ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: Ceramic Fuse 1206 Slo-Blo Product #: 469 Series Issue Date: November 29, 2012 It is hereby certified by Littelfuse, Inc. that there is neither RoHS (EU Directive 2002/95/EC, 2011/65/EU)-restricted substance nor such use, for materials to be used for unit parts, for packing/packaging materials, and for additives and the like in the manufacturing processes. In addition, it is hereby reported to you that the parts and sub-materials, the materials to be used for unit parts, the packing/packaging materials, and the additives and the like in the manufacturing processes, are all composed of the following components. Issued by: <Global EHS Engineer> (1) Parts, sub-materials and unit parts This document covers the Ceramic Fuse 1206 Slo-blo RoHS-Compliant series products manufactured by Littelfuse, Inc. ＜ Raw Materials Used Please see Table 1 (2) The ICP data on all measurable substances Please see appropriate pages as identifed in Table 1 Remarks： Form 585-047 Rev. A 1 2/21/06 Table 1: List of Raw Materials covered by this report Total Parts 1 2 3 4 5 6 7 Raw Material Part Number 011004 011002 011003 011001 010118 010119 039641 Raw Material Description Underglaze / Dielectric Paste Silver (Ag) Conductor Paste Coverglass / Overglaze Paste End Termination Paste Nickel Anode Tin Anode Ceramic Substrate 2 Page(s) 3-11 12-20 21-30 31-40 41-46 47-51 52-58 Test Report Applicant: Number : TWNC00238109 Littelfuse Philippines Inc. LIMA Technology Center, Lipa City, Malvar, Batangas Date : Dec 29, 2011 Sample Description: One (1) group of submitted samples said to be : Part Description : Underglaze(Dielectric) Paste-Sintered Part Number : 011004 Date Sample Received : Dec 22, 2011 Date Test Started : Dec 23, 2011 Test Conducted : As requested by the applicant, for details please refer to attached pages. Authorized By: On Behalf Of Intertek Testing Services Taiwan Limited K. Y. Liang Director This report shall not be reproduced except in full, without the written approval of the laboratory. Page 1 of 9 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401 Number : TWNC00238109 Test Conducted (Ⅰ) Test Result Summary : Test Item Heavy Metal Cadmium (Cd) content Lead (Pb) content Mercury (Hg) content Chromium VI (Cr6+) content Polybrominated Biphenyls (PBBs) Monobrominated Biphenyls (MonoBB) Dibrominated Biphenyls (DiBB) Tribrominated Biphenyls (TriBB) Tetrabrominated Biphenyls (TetraBB) Pentabrominated Biphenyls (PentaBB) Hexabrominated Biphenyls (HexaBB) Heptabrominated Biphenyls (HeptaBB) Octabrominated Biphenyls (OctaBB) Nonabrominated Biphenyls (NonaBB) Decabrominated Biphenyl (DecaBB) Polybrominated Diphenyl Ethers (PBDEs) Monobrominated Diphenyl Ethers (MonoBDE) Dibrominated Diphenyl Ethers (DiBDE) Tribrominated Diphenyl Ethers (TriBDE) Tetrabrominated Diphenyl Ethers (TetraBDE) Pentabrominated Diphenyl Ethers (PentaBDE) Hexabrominated Diphenyl Ethers (HexaBDE) Heptabrominated Diphenyl Ethers (HeptaBDE) Octabrominated Diphenyl Ethers (OctaBDE) Nonabrominated Diphenyl Ethers (NonaBDE) Decabrominated Diphenyl Ether (DecaBDE) Halogen Content Fluorine (F) Chlorine (Cl) Bromine (Br) Iodine (I) Result (ppm) Submitted Samples (Mixed All Parts) ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND Page 2 of 9 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401 Number : TWNC00238109 Test Conducted (Ⅰ) Test Result Summary : Test Item Result (ppm) Submitted Samples (Mixed All Parts) Phthalates Di(2-ethylhexyl) Phthalate (DEHP) Dibutyl Phthalate (DBP) Benzyl Butyl Phthalate (BBP) Others Hexabromocyclododecane (HBCDD) ND ND ND ND Remarks: ppm = Parts per million based on weight of tested sample = mg/kg ND = Not detected Responsibility of Chemist : Irene Chiou / Kevin Liu / Cathy Chen Date Sample Received Test Period : Dec 22, 2011 : Dec 23, 2011 To Dec 29, 2011 (Ⅱ) RoHS Requirement: Restricted Substances Cadmium (Cd) Content Lead (Pb) Content Mercury (Hg) Content Chromium VI (Cr6+) Content Polybrominated Biphenyls (PBBs) Polybrominated Diphenyl Ehters (PBDEs) Limits 0.01% (100ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for homogeneous material. Page 3 of 9 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401 Number : TWNC00238109 Test Conducted (Ⅲ) Test Method: Test Item Test Method Reporting Limit With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the Cadmium (Cd) content 2 ppm tested samples are totally dissolved and determined by ICPOES. With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the Lead (Pb) content 2 ppm tested samples are totally dissolved and determined by ICPOES. With reference to IEC 62321 edition 1.0:2008 in clause 7, by microwave Mercury (Hg) content digestion until the tested samples 2 ppm are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in annex C, by alkaline Chromium VI (Cr6+) 1 ppm content digestion and determined by UV-Vis spectrophotometer. With reference to IEC 62321 edition 1.0:2008 in annex A, by solvent Polybrominated extraction and determined by GC-MS 5 ppm Biphenyls (PBBs) and further HPLC-DAD confirmation when necessary. With reference to IEC 62321 edition 1.0:2008 in annex A, by solvent Polybrominated Diphenyl Ethers extraction and determined by GC-MS 5 ppm (PBDEs) and further HPLC-DAD confirmation when necessary. With reference to EN 14582:2007 by Halogen Content calorimetric bomb with oxygen and 50 ppm determined by Ion Chromatograph. With reference to ASTM D3421-75, by Phthalates solvent extraction and determined by 10 ppm GC-MSD or GC-FID With reference to USEPA 3540C, by Hexabromocyclododecane solvent extraction and determined by 10 ppm (HBCDD) GC-MSD Remark: Reporting limit = Quantitation limit of analyte in sample Page 4 of 9 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401 Number : TWNC00238109 Test Conducted (Ⅳ) Measurement Flowchart: Test