ICP Test Report Certification Packet
Company name :
Littelfuse, Inc.
Product Series:
Pico
Product #:
473xxxHF Series
Issue Date:
May 23, 2011
It is hereby certified by Littelfuse, Inc. that there is neither RoHS (EU Directive
2002/95/EC)-restricted substance nor such use, for materials to be used for unit parts, for
packing/packaging materials, and for additives and the like in the manufacturing processes.
In addition, it is hereby reported to you that the parts and sub-materials, the materials to be used
for unit parts, the packing/packaging materials, and the additives and the like in the manufacturing
processes, are all composed of the following components.
Issued by:
<Global EHS Engineer>
(1) Parts, sub-materials and unit parts
This document covers the Pico RoHS-Compliant series products manufactured by
Littelfuse, Inc.
＜ Raw Materials Used
Please see Table 1
(2) The ICP data on all measurable substances
Please see appropriate pages as identifed in Table 1
Remarks：
Pb (lead) contained in the high temperature melting solder > 85% and is categorized as
exempt under section 7a of the RoHS Annex.
Form 585-047 Rev. A
1
2/21/06
Table 1: List of Raw Materials covered by this report
Total Parts
1
2
3
4
5
6
7
8
Raw Material Part Number
909-371
082xxx-001
692320
910-271
648102
648106-001
648112-001
087340
Raw Material Description
Body
Element - 99% Cu Sn Plated
Solder
Caps & Lead Assay
Yarn
Yarn
Yarn
Epoxy Powder (HF Gold)
2
Page(s)
3-8
9-15
16-21
22-26
27-33
34-39
40-45
46-52
Test Report
Applicant:
Number : TWNC00176941
Littelfuse, Philippines Inc.
LIMA Technology Center, Lipa City,
Malvar, Batangas
Date
: Oct 08, 2010
Sample Description:
One (1) group of submitted samples said to be :
Part Description
: Body
Part Number
: 909-371
Date Sample Received
: Oct 04, 2010
Date Test Started
: Oct 05, 2010
Test Conducted :
As requested by the applicant, for details please refer to attached pages.
Authorized By:
On Behalf Of Intertek Testing Services
Taiwan Limited
K. Y. Liang
Director
This report shall not be reproduced
except in full, without the written
approval of the laboratory.
Page 1 Of 6
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00176941
Test Conducted
(Ⅰ) Test Result Summary :
Testing Item
Result (ppm)
Gray Material
Heavy Metal
Cadmium (Cd) content
Lead (Pb) content
Mercury (Hg) content
Chromium VI (Cr6+) content
Polybrominated Biphenyls (PBBs)
Monobrominated Biphenyls (MonoBB)
Dibrominated Biphenyls (DiBB)
Tribrominated Biphenyls (TriBB)
Tetrabrominated Biphenyls (TetraBB)
Pentabrominated Biphenyls (PentaBB)
Hexabrominated Biphenyls (HexaBB)
Heptabrominated Biphenyls (HeptaBB)
Octabrominated Biphenyls (OctaBB)
Nonabrominated Biphenyls (NonaBB)
Decabrominated Biphenyl (DecaBB)
Polybrominated Diphenyl Ethers (PBDEs)
Monobrominated Diphenyl Ethers (MonoBDE)
Dibrominated Diphenyl Ethers (DiBDE)
Tribrominated Diphenyl Ethers (TriBDE)
Tetrabrominated Diphenyl Ethers (TetraBDE)
Pentabrominated Diphenyl Ethers (PentaBDE)
Hexabrominated Diphenyl Ethers (HexaBDE)
Heptabrominated Diphenyl Ethers (HeptaBDE)
Octabrominated Diphenyl Ethers (OctaBDE)
Nonabrominated Diphenyl Ethers (NonaBDE)
Decabrominated Diphenyl Ether (DecaBDE)
Halogen Content
Fluorine (F)
Chlorine (Cl)
Bromine (Br)
Iodine (I)
ND
94
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Remarks: ppm = Parts per million based on weight of tested sample = mg/kg
ND = Not detected
Responsibility Of Chemist : Irene Chiou / Kevin Liu / Cathy Chen
Date Sample Received
Testing Period
: Oct 04, 2010
: Oct 05, 2010 To Oct 07, 2010
Page 2 Of 6
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00176941
Test Conducted
(Ⅱ) RoHS Requirement:
Restricted Substances
Cadmium (Cd) Content
Lead (Pb) Content
Mercury (Hg) Content
Chromium VI (Cr6+) Content
Polybrominated Biphenyls (PBBs)
Polybrominated Diphenyl Ehters (PBDEs)
Limits
0.01% (100ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for
homogeneous material.
(Ⅲ) Test Method:
Testing Item
Cadmium (Cd)
content
Lead (Pb) content
Mercury (Hg)
content
Chromium VI (Cr6+)
content
Polybrominated
Biphenyls (PBBs)
Polybrominated
Diphenyl Ethers
(PBDEs)
Halogen Content
Testing Method
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 7, by microwave
digestion until the tested samples are
totally dissolved and determined by
ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in annex C, by alkaline
digestion and determined by UV-Vis
spectrophotometer.
With reference to IEC 62321 edition
1.0:2008 in annex A, by solvent
extraction and determined by GC-MSD
and further HPLC confirmation when
necessary.
With reference to IEC 62321 edition
1.0:2008 in annex A, by solvent
extraction and determined by GC-MSD
and further HPLC confirmation when
necessary.
With reference to EN 14582:2007 by
calorimetric bomb with oxygen and
determined by ion chromatography
Reporting Limit
2 ppm
2 ppm
2 ppm
1 ppm
5 ppm
5 ppm
50 ppm
Remark: Reporting limit = Quantitation limit of analyte in sample
Page 3 Of 6
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00176941
Test Conducted
(Ⅳ) Measurement Flowchart:
Test For Cd/Pb/Hg/Chromium (VI)/PBBS/PBDES Contents
Reference Standard: IEC 62321 edition 1.0:2008
Sampling/grinding or cutting
Cd/Pb/Hg
Cr
Weigh sample and
add organic solvent
By spot test
Negative
Confirm the tested
samples are
totally dissolved
Make up with
deionized water
PBBs/PBDEs
Polymers /
electronics
Metal
For different
material, digest
the sample with
*1
appropriate acid
6+
Get 50cm2 sample
By boiling water
extraction
*2
Weigh sample
and add
alkaline
solution
By Soxhlet
extraction or
Solvent extraction
Definite temp.
extraction
Cool and filter
the extract
Concentrate the
extract and make up
with organic
solvent
Analyzed by ICP-OES
Analyzed by GC-MSD
Make up with deionized
water and add diphenylcarbazide solution
Remarks:
*1: List Of Appropriate Acid：
Material
Polymers
Metals
Electronics
Analyzed by UV-VIS
Acid Added For Digestion
HNO3,HCl,HF,H2O2,H3BO3
HNO3,HCl,HF
HNO3,HCl,H2O2,HBF4
*2: If the result of spot test is positive, Chromium VI would be determined as detected.
Page 4 Of 6
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00176941
Test Conducted
(Ⅳ) Measurement Flowchart:
Test For Halogen Content
Reference Standard： EN 14582
Sampling/grinding or
cutting
Add absorbent in a
calorimetric bomb &
place weighed sample in
equipment
Fill the calorimetric
bomb with oxygen
Ignite then leave the
flask at room
temperature
Transfer the absorbent
into a volumetric flask
Make up with deionized
water
Analyzed by ion
chromatography
End Of Report
Page 5 Of 6
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00176941
Test Conducted
Photo
Page 6 Of 6
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Validi
ForQu
Please
Test Report
No.i CE/2010/C0089D4e | 2O1U12108 Page: I of 7
POLYFILAG
OBERALLMENDSTRASSE
2OA,CH{3OOZUG/ SWITZERLAND
Thefollowingsampte(s)tuas/weresubmitted and identified by/on
SampleDe6cription
Buye/OrderNo.
