Test Report. No. SHAEC1207176309 A03 Date: 18 Jun 2012 . Page 1 of 14. JIANGSU CHANGJIANG ELECTRONICS TECHNOLOGY (SUQIAN) CO., LTD. . NO.5 PUTUO MOUNT RD., SUCHENG DISTRICT,SUQIAN,JIANGSU CHINA . THIS REPORT IS TO SUPERSEDE TEST REPORT NO.SHAEC1207176307A02 DATE: 2012/06/06. The following sample(s) was/were submitted and identified on behalf of the clients as : package part TO-247 (include TO-3P/251/252/220/220F/126/126C); pinlead part TO-247 (include TO-3P/251/252/220/220F/126/126C)) . SGS Job No. : SP12-013405 - SH . Composition :. Black Plastic Part . Composition :. Silvery Metal Part . Date of Sample Received : . 09 May 2012. Testing Period : . 09 May 2012 - 13 May 2012 . Test Requested : . Selected test(s) as requested by client. . Test Method : . Please refer to next page(s). . Test Results :. Please refer to next page(s). . Signed for and on behalf of SGS-CSTC Ltd. . Fan Jingjie, JJ. Approved Signatory . 0000747644 Test Report. No. SHAEC1207176309 A03 Date: 18 Jun 2012 . Page 2 of 14. Test Results :. Test Part Description : . Specimen No.. 1. SGS Sample ID. SHA12-071763.001 Description. Black body with silvery metal part(mix all*) . 2. SHA12-071763.002 Silvery pin part . Remarks :. (1) 1 mg/kg = 1 ppm = 0.0001% . (2) MDL = Method Detection Limit . (3) ND = Not Detected ( < MDL ) . (4) "-" = Not Regulated . RoHS Directive 2011/65/EU. Test Method : . With reference to IEC 62321:2008 (1) Determination of Cadmium by ICP-OES. (2) Determination of Lead by ICP-OES. (3) Determination of Mercury by ICP-OES. (4) Determination of Hexavalent Chromium by Colorimetric Method using UV-Vis. (5) Determination of PBBs / PBDEs content by GC-MS. . Test Item(s). Limit. Unit. MDL. 001. Cadmium (Cd) . 100 mg/kg. 2 ND Lead (Pb). 1000 mg/kg. 2 2981▲ Mercury (Hg). 1000 mg/kg. 2 ND Hexavalent Chromium (Cr(VI)) . 1000 mg/kg. 2 ND Sum of PBBs . 1000 mg/kg. - ND Monobromobiphenyl . - mg/kg. 5 ND Dibromobiphenyl . - mg/kg. 5 ND Tribromobiphenyl . - mg/kg. 5 ND Tetrabromobiphenyl . - mg/kg. 5 ND Pentabromobiphenyl . - mg/kg. 5 ND Hexabromobiphenyl . - mg/kg. 5 ND Heptabromobiphenyl . - mg/kg. 5 ND Octabromobiphenyl . - mg/kg. 5 ND Nonabromobiphenyl . - mg/kg. 5 ND - mg/kg. 5 ND 1000 mg/kg. - ND Decabromobiphenyl . Sum of PBDEs . 0000747644 Test Report. No. SHAEC1207176309 A03 Date: 18 Jun 2012 . Limit. Unit. MDL. 001. Monobromodiphenyl ether . - mg/kg. 5 ND Dibromodiphenyl ether . - mg/kg. 5 ND Tribromodiphenyl ether . - mg/kg. 5 ND Tetrabromodiphenyl ether . - mg/kg. 5 ND Pentabromodiphenyl ether . - mg/kg. 5 ND Hexabromodiphenyl ether . - mg/kg. 5 ND Heptabromodiphenyl ether . - mg/kg. 5 ND Octabromodiphenyl ether . - mg/kg. 5 ND Nonabromodiphenyl ether . - mg/kg. 5 ND Decabromodiphenyl ether . - mg/kg. 5 ND Test Item(s). Page 3 of 14. Notes :. (1) The maximum permissible limit is quoted from directive 2011/65/EU, Annex II (2) *The sample(s) was/were analyzed on behalf of the applicant as mixing sample in one testing. The above result(s) was/were only given as the informality value and only for reference. (3) ▲=According to the declaration