ANALYTICAL REPORT Job Number: 660-17097-1 Job Description: Raytheon For: ARCADIS U.S., Inc. 14055 Riveredge Drive Suite 400 Tampa, FL 33637 Attention: Mr. Gus Suarez _____________________________________________ Designee for Natalie Tafuni Project Manager I [email protected] 07/15/2008 Revision: 1 Methods: FDEP, DOH Certification #: E84282, E81005 These test results meet all the requirements of NELAC unless specified in the case narrative. All questions regarding this test report should be directed to the STL Project Manager who signed this test report. The estimated uncertainty associated with these reported results is available upon request. The results contained in this test report relate only to these samples included herein. TestAmerica Laboratories, Inc. TestAmerica Tampa 6712 Benjamin Road, Suite 100, Tampa, FL 33634 Tel (813) 885-7427 Fax (813) 885-7049 www.testamericainc.com Page 1 of 59 07/15/2008 Job Narrative 660-J17097-1 Receipt All samples were received in good condition within temperature requirements. This report was revised on 7/15/08 in order to address FDEP's concerns dated 6/23/08. The issues are as noted: Cooler temperature not noted on Chain of Custody or Laboratory receipt log. Temperature was taken at time of receipt of samples. The temperature was noted on the Chain of Custody but not the Checklist, however, it was included in the sample login acknowledgement which has been attached to this report. 8260B Sample surrogates were missing from the original report. This revised report has included the surrogates and they are all within QC limits. No other analytical or quality issues were noted. Page 2 of 59 07/15/2008 EXECUTIVE SUMMARY - Detections Client: ARCADIS U.S., Inc. Lab Sample ID Analyte 660-17097-1 Client Sample ID Result / Qualifier ug/L 8260B 30 38 100 33 22 12 1.0 1.0 1.0 1.0 1.0 1.0 ug/L ug/L ug/L ug/L ug/L ug/L 8260B 8260B 8260B 8260B 8260B 8260B 87 1.0 ug/L 8260B 73 3.0 4.6 9.4 4.9 0.76 I 1.0 1.0 1.0 1.0 1.0 1.0 ug/L ug/L ug/L ug/L ug/L ug/L 8260B 8260B 8260B 8260B 8260B 8260B 0.60 I 1.0 ug/L 8260B 1.0 ug/L 8260B 1.0 1.0 1.0 ug/L ug/L ug/L 8260B 8260B 8260B CP-14 (24'-26') Trichloroethene 660-17097-9 1.0 CP-14 (19'-21') Trichloroethene 660-17097-8 6.9 CP-22 (48'-50') 1,4-Dioxane 1,1-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene Trichloroethene Vinyl chloride 660-17097-7 Method CP-22 (34'-36') 1,4-Dioxane 660-17097-4 Units CP-22 (20'-22') 1,4-Dioxane 1,1-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene Trichloroethene Vinyl chloride 660-17097-3 Reporting Limit CP-22 (9'-11') cis-1,2-Dichloroethene 660-17097-2 Job Number: 660-17097-1 6.2 CP-14 (29'-31') cis-1,2-Dichloroethene Ethylbenzene Trichloroethene 4.8 0.49 98 I TestAmerica Tampa Page 3 of 59 07/15/2008 EXECUTIVE SUMMARY - Detections Client: ARCADIS U.S., Inc. Lab Sample ID Analyte 660-17097-10 Client Sample ID Result / Qualifier Reporting Limit Units Method CP-14 (38'-40') 1,4-Dioxane cis-1,2-Dichloroethene Trichloroethene 660-17097-11 Job Number: 660-17097-1 10 160 5500 1.0 50 50 ug/L ug/L ug/L 8260B 8260B 8260B 120 68 3400 10 50 50 ug/L ug/L ug/L 8260B 8260B 8260B CP-14 (47'-49') 1,4-Dioxane cis-1,2-Dichloroethene Trichloroethene TestAmerica Tampa Page 4 of 59 07/15/2008 METHOD SUMMARY Client: ARCADIS U.S., Inc. Description Job Number: 660-17097-1 Lab Location Method Preparation Method Matrix: Water Volatile Organic Compounds by GC/MS TAL TAM SW846 8260B Volatile Organics by GC/MS Purge-and-Trap Purge-and-Trap TAL TAM TAL TAM TAL TAM SW846 8260B SW846 5030B SW846 5030B Lab References: TAL TAM = TestAmerica Tampa Method References: SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates. TestAmerica Tampa Page 5 of 59 07/15/2008 SAMPLE SUMMARY Client: ARCADIS U.S., Inc. Job Number: 660-17097-1 Lab Sample ID Client Sample ID Client Matrix 660-17097-1 660-17097-2 660-17097-3 660-17097-4 660-17097-5 660-17097-6 660-17097-7 660-17097-8 660-17097-9 660-17097-10 660-17097-11 660-17097-12 CP-22 (9'-11') CP-22 (20'-22') CP-22 (34'-36') CP-22 (48'-50') CP-22 (56'-58') CP-14 (8'-10') CP-14 (19'-21') CP-14 (24'-26') CP-14 (29'-31') CP-14 (38'-40') CP-14 (47'-49') Trip Blank Water Water Water Water Water Water Water Water Water Water Water Water Date/Time Sampled 07/19/2007 07/19/2007 07/19/2007 07/19/2007 07/19/2007 07/19/2007 07/19/2007 07/19/2007 07/19/2007 07/20/2007 07/20/2007 07/19/2007 0930 0955 1030 1107 1241 1638 1655 1708 1723 0815 0903 0000 Date/Time Received 07/20/2007 07/20/2007 07/20/2007 07/20/2007 07/20/2007 07/20/2007 07/20/2007 07/20/2007 07/20/2007 07/20/2007 07/20/2007 07/20/2007 1410 1410 1410 1410 1410 1410 1410 1410 1410 1410 1410 1410 TestAmerica Tampa Page 6 of 59 07/15/2008 SAMPLE RESULTS TestAmerica Tampa Page 7 of 59 07/15/2008 Analytical Data Client: ARCADIS U.S., Inc. Client Sample ID: CP-22 (9'-11') Lab Sample ID: Client Matrix: 660-17097-1 Water Job Number: 660-17097-1 Date Sampled: Date Received: 07/19/2007 0930 07/20/2007 1410 8260B Volatile Organic Compounds by GC/MS Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260B 5030B 1.0 07/23/2007 1624 07/23/2007 1624 Analyte 1,1,1,2-Tetrachloroethane 1,1,1-Trichloroethane 1,1,2,2-Tetrachloroethane 1,1,2-Trichloroethane 1,1-Dichloroethane 1,1-Dichloroethene 1,1-Dichloropropene 1,2,3-Trichlorobenzene 1,2,3-Trichloropropane 1,2,4-Trichlorobenzene 1,2,4-Trimethylbenzene 1,2-Dibromo-3-Chloropropane 1,2-Dichlorobenzene 1,2-Dichloroethane 1,2-Dichloropropane 1,3,5-Trimethylbenzene 1,3-Dichlorobenzene 1,3-Dichloropropane 1,4-Dichlorobenzene 2,2-Dichloropropane 2-Chlorotoluene 2-Hexanone 4-Chlorotoluene 4-Isopropyltoluene Acetone Benzene Bromobenzene Bromoform Bromomethane Carbon disulfide Carbon tetrachloride Chlorobenzene Chlorobromomethane Chlorodibromomethane Chloroethane Chloroform Chloromethane cis-1,2-Dichloroethene cis-1,3-Dichloropropene Dibromomethane Dichlorobromomethane Dichlorodifluoromethane Ethylbenzene Ethylene Dibromide TestAmerica Tampa Analysis Batch: 660-47317 Result (ug/L) 0.63 0.46 0.15 0.47 0.52 0.45 0.31 0.77 0.18 0.58 0.86 2.5 0.44 0.57 0.52 0.54 0.64 0.39 0.52 0.36 0.65 4.4 0.52 0.69 9.9 0.50 0.58 0.58 2.5 0.85 0.42 0.63 0.58 0.34 2.5 0.90 1.0 6.9 0.14 0.41 0.35 2.5 0.44 0.50 Page 8 of 59 Instrument ID: BVMJ GC/MS Lab File ID: 1JG2318.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U MDL 0.63 0.46 0.15 0.47 0.52 0.45 0.31 0.77 0.18 0.58 0.86 2.5 0.44 0.57 0.52 0.54 0.64 0.39 0.52 0.36 0.65 4.4 0.52 0.69 9.9 0.50 0.58 0.58 2.5 0.85 0.42 0.63 0.58 0.34 2.5 0.90 1.0 0.65 0.14 0.41 0.35 2.5 0.44 0.50 PQL 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 10 1.0 1.0 20 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 4.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 07/15/2008 Analytical Data Client: ARCADIS U.S., Inc. Client Sample ID: CP-22 (9'-11') Lab Sample ID: Client Matrix: 660-17097-1 Water Job Number: 660-17097-1 Date Sampled: Date Received: 07/19/2007 0930 07/20/2007 1410 8260B Volatile Organic Compounds by GC/MS Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260B 5030B 1.0 07/23/2007 1624 07/23/2007 1624 Analyte Hexachlorobutadiene Isopropylbenzene 2-Butanone (MEK) 4-Methyl-2-pentanone (MIBK) Methyl tert-butyl ether Methylene Chloride m-Xylene & p-Xylene Naphthalene n-Butylbenzene N-Propylbenzene o-Xylene sec-Butylbenzene Styrene tert-Butylbenzene Tetrachloroethene Toluene trans-1,2-Dichloroethene trans-1,3-Dichloropropene Trichloroethene Trichlorofluoromethane Vinyl chloride Analysis Batch: 660-47317 Result (ug/L) 0.40 0.19 8.4 3.8 0.44 4.0 0.60 2.5 0.67 0.59 0.50 0.63 0.98 0.84 0.50 0.51 0.44 0.14 0.50 2.5 0.50 Surrogate Toluene-d8 (Surr) 4-Bromofluorobenzene Dibromofluoromethane %Rec 115 118 97 TestAmerica Tampa Page 9 of 59 Instrument ID: BVMJ GC/MS Lab File ID: 1JG2318.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U U U U U U U U U U U U U U U U U U U U U MDL 0.40 0.19 8.4 3.8 0.44 4.0 0.60 2.5 0.67 0.59 0.50 0.63 0.98 0.84 0.50 0.51 0.44 0.14 0.50 2.5 0.50 PQL 1.0 1.0 10 10 1.0 5.0 2.0 5.0 1.0 1.0 1.0 1.0 2.0 1.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 Acceptance Limits 77 - 122 74 - 126 70 - 130 07/15/2008 Analytical Data Client: ARCADIS U.S., Inc. Client Sample ID: CP-22 (9'-11') Lab Sample ID: Client Matrix: 660-17097-1 Water Job Number: 660-17097-1 Date Sampled: Date Received: 07/19/2007 0930 07/20/2007 1410 8260B Volatile Organics by GC/MS Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260B 5030B 1.0 07/23/2007 1624 07/23/2007 1624 Analyte 1,4-Dioxane TestAmerica Tampa Analysis Batch: 660-47328 Result (ug/L) 0.54 Page 10 of 59 Instrument ID: BVMJ GC/MS Lab File ID: 1JG2318.