SampleReceiving
Date
TestingPeriod
Cugg.gMSn
104987
2010t12t01
2010t12t0110 201u 12t08
TestReeult(s)
Pleasereferto nextpage(s).
l]
behalf of the cliont as:
g|||d6.||d
66{cd
lrtadory
cmFnyl trii, { ;,l|t,
- f*d
aG)r8dd
rh s 16! mpod €md
! . 1 , + 1 j , ' 1 t t i : Ji . l . r i i l . r i r r t : = t j : . , t . r . . . . , r { } ! .
ftseumed3$cdbylhecomFnysuqadbi9G6a6|cmdfuBdSa
t* abrmt
tomd do.lm6tu
s6i
b€ €
g *"-,*rn,
lb'.qhbds|€*trssdlb'6
! iddrarzoE.ri*,.o!d!riiwld/r,t6i
Ilr:
rcnoi,
so*r
ttt
ttltl
TestReport
No.I CE2010IC0089 Date: 2010/1208 P a g e t 2 o l T
POLYFILAG
OBEMLLMENOSTRASSE
2OA,CH63OOZUG/ SWITZERLAND
ll!][ttt
Test Ro€ult{sl
PARTNAMENo.1
SILVERCOLOREDMETALWIRE
Testltem (s):
Unit
Cadmium(Q)
Method
MDL
mg/Kg Withreference
to IEC62321:2008anC
2
mgag Withreference
to tEcG232iJZdd8
andperformed
byICP-AES.
mg/Kg Withreference
to lECGI321l2666?iI
perfomed
byICP-AES.
2
performed
by ICP-AES.
Lead (Pb)
Mercury(Hg)
Hexavaler(
Chromium
-r(Vt)If
Spottest / boilingwaterextraction
Halogen
Halogen-Fluodne
(F)
(CASNo.:014762-94-8)
Halogen-Chlorine
(Cl)
(CASNo.:022537-15-1)
Halogen-Bromine
(Br)
(C.AS
No.| 010097-32-2)
Hexabromobiphenyl
Heptabromobiphenyl
Oclabromobiphenyl
Nonabromobiphenyl
Decabromobiphenyl
n.o,
Withreference
to IEC62321:2008€nd 0.02mg/kg Negative
performedby Spottest/ boilingwater with50cm,
extraclionMethod.(SeeNote6)
surtace
Withreferenceto BS EN 1458212007.
mg/Kg
Analysiswasperformedby lC.
Halogenlodine
(l)
(CASNo.i01436244-8)
Sumof PBBS
Monobromobiphenyl
Dibromobiphenyl
Tribrcmobiphenyl
Tetrabromobiphenyl
Pentabromobiphenyl
Result
No.l
n.o.
50
n.d.
50
n.d.
50
n.d.
50
n.d.
n.o.
mg/Kg
n.d.
n.d.
n.d.
n.d.
n.d,
n.d.
n.d.
n.d.
With referenceto IEC 62321:2008€nd
perfomed by GC/MS.
n.o.
5
'n1h!Bll6p.nGi€l0ilybhsgmp3G)bddThsb3i@d€nidbtrFd
cdFry rr'rrEl. i ]i .r 1r r?rFlri dllli ilr, r jr l.ii,rl-\-+:i
nj6d@md€]fudbylbconpanysUqedbbcae6!coidlo^5o's
t
.f r-lrtz]]!.
!,tr :
rr
Ii.]ri
(,e6r]D
n.o.
tt
l
TestReport
No.: CE/201CyC0089
D?f.e
:2O1Oh2tO8P e g e : 3 o f 7
POLYFILAG
OBEMLLMENDSTRASSE
2OA,CH63OO
ZUG/ SWITZERLANO
Test ltem (s):
Sumof PBDES
It4onobomodiphenyl
ether
Dbromodiphenyt
ether
f ribromodiphenyl
ether
Ietrabromodiphenyi
ettter
Pentabromodiphenyl
ether
Unit
mg/kg
Hexablomodiphenyt
ether
rtr] lr||tflrltl!
Mothod
MDL
Withreference
to tEC62321i2OO8
end
performedby GC/[/|S.
Heptabromodiphenyl
ether
Octabromodiphenyl
ether
Nonabromodiphenyl
ether
Decabbmodiphenyl
ether
5
5
5
5
5
5
Result
No.1
n.d.
n.d.
n.d.
n.d.
n.o.
n.d.
n-d.
n.d.
n.d.
n.d.
n.d.
Note:
1. mg/kg= ppm i 0.1wt%= lOOOppm
2. n.d.= Not Detecled
3. MDL= MothodDet€ctionLimit
4-"-"=NotRegulated
5. " = Qualitative
analysis
(NoUnit)
6. Spot-test:
Negative= Abs€nceof cr(vr) coating/ surfac€rayer;po.irive = presenceof cr(vr) coating/ surfacerayer;
(Thet€stedsampleshouldbefurtherverifiedby boaling-water-extraction
methodif thespottestresultcannot
be confi|med.)
BoiIing-eEter-extraction:
Negative= Absenceof Cr(Vl)coating/ surfacetayer; positive= Presenceof Cr(Vl)coating/ surfacelayea;
Thedetected
concent€tion
in boiling-water-extraction
solutionis equalor greaterthan0.02mg/kgwith50cm,
samDlegurfacearea.
cmFiy
ror ebdmd
lLI1l,: rtnr
..I!!li
1i.'-.:11,l.tlltr
^y3u!,adloisG4e6|cddi66olS
ionnd @msnb
su!
siirri
.i :
.
-i :i: j. :
rlanrjt.
f u f ' g h a a d @ E d l o n s u 6 l f u l € m o l b e b p o d u d * c a p l n f u l * i h d
rHr li i::
'rri:.4 r +$6rcrrne
MembsorhescsGolp665sAl
Test Report
No.: CEI2010/C0089Date| 2O1Ot12tO8P age:4 ol7
POLYFILAG
OBEMLLITIENDSTMSSE2OA,CH-6300ZUG / SWTTZERLAND
lllutI|lll|l||tlll
1) Th€s.esafiples were dissoh/€dtotalv by pre-conditioningnEthod
according to below flow chart
I ur tesl rEthod ercluded)
2) Narneof tho personwho rEde llEasurenEr t Climbgreat yang
3) llarE ofthe personin cha.geof nEasuremeit:TroyChang
Cutting/ Preparatbn
Aciddigestion
by suitaueacid
dependedon differentsanDle
nEterial(as belowtabte)
Microwavedigestionwith
HI.IOJHCUHF
Addappropdateanbuntof
digestionreagent
lleat to appropriate
tefiperatureto extrerct
'l) AlkaliFusion
2) rclto dissotue
Add diphenyl-carbezide
for
colordevelopnEnt
Safipb Matedal
DigestionAcid
Steel,copper,
aluninum,solder
Aqua regia,HNO3,HCl,HF,H2O,
Gbss
HNO3/HF
Gold,platinunpalladium,
ceraric
Aquaregia
Situer
HNO3
Plastic
ft so4, ft or, HNo3,Hcl
Others
Anyacidto totaldigestion
cmp.iyi'j|,j.':i;',tti1:.:}lJ::.;iljiii1i..ftl1.}i{.]]
n3dms'€csuadbyihecomp'iy5u$d|oGc*6|cdrddoBols
rq 0i.d,6c romd e{ims6
su!6d b r6ms ad codroB rd Erdm.