for Cd/Pb/Hg/Chromium (VI)/PBBS/PBDES Contents Reference Standard: IEC 62321 edition 1.0:2008 Sample preparation For non-metal part For metal part Take sample and immerse into Aqua Regia, start to strip plating layer Stop the stripping procedure upon color change completely Take the Aqua solution as plating component and stripped body as substrate component Cd/Pb/Hg Cr Weigh sample and add organic solvent By spot test Negative Confirm the tested samples are totally dissolved Make up with deionized water PBBs/PBDEs Polymers / electronics Metal For different material, digest the sample with *1 appropriate acid 6+ Get 50cm2 sample By boiling water extraction *2 Weigh sample and add alkaline solution By Soxhlet extraction or Solvent extraction Definite temp. extraction Cool and filter the extract Analyzed by ICP-OES Concentrate the extract and make up with organic solvent Analyzed by GC-MSD Make up with deionized water and add diphenylcarbazide solution Remarks: *1: List of Appropriate Acid： Material Polymers Metals Electronics Analyzed by UV-VIS Acid Added for Digestion HNO3,HCl,HF,H2O2,H3BO3 HNO3,HCl,HF HNO3,HCl,H2O2,HBF4 *2: If the result of spot test is positive, Chromium VI would be determined as detected. Page 5 of 9 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401 Number : TWNC00238109 Test Conducted (Ⅳ) Measurement Flowchart: Test for Halogen Content Reference Standard：EN 14582 Sampling/grinding or cutting Add absorbent in a combustion flask & place weighed sample in equipment Fill oxygen into calorimetric bomb Ignite then leave the bomb at room temperature Transfer the absorbent into a volumetric flask Make up with deionized water Analyzed by ion chromatography Page 6 of 9 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401 Number : TWNC00238109 Test Conducted (Ⅳ) Measurement Flowchart: Test For Phthalates Contents Reference Method: EN 14372: 2004 Sampling/grinding or cutting Weigh sample and add organic solvent By solvent extraction Concentrate the extract and make up with organic solvent Analyzed by GC-MSD Page 7 of 9 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401 Number : TWNC00238109 Test Conducted (Ⅳ) Measurement Flowchart: Test For Hexabromocyclododecane (HBCDD) Reference Standard：USEPA 3540C Sampling/grinding or cutting Weigh sample and add organic solvent By soxhlet extraction Concentrate the extract and make up with organic solvent Analyzed by GC-MSD End of Report Page 8 of 9 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401 Number : TWNC00238109 Test Conducted Photo Page 9 of 9 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401 Test Report Applicant: Number : TWNC00270123 Littelfuse Philippines Inc. LIMA Technology Center, Lipa City, Malvar, Batangas Date : Aug 10, 2012 Sample Description: One (1) group of submitted samples said to be : Part Description : Sintered Silver Conductor Paste Part Number : 011002 Date Sample Received : Aug 06, 2012 Date Test Started : Aug 07, 2012 Test Conducted : As requested by the applicant, for details please refer to attached pages. Authorized By: On Behalf Of Intertek Testing Services Taiwan Limited K. Y. Liang Director This report shall not be reproduced except in full, without the written approval of the laboratory. Page 1 of 9 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410 Number : TWNC00270123 Test Conducted (Ⅰ) Test Result Summary : Test Item Heavy Metal Cadmium (Cd) content Lead (Pb) content Mercury (Hg) content Chromium VI (Cr6+) content Polybrominated Biphenyls (PBBs) Monobrominated Biphenyls (MonoBB) Dibrominated Biphenyls (DiBB) Tribrominated Biphenyls (TriBB) Tetrabrominated Biphenyls (TetraBB) Pentabrominated Biphenyls (PentaBB) Hexabrominated Biphenyls (HexaBB) Heptabrominated Biphenyls (HeptaBB) Octabrominated Biphenyls (OctaBB) Nonabrominated Biphenyls (NonaBB) Decabrominated Biphenyl (DecaBB) Polybrominated Diphenyl Ethers (PBDEs) Monobrominated Diphenyl Ethers (MonoBDE) Dibrominated Diphenyl Ethers (DiBDE) Tribrominated Diphenyl Ethers (TriBDE) Tetrabrominated Diphenyl Ethers (TetraBDE) Pentabrominated Diphenyl Ethers (PentaBDE) Hexabrominated Diphenyl Ethers (HexaBDE) Heptabrominated Diphenyl Ethers (HeptaBDE) Octabrominated Diphenyl Ethers (OctaBDE) Nonabrominated Diphenyl Ethers (NonaBDE) Decabrominated Diphenyl Ether (DecaBDE) Halogen Content Fluorine (F) Chlorine (Cl) Bromine (Br) Iodine (I) Result (ppm) Submitted Samples ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND Page 2 of 9 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410 Number : TWNC00270123 Test Conducted (Ⅰ) Test Result Summary : Test Item Result (ppm) Submitted Samples Phthalates Di(2-ethylhexyl) Phthalate (DEHP) Dibutyl Phthalate (DBP) Benzyl Butyl Phthalate (BBP) Others Hexabromocyclododecane (HBCDD) ND ND ND ND Remarks: ppm = Parts per million based on weight of tested sample = mg/kg ND = Not detected Responsibility of Chemist : Irene Chiou / Kevin Liu / Cathy Chen Date Sample Received Test Period : Aug 06, 2012 : Aug 07, 2012 To Aug 09, 2012 (Ⅱ) RoHS Limits: Restricted Substances Cadmium (Cd) Content Lead (Pb) Content Mercury (Hg) Content Chromium VI (Cr6+) Content Polybrominated Biphenyls (PBBs) Polybrominated Diphenyl Ehters (PBDEs) Limits 0.01% (100ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) The above limits were quoted from Annex II of 2011/65/EU for homogeneous material. Page 3 of 9 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410 Number : TWNC00270123 Test Conducted (Ⅲ) Test Method: Test Item Test Method With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by Cadmium (Cd) content microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by Lead (Pb) content microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in clause 7, by microwave Mercury (Hg) content digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition Chromium