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U MDL 0.54 PQL 1.0 07/15/2008 Analytical Data Client: ARCADIS U.S., Inc. Client Sample ID: CP-22 (20'-22') Lab Sample ID: Client Matrix: 660-17097-2 Water Job Number: 660-17097-1 Date Sampled: Date Received: 07/19/2007 0955 07/20/2007 1410 8260B Volatile Organic Compounds by GC/MS Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260B 5030B 1.0 07/23/2007 1649 07/23/2007 1649 Analyte 1,1,1,2-Tetrachloroethane 1,1,1-Trichloroethane 1,1,2,2-Tetrachloroethane 1,1,2-Trichloroethane 1,1-Dichloroethane 1,1-Dichloroethene 1,1-Dichloropropene 1,2,3-Trichlorobenzene 1,2,3-Trichloropropane 1,2,4-Trichlorobenzene 1,2,4-Trimethylbenzene 1,2-Dibromo-3-Chloropropane 1,2-Dichlorobenzene 1,2-Dichloroethane 1,2-Dichloropropane 1,3,5-Trimethylbenzene 1,3-Dichlorobenzene 1,3-Dichloropropane 1,4-Dichlorobenzene 2,2-Dichloropropane 2-Chlorotoluene 2-Hexanone 4-Chlorotoluene 4-Isopropyltoluene Acetone Benzene Bromobenzene Bromoform Bromomethane Carbon disulfide Carbon tetrachloride Chlorobenzene Chlorobromomethane Chlorodibromomethane Chloroethane Chloroform Chloromethane cis-1,2-Dichloroethene cis-1,3-Dichloropropene Dibromomethane Dichlorobromomethane Dichlorodifluoromethane Ethylbenzene Ethylene Dibromide TestAmerica Tampa Analysis Batch: 660-47317 Result (ug/L) 0.63 0.46 0.15 0.47 38 100 0.31 0.77 0.18 0.58 0.86 2.5 0.44 0.57 0.52 0.54 0.64 0.39 0.52 0.36 0.65 4.4 0.52 0.69 9.9 0.50 0.58 0.58 2.5 0.85 0.42 0.63 0.58 0.34 2.5 0.90 1.0 33 0.14 0.41 0.35 2.5 0.44 0.50 Page 11 of 59 Instrument ID: BVMJ GC/MS Lab File ID: 1JG2319.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U MDL 0.63 0.46 0.15 0.47 0.52 0.45 0.31 0.77 0.18 0.58 0.86 2.5 0.44 0.57 0.52 0.54 0.64 0.39 0.52 0.36 0.65 4.4 0.52 0.69 9.9 0.50 0.58 0.58 2.5 0.85 0.42 0.63 0.58 0.34 2.5 0.90 1.0 0.65 0.14 0.41 0.35 2.5 0.44 0.50 PQL 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 10 1.0 1.0 20 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 4.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 07/15/2008 Analytical Data Client: ARCADIS U.S., Inc. Client Sample ID: CP-22 (20'-22') Lab Sample ID: Client Matrix: 660-17097-2 Water Job Number: 660-17097-1 Date Sampled: Date Received: 07/19/2007 0955 07/20/2007 1410 8260B Volatile Organic Compounds by GC/MS Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260B 5030B 1.0 07/23/2007 1649 07/23/2007 1649 Analyte Hexachlorobutadiene Isopropylbenzene 2-Butanone (MEK) 4-Methyl-2-pentanone (MIBK) Methyl tert-butyl ether Methylene Chloride m-Xylene & p-Xylene Naphthalene n-Butylbenzene N-Propylbenzene o-Xylene sec-Butylbenzene Styrene tert-Butylbenzene Tetrachloroethene Toluene trans-1,2-Dichloroethene trans-1,3-Dichloropropene Trichloroethene Trichlorofluoromethane Vinyl chloride Surrogate Toluene-d8 (Surr) 4-Bromofluorobenzene Dibromofluoromethane TestAmerica Tampa Analysis Batch: 660-47317 Result (ug/L) 0.40 0.19 8.4 3.8 0.44 4.0 0.60 2.5 0.67 0.59 0.50 0.63 0.98 0.84 0.50 0.51 0.44 0.14 22 2.5 12 %Rec 104 107 89 Page 12 of 59 Instrument ID: BVMJ GC/MS Lab File ID: 1JG2319.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U U U U U U U U U U U U U U U U U U U MDL 0.40 0.19 8.4 3.8 0.44 4.0 0.60 2.5 0.67 0.59 0.50 0.63 0.98 0.84 0.50 0.51 0.44 0.14 0.50 2.5 0.50 PQL 1.0 1.0 10 10 1.0 5.0 2.0 5.0 1.0 1.0 1.0 1.0 2.0 1.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 Acceptance Limits 77 - 122 74 - 126 70 - 130 07/15/2008 Analytical Data Client: ARCADIS U.S., Inc. Client Sample ID: CP-22 (20'-22') Lab Sample ID: Client Matrix: 660-17097-2 Water Job Number: 660-17097-1 Date Sampled: Date Received: 07/19/2007 0955 07/20/2007 1410 8260B Volatile Organics by GC/MS Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260B 5030B 1.0 07/23/2007 1649 07/23/2007 1649 Analyte 1,4-Dioxane TestAmerica Tampa Analysis Batch: 660-47328 Result (ug/L) 30 Page 13 of 59 Instrument ID: BVMJ GC/MS Lab File ID: 1JG2319.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier MDL 0.54 PQL 1.0 07/15/2008 Analytical Data Client: ARCADIS U.S., Inc. Client Sample ID: CP-22 (34'-36') Lab Sample ID: Client Matrix: 660-17097-3 Water Job Number: 660-17097-1 Date Sampled: Date Received: 07/19/2007 1030 07/20/2007 1410 8260B Volatile Organic Compounds by GC/MS Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260B 5030B 1.0 07/23/2007 1714 07/23/2007 1714 Analyte 1,1,1,2-Tetrachloroethane 1,1,1-Trichloroethane 1,1,2,2-Tetrachloroethane 1,1,2-Trichloroethane 1,1-Dichloroethane 1,1-Dichloroethene 1,1-Dichloropropene 1,2,3-Trichlorobenzene 1,2,3-Trichloropropane 1,2,4-Trichlorobenzene 1,2,4-Trimethylbenzene 1,2-Dibromo-3-Chloropropane 1,2-Dichlorobenzene 1,2-Dichloroethane 1,2-Dichloropropane 1,3,5-Trimethylbenzene 1,3-Dichlorobenzene 1,3-Dichloropropane 1,4-Dichlorobenzene 2,2-Dichloropropane 2-Chlorotoluene 2-Hexanone 4-Chlorotoluene 4-Isopropyltoluene Acetone Benzene Bromobenzene Bromoform Bromomethane Carbon disulfide Carbon tetrachloride Chlorobenzene Chlorobromomethane Chlorodibromomethane Chloroethane Chloroform Chloromethane cis-1,2-Dichloroethene cis-1,3-Dichloropropene Dibromomethane Dichlorobromomethane Dichlorodifluoromethane Ethylbenzene Ethylene Dibromide TestAmerica Tampa Analysis Batch: 660-47317 Result (ug/L) 0.63 0.46 0.15 0.47 0.52 0.45 0.31 0.77 0.18 0.58 0.86 2.5 0.44 0.57 0.52 0.54 0.64 0.39 0.52 0.36 0.65 4.4 0.52 0.69 9.9 0.50 0.58 0.58 2.5 0.85 0.42 0.63 0.58 0.34 2.5 0.90 1.0 0.65 0.14 0.41 0.35 2.5 0.44 0.50 Page 14 of 59 Instrument ID: BVMJ GC/MS Lab File ID: 1JG2320.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U MDL 0.63 0.46 0.15 0.47 0.52 0.45 0.31 0.77 0.18 0.58 0.86 2.5 0.44 0.57 0.52 0.54 0.64 0.39 0.52 0.36 0.65 4.4 0.52 0.69 9.9 0.50 0.58 0.58 2.5 0.85 0.42 0.63 0.58 0.34 2.5 0.90 1.0 0.65 0.14 0.41 0.35 2.5 0.44 0.50 PQL 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 10 1.0 1.0 20 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 4.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 07/15/2008 Analytical Data Client: ARCADIS U.S., Inc. Client Sample ID: CP-22 (34'-36') Lab Sample ID: Client Matrix: 660-17097-3 Water Job Number: 660-17097-1 Date Sampled: Date Received: 07/19/2007 1030 07/20/2007 1410 8260B Volatile Organic Compounds by GC/MS Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260B 5030B 1.0 07/23/2007 1714 07/23/2007 1714 Analyte Hexachlorobutadiene Isopropylbenzene 2-Butanone (MEK) 4-Methyl-2-pentanone (MIBK) Methyl tert-butyl ether Methylene Chloride m-Xylene & p-Xylene Naphthalene n-Butylbenzene N-Propylbenzene o-Xylene sec-Butylbenzene Styrene tert-Butylbenzene Tetrachloroethene Toluene trans-1,2-Dichloroethene trans-1,3-Dichloropropene Trichloroethene Trichlorofluoromethane Vinyl chloride Surrogate Toluene-d8 (Surr) 4-Bromofluorobenzene Dibromofluoromethane TestAmerica Tampa Analysis Batch: 660-47317 Result (ug/L) 0.40 0.19 8.4 3.8 0.44 4.0 0.60 2.5 0.67 0.59 0.50 0.63 0.98 0.84 0.50 0.51 0.44 0.14 0.50 2.5 0.50 %Rec 102 105 89 Page 15 of 59 Instrument ID: BVMJ GC/MS Lab File ID: 1JG2320.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U U U U U U U U U U U U U U U U U U U U U MDL 0.40 0.19 8.4 3.8 0.44 4.0 0.60 2.5 0.67 0.59 0.50 0.63 0.98 0.84 0.50 0.51 0.44 0.14 0.50 2.5 0.50 PQL 1.0 1.0 10 10 1.0 5.0 2.0 5.0 1.0 1.0 1.0 1.0 2.0 1.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 Acceptance Limits 77 - 122 74 - 126 70 - 130 07/15/2008 Analytical Data Client: ARCADIS U.S., Inc. Client Sample ID: CP-22 (34'-36') Lab Sample ID: Client Matrix: 660-17097-3 Water Job Number: 660-17097-1 Date Sampled: Date Received: 07/19/2007 1030 07/20/2007 1410 8260B Volatile Organics by GC/MS Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260B 5030B 1.0 07/23/2007 1714 07/23/2007 1714 Analyte 1,4-Dioxane TestAmerica Tampa Analysis Batch: 660-47328 Result (ug/L) 87 Page 16 of 59 Instrument ID: BVMJ GC/MS Lab File ID: 1JG2320.