Ibr'qhtsaM@|Fd65tldlful€
M'on6 rary rEcm@rsso6i€
0o@m6n5d *w sls 6d1.n:
6i.amd
rEasure the ab60rbance
at 540 nmby W-VIS
hm Ard o; s dtui
ro rhe ,mMlo d ,ab,q
msd dk ^d dssEb Fi€s b a r&
Test Report
No.: CE/2010/C0089Oate:2OiOhZO8 P a g e : 5 o f 7
POLYFILAG
OBEMLLMENDSTRASSE2OA,CH63OOZUG / SWITZERTAND
[
[llt]|||tt
Analtticalflow chartof halogencontgnt
1) ll€rle of the p€rsonwho rnade nEasurenEnt: Rita Chen
2) t,lanF ofthe personin chargeof ftEasurenEnt:TroyChang
Saftplepretreatment
/ Separation
Weighting
andputtingsanplein cell
OrygenBombCoflbustion
/AbsoDtion
Dilutionto fixedvoluftE
Analysiswaspertorr€d b\, lC
'
. + :
n6ddmdA3Gbyhecorr
ior€edrcnc foma' doondG. subl
n Gfio.tsh6 comFiy 3 r id]^gs ar bs
rharl'drbadd
0d ms undd66 tra
sponebrt 3ro b cttrr ands s tu6
.ji
.r
ftr
rlif . ti,eozrrer&r+86
arrszT
!__{,<,,
TestReport
No.: CE2010/C0089 Datet2010/1|2108page:6 of z
POLYFIL
AG
OBERALLMENDSTMSSE
2OA,CH$3OO
ZUG/ SWITZERLAND
trl| [tt||||!tllt
PBB/PBDEanatyticatFLOWCHART
1) tbnE of thepe6on who fibcle rEasureriEnl. Rormn Wono
2) Mrne of the personin chargeof i€asurenent: troy Cnanpf
Firsttestingprocess-----'
Odionalscreenprocess--.Confinmtion
process - .>
Screenanalysis
Sanple
extractiod
I
Soxhtet
I=----r----- nEthod
I
I
ConcentratdDilute
Extractedsolulion
t
Filter
-I - - - - - - - - - . - - - - -
I
Analysis
by GC/MS
- il i i : r t r 1 ; , : , r r t : , : . i i i
. l . r i - r t. : : r ; I . . .
n1:.
ny&qed|oiscme6|cddioBolsg
'd.e@,domd
@metu
sdi
, eoamen{hm a,en,o; s d€". ; h"t.6,rerons f 'ny rh. cnpanys $ s,*
d
"b
a
TestReport
No.: CE2010/C0089 Dale| 2O1Ot1ZOaP a g e : 7 o f 7
POLYFILAG
OBERALLMENDSTMSSE2OA,CHS3OOZUG / SWITZERLAND
I|]t|:tt]t||lrl|t
c0089
" Endof Report "
c d n p ' ^ ri : r ' 1 r r l t . , t r r l i r r . r ' r ?.j, r 1 r l t e i . J . : t 1 l t i r . : r \ n r L ! 1 . , i , .
rc ed,mr
rdmai @i.d3
rl1r1..
slq
s enotumemhh
o n t a n dw l h i h 6 r m c d c . d s n r
ndb..qducdoxc€p{iful*lbdl
lPe.o{'rliwai/irLL:jrt]'ItrlB
fr.d,o;
E d,en
Test Report
No: 10222124(1)
Date: 19-Jan-11
Page 1 of 6
Kester Components Pte Ltd
500 Chai Chee Lane, Singapore 469024
The following sample(s) was/were submitted and identified by/on behalf of the client as:
Sample Description
:
RK-3-K71 (P/N: 692320 / Lot: 1004401007)
Sample Receiving Date
Testing Period
:
:
12-Jan-11
13-Jan-11 to 18-Jan-11
Test Requested
:
In accordance with the RoHS Directive 2002/95/EC, and its amendment
directives.
Test Result(s)
:
Please refer to next page(s).
Conclusion
:
Based on the performed tests on submitted sample(s), the results comply
with the RoHS Directive 2002/95/EC and its subsequent amendments.
Signed for and on behalf of
SGS Testing & Control Services Singapore Pte Ltd
Y.C. Tham
Laboratory Manager
Test Location: 26 Ayer Rajah Crescent, #07-08, Singapore 139944
This document is issued by the Company under its General Conditions of Service accessible at www.sgs.com/terms_and_conditions.htm and, for electronic format
documents, subject to Terms and Conditions for Electronic Documents at www.sgs.com/terms_e-document.htm. Attention is drawn to the limitation of liability,
indemnification and jurisdiction issues defined therein. Any holder of this document is advised that information contained hereon reflects the Company’s findings at the time
of its intervention only and within the limits of Client’s instructions, if any. The Company’s sole responsibility is to its Client and this document does not exonerate parties to
a transaction from exercising all their rights and obligations under the transaction documents. Any unauthorized alteration, forgery or falsification of the content or
appearance of this document is unlawful and offenders may be prosecuted to the fullest extent of the law. Unless otherwise stated the results shown in this test report refer
only to the sample(s) tested and such sample(s) are retained for 30 days only. This document cannot be reproduced except in full, without prior approval of the Company.
SGS Testing & Control Services Singapore Pte Ltd
26 Ayer Rajah Crescent #03-07 Singapore 139944 t +65 6379 0111 f+65 6777 2914 www.sgs.com
Member of SGS Group
Test Report
No: 10222124(1)
Date: 19-Jan-11
Page 2 of 6
Test Result(s):
Sample Description
:
Test Item(s):
RK-3-K71 (P/N: 692320 / Lot: 1004401007)
Unit
Method
Results
MDL
RoHS Limit
Cadmium(Cd)
mg/kg With reference to IEC62321,
Ed1:2008. Analysis was
performed by ICP/AES
n.d.
2
100
Lead (Pb)
mg/kg With reference to IEC62321,
Ed1:2008. Analysis was
performed by ICP/AES
901893.9+
2
1000
Mercury (Hg)
mg/kg With reference to IEC62321,
Ed1:2008. Analysis was
performed by ICP/AES
n.d.
2
1000
Negative
0.02 mg/kg
with 50 cm2
surface area
#
n.d.
n.d.
n.d.
n.d.
n.d.
n.d.
n.d.
n.d.
n.d.
n.d.
n.d.
n.d.
n.d.
n.d.
n.d.
n.d.
n.d.
n.d.
n.d.
n.d.
n.d.
n.d.