from the client, Lead (Pb) in No.001 is exempted by EU RoHS Directive 2011/65/EU based on: Lead in high melting temperature type solders (i.e. lead-based alloys containing 85 % by weight or more lead). . RoHS Directive 2011/65/EU. Test Method : . With reference to IEC 62321:2008 (1) Determination of Cadmium by ICP-OES. (2) Determination of Lead by ICP-OES. (3) Determination of Mercury by ICP-OES. (4) Determination of Hexavalent Chromium by Spot test / Colorimetric Method using UV-Vis. (5) Determination of PBBs / PBDEs by GC-MS. . Test Item(s). Limit. Unit. MDL. 002. Cadmium (Cd) . 100 mg/kg. 2 ND Lead (Pb). 1000 mg/kg. 2 ND Mercury (Hg). 1000 mg/kg. 2 ND Hexavalent Chromium (Cr(VI)) . - - ♢ Negative 1000 mg/kg. - ND Monobromobiphenyl . - mg/kg. 5 ND Dibromobiphenyl . - mg/kg. 5 ND Tribromobiphenyl . - mg/kg. 5 ND Tetrabromobiphenyl . - mg/kg. 5 ND Pentabromobiphenyl . - mg/kg. 5 ND Hexabromobiphenyl . - mg/kg. 5 ND Sum of PBBs . 0000747644 Test Report. No. SHAEC1207176309 A03 Date: 18 Jun 2012 . Limit. Unit. MDL. 002. Heptabromobiphenyl . - mg/kg. 5 ND Octabromobiphenyl . - mg/kg. 5 ND Nonabromobiphenyl . - mg/kg. 5 ND Test Item(s). Decabromobiphenyl . - mg/kg. 5 ND 1000 mg/kg. - ND Monobromodiphenyl ether . - mg/kg. 5 ND Dibromodiphenyl ether . - mg/kg. 5 ND Tribromodiphenyl ether . - mg/kg. 5 ND Tetrabromodiphenyl ether . - mg/kg. 5 ND Pentabromodiphenyl ether . - mg/kg. 5 ND Hexabromodiphenyl ether . - mg/kg. 5 ND Heptabromodiphenyl ether . - mg/kg. 5 ND Octabromodiphenyl ether . - mg/kg. 5 ND Nonabromodiphenyl ether . - mg/kg. 5 ND Decabromodiphenyl ether . - mg/kg. 5 ND Sum of PBDEs . Page 4 of 14. Notes :. (1) The maximum permissible limit is quoted from directive 2011/65/EU, Annex II (2) ◇Spot-test: Negative = Absence of Cr(VI) coating, Positive = Presence of Cr(VI) coating; (The tested sample should be further verified by boiling-water-extraction method if the spot test result is Negative or cannot be confirmed.) ◇Boiling-water-extraction: Negative = Absence of Cr(VI) coating Positive = Presence of Cr(VI) coating; the detected concentration in boiling-water-extraction solution is equal or greater than 0.02 mg/kg with 50 cm² sample surface area. For corrosion protection coatings on metals: Information on storage conditions and production date of the tested sample is unavailable and thus results of Cr(VI) represent status of the sample at the time of testing. . Phthalates. Test Method : . With reference to EN14372: 2004, analysis was performed by GC-MS. . Test Item(s). Dibutyl Phthalate (DBP) . Benzylbutyl Phthalate (BBP) . Bis-(2-ethylhexyl) Phthalate (DEHP) . Diisononyl Phthalate (DINP) . Di-n-octyl Phthalate (DNOP) . 0000747644 Unit. MDL. 001. %. %. %. %. %. 0.003 0.003 0.003 0.010 0.003 ND ND ND ND ND Test Report. No. SHAEC1207176309 A03 Test Item(s). Diisodecyl Phthalate (DIDP) . Di-n-hexyl Phthalate (DnHP) . Diisobutyl Phthalate (DIBP) . Date: 18 Jun 2012 . Unit. MDL. 001. %. %. %. 