ICPTest_242_242UAT pdf

ICP Test Report Certification Packet
Company name :
Littelfuse, Inc.
Product Series:
Barrier Network Fuse
Product #:
242 and 242UAT Series
Issue Date:
June 11, 2012
It is hereby certified by Littelfuse, Inc. that there is neither RoHS (2011/65/EU – recast of EU
Directive 2002/95/EC)-restricted substance nor such use, for materials to be used for unit parts,
for packing/packaging materials, and for additives and the like in the manufacturing processes.
In addition, it is hereby reported to you that the parts and sub-materials, the materials to be used
for unit parts, the packing/packaging materials, and the additives and the like in the manufacturing
processes, are all composed of the following components.
Issued by:
< Global EHS Engineer >
(1) Parts, sub-materials and unit parts
This document covers the Barrier Network Fuse, with clip RoHS-Compliant series
products manufactured by Littelfuse, Inc.
＜ Raw Materials Used
Please see Table 1
(2) The ICP data on all measurable substances
Please see appropriate pages as identifed in Table 1
Remarks：
Pb (lead) contained in the high temperature melting solder > 85% and is categorized as
exempt under section 7a of the RoHS Annex.
Form 585-047 Rev. A
1
2/21/06
Table 1: List of Raw Materials covered by this report
Total Parts
1
2
3
4
5
6
7
8
9
10
11
Raw Material Part Number
910-276
C610 (909-537)
4-1357 (497xxx)
11-0803 (497xxx)
091250
091251
692320
7132 (425672)
425904
8829 (425819)
425818
Raw Material Description
Cap
Body
Wire-99% Ni (497xxx)
Wire-Cu Clad Fe5842NiAg by Weight
Sand Filler
Sand Filler
Solder
Black Ink
Blue Ink
Green Ink
Red Ink
2
Page(s)
3-9
10-33
34-40
41-47
48-53
54-59
60-64
65-73
74-87
88-96
97-105
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75349 NO.l
75349 NO.2
"
*[+J*4,
. li 11 .li.,t\
c o m D a ni y, r : jr . r . : , 1 . : _ i , i f . i : , 1 1 , , 1 ;
Th3 6emd 3 igsd by6. conpa
abjeq b rems aid cofd to.s ror E
r.:a,i$
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(End or Repor!) *t
: r. ,.!, frllr!.
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Validi
ForQ
Please
Test Report
own
SGS
No. : CE/2012I14843ADare.2O12J02104Pagel.1o124
tll||Ill
CERAIVTEC
GIVBH
MULTIFUNCTIONAL
CERAI/IICSLUITPOLDSTMSSE
15 D.91207LAUF,GERMANY
ltltt]r
The following sample(s)was/u,€resubmiltsd and identifiedby/on behalfof the client as:
Sample Description
Stle/ltem No.
SampleReceivingDate
TestingPerjod
CERAMIC
c610
2012,01t30
2012J01| 30 TO 201Z 02t04
Te3tRe.ult(s)
: Pleasereferlo nextpage(s).
Conclu6ion
Lead,
: Bas€dontheperformed
testsonsubmitted
samples,
thetestresults
of Cadmium,
lvlercury,
Hexavalent
Cf(Vl),PBBS
andPBDES
comply
withthelimit6assetby
Ch.omium
RoHSDireclive
Annexll; recasting
200295/EC.
2011/65/EU
Sg|rad for||d
Cltorlcd Lborlbry-
T.Fd
comDafrAilB6;RE ,tRd-LXlAllHll lftlCt
!IAIA|
lq"1 )19{
"SFiAE
Th3dodm6dE6ebyfuconMy&bjedbi6Gengg|cddfooi3ds.s6pii6oveis43Eisb.on4wd
aadrsd tui i'no
t'lnld d6 kru6 doinoddroEi Adyhoderot hB tuhed
mt and
f sr rrE comp.nr'EE r.rspombrl'
"ih
comFry Atu sadoEs
. rodon torcsryor rslff€ton d rhe6ibd or sD
nd ofl.id.6 m.y e p,@dk
ih6 r ft or rtsiftmton
.*n, ;S-:HJ'Y
I iH::::gj;t.*t;:,$;;
'-;*,t^--
"
ro s. rd
r !6!a {Brts
***'*
Test Report
No.: CEJ2012/14843ADale| 201Z0ZM
Page: 2 o f 2 4
t]r||lrrfl||fllllt
CERAI\,ITEC
GMBH
MULTIFUNCTIOML
CERAITIICS
LUITPOLDSTMSSE
15 D.91207LAUF,GERIJANY
IeclBecc$GL
PARTNAMENo.l
Test ltem(s)
I
WHITECERAIVIC
lJnit
MDL
Method
R€ult
Limit
l{o.t
2
n,o,
100
2
178
1000
2
n.o.
1000
2
n.d.
1000
0.5
n.d.
mS/kS Withfeference
to USEPA3540C
0.5
n.d.
method.
Analysis
waspedormed
by
GC/MS.
mg/Kg Withreference
to uS EPA3540C
method.
Analysis
wasperformed
by
GC/|VS.
5
n.d.
0.01
n.d.
10
n.d.
Cadmium(Cd)
mS/kS With referenceto IEC 62321:2008 and
perfomed by ICP-AES.
Lead (Pb)
mg/Kg With referenceto IEC62321:2008 and
performedby ICP-AES.
lrercury(Hg)
mg&g Withreferenceto IEC62321:2008and
performedby ICP-AES.
Hexavalent
ChromiumCr(Vl)
mgikg Withreference
to IEC62321:2008and
pedormedby UV-VIS.
Polychlorinated
Biphenyls(PCBS) mgikg Withreference
to USEPA3g0C
(cAS No.:1336-3G3)
method.
Analysis
wasperformed
by
GC/rrs.
Polychlodnated
Terphenyls
(PCTs)
Polychlofi
natedNaphthalene
(PCNs)
oa
Alkanes,C1Gl3, chloro(Shoft
With referenc€to US EPA 3540C
ChainChlodnated
Paraffins)(CAS
method.Analysiswasperformed
by
No.:8553t0a-8)
GC/MS.
Pe|fluoroodanesulfonates
mgKs With referenceto US EPA 3540C:
(PFOS-Acid,
MetalSalt,Amide)
1996 methodfor PFOSContent.
Analysiswasperformed
by LC/MS.
PFOA(CASNo.:335{7-1)
m9Kg With referenceto US EPA 3540C:
1996methodfor PFOACont€nt.
Analysiswasperformed
by LC/MS(CASNo.:50{0-0) mg/kg With referenceto ISO 17226-11200$.
Formaldehyde
Analysiswas perfomed by HPLC/DAD.
Analysiswasperformed
by FTIRand
FLAMETest.
cmEm6, REest hElEielifidizliLbq.6fi-{s6-"
! . ? -" q r ' i
Er,]t&
fttrerdEE$dbyTconp'
I ohF d r.rr'r, 'n&nre'r
a{r]'d'do1's.!
e -.d w's'1 ary -016' d dBderuddad!e
tan*don ft6 a.B no ai h.r dod
comEry ary un&ibai srbEron bM
ori'iBrelon d b6 onbnr d.F
alnnr+nuunar-iI
q
10
3
n.d.
Negative
hr .
oodn.da Ti e oo@nofl @nd F sd
arapdciiv'rawd/firtd'rirr**Hmn:fiE
G
TestReport
Page:3 of 24
D e:2012102104
No.:CE/2012I14843A
Result
Test ltem(s)
Unit
Melhod
MDL
(CAS
BBP(Benzylbutylphthalate)
No-:85-68-7)
DEHP(Di-(2-€thylhexyl)
phthalate)
(CASNo.: 1'17-81-7)
DIDP(Di-isodecylphthalate)(CAS
No.:26761-40-0)
phthalate)
(CAS
DINP(Di-isononyl
No.:2855312-0)
phthalate)
(CAS
DNOP(Di-n-ociyl
No.:117"84-0)
(CASNo.:
DBP(Dibutylphthalate)
%
Withreference
to EN 14372.Analygs
was performedby GC/lVlS.
Withrofefenceto EN 14372.Analysis
wBspedormedby GC/lVlS.
With referenceto EN 14372.Analysis
wBspedormedby GC/IVS.
Withreference
to EN 14372.Analysis
rvasperformedby GC/MS.
Withreference
to EN 14372.Analysis
was perlomed by GC/MS.
0.003
n.d.
0.003
n.d.
0.01
n.d.
0.01
n.d.
0.003
n.d.
0.003
n.o.
0.5
n.d.
0.5
n.d.
0.5
n.d.
0.03
n-d.
0.03
n.d.
%
oa
y'Vith
Analysis
reference
to EN14372.
/vasperfomedby GC/MSl\Ionomethyl
dibromodiphenyl
mg/Kg Withreference
to USEPA8270D
methane(DBBT)
method.Analysiswasperformed
by
Go/tlls.
l\ronomethyl
mgikg Withrefefence
to USEPA8270D
dichlorodiphenyl
method.
Analysis
w€sperfomed
by
methane(Ugilec121)
GC/ttIS.
Monomethyl
tetrachlorodiphenyl mgikg Withrefefenceto USEPA8270D
(Ugilecl41)
methane
method.
Analysis
w6spefomedby
Go/tlls.
llll
|l]|||tllllll
CERAITTEC
GltlBH
MULTIFUNCTIONAL
LUITPOLDSTRASSE
15 D.91207LAUF,GERMANY
CERAI\/IICS
No.l
Limlt
u-74-2)
Organic-tincompounds
IributylTin (TBT)
IriphenylTin (TphT)
Halons
(CASNo.:353-59-3)
Halon-12'11
Halon-13o1
(CASNo.:75-63-8)
(CASNo.:124-73-2)
Halon-2402
mgikg Withrefefenceto DIN38407-13.
Analysiswas performed
by GC/FPD.
mgKs With reference
to DIN3840713.
AnalysiswEsperformed
by GC/FPD.
n.d.
mg/Kg with referenceto US EPA 5021
melhod.Analysiswas performedby
GC/MS.
mg/Kg With referenceto US EPA 5021
by
method-Analysiswas pertormed
Gc/tlls.
mg^g with refercnce
to us EPA5021
waspedormed
by
method.
Analysis
GC/tis.
redu€d..sdntur
comEfr [}ll B E$3! nE-L1l{91:!l:dzttfla
'mEn
a3 ndmsa
! 6_sd 4 bs
E
l Hd- lH4
-
l*lEii9 E
!.r dd*
<Bd4€
h.rr
i-*f,r
b r d or ib 'ftiwdo1
oits so {rhi
'dnffioi
tum ssEsm aii,ffi' nohbaiodcrm!
-ne b6rtuedori
comp.ny er mr6od&
a radoi
ta.ry o, tal6h6doi d rb 6ibd
or s
i "I f, I ft{.
d tE oodafl
n.d.
wLhdl rior k6
pomE! on d t6
;Bousd r.r 'do
a hrF. r Lbai /iurfi#JtE*$6nd4sct
TestReport
Pege: 4 d 24
Dale:2012102104
No.: CE/2012/14843A
rt|| tt]l
CERAIVTEC
GIVBH
LAUF,GERMANY
LUITPOLDSTRASSE
15D-91207
MULTIFUNCTIONAL
CERAI\/IICS
Test ltem(s)
Unit
Halog€n
(F) (CASNo.:
Halogen-Fluorine
14762-94-a)
(cl) (cAs No.:
Halosen-chlorine
22537-15-1)
(Br)(CASNo.:
Halogen-Bromine
10097-32-2)
(l) (CASNo.:
Halogen-lodine
14 24+81
MDL
Method
with ref€renc€
to BS EN 14582:2007Analysiswas performedby lC.
mS/kS Withreference
to BS EN 14582:2007.
Analysis
was performed
by lc.
mgKs With referenceto BS EN 14582:2007.
Analysiswaspedormedby lC.
mgKs r'Vithreference
to BS EN 14582:2007.
qnalysiswasperformed
by lC.
mg/kS
Result
No.l
50
50
n.d.
50
n,d.
50
n.o.
A3b€Bto3
AclinoliteICASNo.:77536-664)
Amosite(CASNo.:12172-73-5)
%
(CASNo.:77536-67Anthophyllite
5)
(CASNo.:12001-29-5)
Chry6otile
%
(CASNo.:12001-284)
Crocidolite
%
Tremolite{CASNo.:7753&686)
%
comD.frKJ AF.fl8n d H:8Rl{6,!
^i-ttlg(
t E-{R
Withreference
to EPA600/R-93/116
method.Analysiswas performedby
SM, PLMandXRD.
With referenceto EPA 600/R-93/116
method.Analysiswas performed
by
SM, PLMandXRD.
with refeence to EPA600/R-93/116
method.AnalysiswEsperformed
by
S[4,PL[4andXRD.
Negatave
Withreference
to EPA600/R'93/116
method.
Analysis
wasperformed
by
S[,],PL[,]andXRD.
Withreference
to EPA600/R-93/116
method.Analysis$raspedormedby
SM,PL[,]andXRD.
Negative
Withreference
to EPA600/R-93/116
method.AnalysiswEsperfomed by
SNl,PLNIandXRD.
Negative
l_" rE/r:
Negative
Negative
Negative
l"rJ n E{.
M€'rbqod.al'.€.b.d1qu
'miirnon or I rii ly. knnnfr€ron
end inld cds r$u6 dornd 6eF n Ad ho der or his dodmd
d.lftdi!'fti@lonf|rad#i
Fnldonbm.^esnoaida'
ndtr and od'G.tr3 ida, bs.6ieddi
a1 ruuroda-d a Fdoi,o$ry
.mFry
o.Elserol
d rhs @-6a o' I
effinr+Irror/rs|laa%|
tded
that into
' q!!g1ryr!:: ! li ll!'l5!:l?! NqrdF c! r'E{ / rirlrnsirL**FErn}t'n
l]l
Limlt
Test
Report
24
Pase:5of
No.: cE/2012/14843A
Date-2o1zo2to4
|ll
CEMMTEC GMBH
15 D.gl207LAUF,GERMANY
I\4ULTIFUNCTIONAL
CEMMICS LUITPOLDSTMSSE
Test liem(s)
Sumof PBBs
Monobromobiphenyl
Dibromobiphenyl
Tribromobiphenyl
Tetrabromobiphenyl
Pentabromobiphenyl
Hexabromobiphenyl
Heptabromobiphenyl
Oclabromobiphenyl
Nonabromobiphenyl
Decabromobiphenyl
Sum of PBDE3
Monobromodiphenyl
ether
Dibromodiphenyl
ether
Tribromodiphenyl
ether
Tetrabromodiphenylether
Pentabromodiphenyl
ether
Hexabromodiphenylether
Unit
MDL
lllethod
5
With referenceto IEC6232112008and
mg/Kg perfofined
by GC/MS.
5
5
5
5
5
5
5
5
|llt
R€sult
No.{
n.d.
n.d.
n.d.
n.d.
n.d.
n.d.
n.d.
n.d.
n.d.
n-d.
n.d.
5
5
5
5
5
5
n.d.
Heptabromodiphenyl
ether
5
n.o.
Octabromodiphenyl
ether
Nonabrcmodiphenyl
ether
5
5
Decabrcmodiphenyl
ether
5
n.d.
n.d.
n.d.
3
n.d.
AZO
to LFGB82.02-2.
1):4AIIINODIPHENYL(CASNo.l mg/kg Withreference
Analysiswasp€rfomedby GC/MS.
92-67-1)
m9/K9 With referenceto LFGB82.02-2.
2)i BENZIDINE(CAS No.: 92-87by GC/lvlS.
Analysiswasperformed
5)
3): +CHLORO-O-TOLUIDINE mg/Kg /Vith referenceto LFGB82.02-2.
Analysiswas performedby GC/MS.
(CASNo.:95692)
(CAS
4):2-MPHTHYLAIIINE
No.:91-59-8)
to LFGB82.02-2.
msftg with reference
Analysiswas perfo.medby GC/l/lS.
to LFGB82.02-2.
(CAS mg/kg with reference
5): O-AIVINOMOToLUENE
Analysis\ /as performedby GC/MS.
No.:97-5&3)
a;;;;hi
rtErca Di'-t+4r{.4-6HEc
(4d-r8..".:'-}
n,o,
n.d.
n.d.
n.d.
n.d.
3
3
n.d.
3
n.d.