VI (Cr6+) 1.0:2008 in annex C, by alkaline digestion and determined by UV-Vis content spectrophotometer. With reference to IEC 62321 edition 1.0:2008 in annex A, by solvent Polybrominated extraction and determined by GC-MS Biphenyls (PBBs) and further HPLC-DAD confirmation when necessary. With reference to IEC 62321 edition Polybrominated 1.0:2008 in annex A, by solvent Diphenyl Ethers extraction and determined by GC-MS and further HPLC-DAD confirmation (PBDEs) when necessary. With reference to EN 14582:2007 by Halogen Content calorimetric bomb with oxygen and determined by Ion Chromatograph. With reference to EN 14372: 2004, by Phthalates solvent extraction and determined by GC-MS. With reference to USEPA 3540C, by Hexabromocyclododecane solvent extraction and determined by (HBCDD) GC-MSD. Reporting Limit 2 ppm 2 ppm 2 ppm 1 ppm 5 ppm 5 ppm 50 ppm 50 ppm 10 ppm Remark: Reporting limit = Quantitation limit of analyte in sample Page 4 of 9 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410 Number : TWNC00270123 Test Conducted (Ⅳ) Measurement Flowchart: Test for Cd/Pb/Hg/Chromium (VI)/PBBS/PBDES Contents Reference Standard: IEC 62321 edition 1.0:2008 Sample preparation For non-metal part For metal part Take sample and immerse into Aqua Regia, start to strip plating layer Stop the stripping procedure upon color change completely Take the Aqua solution as plating component and stripped body as substrate component Cd/Pb/Hg Cr Confirm the tested samples are totally dissolved Make up with deionized water PBBs/PBDEs Polymers / electronics Metal For different material, digest the sample with *1 appropriate acid 6+ Weigh sample and add organic solvent By spot test Negative Get 50cm2 sample By boiling water extraction *2 Weigh sample and add alkaline solution By Soxhlet extraction or Solvent extraction Definite temp. extraction Cool and filter the extract Analyzed by ICP-OES Concentrate the extract and make up with organic solvent Analyzed by GC-MSD Make up with deionized water and add diphenylcarbazide solution Analyzed by UV-VIS Remarks: *1: List of Appropriate Acid： Acid Added for Digestion Material Polymers HNO3,HCl,HF,H2O2,H3BO3 Metals HNO3,HCl,HF Electronics HNO3,HCl,H2O2,HBF4 *2: If the result of spot test is positive, Chromium VI would be determined as detected. Page 5 of 9 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410 Number : TWNC00270123 Test Conducted (Ⅳ) Measurement Flowchart: Test for Halogen Content Reference Standard：EN 14582 Sampling/grinding or cutting Add absorbent in a combustion flask & place weighed sample in equipment Fill oxygen into calorimetric bomb Ignite then leave the bomb at room temperature Transfer the absorbent into a volumetric flask Make up with deionized water Analyzed by ion chromatography Page 6 of 9 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410 Number : TWNC00270123 Test Conducted (Ⅳ) Measurement Flowchart: Test For Phthalates Contents Reference Method: EN 14372: 2004 Sampling/grinding or cutting Weigh sample and add organic solvent By solvent extraction Concentrate the extract and make up with organic solvent Analyzed by GC-MSD Page 7 of 9 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410 Number : TWNC00270123 Test Conducted (Ⅳ) Measurement Flowchart: Test For Hexabromocyclododecane (HBCDD) Reference Standard：USEPA 3540C Sampling/grinding or cutting Weigh sample and add organic solvent By soxhlet extraction Concentrate the extract and make up with organic solvent Analyzed by GC-MSD End of Report This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a recommendation for any particular course of action. Intertek does not accept a duty of care or any other responsibility to any person other than the Client in respect of this report and only accepts liability to the Client insofar as is expressly contained in the terms and conditions governing Intertek's provision of services to you. Intertek makes no warranties or representations either express or implied with respect to this report save as provided for in those terms and conditions. We have aimed to conduct the Review on a diligent and careful basis and we do not accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by statute or otherwise, except in the event of our gross negligence or wilful misconduct. Page 8 of 9 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410 Number : TWNC00270123 Test Conducted Photo Page 9 of 9 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410 Test Report Applicant: Number : TWNC00286468 Littelfuse Philippines Inc. LIMA Technology Center, Lipa City, Malvar, Batangas Date : Nov 22, 2012 Sample Description: One (1) group of submitted samples said to be : Part Description : Overglaze (Coverglass) Paste (Sintered) Part Number : 011003 Date Sample Received : Nov 15, 2012 Date Test Started : Nov 17, 2012 Test Conducted : As requested by the applicant, for details please refer to attached pages. Authorized By: On Behalf Of Intertek Testing Services Taiwan Limited K. Y. Liang Director *THJ0286468* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410 Page 1 of 10 Number : TWNC00286468 Test Conducted (Ⅰ) Test Result Summary : Result (ppm) Submitted Samples Test Item Heavy Metal Cadmium (Cd) content Lead (Pb) content Mercury (Hg) content Chromium VI (Cr6+) content Polybrominated Biphenyls (PBBs) Monobrominated Biphenyls (MonoBB) Dibrominated Biphenyls (DiBB) Tribrominated Biphenyls (TriBB) Tetrabrominated Biphenyls (TetraBB) Pentabrominated Biphenyls (PentaBB) Hexabrominated Biphenyls (HexaBB) Heptabrominated Biphenyls (HeptaBB) Octabrominated Biphenyls (OctaBB) Nonabrominated Biphenyls (NonaBB) Decabrominated Biphenyl (DecaBB) Polybrominated Diphenyl Ethers (PBDEs) Monobrominated Diphenyl Ethers (MonoBDE) Dibrominated Diphenyl Ethers (DiBDE) Tribrominated Diphenyl Ethers (TriBDE) Tetrabrominated Diphenyl Ethers (TetraBDE) Pentabrominated Diphenyl Ethers (PentaBDE) Hexabrominated Diphenyl Ethers (HexaBDE) Heptabrominated Diphenyl Ethers (HeptaBDE) Octabrominated Diphenyl Ethers (OctaBDE) Nonabrominated Diphenyl Ethers (NonaBDE) Decabrominated Diphenyl Ether (DecaBDE) Halogen Content Fluorine (F) Chlorine (Cl) Bromine (Br) Iodine (I) ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND *THJ0286468* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410 Page 2 of 10 Number : TWNC00286468 Test Conducted (Ⅰ) Test Result Summary : Result (ppm) Submitted Samples Test Item Phthalates Di(2-ethylhexyl) Phthalate (DEHP) Dibutyl Phthalate (DBP) Benzyl Butyl Phthalate (BBP) Others Hexabromocyclododecane (HBCDD) ND ND ND ND Remarks: ppm = Parts per million based on weight of tested sample = mg/kg ND = Not detected Responsibility of Chemist : Irene Chiou / Kevin Liu / Cathy Chen Date Sample Received Test Period : Nov 15, 2012 : Nov 17, 2012 To Nov 21, 2012 (Ⅱ) RoHS Limits: Restricted Substances Cadmium (Cd) Content Lead (Pb) Content Mercury (Hg) Content Chromium VI (Cr6+) Content Polybrominated Biphenyls (PBBs) Polybrominated Diphenyl Ehters (PBDEs) Limits 0.01% (100ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) The above limits were quoted from Annex II of 2011/65/EU for homogeneous material. *THJ0286468* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410 Page 3 of 10 Number : TWNC00286468 Test Conducted (Ⅲ) Test Method: Test Item Reporting Limit Test Method With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the Cadmium (Cd) content 2 ppm tested samples are totally dissolved and determined by ICPOES. With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the Lead (Pb) content 2 ppm tested samples are totally dissolved and determined by ICPOES. With reference to IEC 62321 edition 1.0:2008 in clause 7, by microwave digestion until the Mercury (Hg) content 2 ppm tested samples are totally dissolved and determined by ICPOES. With reference to IEC 62321 edition Chromium VI (Cr6+) 1.0:2008 in annex C, by alkaline 1 ppm content digestion and determined by UV-Vis spectrophotometer. With reference to IEC 62321 edition 1.0:2008 in annex A, by Polybrominated solvent extraction and determined 5 ppm Biphenyls (PBBs) by GC-MS and further HPLC-DAD confirmation when necessary. With reference to IEC 62321 edition 1.0:2008 in annex A, by Polybrominated Diphenyl solvent extraction and determined 5 ppm Ethers (PBDEs) by GC-MS and further HPLC-DAD confirmation when necessary. *THJ0286468* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410 Page 4 of 10 Number : TWNC00286468 Test Conducted (Ⅲ) Test Method: Test Item Test Method With reference to EN 14582:2007 by Halogen Content calorimetric bomb with oxygen and determined by Ion Chromatograph. With reference to EN 14372: 2004, Phthalates by solvent extraction and determined by GC-MS. With reference to USEPA 3540C, by Hexabromocyclododecane solvent extraction and determined (HBCDD) by GC-MS. Reporting Limit 50 ppm 50 ppm 10 ppm Remark: Reporting limit = Quantitation limit of analyte in sample *THJ0286468* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410 Page 5 of 10 Number : TWNC00286468 Test Conducted (Ⅳ) Measurement Flowchart: Test for Cd/Pb/Hg/Chromium (VI)/PBBS/PBDES Contents Reference Standard: IEC 62321 edition 1.0:2008 Sample preparation For non-metal part For metal part Take sample and immerse into Aqua Regia, start to strip plating layer Stop the stripping procedure upon color change completely Take the Aqua solution as plating component and stripped body as substrate component PBBs/PBDEs Weigh sample and add organic solvent By Soxhlet extraction or Solvent extraction Concentrate the extract and make up with organic solvent Cr 6+ Substrate Cd/Pb/Hg Weigh sample and add alkaline solution For different material, digest the sample with *1 appropriate acid Plating Cr 6+ By spot test Definite temp. extraction Cool and filter the extract Confirm the tested samples are totally dissolved Negative *2 Get 50cm2 sample Make up with deionized water By boiling water extraction Analyzed by ICP-OES Analyzed by GC-MSD Make up with deionized water and add diphenyl-carbazide solution Remarks: *1: List of Appropriate Acid： Material Polymers Metals Electronics Analyzed by UV-VIS Acid Added for Digestion HNO3,HCl,HF,H2O2,H3BO3 HNO3,HCl,HF HNO3,HCl,H2O2,HBF4 *2: If the result of spot test is positive, Chromium VI would be determined as detected. *THJ0286468* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410 Page 6 of 10 Number : TWNC00286468 Test Conducted (Ⅳ) Measurement Flowchart: Test for Halogen Content Reference Standard：EN 14582 Sampling/grinding or cutting Add absorbent in a combustion flask & place weighed sample in equipment Fill oxygen into calorimetric bomb Ignite then leave the bomb at room temperature Transfer the absorbent into a volumetric flask Make up with deionized water Analyzed by ion chromatography *THJ0286468* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410 Page 7 of 10 Number : TWNC00286468 Test Conducted (Ⅳ) Measurement Flowchart: Test For Phthalates Contents Reference Method: EN 14372: 2004 Sampling/grinding or cutting Weigh sample and add organic solvent By solvent extraction Concentrate the extract and make up with organic solvent Analyzed by GC-MSD *THJ0286468* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410 Page 8 of 10 Number : TWNC00286468 Test Conducted (Ⅳ) Measurement Flowchart: Test For Hexabromocyclododecane (HBCDD) Reference Standard：USEPA 3540C Sampling/grinding or cutting Weigh sample and add organic solvent By soxhlet extraction Concentrate the extract and make up with organic solvent Analyzed by GC-MSD End of Report This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a recommendation for any particular course of action. Intertek does not accept a duty of care