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
1000
1000
-
Hexavalent Chromium (CrVI)
(By spot test / boiling water
extraction)
Sum of PBBs
Monobromobiphenyl
Dibromobiphenyl
Tribromobiphenyl
Tetrabromobiphenyl
Hexabromobiphenyl
Pentabromobiphenyl
Heptabromobiphenyl
Octabromobiphenyl
Nonabromobiphenyl
Decabromobiphenyl
Sum of PBDEs
Monobromodiphenyl ether
Dibromodiphenyl ether
Tribromodiphenyl ether
Tetrabromodiphenyl ether
Pentabromodiphenyl ether
Hexabromodiphenyl ether
Heptabromodiphenyl ether
Octabromodiphenyl ether
Nonabromodiphenyl ether
Decabromodiphenyl ether ##
---
With reference to IEC62321,
Ed1:2008 and performed by Spot
test / boiling water extraction
method. (see Note 9)
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
With reference to IEC62321,
mg/kg
Ed1:2008. Analysis was
mg/kg
performed by GC/MS
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
Test Location: 26 Ayer Rajah Crescent, #07-08, Singapore 139944
This document is issued by the Company under its General Conditions of Service accessible at www.sgs.com/terms_and_conditions.htm and, for electronic format documents,
subject to Terms and Conditions for Electronic Documents at www.sgs.com/terms_e-document.htm. Attention is drawn to the limitation of liability, indemnification and
jurisdiction issues defined therein. Any holder of this document is advised that information contained hereon reflects the Company’s findings at the time of its intervention only
and within the limits of Client’s instructions, if any. The Company’s sole responsibility is to its Client and this document does not exonerate parties to a transaction from
exercising all their rights and obligations under the transaction documents. Any unauthorized alteration, forgery or falsification of the content or appearance of this document is
unlawful and offenders may be prosecuted to the fullest extent of the law. Unless otherwise stated the results shown in this test report refer only to the sample(s) tested and
such sample(s) are retained for 30 days only. This document cannot be reproduced except in full, without prior approval of the Company.
SGS Testing & Control Services Singapore Pte Ltd
26 Ayer Rajah Crescent #03-07 Singapore 139944 t +65 6379 0111 f+65 6777 2914 www.sgs.com
Member of SGS Group
Test Report
No: 10222124(1)
Date: 19-Jan-11
Page 3 of 6
Note:
(1) mg/kg = ppm ; 0.1wt% = 1000ppm
(2) n.d.= Not Detected
(3) MDL = Method Detection Limit
(4) ## = The exemption of DecaBDE in polymeric application according 2005/717/EC was
overruled by the European Court of Justice by its decision of 01.04.2008. Subsequently
DecaBDE will be included in the sum of PBDE after 01.07.2008.
(5) “-“ = Not regulated
(6) “---“: No unit (Qualitative Test)
(7) * : Exceeds limit
(8) # : Positive means the presence of CrVI on the tested areas.
Negative means the absence of CrVI on the tested areas.
(9) Spot-test:
Negative = Absence of Cr(VI) coating / surface layer
Positive = Presence of Cr(VI) coating / surface layer
The tested sample should be further verified by boiling-water-extraction method if the spot
test result cannot be confirmed.
Boiling-water extraction:
Negative = Absence of Cr(VI) coating / surface layer
Positive = Presence of Cr(VI) coating / surface layer
the detected concentration in boiling-water-extraction solution is equal or greater
2
than 0.02 mg/kg with 50 cm sample surface area.
+
Exemption: The received sample is exempted under directive 2002/95/EC Annex Article 7: lead in high
melting temperature solder type solders (i.e. tin-lead solder alloys containing more than 85% of lead).
Lab Analyst(s): Jay, Jojo and Eileen
Remarks: Sample received was totally dissolved by preconditioning method.
Sample photo:
Sample Description
:
RK-3-K71 (P/N: 692320 / Lot: 1004401007)
SGS authenticate the photo on original report only
Test Location: 26 Ayer Rajah Crescent, #07-08, Singapore 139944
This document is issued by the Company under its General Conditions of Service accessible at www.sgs.com/terms_and_conditions.htm and, for electronic format documents,
subject to Terms and Conditions for Electronic Documents at www.sgs.com/terms_e-document.htm. Attention is drawn to the limitation of liability, indemnification and
jurisdiction issues defined therein. Any holder of this document is advised that information contained hereon reflects the Company’s findings at the time of its intervention only
and within the limits of Client’s instructions, if any. The Company’s sole responsibility is to its Client and this document does not exonerate parties to a transaction from
exercising all their rights and obligations under the transaction documents. Any unauthorized alteration, forgery or falsification of the content or appearance of this document is
unlawful and offenders may be prosecuted to the fullest extent of the law. Unless otherwise stated the results shown in this test report refer only to the sample(s) tested and
such sample(s) are retained for 30 days only. This document cannot be reproduced except in full, without prior approval of the Company.
SGS Testing & Control Services Singapore Pte Ltd
26 Ayer Rajah Crescent #03-07 Singapore 139944 t +65 6379 0111 f+65 6777 2914 www.sgs.com
Member of SGS Group
Test Report
No: 10222124(1)
Date: 19-Jan-11
Page 4 of 6
Process Flow of IEC 62321 (Pb, Cd, Hg & Cr 6+)
Cutting / Preparation
Cr (Vl)
Sample Measurement
Hg
Pb,Cd
Acid digestion by suitable
acid depended on different
sample material
Microwave digestion
with HNO3/HCl/HF
Add appropriate amount
of digestion reagent
Heat to appropriate
temperature to extract
Filtration
Solution
Residue
Cool, filter digestate
through filter
1)Alkali Fusion
2)HCl to dissolve
Add diphenyl-carbazide
for color development
ICP-AES
Measure the absorbance
at 540 nm by UV-VIS
Remarks: Sample received was totally dissolved by preconditioning method. (CrVl method excluded)
Test Location: 26 Ayer Rajah Crescent, #07-08, Singapore 139944
This document is issued by the Company under its General Conditions of Service accessible at www.sgs.com/terms_and_conditions.htm and, for electronic format documents,
subject to Terms and Conditions for Electronic Documents at www.sgs.com/terms_e-document.htm. Attention is drawn to the limitation of liability, indemnification and
jurisdiction issues defined therein. Any holder of this document is advised that information contained hereon reflects the Company’s findings at the time of its intervention only
and within the limits of Client’s instructions, if any. The Company’s sole responsibility is to its Client and this document does not exonerate parties to a transaction from
exercising all their rights and obligations under the transaction documents. Any unauthorized alteration, forgery or falsification of the content or appearance of this document is
unlawful and offenders may be prosecuted to the fullest extent of the law. Unless otherwise stated the results shown in this test report refer only to the sample(s) tested and
such sample(s) are retained for 30 days only. This document cannot be reproduced except in full, without prior approval of the Company.
SGS Testing & Control Services Singapore Pte Ltd
26 Ayer Rajah Crescent #03-07 Singapore 139944 t +65 6379 0111 f+65 6777 2914 www.sgs.com
Member of SGS Group
Test Report
No: 10222124(1)
Date: 19-Jan-11
Page 5 of 6
Process Flow of Cr(Vl) by Boiling Water Extraction (IEC62321)
Add appropriate amount of DI water
Heat to appropriate temperature to extract
Cool, filter digestate through filter
Add diphenyl-carbazide for color
development
A red color indicates the presence of CrVl
Test Location: 26 Ayer Rajah Crescent, #07-08, Singapore 139944
This document is issued by the Company under its General Conditions of Service accessible at www.sgs.com/terms_and_conditions.htm and, for electronic format documents,
subject to Terms and Conditions for Electronic Documents at www.sgs.com/terms_e-document.htm. Attention is drawn to the limitation of liability, indemnification and
jurisdiction issues defined therein. Any holder of this document is advised that information contained hereon reflects the Company’s findings at the time of its intervention only
and within the limits of Client’s instructions, if any. The Company’s sole responsibility is to its Client and this document does not exonerate parties to a transaction from
exercising all their rights and obligations under the transaction documents. Any unauthorized alteration, forgery or falsification of the content or appearance of this document is
unlawful and offenders may be prosecuted to the fullest extent of the law. Unless otherwise stated the results shown in this test report refer only to the sample(s) tested and
such sample(s) are retained for 30 days only. This document cannot be reproduced except in full, without prior approval of the Company.