0.010 0.003 0.003 ND ND ND Page 5 of 14. Notes :. (1) DBP,BBP,DEHP Reference information: Entry 51 of Regulation (EC) No 552/2009 amending Annex XVII of REACH Regulation (EC) No 1907/2006 (previously restricted under Directive 2005/84/EC): i) Shall not be used as substances or in mixtures, in concentrations greater than 0,1 % by weight of the plasticised material, in toys and childcare articles. ii) Toys and childcare articles containing these phthalates in a concentration greater than 0.1 % by weight of the plasticised material shall not be placed on the market. Please refer to Regulation (EC) No 552/2009 to get more detail information DINP, DNOP, DIDP Reference information: Entry 52 of Regulation (EC) No 552/2009 amending Annex XVII of REACH Regulation (EC) No 1907/2006 (previously restricted under Directive 2005/84/EC). i) Shall not be used as substances or in mixtures, in concentrations greater than 0.1 % by weight of the plasticised material, in toys and childcare articles which can be placed in the mouth by children. ii) Such toys and childcare articles containing these phthalates in a concentration greater than 0.1 % by weight of the plasticised material shall not be placed on the market. Please refer to Regulation (EC) No 552/2009 to get more detail information . Polynuclear Aromatic Hydrocarbons (PAH). Test Method : . With reference to ZEK 01.2-08 of German ZLS and its amendments, analysis was performed by GC-MS.. Test Item(s). Unit. MDL. 001. Total 18 PAHs . mg/kg. - ND Naphthalene(NAP) . mg/kg. 0.2 ND Acenaphthylene(ANY) . mg/kg. 0.2 ND Acenaphthene(ANA) . mg/kg. 0.2 ND Fluorene(FLU) . mg/kg. 0.2 ND Phenanthrene(PHE) . mg/kg. 0.2 ND Anthracene(ANT) . mg/kg. 0.2 ND 0000747644 Test Report. No. SHAEC1207176309 A03 Date: 18 Jun 2012 . Unit. MDL. 001. Fluoranthene(FLT) . mg/kg. 0.2 ND Pyrene(PYR) . mg/kg. 0.2 ND Benzo(a)anthracene(BaA) . mg/kg. 0.2 ND Chrysene(CHR) . mg/kg. 0.2 ND Benzo(b)fluoranthene(BbF) Benzo(j)fluoranthene(BjF) . Benzo(k)fluoranthene(BkF) . mg/kg. 0.4 ND mg/kg. 0.2 ND Benzo(a)pyrene(BaP) . mg/kg. 0.2 ND Indeno(1,2,3-c,d)pyrene(IPY) . mg/kg. 0.2 ND Dibenzo(a,h)anthracene(DBA) . mg/kg. 0.2 ND Benzo(g,h,i)perylene(BPE) . mg/kg. 0.2 ND Benzo(e)pyrene(BeP) . mg/kg. 0.2 ND Test Item(s). Tetrabromobisphenol A (TBBP-A). Test Method : . With reference to US EPA 3550C: 2007, analysis was performed by GC-MS. . Test Item(s). Unit. Tetrabromobisphenol A (TBBP-A) . mg/kg. MDL. 001. 10 ND Hexabromocyclododecane (HBCDD). Test Method : . With reference to US EPA 3550C: 2007, analysis was performed by GC-MS. . Unit. MDL. 001. mg/kg. 10 ND Test Item(s). Hexabromocyclododecane (HBCDD) . PFOS (Perfluorooctane Sulfonates) and PFOA (Perfluorooctanoic Acid). 0000747644 Page 6 of 14. Test Report. No. SHAEC1207176309 A03 Date: 18 Jun 2012 . Page 7 of 14. Test Method : . With reference to US EPA 3550C: 2007, analysis was performed by HPLC-MS. . Test Item(s). Perfluorooctane Sulfonates (PFOS) and related Acid,Metal Salt and Amide . Perfluorooctanoic Acid (PFOA) . Limit. 1000. Unit. mg/kg. MDL. 10. 001. ND. - mg/kg. 10. ND. Notes :. Max. limit specified by commission regulation (EU) No. 757/2010 (previously restricted under entry 53 of Regulation (EC) No 552/2009 amending Annex XVII of REACH Regulation (EC) No 1907/2006) . 