3
n.d,
ro r)rl&"
inhel!lEI.'*i.d*d.dno'-*""d."**dcoturd;s
irii6iim-"j"in-inii*ij'iiilb''bnF.''.'[email protected]|fma.Doi!as1g{ws!sods4€i!g
]ii;;'6iifoidhnic!!aidiiirnidoili$@dmdMdn:ii;h;bl's];di{'md,i'ddmdi
ii
bs In !d c.a.n6rcr;i
i , i i , l i n d r,;"
,nii"e-- -r *"".i
;1;;
;-o
d, r*' "qtu ro d, odotu Ln6 h. t'nsdoi ooer.ma
baea d b 3'* * d ' r d;;:;;;';;;;l;
.o.oan, ay ..arho-a ,! s d-
-6{0''esb6d*w43@n|f!-!j'dgldg::ll
6cFaf,do.o!*rcdd6.dd
ni s [email protected] @nr b' €
doan"i4,"; ad a.o ot
llllll
Limit
1000
'1000
TestReport
No. ICE/2012114843ADaie:2O1Z0ZO4 Paoe:6 ot 24
tl]tI|tt
CERAIVTEC
GITIBH
MULTIFUNCTIOML
CERAIIIICSLUITPOLDSTMSSE
15 D-91207LAUF,GERIVANY
Testltem(s)
Unit
6)i 2'AMINO-4-NITROTOLUENEmgftg
(CASNo.:99-55.8)
7): P-CHLOROANILINE
(CASNo.: mdks
10647-8)
8): 2,4-DIAMINOANISOLE
(cAS
m9Kg
No.:615-05-4)
mg/Kg
9): 4,4L
DIAIIIINODIPHENYLMETHANE
(CASNo.:101-77-9)
10)r3,3'-DICHLOROBENZIDINEmg/kS
(CASNo.:91-9+1)
11): 3,3'-DIMETHOX/BENZIDINEmgikg
(CASNo.:11990-4)
12):3,3!DIMETHYLBENZIDINE mg/kg
(CASNo.:11993-7)
MDL
Method
With refercnceto LFGB82.02-2.
Analysiswas performed
by GC/MS.
With reference
to LFGB82.02-2.
Analysisw€sperfomedby GC/lVlS.
With reference
to LFGB82.02-2.
Analysiswasp€rformed
by GC/|\IS.
With reference
LFGB
to
82.02-2.
Analysiswas performedby GC/I\IS.
3
No.1
3
n.d.
3
n-d.
3
n.d.
Withreference
to LFGB82.02-2.
Analysiswasperformedby GC/MS.
3
n.d.
With relerenceto LFGB82.02-2.
Analysis\ /as performedby GC/MS.
3
n,o,
3
n.o.
3
n.d.
3
n.d.
3
n.d.
mgftg Withrcfercnceto LFGB82.02-2.
Analysiswasperformed
by GC/MS-
3
n.d.
mgKg With reference
to LFGB82.02-2.
by Gc/lvls.
Analysiswas performed
3
n.d.
3
n.d.
3
n.d.
3
n.d.
3
n,d.
Withreference
to LFGB82.02-2.
Analy6iswasperfomedby GC/MS.
'|3):3,3-DlMETl-lYL-4,4'msfts With referenceto LFGB82.02-2.
DIAMINODIPHEI.IYLIIIETHANE
Analysiswaspertormed
by GC/lVlS.
(CASNo.:838-8&0)
(2]!IETHOXY- mg/Kg A/ithreference
14):P-CRESIDINE
to LFGB82.02-2.
(CASNo.:
5-METHYLANILINE)
Analysis
waspedomedbyGC/l\Is.
120-71-8)
(215):4,4'-[,IETHYLENE-BIS(CASNo.:
CHLOROANILINE)
101-14-4)
(CAS
16):4,4LOXYDIANILINE
No.:101-80-4)
(CAS
17):4,4'-THIODIANILINE
No.:13965-1)
(CASNo.:9$
18):O-TOLUIDINE
Result
mg&g With referenceto LFGB82.02-2.
||ttll!t
Limit
Analysiswas performedby GC/MS.
mg/Kg
5s)
Withreference
to LFGB82.02-2.
Analysiswasperfomedby GC/IVS.
19):2,4-TOLUYLENEDIAMINEmg/kg With .eferenceto LFGB82.02-2.
(CASNo.:95-80-7)
Analysiswas perfonnedby GC/MS.
20):2,4,5-TRIItIETHYLANILINE mg/Kg
(CASNo.:137-17-7)
(CAs No.:9G
mg/kg
2'l): O-ANISIDINE
04-0)
With referenceto LFGB82.02-2.
Analysiswasperfomedby GC/lVlS.
y]/ith.eferenceto LFGB82.02-2.
Analysiswas performedby GC/MS.
inALF,{rr!-i-Eeaa
tdd- iMt, lg6"+_I T lil:' u?
fi;6d,n;dB;;;'iti;@ind]li'ibd.o'i..fgeicsdnf.,*rn6qrbilode,'6|.d.o'Gqus
ed io,asdtr'ctud6.r.n!
*tidri,Tds.{cdmiomb-6d
;i;bn;]ni'i;;.ii'nd6'ilnijii'nd;fusd.mn60DDnAilhdde.dFEoodnaa''.oIsdF,''ft
-€conFnvt{ts@o13b"t'
-mdor
ary
hs m' d tr! 'nbii$ron 6k and*'rin h 'redlrsrtr
adb.cpdLddrcpl|1tr|
Jiii'i''neton a L* ontoni;ii,pp*Eme t 'h s [email protected] k mrdd sna or*dare mai bo prcedd
ii;i'inil;lii;dn;;a;G;;;1iiiriiry
];i1ira&eD6ri^;i
I
iiij;j;;:;;;t
'l;idD;;;t
i;;J;
d3rcE
!t ea tu
r$JrLfi*l[**l!6tfiflffi*tr
1.p.n6-bs
Test Report
No. : CE/2012/14843A Dele : 201210204 Page | 7 of 24
l]|||lll
CERAMTEC
GI/lBH
15 D.91207LAUF,GERMANY
I\4ULTIFUNCTIONAL
CERAMICSLUITPOLDSTRASSE
unit
T€st ltem(s)
22):P-A[,IINOAZOBENZENE
(CASNo.:60-09-3)
(CASNo.:9$
23):2,4-XYLIDINE
68-1)
(CASNo.:8724):2,6-XYLIDINE
62-n
CFC's(Chlorofluorocarbons)
Group I
luorccabonl 1 (CASNo.:
Chlorof
75-694)
(CASNo.:
Chlorofluorocarbon-12
7171-8)
3
ReBult
No.1
n.d.
3
n.d,
MDL
Method
msfts With referenceto LFGB82.02-2.
by GC/lVlS.
Analysis
was performed
to LFGB82-02-2.
mg/Kg /Vithreference
Analysiswas p€rformedby GC/MS.
mdks Withref€renceto LFGB82.02-2.
by GC/MS.
Analysiswas performed
ll
llll
Limlt
3
mg/kg With referenceto US EPA 5021
method.Analysiswas performedby
GC/MS,
to USEPA5021
mg/Kg Wth reference
n.d.
method.Analysiswasperformedby
Gc/rlls.
to uS EPA5021
13 (CASNo.: MEKg with reference
Chlorofluorocalbonl
wasperformed
by
method.
Analysis
76-13-1)
GCiMS.
n.d.
luoroca|bon-1
14 (CASNo.: mgikg With referenceto US EPA 502'1
Chlorof
method.AnalysiswaspedormedbY
76-14-2)
GC/MS.
to Us EPA5021
115 (CASNo.: mg/Kg Withreference
Chlorofluorocarbon-
'|
n.d.
1
n.d.
1
n.d.
1
n.d.
1
n.d.
bY
Analysis
wasPertormed
method.
6C/MS.
7&'ts-3)
Grouplll
3 (CASNo.:
Chlorof
luorocarbon-l
7U72-9)
mg/kg With .eferenceto US EPA 5021
method.Analysiswas performedbY
GC/MS.
(CAS
m9Kg
with referenceto us EPA 5021
I1
No.:
Chlorofluorocarbon-1
method.Analysisvrasperformedby
354-56-3)
GC/|\,IS.
to IJSEPA5021
Chlorofluoroca6on-112 (CAS No.: mgKg Withreference
mehod.Analysis\o?sperfomedbY
GC/tVlS.
7B-12-0)
Chlorofluorocarbon-2l1 (CAS No.
422-784)
n,o.
mg/kg Wilh feferenceto US EPA 5021
method.Analysiswas PerformedbY
GC/t\4S.
r5!E?;':r"
YisfPlT
?':;'il*'Tl"il]lli*:::]]:il :"*'"-**-'"-"-"
"f::Fri
;:li";iy*T
B#;rftETtisi4u
?ilrl",il
ffffi**;"lu*:ffir*"ieB,:.mr""*r*:[''*'inmv""r*irf#ilfi€sitr;:t$ijii"{s#xpa#
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i;6;;:!,;uft
d; r;,oi'"
t . . . u , g . . * " ' ' o ' r . r ' g . ; ; 6 ; ; d n ' " d * r g d * " ' b . 6r;;;"n;;id'ialia
a * -'.j;:;;;;;
s",r ri'tdo'
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TestReport
No.: CE/201214843ADale:2o1Z0AU Page:8 or24
l:]
CERAMTEC
GIVBH
't5 D-91207LAUF,GERMANY
ItIULTIFUNCTIONAL
CERAlrlcS LUITPOLDSTMSSE
Test ltem(6)
(CASNo.:
luoroca6on-212
Chlorof
3182- -1)
Unit
MDL
ll/lethod
to uS EPA5021
mdks Withreference
lrn
Result
No.l
n,d,
tllllll
Limit
Analysis
wasperfomed
by
method.
GC/MS.
3 (CASNo.: mg/Kg With referenceto US EPA 5021
Chlorofluorocarbon-21
method-Analysiswas performedby
235,L0e5)
GC/ttIS.
(CASNo.: mgKg With referenceto uS EPA 5021
Chlorofl
uorocarbon-2'l4
method.Analysiswas performedby
292sr31-0)
GC/MS.
luorocarbon-2l
5 (CASNo.: mgikg With referenceto L,SEPA 502'l
Chlorof
method.AnalysiswaspedormedbY
425943-2)
GC/MS.
to uS EPA5021
Chlorof
luorocarbon-21
6 (CASNo.: mg/Kg Withreference
method.Analysiswasp€rformedby
661-97-2)
n.d.
n.d.
1
n.d.
mgKs With referenceto uS EPA 5021
method.Analysiswas perfomed by
GC/MS.
1
n.d.
With feferenceto uS EPA 5021
method.AnalysiswEsperformedby
GC/t\4S.
mdks With refeence to US EPA 5021
method.Analysiswas performedbY
GC/MS,
1
n.d.
1
n,o,
mg'ks with referenceto us EPA5021
1
n.d.
1
n.d.
GC/l\rs.
7 (CAS No.:
Chlorofluorocarbon-21
422-86-6)
CHCa(Chlorinalehydroca.bon)
(CAS
1,1,1,2-Tetrachloro€thane
No.r630-20-6)
(CASNo.:
1,1,1-Trichloro€thane
71-556)
(CAS
1,1,2,2-Tetrachloroethane
No.:79-3+5)
(CASNo.:
1,1,2-Trichlorcethane
7900-5)
mgKg
bY
waspedormed
method.
Analysis
GC/MS.
to USEPA5021
mg/kg Withreference
method.AnalysiswasperfomedbY
GC/MS.
to USEPA5021
Withreference
bY
wasPerformed
Analysis
method.
(CASNo.:751,1-Diclloroethane
mg/Kg
(CASNo.:751,1-Dichloroethene
GC/|VS.
mg/Kg With referenceto IJS EPA 5021
s+3)
3s)
n.d.
method.Analysiswas PerformedbY
GC/|VS.
""" *- *"*'*
?.gT+:ex;1:FdT6l.f
8"*affirli;sffr':!t'i?+riFs.t'li::E?'"iri:'13i:
ib::T::a:":1:
::,T"
.morr;dti
r*bFbGq€E
'#.?n"i*inni#noi*i*t*b]66d'.tcodm!b,Ei.:i;;'d;;;6iw4.;'.''n
il"i].i,i.ii"ni.ii'i.ini"ii'i&tona"ai"d@,$6dd"*b.1";.;;;;;b';mda'1'''e"9dFai'
*r q-'r"r
i"i =n: j;nryt
r"a"'#te-a
n tr' do' oM r
*'pd'dsod
-"''-.*d;'a"'"j'iJ
;:'laa *6 n'@s rui € d@dd 't traikd 'asr db' &
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Test Report
Paqe:9of24
No. : CE/201214843A Date:2012,0i,M
rrrfirnl||
CERAIVTEC
GIlIBH
15 D-91207LAUF,GERMANY
MULTIFUNCTIONAL
CERAIVICSLUITPOLDSTMSSE
Testltem(s)
Unit
(CASNo.:
1,1-Dichloropropene
563-5&6)
'1,2,3-Tridlloropropane
(CASNo.:
9618-4)
(CASNo.:
1,2-Dichloroethane
1O7-06-2)
MOL
ilethod
Result
No.l
mg/kg Withreference
to USEPA5021
n.o.
Analysis
wasperformed
by
method.
GC/MS,
MEKq Wiihreference
to uS EPA5021
method.Analysiswasperfomedby
GC/MS.
n.d.
mg/Kg With referenceto US EPA 5021
n.d.
method.Analysis\ rasperfomed by
Gc/ltlS.
(CASNo.:
1,2-Dichloropropane
msr'(g With refefenceto US EPA 5021
method.Analysiswasperformed
by
78-87-5)
GC/MS.
(CASNo.:
l,SDichtoropropane
mg/Kg With referenceto US EPA 5021
method.Analysis\oasperformedby
142-28-3)
GC/MS.
(CASNo.:
2,2-Dichloropropane
mg,Kg Wth referenceto US EPA 5021
method.Analysjswas performedby
594-20-7)
GC/MS.
Carbontetrachlonde(CAS No.:
mg/kg With referenceto US EPA 5021
56-235)
method.Analysis$/asp€rformedby
GC/ltlS.
(CASNo-:75-00-3) mgikg With .eferenceto US EPA 5021
Chloroethane
method.AnalysiswEsperformed
by
GC/|VS.
(CASNo.:67-66-3)
Chloroform
m9K9 With referenceto US EPA 5021
method.Analysiswasperformed
by
GC/MS.
(CASNo-:74-87- m9KS With referenceto US EPA 5021
Chloromethane
3)
method,Analysiswas performeclby
GCiMS.
(CASNo.: mg/Kg Withreference
cis-1,2-Dichloroethene
to USEPA5021
n.d.
n.d-
n.d.
n.d.
n.d.
n.d,
n.d.
method.Analysiswasperformedby
GC/MS.
15G59-2)
(CASNo.: mg/Kg With referenceto US EPA 5021
cis-1,3-Dichloropropene
10061-01-5)
melhod.Analysiswes performedby
GC/t\4S.
n.d.
pdued&€pl'nfujmhodpndd
i-h'.on
cohpaa
^iy !i'6od;j
Bsddh?n
o b,6r 6i toaery tr hrsheb
d h6 trhr
*ydeddroo*readlq{std
o
or apts
qrdF
.M ta wd / ii:lld,|ilt**FmliEffitri
:]l
Limit
Test Report
No.:CU2O1Z14U3A Dale 201210i,04 Page: 10 of 24
t]|lrr
CERAI/ITEC
GIlIBH
LUITPOLDSTMSSE
15 D-91207LAUF,GERIJANY
MULTIFUNCTIONALCERAI\'ICS
Tost ltem(s)
(CASNo.:
Hexachlorobutadiene
8748-3)
unit
MDL
llethod
mgKg Withrefercnce
to uS EPA5021
by
method.Analysiswasperfo{med
GCiMS.
to Lls EPA5021
lMethylene
Chloride(CASNo.:7+ mg/kg Withreference
by
method.Analysiswaspertormed
0$.2)
GC/l\rs.
(CASNo.:127- mgKg Withrefercnce
to USEPA5021
Tetrachloroethene
method.Analysiswasperfomedby
184)
GC/MS.
msikg With referenceto L,S EPA 5021
ttang1,2-Dichloro6thene
{CAS
No.:15G60-5)
(CAS
trans-l,3-Dichloropropene
No.:10061-02-6)
(CASNo.:79Trichloroethylene
014)
method.Analysiswaspedormedby
GC/MS.
mg/Kg With referenceto US EPA 5021
method.Analysiswas performedbY
Go/tlls.
mgKg With rcferenceto IJS EPA 5021
method.Analysiswas perfomed bY
GC/rVlS.
Result
No.l
n.d.
|ll|rlr
Limit
n.d.
n.d.
n,d.
n.d,
1
n.d.
1
n.d.
1
n.d.
1
n.d.
1
n.o,
HCFcs
(llydrochlorofiuorocarbom)
HCFC-21(CASNo.:75-43-4)
HcFc-22(cAs No.: 7545{)
HCFG3l (CASNo.:593-7G4)
mg/Kg With referenceto IJS EPA 5021
method-Analysiswas performedbY
Gc/lrlS.
mg/Kg With rcferenceto uS EPA 5021
melhod.Analysiswas perfomed bY
Go/tlls.
to lJs EPA5021
mgKg with rcference
melhod.AnalysiswasperfomedbY
GC/l\,IS.
