ICPTest_251L_with_Low_Bromine_6 15 12 pdf

ICP Test Report Certification Packet
Company name :
Littelfuse, Inc.
Product Series:
Pico
Product #:
251xxxL Series with low halogen content
Issue Date:
June 15, 2012
It is hereby certified by Littelfuse, Inc. that there is neither RoHS (EU Directive
2002/95/EC)-restricted substance nor such use, for materials to be used for unit parts, for
packing/packaging materials, and for additives and the like in the manufacturing processes.
In addition, it is hereby reported to you that the parts and sub-materials, the materials to be used
for unit parts, the packing/packaging materials, and the additives and the like in the manufacturing
processes, are all composed of the following components.
Issued by:
<Global EHS Engineer>
(1) Parts, sub-materials and unit parts
This document covers the Pico RoHS-Compliant series products manufactured by
Littelfuse, Inc.
＜ Raw Materials Used
Please see Table 1
(2) The ICP data on all measurable substances
Please see appropriate pages as identifed in Table 1
Remarks：
Pb (lead) contained in the high temperature melting solder > 85% and is categorized as
exempt under section 7a of the RoHS Annex.
Form 585-047 Rev. A
1
2/21/06
Table 1: List of Raw Materials covered by this report
Total Parts
1
2
3
4
5
6
7
Raw Material Part Number
910-xxx (910-263/ 910-023)
SIKOR C410 (909-144)
11-0803 (497xxx)
082xxx
082xxx
692320
087341
Raw Material Description
Cap and Lead Assembly
Body – Ceramic Tube
Element – Ni42Fe58MCuMAg5%
Element – 5% by weight Ag Clad Cu
Element – 2% Ag plated Cu
Solder
Epoxy Powder
2
Page(s)
3-7
8-31
32-38
39-48
39-48
49-53
54-62
Test Report
Applicant:
Number : TWNC00256249
Littelfuse Philippines Inc.
LIMA Technology Center, Lipa City,
Malvar, Batangas
Date
: May 10, 2012
Sample Description:
One (1) group of submitted samples said to be :
Part Description
: Cap and Lead Assay
Part Number
: 910-023/910-263(910XXX)
Date Sample Received
: May 07, 2012
Date Test Started
: May 09, 2012
Test Conducted :
As requested by the applicant, for details please refer to attached pages.
Authorized By:
On Behalf Of Intertek Testing Services
Taiwan Limited
K. Y. Liang
Director
This report shall not be reproduced
except in full, without the written
approval of the laboratory.
Page 1 of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00256249
Test Conducted
(Ⅰ) Test Result Summary :
Test Item
Heavy Metal
Cadmium (Cd) content
Lead (Pb) content
Mercury (Hg) content
Chromium VI (Cr6+) content (mg/kg with 50cm2)
Test Item
Heavy Metal
Cadmium (Cd) content
Lead (Pb) content
Mercury (Hg) content
Chromium VI (Cr6+) content (mg/kg with 50cm2)
Result (ppm)
(1)
(2)
ND
ND
ND
Negative
(< 0.02)
(#)
ND
55
ND
Negative
(< 0.02)
(#)
Result (ppm)
(3)
(4)
ND
ND
ND
Negative
(< 0.02)
(#)
ND
196
ND
Negative
(< 0.02)
(#)
Remarks: ppm = Parts per million based on weight of tested sample = mg/kg
ND = Not detected
<
= Less than
mg/kg with 50cm2 = milligram per kilogram with 50 square centimetre
Negative = A negative test result indicated positive observation
was not found at the time of Test.
#
= Due to the insufficient sample area, reduced total sample
surface of 10 cm2 was used and the dilution factor was
adjusted accordingly.
Tested Components
(1) Coppery Substrate(Body)
(2) Silvery Plating(Body)
(3) Coppery Substrate(Pin)
(4) Silvery Plating(Pin)
Responsibility of Chemist : Irene Chiou / Kevin Liu / Cathy Chen
Date Sample Received
Test Period
: May 07, 2012
: May 09, 2012 To May 10, 2012
Page 2 of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00256249
Test Conducted
(Ⅱ) RoHS Requirement:
Restricted Substances
Cadmium (Cd) Content
Lead (Pb) Content
Mercury (Hg) Content
Chromium VI (Cr6+) Content
Limits
0.01% (100ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for
homogeneous material.