SGS Testing & Control Services Singapore Pte Ltd
26 Ayer Rajah Crescent #03-07 Singapore 139944 t +65 6379 0111 f+65 6777 2914 www.sgs.com
Member of SGS Group
Test Report
No: 10222124(1)
Date: 19-Jan-11
Page 6 of 6
Process Flow of PBBs and PBDEs by GC/MS (IEC 62321)
First Testing Process →
Optional screen process …… Confirmation process ...→
Cutting/Preparation
Sample Pre-treatment
Screening Analysis
Solvent Extraction
Concentrate/Dilute extracted
solution
Filter
High Mass Range GC/MS
Data
***End of Report***
Test Location: 26 Ayer Rajah Crescent, #07-08, Singapore 139944
This document is issued by the Company under its General Conditions of Service accessible at www.sgs.com/terms_and_conditions.htm and, for electronic format documents,
subject to Terms and Conditions for Electronic Documents at www.sgs.com/terms_e-document.htm. Attention is drawn to the limitation of liability, indemnification and
jurisdiction issues defined therein. Any holder of this document is advised that information contained hereon reflects the Company’s findings at the time of its intervention only
and within the limits of Client’s instructions, if any. The Company’s sole responsibility is to its Client and this document does not exonerate parties to a transaction from
exercising all their rights and obligations under the transaction documents. Any unauthorized alteration, forgery or falsification of the content or appearance of this document is
unlawful and offenders may be prosecuted to the fullest extent of the law. Unless otherwise stated the results shown in this test report refer only to the sample(s) tested and
such sample(s) are retained for 30 days only. This document cannot be reproduced except in full, without prior approval of the Company.
SGS Testing & Control Services Singapore Pte Ltd
26 Ayer Rajah Crescent #03-07 Singapore 139944 t +65 6379 0111 f+65 6777 2914 www.sgs.com
Member of SGS Group
Test Report
Applicant:
Number : TWNC00182566
Littelfuse, Philippines Inc.
LIMA Technology Center, Lipa City,
Malvar, Batangas
Date
: Nov 22, 2010
Sample Description:
One (1) group of submitted samples said to be :
Part Description
: Caps/ Lead Assay (metal)
Part Number
: 910-271
Date Sample Received
: Nov 17, 2010
Date Test Started
: NOV 17, 2010
Test Conducted :
As requested by the applicant, for details please refer to attached pages.
Authorized By:
On Behalf Of Intertek Testing Services
Taiwan Limited
K. Y. Liang
Director
This report shall not be reproduced
except in full, without the written
approval of the laboratory.
Page 1 Of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00182566
Test Conducted
Result (ppm)
(1)
(2)
Testing Item
Heavy Metal
Cadmium (Cd) content
Lead (Pb) content
Mercury (Hg) content
Chromium VI (Cr6+) content (mg/kg with 50cm2)
ND
ND
ND
ND
ND
ND
Negative
Negative
(< 0.02)(#) (< 0.02)(#)
Remarks: ppm = Parts per million based on weight of tested sample = mg/kg
ND = Not detected
<
= Less than
mg/kg with 50cm2 = milligram per kilogram with 50 square centimetre
Negative = A negative test result indicated positive observation
was not found at the time of testing.
#
= Due to the insufficient sample area, reduced total sample
surface of 10 cm2 was used and the dilution factor was
adjusted accordingly.
Tested Components
(1) Coppery Substrate
(2) Silvery Plating
Responsibility Of Chemist : Irene Chiou / Kevin Liu / Cathy Chen
Date Sample Received
Testing Period
: Nov 17, 2010
: Nov 17, 2010 To Nov 22, 2010
(Ⅱ) RoHS Requirement:
Restricted Substances
Cadmium (Cd) Content
Lead (Pb) Content
Mercury (Hg) Content
Chromium VI (Cr6+) Content
Limits
0.01% (100ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for
homogeneous material.
Page 2 Of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00182566
Test Conducted
(Ⅲ) Test Method:
Testing Item
Cadmium (Cd)
content
Lead (Pb) content
Mercury (Hg)
content
Chromium VI (Cr6+)
content
Testing Method
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 7, by microwave
digestion until the tested samples are
totally dissolved and determined by
ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in annex B, by boiling water
extraction and determined by UV-Vis
spectrophotometer.
Reporting Limit
2 ppm
2 ppm
2 ppm
0.02
mg/kg with 50cm2
Remark: Reporting limit = Quantitation limit of analyte in sample
Page 3 Of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00182566
Test Conducted
(IV) Measurement Flowchart:
Test For Cd/Pb/Hg/Chromium (VI)
Reference Standard：IEC 62321 edition 1.0:2008
Sample preparation
Take sample and immerse into Aqua Regia, start to strip plating layer
Stop the stripping procedure upon color change completely
Take the Aqua solution as plating component and stripped body as substrate component
Cd/Pb/Hg
Cr
Polymers /
electronics
Metal
For different
material, digest
the sample with
*1
appropriate acid
By spot test
Negative
Confirm the tested
samples are
totally dissolved
Make up with
deionized water
6+
*2
Weigh sample
and add
alkaline
solution
Get 50cm2 sample
Definite temp.
extraction
By boiling water
extraction
Cool and filter
the extract
Analyzed by ICP-OES
Make up with deionized water and add
diphenyl-carbazide solution
Remarks:
*1: List Of Appropriate Acid：
Material
Polymers
Metals
Electronics
Analyzed by UV-VIS
Acid Added For Digestion
HNO3,HCl,HF,H2O2,H3BO3
HNO3,HCl,HF
HNO3,HCl,H2O2,HBF4
*2: If the result of spot test is positive, Chromium VI would be determined as detected.
End Of Report
Page 4 Of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00182566
Test Conducted
Photo
Page 5 Of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Test Report
Applicant:
Number : TWNC00176948
Littelfuse, Philippines Inc.
LIMA Technology Center, Lipa City,
Malvar, Batangas
Date
: Oct 07, 2010
Sample Description:
One (1) group of submitted samples said to be :
Part Description
: Yarn
Part Number
: 648102
Date Sample Received
: Oct 04, 2010
Date Test Started
: Oct 05, 2010
Test Conducted :
As requested by the applicant, for details please refer to attached pages.
Authorized By:
On Behalf Of Intertek Testing Services
Taiwan Limited
K. Y. Liang
Director
This report shall not be reproduced
except in full, without the written
approval of the laboratory.
Page 1 Of 7
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00176948
Test Conducted
(Ⅰ) Test Result Summary :
Testing Item
Heavy Metal
Cadmium (Cd) content
Lead (Pb) content
Mercury (Hg) content
Chromium VI (Cr6+) content
Polybrominated Biphenyls (PBBs)
Monobrominated Biphenyls (MonoBB)
Dibrominated Biphenyls (DiBB)
Tribrominated Biphenyls (TriBB)
Tetrabrominated Biphenyls (TetraBB)
Pentabrominated Biphenyls (PentaBB)
Hexabrominated Biphenyls (HexaBB)
Heptabrominated Biphenyls (HeptaBB)
Octabrominated Biphenyls (OctaBB)
Nonabrominated Biphenyls (NonaBB)
Decabrominated Biphenyl (DecaBB)
Polybrominated Diphenyl Ethers (PBDEs)
Monobrominated Diphenyl Ethers (MonoBDE)
Dibrominated Diphenyl Ethers (DiBDE)
Tribrominated Diphenyl Ethers (TriBDE)
Tetrabrominated Diphenyl Ethers (TetraBDE)
Pentabrominated Diphenyl Ethers (PentaBDE)
Hexabrominated Diphenyl Ethers (HexaBDE)
Heptabrominated Diphenyl Ethers (HeptaBDE)
Octabrominated Diphenyl Ethers (OctaBDE)
Nonabrominated Diphenyl Ethers (NonaBDE)
Decabrominated Diphenyl Ether (DecaBDE)
Result (ppm)
White Fabric
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Page 2 Of 7
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00176948
Test Conducted
(Ⅰ) Test Result Summary :
Testing Item
Result (ppm)
White Fabric
Halogen Content
Fluorine (F)
Chlorine (Cl)
Bromine (Br)
Iodine (I)
ND
ND
ND
ND
Remarks: ppm = Parts per million based on weight of tested sample = mg/kg
ND = Not detected
Responsibility Of Chemist : Irene Chiou / Kevin Liu / Cathy Chen
Date Sample Received
Testing Period
: Oct 04, 2010
: Oct 05, 2010 To Oct 07, 2010
(Ⅱ) RoHS Requirement:
Restricted Substances
Cadmium (Cd) Content
Lead (Pb) Content
Mercury (Hg) Content
Chromium VI (Cr6+) Content
Polybrominated Biphenyls (PBBs)
Polybrominated Diphenyl Ehters (PBDEs)
Limits
0.01% (100ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for
homogeneous material.
