Test Report. No. SHAEC1322965311 Date: 04 Dec 2013 . Page 1 of 13. Heraeus (Zhaoyuan )Metal Materials Co.,Ltd/Heraeus Zhaoyuan (Changshu) Electronic Materials Co., Ltd. . No.238 Linglong Road Zhaoyuan Shandong/Huangpujiang Road, Changshu Southeast Economic Development Zone, Changshu, Jiangsu . . The following sample(s) was/were submitted and identified on behalf of the clients as : GOLD BONDING WIRE HA. SGS Job No. : SP13-033894 - SH . Model No. :. HA. Composition :. GOLD. Date of Sample Received : . 22 Nov 2013. Testing Period : . 22 Nov 2013 - 03 Dec 2013 . Test Requested : . Selected test(s) as requested by client. . Test Method : . Please refer to next page(s). . Test Results :. Please refer to next page(s). . Conclusion :. Based on the performed tests on submitted samples, the results of Lead, Mercury, Cadmium, Hexavalent chromium, Polybrominated biphenyls (PBB), Polybrominated diphenyl ethers (PBDE) comply with the limits as set by RoHS Directive 2011/65/EU Annex II; recasting 2002/95/EC. . Signed for and on behalf of SGS-CSTC Ltd. . JJ Fan. Approved Signatory . Test Report. No. SHAEC1322965311 Date: 04 Dec 2013 . Page 2 of 13. Test Results :. Test Part Description : . Specimen No.. SN1. SGS Sample ID. SHA13-229653.001 Description. Gold metal wire . Remarks :. (1) 1 mg/kg = 1 ppm = 0.0001% . (2) MDL = Method Detection Limit . (3) ND = Not Detected ( < MDL ) . (4) "-" = Not Regulated . RoHS Directive 2011/65/EU. Test Method : . (1) With reference to IEC 62321-5:2013, determination of Cadmium by ICP-OES. (2) With reference to IEC 62321-5:2013, determination of Lead by ICP-OES. (3) With reference to IEC 62321-4:2013, determination of Mercury by ICP-OES. (4) With reference to IEC 62321:2008, determination of Hexavalent Chromium by spot test / Colorimetric Method using UV-Vis. (5) With reference to IEC 62321:2008, determination of PBBs and PBDEs by GC-MS. . Limit. Unit. MDL. 001. Cadmium (Cd) . 100 mg/kg. 2 ND Lead (Pb). 1000 mg/kg. 2 ND Mercury (Hg). 1000 mg/kg. 2 ND - - ♢ Negative 1000 mg/kg. - ND Monobromobiphenyl . - mg/kg. 5 ND Dibromobiphenyl . - mg/kg. 5 ND Tribromobiphenyl . - mg/kg. 5 ND Tetrabromobiphenyl . - mg/kg. 5 ND Pentabromobiphenyl . - mg/kg. 5 ND Hexabromobiphenyl . - mg/kg. 5 ND Heptabromobiphenyl . - mg/kg. 5 ND Octabromobiphenyl . - mg/kg. 5 ND Nonabromobiphenyl . - mg/kg. 5 ND Decabromobiphenyl . - mg/kg. 5 ND 1000 mg/kg. - ND - mg/kg. 5 ND Test Item(s). Hexavalent Chromium (Cr(VI)) . Sum of PBBs . Sum of PBDEs . Monobromodiphenyl ether . Test Report. No. SHAEC1322965311 Date: 04 Dec 2013 . Limit. Unit. MDL. 001. Dibromodiphenyl ether . - mg/kg. 5 ND Tribromodiphenyl ether . - mg/kg. 5 ND Tetrabromodiphenyl ether . - mg/kg. 5 ND Pentabromodiphenyl ether . - mg/kg. 5 ND Hexabromodiphenyl ether . - mg/kg. 5 ND Heptabromodiphenyl ether . - mg/kg. 5 ND Octabromodiphenyl ether . - mg/kg. 5 ND Nonabromodiphenyl ether . - mg/kg. 5 ND Decabromodiphenyl ether . - mg/kg. 5 ND Test Item(s). Page 3 of 13. Notes :. (1) The maximum permissible limit is quoted from directive 2011/65/EU, Annex II (2) ◇Spot-test: Negative = Absence of Cr(VI) coating, Positive = Presence of Cr(VI) coating; (The tested sample should be further