(cAs No.:35,4-14-3) msn(gWithrcfef€nc€to USEPA5021
HCFo12'1
bY
method.Analysiswasperformed
GC/tus.
(CAsNo.:3*21-2)
HCFG122
mgrs
to USEPA5021
Withreference
bY
wasPedomed
Analysis
method.
GC/MS.
n.d.
*-"f
stf,i"S"13::89';'.i:'rs,":g"r",F:'r'..i:iEr8ffintr8yq;HlErTftf
ill1:-:1"::--':,::"'""***'*'*
'i,?i;d,r.a !;dbyb6hE
y*b@bbk..
c-d *.d;
i lti;it
ds'bcorim!'0,e6ft
iA;;
:i,itn,iar'Jniii.innft-m"*oi"ao"-*"a"-to-.*"'i'nd;;'F,;-..-''*d*drd";;:;;;;;;i;;
d n ; ; : ; ; ; ; i ; ; : ; ; a ; F ' i i i . , . 6 d c | f l s ' M d m . , a " y € c d n s n Y ' ! d . l . : p o 1 6 b ' i t } -ir err'
@;.;3
. -"....
tr. 8a...0
i;sd m 'n o.€r,i
o n d t . @ +"-*n
{dr4
_a'6
a @ n l D m a . , T a l d b E t o ' i b w d ' 5"o,s*"
n ir
6-d b trpq"-ed
"h113fr.{;*'""".HT:iS X
"€er
I lLmfrtE*FffinfiRtfi
TestReport
No.: C9201214843A OaIe:201210204 Page:11of 24
llfir
CERAIVTEC
GIlIBH
15 D-91207LAUF,GERMANY
MULTIFUNCTIONAL
CERAIIIICSLUITPOLDSTMSSE
Te3t lt€m(s)
(CASNo.:30G83-2)
HCFG123
Unit
MDL
ilethod
Result
No.{
n.d.
to uS EPA5021
mgKg Withreference
method.Analysiswasperformedby
GC/tMS.
(CAS
to USEPA5021
HCFC-124
No.i2837-89-0) mg/kg Withreference
by
method.
Analysis
wasperformed
GC/MS.
n.d.
mgKg With referenceto US EPA 5021
method.Analysiswas perfomed by
GC/l\,1S.
(CASNo.:1649-0&n mg/kg With refe.enc€to US EPA 5021
HCFC-132b
by
method.Analysiswasperformed
GC/MS,
to USEPA5021
(CASNo.:75-88-7)
mg/Kg Withreference
HCFC-133a
n.d.
(CASNo.:1717-006) mg/Kg with referenceto US EPA 5021
HCFC-141b
method.Analysis\Nasperfomod bY
GC/MS.
mdts With referenceto US EPA 5021
HCFG142b(CASNo.:7568-3)
by
method.AnalysiswEsperfoamed
GC/MS.
HcFc-221(cASNo.:422-26-4) mg/kg With referenceto US EPA 502'l
bY
m€thod.Analysiswas performed
GC/t S.
(CASNo.r42249-1)
mg/Kg With referenceto US EPA 5021
HCFC-222
melhod-Analysiswas performedbY
n.d.
HCFG131(CASNo.r35$28-4)
n.d.
method.Analysiswasp6rformedby
GC/tS.
1
n.d.
'I
n,d,
I
n.d.
1
n.d.
1
n.d.
Gc/rlls.
(CASNo.r422-526)
HCFC-223
mgKg
With referenceto IJS EPA 5021
melhod.Analysis\ /as performedby
GC/|\,IS.
(CASNo.:422-54-8) mgKg Withfeference
to USEPA5021
HCFG224
bY
method.Analysiswasperformed
GC/tVlS.
to USEPA5021
(CASNo.:422-56-0) msftg Withreference
HCFG22sca
bY
wasperformed
Analysis
method.
GC/MS.
n.d.
iilit f&iFi#riE:ii:E8fdJrjie'€BlYs"'r,Fi:*r51':*dI'sEi':'or:nrF6::i-::1::l
l"*^'*-*-"*
asq.dregL6n.?!omsd..66e1ado!..adaI'!b€olELg'
;;;;;H.;.;t-d"*..ft!'.idhr"-.-dc*d'6-b#;i;6;,n'i's*4!or,sf.m
; i ; ; d ; n ; i * d - - | v * " * h 1 " " r . " e c . l .".n* .r -' a. i-i -] r- y* ei d. .; "c*o"a, i;''i;"!.do.6€dsdf gs od |E, vt dl b, i a d s o ' ft'"*r'nrrc'b'Fru
'"
*;"iihr;tui
r" or s,r *' *s
ldr
':;"@i':ri;in
- * ". -;:E;;;;
md ftnds
fuY b Pm
a rred. vr.dii
/ ttitirfiJ|x*mBndst6t
l
lllll
Limit
TeSt
RepOft
No.:cs201214843ADare:2o1zozo4Pasetl2ot24
tl
CERAIIITEC
GITIBH
MULTIFUNCTIONAL
CERAIVIICS
LUITPOLDSTMSSE
15 D-91207LAUF.GERITIANY
Test ltem(s)
Unit
MDL
Method
(CASNo.:507"55-1) mgKg Withreference
HCFC-22scb
to USEPA5021
method.Analysis\oasperfomedby
GC/t\4S.
-87-8)
(CAS
HCFC-226
No.:431
mg/kg Withreference
to USEPA5021
wasperformed
by
method.
Analysis
Go/tlls.
HCFG231(CASNo.:421-94-3)
m(/kg Withrefercnce
to uS EPA5021
method.Analysiswasperformed
by
GCiMS.
(CASNo.:460-89-9)
HCFC-232
mg/Kg Withreference
to USEPA5021
melhod.Analysiswasperformedby
GC/t\4S.
HCFG233(CASNo.:7125-84-0) m9ks Withrefercnceto US EPA5021
(CASNo.;666-27-3)
HCFC-241
by
method.Analysiswasperformed
GC/MS.
mg/Kg With referenceto US EPA 5021
method-Analysiswas performedby
GC/t S.
mgKg With rcferenceto US EPA 5021
method.Analysiswas performedby
GCA4S.
to USEPA502t
mg/kg Withreference
(CASNo.:460-63-9)
HCFC-242
mgKg
HCFC-234
{CASNo.:425-94-5)
HCFG235(CASNo.:46G92-4)
HCFS243(CASNo.:46G69-5)
Resull
t{o.'l
r mrrll|l
Limlt
n.d.
n.d.
n,d.
1
n.d-
1
n.d.
1
n.d.
1
n,d.
1
n,d,
1
n.d.
wasperformed
by
method,
Analysis
GC/MS.
With rsfefenceto US EPA 5021
method.Analysiswas perfomed bY
GC/MS.
mgfts With rcfefenceto US EPA 5021
method.Analysiswas performedbY
1
GC/tVrS.
HCFG244
(CASNo.:42141-0)
HCFC-251
msas Withreferenceto uS EPA5021
n.d.
by
Analysis
wasperformed
method.
GC/MS.
to USEPA5021
mg/kg Withreference
bY
method.Analysiswasper{ormed
GC/MS.
n.d.
":1::: - ll-:"'*-***""*
H#n#Hyqgg1:iffdf
+rsfi;T,.ffi8flq;i:"r."fi-tq"r'
jrj"er***:n*,f*njtru"rln*:."sltr,s:sr.".1x-rffrf*rrlgirsi"",Lrx$;"'trili:'#*tr"'r#ii**'".o*;
EUs o.rne t6c' 'ii; hod.'d rF .oor.a teied rar 'r'io
i"iu'.,i,i mnrii
oo iiddr
t i , i i i . ' . . g ' n r o - ."i'i#i-m^
* - ' - o . r i n ' h . ' n | E d c | 5 1 s , d d o T : ; i ' ; i . i ' " " J i " d . g p o * b ' . ' o -' ti s' oco| €d nn hi ' d6 '110- ', B
. d ' m o a m 4 m . 6 @ p rn a l
aad'ed
€maffqoo.e_'
r;;;;n';;ou_od
rs ns.
bilru;ad
36rdu 4d on ideB rut b p@ork
bs'ry d dr ier m d b.6nbdi;;F-;;at
cam;ry Ary-.dtu;.dEErm.
b he tuhd 'ns( d b' a*
ryrr+! crr ri wd / firlfisrlE+FmnERt*
TeSt
RepOft
Date.2o1zozo4
Pase:13or24
No.rcE/201214843A
|l] ||ttl[Ilrt]r
CEMMTEC GMBH
IVIULTIFUNCTIONAL
CERAMICSLUITPOLDSTMSSE
15 D-91207LAUF.GERMANY
Teetltem(s)
(CASNo.:819-0t!1)
HCFC-252
HCFC-253
{CASNo.:460-35-5)
Unit
Resull
MDL
Mothod
mgikg with refefenceto US EPA 5021
method.Analysiswaspedormedby
GC/MS.
mgKg Withreference
to USEPA5021
No.l
1
n.d.
1
n.d.
method.Analysiswasperfomedby
GC/MS.
(CASNo.:420-97-3)
HCFC-261
mg/kg Withreference
to USEPA5021
method.
Analysis
waspedormed
by
GC/|VS.
(CASNo.:421-02-03) m9Kg Withreference
HCFG262
to USEPA5021
method.Analysiswasperfotmedby
GCiMS.
(CASNo.:430-55-7)
HCFC-271
Limit
n.o.
n,d,
n.d.
mg/Kg With referenceto US EPA 5021
method.Analysiswas perfomed by
GC/MS.
= 1000ppm
1. mg/kg= ppm : 0.1wro,6
2. n.d.= NotDetected
3. MDL= llethod DetectionLimit
4."-"=NotRegulated
5- * = Qualitative
analysis(No Unit)
6. Negative= lJndeteclable/ Positive= Detectable
7. Asbestos: Negative= "< 1.0%", Positive= "> 1.0%"
PFOS Reterence Information : POPS- (EU) 757/20'10
productsor
above0.001%(10ppm),in s€mi-finished
or preparations
in conc€ntrations
OutlawingPFOSas substances
in textilesor othercoatedmatedalsabove1ug/m2
adiclesor partsat a levelabove0.1%(1000ppm),
'ntrBb3l€Fntt'01ylo.h.qd
cdmdi!kJr
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A;;;i#';€!s;;;'atii"d
brd dntr+b &d@ b-!-' {d c"-ft-, h' ii;;;;
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i;;ft;d;
rbtilt'. hdanMata'iii"d i'iir;liai(n ''is ddlrei iDrein it; i'di* t h€ demi, 'isd{si ba iro
ftled'B'fumdmfxflo*o:1l€|fi.3dL.dlBl1ffgi!nyD.!mpa1yss€ceo'3'b|i,Gb
ft6 d*rsd e..d ba F
re
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or $h edm$r ts m r[{ur sd
. i.dbi; hosry d h]!'idi
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4 hlts .lq,rawd / FirLrrirrd*Erdrifrffirs
Test Report
paoe: 14 of 24
No.: CE/201214843A Date:201i,02t}4
CERAMTEC
GMBH
MULTIFUNCTIONAL
CERAIJICSLUITPOLDSTMSSE
15 D-91207LAUF,GERIJANY
t]
tl| [ttttlrl
1 ) Thes€sampiesweredissolved
totallyby pre-conditioning
meihodaccording
to betowttowchart.
( Cf'lest methodexcluded)
yang
2) Nameoflhe personwho mademeasuremenl:
Climbgreat
3) Nameoflhe personin chargeof measurement
TroyChang
Samplelvleasurement
Aciddigestionby suitableacid
clepended
on differenlsample
mateial(as belowtable)
Microwave
digeslionwith
HNO/HCI/HF
Heatlo appropriate
temperalurelo exiract
Cool,tilterdigesiate
AlkaliFusion
HCllo dissolve
ICP-AES
SampleIVaterial
throughfilter
Add diphen9-carbazide
for
DigestionAcid
Steel,copper,aluminum,solder
Aquaregia,HNOr,HCl,HF,H,O,
Glass
HNO3/HF
measurethe absorbance
Gold,platinum,palladium,
ceramic
Aquarcgra
at 540nm by UV-VIS
Silver
HN03
Plastic
HrSO4,HrOr,HNO3,HCI
Others
Any acidlo totaldigestion
[email protected]
co.Dar t? / B l ;?!i .rlRA1l Rl6?ldlSt,&AlF? 4E- 1144- "i*EjAl
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TestReport
No.: C9201214843A D3l.e:201210?,04Paoe:15 ol24
CERAIIITEC
GITIBH
MULTIFUNCTIOML
CEMI\4lCS LUITPOLDSTMSSE
15 II91207 LAUF.cERltlANY
t][Ilmfirllltl
Analyticalflow chan of Soxhletextracgon(LCIMS)procadure
a
r
Nameoflhe perconwhomademeasurementRomanWong
TroyChang
Nameof lhe perconin chafgeof measurement:
I Test lten3: PFOS/PFOA' Benzotriazole)
pretrcatmenuseparation
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I
Data
comDafr
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ooomsds.t trw $'@n/ddnE
@!rn a.yrredd!dcmrdad!Hhi
l;-{rrdn <isdd
dir€'
[email protected],
.nd drsdon!
d edon! une
Lnd u.
b. hns.dori
[email protected]
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No.:cEt2o12t14843A
24
Date.2o12to2to4
Pase:16of
RepOft
CERAMTEC
GMBH
I\4ULTIFUNCTIONAL
CERAI/IICSLUITPOLDSTMSSE
15 D-91207LAUF.GERMANY
Chlorinated Flamc retardant analytical flow chart
1) Nameoftheperson
whomademeasurcment:
BaryTseng
2) Nameoftheperson
in chaeeof measurenent:
TroyChang
I
r
Refercnce
method:
USEPA8270D,
USEPA3540
Teslltems:PCBS,
PCNS,
PCTS,
ltlkex,Ce MCCP
Data
C o m o a n h lq F e s r ' n E ; g F l { ? , s : i z t s , r E ! .
nbrond16rq'T*rnelonsrd
i
rn-I&
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pr€13)
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" ilr"q :r' I "rn E{.
rfy
rh comFny6 de 4o$
'bi,v
rdbEpdl€d3cpli1fu|
ll|l|t
[|rrlr|r
Test
No.: cE/201214843A
Date:2o1zo2!o4PasetlTof24
Report
|l][t
CERAMTEC
GMBH
ItIULTIFUNCTIONAL
CERAMICSLUITPOLDSTMSSE
l5 D'91207LAUF,GERMANY
Analysis flow chart for delerminalion of PVC in matorial
r
I
GinnyChen
Nameoflhe personwho mademeasuremenl:
Nameofthe personin charceof m€asurcmentr
TroyChang
Sampleanalyzedby FTIR
Chec* wave-numberof C-Clbonding
i n s s b { D F n ' $ e l o n ] y l o l h € & o p l @ d u d r e p t i f u | , d o d p i d " r i
'nEryrilTEl,&sj
,{HAl"i*l49l1li"E.:&flAE lEd- kl,l1, \.13 til
lq! llCS
rnhd€um$tlaig.dby1h6c0np.ry!ub]6dbbGsmBcodlon6ds
blddbr.-..nd cf d !0.Eb Er*n
-.*".;;i: il:|
:.*:ij;*.)T.i."'"#',H.*-*;*ii"- '
" """-'*','
t!l||r
Test Report
No. : CE/2012l148434 Dai€.2O1ZOZO4 Paoe: 18 of 24
CERAIVTEC
GITIBH
MULTIFUNCTIONAL
CERAMICSLUITPOLDSTMSSE
15 D-91207LAUF,GERIVANY
trfllrI.
tllllll
Analyticalflowcha of Soxhlet€xlraction(GC/MS)procedure
I
r
Nameof lhe personwhomademeasurement
RomanWong
Nameoflhe personin chargeofmeasuremenlTroyChang
(TeEtltems:Phthalate' B€nzotriazole. HBCDD. NP . DBBT.