0000747644 Test Report. No. SHAEC1207176309 A03 Date: 18 Jun 2012 . Page 8 of 14. ATTACHMENTS RoHS Testing Flow Chart 1) Name of the person who made testing: Jan Shi/Yoyo Wang/Allen Xiao/Gary Xu 2) Name of the person in charge of testing: Jeff Zhang/George Xu/ Linda Li 3) These samples were dissolved totally by pre-conditioning method according to below flow chart. (Cr6+ and PBBs/PBDEs test method excluded) Sample Preparation Sample Measurement Pb/Cd/Hg Acid digestion with microwave/ hotplate Sample solvent extraction Filtration Concentration/ Dilution of extraction solution Solution + Cr6 PBBs/PBDEs Nonmetallic material Adding digestion reagent Residue Positive Spot test Negative Filtration 1) Alkali Fusion / Dry Ashing 2) Acid to dissolve Metallic material GC/MS Heating to 90~95℃ for extraction Filtration and pH adjustment DATA ICP-OES Adding 1,5diphenylcarbazide for color development DATA UV-Vis DATA 0000747644 Boiling water extraction Adding 1,5diphenylcarbazide for color development A red color indicates the 6+ presence of Cr . If necessary, confirm with UV-Vis. DATA Test Report. No. SHAEC1207176309 A03 Date: 18 Jun 2012 . PFOS/PFOA Testing Flow Chart 1) Name of the person who made testing: Judy Li 2) Name of the person in charge of testing: Linda Li Sample cutting/preparation Sample measurement Solvent extraction Concentration/Dilution Filtration LC-MS DATA 0000747644 Page 9 of 14. Test Report. No. SHAEC1207176309 A03 Date: 18 Jun 2012 . Phthalates Testing Flow Chart 1) Name of the person who made testing: Elyn Yao 2) Name of the person in charge of testing: Rachel Zhang Sample cutting/preparation Sample measurement Solvent extraction Concentration/Dilution Filtration GC-MS DATA 0000747644 Page 10 of 14. Test Report. No. SHAEC1207176309 A03 Date: 18 Jun 2012 . HBCDD Testing Flow Chart 1) Name of the person who made testing: Gary Xu 2) Name of the person in charge of testing: Linda Li Sample cutting/preparation Sample measurement Solvent extraction Concentration/Dilution Filtration GC-MS DATA 0000747644 Page 11 of 14. Test Report. No. SHAEC1207176309 A03 Date: 18 Jun 2012 . PAHs Testing Flow Chart 1) Name of the person who made testing: Lisa Duan 2) Name of the person in charge of testing: Jessie Huang Sample cutting/preparation Sample measurement Solvent extraction Concentration/Dilution Filtration GC-MS DATA 0000747644 Page 12 of 14. Test Report. No. SHAEC1207176309 A03 Date: 18 Jun 2012 . TBBP-A Testing Flow Chart 1) Name of the person who made testing: Gary Xu 2) Name of the person in charge of testing: Linda Li Sample cutting/preparation Sample measurement Solvent extraction Derivatization Liquid-liquid extraction Concentration/Dilution Filtration GC-MS DATA 0000747644 Page 13 of 14. Test Report. No. SHAEC1207176309 A03 Date: 18 Jun 2012 . Sample photo: . SHAEC1207176309 A03 SHA12-071763.001 . SHAEC1207176309 A03 SHA12-071763.002 . SGS authenticate the photo on original report only . *** End of Report *** . 0000747644 Page 14 of 14.