(Ⅲ) Test Method:
Test Item
Cadmium (Cd)
content
Lead (Pb) content
Mercury (Hg)
content
Chromium VI (Cr6+)
content
Test Method
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 7, by microwave
digestion until the tested samples are
totally dissolved and determined by
ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in annex B, by boiling water
extraction and determined by UV-Vis
Spectrophotometer.
Reporting Limit
2 ppm
2 ppm
2 ppm
0.02
mg/kg with 50cm2
Remark: Reporting limit = Quantitation limit of analyte in sample
Page 3 of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00256249
Test Conducted
(Ⅳ) Measurement Flowchart:
Test for Cd/Pb/Hg/Chromium (VI)
Reference Standard：IEC 62321 edition 1.0:2008
Sample preparation
Take sample and immerse into Aqua Regia, start to strip plating layer
Stop the stripping procedure upon color change completely
Take the Aqua solution as plating component and stripped body as substrate component
Cd/Pb/Hg
Cr
Polymers /
electronics
Metal
For different
material, digest
the sample with
*1
appropriate acid
By spot test
Negative
Confirm the tested
samples are
totally dissolved
Make up with
deionized water
6+
*2
Weigh sample
and add
alkaline
solution
Get 50cm2 sample
Definite temp.
extraction
By boiling water
extraction
Cool and filter
the extract
Analyzed by ICP-OES
Make up with deionized water and add
diphenyl-carbazide solution
Remarks:
*1: List of Appropriate Acid：
Material
Polymers
Metals
Electronics
Analyzed by UV-VIS
Acid Added for Digestion
HNO3,HCl,HF,H2O2,H3BO3
HNO3,HCl,HF
HNO3,HCl,H2O2,HBF4
*2: If the result of spot test is positive, Chromium VI would be determined as detected.
End of Report
Page 4 of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00256249
Test Conducted
Photo
Page 5 of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Validit
ForQuestl
PleaseCo
TestReport
nown
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No.: CE/2012l'14848AOale: 2012102104Page: 1 of 24
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SampleDescriPtion
Styl€/ltemNo.
Date
SampleReceiving
Te6tingPeriod
CERAMIC
stKoRc410
2012101130
130'lO 201210?,04
2012101
Pleasereferto ne)dpage(s)-
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samples
t€stsonsubmitted
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Based
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and
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2002/95/EC
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PARTMME No.1
GRAYCERAIMIC
2
Result
No.t
n.d.
2
79
1000
2
n.d.
1000
2
n.d.
1000
us EPA3540c
ffi ffi Eiphe"-vElFeEJmg/Kg Wii-referencetowas
Pd),cfi
bY
Analysis Performed
method.
(CASNo.:'1336-36-3)
0.5
n.d.
to us ErA Je'+uv
with refeaence
bY
wasPerformed
Analysis
method.
GCiMS.
0.5
n.d.
5
n.d.
Te6t ltem(s)
eadmi,n(cd)
Gad (Pb)
(Hg)
Mercury
Cr(Vl)
Chromium
FExavatent
MDL
Method
Unil
mgftg With referenceto lE(; bzJzl: zuuo arru
oerformedby ICP-AES
mg/kg with referencelo lEu bztlt: zuvo 4l
oedormedbv |CPAES.
mg/Kg With @lerenceto lEu olrz r: zuuo
oerformedbv ICP-AES
mg/Kg With referenceto IEU bzlzt- z\ Jo ate
perfomed bYW-VIS
GC/MS.
-olychlorinatedNaPhthalene
(PCNs)
mg/kg Nith reference to us EPA Jc4ue
nethod.Analysiswas PerformedbY
3C/MS.
frm';;;rence to USEPA3540C
chbro(snon
C'10-13,
Alkanes,
AnalyriswasPerfomedbY
method.
(CAS
Paraffins)
ChainChlodnated
GC/MS.
No.:85535-84-8)
WliffEence to uSePnss+Oc:
m9Kg
terf luorooctanesulfonates
'1996methodfor PFOSContent
MetalSalt,Amide)
(PFOS-Acid,
AnalysiswasPer{ormedbYLC/MS
p-fqA(cAs No.:s35€7-1)
mg/Kg
WiifrEEncetouSePngsaOc:
0.01
n.d.
'10
n.d.
10
n.d.
3
n.d.
