID 1,4-Dioxane by SIM/Isotopic Dilution
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260C _SIM/ID
5030C
1.0
02/01/2010 1221
02/01/2010 1221
Analyte
1,4-Dioxane
TestAmerica Tampa
Analysis Batch: 660-90107
Result (ug/L)
4.9
Page 8 of 17
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Qualifier
MDL
1.0
BVMM5971
1MB0109.D
5 mL
5 mL
PQL
2.0
Analytical Data
Client: ARCADIS U.S., Inc.
Client Sample ID:
IMW-V_012910
Lab Sample ID:
Client Matrix:
660-33568-2
Water
Job Number: 660-33568-1
Date Sampled: 01/29/2010 1119
Date Received: 01/29/2010 1315
8260C _SIM/ID 1,4-Dioxane by SIM/Isotopic Dilution
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260C _SIM/ID
5030C
1.0
02/01/2010 1240
02/01/2010 1240
Analyte
1,4-Dioxane
TestAmerica Tampa
Analysis Batch: 660-90107
Result (ug/L)
2.1
Page 9 of 17
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Qualifier
MDL
1.0
BVMM5971
1MB0110.D
5 mL
5 mL
PQL
2.0
Analytical Data
Client: ARCADIS U.S., Inc.
Job Number: 660-33568-1
Client Sample ID:
SMW-B_012910
Lab Sample ID:
Client Matrix:
660-33568-3
Water
Date Sampled: 01/29/2010 1230
Date Received: 01/29/2010 1315
8260C _SIM/ID 1,4-Dioxane by SIM/Isotopic Dilution
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260C _SIM/ID
5030C
1.0
02/01/2010 1301
02/01/2010 1301
Analyte
1,4-Dioxane
TestAmerica Tampa
Analysis Batch: 660-90107
Result (ug/L)
58
Page 10 of 17
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Qualifier
MDL
1.0
BVMM5971
1MB0111.D
5 mL
5 mL
PQL
2.0
Analytical Data
Client: ARCADIS U.S., Inc.
Job Number: 660-33568-1
Client Sample ID:
Trip Blank_012910
Lab Sample ID:
Client Matrix:
660-33568-4
Water
Date Sampled: 01/29/2010 1008
Date Received: 01/29/2010 1315
8260C _SIM/ID 1,4-Dioxane by SIM/Isotopic Dilution
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260C _SIM/ID
5030C
1.0
02/01/2010 1103
02/01/2010 1103
Analyte
1,4-Dioxane
TestAmerica Tampa
Analysis Batch: 660-90107
Result (ug/L)
1.0
Page 11 of 17
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Qualifier
U
MDL
1.0
BVMM5971
1MB0108.D
5 mL
5 mL
PQL
2.0
DATA REPORTING QUALIFIERS
Client: ARCADIS U.S., Inc.
Lab Section
Job Number: 660-33568-1
Qualifier
Description
U
Indicates that the compound was analyzed for but not
detected.
GC/MS VOA
TestAmerica Tampa
Page 12 of 17
QUALITY CONTROL RESULTS
TestAmerica Tampa
Page 13 of 17
Quality Control Results
Client: ARCADIS U.S., Inc.
Job Number: 660-33568-1
Method Blank - Batch: 660-90107
Lab Sample ID:
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
Method: 8260C _SIM/ID
Preparation: 5030C
MB 660-90107/2
Water
1.0
02/01/2010 1026
02/01/2010 1026
Analysis Batch: 660-90107
Prep Batch: N/A
Units: ug/L
Instrument ID: 5971 GC/MS
Lab File ID:
1MB0106.D
Initial Weight/Volume: 5 mL
Final Weight/Volume: 5 mL
Analyte
Result
Qual
MDL
PQL
1,4-Dioxane
1.0
U
1.0
2.0
Lab Control Sample - Batch: 660-90107
Lab Sample ID:
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
LCS 660-90107/1
Water
1.0
02/01/2010 0947
02/01/2010 0947
Method: 8260C _SIM/ID
Preparation: 5030C
Analysis Batch: 660-90107
Prep Batch: N/A
Units: ug/L
Instrument ID: 5971 GC/MS
Lab File ID:
1MB0104.D
Initial Weight/Volume: 5 mL
Final Weight/Volume: 5 mL
Analyte
Spike Amount
Result
% Rec.
Limit
1,4-Dioxane
25.0
26.8
107
50 - 150
Matrix Spike - Batch: 660-90107
Lab Sample ID:
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
660-33568-1
Water
1.0
02/01/2010 1338
02/01/2010 1338
Method: 8260C _SIM/ID
Preparation: 5030C
Analysis Batch: 660-90107
Prep Batch: N/A
Units: ug/L
Instrument ID: 5971 GC/MS
Lab File ID:
1MB0113.D
Initial Weight/Volume: 5 mL
Final Weight/Volume: 5 mL
Analyte
Sample Result/Qual
Spike Amount
Result
% Rec.
1,4-Dioxane
4.9
25.0
30.1
101
Calculations are performed before rounding to avoid round-off errors in calculated results.
TestAmerica Tampa
Qual
Page 14 of 17
Limit
50 - 150
Qual
Quality Control Results
Client: ARCADIS U.S., Inc.
Job Number: 660-33568-1
Duplicate - Batch: 660-90107
Lab Sample ID:
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
660-33568-1
Water
1.0
02/01/2010 1319
02/01/2010 1319
Method: 8260C _SIM/ID
Preparation: 5030C
Analysis Batch: 660-90107
Prep Batch: N/A
Units: ug/L
Instrument ID: 5971 GC/MS
Lab File ID:
1MB0112.D
Initial Weight/Volume: 5 mL
Final Weight/Volume: 5 mL
Analyte
Sample Result/Qual
Result
RPD
Limit
1,4-Dioxane
4.9
8.00
48
50
Calculations are performed before rounding to avoid round-off errors in calculated results.
TestAmerica Tampa
Page 15 of 17
Qual
Page 16 of 17
Login Sample Receipt Check List
Client: ARCADIS U.S., Inc.
Job Number: 660-33568-1
Login Number: 33568
Creator: Volz, Charles
List Number: 1
List Source: TestAmerica Tampa
Question
T / F/ NA
Radioactivity either was not measured or, if measured, is at or below
background
The cooler's custody seal, if present, is intact.
The cooler or samples do not appear to have been compromised or
tampered with.
Samples were received on ice.
Cooler Temperature is acceptable.
Cooler Temperature is recorded.
COC is present.
COC is filled out in ink and legible.
COC is filled out with all pertinent information.
There are no discrepancies between the sample IDs on the containers and
the COC.
Samples are received within Holding Time.
Sample containers have legible labels.
Containers are not broken or leaking.
Sample collection date/times are provided.
Appropriate sample containers are used.
Sample bottles are completely filled.
There is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
VOA sample vials do not have headspace or bubble is <6mm (1/4") in
diameter.
If necessary, staff have been informed of any short hold time or quick TAT
needs
Multiphasic samples are not present.
Samples do not require splitting or compositing.
Is the Field Sampler's name present on COC?
Sample Preservation Verified
N/A
Comment
True
True
True
True
True
True
True
True
True
True
True
True
True
True
True
True
True
True
True
True
True
True
TestAmerica Tampa
Page 17 of 17
4.3 Degrees C. CU-07
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