Oryanicphosphorus
compoundrs)
* ihdr Fiorwins p€m3sond h3
nrh.radGoodcrdontb{i.*nr€{e)l.sd.h6bn@od6nmLsrcpodu€d.€^6prrntur
'"lJl-atv
td&l:ldf-qEFdb
corraaBr. e e@ !BS4Fr*tdj^+-as
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ns4{4oT
on/rsd*0oor.i
andror..dM( rffi dem.nr &t.di,-nr
am codtms w
imibron d rdrt idmnneton l;d ':id doi i$u.s dsfind b.6 i Air io d.r ol rhi3doonenl adu$d hlr 'ft
u.lim.fi1!nEii€ntmd'ands.liin1i.imibo'c||€n|li9rudo6iai,rhconFnybd3r..ponEb''
-@didouMts
-b doLnfr 6
cmFny Ary uruubodair abdon foasry or fsltr€ron or h' @i6d or ap
TestReport
No. : CE/201214843A Date:201i,02104 Page: 19of 24
CERAI/ITEC
GI/tBH
MULTIFUNCTIONAL
CERAIVICSLUITPOLDSTMSSE
15 D-91207LAUF,GERMANY
lll|t|::
l]t
Analyticalflow chart of Organic-Tincontent
I
I
Nameofthe personwhomademeasurement
GinnyChen
Nameoflhe perconin chaee of measurement:
T.oyChang
Concenbate/Dilute
Exkacted
solution
Analysiswas perfomedby GC/FPD
Dala
CmEi!hl
EJ8!
i E ,ERHtlr€ll2ll
l A r " IE"{t{|
i J.,b8l
"4h:n:
,ond oftdSe1uDnftdoER
drrdr.rerdco.ono$6rEr.m
oducdeeplifuldbodp'old
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iandid on E6
dnd
tudn An' h
rh rh6 dbideiadoi
onrvsnd * ihii h6 rh r d c iad3 insdons
iiry
hneo m rdm .rcEsm dl hq notu so dro.ron! und h. b.n*dod @
compary Ary unadhoruA rE,!r n bqary q bls i€ln
d hs trhr
or ap
n"**.,ffiiu';tl.':ji,;H.Jiil*iilI1n
$ff,991"**tr,i:1.""-,nu*'u***oon*.*
I
Test Report
No.: CE/201214e43ADale: 201210?,04Paoe:20 ot 24
CERAMTEC
GMBH
II,IULTIFUNCTIONAL
CERAMICSLUITPOLDSTMSSE
15 D.91207LAUF,GERMANY
Analyticalflow chart of halogencontent
1) Nameofthe personwho mademeasuremenl:
RitaChen
2) Nameofthe personin chafgeof measurement:
TroyChang
Sampleprelreatment
/ Sepataiion
Weighting
andputtingsamplein cell
OxygenBombCombustion
/ Absorpiion
Dilutbn10fixedvolume
Analysis
wasperformed
by lC
conFl[i]l teS3! -[HiL+liti]13
lliiAA. ldA f Ad .-FditE
rcddm. E s".d d u. cmEn
3d ro dftnrbrddLnfb
&drF16 smEfd cortonsto'Ebtu
i'ln*idm s6
ddd
badn. Anr fd
tErm.d6'miwmononkaowft
ihrmcrC
ads n$trotr3 iin
hiso
m irem &sE,ft
dl h.r iotu eo dr oar on! Lne h. hlnsdort
ecmda
comp'a Any!m6o,ze
dEErm'toEerydbsidbdhstrblorap
i " Eo\tqr'
ms odr6a
6nd
ba Eru
*-,nu"nuo*"*"oo"o
*"*'*ffilil]iio\'3;Il;k,ifig;|ff l"t*$$#gll"*.,lll:]"!k
TestReport
No.: CE|2O1Z14843A.Date: 2O1ZOZO4 Paae: 21 of 24
CEMMTEC GIMBH
MULTIFUNCTIONAL
CERAIJICSLUITPOLDSTMSSE
15 D-91207LAUF,GERIVANY
Analysis flow chart for determinationof Aabestos
1) Nameof the Dersonwho mademea6urcmenl:
VictorKao
2) Nameofthe personin chargeof measuremeni:
WendyWei
l6 )
I Refercncemothod:EPA600/R-93/l
Conlinuewh€nproblem€
a€ encounle€dwithPLlvl
and/orfor qualily assurancepurpo€€s
Inleriercncemahi\ removal
Asbeslos identificationby dispersion
stainingpobnzationlightmicroscopy
A€bestosidentiticationby X-€y
Notconraining
Asbesros/
cnFnyRJ BA&.8 {E: *lRl6flnld -AB Frt IEd-*l{4 \:ltffril
nidhi
d ri'driry. id.mn ieln
rE$don tm d.eno.i
cdmFry Ary u@rb4n
r.JfllSp
@dudrepliful.dodpidfr
'id j
h., nod
sbdon
blw
or raibf€ton
F hnEdon oodn.nri
d b. @ftdtr
@
Tdeoo@r
** f,iFi$l' I ;i*,?1.;r,];'i[il::t;.,]-**u;]'*.,
r ar'eb.,.lr
'**...*.
Test Report
No.: CEi2012l14843A Date: 2O1Z0ZM
Paoe: 22 ol 24
CERAITITEC
GMBH
IJULTIFUNCTIONAL
CERAMICSLUITPOLDSTMSSE
15 I}91207LAUF,GERITIANY
Analyticalflowchart
I
I
Nameof lhe personwho mademeasurcmentRomanWong
Nameof lhe personin chargeofmeasurement
TroyChang
TBBP-A-bb)
I Tesl llem3:PBB/PBDE,
pfoceEs---.
Firsllestingproc€ss-----+ Optionalscrcen
proces€-.>
Confirmation
Screenanalysis
'Li-;iirn-rrn;i;;;i.ii
.i;ii.
Sampleextraclion
method
Concentrale/DiluteExtractedsolulion
Filter
Analysisby GC/lt/S
lssueRepod
c o F o . r a JF H & ! i - { & d E
- l l q U d l nI E E A { . i € b f l 4 d r " - s a , q .
-d6rnh6dolend
irturondrdi
t
sa.ftdn<ifuMonf|ya'od
bjd b rffir
ad codi
r" iid!.
m3 tu E 6dm
b a ' d d i s . f 3 ' r d e . ' 0 . ? 9 d o n p d L e d 4 e p l i l f u |
.r
t]ttllll||Iltt]l
Test Report
No.: CE|2O1Z14A$A Dale:2012102104Paoe:23 of 24
CERAMTEC
GI\,iBH
MULTIFUNCTIONAL
CERAI\/IICS
LUITPOLDSTMSSE
15 D,91207LAUF.GERMANY
Analyticalflow cha(otvolatils oryaniccompounds(VOCS)
I
I
Nameof lhe personwhomademeasuremenl
: ChunWu
Nameof the personin chargeofmeasurement
: ShinjyhChen
I Referencemelhod : US EPA 5021)
Samplepretrealmenl
Takesampleandputil into
glassware.
headspace
o r p a n y u Jt l r ; t 8 r ' { F 1 t : R @ 9 l d l t 4
&-AE
lEl,-{lil
":-"q
. rE&"
nlfltm
lm0trmt
Test Report
No.: CEI2O1Z14U3A, Date 201210?,A4 Page 24 ot 24
CEMMTEC G[/lBH
MULTIFUNCTIONAL
CERAIVICSLUITPOLDSTMSSE
15 D-91207LAUF,GERMANY
r:|| tt]||ln|rr|l
* The tested sample / paft i6 marl(ed by an anow if if,s shown on the photo. .
L4843
** End of Report "
cmF.th/
- t s f u 9 1 3 i gtq$qS
. d b y s o .llmel
ffF
.?l49jii];i -df{R&.,lE:
llt li"
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|edhbdoUm'di3'sdtsdhatdo
h t m d B d s ' e d i o i o n | , a n d d l h f t s c m F r y s s o € E s o i d b l i l y i s b
-_*-***-_*^_1
|
rdF cie ri wd / fittir5:]ijf*Ld6n}f*r*
Validit
nown
ForQues-ti
PleaseCo
Test Report
No. : CE/2011/84958
l
The following sample(s)was/weresubmitted and id€ntifi€d by/on behalf of the client a6:
SampleDescription
Buyer/OderNo.
Date
SampleReceiving
TestingPeriod
TeEtRoault(a)
Page:1of7
Dale: 201111?,01
POLYFILAG
OBERALLMENDSTMSSE2OA,CH-6300ZUG / SWITZERLAND
Ni99.9
+1357
2011t11t25
201Ih1t2510 201II12t01
Pleasereferto nexlpage(s).
glnaa forrnd
Or..| cd L-or.tory - flhd
mpr.G)r.sbdftr3 b..epdd 6nior b
l:.Lntll il ,.1'fi f.i,i:-\.
com*iyiirilil!,:['irl
i ! , ]. 4 ! r l : 1 , l i r "} l
rhsdodnara sdbyhccompanys!b!3db bcai*rcoddrdi3br se'epi.€doledstsvaiadeoncq
poisb '9 c b b cr ed andrbs doum
q dsnrze.exewDpeicq,rr-r/iL-,,-
r *:r
tiJr4.-i+3361orrr?e
sGs
lfi||| lurrrr
TestReport
No.I CE/201'1/84958
Page:2ol7
Dale:201111201
Il]lIltt]||tttt
POLYFILAG
2OA.CH€3OO
OBERALLMENDSTRASSE
ZUG/ SWITZERLAND
Test R6ult{s)
PARTNAMENo,,1
SILVERCOLOREDMETALWIRE
Tost ltem(8)
tlethod
Unit
(Cd)
Cadmium
mg/Kg With referenceto IEC62321:2008and
perfomedby ICP-AES.
mg/Kg A/ithreferenceto IEC62321: 2008and
cerfomedbv ICP-AESmS/kS Withreference
to IEC62321:2008and
pertormed
by ICP-AES.
and
Withreference
to IEC62321:2008
performedby Boilingwaterexkaction
Method.#
Lead (Pb)
Mercury(Hg)
Hexavalent
Chromium
Cr(Vl)
Sum of PBB6
Monobromobiphenyl
Dibromobiphenyl
Tribrcmobiphenyl
Tetrabromobiphenyl
Pentabromobiohenvl
Hexabromobiphenvl
Heptabromobiphenyl
Oclabromobiphenyl
Nonabromobiphenyl
D€cabromobiohenvl
Sum of PBDE8
Monobromodiohenvl
ether
Dibromodiphenyl
ether
Tribromodiphenyl
ether
MDL
Re8ult
No.1
2
n.d.
2
n.o,
2
n.d.
Negative
5
With referenceto IEC 62321: 2008 and
mg/Kg performed
by GC/MS.
5
5
5
5
5
5
5
n.d.
n.d.
n.d.
n.d.
n.o.
n.d.
n.d.
n.d.
n.d.
n.d.
n.o.
n.d.
5
5
5
n.d.
n.d.
n.d.
Tetrabromodiphenylether
5
5
5
Pentabrcmodiohenvl
ether
Hexabromodiphenyl
ether
HeotabromodiDhenvl
ether
n.d-
n.d.
n.d.
ethgr
Octabromodiphenvl
n.o.
ether
Nonabromodiohenvl
n.d.
5
ether
O€cabromodiphenyl
fililnil*
cmpsiy h,:fr 1 rlt lN'i,rl
rh";;*.,6
**d by,h"c".p,
b.gdrcftcromd dlmm6. iba
-]*d*b'h'inkdc.d"
*
il i
tft
it'rrll
.
n.d.
m.ra(s)radsdst b{ 6pod e^ioi b
iL, "",ar,r;ln'
e mid'onorrsbirv
lpoisb98b bcredsndrrsdoe
. : . l . : 1 1f l r : + i 4 . . , , 1 + e t o r t r e e t r e r r s 6 o a r e e tR
t was<oo
TestReport
No. CE/2011/84958
Page:3 of 7
Dale'.2011112101
:m ItNnt||||r
POLYFILAG
OBERALLIVENDSTMSSE
2OA,CH$3OOZUG / SWITZERLAND
Test ltem(s)
Halogen
(F)
Halogen-Fluorine
(CASNo.:14762-94-a)
Halogen-Chlorine
(Cl)
(CASNo.:22537-15-1)
(Br)
Halogen-Bromine
(CASNo.:10097-32-2)
Unit
mslkg
toL
Mothod
Withreference
to BS ENMSAZ2007.
Analysis
waspefoamed
by lC.
Halogenlodine(l)
(CAS No.: 14362-44-8)
Result
No.l
50
n.o.
50
n.d.
50
n.d.
50
n.d.
Note:
'1.mg/kg= ppm; 0.1wt%= 1000ppm
2. n.d.= NotDetecled
3. [rDL = l,ilethod
Detection
Limit
4."-"=NotRegulated
(NoUnit)
5. " = Qualitative
analysis
6. # = a. Positivemeansthepresence
of CrVlonthetestedareas
b. Negativemeansthe abs€nc€of CrVlon the testedareas
jn boiling-water-extraction
Thedetected
concentration
solutionis equalor greaterthan0.02mg/kgwith50cm'
testedareas.
l:i!z;li
i: i.tt'
r 1lr . "1 il i r.' -r:'1itli
nysled ro 6 &israrcod r oG or s
fors]sdrcnciom.1doem.itssub]
conpsii rir
1,.
1.!.ij'l'!4'
3@gbitr€lo&cl€d,ndh'3('ffi
'.1 , r.Li- ri:,
l
Fn?,,'tle6lor)ze
Test Report
No. : CE/2011/84958
Page:4 of 7
Da,e :2011112,01
POLYFILAG
OBERALLMENDSTMSSE2OA.CH.63OO
ZUG / SWITZERLAND
tt][]|l[[[]
]l
1) Thesesamples
weredissolved
totallyby pre-conditioning
methodaccording
to belowflowchart.
( Cf' test methodexcluded)
2) Nameof the personwhomademeasurement:
Climbgreat
Yang
3) Nameof the pe6on in cha.geof measurementr
TroyChang
Cutting
/ Preparation
Aciddigestion
by suitable
acid
depended
ondifierent
sample
material
las belowtable)
Add appropriateamountof
digestion
reagent
Heatto appropriate
tgnpe€tu€ to ex€ct
'1) AlkaliFusion
2) HClto dissolve
ICP.AES
DigestionAcid
S1eel,
copper,aluminum,
solder
Aquaregia,HNOs,HCl,HF,H,O,
Gla6s
HNO3/HF
p€lladium,
Gold,platinum,
ceramic Aquaregia
Silver
HNO.I
Plastic
HCI
HrSOr,Hroa HNOg,
Others
Anyacidlo tobldige6tion
1.:.ati
i;llri
abjed ro.ems 3id cofdtoG rof E
throughfilter
Add diphenyl-carbazide
for
SampleMaterial
c o m o , i rt t - , i . r i r l L l { i I r . , r l , J i : n i i !
Cool,filterdigestate
colordevelopment
measurethe absobance
at 540 nm by UV-VIS
1r.rrlri}ll.
Atenoi sdrawiroh.rn'bloior
'ab't
TestReport
No.:CEl20'11184958
Dale:201111i,01
POLYFILAG
OBERALLMENDSTRASSE
2OA,CH€3OO
ZUG/ SWITZERLAND
Page: 5 of 7
lU[uIl||t
[t|]l
PBB/PBDEanalyticalFLOWCHART
'1) l{anEofthepersonwholrEderEaru.enEnt:RofiEnWong
2) lhmeoftheperson
incharge
of nEasurerEnt
TroyChang
Firsttestingprocess----+
process-- Optionalscreen
process - .>
Confinmtion
Screen
analysis
Safipleei€ction/
So* et rnethod
concenkate/Dilute
Extractedsolution
Filter
Analysisby GC/IMS
c o m o a nl ivi i l r / t r i , r L r i ' r , - r l , 1 i , ! n i l i ) : i r r ' l j d i
l?q{!.\.
.,
r'.rll'trl'
mdbaGpJdu€dexeplnig].wbou
!hdsrdzoie N.!r:iFcryttrw:orrr:
:r,'
t::Ii+fi,'
's6i0r)2etDr+336(orrstt
ffis'g'.om
TestReport
No.: CE/2011/84958
Dale:2011h2/01
Page:6 of 7
l]m||ufi]ltl|l]
POLYFILAG
OBEMLLMENDSTRASSE2OA,CH-6300
ZUG/ SWITZERLAND
AnaMical flow chart of halogen content
'1) Nafi€ of the oerson who arEderEasurernenl Rita Chen
2) Narneofthe person in charg€ of rEasurerEnt: Troy Chang
Sanplepretreatrnent
/ Separatbn
Weighting
andputting
samplein cell
OrygenBombCombustion
/ Ab€orption
Dilution
lo fixedvolunE
AnalysiswasperfonrEdby lC
c o m p . n yn ; , i r r , l r l , ; ! i ' i l r r j J l l ; ' h
rh s @msnr s 'sred by 6e compa
l,.ljf
,ltirllt
psls)6sbd hb red rcPodanioi bs
i 1 ! . . 1 . " .i , r i ' i j ! .