Page 3 Of 7
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00176948
Test Conducted
(Ⅲ) Test Method:
Testing Item
Cadmium (Cd)
content
Lead (Pb) content
Mercury (Hg)
content
Chromium VI (Cr6+)
content
Polybrominated
Biphenyls (PBBs)
Polybrominated
Diphenyl Ethers
(PBDEs)
Halogen Content
Testing Method
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 7, by microwave
digestion until the tested samples are
totally dissolved and determined by
ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in annex C, by alkaline
digestion and determined by UV-Vis
spectrophotometer.
With reference to IEC 62321 edition
1.0:2008 in annex A, by solvent
extraction and determined by GC-MSD
and further HPLC confirmation when
necessary.
With reference to IEC 62321 edition
1.0:2008 in annex A, by solvent
extraction and determined by GC-MSD
and further HPLC confirmation when
necessary.
With reference to EN 14582:2007 by
calorimetric bomb with oxygen and
determined by ion chromatography
Reporting Limit
2 ppm
2 ppm
2 ppm
1 ppm
5 ppm
5 ppm
50 ppm
Remark: Reporting limit = Quantitation limit of analyte in sample
Page 4 Of 7
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00176948
Test Conducted
(Ⅳ) Measurement Flowchart:
Test For Cd/Pb/Hg/Chromium (VI)/PBBS/PBDES Contents
Reference Standard: IEC 62321 edition 1.0:2008
Sampling/grinding or cutting
Cd/Pb/Hg
Cr
Confirm the tested
samples are
totally dissolved
Make up with
deionized water
PBBs/PBDEs
Polymers /
electronics
Metal
For different
material, digest
the sample with
*1
appropriate acid
6+
Weigh sample and
add organic solvent
By spot test
Negative
Get 50cm2 sample
By boiling water
extraction
*2
Weigh sample
and add
alkaline
solution
By Soxhlet
extraction or
Solvent extraction
Definite temp.
extraction
Cool and filter
the extract
Analyzed by ICP-OES
Concentrate the
extract and make up
with organic
solvent
Analyzed by GC-MSD
Make up with deionized
water and add diphenylcarbazide solution
Analyzed by UV-VIS
Remarks:
*1: List Of Appropriate Acid：
Material
Polymers
Metals
Electronics
Acid Added For Digestion
HNO3,HCl,HF,H2O2,H3BO3
HNO3,HCl,HF
HNO3,HCl,H2O2,HBF4
*2: If the result of spot test is positive, Chromium VI would be determined as detected.
Page 5 Of 7
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00176948
Test Conducted
(Ⅳ) Measurement Flowchart:
Test For Halogen Content
Reference Standard： EN 14582
Sampling/grinding or
cutting
Add absorbent in a
calorimetric bomb &
place weighed sample in
equipment
Fill the calorimetric
bomb with oxygen
Ignite then leave the
flask at room
temperature
Transfer the absorbent
into a volumetric flask
Make up with deionized
water
Analyzed by ion
chromatography
End Of Report
Page 6 Of 7
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00176948
Test Conducted
Photo
Page 7 Of 7
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Test Report
Applicant:
Number : TWNC00183561
Littelfuse, Philippines Inc.
LIMA Technology Center, Lipa City,
Malvar, Batangas
Date
: Nov 30, 2010
Sample Description:
One (1) group of submitted samples said to be :
Part Description
: Yarn
Part Number
: 648106-001
Date Sample Received
: Nov 25, 2010
Date Test Started
: Nov 25, 2010
Test Conducted :
As requested by the applicant, for details please refer to attached pages.
Authorized By:
On Behalf Of Intertek Testing Services
Taiwan Limited
K. Y. Liang
Director
This report shall not be reproduced
except in full, without the written
approval of the laboratory.
Page 1 Of 6
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00183561
Test Conducted
(Ⅰ) Test Result Summary :
Testing Item
Result (ppm)
White Yarn
Heavy Metal
Cadmium (Cd) content
Lead (Pb) content
Mercury (Hg) content
Chromium VI (Cr6+) content
Polybrominated Biphenyls (PBBs)
Monobrominated Biphenyls (MonoBB)
Dibrominated Biphenyls (DiBB)
Tribrominated Biphenyls (TriBB)
Tetrabrominated Biphenyls (TetraBB)
Pentabrominated Biphenyls (PentaBB)
Hexabrominated Biphenyls (HexaBB)
Heptabrominated Biphenyls (HeptaBB)
Octabrominated Biphenyls (OctaBB)
Nonabrominated Biphenyls (NonaBB)
Decabrominated Biphenyl (DecaBB)
Polybrominated Diphenyl Ethers (PBDEs)
Monobrominated Diphenyl Ethers (MonoBDE)
Dibrominated Diphenyl Ethers (DiBDE)
Tribrominated Diphenyl Ethers (TriBDE)
Tetrabrominated Diphenyl Ethers (TetraBDE)
Pentabrominated Diphenyl Ethers (PentaBDE)
Hexabrominated Diphenyl Ethers (HexaBDE)
Heptabrominated Diphenyl Ethers (HeptaBDE)
Octabrominated Diphenyl Ethers (OctaBDE)
Nonabrominated Diphenyl Ethers (NonaBDE)
Decabrominated Diphenyl Ether (DecaBDE)
Halogen Content
Fluorine (F)
Chlorine (Cl)
Bromine (Br)
Iodine (I)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Remarks: ppm = Parts per million based on weight of tested sample = mg/kg
ND = Not detected
Responsibility Of Chemist : Irene Chiou / Kevin Liu / Cathy Chen
Date Sample Received
Testing Period
: Nov 25, 2010
: Nov 25, 2010 To Nov 29, 2010
Page 2 Of 6
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00183561
Test Conducted
(Ⅱ) RoHS Requirement:
Restricted Substances
Cadmium (Cd) Content
Lead (Pb) Content
Mercury (Hg) Content
Chromium VI (Cr6+) Content
Polybrominated Biphenyls (PBBs)
Polybrominated Diphenyl Ehters (PBDEs)
Limits
0.01% (100ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for
homogeneous material.
(Ⅲ) Test Method:
Testing Item
Cadmium (Cd)
content
Lead (Pb) content
Mercury (Hg)
content
Chromium VI (Cr6+)
content
Polybrominated
Biphenyls (PBBs)
Polybrominated
Diphenyl Ethers
(PBDEs)
Halogen Content
Testing Method
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 7, by microwave
digestion until the tested samples are
totally dissolved and determined by
ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in annex C, by alkaline
digestion and determined by UV-Vis
spectrophotometer.