't996methodfor PFOAContent
An'lvsis wasoerfomedbYLC/MS
-t
(cnSuo.:5040-o) mg/Kg With referenceto ls(J /zzo- t\zwol
F6-atoehyae
performed by HPLC/DAo
Analvsis was
PVC
n*ffiffi$
oYr I rr\ aru
wasPenormeo
Analysis
Test.
FLAME
Negative
rrrni{
rrj ir::
Limit
'!00
Test RePort
| 3 ol24
No. : CEl2012,'14848A De/:e2O12tO2t04Page
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T€6t ltom(s)
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MOL
butylphthalate)(cAS
Bflemyl
No.:85€8-7)
./"
With referencelo EN l4J/z ^rrdrys's
wa6 DerformedbYGC/MS
0.003
No.1
n.d.
o/o
With reference to EN l4J/2. AIErysr-
0.003
n,o.
Anarysrb
0.01
n.d.
Alrcrvsl
0.01
n.d.
^narv!
0.003
n.d.
Anarys's
0.003
n.d.
to us EFAoztuu
mgKg with refefence
M6i6fretnvletngdibromociPnenYt
bY
was
0.5
n.d.
us EPn8270D
M-nomethyldichlorodiPnenYl mg/Kg @referenceo
bY
w€s
Analysis
method.
Performed
methane(Ugilec121)
0.5
n,d.
lo u! ErA 62luu
mg/K9 Nithreference
M6-nometnytaracntorodiptrenyl
wasPerfomedbY
nethod.Analysis
(Ugilec141)
methane
0.5
n.d.
0.03
n.d.
0.03
n.o,
1
n.d.
1
n.d.
(Di-(2-ethylheryD
dEHPHP
(CASNoi 1'17-81-7)
phthalate)
6i5Fi6ii$ldi
bYGC/MS.
wasDerformed
(cAs
ptrttratate)
No.:26761-40-0)
(CAS
SifiFlS sononylPhthalate)
No.:28553-12-0)
o
(Di-n-octylPhthalate)(cAs
d
No.:117-844)
o/o
(cAs No:
-BP (Ditcuvlphthalate)
u-74-2)
%
methane(DBBT)
With rcferenceto EN 14J/z
wes Derformedbv GC/MS
With rcterenceto EN l'+c/z
was performedbYGC/MS.
with referenceto EN 14c/z
was performed bYGo/MS
With rcferenceto EN 14Jlz
was oerformed bYGC/MS.
Analysis
method.
GC/MS.
Pedormed
GC/MS.
3C/MS.
Organic-lincomPounds
TributylTin OBT)
Tin (TPhT)
Triphenyl
mg/kg With €lerence to ulN Jo4u / - |o
Analysiswas PerfomedbYGC/FPD
mg/Kg With referenceto DIN Ju4u/- l,t.
Analysiswas PerfomedbYGC/FPD'
Halons
us Er,A ouz I
E;6 -1211(cAs No.:353-59-3) mg/kg With teierence to was
PerfomedbY
method.Analysis
GC/MS,
mgKg Wilh referenceto us Er,Acuz I
bY
wasPedormed
Analysis
methodGC/MS,
(cAs No: '12+73-2) m9Kg With referenceto us El,A cuz I
FGlorF24o2
bY
wasPerformed
Analysis
method.
GC/MS.
(CASNo : 75.63-8)
Halon-1301
lilffi
ffiffii#ffi
Hffi
htrfti
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No.t
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m9Kg with referenceto Es EN l'+ooz zvu
Analvsi€was PerformedbY lC
50
n-d.
mg./Kg With reielence to t b EN raooz zw
50
n.d.
50
n.d.
Method
Unit
Te6t lt.m(s)
Hili#i,"*--'-,om;1476244-a'
mg/Kg
(ct)(cAs t'to.:
Faogenctrlorine
22537-15-1)
l[I||ll llllll
F;i6;;Bromine (Br)(cAsNo,:
to gs EH14582:2007'
fu-ithreterence
bYlC
wasPerformed
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bYlC.
wasPerformed
Analvsis
mg/tg w-rttrreferenceto BS eN 1458212007
AnalysiswasPerformedbYlC
10097-32-2)
(l) (CAS No.:
HalogBn-lodine
1436244-8]
A3be6tos
Aiifi6ti-iE
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v.