'ndom^ioroiaidluisdclon $uord
iidbe6pd!€dai6plniu]qho'
'.1 . :: ji
::r,ii{
jl + e6ior)rs !^
r+ $61orre tt
@r a*on
TestReport
No.: CE/2011/84958
Page:7of 7
Dale| 201111201
POLYFILAG
OBERALLMENDSTMSSE2OA.CH.63OO
ZUG / SWITZERLAND
I ]I||||t
||]|l]r
r Thetestedsample/ part is mafted by an arow if ifs shownon the photo.*
'* EndofReport'*
c o m o a t uf r , 1
r!.:R
irr!rj;i:liJ*
rhc ddomsr a sdbyrhecdnpaiyslqedb
i: i tli
l$ali
6 6ed
cond r oi3 of s
mpre(s) re{ed rh s bn Gpod e^d
: l. I l'!rj]t'!
b
pmgb''y6locc|ada.dlh3ddm
L r a!r . s:i:rc,
, ,,r + s6 t0r)2!e3re I r336to2lrree.131
wN s\.6h
Validi
nown
ForQueEll
PleaseCo
Test Report
No.: CEl2011184955
Datet20'1111201
POLYFILAG
OBERALLMENDSTMSSE2OA,CH€3OOZUG / SWITZERLAND
ithscs
Page:'l of 7
ll]uttfi
[[m
Thefollowingsample(s)wa3/weresubmitledand identitiedby/onbehalfof the clientas:
SampleDesciption
Buyer/OrderNo.
SampleReceiving
Date
TestingPeriod
Ni42Fe58MCuMAgs%
11-0803
2011t11t25
2011t11t25'l O 2011I 1'J01
T€stResult(s)
Pleasereferto nextpage(s).
(NW4E
f,lmdiorrd
Or.rlcd l,.bor|b.t - Trlpd
ps(31i€ded rhs ied rcpod eiior be
cwpanye
!,
rt
rr-ri'f.,ri,il]ilntlli ir ].ri
iiil-:i I
ny tublsd b b Gene6 coideoB d se
1,.
|.lrrrr?!t!:.
dbis r aiy'Iha cohpantssoo r69onsbiI s b r ct'odaddrhs dodm
! hdsrLrzore.N4lrFr .o ri p,i /F L I I|t,
f: lFt
. ,;,i+ @610?)ree
14 | + 8610r)2ee
ry
(w ar.on
TestReport
No.: CE/201
1/84955
Page:2of 7
Dale: 2111/12t01
POLYFILAG
OBERALLI\4ENDSTMSSE
2OA,CH63OO
ZUG/ SWITZERLAND
lm[tmlrltttll
Test Reault{s}
PARTNAMENo.1
SILVERCOLOREDI'ETAL WIRE (INCLUDINGTHE PLATINGLAYER)
T66l ltem(s)
Unit
Cadmium(Cd)
Method
mSikS Witheferenceto tEC62321:2008and
perfom€dby lCPdES.
mgKg Withreference
to IEC62321:2008and
perfomedby ICP-AES.
mg/Kg Withreference
to IEC62321:2008and
pe.formed
by ICP-AES.
Withreferenc€
to IEC6232'1:
2008and
performed
by Boilingwaterextraction
M€thod.#
Lead (Pb)
(Hg)
Mercury
Hexavalent
Chromium
Cr(Vl)
Sumof PBB9
l\4onobromobiphenyl
Dibromobiphenyl
Tribromobiphenyl
Tetrabromobiphenyl
MDL
2
R6sult
No.l
n.o.
2
2
n.d.
Negative
n.d.
n.d.
n.d.
n.d.
n.d.
n.d.
n.d.
n.d.
n,d,
n.o.
5
5
5
Pentabromobiphenyl
Hexabromobiphenyl
Heptabromobiphenyl
Octabromobiphenyl
Nonabromobiphenyl
Decabromobiphenyl
Sumof PBOE3
Monobromodiphenyl
ether
5
mgikg
Withreference
to IEC62321:2008and
per{ormedby GC/lrS.
DibromodiDhenvl
ether
TribromodiDhenvl
ether
Tetrabromodiphenyl
ether
PentabromodiDh9nvl
ether
Hexabromodiohenvl
ether
Heplabro.nodiphenylether
5
5
n.d.
n,o.
5
5
5
n.d.
n.d.
n.d.
n.d.
5
n.o.
n.d.
5
5
5
Octabromodiphenvl
ether
NonabaomodiDhenvl
ether
n.d.
n.d.
n.d.
Decabromodiohenvl
ether
c o m o a n yi r r l ! /
tu.f-]i'
I rlirlltr] ntlrli
n,o,
I
:.i
i
^r!.l;li,
I r.. r.i. rriilA.
L@nnieroi
aidllr edd'on $@3 d
onry3id*ib'.lhormrrsorcenrsnsrld'on.f,'ryth6compaiyssecsponsurrysiobc,enraidhcdm!
iidbe€pduedexeptniur*6oq
!^r+s6(0nreenr
@! a!@n
M€f,be,or 'he 5616,@p (s6sr{)
TestReport
No.: CFJ2011184955
Page:3 of 7
Dale:2O11h21O1
POLYFIL
AG
OBEMLLMENDSTRASSE
2OA,CH-6300ZUG/ SWITZERLAND
Testltem(s)
Halogen
Halogen-Fluorine
(F)
(CASNo.:14762-9+8)
Halogen.chlorine
(Cl)
(CASNo.:22537-15-1)
Halogen-Bromine
(Br)
(CASNo.:10097-32-2)
Unit
lrethod
With refe.enc€to BS EN 14582].2007
.
mg/Kg
Analysis
wasperformod
by lC.
Halogen-lodine
(l)
(CAS No.: 14362-4,4-8)
|l]rl||l]
MDL
t[]||n
Result
No.1
50
n.d.
50
n.d-
50
n.d.
50
n.o.
NoteI
1. mg/kg= ppm; 0.1wt%= 1000ppm
2. n.d.= NotDetected
3. [4DL= MethodDetection
Limit
4."-"=NotRegulated
5. " = Qualitative
(NoUnit)
analysis
=
6. # a. Positivemeansthe presenceof CrVlon the testedareas
b. Negativemeansthe abgenceof CrVlon the testedareas
Thedetected
concentration
in boiling-wEter€xtraction
6olution
is equalor greaterthanO.O2
mg/kgwithS0cm,
testedareas.
7. The6ample(s)
was^rereanalyzed
on behalfoftheapplicant
as mixingsamplein onetesting.Theaboveresult(s)
was^^€re
onlygiv€nas theinformality
vaue.
c m e a i ya r | 1 l l r ' r d 1 1 ' t , r , i i l l , n r 4 L . i . r 1
iirl4li
r3G)rssrd rh I r€d'+on €nnd e '
ir'r'r Nlttll\.
tfi r:li {:/:rFi4,t;r+s6Frtreer7e r}s6Or)xerr
Ewar.on
Test Report
No.: CEl2011/84955
Paget 4 of 7
Dale:2011h2101
POLYFILAG
OBERALLMENDSTMSSE2OA,CH-6300ZUG / SWITZERLAND
t[| tl
rrr ]l
'1) Thesesamples
! €re dissolved
totallyby prcconditioning
methodaccording
to belowflowchart.
( Cf' test methode(cluded)
yang
2) Nameof the personwfiomademeasurement:
Climbgle€t
3) Nameof the personin chargeof measurement:
TroyChang
Cutling/ Preparation
Aciddigestion
by suitable
acid
dependedon differentsample
matedal(as belodtable)
Add appropriateamountof
digestion
reagent
Heatto eppropriate
temp€ratueto extract
Cool, filter digestate
1) AlkaliFusion
2) HCltodissolve
ICP-AES
throughfilter
AdddiphenyFcarbazide
for
SampleMaterial
colordevelopment
DigestionAcid
Steel,copper,aluminum,
solder
Aqua regia,HNO3,HCl,HF,HrO,
Glass
HNO/HF
measure the absorbance
Gold,platinum,palladium,ceramic
Aqua regia
at 540 nm by UV-VIS
Silver
HNOs
Plastic
H,SOI, H'O', HNO3,HCI
Others
Anyacidtototaldigestion
rlrlt
c f f i o . n yB : . 1
t-f
i,l'irl!
!,i
i,.t'l
lii]]irl)
! rd4krzE,
'r
1rItihl-
Nlwri @.ry.tuM{/}i.:
r ;r
+1 r rtLtri,ni+ s6 orrree
Test Report
No.: CE/2011/84955
POLYFILAG
OBEMLLMENDSTRASSE2OA,CH€3OO
ZUG/ SWITZERLAND
|t
PBB/PBDEanalyticalFLOW CHART
1) Name
of theperson
whorEdenEasurer€nt:
RormnWong
2) Mrneof theperson
incharge
of fipasurenEnt:
TroyChang
Firsttestingprocess----+
Optional
screenprocess---process - .>
Confifination
Scfeenanalysis
Sanpleextractiort
So*rlet nEthod
ConcedtratdDilute
Extractedsolution
Filter
Analysisby GCiMS
kriue Relp-l1
c o m p a n yG i ! I
rltl
ri-11'!,liill,lnll].i
tudois
i
.Ir;
riit!-l
]
p3G)!6ied rh s ied €pd eiio,
r'rr.l,ljrll.
rary rh,ComFnys30eGspdisb
r1l6b
Page:5 of 7
Date| 2011h2t01
bddnraidrbsdoem
be
r |l t[]
]l
TestReport
No.: CE/2011/84955
Page:6 of 7
Date 2011,1|:]01
POLYFILAG
OBERALLIVENDSTRASSE
2OA,CH$3OO
ZUG/ SWITZERLAND
rt][]|l
rtl[]ll
Analltical flow chart of halogen content
1) Narneofthe pe6on who rcde fiEasurenEnt:Rita Chen
2) Narneof the person in charge of rEasureient: Troy Chang
SaftplepretreatnEnt/ Separatbn
Weightiryandputting
sanplein cell
OrygenBombConbustion
/ Ahsorption
Dilution
to fixedvolunE
AnalysiswasperforfiEdby lC
cdnp,iy til ,il irl,rlli'i
r l r r r j r J ,n j r l ; .
{i!-rL\
.,, tF
Th s dofuneil 6 'sued h' 6e c onpa
$bjed b tens &d cdidrrois rof E
I
mp31s)rsded nE bd rcpod.aiioi b
r1",1."inr'!.!.
Abnron
nndbaBFdu4detepiilui.whou
6 drtun ro be rmlarioi o, abit
Test Report
No.: CE/2011/84955
Page.7of 7
Dai.e| 2O11112J01
POLYFIL
AG
OBEMLLMENDSTMSSE
2OA,CH{3OOZUG/ SWITZERLAND
][|l
||ttl
' Thetsgtedsample,/pa is ma*ed by an
anow if ifs shownon the photo..
" Endof Repod*'
a o h p a n y, : j f r : | t r j , f _ i '
r , r i r r , , l :i l r l ) : i . . . ! , i
r.{ttLa I
p3(sliseedrhs Gd rcpodeiiolbe
1". ' 1., ijl lt:.
h0r iq6 $d obrrgdioEundartu ra
LnLt:i ,+ = [E?4 ),t+ 86 \a2vee
Mem6edrhe scsGrclp6cssAr
l
Number : TWNC00233072
Test Report
Applicant:
Littelfuse Philippines Inc.
LIMA Technology Center, Lipa City,
Malvar, Batangas
Date
: Nov 23, 2011
Sample Description:
One (1) group of submitted samples said to be :
Part Description
: Sand Filler
Part Number
: 091250
Date Sample Received
: Nov 17, 2011
Date Test Started
: Nov 18, 2011
Test Conducted :
As requested by the applicant, for details please refer to attached pages.
Authorized By:
On Behalf Of Intertek Testing Services
Taiwan Limited
K. Y. Liang
Director
This report shall not be reproduced
except in full, without the written
approval of the laboratory.
Page 1 of 6
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00233072
Test Conducted
(Ⅰ) Test Result Summary :
Test Item
Result (ppm)
Grey Powder
Heavy Metal
Cadmium (Cd) content
Lead (Pb) content
Mercury (Hg) content
Chromium VI (Cr6+) content
Polybrominated Biphenyls (PBBs)
Monobrominated Biphenyls (MonoBB)
Dibrominated Biphenyls (DiBB)
Tribrominated Biphenyls (TriBB)
Tetrabrominated Biphenyls (TetraBB)
Pentabrominated Biphenyls (PentaBB)
Hexabrominated Biphenyls (HexaBB)
Heptabrominated Biphenyls (HeptaBB)
Octabrominated Biphenyls (OctaBB)
Nonabrominated Biphenyls (NonaBB)
Decabrominated Biphenyl (DecaBB)
Polybrominated Diphenyl Ethers (PBDEs)
Monobrominated Diphenyl Ethers (MonoBDE)
Dibrominated Diphenyl Ethers (DiBDE)
Tribrominated Diphenyl Ethers (TriBDE)
Tetrabrominated Diphenyl Ethers (TetraBDE)
Pentabrominated Diphenyl Ethers (PentaBDE)
Hexabrominated Diphenyl Ethers (HexaBDE)
Heptabrominated Diphenyl Ethers (HeptaBDE)
Octabrominated Diphenyl Ethers (OctaBDE)
Nonabrominated Diphenyl Ethers (NonaBDE)
Decabrominated Diphenyl Ether (DecaBDE)
Halogen Content
Fluorine (F)
Chlorine (Cl)
Bromine (Br)
Iodine (I)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Remarks: ppm = Parts per million based on weight of tested sample = mg/kg
ND = Not detected
Responsibility of Chemist : Irene Chiou / Kevin Liu / Cathy Chen
Date Sample Received
Test Period
: Nov 17, 2011
: Nov 18, 2011 To Nov 21, 2011
Page 2 of 6
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00233072
Test Conducted
(Ⅱ) RoHS Requirement:
Restricted Substances
Cadmium (Cd) Content
Lead (Pb) Content
Mercury (Hg) Content
Chromium VI (Cr6+) Content
Polybrominated Biphenyls (PBBs)
Polybrominated Diphenyl Ehters (PBDEs)
Limits
0.01% (100ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for
homogeneous material.
(Ⅲ) Test Method:
Test Item
Cadmium (Cd)
content
Lead (Pb) content
Mercury (Hg)
content
Chromium VI (Cr6+)
content
Polybrominated
Biphenyls (PBBs)
Polybrominated
Diphenyl Ethers
(PBDEs)
Halogen Content
Test Method
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 7, by microwave
digestion until the tested samples are
totally dissolved and determined by
ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in annex C, by alkaline
digestion and determined by UV-Vis
spectrophotometer.
With reference to IEC 62321 edition
1.0:2008 in annex A, by solvent
extraction and determined by GC-MSD
and further HPLC confirmation when
necessary.
With reference to IEC 62321 edition
1.0:2008 in annex A, by solvent
extraction and determined by GC-MSD
and further HPLC confirmation when
necessary.
With reference to EN 14582:2007 by
calorimetric bomb with oxygen and
determined by ion chromatography
Reporting Limit
2 ppm
2 ppm
2 ppm
1 ppm
5 ppm
5 ppm
50 ppm
Remark: Reporting limit = Quantitation limit of analyte in sample
Page 3 of 6
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00233072
Test Conducted
(Ⅳ) Measurement Flowchart:
Test for Cd/Pb/Hg/Chromium (VI)/PBBS/PBDES Contents
Reference Standard: IEC 62321 edition 1.0:2008
Sample preparation
For non-metal part
For metal part
Take sample and immerse into Aqua Regia, start to strip plating layer
Stop the stripping procedure upon color change completely
Take the Aqua solution as plating component and stripped body as substrate component
Cd/Pb/Hg
Cr
Weigh sample and
add organic solvent
By spot test
Negative
Confirm the tested
samples are
totally dissolved
Make up with
deionized water
PBBs/PBDEs
Polymers /
electronics
Metal
For different
material, digest
the sample with
*1
appropriate acid
6+
Get 50cm2 sample
By boiling water
extraction
*2
Weigh sample
and add
alkaline
solution
By Soxhlet
extraction or
Solvent extraction
Definite temp.
extraction
Cool and filter
the extract
Analyzed by ICP-OES
Concentrate the
extract and make up
with organic
solvent
Analyzed by GC-MSD
Make up with deionized
water and add diphenylcarbazide solution
Remarks:
*1: List of Appropriate Acid：
Material
Polymers
Metals
Electronics
Analyzed by UV-VIS
Acid Added for Digestion
HNO3,HCl,HF,H2O2,H3BO3
HNO3,HCl,HF
HNO3,HCl,H2O2,HBF4
*2: If the result of spot test is positive, Chromium VI would be determined as detected.
Page 4 of 6
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00233072
Test Conducted
(Ⅳ) Measurement Flowchart:
Test for Halogen Content
Reference Standard：EN 14582
Sampling/grinding or
cutting
Add absorbent in a
combustion flask &
place weighed sample in
equipment
Fill oxygen into
calorimetric bomb
Ignite then leave the
flask at room
temperature
Transfer the absorbent
into a volumetric flask
Make up with deionized
water
Analyzed by ion
chromatography
End of Report
Page 5 of 6
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00233072
Test Conducted
Photo
Page 6 of 6
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00233073
Test Report
Applicant:
Littelfuse Philippines Inc.