With reference to IEC 62321 edition
1.0:2008 in annex A, by solvent
extraction and determined by GC-MSD
and further HPLC confirmation when
necessary.
With reference to IEC 62321 edition
1.0:2008 in annex A, by solvent
extraction and determined by GC-MSD
and further HPLC confirmation when
necessary.
With reference to EN 14582:2007 by
calorimetric bomb with oxygen and
determined by ion chromatography
Reporting Limit
2 ppm
2 ppm
2 ppm
1 ppm
5 ppm
5 ppm
50 ppm
Remark: Reporting limit = Quantitation limit of analyte in sample
Page 3 Of 6
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00183561
Test Conducted
(Ⅳ) Measurement Flowchart:
Test For Cd/Pb/Hg/Chromium (VI)/PBBS/PBDES Contents
Reference Standard: IEC 62321 edition 1.0:2008
Sample preparation
For non-metal part
For metal part
Take sample and immerse into Aqua Regia, start to strip plating layer
Stop the stripping procedure upon color change completely
Take the Aqua solution as plating component and stripped body as substrate component
Cd/Pb/Hg
Cr
Weigh sample and
add organic solvent
By spot test
Negative
Confirm the tested
samples are
totally dissolved
Make up with
deionized water
PBBs/PBDEs
Polymers /
electronics
Metal
For different
material, digest
the sample with
*1
appropriate acid
6+
Get 50cm2 sample
By boiling water
extraction
*2
Weigh sample
and add
alkaline
solution
By Soxhlet
extraction or
Solvent extraction
Definite temp.
extraction
Cool and filter
the extract
Analyzed by ICP-OES
Concentrate the
extract and make up
with organic
solvent
Analyzed by GC-MSD
Make up with deionized
water and add diphenylcarbazide solution
Analyzed by UV-VIS
Remarks:
*1: List Of Appropriate Acid：
Material
Polymers
Metals
Electronics
Acid Added For Digestion
HNO3,HCl,HF,H2O2,H3BO3
HNO3,HCl,HF
HNO3,HCl,H2O2,HBF4
*2: If the result of spot test is positive, Chromium VI would be determined as detected.
Page 4 Of 6
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00183561
Test Conducted
(Ⅳ) Measurement Flowchart:
Test For Halogen Content
Reference Standard：EN 14582
Sampling/grinding or
cutting
Add absorbent in a
calorimetric bomb &
place weighed sample in
equipment
Fill oxygen into
calorimetric bomb
Ignite then leave the
flask at room
temperature
Transfer the absorbent
into a volumetric flask
Make up with deionized
water
Analyzed by ion
chromatography
End Of Report
Page 5 Of 6
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00183561
Test Conducted
Photo
Page 6 Of 6
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Test Report
Applicant:
Number : TWNC00183563
Littelfuse, Philippines Inc.
LIMA Technology Center, Lipa City,
Malvar, Batangas
Date
: Nov 30, 2010
Sample Description:
One (1) group of submitted samples said to be :
Part Description
: Yarn
Part Number
: 648112-001
Date Sample Received
: Nov 25, 2010
Date Test Started
: Nov 25, 2010
Test Conducted :
As requested by the applicant, for details please refer to attached pages.
Authorized By:
On Behalf Of Intertek Testing Services
Taiwan Limited
K. Y. Liang
Director
This report shall not be reproduced
except in full, without the written
approval of the laboratory.
Page 1 Of 6
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00183563
Test Conducted
(Ⅰ) Test Result Summary :
Testing Item
Result (ppm)
White Yarn
Heavy Metal
Cadmium (Cd) content
Lead (Pb) content
Mercury (Hg) content
Chromium VI (Cr6+) content
Polybrominated Biphenyls (PBBs)
Monobrominated Biphenyls (MonoBB)
Dibrominated Biphenyls (DiBB)
Tribrominated Biphenyls (TriBB)
Tetrabrominated Biphenyls (TetraBB)
Pentabrominated Biphenyls (PentaBB)
Hexabrominated Biphenyls (HexaBB)
Heptabrominated Biphenyls (HeptaBB)
Octabrominated Biphenyls (OctaBB)
Nonabrominated Biphenyls (NonaBB)
Decabrominated Biphenyl (DecaBB)
Polybrominated Diphenyl Ethers (PBDEs)
Monobrominated Diphenyl Ethers (MonoBDE)
Dibrominated Diphenyl Ethers (DiBDE)
Tribrominated Diphenyl Ethers (TriBDE)
Tetrabrominated Diphenyl Ethers (TetraBDE)
Pentabrominated Diphenyl Ethers (PentaBDE)
Hexabrominated Diphenyl Ethers (HexaBDE)
Heptabrominated Diphenyl Ethers (HeptaBDE)
Octabrominated Diphenyl Ethers (OctaBDE)
Nonabrominated Diphenyl Ethers (NonaBDE)
Decabrominated Diphenyl Ether (DecaBDE)
Halogen Content
Fluorine (F)
Chlorine (Cl)
Bromine (Br)
Iodine (I)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Remarks: ppm = Parts per million based on weight of tested sample = mg/kg
ND = Not detected
Responsibility Of Chemist : Irene Chiou / Kevin Liu / Cathy Chen
Date Sample Received
Testing Period
: Nov 25, 2010
: Nov 25, 2010 To Nov 29, 2010
Page 2 Of 6
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00183563
Test Conducted
(Ⅱ) RoHS Requirement:
Restricted Substances
Cadmium (Cd) Content
Lead (Pb) Content
Mercury (Hg) Content
Chromium VI (Cr6+) Content
Polybrominated Biphenyls (PBBs)
Polybrominated Diphenyl Ehters (PBDEs)
Limits
0.01% (100ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for
homogeneous material.
(Ⅲ) Test Method:
Testing Item
Cadmium (Cd)
content
Lead (Pb) content
Mercury (Hg)
content
Chromium VI (Cr6+)
content
Polybrominated
Biphenyls (PBBs)
Polybrominated
Diphenyl Ethers
(PBDEs)
Halogen Content
Testing Method
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 7, by microwave
digestion until the tested samples are
totally dissolved and determined by
ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in annex C, by alkaline
digestion and determined by UV-Vis
spectrophotometer.
With reference to IEC 62321 edition
1.0:2008 in annex A, by solvent
extraction and determined by GC-MSD
and further HPLC confirmation when
necessary.
With reference to IEC 62321 edition
1.0:2008 in annex A, by solvent
extraction and determined by GC-MSD
and further HPLC confirmation when
necessary.
With reference to EN 14582:2007 by
calorimetric bomb with oxygen and
determined by ion chromatography
Reporting Limit
2 ppm
2 ppm
2 ppm
1 ppm
5 ppm
5 ppm
50 ppm
Remark: Reporting limit = Quantitation limit of analyte in sample
Page 3 Of 6
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00183563
Test Conducted
(Ⅳ) Measurement Flowchart:
Test For Cd/Pb/Hg/Chromium (VI)/PBBS/PBDES Contents
Reference Standard: IEC 62321 edition 1.0:2008
Sample preparation
For non-metal part
For metal part
Take sample and immerse into Aqua Regia, start to strip plating layer
Stop the stripping procedure upon color change completely
Take the Aqua solution as plating component and stripped body as substrate component
Cd/Pb/Hg
Cr
Weigh sample and
add organic solvent
By spot test
Negative
Confirm the tested
samples are
totally dissolved
Make up with
deionized water
PBBs/PBDEs
Polymers /
electronics
Metal
For different
material, digest
the sample with
*1
appropriate acid
6+
Get 50cm2 sample
By boiling water
extraction
*2
Weigh sample
and add
alkaline
solution
By Soxhlet
extraction or
Solvent extraction
Definite temp.
extraction
Cool and filter
the extract
Analyzed by ICP-OES
Concentrate the
extract and make up
with organic
solvent
Analyzed by GC-MSD
Make up with deionized
water and add diphenylcarbazide solution
Analyzed by UV-VIS
Remarks:
*1: List Of Appropriate Acid：
Material
Polymers
Metals
Electronics
Acid Added For Digestion
HNO3,HCl,HF,H2O2,H3BO3
HNO3,HCl,HF
HNO3,HCl,H2O2,HBF4
*2: If the result of spot test is positive, Chromium VI would be determined as detected.