(cnSm.:zs36'ozAiifi6ifrlttite
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o/o
d6iuo-ite(CASt'lo.rrz00r-28'+)
oh
iE;olite (CAsNo.:77536686)
%
With reterenceto EFAouu,n-vi' | "
bY
wa6Pedormed
Analysis
method.
sM PLMandXRD.
Wlth referenceto EPAbuu,n_vr'I ro
bY
wasPerformed
Analysis
method.
SM.PLMand)(RD.
with reterenceto Er/Aouu/n_vr/| rr
method.Analysis!!as performedby
SM.PLMANdXRD.
With rcferenceto EPAbuu/n_r.r,I ro
bY
wasPerformed
Analysis
method.
sM PLMandXRD.
uvith reference to EPA buutrl_vr, I ro
method.Analysiswas Pe.formedbY
SM. PLM ANdXRD.
with referencelo EPAouu/K-vo,t I
bY
wasPedormed
Analysis
method.
SM,PLMandXRD.
Negative
I
Negative
1
Negative
1
N€gative
Negative
Negative
1
iffiffitr##l,ffifttffi
:r ' iii
i.!!:*trlLrrJjr.,!l_.
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No.: CE/201214848ADalet2o12l0u04 Page:5 of 24
Test Report
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CERAMTEC
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15D-91207
CERAMICSLUITPOLDSTMSSE
MULTIFUNCTIONAL
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I
Sum of PBB3
MonobromobiPhenyl
Dibromobiphenyl
Tribromobiphenyl
TetrabromobiPhenyl
Pentabromobiphenyl
HexabromobiPhenYl
lHeDtabromobiPhenyl
lOctabromobiphenyl
lNonabromobiphenyl
lDecabromobiphenyl
lSumof PBOES
ether
lMonobomodiphenyl
ether
IDibromodiphenvl
ether
lTribromodiphenyl
ether
lTetrabromodiphenYl
ether
lPentabromodiphenyl
ether
lHexabromodiphenyl
ether
IHeptabromodiphenyl
ether
lOctabromodiPhenyl
etner
INonabromodrphenyl
ether
lDecabromodiphenyl
AZO
MOL
Method
Unit
5
5
Result
No.l
n.d.
n.d.
n.d.
n.d.
n.o.
n.d.
5
5
lperfomed
,rrr""j
5
5
5
5
n.d.
n,dn.d.
n.d.
n.d.
1000
n.d.
n.o.
5
5
5
5
n.d.
n.d.
5
n.d.
n.d.
n.d.
n.d.
n.d.
n.d.
to LFGB82.02-2.
(cAs No.: mg/Kg Withreference
t: 4-AMtNoDIPHENYL
performed
by GC/lllS.
was
Analysis
9247-1')
to LFGB82.02-2.
(CASNo.:92-87- mg/Kg WiiFreference
BENZIDiNE
bYGC/MS.
w€sperfomed
Analysis
3
n-d.
3
n.d.
mg/tg Withreferenceto LFGB82.02-2
wasperfomedbYGC/MS
Analysis
to LFGS82.02-2.
mg/Kg W]threterence
AnalysiswasPerformedbYGC/MS
to LFGB82.02-2.
(CAS mg/Kg Witfrreference
5):O-AMINOAZOTOLUENE
performed
bYGC/MS
was
Analysis
No.:97-56-3)
3
n.d.
3
n.d.
3
n.d.
3). 4-CHLORO-O-TOLUIDINE
(CASNo.: 9549-2)
(CAS
4)..2-NAPHTHYLAMINE
No.:91-59-8)
lM
1000
n.d.
5
to lEc 623211
reference
mg/Kg lwrth
Gc/lvs.
by
Limit
r dis 'i$ apo
FP" 01 ! P rT
::+::Sll'Ufff"3*$l+;+:;'r,"+iffi:'^+i;i!Tfl";"s"f#fi1;":$i
a#s:""fiT"".:qii"'"1:,:i#,,ts*,,*.,*,"",,'*-ijj*ijl*{*#'*"n-"i':U*'il*"+:"ij:ijl['5
.;ri?a
rlin!:'
Test Report
No.: CE/2012J14848AD e.2012lO2lO4 Page:6of24
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Result
No,'l
3
n.o.