LIMA Technology Center, Lipa City,
Malvar, Batangas
Date
: Nov 23, 2011
Sample Description:
One (1) group of submitted samples said to be :
Part Description
: Sand Filler
Part Number
: 091251
Date Sample Received
: Nov 17, 2011
Date Test Started
: Nov 18, 2011
Test Conducted :
As requested by the applicant, for details please refer to attached pages.
Authorized By:
On Behalf Of Intertek Testing Services
Taiwan Limited
K. Y. Liang
Director
This report shall not be reproduced
except in full, without the written
approval of the laboratory.
Page 1 of 6
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00233073
Test Conducted
(Ⅰ) Test Result Summary :
Test Item
Result (ppm)
Light Grey Powder
Heavy Metal
Cadmium (Cd) content
Lead (Pb) content
Mercury (Hg) content
Chromium VI (Cr6+) content
Polybrominated Biphenyls (PBBs)
Monobrominated Biphenyls (MonoBB)
Dibrominated Biphenyls (DiBB)
Tribrominated Biphenyls (TriBB)
Tetrabrominated Biphenyls (TetraBB)
Pentabrominated Biphenyls (PentaBB)
Hexabrominated Biphenyls (HexaBB)
Heptabrominated Biphenyls (HeptaBB)
Octabrominated Biphenyls (OctaBB)
Nonabrominated Biphenyls (NonaBB)
Decabrominated Biphenyl (DecaBB)
Polybrominated Diphenyl Ethers (PBDEs)
Monobrominated Diphenyl Ethers (MonoBDE)
Dibrominated Diphenyl Ethers (DiBDE)
Tribrominated Diphenyl Ethers (TriBDE)
Tetrabrominated Diphenyl Ethers (TetraBDE)
Pentabrominated Diphenyl Ethers (PentaBDE)
Hexabrominated Diphenyl Ethers (HexaBDE)
Heptabrominated Diphenyl Ethers (HeptaBDE)
Octabrominated Diphenyl Ethers (OctaBDE)
Nonabrominated Diphenyl Ethers (NonaBDE)
Decabrominated Diphenyl Ether (DecaBDE)
Halogen Content
Fluorine (F)
Chlorine (Cl)
Bromine (Br)
Iodine (I)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Remarks: ppm = Parts per million based on weight of tested sample = mg/kg
ND = Not detected
Responsibility of Chemist : Irene Chiou / Kevin Liu / Cathy Chen
Date Sample Received
Test Period
: Nov 17, 2011
: Nov 18, 2011 To Nov 22, 2011
Page 2 of 6
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Test Conducted
(Ⅱ) RoHS Requirement:
Restricted Substances
Cadmium (Cd) Content
Lead (Pb) Content
Mercury (Hg) Content
Chromium VI (Cr6+) Content
Polybrominated Biphenyls (PBBs)
Polybrominated Diphenyl Ehters (PBDEs)
Number : TWNC00233073
Limits
0.01% (100ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for
homogeneous material.
(Ⅲ) Test Method:
Test Item
Cadmium (Cd)
content
Lead (Pb) content
Mercury (Hg)
content
Chromium VI (Cr6+)
content
Polybrominated
Biphenyls (PBBs)
Polybrominated
Diphenyl Ethers
(PBDEs)
Halogen Content
Test Method
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 7, by microwave
digestion until the tested samples are
totally dissolved and determined by
ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in annex C, by alkaline
digestion and determined by UV-Vis
spectrophotometer.
With reference to IEC 62321 edition
1.0:2008 in annex A, by solvent
extraction and determined by GC-MSD
and further HPLC confirmation when
necessary.
With reference to IEC 62321 edition
1.0:2008 in annex A, by solvent
extraction and determined by GC-MSD
and further HPLC confirmation when
necessary.
With reference to EN 14582:2007 by
calorimetric bomb with oxygen and
determined by ion chromatography
Reporting Limit
2 ppm
2 ppm
2 ppm
1 ppm
5 ppm
5 ppm
50 ppm
Remark: Reporting limit = Quantitation limit of analyte in sample
Page 3 of 6
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00233073
Test Conducted
(Ⅳ) Measurement Flowchart:
Test for Cd/Pb/Hg/Chromium (VI)/PBBS/PBDES Contents
Reference Standard: IEC 62321 edition 1.0:2008
Sample preparation
For non-metal part
For metal part
Take sample and immerse into Aqua Regia, start to strip plating layer
Stop the stripping procedure upon color change completely
Take the Aqua solution as plating component and stripped body as substrate component
Cd/Pb/Hg
Cr
Confirm the tested
samples are
totally dissolved
Make up with
deionized water
PBBs/PBDEs
Polymers /
electronics
Metal
For different
material, digest
the sample with
*1
appropriate acid
6+
Weigh sample and
add organic solvent
By spot test
Negative
Get 50cm2 sample
By boiling water
extraction
*2
Weigh sample
and add
alkaline
solution
By Soxhlet
extraction or
Solvent extraction
Definite temp.
extraction
Cool and filter
the extract
Analyzed by ICP-OES
Concentrate the
extract and make up
with organic
solvent
Analyzed by GC-MSD
Make up with deionized
water and add diphenylcarbazide solution
Remarks:
*1: List of Appropriate Acid：
Material
Polymers
Metals
Electronics
Analyzed by UV-VIS
Acid Added for Digestion
HNO3,HCl,HF,H2O2,H3BO3
HNO3,HCl,HF
HNO3,HCl,H2O2,HBF4
*2: If the result of spot test is positive, Chromium VI would be determined as detected.
Page 4 of 6
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00233073
Test Conducted
(Ⅳ) Measurement Flowchart:
Test for Halogen Content
Reference Standard：EN 14582
Sampling/grinding or
cutting
Add absorbent in a
combustion flask &
place weighed sample in
equipment
Fill oxygen into
calorimetric bomb
Ignite then leave the
flask at room
temperature
Transfer the absorbent
into a volumetric flask
Make up with deionized
water
Analyzed by ion
chromatography
End of Report
Page 5 of 6
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00233073
Test Conducted
Photo
Page 6 of 6
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
TWNCo0240906
TeaE R€DoTt
Applicant:
T i 1-f6l
l,'ca
Dhilinhirae
Jan 79, 20!2
Th.
LIMA Technologry Center,
Lipa
CiEy,
one (1) sroup
of submitsted samples said to be :
'Solder
Part Nu.arber
| 692320
DaEe Sample Received
I Ja'r 16, 2012
Datse Tests Started
. JaIr 16, 2412
TesE Conducled :
As requestsed by Lhe applicanE,
Authorized
or
Il-hF
Taiwan
!
for
deEails
please
refer
to attached
paqres,
By:
o.
.rta_tFt
'Tesriro
Services
Liinited
shall nol be reproduced
This report
except in fu1l, wilhout the written
approval of the laboratory.
IntertekTesting ServlcesTaiwanLtd.
8F., No. 423, RuiguangRd., NeihuOistdct,Taipel 114, Taiwan R O C.
tEA*&&&6E FAA
1145ltfi^*EH,6B423 S8||
rerr(+886'2)6€02-28882797-8885Fax (+88F2)6602-24006602_2401
Nunber
: TWNC00240906
Conducted
Test Result
Summary :
TesL Item
Result
(ppm)
Silvery
Metal
E6avy X€tel
cadmium (cd) content
ND
T,ead (Pb) content
(Hg) conLent
Mercury
Chromium VI (Cr6 ) conlen-
92'72',73
ND
lng/kg wilh
50cm')
NeqraEive (< 0.02 )
based on weights of tesLed sample = mg/kg
Remarks: ppm = Parls per million
ND = Not' detected
= Less than
<
per kilogram witsh 50 square centsimetre
mg/ks wiLh 5ocm'1= millisram
observaLion
=
indicaLed positive
test
result
A
negatsive
Negatsive
was nots found at lhe tsiine of Test.
Responsibility
of Chemist
Date Sample Received
Tests Perlod
(tr)
: Irene
Chiou / Kevin Liu
I Ja 16, 20L2
: L T a n1 6 , 2 0 1 2 T o J a n 1 9 , 2 0 1 2
RoHS Requirements:
Substances
Restrrcted
(cd)
ConEent
cadnd unl
Lead
(Pb)
0 . 0 1 * (1 0 o p p m )
0.1t (100oppm)
0.1t (100oppm)
0.1t (t00oppm)
Content
(Eg) ConLent
Mercury
Chromium vr tCr6t) Conlent
The above limitss were quotsed from 2AO2/95/EC and amendnent 2OO5/6lA/EC tor
homogeneous material,
PaEre 2 of
htenek T€tlng Servic* Taiwan Ltd.
Rd.,NeihuDistnclTaiper'll4 TaiwanR o C
8F , No 423,Ruiguang
4EaB*fr&6€&AE
114alhft^*Efl)t*423is|l
Tel:r+88e2)e6o2'2888 27974885 Fax (+88G2)6602-24006602_2401
5
Numlcer : 1\^1NC00240906
Tests Conducted
( I I I ) Test Metshod:
Cadrnium (Cd)
Lead (Pb) conlent
Mercury (Hs)
chromiun vr
(cr5*)
(mg/k€'witsh 50cm')
Remark:
ReporEingr
Tests Method
With reference to IEC 62321 edition
1.0r2008 in clause 8/9/10, by
lhe tested
nricrowawe digest.ion until
samples are Lotalfy dissolved and
deterndned by ICP-OES.
jgiLh reference to IEC 62321 ediLion
1.0:2008 in cLause 8/9/10, by
tshe testsed
microwave digestsion until
dissolved and
samples are totally
deLeimi'led by ICP-OES.
llith reference to IEC 62321 edition
1.0:2008 in clause 7r by microitave
Cigestsion unLil Ehe tested samples are
dissolved and delermined by
totally
TCP-OES.
With reference lo IEC 62321 ediEion
1.0:2008 in annex B, bY boilinq water
and determined by W-vis
extraction
limit
= Quantitalion
limit
of
analvte
in
lntertek T€tlng Service3 Taiwan Ltd.
Rd.,NeihuDi{nd, Taipei114 TaiwanR.Oc
8f., No.423,Ruiguang
EEAE*R&6€EAE
114elLfi ^xE*)tlg423i0||
, 2?974885Fax:(+88&2)
6602_2401
6602-2400
6602-28a8
Tel:(+88e2)
Reportins
1,imit
2 ppm
2 ppm
2 ppm
0.02
mgr/kg witsh 5ocm'z
sample
Numloer : TWNCo0240906
TesL Conducted
(IV) Measurdent
Florchari::
Test For Cd/Pb/HSlChxomlum (VI)
Reference SLandaid: rEC 6232a ediLion
sartplirs/grlldins
applolliate
contim
Malyzed
1.0:2008
or cultins
acid't
lhe
tesied
bY IcP
ols
Make up witn
calbazide
"li
List
d€ionized
solution
Of Applopliate
Acid
Added
Fof
Digestion
lNor Hc1, HF,H,O) HIBOr
ENO3.lIC1,HF
HNOr HCl, E)O, nBF.
*2:
If
the lesu1t
of
spot test
is posiEive,
Chronim
VI would L'e detennined
aE detected'
End of
Report
Page
Inte(€k Testing Se.vicesTalwan Ltd.
Taipei114,Taiwan,R O C.
Rd.,NeihuOistncl,
8F.,No.423,Ruiguang
EEAE**&6EEAA
1146ltfifrflEHrfB423 r 8|
6602-2400
6@2-2'101
27sru885 Fsx(+88€'2)
T€li(+846'2)
6602-2884
4 of
5
Nunilcer : T!']Nc00240906
TesE Conductsed
Photo
IntertekT€tlng servic* TaiwanLtd.
8F., No. 423, RuiguangRd., NeihuOistriol.Taipei 114, Taiwan,R O C.
6daa&&&6€'F'
E
114altfifrfl[Hr69423 s 8l
66022',101
6602_2400
Fa( (+8a6-2)
faroa€6-2tefo2'28f€2J97_3835
Number : TWNC00256916
Test Report
Applicant:
Littelfuse Philippines Inc.
LIMA Technology Center, Lipa City,
Malvar, Batangas
Date
: May 16, 2012
Sample Description:
One (1) group of submitted samples said to be :
Part Description
: Ink
Part Number
: 425672
Date Sample Received
: May 10, 2012
Date Test Started
: May 10, 2012
Test Conducted :
As requested by the applicant, for details please refer to attached pages.
Authorized By:
On Behalf Of Intertek Testing Services
Taiwan Limited
K. Y. Liang
Director
This report shall not be reproduced
except in full, without the written
approval of the laboratory.
Page 1 of 9
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00256916
Test Conducted
(Ⅰ) Test Result Summary :
Test Item
Heavy Metal
Cadmium (Cd) content
Lead (Pb) content
Mercury (Hg) content
Chromium VI (Cr6+) content
Polybrominated Biphenyls (PBBs)
Monobrominated Biphenyls (MonoBB)
Dibrominated Biphenyls (DiBB)
Tribrominated Biphenyls (TriBB)
Tetrabrominated Biphenyls (TetraBB)
Pentabrominated Biphenyls (PentaBB)
Hexabrominated Biphenyls (HexaBB)
Heptabrominated Biphenyls (HeptaBB)
Octabrominated Biphenyls (OctaBB)
Nonabrominated Biphenyls (NonaBB)
Decabrominated Biphenyl (DecaBB)
Polybrominated Diphenyl Ethers (PBDEs)
Monobrominated Diphenyl Ethers (MonoBDE)
Dibrominated Diphenyl Ethers (DiBDE)
Tribrominated Diphenyl Ethers (TriBDE)
Tetrabrominated Diphenyl Ethers (TetraBDE)
Pentabrominated Diphenyl Ethers (PentaBDE)
Hexabrominated Diphenyl Ethers (HexaBDE)
Heptabrominated Diphenyl Ethers (HeptaBDE)
Octabrominated Diphenyl Ethers (OctaBDE)
Nonabrominated Diphenyl Ethers (NonaBDE)
Decabrominated Diphenyl Ether (DecaBDE)
Halogen Content
Fluorine (F)
Chlorine (Cl)
Bromine (Br)
Iodine (I)
Result (ppm)
Black Paste
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Page 2 of 9
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00256916
Test Conducted
(Ⅰ) Test Result Summary :
Test Item
Result (ppm)
Black Paste
Phthalates
Di(2-ethylhexyl) Phthalate (DEHP)
Dibutyl Phthalate (DBP)
Benzyl Butyl Phthalate (BBP)
Others
Hexabromocyclododecane (HBCDD)
ND
ND
ND
ND
Remarks: ppm = Parts per million based on wet weight of tested sample =
mg/kg
ND = Not detected
Responsibility of Chemist : Irene Chiou / Kevin Liu / Cathy Chen
Date Sample Received
Test Period
: May 10, 2012
: May 10, 2012 To May 16, 2012
(Ⅱ) RoHS Requirement:
Restricted Substances
Cadmium (Cd) Content
Lead (Pb) Content
Mercury (Hg) Content
Chromium VI (Cr6+) Content
Polybrominated Biphenyls (PBBs)
Polybrominated Diphenyl Ehters (PBDEs)
Limits
0.01% (100ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for
homogeneous material.
Page 3 of 9
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00256916
Test Conducted
(Ⅲ) Test Method:
Test Item
Test Method
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
Cadmium (Cd)
microwave digestion until the tested
content
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
Lead (Pb) content
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 7, by microwave
Mercury (Hg)
digestion until the tested samples are
content
totally dissolved and determined by
ICP-OES.
With reference to IEC 62321 edition
6+
Chromium VI (Cr ) 1.0:2008 in annex C, by alkaline
content
digestion and determined by UV-Vis
spectrophotometer.
With reference to IEC 62321 edition
1.0:2008 in annex A, by solvent
Polybrominated
extraction and determined by GC-MS and
Biphenyls (PBBs)
further HPLC-DAD confirmation when
necessary.
With reference to IEC 62321 edition
Polybrominated
1.0:2008 in annex A, by solvent
Diphenyl Ethers
extraction and determined by GC-MS and
(PBDEs)
further HPLC-DAD confirmation when
necessary.
With reference to EN 14582:2007 by
Halogen Content
calorimetric bomb with oxygen and
determined by Ion Chromatograph.
With reference to EN 14372: 2004, by
Phthalates
solvent extraction and determined by
GC-MS.
With reference to USEPA 3540C, by
Hexabromocyclodode
solvent extraction and determined by
cane (HBCDD)
GC-MSD.