or any other responsibility to any person other than the Client in respect of this report and only accepts liability to the Client insofar as is expressly contained in the terms and conditions governing Intertek's provision of services to you. Intertek makes no warranties or representations either express or implied with respect to this report save as provided for in those terms and conditions. We have aimed to conduct the Review on a diligent and careful basis and we do not accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by statute or otherwise, except in the event of our gross negligence or wilful misconduct. *THJ0286468* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410 Page 9 of 10 Number : TWNC00286468 Test Conducted Photo *THJ0286468* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410 Page 10 of 10 Test Report Applicant: Number : TWNC00286469 Littelfuse Philippines Inc. LIMA Technology Center, Lipa City, Malvar, Batangas Date : Nov 22, 2012 Sample Description: One (1) group of submitted samples said to be : Part Description : Silver - End Termination Paste (Sintered) Part Number : 011001 Date Sample Received : Nov 15, 2012 Date Test Started : Nov 16, 2012 Test Conducted : As requested by the applicant, for details please refer to attached pages. Authorized By: On Behalf Of Intertek Testing Services Taiwan Limited K. Y. Liang Director *THJ0286469* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410 Page 1 of 10 Number : TWNC00286469 Test Conducted (Ⅰ) Test Result Summary : Result (ppm) Silvery material Test Item Heavy Metal Cadmium (Cd) content Lead (Pb) content Mercury (Hg) content Chromium VI (Cr6+) content Polybrominated Biphenyls (PBBs) Monobrominated Biphenyls (MonoBB) Dibrominated Biphenyls (DiBB) Tribrominated Biphenyls (TriBB) Tetrabrominated Biphenyls (TetraBB) Pentabrominated Biphenyls (PentaBB) Hexabrominated Biphenyls (HexaBB) Heptabrominated Biphenyls (HeptaBB) Octabrominated Biphenyls (OctaBB) Nonabrominated Biphenyls (NonaBB) Decabrominated Biphenyl (DecaBB) Polybrominated Diphenyl Ethers (PBDEs) Monobrominated Diphenyl Ethers (MonoBDE) Dibrominated Diphenyl Ethers (DiBDE) Tribrominated Diphenyl Ethers (TriBDE) Tetrabrominated Diphenyl Ethers (TetraBDE) Pentabrominated Diphenyl Ethers (PentaBDE) Hexabrominated Diphenyl Ethers (HexaBDE) Heptabrominated Diphenyl Ethers (HeptaBDE) Octabrominated Diphenyl Ethers (OctaBDE) Nonabrominated Diphenyl Ethers (NonaBDE) Decabrominated Diphenyl Ether (DecaBDE) Halogen Content Fluorine (F) Chlorine (Cl) Bromine (Br) Iodine (I) ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND *THJ0286469* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410 Page 2 of 10 Number : TWNC00286469 Test Conducted (Ⅰ) Test Result Summary : Result (ppm) Silvery material Test Item Phthalates Di(2-ethylhexyl) Phthalate (DEHP) Dibutyl Phthalate (DBP) Benzyl Butyl Phthalate (BBP) Others Hexabromocyclododecane (HBCDD) ND ND ND ND Remarks: ppm = Parts per million based on weight of tested sample = mg/kg ND = Not detected Responsibility of Chemist : Irene Chiou / Kevin Liu / Cathy Chen Date Sample Received Test Period : Nov 15, 2012 : Nov 16, 2012 to Nov 21, 2012 (Ⅱ) RoHS Limits: Restricted Substances Cadmium (Cd) Content Lead (Pb) Content Mercury (Hg) Content Chromium VI (Cr6+) Content Polybrominated Biphenyls (PBBs) Polybrominated Diphenyl Ehters (PBDEs) Limits 0.01% (100ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) The above limits were quoted from Annex II of 2011/65/EU for homogeneous material. *THJ0286469* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410 Page 3 of 10 Number : TWNC00286469 Test Conducted (Ⅲ) Test Method: Test Item Reporting Limit Test Method With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the Cadmium (Cd) content 2 ppm tested samples are totally dissolved and determined by ICPOES. With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the Lead (Pb) content 2 ppm tested samples are totally dissolved and determined by ICPOES. With reference to IEC 62321 edition 1.0:2008 in clause 7, by microwave digestion until the Mercury (Hg) content 2 ppm tested samples are totally dissolved and determined by ICPOES. With reference to IEC 62321 edition Chromium VI (Cr6+) 1.0:2008 in annex C, by alkaline 1 ppm content digestion and determined by UV-Vis spectrophotometer. With reference to IEC 62321 edition 1.0:2008 in annex A, by Polybrominated 5 ppm solvent extraction and determined Biphenyls (PBBs) by GC-MS and further HPLC-DAD confirmation when necessary. With reference to IEC 62321 edition 1.0:2008 in annex A, by Polybrominated Diphenyl 5 ppm solvent extraction and determined Ethers (PBDEs) by GC-MS and further HPLC-DAD confirmation when necessary. *THJ0286469* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410 Page 4 of 10 Number : TWNC00286469 Test Conducted (Ⅲ) Test Method: Test Item Test Method With reference to EN 14582:2007 by Halogen Content calorimetric bomb with oxygen and determined by Ion Chromatograph. With reference to EN 14372: 2004, Phthalates by solvent extraction and determined by GC-MS. With reference to USEPA 3540C, by Hexabromocyclododecane solvent extraction and determined (HBCDD) by GC-MS. Reporting Limit 50 ppm 50 ppm 10 ppm Remark: Reporting limit = Quantitation limit of analyte in sample *THJ0286469* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410 Page 5 of 10 Number : TWNC00286469 Test Conducted (Ⅳ) Measurement Flowchart: Test for Cd/Pb/Hg/Chromium (VI)/PBBS/PBDES Contents Reference Standard: IEC 62321 edition 1.0:2008 Sample preparation For non-metal part For metal part Take sample and immerse into Aqua Regia, start to strip plating layer Stop the stripping procedure upon color change completely Take the Aqua solution as plating component and stripped body as substrate component PBBs/PBDEs Weigh sample and add organic solvent