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier MDL 0.54 PQL 1.0 07/15/2008 Analytical Data Client: ARCADIS U.S., Inc. Client Sample ID: CP-22 (48'-50') Lab Sample ID: Client Matrix: 660-17097-4 Water Job Number: 660-17097-1 Date Sampled: Date Received: 07/19/2007 1107 07/20/2007 1410 8260B Volatile Organic Compounds by GC/MS Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260B 5030B 1.0 07/23/2007 1738 07/23/2007 1738 Analyte 1,1,1,2-Tetrachloroethane 1,1,1-Trichloroethane 1,1,2,2-Tetrachloroethane 1,1,2-Trichloroethane 1,1-Dichloroethane 1,1-Dichloroethene 1,1-Dichloropropene 1,2,3-Trichlorobenzene 1,2,3-Trichloropropane 1,2,4-Trichlorobenzene 1,2,4-Trimethylbenzene 1,2-Dibromo-3-Chloropropane 1,2-Dichlorobenzene 1,2-Dichloroethane 1,2-Dichloropropane 1,3,5-Trimethylbenzene 1,3-Dichlorobenzene 1,3-Dichloropropane 1,4-Dichlorobenzene 2,2-Dichloropropane 2-Chlorotoluene 2-Hexanone 4-Chlorotoluene 4-Isopropyltoluene Acetone Benzene Bromobenzene Bromoform Bromomethane Carbon disulfide Carbon tetrachloride Chlorobenzene Chlorobromomethane Chlorodibromomethane Chloroethane Chloroform Chloromethane cis-1,2-Dichloroethene cis-1,3-Dichloropropene Dibromomethane Dichlorobromomethane Dichlorodifluoromethane Ethylbenzene Ethylene Dibromide TestAmerica Tampa Analysis Batch: 660-47317 Result (ug/L) 0.63 0.46 0.15 0.47 3.0 4.6 0.31 0.77 0.18 0.58 0.86 2.5 0.44 0.57 0.52 0.54 0.64 0.39 0.52 0.36 0.65 4.4 0.52 0.69 9.9 0.50 0.58 0.58 2.5 0.85 0.42 0.63 0.58 0.34 2.5 0.90 1.0 9.4 0.14 0.41 0.35 2.5 0.44 0.50 Page 17 of 59 Instrument ID: BVMJ GC/MS Lab File ID: 1JG2321.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U MDL 0.63 0.46 0.15 0.47 0.52 0.45 0.31 0.77 0.18 0.58 0.86 2.5 0.44 0.57 0.52 0.54 0.64 0.39 0.52 0.36 0.65 4.4 0.52 0.69 9.9 0.50 0.58 0.58 2.5 0.85 0.42 0.63 0.58 0.34 2.5 0.90 1.0 0.65 0.14 0.41 0.35 2.5 0.44 0.50 PQL 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 10 1.0 1.0 20 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 4.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 07/15/2008 Analytical Data Client: ARCADIS U.S., Inc. Client Sample ID: CP-22 (48'-50') Lab Sample ID: Client Matrix: 660-17097-4 Water Job Number: 660-17097-1 Date Sampled: Date Received: 07/19/2007 1107 07/20/2007 1410 8260B Volatile Organic Compounds by GC/MS Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260B 5030B 1.0 07/23/2007 1738 07/23/2007 1738 Analyte Hexachlorobutadiene Isopropylbenzene 2-Butanone (MEK) 4-Methyl-2-pentanone (MIBK) Methyl tert-butyl ether Methylene Chloride m-Xylene & p-Xylene Naphthalene n-Butylbenzene N-Propylbenzene o-Xylene sec-Butylbenzene Styrene tert-Butylbenzene Tetrachloroethene Toluene trans-1,2-Dichloroethene trans-1,3-Dichloropropene Trichloroethene Trichlorofluoromethane Vinyl chloride Surrogate Toluene-d8 (Surr) 4-Bromofluorobenzene Dibromofluoromethane TestAmerica Tampa Analysis Batch: 660-47317 Result (ug/L) 0.40 0.19 8.4 3.8 0.44 4.0 0.60 2.5 0.67 0.59 0.50 0.63 0.98 0.84 0.50 0.51 0.44 0.14 4.9 2.5 0.76 %Rec 103 106 89 Page 18 of 59 Instrument ID: BVMJ GC/MS Lab File ID: 1JG2321.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U U U U U U U U U U U U U U U U U U U I MDL 0.40 0.19 8.4 3.8 0.44 4.0 0.60 2.5 0.67 0.59 0.50 0.63 0.98 0.84 0.50 0.51 0.44 0.14 0.50 2.5 0.50 PQL 1.0 1.0 10 10 1.0 5.0 2.0 5.0 1.0 1.0 1.0 1.0 2.0 1.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 Acceptance Limits 77 - 122 74 - 126 70 - 130 07/15/2008 Analytical Data Client: ARCADIS U.S., Inc. Client Sample ID: CP-22 (48'-50') Lab Sample ID: Client Matrix: 660-17097-4 Water Job Number: 660-17097-1 Date Sampled: Date Received: 07/19/2007 1107 07/20/2007 1410 8260B Volatile Organics by GC/MS Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260B 5030B 1.0 07/23/2007 1738 07/23/2007 1738 Analyte 1,4-Dioxane TestAmerica Tampa Analysis Batch: 660-47328 Result (ug/L) 73 Page 19 of 59 Instrument ID: BVMJ GC/MS Lab File ID: 1JG2321.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier MDL 0.54 PQL 1.0 07/15/2008 Analytical Data Client: ARCADIS U.S., Inc. Client Sample ID: CP-22 (56'-58') Lab Sample ID: Client Matrix: 660-17097-5 Water Job Number: 660-17097-1 Date Sampled: Date Received: 07/19/2007 1241 07/20/2007 1410 8260B Volatile Organic Compounds by GC/MS Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260B 5030B 1.0 07/23/2007 1803 07/23/2007 1803 Analyte 1,1,1,2-Tetrachloroethane 1,1,1-Trichloroethane 1,1,2,2-Tetrachloroethane 1,1,2-Trichloroethane 1,1-Dichloroethane 1,1-Dichloroethene 1,1-Dichloropropene 1,2,3-Trichlorobenzene 1,2,3-Trichloropropane 1,2,4-Trichlorobenzene 1,2,4-Trimethylbenzene 1,2-Dibromo-3-Chloropropane 1,2-Dichlorobenzene 1,2-Dichloroethane 1,2-Dichloropropane 1,3,5-Trimethylbenzene 1,3-Dichlorobenzene 1,3-Dichloropropane 1,4-Dichlorobenzene 2,2-Dichloropropane 2-Chlorotoluene 2-Hexanone 4-Chlorotoluene 4-Isopropyltoluene Acetone Benzene Bromobenzene Bromoform Bromomethane Carbon disulfide Carbon tetrachloride Chlorobenzene Chlorobromomethane Chlorodibromomethane Chloroethane Chloroform Chloromethane cis-1,2-Dichloroethene cis-1,3-Dichloropropene Dibromomethane Dichlorobromomethane Dichlorodifluoromethane Ethylbenzene Ethylene Dibromide TestAmerica Tampa Analysis Batch: 660-47317 Result (ug/L) 0.63 0.46 0.15 0.47 0.52 0.45 0.31 0.77 0.18 0.58 0.86 2.5 0.44 0.57 0.52 0.54 0.64 0.39 0.52 0.36 0.65 4.4 0.52 0.69 9.9 0.50 0.58 0.58 2.5 0.85 0.42 0.63 0.58 0.34 2.5 0.90 1.0 0.65 0.14 0.41 0.35 2.5 0.44 0.50 Page 20 of 59 Instrument ID: BVMJ GC/MS Lab File ID: 1JG2322.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U MDL 0.63 0.46 0.15 0.47 0.52 0.45 0.31 0.77 0.18 0.58 0.86 2.5 0.44 0.57 0.52 0.54 0.64 0.39 0.52 0.36 0.65 4.4 0.52 0.69 9.9 0.50 0.58 0.58 2.5 0.85 0.42 0.63 0.58 0.34 2.5 0.90 1.0 0.65 0.14 0.41 0.35 2.5 0.44 0.50 PQL 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 10 1.0 1.0 20 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 4.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 07/15/2008 Analytical Data Client: ARCADIS U.S., Inc. Client Sample ID: CP-22 (56'-58') Lab Sample ID: Client Matrix: 660-17097-5 Water Job Number: 660-17097-1 Date Sampled: Date Received: 07/19/2007 1241 07/20/2007 1410 8260B Volatile Organic Compounds by GC/MS Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260B 5030B 1.0 07/23/2007 1803 07/23/2007 1803 Analyte Hexachlorobutadiene Isopropylbenzene 2-Butanone (MEK) 4-Methyl-2-pentanone (MIBK) Methyl tert-butyl ether Methylene Chloride m-Xylene & p-Xylene Naphthalene n-Butylbenzene N-Propylbenzene o-Xylene sec-Butylbenzene Styrene tert-Butylbenzene Tetrachloroethene Toluene trans-1,2-Dichloroethene trans-1,3-Dichloropropene Trichloroethene Trichlorofluoromethane Vinyl chloride Surrogate Toluene-d8 (Surr) 4-Bromofluorobenzene Dibromofluoromethane TestAmerica Tampa Analysis Batch: 660-47317 Result (ug/L) 0.40 0.19 8.4 3.8 0.44 4.0 0.60 2.5 0.67 0.59 0.50 0.63 0.98 0.84 0.50 0.51 0.44 0.14 0.50 2.5 0.50 %Rec 97 97 83 Page 21 of 59 Instrument ID: BVMJ GC/MS Lab File ID: 1JG2322.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U U U U U U U U U U U U U U U U U U U U U MDL 0.40 0.19 8.4 3.8 0.44 4.0 0.60 2.5 0.67 0.59 0.50 0.63 0.98 0.84 0.50 0.51 0.44 0.14 0.50 2.5 0.50 PQL 1.0 1.0 10 10 1.0 5.0 2.0 5.0 1.0 1.0 1.0 1.0 2.0 1.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 Acceptance Limits 77 - 122 74 - 126 70 - 130 07/15/2008 Analytical Data Client: ARCADIS U.S., Inc. Client Sample ID: CP-22 (56'-58') Lab Sample ID: Client Matrix: 660-17097-5 Water Job Number: 660-17097-1 Date Sampled: Date Received: 07/19/2007 1241 07/20/2007 1410 8260B Volatile Organics by GC/MS Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260B 5030B 1.0 07/23/2007 1803 07/23/2007 1803 Analyte 1,4-Dioxane TestAmerica Tampa Analysis Batch: 660-47328 Result (ug/L) 0.54 Page 22 of 59 Instrument ID: BVMJ GC/MS Lab File ID: 1JG2322.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U MDL 0.54 PQL 1.0 07/15/2008 Analytical Data Client: ARCADIS U.S., Inc. Client Sample ID: CP-14 (8'-10') Lab Sample ID: Client Matrix: 660-17097-6 Water Job Number: 660-17097-1 Date Sampled: Date Received: 07/19/2007 1638 07/20/2007 1410 8260B Volatile Organic Compounds by GC/MS Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260B 5030B 1.0 07/23/2007 1828 07/23/2007 1828 Analyte 1,1,1,2-Tetrachloroethane 1,1,1-Trichloroethane 1,1,2,2-Tetrachloroethane 1,1,2-Trichloroethane 1,1-Dichloroethane 1,1-Dichloroethene 1,1-Dichloropropene 1,2,3-Trichlorobenzene 1,2,3-Trichloropropane 1,2,4-Trichlorobenzene 1,2,4-Trimethylbenzene 1,2-Dibromo-3-Chloropropane 1,2-Dichlorobenzene 1,2-Dichloroethane 1,2-Dichloropropane 1,3,5-Trimethylbenzene 1,3-Dichlorobenzene 1,3-Dichloropropane 1,4-Dichlorobenzene 2,2-Dichloropropane 2-Chlorotoluene 2-Hexanone 4-Chlorotoluene 4-Isopropyltoluene Acetone Benzene Bromobenzene Bromoform Bromomethane Carbon disulfide Carbon tetrachloride Chlorobenzene Chlorobromomethane Chlorodibromomethane Chloroethane Chloroform Chloromethane cis-1,2-Dichloroethene cis-1,3-Dichloropropene Dibromomethane Dichlorobromomethane Dichlorodifluoromethane Ethylbenzene Ethylene Dibromide TestAmerica Tampa Analysis Batch: 660-47317 Result (ug/L) 0.63 0.46 0.15 0.47 0.52 0.45 0.31 0.77 0.18 0.58 0.86 2.5 0.44 0.57 0.52 0.54 0.64 0.39 0.52 0.36 0.65 4.4 0.52 0.69 9.9 0.50 0.58 0.58 2.5 0.85 0.42 0.63 0.58 0.34 2.5 0.90 1.0 0.65 0.14 0.41 0.35 2.5 0.44 0.50 Page 23 of 59 Instrument ID: BVMJ GC/MS Lab File ID: 1JG2323.