Reporting Limit
2 ppm
2 ppm
2 ppm
1 ppm
5 ppm
5 ppm
50 ppm
10 ppm
10 ppm
Remark: Reporting limit = Quantitation limit of analyte in sample
Page 4 of 9
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00256916
Test Conducted
(Ⅳ) Measurement Flowchart:
Test for Cd/Pb/Hg/Chromium (VI)/PBBS/PBDES Contents
Reference Standard: IEC 62321 edition 1.0:2008
Sample preparation
For non-metal part
For metal part
Take sample and immerse into Aqua Regia, start to strip plating layer
Stop the stripping procedure upon color change completely
Take the Aqua solution as plating component and stripped body as substrate component
Cd/Pb/Hg
Cr
Weigh sample and
add organic solvent
By spot test
Negative
Confirm the tested
samples are
totally dissolved
Make up with
deionized water
PBBs/PBDEs
Polymers /
electronics
Metal
For different
material, digest
the sample with
*1
appropriate acid
6+
Get 50cm2 sample
By boiling water
extraction
*2
Weigh sample
and add
alkaline
solution
By Soxhlet
extraction or
Solvent extraction
Definite temp.
extraction
Cool and filter
the extract
Analyzed by ICP-OES
Concentrate the
extract and make up
with organic
solvent
Analyzed by GC-MSD
Make up with deionized
water and add diphenylcarbazide solution
Analyzed by UV-VIS
Remarks:
*1: List of Appropriate Acid：
Acid Added for Digestion
Material
Polymers
HNO3,HCl,HF,H2O2,H3BO3
Metals
HNO3,HCl,HF
Electronics
HNO3,HCl,H2O2,HBF4
*2: If the result of spot test is positive, Chromium VI would be determined as detected.
Page 5 of 9
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00256916
Test Conducted
(Ⅳ) Measurement Flowchart:
Test for Halogen Content
Reference Standard：EN 14582
Sampling/grinding or
cutting
Add absorbent in a
combustion flask &
place weighed sample in
equipment
Fill oxygen into
calorimetric bomb
Ignite then leave the
bomb at room
temperature
Transfer the absorbent
into a volumetric flask
Make up with deionized
water
Analyzed by ion
chromatography
Page 6 of 9
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00256916
Test Conducted
(Ⅳ) Measurement Flowchart:
Test For Phthalates Contents
Reference Method: EN 14372: 2004
Sampling/grinding or
cutting
Weigh sample and add
organic solvent
By solvent extraction
Concentrate the extract
and make up with
organic solvent
Analyzed by GC-MSD
Page 7 of 9
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00256916
Test Conducted
(Ⅳ) Measurement Flowchart:
Test For Hexabromocyclododecane (HBCDD)
Reference Standard：USEPA 3540C
Sampling/grinding or cutting
Weigh sample and add organic
solvent
By soxhlet extraction
Concentrate the extract and
make up with organic solvent
Analyzed by GC-MSD
End of Report
Page 8 of 9
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00256916
Test Conducted
Photo
Page 9 of 9
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Intertek Testing Services Ltd., Shanghai
TFH Division
Block B, Jinling Business Square,No.801 Yi Shan Road,
Shanghai, China, 200233
Tel: +86 21 6120 6565
Fax: +86 21 6127 9740
www.intertek.com
www.intertek.com.cn
China Toll-Free: 800 999 1338
TEST REPORT
APPLICANT: LITTELFUSE,INC.
800 E. NORTHWEST HWY
ATTN: A. CESISTA/ K. BACILA
NUMBER: SHAH00287549
DATE: OCT 31, 2011
SAMPLE DESCRIPTION:
One (1) submitted sample said to be: Blue ink.
Part Description
: Ink - blue.
Part Number
: 425904.
Date Sample Received
: Oct.25, 2011.
Date Test Started
: Oct.25, 2011.
***********************************************************************
TESTS CONDUCTED:
AS REQUESTED BY THE APPLICANT, FOR DETAILS REFER TO ATTACHED PAGE(S)
**********************************************************************
TO BE CONTINUED
PREPARED AND CHECKED BY:
FOR INTERTEK TESTING SERVICES
LTD., SHANGHAI
AUTHORIZED BY:
FOR INTERTEK TESTING SERVICES
LTD., SHANGHAI
MYRA LV
CHEMICAL LAB SENIOR MANAGER
STEPHEN TSANG
GENERAL MANAGER
PAGE 1 OF 14
Intertek Testing Services Ltd., Shanghai
TFH Division
Block B, Jinling Business Square,No.801 Yi Shan Road,
Shanghai, China, 200233
Tel: +86 21 6120 6565
Fax: +86 21 6127 9740
www.intertek.com
www.intertek.com.cn
China Toll-Free: 800 999 1338
TEST REPORT
NUMBER: SHAH00287549
TESTS CONDUCTED
1
PHTHALATE CONTENT TEST
WITH REFERENCE TO EN14372, BY GAS CHROMATOGRAPHY-MASS
SPECTROMETRY (GC-MS) ANALYSIS.
TESTED COMPOUND
DIBUTYL PHTHALATE (DBP)
DI(2-ETHYL HEXYL) PHTHALATE(DEHP)
BENZYL BUTYL PHTHALATE (BBP)
SUM OF THREE PHTHALATES
RESULT (%,W/W)
ND
ND
ND
ND
LIMIT(%,W/W)
(MAX.)
------0.1
REMARK：THE ABOVE LIMIT WAS QUOTED ACCORDING TO ANNEX XVII
ITEMS 51 & 52 OF THE REACH REGULATION (EC) NO. 1907/2006
& AMENDENT NO.552/2009 (FORMERLY KNOWN AS DIRECTIVE
2005/84/EC) FOR PHTHALATE CONTENT IN TOYS AND CHILDREN
CARE ARTICLES.
DETECTION LIMIT = 0.01%(W/W)
ND = NOT DETECTED
**********************************************************************
TO BE CONTINUED
PAGE 2 OF 14
Intertek Testing Services Ltd., Shanghai
TFH Division
Block B, Jinling Business Square,No.801 Yi Shan Road,
Shanghai, China, 200233
Tel: +86 21 6120 6565
Fax: +86 21 6127 9740
www.intertek.com
www.intertek.com.cn
China Toll-Free: 800 999 1338
TEST REPORT
NUMBER: SHAH00287549
TESTS CONDUCTED
MEASUREMENT FLOWCHART:
TEST FOR PHTHALATES (EN14372) CONTENTS
Weigh sample and
place in a thimble
Extracted by Soxhlet
extraction with
organic solvent for
6 hours
Concentrate the
extract
Transfer the extract
into a volumetric
flask
Make up with organic
solvent
Analyze by GC-MSD
**********************************************************************
TO BE CONTINUED
PAGE 3 OF 14
Intertek Testing Services Ltd., Shanghai
TFH Division
Block B, Jinling Business Square,No.801 Yi Shan Road,
Shanghai, China, 200233
Tel: +86 21 6120 6565
Fax: +86 21 6127 9740
www.intertek.com
www.intertek.com.cn
China Toll-Free: 800 999 1338
TEST REPORT
NUMBER: SHAH00287549
TESTS CONDUCTED
2 (Ⅰ) Test Result Summary :
Testing Item
Halogen Content
Fluorine (F)
Chlorine (Cl)
Bromine (Br)
Iodine (I)
Result (ppm)
ND
500
ND
ND
Remarks: ppm = Parts per million based on weight of tested sample =
mg/kg
ND = Not detected
Responsibility Of Chemist
Date Sample Received
Testing Period
(Ⅱ) Test Method:
Testing Item
Halogen Content
: Ken He
: OCT.25, 2011
: OCT.28, 2011
Testing Method
With reference to EN 14582:2007 by
combustion flask with oxygen and
determined by ion chromatography
Reporting Limit
50 ppm
Remark: Reporting limit = Quantitation limit of analyte in sample
***********************************************************************
TO BE CONTINUED
PAGE 4 OF 14
Intertek Testing Services Ltd., Shanghai
TFH Division
Block B, Jinling Business Square,No.801 Yi Shan Road,
Shanghai, China, 200233
Tel: +86 21 6120 6565
Fax: +86 21 6127 9740
www.intertek.com
www.intertek.com.cn
China Toll-Free: 800 999 1338
TEST REPORT
NUMBER: SHAH00287549
TESTS CONDUCTED
(Ⅲ) Measurement Flowchart:
Test For Halogen Content
Reference Standard： EN 14582
sampling/grinding or
cutting
add absorbent in a
combustion flask &
place weighed sample in
equipment
fill the combustion
flask with oxygen
ignite then leave the
flask at room
temperature
transfer the absorbent
into a volumetric flask
make up with deionized
water
analyzed by ion
chromatography
************************************************************************
TO BE CONTINUED
PAGE 5 OF 14
Intertek Testing Services Ltd., Shanghai
TFH Division
Block B, Jinling Business Square,No.801 Yi Shan Road,
Shanghai, China, 200233
Tel: +86 21 6120 6565
Fax: +86 21 6127 9740
www.intertek.com
www.intertek.com.cn
China Toll-Free: 800 999 1338
TEST REPORT
NUMBER: SHAH00287549
TESTS CONDUCTED
3 (Ⅰ) Test Result Summary :
Result (ppm)
Testing Item
Heavy Metal
Cadmium (Cd) content
ND
Lead (Pb) content
ND
Mercury (Hg) content
ND
6+
Chromium VI (Cr ) content
ND
Polybrominated Biphenyls (PBBs)
Monobrominated Biphenyls (MonoBB)
ND
Dibrominated Biphenyls (DiBB)
ND
Tribrominated Biphenyls (TriBB)
ND
Tetrabrominated Biphenyls (TetraBB)
ND
Pentabrominated Biphenyls (PentaBB)
ND
Hexabrominated Biphenyls (HexaBB)
ND
Heptabrominated Biphenyls (HeptaBB)
ND
Octabrominated Biphenyls (OctaBB)
ND
Nonabrominated Biphenyls (NonaBB)
ND
Decabrominated Biphenyl (DecaBB)
ND
Polybrominated Diphenyl Ethers (PBDEs)
Monobrominated Diphenyl Ethers (MonoBDE)
ND
Dibrominated Diphenyl Ethers (DiBDE)
ND
Tribrominated Diphenyl Ethers (TriBDE)
ND
Tetrabrominated Diphenyl Ethers (TetraBDE)
ND
Pentabrominated Diphenyl Ethers (PentaBDE)
ND
Hexabrominated Diphenyl Ethers (HexaBDE)
ND
Heptabrominated Diphenyl Ethers (HeptaBDE)
ND
Octabrominated Diphenyl Ethers (OctaBDE)
ND
Nonabrominated Diphenyl Ethers (NonaBDE)
ND
Decabrominated Diphenyl Ether (DecaBDE)
ND
************************************************************************
TO BE CONTINUED
PAGE 6 OF 14
Intertek Testing Services Ltd., Shanghai
TFH Division
Block B, Jinling Business Square,No.801 Yi Shan Road,
Shanghai, China, 200233
Tel: +86 21 6120 6565
Fax: +86 21 6127 9740
www.intertek.com
www.intertek.com.cn
China Toll-Free: 800 999 1338
TEST REPORT
NUMBER: SHAH00287549
TESTS CONDUCTED
Remarks: ppm = Parts per million = mg/kg
ND = Not detected
Responsibility Of Chemist : Dent Fang / Ken He
Date Sample Received
Testing Period
: OCT.28, 2011
: OCT.28, 2011
(Ⅱ) RoHS Requirement:
Restricted Substances
Cadmium (Cd) Content
Lead (Pb) Content
Mercury (Hg) Content
Chromium VI (Cr6+) Content
Polybrominated Biphenyls (PBBs)
Polybrominated Diphenyl Ehters (PBDEs)
Limits
0.01% (100ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
The above limits were quoted from 2002/95/EC and amendment
2005/618/EC for homogeneous material.
************************************************************************
TO BE CONTINUED
PAGE 7 OF 14
Intertek Testing Services Ltd., Shanghai
TFH Division
Block B, Jinling Business Square,No.801 Yi Shan Road,
Shanghai, China, 200233
Tel: +86 21 6120 6565
Fax: +86 21 6127 9740
www.intertek.com
www.intertek.com.cn
China Toll-Free: 800 999 1338
TEST REPORT
NUMBER: SHAH00287549
TESTS CONDUCTED
(Ⅲ) Test Method:
Testing Item
Testing Method
Reporting Limit
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
Cadmium (Cd)
microwave digestion until the
2 ppm
content
tested samples are totally
dissolved and determined by ICPOES.
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the
Lead (Pb) content
2 ppm
tested samples are totally
dissolved and determined by ICPOES.
With reference to IEC 62321 edition
1.0:2008 in clause 7, by microwave
Mercury (Hg)
digestion until the tested samples
2 ppm
content
are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
Chromium VI (Cr6+) 1.0:2008 in annex C, by alkaline
1 ppm
content
digestion and determined by UV-Vis
spectrophotometer.
With reference to IEC 62321 edition
1.0:2008 in annex A, by solvent
Polybrominated
extraction and determined by GC-MSD
5 ppm
Biphenyls (PBBs)
and further HPLC confirmation when
necessary.
With reference to IEC 62321 edition
Polybrominated
1.0:2008 in annex A, by solvent
Diphenyl Ethers
extraction and determined by GC-MSD
5 ppm
(PBDEs)
and further HPLC confirmation when
necessary.
Remark: Reporting limit = Quantitation limit of analyte in sample
************************************************************************
TO BE CONTINUED
PAGE 8 OF 14
Intertek Testing Services Ltd., Shanghai
TFH Division
Block B, Jinling Business Square,No.801 Yi Shan Road,
Shanghai, China, 200233
Tel: +86 21 6120 6565
Fax: +86 21 6127 9740
www.intertek.com
www.intertek.com.cn
China Toll-Free: 800 999 1338
TEST REPORT
NUMBER: SHAH00287549
TESTS CONDUCTED
(Ⅳ) Measurement Flowchart:
Test For Cd/Pb/Hg/Chromium (VI)/PBBs/PBDEs Contents
Reference Standard: IEC 62321 edition 1.0:2008
************************************************************************
TO BE CONTINUED
PAGE 9 OF 14
Intertek Testing Services Ltd., Shanghai
TFH Division
Block B, Jinling Business Square,No.801 Yi Shan Road,
Shanghai, China, 200233
Tel: +86 21 6120 6565
Fax: +86 21 6127 9740
www.intertek.com
www.intertek.com.cn
China Toll-Free: 800 999 1338
TEST REPORT
NUMBER: SHAH00287549
TESTS CONDUCTED
4
PHTHALATE CONTENT TEST
WITH REFERENCE TO ASTM D3421, BY GAS CHROMATOGRAPHY-MASS
SPECTROMETRY (GC-MS) ANALYSIS.
RESULT (%, w/w) LIMIT (%, w/w)
(MAX.)
DIBUTYL PHTHALATE (DBP)
DI(2-ETHYL HEXYL) PHTHALATE (DEHP)
BENZYL BUTYL PHTHALATE (BBP)
ND
ND
ND
0.1
0.1
0.1
REMARK：THE ABOVE LIMIT WAS QUOTED ACCORDING TO US CONSUMER
PRODUCT SAFETY IMPROVEMENT ACT 2008 FOR PROHIBITION ON
SALE OF CERTAIN PRODUCTS CONTAINING SPECIFIED PHTHALATES.