verified by boiling-water-extraction method if the spot test result is Negative or cannot be confirmed.) ◇Boiling-water-extraction: Negative = Absence of Cr(VI) coating Positive = Presence of Cr(VI) coating; the detected concentration in boiling-water-extraction solution is equal or greater than 0.02 mg/kg with 50 cm² sample surface area. Information on storage conditions and production date of the tested sample is unavailable and thus Cr(VI) results represent status of the sample at the time of testing. (3) The test results are taken from report SHAEC1323206901 . Halogen. Test Method : . With reference to EN 14582: 2007, analysis was performed by Ion Chromatograph (IC). . Test Item(s). Fluorine (F). Chlorine (Cl). Bromine (Br). Iodine (I). Unit. MDL. 001. mg/kg. mg/kg. mg/kg. mg/kg. 50 50 50 50 ND ND ND ND Notes :. The test results are taken from report SHAEC1323206901 . Element(s). Test Method : . With reference to US EPA Method 3050B:1996, analysis was performed by ICP-OES. . Test Report. No. SHAEC1322965311 Test Item(s). Antimony (Sb) . Antimony trioxide (Sb₂O₃)◆ . Phosphorus (P) . Date: 04 Dec 2013 . Unit. MDL. 001. mg/kg. mg/kg. mg/kg. 10 12 20 ND ND ND Page 4 of 13. Notes :. (1) ◆ Calculated concentration of Sb₂O₃ is based on the identified Sb (2) The test results are taken from report SHAEC1323206901 . Phthalates. Test Method : . Determination of phthalates by GC-MS based on EN 14372:2004. . CAS NO. Unit. MDL. 001. Dibutyl Phthalate (DBP) . 84-74-2. %. 0.003 ND Benzylbutyl Phthalate (BBP) . 85-68-7. %. 0.003 ND Bis-(2-ethylhexyl) Phthalate (DEHP). Diisobutyl Phthalate (DIBP) . 117-81-7. %. 0.003 ND 84-69-5. %. 0.003 ND Test Item(s). Notes :. (1) Reference Information: Directive 2011/65/EU recasting RoHS directive 2002/95/EC: Bis (2-ethylhexyl) phthalate (DEHP), Butyl benzyl phthalate (BBP) and Dibutyl phthalate (DBP) are considered as a priority for risk evaluation and substance restriction. . Tetrabromobisphenol A (TBBP-A). Test Method : . With reference to US EPA 3540C: 1996, analysis was performed by GC-MS. . Test Item(s). Unit. Tetrabromobisphenol A (TBBP-A) . mg/kg. MDL. 001. 10 ND Hexabromocyclododecane (HBCDD). Test Method : . Determination of HBCDD by GC-MS based on IEC 62321:2008. . Test Report. No. SHAEC1322965311 Date: 04 Dec 2013 . Test Item(s). Unit. Hexabromocyclododecane (HBCDD) . mg/kg. MDL. 001. 10 ND Page 5 of 13. Notes :. (1) Reference Information: Directive 2011/65/EU recasting RoHS directive 2002/95/EC: Hexabromocyclododecane (HBCDD) is considered as a priority for risk evaluation and substance restriction. . PFOS (Perfluorooctane Sulfonates) and PFOA (Perfluorooctanoic Acid). Test Method : . With reference to US EPA 3550C: 2007, analysis was performed by HPLC-MS. . Test Item(s). Perfluorooctane Sulfonates (PFOS) and related Acid,Metal Salt and Amide . Perfluorooctanoic Acid (PFOA) . Limit. Unit. 1000. mg/kg. MDL. 10. ND. 001. - mg/kg. 10. ND. Notes :. Max. limit specified by commission regulation (EU) No. 757/2010 (previously restricted under entry 53 of Regulation (EC) No 552/2009 amending Annex XVII of REACH Regulation (EC) No 1907/2006) . Test Report. No. SHAEC1322965311 Date: 04 Dec 2013 . Page 6 of 