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U MDL 0.63 0.46 0.15 0.47 0.52 0.45 0.31 0.77 0.18 0.58 0.86 2.5 0.44 0.57 0.52 0.54 0.64 0.39 0.52 0.36 0.65 4.4 0.52 0.69 9.9 0.50 0.58 0.58 2.5 0.85 0.42 0.63 0.58 0.34 2.5 0.90 1.0 0.65 0.14 0.41 0.35 2.5 0.44 0.50 PQL 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 10 1.0 1.0 20 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 4.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 07/15/2008 Analytical Data Client: ARCADIS U.S., Inc. Client Sample ID: CP-14 (8'-10') Lab Sample ID: Client Matrix: 660-17097-6 Water Job Number: 660-17097-1 Date Sampled: Date Received: 07/19/2007 1638 07/20/2007 1410 8260B Volatile Organic Compounds by GC/MS Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260B 5030B 1.0 07/23/2007 1828 07/23/2007 1828 Analyte Hexachlorobutadiene Isopropylbenzene 2-Butanone (MEK) 4-Methyl-2-pentanone (MIBK) Methyl tert-butyl ether Methylene Chloride m-Xylene & p-Xylene Naphthalene n-Butylbenzene N-Propylbenzene o-Xylene sec-Butylbenzene Styrene tert-Butylbenzene Tetrachloroethene Toluene trans-1,2-Dichloroethene trans-1,3-Dichloropropene Trichloroethene Trichlorofluoromethane Vinyl chloride Surrogate Toluene-d8 (Surr) 4-Bromofluorobenzene Dibromofluoromethane TestAmerica Tampa Analysis Batch: 660-47317 Result (ug/L) 0.40 0.19 8.4 3.8 0.44 4.0 0.60 2.5 0.67 0.59 0.50 0.63 0.98 0.84 0.50 0.51 0.44 0.14 0.50 2.5 0.50 %Rec 104 113 92 Page 24 of 59 Instrument ID: BVMJ GC/MS Lab File ID: 1JG2323.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U U U U U U U U U U U U U U U U U U U U U MDL 0.40 0.19 8.4 3.8 0.44 4.0 0.60 2.5 0.67 0.59 0.50 0.63 0.98 0.84 0.50 0.51 0.44 0.14 0.50 2.5 0.50 PQL 1.0 1.0 10 10 1.0 5.0 2.0 5.0 1.0 1.0 1.0 1.0 2.0 1.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 Acceptance Limits 77 - 122 74 - 126 70 - 130 07/15/2008 Analytical Data Client: ARCADIS U.S., Inc. Client Sample ID: CP-14 (8'-10') Lab Sample ID: Client Matrix: 660-17097-6 Water Job Number: 660-17097-1 Date Sampled: Date Received: 07/19/2007 1638 07/20/2007 1410 8260B Volatile Organics by GC/MS Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260B 5030B 1.0 07/23/2007 1828 07/23/2007 1828 Analyte 1,4-Dioxane TestAmerica Tampa Analysis Batch: 660-47328 Result (ug/L) 0.54 Page 25 of 59 Instrument ID: BVMJ GC/MS Lab File ID: 1JG2323.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U MDL 0.54 PQL 1.0 07/15/2008 Analytical Data Client: ARCADIS U.S., Inc. Client Sample ID: CP-14 (19'-21') Lab Sample ID: Client Matrix: 660-17097-7 Water Job Number: 660-17097-1 Date Sampled: Date Received: 07/19/2007 1655 07/20/2007 1410 8260B Volatile Organic Compounds by GC/MS Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260B 5030B 1.0 07/23/2007 1853 07/23/2007 1853 Analyte 1,1,1,2-Tetrachloroethane 1,1,1-Trichloroethane 1,1,2,2-Tetrachloroethane 1,1,2-Trichloroethane 1,1-Dichloroethane 1,1-Dichloroethene 1,1-Dichloropropene 1,2,3-Trichlorobenzene 1,2,3-Trichloropropane 1,2,4-Trichlorobenzene 1,2,4-Trimethylbenzene 1,2-Dibromo-3-Chloropropane 1,2-Dichlorobenzene 1,2-Dichloroethane 1,2-Dichloropropane 1,3,5-Trimethylbenzene 1,3-Dichlorobenzene 1,3-Dichloropropane 1,4-Dichlorobenzene 2,2-Dichloropropane 2-Chlorotoluene 2-Hexanone 4-Chlorotoluene 4-Isopropyltoluene Acetone Benzene Bromobenzene Bromoform Bromomethane Carbon disulfide Carbon tetrachloride Chlorobenzene Chlorobromomethane Chlorodibromomethane Chloroethane Chloroform Chloromethane cis-1,2-Dichloroethene cis-1,3-Dichloropropene Dibromomethane Dichlorobromomethane Dichlorodifluoromethane Ethylbenzene Ethylene Dibromide TestAmerica Tampa Analysis Batch: 660-47317 Result (ug/L) 0.63 0.46 0.15 0.47 0.52 0.45 0.31 0.77 0.18 0.58 0.86 2.5 0.44 0.57 0.52 0.54 0.64 0.39 0.52 0.36 0.65 4.4 0.52 0.69 9.9 0.50 0.58 0.58 2.5 0.85 0.42 0.63 0.58 0.34 2.5 0.90 1.0 0.65 0.14 0.41 0.35 2.5 0.44 0.50 Page 26 of 59 Instrument ID: BVMJ GC/MS Lab File ID: 1JG2324.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U MDL 0.63 0.46 0.15 0.47 0.52 0.45 0.31 0.77 0.18 0.58 0.86 2.5 0.44 0.57 0.52 0.54 0.64 0.39 0.52 0.36 0.65 4.4 0.52 0.69 9.9 0.50 0.58 0.58 2.5 0.85 0.42 0.63 0.58 0.34 2.5 0.90 1.0 0.65 0.14 0.41 0.35 2.5 0.44 0.50 PQL 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 10 1.0 1.0 20 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 4.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 07/15/2008 Analytical Data Client: ARCADIS U.S., Inc. Client Sample ID: CP-14 (19'-21') Lab Sample ID: Client Matrix: 660-17097-7 Water Job Number: 660-17097-1 Date Sampled: Date Received: 07/19/2007 1655 07/20/2007 1410 8260B Volatile Organic Compounds by GC/MS Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260B 5030B 1.0 07/23/2007 1853 07/23/2007 1853 Analyte Hexachlorobutadiene Isopropylbenzene 2-Butanone (MEK) 4-Methyl-2-pentanone (MIBK) Methyl tert-butyl ether Methylene Chloride m-Xylene & p-Xylene Naphthalene n-Butylbenzene N-Propylbenzene o-Xylene sec-Butylbenzene Styrene tert-Butylbenzene Tetrachloroethene Toluene trans-1,2-Dichloroethene trans-1,3-Dichloropropene Trichloroethene Trichlorofluoromethane Vinyl chloride Surrogate Toluene-d8 (Surr) 4-Bromofluorobenzene Dibromofluoromethane TestAmerica Tampa Analysis Batch: 660-47317 Result (ug/L) 0.40 0.19 8.4 3.8 0.44 4.0 0.60 2.5 0.67 0.59 0.50 0.63 0.98 0.84 0.50 0.51 0.44 0.14 0.60 2.5 0.50 %Rec 103 105 88 Page 27 of 59 Instrument ID: BVMJ GC/MS Lab File ID: 1JG2324.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U U U U U U U U U U U U U U U U U U I U U MDL 0.40 0.19 8.4 3.8 0.44 4.0 0.60 2.5 0.67 0.59 0.50 0.63 0.98 0.84 0.50 0.51 0.44 0.14 0.50 2.5 0.50 PQL 1.0 1.0 10 10 1.0 5.0 2.0 5.0 1.0 1.0 1.0 1.0 2.0 1.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 Acceptance Limits 77 - 122 74 - 126 70 - 130 07/15/2008 Analytical Data Client: ARCADIS U.S., Inc. Client Sample ID: CP-14 (19'-21') Lab Sample ID: Client Matrix: 660-17097-7 Water Job Number: 660-17097-1 Date Sampled: Date Received: 07/19/2007 1655 07/20/2007 1410 8260B Volatile Organics by GC/MS Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260B 5030B 1.0 07/23/2007 1853 07/23/2007 1853 Analyte 1,4-Dioxane TestAmerica Tampa Analysis Batch: 660-47328 Result (ug/L) 0.54 Page 28 of 59 Instrument ID: BVMJ GC/MS Lab File ID: 1JG2324.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U MDL 0.54 PQL 1.0 07/15/2008 Analytical Data Client: ARCADIS U.S., Inc. Client Sample ID: CP-14 (24'-26') Lab Sample ID: Client Matrix: 660-17097-8 Water Job Number: 660-17097-1 Date Sampled: Date Received: 07/19/2007 1708 07/20/2007 1410 8260B Volatile Organic Compounds by GC/MS Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260B 5030B 1.0 07/23/2007 1918 07/23/2007 1918 Analyte 1,1,1,2-Tetrachloroethane 1,1,1-Trichloroethane 1,1,2,2-Tetrachloroethane 1,1,2-Trichloroethane 1,1-Dichloroethane 1,1-Dichloroethene 1,1-Dichloropropene 1,2,3-Trichlorobenzene 1,2,3-Trichloropropane 1,2,4-Trichlorobenzene 1,2,4-Trimethylbenzene 1,2-Dibromo-3-Chloropropane 1,2-Dichlorobenzene 1,2-Dichloroethane 1,2-Dichloropropane 1,3,5-Trimethylbenzene 1,3-Dichlorobenzene 1,3-Dichloropropane 1,4-Dichlorobenzene 2,2-Dichloropropane 2-Chlorotoluene 2-Hexanone 4-Chlorotoluene 4-Isopropyltoluene Acetone Benzene Bromobenzene Bromoform Bromomethane Carbon disulfide Carbon tetrachloride Chlorobenzene Chlorobromomethane Chlorodibromomethane Chloroethane Chloroform Chloromethane cis-1,2-Dichloroethene cis-1,3-Dichloropropene Dibromomethane Dichlorobromomethane Dichlorodifluoromethane Ethylbenzene Ethylene Dibromide TestAmerica Tampa Analysis Batch: 660-47317 Result (ug/L) 0.63 0.46 0.15 0.47 0.52 0.45 0.31 0.77 0.18 0.58 0.86 2.5 0.44 0.57 0.52 0.54 0.64 0.39 0.52 0.36 0.65 4.4 0.52 0.69 9.9 0.50 0.58 0.58 2.5 0.85 0.42 0.63 0.58 0.34 2.5 0.90 1.0 0.65 0.14 0.41 0.35 2.5 0.44 0.50 Page 29 of 59 Instrument ID: BVMJ GC/MS Lab File ID: 1JG2325.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U MDL 0.63 0.46 0.15 0.47 0.52 0.45 0.31 0.77 0.18 0.58 0.86 2.5 0.44 0.57 0.52 0.54 0.64 0.39 0.52 0.36 0.65 4.4 0.52 0.69 9.9 0.50 0.58 0.58 2.5 0.85 0.42 0.63 0.58 0.34 2.5 0.90 1.0 0.65 0.14 0.41 0.35 2.5 0.44 0.50 PQL 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 10 1.0 1.0 20 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 4.