DETECTION LIMIT = 0.01% (w/w)
ND = NOT DETECTED
**********************************************************************
TO BE CONTINUED
PAGE 10 OF 14
Intertek Testing Services Ltd., Shanghai
TFH Division
Block B, Jinling Business Square,No.801 Yi Shan Road,
Shanghai, China, 200233
Tel: +86 21 6120 6565
Fax: +86 21 6127 9740
www.intertek.com
www.intertek.com.cn
China Toll-Free: 800 999 1338
TEST REPORT
NUMBER: SHAH00287549
TESTS CONDUCTED
MEASUREMENT FLOWCHART:
TEST FOR PHTHALATES (ASTM D3421) CONTENTS
Weigh sample and
place in a thimble
Extracted by Soxhlet
extraction with
organic solvent for
16 hours
Concentrate the
extract
Transfer the extract
into a volumetric
flask
Make up with organic
solvent
Analyze by GC-MSD
**********************************************************************
TO BE CONTINUED
PAGE 11 OF 14
Intertek Testing Services Ltd., Shanghai
TFH Division
Block B, Jinling Business Square,No.801 Yi Shan Road,
Shanghai, China, 200233
Tel: +86 21 6120 6565
Fax: +86 21 6127 9740
www.intertek.com
www.intertek.com.cn
China Toll-Free: 800 999 1338
TEST REPORT
NUMBER: SHAH00287549
TESTS CONDUCTED
5 (A) TEST RESULT SUMMARY:
TESTING ITEM
HBCDD (HEXABROMOCYCLODODECANE)
RESULT(ppm)
ND
REMARKS:
ppm = PARTS PER MILLION = mg/kg
ND = NOT DETECTED
(B) TEST METHOD :
TESTING ITEM
TESTING METHOD
WITH REFERENCE TO USEPA
3540C, BY SOLVENT
HBCDD (HEXABROMOCYCLODODECANE)
EXTRACTION AND DETERMINED
BY GC/MS
REPORTING
LIMIT
10 ppm
DATE SAMPLE RECEIVED : OCT.25, 2011
TESTING PERIOD : OCT.25, 2011 TO OCT.28, 2011
**********************************************************************
TO BE CONTINUED
PAGE 12 OF 14
Intertek Testing Services Ltd., Shanghai
TFH Division
Block B, Jinling Business Square,No.801 Yi Shan Road,
Shanghai, China, 200233
Tel: +86 21 6120 6565
Fax: +86 21 6127 9740
www.intertek.com
www.intertek.com.cn
China Toll-Free: 800 999 1338
TEST REPORT
NUMBER: SHAH00287549
TESTS CONDUCTED
MEASUREMENT FLOWCHART:
TEST FOR HBCDD (Hexabromocyclododecane) CONTENT
Weigh sample and place
into a thimble
Soxhlet extraction with
organic solvent
Concentrate the extract
Transfer the extract
into a volumetric flask
Make up with organic
solvent
Analyze by GC-MSD
**********************************************************************
TO BE CONTINUED
PAGE 13 OF 14
Intertek Testing Services Ltd., Shanghai
TFH Division
Block B, Jinling Business Square,No.801 Yi Shan Road,
Shanghai, China, 200233
Tel: +86 21 6120 6565
Fax: +86 21 6127 9740
www.intertek.com
www.intertek.com.cn
China Toll-Free: 800 999 1338
TEST REPORT
NUMBER: SHAH00287549
TESTS CONDUCTED
**********************************************************************
END OF REPORT
PAGE 14 OF 14
Test Report
Applicant:
Littelfuse Philippines Inc.
LIMA Technology Center, Lipa City,
Malvar, Batangas
Number
: TWNC00256915
Date
: May 15, 2012
Sample Description:
One (1) group of submitted samples said to be :
Part Description
: Green Ink
Part Number
: 425819
Date Sample Received
: May 10, 2012
Date Test Started
: May 10, 2012
Test Conducted :
As requested by the applicant, for details please refer to attached pages.
Authorized By:
On Behalf Of Intertek Testing Services
Taiwan Limited
K. Y. Liang
Director
This report shall not be reproduced
except in full, without the written
approval of the laboratory.
Page 1 of 9
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number:
TWNC00256915
Test Conducted
(Ⅰ) Test Result Summary :
Test Item
Heavy Metal
Cadmium (Cd) content
Lead (Pb) content
Mercury (Hg) content
Chromium VI (Cr6+) content
Polybrominated Biphenyls (PBBs)
Monobrominated Biphenyls (MonoBB)
Dibrominated Biphenyls (DiBB)
Tribrominated Biphenyls (TriBB)
Tetrabrominated Biphenyls (TetraBB)
Pentabrominated Biphenyls (PentaBB)
Hexabrominated Biphenyls (HexaBB)
Heptabrominated Biphenyls (HeptaBB)
Octabrominated Biphenyls (OctaBB)
Nonabrominated Biphenyls (NonaBB)
Decabrominated Biphenyl (DecaBB)
Polybrominated Diphenyl Ethers (PBDEs)
Monobrominated Diphenyl Ethers (MonoBDE)
Dibrominated Diphenyl Ethers (DiBDE)
Tribrominated Diphenyl Ethers (TriBDE)
Tetrabrominated Diphenyl Ethers (TetraBDE)
Pentabrominated Diphenyl Ethers (PentaBDE)
Hexabrominated Diphenyl Ethers (HexaBDE)
Heptabrominated Diphenyl Ethers (HeptaBDE)
Octabrominated Diphenyl Ethers (OctaBDE)
Nonabrominated Diphenyl Ethers (NonaBDE)
Decabrominated Diphenyl Ether (DecaBDE)
Halogen Content
Fluorine (F)
Chlorine (Cl)
Bromine (Br)
Iodine (I)
Result (ppm)
Submitted Samples
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
7316
6027
ND
Page 2 of 9
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number:
TWNC00256915
Test Conducted
(Ⅰ) Test Result Summary :
Test Item
Result (ppm)
Submitted Samples
Phthalates
Di(2-ethylhexyl) Phthalate (DEHP)
Dibutyl Phthalate (DBP)
Benzyl Butyl Phthalate (BBP)
Others
Hexabromocyclododecane (HBCDD)
ND
ND
ND
ND
Remarks: ppm = Parts per million based on wet weight of tested sample = mg/kg
ND = Not detected
Responsibility of Chemist : Irene Chiou / Kevin Liu / Cathy Chen
Date Sample Received
Test Period
: May 10, 2012
: May 10, 2012 To May 14, 2012
(Ⅱ) RoHS Requirement:
Restricted Substances
Cadmium (Cd) Content
Lead (Pb) Content
Mercury (Hg) Content
Chromium VI (Cr6+) Content
Polybrominated Biphenyls (PBBs)
Polybrominated Diphenyl Ehters (PBDEs)
Limits
0.01% (100ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for
homogeneous material.
Page 3 of 9
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number:
TWNC00256915
Test Conducted
(Ⅲ) Test Method:
Test Item
Test Method
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
Cadmium (Cd)
microwave digestion until the tested
content
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
Lead (Pb) content
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 7, by microwave
Mercury (Hg)
digestion until the tested samples are
content
totally dissolved and determined by
ICP-OES.
With reference to IEC 62321 edition
Chromium VI (Cr6+) 1.0:2008 in annex C, by alkaline
digestion and determined by UV-Vis
content
spectrophotometer.
With reference to IEC 62321 edition
1.0:2008 in annex A, by solvent
Polybrominated
extraction and determined by GC-MS and
Biphenyls (PBBs)
further HPLC-DAD confirmation when
necessary.
With reference to IEC 62321 edition
Polybrominated
1.0:2008 in annex A, by solvent
Diphenyl Ethers
extraction and determined by GC-MS and
further HPLC-DAD confirmation when
(PBDEs)
necessary.
With reference to EN 14582:2007 by
Halogen Content
calorimetric bomb with oxygen and
determined by Ion Chromatograph.
With reference to EN 14372: 2004, by
Phthalates
solvent extraction and determined by
GC-MS.
With reference to USEPA 3540C, by
Hexabromocyclodode
solvent extraction and determined by
cane (HBCDD)
GC-MSD.
Reporting Limit
2 ppm
2 ppm
2 ppm
1 ppm
5 ppm
5 ppm
50 ppm
10 ppm
10 ppm
Remark: Reporting limit = Quantitation limit of analyte in sample
Page 4 of 9
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number:
TWNC00256915
Test Conducted
(Ⅳ) Measurement Flowchart:
Test for Cd/Pb/Hg/Chromium (VI)/PBBS/PBDES Contents
Reference Standard: IEC 62321 edition 1.0:2008
Sample preparation
For non-metal part
For metal part
Take sample and immerse into Aqua Regia, start to strip plating layer
Stop the stripping procedure upon color change completely
Take the Aqua solution as plating component and stripped body as substrate component
Cd/Pb/Hg
Cr
Weigh sample and
add organic solvent
By spot test
Negative
Confirm the tested
samples are
totally dissolved
Make up with
deionized water
PBBs/PBDEs
Polymers /
electronics
Metal
For different
material, digest
the sample with
*1
appropriate acid
6+
Get 50cm2 sample
By boiling water
extraction
*2
Weigh sample
and add
alkaline
solution
By Soxhlet
extraction or
Solvent extraction
Definite temp.
extraction
Cool and filter
the extract
Analyzed by ICP-OES
Concentrate the
extract and make up
with organic
solvent
Analyzed by GC-MSD
Make up with deionized
water and add diphenylcarbazide solution
Analyzed by UV-VIS
Remarks:
*1: List of Appropriate Acid：
Material
Polymers
Metals
Electronics
Acid Added for Digestion
HNO3,HCl,HF,H2O2,H3BO3
HNO3,HCl,HF
HNO3,HCl,H2O2,HBF4
*2: If the result of spot test is positive, Chromium VI would be determined as detected.
Page 5 of 9
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number:
TWNC00256915
Test Conducted
(Ⅳ) Measurement Flowchart:
Test for Halogen Content
Reference Standard：EN 14582
Sampling/grinding or
cutting
Add absorbent in a
combustion flask &
place weighed sample in
equipment
Fill oxygen into
calorimetric bomb
Ignite then leave the
bomb at room
temperature
Transfer the absorbent
into a volumetric flask
Make up with deionized
water
Analyzed by ion
chromatography
Page 6 of 9
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number:
TWNC00256915
Test Conducted
(Ⅳ) Measurement Flowchart:
Test For Phthalates Contents
Reference Method: EN 14372: 2004
Sampling/grinding or
cutting
Weigh sample and add
organic solvent
By solvent extraction
Concentrate the extract
and make up with
organic solvent
Analyzed by GC-MSD
Page 7 of 9
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number:
TWNC00256915
Test Conducted
(Ⅳ) Measurement Flowchart:
Test For Hexabromocyclododecane (HBCDD)
Reference Standard：USEPA 3540C
Sampling/grinding or cutting
Weigh sample and add organic
solvent
By soxhlet extraction
Concentrate the extract and
make up with organic solvent
Analyzed by GC-MSD
End of Report
Page 8 of 9
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number:
TWNC00256915
Test Conducted
Photo
Page 9 of 9
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00233070
Test Report
Applicant:
Littelfuse Philippines Inc.
LIMA Technology Center, Lipa City,
Malvar, Batangas
Date
: Nov 28, 2011
Sample Description:
One (1) group of submitted samples said to be :
Part Description
: Red ink
Part Number
: 425818
Date Sample Received
: Nov 17, 2011
Date Test Started
: Nov 18, 2011
Test Conducted :
As requested by the applicant, for details please refer to attached pages.
Authorized By:
On Behalf Of Intertek Testing Services
Taiwan Limited
K. Y. Liang
Director
This report shall not be reproduced
except in full, without the written
approval of the laboratory.
Page 1 of 9
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00233070
Test Conducted
(Ⅰ) Test Result Summary :
Test Item
Result (ppm)
Submitted Samples
Heavy Metal
Cadmium (Cd) content
Lead (Pb) content
Mercury (Hg) content
Chromium VI (Cr6+) content
Polybrominated Biphenyls (PBBs)
Monobrominated Biphenyls (MonoBB)
Dibrominated Biphenyls (DiBB)
Tribrominated Biphenyls (TriBB)
Tetrabrominated Biphenyls (TetraBB)
Pentabrominated Biphenyls (PentaBB)
Hexabrominated Biphenyls (HexaBB)
Heptabrominated Biphenyls (HeptaBB)
Octabrominated Biphenyls (OctaBB)
Nonabrominated Biphenyls (NonaBB)
Decabrominated Biphenyl (DecaBB)
Polybrominated Diphenyl Ethers (PBDEs)
Monobrominated Diphenyl Ethers (MonoBDE)
Dibrominated Diphenyl Ethers (DiBDE)
Tribrominated Diphenyl Ethers (TriBDE)
Tetrabrominated Diphenyl Ethers (TetraBDE)
Pentabrominated Diphenyl Ethers (PentaBDE)
Hexabrominated Diphenyl Ethers (HexaBDE)
Heptabrominated Diphenyl Ethers (HeptaBDE)
Octabrominated Diphenyl Ethers (OctaBDE)
Nonabrominated Diphenyl Ethers (NonaBDE)
Decabrominated Diphenyl Ether (DecaBDE)
Halogen Content
Fluorine (F)
Chlorine (Cl)
Bromine (Br)
Iodine (I)
Phthalates
Di(2-ethylhexyl) Phthalate (DEHP)
Dibutyl Phthalate (DBP)
Benzyl Butyl Phthalate (BBP)
Others
Hexabromocyclododecane (HBCDD)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
5800
ND
ND
ND
ND
ND
ND
Remarks: ppm = Parts per million based on wet weight of tested sample =
mg/kg
ND = Not detected
Responsibility of Chemist : Irene Chiou / Kevin Liu / Cathy Chen
Date Sample Received
Test Period
: Nov 17, 2011
: Nov 18, 2011 To Nov 22, 2011
Page 2 of 9
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00233070
Test Conducted
(Ⅱ) RoHS Requirement:
Restricted Substances
Cadmium (Cd) Content
Lead (Pb) Content
Mercury (Hg) Content
Chromium VI (Cr6+) Content
Polybrominated Biphenyls (PBBs)
Polybrominated Diphenyl Ehters (PBDEs)
Limits
0.01% (100ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for
homogeneous material.
(Ⅲ) Test Method:
Test Item
Test Method
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
Cadmium (Cd) content microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
Lead (Pb) content
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 7, by microwave
Mercury (Hg) content digestion until the tested samples
are totally dissolved and determined
by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in annex C, by alkaline
Chromium VI (Cr6+)
content
digestion and determined by UV-Vis
spectrophotometer.
With reference to IEC 62321 edition
1.0:2008 in annex A, by solvent
Polybrominated
extraction and determined by GC-MSD
Biphenyls (PBBs)
and further HPLC confirmation when
necessary.
With reference to IEC 62321 edition
1.0:2008 in annex A, by solvent
Polybrominated
Diphenyl Ethers
extraction and determined by GC-MSD
(PBDEs)
and further HPLC confirmation when
necessary.
Reporting Limit
2 ppm
2 ppm
2 ppm
1 ppm
5 ppm
5 ppm
Page 3 of 9
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00233070
Test Conducted
(Ⅲ) Test Method:
Test Item
Test Method
With reference to EN 14582:2007 by
Halogen Content
calorimetric bomb with oxygen and
determined by ion chromatography
With reference to EN 14372: 2004, by
Phthalates
solvent extraction and determined by
GC-MSD
With reference to USEPA 3540C, by
Hexabromocyclododecane
solvent extraction and determined by
(HBCDD)
GC-MSD
Reporting Limit
50 ppm
50 ppm
10 ppm
Remark: Reporting limit = Quantitation limit of analyte in sample
Page 4 of 9
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00233070
Test Conducted
(Ⅳ) Measurement Flowchart:
Test for Cd/Pb/Hg/Chromium (VI)/PBBS/PBDES Contents
Reference Standard: IEC 62321 edition 1.0:2008
Sample preparation
For non-metal part
For metal part
Take sample and immerse into Aqua Regia, start to strip plating layer
Stop the stripping procedure upon color change completely
Take the Aqua solution as plating component and stripped body as substrate component
Cd/Pb/Hg
Cr
Confirm the tested
samples are
totally dissolved
Make up with
deionized water
PBBs/PBDEs
Polymers /
electronics
Metal
For different
material, digest
the sample with
*1
appropriate acid
6+
Weigh sample and
add organic solvent
By spot test
Negative
Get 50cm2 sample
By boiling water
extraction
*2
Weigh sample
and add
alkaline
solution
By Soxhlet
extraction or
Solvent extraction
Definite temp.
extraction
Cool and filter
the extract
Analyzed by ICP-OES
Concentrate the
extract and make up
with organic
solvent
Analyzed by GC-MSD
Make up with deionized
water and add diphenylcarbazide solution
Remarks:
*1: List of Appropriate Acid：
Material
Polymers
Metals
Electronics
Analyzed by UV-VIS
Acid Added for Digestion
HNO3,HCl,HF,H2O2,H3BO3
HNO3,HCl,HF
HNO3,HCl,H2O2,HBF4
*2: If the result of spot test is positive, Chromium VI would be determined as detected.
Page 5 of 9
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00233070
Test Conducted
(Ⅳ) Measurement Flowchart:
Test for Halogen Content
Reference Standard：EN 14582
Sampling/grinding or
cutting
Add absorbent in a
combustion flask &
place weighed sample in
equipment
Fill oxygen into
calorimetric bomb
Ignite then leave the
flask at room
temperature
Transfer the absorbent
into a volumetric flask
Make up with deionized
water
Analyzed by ion
chromatography
Page 6 of 9
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00233070
Test Conducted
(Ⅳ) Measurement Flowchart:
Test For Phthalates Contents
Reference Method: EN 14372: 2004
Sampling/grinding or
cutting
Weigh sample and add
organic solvent
By solvent extraction
Concentrate the extract
and make up with
organic solvent
Analyzed by GC-MSD
Page 7 of 9
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00233070
Test Conducted
(Ⅳ) Measurement Flowchart:
Test For Hexabromocyclododecane (HBCDD)
Reference Standard：USEPA 3540C
Sampling/grinding or cutting
Weigh sample and add organic
solvent
By soxhlet extraction
Concentrate the extract and
make up with organic solvent
Analyzed by GC-MSD
End of Report
Page 8 of 9
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00233070
Test Conducted
Photo
Page 9 of 9
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401