By Soxhlet extraction or Solvent extraction Concentrate the extract and make up with organic solvent Cr 6+ Substrate Cd/Pb/Hg Weigh sample and add alkaline solution For different material, digest the sample with *1 appropriate acid Plating Cr 6+ By spot test Definite temp. extraction Cool and filter the extract Confirm the tested samples are totally dissolved Negative *2 Get 50cm2 sample Make up with deionized water By boiling water extraction Analyzed by ICP-OES Analyzed by GC-MSD Make up with deionized water and add diphenyl-carbazide solution Remarks: *1: List of Appropriate Acid： Material Polymers Metals Electronics Analyzed by UV-VIS Acid Added for Digestion HNO3,HCl,HF,H2O2,H3BO3 HNO3,HCl,HF HNO3,HCl,H2O2,HBF4 *2: If the result of spot test is positive, Chromium VI would be determined as detected. *THJ0286469* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410 Page 6 of 10 Number : TWNC00286469 Test Conducted (Ⅳ) Measurement Flowchart: Test for Halogen Content Reference Standard：EN 14582 Sampling/grinding or cutting Add absorbent in a combustion flask & place weighed sample in equipment Fill oxygen into calorimetric bomb Ignite then leave the bomb at room temperature Transfer the absorbent into a volumetric flask Make up with deionized water Analyzed by ion chromatography *THJ0286469* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410 Page 7 of 10 Number : TWNC00286469 Test Conducted (Ⅳ) Measurement Flowchart: Test For Phthalates Contents Reference Method: EN 14372: 2004 Sampling/grinding or cutting Weigh sample and add organic solvent By solvent extraction Concentrate the extract and make up with organic solvent Analyzed by GC-MSD *THJ0286469* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410 Page 8 of 10 Number : TWNC00286469 Test Conducted (Ⅳ) Measurement Flowchart: Test For Hexabromocyclododecane (HBCDD) Reference Standard：USEPA 3540C Sampling/grinding or cutting Weigh sample and add organic solvent By soxhlet extraction Concentrate the extract and make up with organic solvent Analyzed by GC-MSD End of Report This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a recommendation for any particular course of action. Intertek does not accept a duty of care or any other responsibility to any person other than the Client in respect of this report and only accepts liability to the Client insofar as is expressly contained in the terms and conditions governing Intertek's provision of services to you. Intertek makes no warranties or representations either express or implied with respect to this report save as provided for in those terms and conditions. We have aimed to conduct the Review on a diligent and careful basis and we do not accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by statute or otherwise, except in the event of our gross negligence or wilful misconduct. *THJ0286469* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410 Page 9 of 10 Number : TWNC00286469 Test Conducted Photo *THJ0286469* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410 Page 10 of 10 Test Report Applicant: Number : TWNC00286465 Littelfuse Philippines Inc. LIMA Technology Center, Lipa City, Malvar, Batangas Date : Nov 22, 2012 Sample Description: One (1) group of submitted samples said to be : Part Description : Nickel Anode Part Number : 010118 Date Sample Received : Nov 15, 2012 Date Test Started : Nov 16, 2012 Test Conducted : As requested by the applicant, for details please refer to attached pages. Authorized By: On Behalf Of Intertek Testing Services Taiwan Limited K. Y. Liang Director *THJ0286465* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410 Page 1 of 6 Number : TWNC00286465 Test Conducted (Ⅰ) Test Result Summary : Result (ppm) Silvery Metal Test Item Heavy Metal Cadmium (Cd) content Lead (Pb) content Mercury (Hg) content Chromium VI (Cr6+) content (mg/kg with 50cm2) ND ND ND Negative (< 0.02)(#) Remarks: ppm = Parts per million based on weight of tested sample = mg/kg ND = Not detected < = Less than mg/kg with 50cm2 = milligram per kilogram with 50 square centimetre Negative = A negative test result indicated positive observation was not found at the time of Test. # = Due to the insufficient sample area, reduced total sample surface of 10 cm2 was used and the dilution factor was adjusted accordingly. Responsibility of Chemist : Irene Chiou / Kevin Liu Date Sample Received Test Period : Nov 15, 2012 : Nov 16, 2012 To Nov 21, 2012 (Ⅱ) RoHS Limits: Restricted Substances Cadmium (Cd) Content Lead (Pb) Content Mercury (Hg) Content Chromium VI (Cr6+) Content Limits 0.01% (100ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) The above limits were quoted from Annex II of 2011/65/EU for homogeneous material. *THJ0286465* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410 Page 2 of 6 Number : TWNC00286465 Test Conducted (Ⅲ) Test Method: Test Item Cadmium (Cd) content Lead (Pb) content Mercury (Hg) content Chromium VI (Cr6+) content Test Method With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in clause 7, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in annex B, by boiling water extraction and determined by UV-Vis Spectrophotometer. Reporting Limit 2 ppm 2 ppm 2 ppm 0.02 mg/kg with 50cm2 Remark: Reporting limit = Quantitation limit of analyte in sample *THJ0286465* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410 Page 3 of 6 Number : TWNC00286465 Test Conducted (Ⅳ) Measurement Flowchart: Test For Cd/Pb/Hg/Chromium (VI) Reference Standard：IEC 62321 edition 1.0:2008 Sampling/grinding or cutting Cd/Pb/Hg Cr 6+ Polymers / Electronics Metal For different material, digest the sample with *1 appropriate acid By spot test Negative Confirm the tested samples are totally dissolved Make up with deionized water *2 Weigh sample and add alkaline solution Get 50cm2 sample Definite temp. extraction Boiling water