13. ATTACHMENTS RoHS Testing Flow Chart 1) Name of the person who made testing: Jan Shi/Star Wang/Shara Wang/Gary Xu 2) Name of the person in charge of testing: Jeff Zhang/George Xu/ Jessy Huang 6+ 3) These samples were dissolved totally by pre-conditioning method according to below flow chart. (Cr and PBBs/PBDEs test method excluded) Sample Preparation Sample Measurement Pb/Cd/Hg Acid digestion with microwave/ hotplate Sample solvent extraction Filtration Concentration/ Dilution of extraction solution Solution + Cr6 PBBs/PBDEs Nonmetallic material Adding digestion reagent Residue GC/MS Heating to 90~95℃ for extraction Filtration and pH adjustment DATA ICP-OES DATA Positive Spot test Negative Filtration 1) Alkali Fusion / Dry Ashing 2) Acid to dissolve Metallic material Adding 1,5diphenylcarbazide for color development UV-Vis DATA Boiling water extraction Adding 1,5diphenylcarbazide for color development A red color indicates the 6+ presence of Cr . If necessary, confirm with UV-Vis. DATA Test Report. No. SHAEC1322965311 Date: 04 Dec 2013 . Phthalates Testing Flow Chart 1) Name of the person who made testing: Elyn Yao 2) Name of the person in charge of testing: Myra Ma Sample cutting/preparation Sample measurement Solvent extraction Concentration/Dilution Filtration GC-MS DATA Page 7 of 13. Test Report. No. SHAEC1322965311 Date: 04 Dec 2013 . HBCDD Testing Flow Chart 1) Name of the person who made testing: Gary Xu 2) Name of the person in charge of testing: Jessy Huang Sample cutting/preparation Sample measurement Solvent extraction Concentration/Dilution Filtration GC-MS DATA Page 8 of 13. Test Report. No. SHAEC1322965311 Date: 04 Dec 2013 . Halogen Testing (oxygen bomb) Flow Chart 1) Name of the person who made testing: Sisily Yin 2) Name of the person in charge of testing: Linda Li Sample cutting/preparation Sample measurement Combustion in oxygen bomb Dissolved in an absorption solution Filtration Analyzed by ion chromatography. Double confirm by other instruments, if necessary DATA Page 9 of 13. Test Report. No. SHAEC1322965311 Date: 04 Dec 2013 . PFOS/PFOA Testing Flow Chart 1) Name of the person who made testing: Mary Yang 2) Name of the person in charge of testing: Judy Li Sample cutting/preparation Sample measurement Solvent extraction Concentration/Dilution Filtration LC-MS DATA Page 10 of 13. Test Report. No. SHAEC1322965311 Date: 04 Dec 2013 . TBBP-A Testing Flow Chart 1) Name of the person who made testing: Gary Xu 2) Name of the person in charge of testing: Jessy Huang Sample cutting/preparation Sample measurement Solvent extraction Derivatization Liquid-liquid extraction Concentration/Dilution Filtration GC-MS DATA Page 11 of 13. Test Report. No. SHAEC1322965311 Date: 04 Dec 2013 . Elements Testing Flow Chart 1) Name of the person who made testing: Star Wang/ Jan Shi 2) Name of the person in charge of testing: Jeff Zhang Sample cutting/preparation Sample measurement Acid digestion Filtration Solution ICP-OES DATA Page 12 of 13. Test Report. No. SHAEC1322965311 Date: 04 Dec 2013 . Sample photo: . SHAEC1322965311 SHA13-229653.001 . SGS authenticate the photo on original report only . *** End of Report *** . Page 13 of 13.