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 07/15/2008 Analytical Data Client: ARCADIS U.S., Inc. Client Sample ID: CP-14 (24'-26') Lab Sample ID: Client Matrix: 660-17097-8 Water Job Number: 660-17097-1 Date Sampled: Date Received: 07/19/2007 1708 07/20/2007 1410 8260B Volatile Organic Compounds by GC/MS Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260B 5030B 1.0 07/23/2007 1918 07/23/2007 1918 Analyte Hexachlorobutadiene Isopropylbenzene 2-Butanone (MEK) 4-Methyl-2-pentanone (MIBK) Methyl tert-butyl ether Methylene Chloride m-Xylene & p-Xylene Naphthalene n-Butylbenzene N-Propylbenzene o-Xylene sec-Butylbenzene Styrene tert-Butylbenzene Tetrachloroethene Toluene trans-1,2-Dichloroethene trans-1,3-Dichloropropene Trichloroethene Trichlorofluoromethane Vinyl chloride Surrogate Toluene-d8 (Surr) 4-Bromofluorobenzene Dibromofluoromethane TestAmerica Tampa Analysis Batch: 660-47317 Result (ug/L) 0.40 0.19 8.4 3.8 0.44 4.0 0.60 2.5 0.67 0.59 0.50 0.63 0.98 0.84 0.50 0.51 0.44 0.14 6.2 2.5 0.50 %Rec 104 103 84 Page 30 of 59 Instrument ID: BVMJ GC/MS Lab File ID: 1JG2325.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U U U U U U U U U U U U U U U U U U U U MDL 0.40 0.19 8.4 3.8 0.44 4.0 0.60 2.5 0.67 0.59 0.50 0.63 0.98 0.84 0.50 0.51 0.44 0.14 0.50 2.5 0.50 PQL 1.0 1.0 10 10 1.0 5.0 2.0 5.0 1.0 1.0 1.0 1.0 2.0 1.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 Acceptance Limits 77 - 122 74 - 126 70 - 130 07/15/2008 Analytical Data Client: ARCADIS U.S., Inc. Client Sample ID: CP-14 (24'-26') Lab Sample ID: Client Matrix: 660-17097-8 Water Job Number: 660-17097-1 Date Sampled: Date Received: 07/19/2007 1708 07/20/2007 1410 8260B Volatile Organics by GC/MS Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260B 5030B 1.0 07/23/2007 1918 07/23/2007 1918 Analyte 1,4-Dioxane TestAmerica Tampa Analysis Batch: 660-47328 Result (ug/L) 0.54 Page 31 of 59 Instrument ID: BVMJ GC/MS Lab File ID: 1JG2325.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U MDL 0.54 PQL 1.0 07/15/2008 Analytical Data Client: ARCADIS U.S., Inc. Client Sample ID: CP-14 (29'-31') Lab Sample ID: Client Matrix: 660-17097-9 Water Job Number: 660-17097-1 Date Sampled: Date Received: 07/19/2007 1723 07/20/2007 1410 8260B Volatile Organic Compounds by GC/MS Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260B 5030B 1.0 07/23/2007 1943 07/23/2007 1943 Analyte 1,1,1,2-Tetrachloroethane 1,1,1-Trichloroethane 1,1,2,2-Tetrachloroethane 1,1,2-Trichloroethane 1,1-Dichloroethane 1,1-Dichloroethene 1,1-Dichloropropene 1,2,3-Trichlorobenzene 1,2,3-Trichloropropane 1,2,4-Trichlorobenzene 1,2,4-Trimethylbenzene 1,2-Dibromo-3-Chloropropane 1,2-Dichlorobenzene 1,2-Dichloroethane 1,2-Dichloropropane 1,3,5-Trimethylbenzene 1,3-Dichlorobenzene 1,3-Dichloropropane 1,4-Dichlorobenzene 2,2-Dichloropropane 2-Chlorotoluene 2-Hexanone 4-Chlorotoluene 4-Isopropyltoluene Acetone Benzene Bromobenzene Bromoform Bromomethane Carbon disulfide Carbon tetrachloride Chlorobenzene Chlorobromomethane Chlorodibromomethane Chloroethane Chloroform Chloromethane cis-1,2-Dichloroethene cis-1,3-Dichloropropene Dibromomethane Dichlorobromomethane Dichlorodifluoromethane Ethylbenzene Ethylene Dibromide TestAmerica Tampa Analysis Batch: 660-47317 Result (ug/L) 0.63 0.46 0.15 0.47 0.52 0.45 0.31 0.77 0.18 0.58 0.86 2.5 0.44 0.57 0.52 0.54 0.64 0.39 0.52 0.36 0.65 4.4 0.52 0.69 9.9 0.50 0.58 0.58 2.5 0.85 0.42 0.63 0.58 0.34 2.5 0.90 1.0 4.8 0.14 0.41 0.35 2.5 0.49 0.50 Page 32 of 59 Instrument ID: BVMJ GC/MS Lab File ID: 1JG2326.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U I U MDL 0.63 0.46 0.15 0.47 0.52 0.45 0.31 0.77 0.18 0.58 0.86 2.5 0.44 0.57 0.52 0.54 0.64 0.39 0.52 0.36 0.65 4.4 0.52 0.69 9.9 0.50 0.58 0.58 2.5 0.85 0.42 0.63 0.58 0.34 2.5 0.90 1.0 0.65 0.14 0.41 0.35 2.5 0.44 0.50 PQL 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 10 1.0 1.0 20 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 4.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 07/15/2008 Analytical Data Client: ARCADIS U.S., Inc. Client Sample ID: CP-14 (29'-31') Lab Sample ID: Client Matrix: 660-17097-9 Water Job Number: 660-17097-1 Date Sampled: Date Received: 07/19/2007 1723 07/20/2007 1410 8260B Volatile Organic Compounds by GC/MS Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260B 5030B 1.0 07/23/2007 1943 07/23/2007 1943 Analyte Hexachlorobutadiene Isopropylbenzene 2-Butanone (MEK) 4-Methyl-2-pentanone (MIBK) Methyl tert-butyl ether Methylene Chloride m-Xylene & p-Xylene Naphthalene n-Butylbenzene N-Propylbenzene o-Xylene sec-Butylbenzene Styrene tert-Butylbenzene Tetrachloroethene Toluene trans-1,2-Dichloroethene trans-1,3-Dichloropropene Trichloroethene Trichlorofluoromethane Vinyl chloride Surrogate Toluene-d8 (Surr) 4-Bromofluorobenzene Dibromofluoromethane TestAmerica Tampa Analysis Batch: 660-47317 Result (ug/L) 0.40 0.19 8.4 3.8 0.44 4.0 0.60 2.5 0.67 0.59 0.50 0.63 0.98 0.84 0.50 0.51 0.44 0.14 98 2.5 0.50 %Rec 108 110 93 Page 33 of 59 Instrument ID: BVMJ GC/MS Lab File ID: 1JG2326.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U U U U U U U U U U U U U U U U U U U U MDL 0.40 0.19 8.4 3.8 0.44 4.0 0.60 2.5 0.67 0.59 0.50 0.63 0.98 0.84 0.50 0.51 0.44 0.14 0.50 2.5 0.50 PQL 1.0 1.0 10 10 1.0 5.0 2.0 5.0 1.0 1.0 1.0 1.0 2.0 1.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 Acceptance Limits 77 - 122 74 - 126 70 - 130 07/15/2008 Analytical Data Client: ARCADIS U.S., Inc. Client Sample ID: CP-14 (29'-31') Lab Sample ID: Client Matrix: 660-17097-9 Water Job Number: 660-17097-1 Date Sampled: Date Received: 07/19/2007 1723 07/20/2007 1410 8260B Volatile Organics by GC/MS Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260B 5030B 1.0 07/23/2007 1943 07/23/2007 1943 Analyte 1,4-Dioxane TestAmerica Tampa Analysis Batch: 660-47328 Result (ug/L) 0.54 Page 34 of 59 Instrument ID: BVMJ GC/MS Lab File ID: 1JG2326.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U MDL 0.54 PQL 1.0 07/15/2008 Analytical Data Client: ARCADIS U.S., Inc. Client Sample ID: CP-14 (38'-40') Lab Sample ID: Client Matrix: 660-17097-10 Water Job Number: 660-17097-1 Date Sampled: Date Received: 07/20/2007 0815 07/20/2007 1410 8260B Volatile Organic Compounds by GC/MS Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260B 5030B 50 07/25/2007 1351 07/25/2007 1351 Analyte 1,1,1,2-Tetrachloroethane 1,1,1-Trichloroethane 1,1,2,2-Tetrachloroethane 1,1,2-Trichloroethane 1,1-Dichloroethane 1,1-Dichloroethene 1,1-Dichloropropene 1,2,3-Trichlorobenzene 1,2,3-Trichloropropane 1,2,4-Trichlorobenzene 1,2,4-Trimethylbenzene 1,2-Dibromo-3-Chloropropane 1,2-Dichlorobenzene 1,2-Dichloroethane 1,2-Dichloropropane 1,3,5-Trimethylbenzene 1,3-Dichlorobenzene 1,3-Dichloropropane 1,4-Dichlorobenzene 2,2-Dichloropropane 2-Chlorotoluene 2-Hexanone 4-Chlorotoluene 4-Isopropyltoluene Acetone Benzene Bromobenzene Bromoform Bromomethane Carbon disulfide Carbon tetrachloride Chlorobenzene Chlorobromomethane Chlorodibromomethane Chloroethane Chloroform Chloromethane cis-1,2-Dichloroethene cis-1,3-Dichloropropene Dibromomethane Dichlorobromomethane Dichlorodifluoromethane Ethylbenzene Ethylene Dibromide TestAmerica Tampa Analysis Batch: 660-47471 Result (ug/L) 32 23 7.5 24 26 23 16 39 9.0 29 43 130 22 29 26 27 32 20 26 18 33 220 26 35 500 25 29 29 130 43 21 32 29 17 130 45 50 160 7.0 21 18 130 22 25 Page 35 of 59 Instrument ID: BVMJ GC/MS Lab File ID: 1JG2512.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U MDL 32 23 7.5 24 26 23 16 39 9.0 29 43 130 22 29 26 27 32 20 26 18 33 220 26 35 500 25 29 29 130 43 21 32 29 17 130 45 50 33 7.0 21 18 130 22 25 PQL 50 50 50 50 50 50 50 50 50 50 50 250 50 50 50 50 50 50 50 50 50 500 50 50 1000 50 50 50 250 50 50 50 50 50 250 50 200 50 50 50 50 250 50 50 07/15/2008 Analytical Data Client: ARCADIS U.S., Inc. Client Sample ID: CP-14 (38'-40') Lab Sample ID: Client Matrix: 660-17097-10 Water Job Number: 660-17097-1 Date Sampled: Date Received: 07/20/2007 0815 07/20/2007 1410 8260B Volatile Organic Compounds by GC/MS Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260B 5030B 50 07/25/2007 1351 07/25/2007 1351 Analyte Hexachlorobutadiene Isopropylbenzene 2-Butanone (MEK) 4-Methyl-2-pentanone (MIBK) Methyl tert-butyl ether Methylene Chloride m-Xylene & p-Xylene Naphthalene n-Butylbenzene N-Propylbenzene o-Xylene sec-Butylbenzene Styrene tert-Butylbenzene Tetrachloroethene Toluene trans-1,2-Dichloroethene trans-1,3-Dichloropropene Trichloroethene Trichlorofluoromethane Vinyl chloride Surrogate Toluene-d8 (Surr) 4-Bromofluorobenzene Dibromofluoromethane TestAmerica Tampa Analysis Batch: 660-47471 Result (ug/L) 20 9.5 420 190 22 200 30 130 34 30 25 32 49 42 25 26 22 7.0 5500 130 25 %Rec 109 115 92 Page 36 of 59 Instrument ID: BVMJ GC/MS Lab File ID: 1JG2512.