extraction Cool and filter the extract Analyzed by ICP-OES Make up with deionized water and add diphenylcarbazide solution Analyzed by UV-VIS *THJ0286465* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410 Page 4 of 6 Number : TWNC00286465 Test Conducted Remarks: *1: List of Appropriate Acid： Material Acid Added for Digestion Polymers HNO3,HCl,HF,H2O2,H3BO3 Metals HNO3,HCl,HF Electronics HNO3,HCl,H2O2,HBF4 *2: If the result of spot test is positive, Chromium VI would be determined as detected. End of Report This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a recommendation for any particular course of action. Intertek does not accept a duty of care or any other responsibility to any person other than the Client in respect of this report and only accepts liability to the Client insofar as is expressly contained in the terms and conditions governing Intertek's provision of services to you. Intertek makes no warranties or representations either express or implied with respect to this report save as provided for in those terms and conditions. We have aimed to conduct the Review on a diligent and careful basis and we do not accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by statute or otherwise, except in the event of our gross negligence or wilful misconduct. *THJ0286465* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410 Page 5 of 6 Number : TWNC00286465 Test Conducted Photo *THJ0286465* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410 Page 6 of 6 Test Report Applicant: Number : TWNC00236188 Littelfuse, Philippines Inc. Date LIMA Technology Center, Lipa City, Malvar, Batangas : Dec 13, 2011 Sample Description: One (1) group of submitted samples said to be : Part Description : Tin Anode Part Number : 010119 Date Sample Received : Dec 08, 2011 Date Test Started : Dec 09, 2011 Test Conducted : As requested by the applicant, for details please refer to attached pages. Authorized By: On Behalf Of Intertek Testing Services Taiwan Limited K. Y. Liang Director This report shall not be reproduced except in full, without the written approval of the laboratory. Page 1 of 5 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401 Number : TWNC00236188 Test Conducted (Ⅰ) Test Result Summary : Test Item Heavy Metal Cadmium (Cd) content Lead (Pb) content Mercury (Hg) content Chromium VI (Cr6+) content (mg/kg with 50cm2) Result (ppm) Silvery Metal ND 54 ND Negative (< 0.02) Remarks: ppm = Parts per million based on weight of tested sample = mg/kg ND = Not detected < = Less than mg/kg with 50cm2 = milligram per kilogram with 50 square centimetre Negative = A negative test result indicated positive observation was not found at the time of Test. Responsibility of Chemist : Irene Chiou / Kevin Liu Date Sample Received Test Period : Dec 08, 2011 : Dec 09, 2011 To Dec 13, 2011 (Ⅱ) RoHS Requirement: Restricted Substances Cadmium (Cd) Content Lead (Pb) Content Mercury (Hg) Content Chromium VI (Cr6+) Content Limits 0.01% (100ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for homogeneous material. Page 2 of 5 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401 Number : TWNC00236188 Test Conducted (Ⅲ) Test Method: Test Item Test Method With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by Cadmium (Cd) content microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by Lead (Pb) content microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in clause 7, by microwave Mercury (Hg) content digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition Chromium VI (Cr6+) 1.0:2008 in annex B, by boiling content water extraction and determined by UV-Vis spectrophotometer. Reporting Limit 2 ppm 2 ppm 2 ppm 0.02 mg/kg with 50cm2 Remark: Reporting limit = Quantitation limit of analyte in sample Page 3 of 5 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401 Number : TWNC00236188 Test Conducted (Ⅳ) Measurement Flowchart: Test for Cd/Pb/Hg/Chromium (VI)/PBBS/PBDES Contents Reference Standard: IEC 62321 edition 1.0:2008 Sample preparation For metal part Take sample and immerse into Aqua Regia, start to strip plating layer Stop the stripping procedure upon color change completely Take the Aqua solution as plating component and stripped body as substrate component Cd/Pb/Hg Cr Weigh sample and add organic solvent By spot test Negative Confirm the tested samples are totally dissolved Make up with deionized water PBBs/PBDEs Polymers / electronics Metal For different material, digest the sample with *1 appropriate acid 6+ Get 50cm2 sample By boiling water extraction *2 Weigh sample and add alkaline solution By Soxhlet extraction or Solvent extraction Definite temp. extraction Cool and filter the extract Analyzed by ICP-OES Concentrate the extract and make up with organic solvent Analyzed by GC-MSD Make up with deionized water and add diphenylcarbazide solution Remarks: *1: List of Appropriate Acid： Material Polymers Metals Electronics Analyzed by UV-VIS Acid Added for Digestion HNO3,HCl,HF,H2O2,H3BO3 HNO3,HCl,HF HNO3,HCl,H2O2,HBF4 *2: If the result of spot test is positive, Chromium VI would be determined as detected. End of Report Page 4 of 5 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401 Number : TWNC00236188 Test Conducted Photo Page 5 of 5 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401 Test Report Applicant: Number : TWNC00286466 Littelfuse Philippines Inc. LIMA Technology Center, Lipa City, Malvar, Batangas Date : Nov 22, 2012 Sample Description: One (1) group of submitted samples said to be : Part Description : Ceramic Substrate Part Number : 039641 Date Sample Received : Nov 15, 2012 Date Test Started : Nov 17, 2012 Test Conducted : As requested by the applicant, for details please refer to attached pages. Authorized By: On Behalf Of Intertek Testing Services Taiwan Limited K. Y. Liang Director *THJ0286466* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410 Page 1 of 7 Number : TWNC00286466 Test Conducted (Ⅰ) Test Result Summary : Result (ppm) White ceramic Test Item Heavy Metal Cadmium (Cd) content Lead (Pb) content Mercury (Hg) content Chromium VI (Cr6+) content Polybrominated Biphenyls (PBBs) Monobrominated Biphenyls (MonoBB) Dibrominated Biphenyls (DiBB) Tribrominated Biphenyls (TriBB) Tetrabrominated Biphenyls (TetraBB) Pentabrominated Biphenyls (PentaBB) Hexabrominated Biphenyls (HexaBB) Heptabrominated Biphenyls (HeptaBB) Octabrominated Biphenyls (OctaBB) Nonabrominated Biphenyls (NonaBB) Decabrominated Biphenyl (DecaBB) Polybrominated Diphenyl Ethers (PBDEs) Monobrominated Diphenyl Ethers (MonoBDE) Dibrominated Diphenyl Ethers (DiBDE) Tribrominated Diphenyl Ethers (TriBDE) Tetrabrominated Diphenyl Ethers (TetraBDE) Pentabrominated Diphenyl Ethers (PentaBDE) Hexabrominated Diphenyl Ethers (HexaBDE) Heptabrominated Diphenyl Ethers (HeptaBDE) Octabrominated Diphenyl Ethers (OctaBDE) Nonabrominated Diphenyl Ethers (NonaBDE) Decabrominated Diphenyl Ether (DecaBDE) Halogen Content Fluorine (F) Chlorine (Cl) Bromine (Br) Iodine (I) ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND Remarks: ppm = Parts per million based on weight of tested sample = mg/kg ND = Not detected Responsibility of Chemist : Irene Chiou / Kevin Liu / Cathy Chen Date Sample Received Test Period : Nov 15 : Nov 17, 2012 to Nov 21, 2012 *THJ0286466* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410 Page 2 of 7 Number : TWNC00286466 Test Conducted (Ⅱ) RoHS Limits: Restricted Substances Cadmium (Cd) Content Lead (Pb) Content Mercury (Hg) Content Chromium VI (Cr6+) Content Polybrominated Biphenyls (PBBs) Polybrominated Diphenyl Ehters (PBDEs) Limits 0.01% (100ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) The above limits were quoted from Annex II of 2011/65/EU for homogeneous material. (Ⅲ) Test Method: Test Item Cadmium (Cd) content Lead (Pb) content Mercury (Hg) content Chromium VI (Cr6+) content Test Method With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in clause 7, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in annex C, by alkaline digestion and determined by UV-Vis spectrophotometer. Reporting Limit *THJ0286466* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410 2 ppm 2 ppm 2 ppm 1 ppm Page 3 of 7 Number : TWNC00286466 Test Conducted (Ⅲ) Test Method: Test Item Polybrominated Biphenyls (PBBs) Polybrominated Diphenyl Ethers (PBDEs) Halogen Content Test Method With reference to IEC 62321 edition 1.0:2008 in annex A, by solvent extraction and determined by GC-MS and further HPLC-DAD confirmation when necessary. With reference to IEC 62321 edition 1.0:2008 in annex A, by solvent extraction and determined by GC-MS and further HPLC-DAD confirmation when necessary. With reference to EN 14582:2007 by calorimetric bomb with oxygen and determined by Ion Chromatograph. Reporting Limit 5 ppm 5 ppm 50 ppm Remark: Reporting limit = Quantitation limit of analyte in sample *THJ0286466* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410 Page 4 of 7 Number : TWNC00286466 Test Conducted (Ⅳ) Measurement Flowchart: Test for Cd/Pb/Hg/Chromium (VI)/PBBS/PBDES Contents Reference Standard: IEC 62321 edition 1.0:2008 Sample preparation For non-metal part For metal part Take sample and immerse into Aqua Regia, start to strip plating layer Stop the stripping procedure upon color change completely Take the Aqua solution as plating component and stripped body as substrate component PBBs/PBDEs Weigh sample and add organic solvent By Soxhlet extraction or Solvent extraction Concentrate the extract and make up with organic solvent Cr 6+ Substrate Cd/Pb/Hg Weigh sample and add alkaline solution For different material, digest the sample with *1 appropriate acid Plating Cr 6+ By spot test Definite temp. extraction Cool and filter the extract Confirm the tested samples are totally dissolved Negative *2 Get 50cm2 sample Make up with deionized water By boiling water extraction Analyzed by ICP-OES Analyzed by GC-MSD Make up with deionized water and add diphenyl-carbazide solution Remarks: *1: List of Appropriate Acid： Material Polymers Metals Electronics Analyzed by UV-VIS Acid Added for Digestion HNO3,HCl,HF,H2O2,H3BO3 HNO3,HCl,HF HNO3,HCl,H2O2,HBF4 *2: If the result of spot test is positive, Chromium VI would be determined as detected. *THJ0286466* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410 Page 5 of 7 Number : TWNC00286466 Test Conducted (Ⅳ) Measurement Flowchart: Test for Halogen Content Reference Standard：EN 14582 Sampling/grinding or cutting Add absorbent in a combustion flask & place weighed sample in equipment Fill oxygen into calorimetric bomb Ignite then leave the bomb at room temperature Transfer the absorbent into a volumetric flask Make up with deionized water Analyzed by ion chromatography End of Report This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a recommendation for any particular course of action. Intertek does not accept a duty of care or any other responsibility to any person other than the Client in respect of this report and only accepts liability to the Client insofar as is expressly contained in the terms and conditions governing Intertek's provision of services to you. Intertek makes no warranties or representations either express or implied with respect to this report save as provided for in those terms and conditions. We have aimed to conduct the Review on a diligent and careful basis and we do not accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by statute or otherwise, except in the event of our gross negligence or wilful misconduct. *THJ0286466* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410 Page 6 of 7 Number : TWNC00286466 Test Conducted Photo *THJ0286466* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410 Page 7 of 7