Page 4 Of 6
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00183563
Test Conducted
(Ⅳ) Measurement Flowchart:
Test For Halogen Content
Reference Standard：EN 14582
Sampling/grinding or
cutting
Add absorbent in a
calorimetric bomb &
place weighed sample in
equipment
Fill oxygen into
calorimetric bomb
Ignite then leave the
flask at room
temperature
Transfer the absorbent
into a volumetric flask
Make up with deionized
water
Analyzed by ion
chromatography
End Of Report
Page 5 Of 6
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00183563
Test Conducted
Photo
Page 6 Of 6
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Test Report
Applicant:
Number : TWNC00182411
Littelfuse, Philippines Inc.
LIMA Technology Center, Lipa City,
Malvar, Batangas
Date
: Nov 22, 2010
Sample Description:
One (1) group of submitted samples said to be :
Part Description
: Epoxy Powder (Gold-HF)
Part Number
: 087340
Date Sample Received
: Nov 16, 2010
Date Test Started
: Nov 17, 2010
Test Conducted :
As requested by the applicant, for details please refer to attached pages.
Authorized By:
On Behalf Of Intertek Testing Services
Taiwan Limited
K. Y. Liang
Director
This report shall not be reproduced
except in full, without the written
approval of the laboratory.
Page 1 Of 7
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00182411
Test Conducted
(Ⅰ) Test Result Summary :
Testing Item
Heavy Metal
Cadmium (Cd) content
Lead (Pb) content
Mercury (Hg) content
Chromium VI (Cr6+) content
Polybrominated Biphenyls (PBBs)
Monobrominated Biphenyls (MonoBB)
Dibrominated Biphenyls (DiBB)
Tribrominated Biphenyls (TriBB)
Tetrabrominated Biphenyls (TetraBB)
Pentabrominated Biphenyls (PentaBB)
Hexabrominated Biphenyls (HexaBB)
Heptabrominated Biphenyls (HeptaBB)
Octabrominated Biphenyls (OctaBB)
Nonabrominated Biphenyls (NonaBB)
Decabrominated Biphenyl (DecaBB)
Polybrominated Diphenyl Ethers (PBDEs)
Monobrominated Diphenyl Ethers (MonoBDE)
Dibrominated Diphenyl Ethers (DiBDE)
Tribrominated Diphenyl Ethers (TriBDE)
Tetrabrominated Diphenyl Ethers (TetraBDE)
Pentabrominated Diphenyl Ethers (PentaBDE)
Hexabrominated Diphenyl Ethers (HexaBDE)
Heptabrominated Diphenyl Ethers (HeptaBDE)
Octabrominated Diphenyl Ethers (OctaBDE)
Nonabrominated Diphenyl Ethers (NonaBDE)
Decabrominated Diphenyl Ether (DecaBDE)
Result (ppm)
Yellow Powder
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Page 2 Of 7
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00182411
Test Conducted
(Ⅰ) Test Result Summary :
Testing Item
Result (ppm)
Yellow Powder
Halogen Content
Fluorine (F)
Chlorine (Cl)
Bromine (Br)
Iodine (I)
ND
651
ND
ND
Remarks: ppm = Parts per million based on weight of tested sample = mg/kg
ND = Not detected
Responsibility Of Chemist : Irene Chiou / Kevin Liu / Cathy Chen
Date Sample Received
Testing Period
: Nov 16, 2010
: Nov 17, 2010 To Nov 19, 2010
(Ⅱ) RoHS Requirement:
Restricted Substances
Cadmium (Cd) Content
Lead (Pb) Content
Mercury (Hg) Content
Chromium VI (Cr6+) Content
Polybrominated Biphenyls (PBBs)
Polybrominated Diphenyl Ehters (PBDEs)
Limits
0.01% (100ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for
homogeneous material.
Page 3 Of 7
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00182411
Test Conducted
(Ⅲ) Test Method:
Testing Item
Cadmium (Cd)
content
Lead (Pb) content
Mercury (Hg)
content
Chromium VI (Cr6+)
content
Polybrominated
Biphenyls (PBBs)
Polybrominated
Diphenyl Ethers
(PBDEs)
Halogen Content
Testing Method
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 7, by microwave
digestion until the tested samples are
totally dissolved and determined by
ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in annex C, by alkaline
digestion and determined by UV-Vis
spectrophotometer.
With reference to IEC 62321 edition
1.0:2008 in annex A, by solvent
extraction and determined by GC-MSD
and further HPLC confirmation when
necessary.
With reference to IEC 62321 edition
1.0:2008 in annex A, by solvent
extraction and determined by GC-MSD
and further HPLC confirmation when
necessary.
With reference to EN 14582:2007 by
calorimetric bomb with oxygen and
determined by ion chromatography
Reporting Limit
2 ppm
2 ppm
2 ppm
1 ppm
5 ppm
5 ppm
50 ppm
Remark: Reporting limit = Quantitation limit of analyte in sample
Page 4 Of 7
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00182411
Test Conducted
(Ⅳ) Measurement Flowchart:
Test For Cd/Pb/Hg/Chromium (VI)/PBBS/PBDES Contents
Reference Standard: IEC 62321 edition 1.0:2008
Sampling/grinding or cutting
Cd/Pb/Hg
Cr
Weigh sample and
add organic solvent
By spot test
Negative
Confirm the tested
samples are
totally dissolved
Make up with
deionized water
PBBs/PBDEs
Polymers /
electronics
Metal
For different
material, digest
the sample with
*1
appropriate acid
6+
Get 50cm2 sample
By boiling water
extraction
*2
Weigh sample
and add
alkaline
solution
By Soxhlet
extraction or
Solvent extraction
Definite temp.
extraction
Cool and filter
the extract
Concentrate the
extract and make up
with organic
solvent
Analyzed by ICP-OES
Analyzed by GC-MSD
Make up with deionized
water and add diphenylcarbazide solution
Analyzed by UV-VIS
Remarks:
*1: List Of Appropriate Acid：
Material
Polymers
Metals
Electronics
Acid Added For Digestion
HNO3,HCl,HF,H2O2,H3BO3
HNO3,HCl,HF
HNO3,HCl,H2O2,HBF4
*2: If the result of spot test is positive, Chromium VI would be determined as detected.
Page 5 Of 7
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00182411
Test Conducted
(Ⅳ) Measurement Flowchart:
Test For Halogen Content
Reference Standard： EN 14582
Sampling/grinding or
cutting
Add absorbent in a
calorimetric bomb &
place weighed sample in
equipment
Fill the calorimetric
bomb with oxygen
Ignite then leave the
flask at room
temperature
Transfer the absorbent
into a volumetric flask
Make up with deionized
water
Analyzed by ion
chromatography
End Of Report
Page 6 Of 7
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00182411
Test Conducted
Photo
Page 7 Of 7
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401