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U U U U U U U U U U U U U U U U U U U U MDL 20 9.5 420 190 22 200 30 130 34 30 25 32 49 42 25 26 22 7.0 25 130 25 PQL 50 50 500 500 50 250 100 250 50 50 50 50 100 50 50 50 50 50 50 250 50 Acceptance Limits 77 - 122 74 - 126 70 - 130 07/15/2008 Analytical Data Client: ARCADIS U.S., Inc. Client Sample ID: CP-14 (38'-40') Lab Sample ID: Client Matrix: 660-17097-10 Water Job Number: 660-17097-1 Date Sampled: Date Received: 07/20/2007 0815 07/20/2007 1410 8260B Volatile Organics by GC/MS Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260B 5030B 1.0 07/23/2007 2007 07/23/2007 2007 Analyte 1,4-Dioxane TestAmerica Tampa Analysis Batch: 660-47328 Result (ug/L) 10 Page 37 of 59 Instrument ID: BVMJ GC/MS Lab File ID: 1JG2327.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier MDL 0.54 PQL 1.0 07/15/2008 Analytical Data Client: ARCADIS U.S., Inc. Client Sample ID: CP-14 (47'-49') Lab Sample ID: Client Matrix: 660-17097-11 Water Job Number: 660-17097-1 Date Sampled: Date Received: 07/20/2007 0903 07/20/2007 1410 8260B Volatile Organic Compounds by GC/MS Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260B 5030B 50 07/24/2007 1853 07/24/2007 1853 Analyte 1,1,1,2-Tetrachloroethane 1,1,1-Trichloroethane 1,1,2,2-Tetrachloroethane 1,1,2-Trichloroethane 1,1-Dichloroethane 1,1-Dichloroethene 1,1-Dichloropropene 1,2,3-Trichlorobenzene 1,2,3-Trichloropropane 1,2,4-Trichlorobenzene 1,2,4-Trimethylbenzene 1,2-Dibromo-3-Chloropropane 1,2-Dichlorobenzene 1,2-Dichloroethane 1,2-Dichloropropane 1,3,5-Trimethylbenzene 1,3-Dichlorobenzene 1,3-Dichloropropane 1,4-Dichlorobenzene 2,2-Dichloropropane 2-Chlorotoluene 2-Hexanone 4-Chlorotoluene 4-Isopropyltoluene Acetone Benzene Bromobenzene Bromoform Bromomethane Carbon disulfide Carbon tetrachloride Chlorobenzene Chlorobromomethane Chlorodibromomethane Chloroethane Chloroform Chloromethane cis-1,2-Dichloroethene cis-1,3-Dichloropropene Dibromomethane Dichlorobromomethane Dichlorodifluoromethane Ethylbenzene Ethylene Dibromide TestAmerica Tampa Analysis Batch: 660-47471 Result (ug/L) 32 23 7.5 24 26 23 16 39 9.0 29 43 130 22 29 26 27 32 20 26 18 33 220 26 35 500 25 29 29 130 43 21 32 29 17 130 45 50 68 7.0 21 18 130 22 25 Page 38 of 59 Instrument ID: BVMJ GC/MS Lab File ID: 1JG2418.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U MDL 32 23 7.5 24 26 23 16 39 9.0 29 43 130 22 29 26 27 32 20 26 18 33 220 26 35 500 25 29 29 130 43 21 32 29 17 130 45 50 33 7.0 21 18 130 22 25 PQL 50 50 50 50 50 50 50 50 50 50 50 250 50 50 50 50 50 50 50 50 50 500 50 50 1000 50 50 50 250 50 50 50 50 50 250 50 200 50 50 50 50 250 50 50 07/15/2008 Analytical Data Client: ARCADIS U.S., Inc. Client Sample ID: CP-14 (47'-49') Lab Sample ID: Client Matrix: 660-17097-11 Water Job Number: 660-17097-1 Date Sampled: Date Received: 07/20/2007 0903 07/20/2007 1410 8260B Volatile Organic Compounds by GC/MS Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260B 5030B 50 07/24/2007 1853 07/24/2007 1853 Analyte Hexachlorobutadiene Isopropylbenzene 2-Butanone (MEK) 4-Methyl-2-pentanone (MIBK) Methyl tert-butyl ether Methylene Chloride m-Xylene & p-Xylene Naphthalene n-Butylbenzene N-Propylbenzene o-Xylene sec-Butylbenzene Styrene tert-Butylbenzene Tetrachloroethene Toluene trans-1,2-Dichloroethene trans-1,3-Dichloropropene Trichloroethene Trichlorofluoromethane Vinyl chloride Surrogate Toluene-d8 (Surr) 4-Bromofluorobenzene Dibromofluoromethane TestAmerica Tampa Analysis Batch: 660-47471 Result (ug/L) 20 9.5 420 190 22 200 30 130 34 30 25 32 49 42 25 26 22 7.0 3400 130 25 %Rec 114 115 97 Page 39 of 59 Instrument ID: BVMJ GC/MS Lab File ID: 1JG2418.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U U U U U U U U U U U U U U U U U U U U MDL 20 9.5 420 190 22 200 30 130 34 30 25 32 49 42 25 26 22 7.0 25 130 25 PQL 50 50 500 500 50 250 100 250 50 50 50 50 100 50 50 50 50 50 50 250 50 Acceptance Limits 77 - 122 74 - 126 70 - 130 07/15/2008 Analytical Data Client: ARCADIS U.S., Inc. Client Sample ID: CP-14 (47'-49') Lab Sample ID: Client Matrix: 660-17097-11 Water Job Number: 660-17097-1 Date Sampled: Date Received: 07/20/2007 0903 07/20/2007 1410 8260B Volatile Organics by GC/MS Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260B 5030B 10 07/24/2007 1918 07/24/2007 1918 Analyte 1,4-Dioxane TestAmerica Tampa Analysis Batch: 660-47480 Result (ug/L) 120 Page 40 of 59 Instrument ID: BVMJ GC/MS Lab File ID: 1JG2419.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier MDL 5.4 PQL 10 07/15/2008 Analytical Data Client: ARCADIS U.S., Inc. Client Sample ID: Trip Blank Lab Sample ID: Client Matrix: 660-17097-12 Water Job Number: 660-17097-1 Date Sampled: Date Received: 07/19/2007 0000 07/20/2007 1410 8260B Volatile Organic Compounds by GC/MS Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260B 5030B 1.0 07/23/2007 2057 07/23/2007 2057 Analyte 1,1,1,2-Tetrachloroethane 1,1,1-Trichloroethane 1,1,2,2-Tetrachloroethane 1,1,2-Trichloroethane 1,1-Dichloroethane 1,1-Dichloroethene 1,1-Dichloropropene 1,2,3-Trichlorobenzene 1,2,3-Trichloropropane 1,2,4-Trichlorobenzene 1,2,4-Trimethylbenzene 1,2-Dibromo-3-Chloropropane 1,2-Dichlorobenzene 1,2-Dichloroethane 1,2-Dichloropropane 1,3,5-Trimethylbenzene 1,3-Dichlorobenzene 1,3-Dichloropropane 1,4-Dichlorobenzene 2,2-Dichloropropane 2-Chlorotoluene 2-Hexanone 4-Chlorotoluene 4-Isopropyltoluene Acetone Benzene Bromobenzene Bromoform Bromomethane Carbon disulfide Carbon tetrachloride Chlorobenzene Chlorobromomethane Chlorodibromomethane Chloroethane Chloroform Chloromethane cis-1,2-Dichloroethene cis-1,3-Dichloropropene Dibromomethane Dichlorobromomethane Dichlorodifluoromethane Ethylbenzene Ethylene Dibromide TestAmerica Tampa Analysis Batch: 660-47317 Result (ug/L) 0.63 0.46 0.15 0.47 0.52 0.45 0.31 0.77 0.18 0.58 0.86 2.5 0.44 0.57 0.52 0.54 0.64 0.39 0.52 0.36 0.65 4.4 0.52 0.69 9.9 0.50 0.58 0.58 2.5 0.85 0.42 0.63 0.58 0.34 2.5 0.90 1.0 0.65 0.14 0.41 0.35 2.5 0.44 0.50 Page 41 of 59 Instrument ID: BVMJ GC/MS Lab File ID: 1JG2329.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U MDL 0.63 0.46 0.15 0.47 0.52 0.45 0.31 0.77 0.18 0.58 0.86 2.5 0.44 0.57 0.52 0.54 0.64 0.39 0.52 0.36 0.65 4.4 0.52 0.69 9.9 0.50 0.58 0.58 2.5 0.85 0.42 0.63 0.58 0.34 2.5 0.90 1.0 0.65 0.14 0.41 0.35 2.5 0.44 0.50 PQL 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 10 1.0 1.0 20 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 4.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 07/15/2008 Analytical Data Client: ARCADIS U.S., Inc. Client Sample ID: Trip Blank Lab Sample ID: Client Matrix: 660-17097-12 Water Job Number: 660-17097-1 Date Sampled: Date Received: 07/19/2007 0000 07/20/2007 1410 8260B Volatile Organic Compounds by GC/MS Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260B 5030B 1.0 07/23/2007 2057 07/23/2007 2057 Analyte Hexachlorobutadiene Isopropylbenzene 2-Butanone (MEK) 4-Methyl-2-pentanone (MIBK) Methyl tert-butyl ether Methylene Chloride m-Xylene & p-Xylene Naphthalene n-Butylbenzene N-Propylbenzene o-Xylene sec-Butylbenzene Styrene tert-Butylbenzene Tetrachloroethene Toluene trans-1,2-Dichloroethene trans-1,3-Dichloropropene Trichloroethene Trichlorofluoromethane Vinyl chloride Surrogate Toluene-d8 (Surr) 4-Bromofluorobenzene Dibromofluoromethane TestAmerica Tampa Analysis Batch: 660-47317 Result (ug/L) 0.40 0.19 8.4 3.8 0.44 4.0 0.60 2.5 0.67 0.59 0.50 0.63 0.98 0.84 0.50 0.51 0.44 0.14 0.50 2.5 0.50 %Rec 108 112 93 Page 42 of 59 Instrument ID: BVMJ GC/MS Lab File ID: 1JG2329.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U U U U U U U U U U U U U U U U U U U U U MDL 0.40 0.19 8.4 3.8 0.44 4.0 0.60 2.5 0.67 0.59 0.50 0.63 0.98 0.84 0.50 0.51 0.44 0.14 0.50 2.5 0.50 PQL 1.0 1.0 10 10 1.0 5.0 2.0 5.0 1.0 1.0 1.0 1.0 2.0 1.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 Acceptance Limits 77 - 122 74 - 126 70 - 130 07/15/2008 Analytical Data Client: ARCADIS U.S., Inc. Client Sample ID: Trip Blank Lab Sample ID: Client Matrix: 660-17097-12 Water Job Number: 660-17097-1 Date Sampled: Date Received: 07/19/2007 0000 07/20/2007 1410 8260B Volatile Organics by GC/MS Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260B 5030B 1.0 07/23/2007 2057 07/23/2007 2057 Analyte 1,4-Dioxane TestAmerica Tampa Analysis Batch: 660-47328 Result (ug/L) 0.54 Page 43 of 59 Instrument ID: BVMJ GC/MS Lab File ID: 1JG2329.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U MDL 0.54 PQL 1.0 07/15/2008 DATA REPORTING QUALIFIERS Client: ARCADIS U.S., Inc. Lab Section Job Number: 660-17097-1 Qualifier Description U Indicates that the compound was analyzed for but not detected. I The reported value is between the laboratory method detection limit and the laboratory practical quantitation limit. GC/MS VOA TestAmerica Tampa Page 44 of 59 07/15/2008 QUALITY CONTROL RESULTS TestAmerica Tampa Page 45 of 59 07/15/2008 Quality Control Results Client: ARCADIS U.S., Inc. Job Number: 660-17097-1 Surrogate Recovery Report 8260B Volatile Organic Compounds by GC/MS Client Matrix: Water TOL %Rec BFB %Rec DBFM %Rec CP-22 (9'-11') 115 118 97 CP-22 (20'-22') 104 107 89 660-17097-3 CP-22 (34'-36') 102 105 89 660-17097-4 CP-22 (48'-50') 103 106 89 660-17097-5 CP-22 (56'-58') 97 97 83 660-17097-6 CP-14 (8'-10') 104 113 92 660-17097-7 CP-14 (19'-21') 103 105 88 660-17097-8 CP-14 (24'-26') 104 103 84 660-17097-9 CP-14 (29'-31') 108 110 93 660-17097-10 CP-14 (38'-40') 109 115 92 660-17097-11 CP-14 (47'-49') 114 115 97 660-17097-12 Trip Blank 108 112 93 MB 660-47317/7 103 111 88 MB 660-47471/3 97 104 83 LCS 660-47317/1 99 108 86 LCS 660-47471/1 97 101 83 LCSD 660-47317/2 93 105 85 LCSD 660-47471/2 99 101 88 Lab Sample ID Client Sample ID 660-17097-1 660-17097-2 660-17097-1 MS CP-22 (9'-11') MS 99 103 85 660-17097-1 MSD CP-22 (9'-11') MSD 96 97 84 Surrogate TOL = Toluene-d8 (Surr) BFB = 4-Bromofluorobenzene DBFM = Dibromofluoromethane Acceptance Limits 77-122 74-126 70-130 TestAmerica Tampa Page 46 of 59 07/15/2008 Quality Control Results Client: ARCADIS U.S., Inc. Job Number: 660-17097-1 Method Blank - Batch: 660-47317 Lab Sample ID: Client Matrix: Dilution: Date Analyzed: Date Prepared: MB 660-47317/7 Water 1.0 07/23/2007 1534 07/23/2007 1534 Method: 8260B Preparation: 5030B Analysis Batch: 660-47317 Prep Batch: N/A Units: ug/L Instrument ID: BVMJ GC/MS Lab File ID: 1JG2316.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Analyte Result Qual MDL PQL 1,1,1,2-Tetrachloroethane 1,1,1-Trichloroethane 1,1,2,2-Tetrachloroethane 1,1,2-Trichloroethane 1,1-Dichloroethane 1,1-Dichloroethene 1,1-Dichloropropene 1,2,3-Trichlorobenzene 1,2,3-Trichloropropane 1,2,4-Trichlorobenzene 1,2,4-Trimethylbenzene 1,2-Dibromo-3-Chloropropane 1,2-Dichlorobenzene 1,2-Dichloroethane 1,2-Dichloropropane 1,3,5-Trimethylbenzene 1,3-Dichlorobenzene 1,3-Dichloropropane 1,4-Dichlorobenzene 2,2-Dichloropropane 2-Chlorotoluene 2-Hexanone 4-Chlorotoluene 4-Isopropyltoluene Acetone Benzene Bromobenzene Bromoform Bromomethane Carbon disulfide Carbon tetrachloride Chlorobenzene Chlorobromomethane Chlorodibromomethane Chloroethane Chloroform Chloromethane cis-1,2-Dichloroethene cis-1,3-Dichloropropene Dibromomethane Dichlorobromomethane 0.63 0.46 0.15 0.47 0.52 0.45 0.31 0.77 0.18 0.58 0.86 2.5 0.44 0.57 0.52 0.54 0.64 0.39 0.52 0.36 0.65 4.4 0.52 0.69 9.9 0.50 0.58 0.58 2.5 0.85 0.42 0.63 0.58 0.34 2.5 0.90 1.0 0.65 0.14 0.41 0.35 U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U 0.63 0.46 0.15 0.47 0.52 0.45 0.31 0.77 0.18 0.58 0.86 2.5 0.44 0.57 0.52 0.54 0.64 0.39 0.52 0.36 0.65 4.4 0.52 0.69 9.9 0.50 0.58 0.58 2.5 0.85 0.42 0.63 0.58 0.34 2.5 0.90 1.0 0.65 0.14 0.41 0.35 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 10 1.0 1.0 20 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 4.0 1.0 1.0 1.0 1.0 Calculations are performed before rounding to avoid round-off errors in calculated results. TestAmerica Tampa Page 47 of 59 07/15/2008 Quality Control Results Client: ARCADIS U.S., Inc. Job Number: 660-17097-1 Method Blank - Batch: 660-47317 Lab Sample ID: Client Matrix: Dilution: Date Analyzed: Date Prepared: MB 660-47317/7 Water 1.0 07/23/2007 1534 07/23/2007 1534 Method: 8260B Preparation: 5030B Analysis Batch: 660-47317 Prep Batch: N/A Units: ug/L Instrument ID: BVMJ GC/MS Lab File ID: 1JG2316.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Analyte Result Qual MDL PQL Dichlorodifluoromethane Ethylbenzene Ethylene Dibromide Hexachlorobutadiene Isopropylbenzene 2-Butanone (MEK) 4-Methyl-2-pentanone (MIBK) Methyl tert-butyl ether Methylene Chloride m-Xylene & p-Xylene Naphthalene n-Butylbenzene N-Propylbenzene o-Xylene sec-Butylbenzene Styrene tert-Butylbenzene Tetrachloroethene Toluene trans-1,2-Dichloroethene trans-1,3-Dichloropropene Trichloroethene Trichlorofluoromethane Vinyl chloride 2.5 0.44 0.50 0.40 0.19 8.4 3.8 0.44 4.0 0.60 2.5 0.67 0.59 0.50 0.63 0.98 0.84 0.50 0.51 0.44 0.14 0.50 2.5 0.50 U U U U U U U U U U U U U U U U U U U U U U U U 2.5 0.44 0.50 0.40 0.19 8.4 3.8 0.44 4.0 0.60 2.5 0.67 0.59 0.50 0.63 0.98 0.84 0.50 0.51 0.44 0.14 0.50 2.5 0.50 5.0 1.0 1.0 1.0 1.0 10 10 1.0 5.0 2.0 5.0 1.0 1.0 1.0 1.0 2.0 1.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 Surrogate Toluene-d8 (Surr) 4-Bromofluorobenzene Dibromofluoromethane % Rec Acceptance Limits 103 111 88 77 - 122 74 - 126 70 - 130 Calculations are performed before rounding to avoid round-off errors in calculated results. TestAmerica Tampa Page 48 of 59 07/15/2008 Quality Control Results Client: ARCADIS U.S., Inc. Job Number: 660-17097-1 Lab Control Spike/ Lab Control Spike Duplicate Recovery Report - Batch: 660-47317 Method: 8260B Preparation: 5030B LCS Lab Sample ID: LCS 660-47317/1 Client Matrix: Water Dilution: 1.0 Date Analyzed: 07/23/2007 1215 Date Prepared: 07/23/2007 1215 Analysis Batch: 660-47317 Prep Batch: N/A Units: ug/L Instrument ID: BVMJ GC/MS Lab File ID: 1JG2308.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL LCSD Lab Sample ID: LCSD 660-47317/2 Client Matrix: Water Dilution: 1.0 Date Analyzed: 07/23/2007 1240 Date Prepared: 07/23/2007 1240 Analysis Batch: 660-47317 Prep Batch: N/A Units: ug/L Instrument ID: BVMJ GC/MS Lab File ID: 1JG2309.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Analyte LCS 1,1-Dichloroethene Benzene Chlorobenzene Toluene Trichloroethene 91 92 98 97 84 % Rec. LCSD 72 75 81 77 67 Limit RPD RPD Limit 46 - 147 62 - 135 72 - 127 68 - 131 56 - 143 23 21 19 23 22 30 37 22 33 35 LCS Qual LCSD Qual Calculations are performed before rounding to avoid round-off errors in calculated results. TestAmerica Tampa Page 49 of 59 07/15/2008 Quality Control Results Client: ARCADIS U.S., Inc. Job Number: 660-17097-1 Matrix Spike/ Matrix Spike Duplicate Recovery Report - Batch: 660-47317 Method: 8260B Preparation: 5030B MS Lab Sample ID: Client Matrix: Dilution: Date Analyzed: Date Prepared: 660-17097-1 Water 1.0 07/26/2007 0446 07/26/2007 0446 Analysis Batch: 660-47317 Prep Batch: N/A Instrument ID: BVMJ GC/MS Lab File ID: 1JG2548.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL MSD Lab Sample ID: Client Matrix: Dilution: Date Analyzed: Date Prepared: 660-17097-1 Water 1.0 07/26/2007 0510 07/26/2007 0510 Analysis Batch: 660-47317 Prep Batch: N/A Instrument ID: BVMJ GC/MS Lab File ID: 1JG2549.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Analyte MS 1,1-Dichloroethene Benzene Chlorobenzene Toluene Trichloroethene 100 98 106 110 92 % Rec. MSD 89 89 96 96 82 Limit RPD RPD Limit 46 - 147 62 - 135 72 - 127 68 - 131 56 - 143 11 9 10 13 12 30 37 22 33 35 MS Qual MSD Qual Calculations are performed before rounding to avoid round-off errors in calculated results. TestAmerica Tampa Page 50 of 59 07/15/2008 Quality Control Results Client: ARCADIS U.S., Inc. Job Number: 660-17097-1 Method Blank - Batch: 660-47328 Lab Sample ID: Client Matrix: Dilution: Date Analyzed: Date Prepared: MB 660-47328/3 Water 1.0 07/23/2007 1305 07/23/2007 1305 Method: 8260B Preparation: 5030B Analysis Batch: 660-47328 Prep Batch: N/A Units: ug/L Instrument ID: BVMJ GC/MS Lab File ID: 1JG2310.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Analyte Result Qual MDL PQL 1,4-Dioxane 0.54 U 0.54 1.0 Lab Control Spike/ Lab Control Spike Duplicate Recovery Report - Batch: 660-47328 Method: 8260B Preparation: 5030B LCS Lab Sample ID: LCS 660-47328/1 Client Matrix: Water Dilution: 1.0 Date Analyzed: 07/23/2007 1215 Date Prepared: 07/23/2007 1215 Analysis Batch: 660-47328 Prep Batch: N/A Units: ug/L Instrument ID: BVMJ GC/MS Lab File ID: 1JG2308.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL LCSD Lab Sample ID: LCSD 660-47328/2 Client Matrix: Water Dilution: 1.0 Date Analyzed: 07/23/2007 1240 Date Prepared: 07/23/2007 1240 Analysis Batch: 660-47328 Prep Batch: N/A Units: ug/L Instrument ID: BVMJ GC/MS Lab File ID: 1JG2309.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Analyte LCS % Rec. LCSD 1,4-Dioxane 101 99 Limit RPD RPD Limit 50 - 150 2 50 LCS Qual LCSD Qual Calculations are performed before rounding to avoid round-off errors in calculated results. TestAmerica Tampa Page 51 of 59 07/15/2008 Quality Control Results Client: ARCADIS U.S., Inc. Job Number: 660-17097-1 Matrix Spike/ Matrix Spike Duplicate Recovery Report - Batch: 660-47328 Method: 8260B Preparation: 5030B MS Lab Sample ID: Client Matrix: Dilution: Date Analyzed: Date Prepared: 660-17097-1 Water 1.0 07/26/2007 0446 07/26/2007 0446 Analysis Batch: 660-47328 Prep Batch: N/A Instrument ID: BVMJ GC/MS Lab File ID: 1JG2548.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL MSD Lab Sample ID: Client Matrix: Dilution: Date Analyzed: Date Prepared: 660-17097-1 Water 1.0 07/26/2007 0510 07/26/2007 0510 Analysis Batch: 660-47328 Prep Batch: N/A Instrument ID: BVMJ GC/MS Lab File ID: 1JG2549.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Analyte MS 1,4-Dioxane 84 % Rec. MSD 96 Limit RPD RPD Limit 50 - 150 14 50 MS Qual MSD Qual Calculations are performed before rounding to avoid round-off errors in calculated results. TestAmerica Tampa Page 52 of 59 07/15/2008 Quality Control Results Client: ARCADIS U.S., Inc. Job Number: 660-17097-1 Method Blank - Batch: 660-47471 Lab Sample ID: Client Matrix: Dilution: Date Analyzed: Date Prepared: MB 660-47471/3 Water 1.0 07/24/2007 1714 07/24/2007 1714 Method: 8260B Preparation: 5030B Analysis Batch: 660-47471 Prep Batch: N/A Units: ug/L Instrument ID: BVMJ GC/MS Lab File ID: 1JG2414.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Analyte Result Qual MDL PQL 1,1,1,2-Tetrachloroethane 1,1,1-Trichloroethane 1,1,2,2-Tetrachloroethane 1,1,2-Trichloroethane 1,1-Dichloroethane 1,1-Dichloroethene 1,1-Dichloropropene 1,2,3-Trichlorobenzene 1,2,3-Trichloropropane 1,2,4-Trichlorobenzene 1,2,4-Trimethylbenzene 1,2-Dibromo-3-Chloropropane 1,2-Dichlorobenzene 1,2-Dichloroethane 1,2-Dichloropropane 1,3,5-Trimethylbenzene 1,3-Dichlorobenzene 1,3-Dichloropropane 1,4-Dichlorobenzene 2,2-Dichloropropane 2-Chlorotoluene 2-Hexanone 4-Chlorotoluene 4-Isopropyltoluene Acetone Benzene Bromobenzene Bromoform Bromomethane Carbon disulfide Carbon tetrachloride Chlorobenzene Chlorobromomethane Chlorodibromomethane Chloroethane Chloroform Chloromethane cis-1,2-Dichloroethene cis-1,3-Dichloropropene Dibromomethane Dichlorobromomethane 0.63 0.46 0.15 0.47 0.52 0.45 0.31 0.77 0.18 0.58 0.86 2.5 0.44 0.57 0.52 0.54 0.64 0.39 0.52 0.36 0.65 4.4 0.52 0.69 9.9 0.50 0.58 0.58 2.5 0.85 0.42 0.63 0.58 0.34 2.5 0.90 1.0 0.65 0.14 0.41 0.35 U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U 0.63 0.46 0.15 0.47 0.52 0.45 0.31 0.77 0.18 0.58 0.86 2.5 0.44 0.57 0.52 0.54 0.64 0.39 0.52 0.36 0.65 4.4 0.52 0.69 9.9 0.50 0.58 0.58 2.5 0.85 0.42 0.63 0.58 0.34 2.5 0.90 1.0 0.65 0.14 0.41 0.35 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 10 1.0 1.0 20 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 4.0 1.0 1.0 1.0 1.0 Calculations are performed before rounding to avoid round-off errors in calculated results. TestAmerica Tampa Page 53 of 59 07/15/2008 Quality Control Results Client: ARCADIS U.S., Inc. Job Number: 660-17097-1 Method Blank - Batch: 660-47471 Lab Sample ID: Client Matrix: Dilution: Date Analyzed: Date Prepared: MB 660-47471/3 Water 1.0 07/24/2007 1714 07/24/2007 1714 Method: 8260B Preparation: 5030B Analysis Batch: 660-47471 Prep Batch: N/A Units: ug/L Instrument ID: BVMJ GC/MS Lab File ID: 1JG2414.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Analyte Result Qual MDL PQL Dichlorodifluoromethane Ethylbenzene Ethylene Dibromide Hexachlorobutadiene Isopropylbenzene 2-Butanone (MEK) 4-Methyl-2-pentanone (MIBK) Methyl tert-butyl ether Methylene Chloride m-Xylene & p-Xylene Naphthalene n-Butylbenzene N-Propylbenzene o-Xylene sec-Butylbenzene Styrene tert-Butylbenzene Tetrachloroethene Toluene trans-1,2-Dichloroethene trans-1,3-Dichloropropene Trichloroethene Trichlorofluoromethane Vinyl chloride 2.5 0.44 0.50 0.40 0.19 8.4 3.8 0.44 4.0 0.60 2.5 0.67 0.59 0.50 0.63 0.98 0.84 0.50 0.51 0.44 0.14 0.50 2.5 0.50 U U U U U U U U U U U U U U U U U U U U U U U U 2.5 0.44 0.50 0.40 0.19 8.4 3.8 0.44 4.0 0.60 2.5 0.67 0.59 0.50 0.63 0.98 0.84 0.50 0.51 0.44 0.14 0.50 2.5 0.50 5.0 1.0 1.0 1.0 1.0 10 10 1.0 5.0 2.0 5.0 1.0 1.0 1.0 1.0 2.0 1.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 Surrogate Toluene-d8 (Surr) 4-Bromofluorobenzene Dibromofluoromethane % Rec Acceptance Limits 97 104 83 77 - 122 74 - 126 70 - 130 Calculations are performed before rounding to avoid round-off errors in calculated results. TestAmerica Tampa Page 54 of 59 07/15/2008 Quality Control Results Client: ARCADIS U.S., Inc. Job Number: 660-17097-1 Lab Control Spike/ Lab Control Spike Duplicate Recovery Report - Batch: 660-47471 Method: 8260B Preparation: 5030B LCS Lab Sample ID: LCS 660-47471/1 Client Matrix: Water Dilution: 1.0 Date Analyzed: 07/24/2007 1559 Date Prepared: 07/24/2007 1559 Analysis Batch: 660-47471 Prep Batch: N/A Units: ug/L Instrument ID: BVMJ GC/MS Lab File ID: 1JG2411.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL LCSD Lab Sample ID: LCSD 660-47471/2 Client Matrix: Water Dilution: 1.0 Date Analyzed: 07/24/2007 1625 Date Prepared: 07/24/2007 1625 Analysis Batch: 660-47471 Prep Batch: N/A Units: ug/L Instrument ID: BVMJ GC/MS Lab File ID: 1JG2412.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Analyte LCS % Rec. LCSD 1,1-Dichloroethene Benzene Chlorobenzene Toluene Trichloroethene 105 103 105 108 93 93 91 95 96 83 Limit RPD RPD Limit 46 - 147 62 - 135 72 - 127 68 - 131 56 - 143 13 12 10 12 11 30 37 22 33 35 LCS Qual LCSD Qual Calculations are performed before rounding to avoid round-off errors in calculated results. TestAmerica Tampa Page 55 of 59 07/15/2008 Quality Control Results Client: ARCADIS U.S., Inc. Job Number: 660-17097-1 Method Blank - Batch: 660-47480 Lab Sample ID: Client Matrix: Dilution: Date Analyzed: Date Prepared: MB 660-47480/3 Water 1.0 07/24/2007 1714 07/24/2007 1714 Method: 8260B Preparation: 5030B Analysis Batch: 660-47480 Prep Batch: N/A Units: ug/L Instrument ID: BVMJ GC/MS Lab File ID: 1JG2414.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Analyte Result Qual MDL PQL 1,4-Dioxane 0.54 U 0.54 1.0 Lab Control Spike/ Lab Control Spike Duplicate Recovery Report - Batch: 660-47480 Method: 8260B Preparation: 5030B LCS Lab Sample ID: LCS 660-47480/1 Client Matrix: Water Dilution: 1.0 Date Analyzed: 07/24/2007 1559 Date Prepared: 07/24/2007 1559 Analysis Batch: 660-47480 Prep Batch: N/A Units: ug/L Instrument ID: BVMJ GC/MS Lab File ID: 1JG2411.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL LCSD Lab Sample ID: LCSD 660-47480/2 Client Matrix: Water Dilution: 1.0 Date Analyzed: 07/24/2007 1625 Date Prepared: 07/24/2007 1625 Analysis Batch: 660-47480 Prep Batch: N/A Units: ug/L Instrument ID: BVMJ GC/MS Lab File ID: 1JG2412.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Analyte LCS % Rec. LCSD 1,4-Dioxane 110 90 Limit RPD RPD Limit 50 - 150 20 50 LCS Qual LCSD Qual Calculations are performed before rounding to avoid round-off errors in calculated results. TestAmerica Tampa Page 56 of 59 07/15/2008 Page 57 of 59 07/15/2008 Page 58 of 59 07/15/2008 Login Sample Receipt Check List Client: ARCADIS U.S., Inc. Job Number: 660-17097-1 Login Number: 17097 Creator: McNulty, Carol List Number: 1 List Source: TestAmerica Tampa Question T / F/ NA Radioactivity either was not measured or, if measured, is at or below background The cooler's custody seal, if present, is intact. The cooler or samples do not appear to have been compromised or tampered with. Samples were received on ice. Cooler Temperature is acceptable. Cooler Temperature is recorded. COC is present. COC is filled out in ink and legible. COC is filled out with all pertinent information. There are no discrepancies between the sample IDs on the containers and the COC. Samples are received within Holding Time. Sample containers have legible labels. Containers are not broken or leaking. Sample collection date/times are provided. Appropriate sample containers are used. Sample bottles are completely filled. There is sufficient vol. for all requested analyses, incl. any requested MS/MSDs VOA sample vials do not have headspace or bubble is <6mm (1/4") in diameter. If necessary, staff have been informed of any short hold time or quick TAT needs Multiphasic samples are not present. Samples do not require splitting or compositing. N/A TestAmerica Tampa Comment N/A True True True True True True True True True True True True True True True True True True True Page 59 of 59 07/15/2008