3
n.d.
mg/kg With referenceto LFGB82 02-2
wasperfomedbYGC/MS
Analysis
No.:615-05.4)
mg/Kg With referenceto LFGB82 02-2
9):4,4'bYGC/MS
wasperformed
Analysis
DIAMINODIPHENYLMETHANE
3
n.d.
tr###t*'u'of:FiPffi-*
3
n.d.
3
n.d.
3
n.d.
3
n.d.
3
n,d,
3
n.d.
3
n.d.
3
n.d.
3
n.d.
3
n.o.
to LfGB8z o2-2.
mgKg wittr reierence
6j-2-AMrNo-4-NlrRoroLUENE
{CASNo.r99-55-8)
Z-trro-mmilmieESC
106-47-8)
bYGC/liS
wasPerformed
Analysis
mgft€- WiiEErence to LFGB82.02-2
bYGC/MS.
\/asperfomed
Analysis
(cAs
5j:2+DrAMrNoANtsoLE
Limit
n.d.
to LFGB82.02-2
mg/Kg Wth reference
AnalysiswasperformedbYGC/MS
(CASNo.:91-94-1)
mgKg With referenceto LFGB82 02_2.
by GC/lllS
wasperformed
Analy6is
mg/Kg FiiF referenceto LFGB82.02-2
i-:33LDIMETHYLBENZIDINE
AnalysiswasPerformedbYGC/MS.
No.:
119-93-7)
ICAS
to LFGB82.02-2.
mg/kg Withreference
13):3,3'-DIMETHYL-4,4performed
bYGC/MS
was
Analysis
DIAMINODIPHENYLMETHANE
(CASNo.:838€8{)
to LFGB82.02-2
mg/Kg Wittrreference
(2-METHoxYiztTcREstDtNE
performed
by GC/MS
r /as
Analysis
(CASNo :
s-METHYLANILINE)
120-71-8\
to LFGB82.02-2.
(2ms,/Kgwith refere,nce
15):4,4'-METHYLENE-B|SbYGC/IVS
was
Analysis
Performed
(CAS
No.:
CHLOROANILINE)
101-144)
mg/Kg Wth referenceto LFGB82 02_2
(CAS
16143'-OXYD|ANILINE
bYGC/IIS
'101€0-4)
wasperformed
Analysis
No.r
to LFGB82.02-2
mg/Kg Wittrreference
17)44rTHtODlANlLlNE(CAS
bYGC/MS.
was
Analysi6 Perfomed
No.:13965-!)
(CAsNo : 95- mg/Kg Wli6 referenceto LFGB82.02-2.
18).GTOLUIDINE
AnalysiswasPerformedbYGC/MS
53-4)
referenceto LFGB82.02-2.
mg/Kg Wii.-h
1r-rrl-l--r-t4--TOLWLEN'E5rAM-iNE
wasPerformedbYGC/MS.
Analysis
(CASNo.:95-80-7)
ETFVGII]fiE mg/kg Willr referenceto LFGB82 02-2
tot2--4-j--rli'5iRifr
bYGC/MSwasPerformed
Analysis
(CASNo.:13717-7)
Zd5-AN-Ei6NE@Sffij--G- mg/Kg Wlith€ferenceto LFGB82.02-2
bYGC/MS
wa6performed
Analysis
04-0)
n.d.
3
n.d.
'mtr#ffi
trttr*fp*',ffi
ffi
t;qtrffi tr$#m$Ngf'ffi.#:f
'r'
'lr
i*f .,*'rr1rr, L,:,'
{,l;t"1a2!::,':lrg.1ll)4::=7_
Il.y,!,.,-
Test RePort
No.: CE/2012/14848ADate|2012J02104Page:7 d 24
Ll[||||nw|:||lullll
GMBH
CERAMTEC
LUITPOLDSTMSSE15 D-91207LAUF' GERMANY
CERAIVICS
IVULTIFUNCTIOML
Test ltem(s)
22)PAMTNOAZOBENZENE
rcAs No : 60-09-3)
F-xYLlDl NE(cAs No.: 956&1)
(cAs No.:87,Z).2,6-xYLtDlNE
62-71
FFcb(chlorofluorocarbons)
GroupI
1 ICASHo;
df,lorofluorocarbon-1
75€94)
(CASl"to:
dfilorofluorocarbon-12
75-71-A)
mdks Freference
3
mg/Kg Wil[referenceto LFGB8202-2
3
n.d.
mg/Kg With refetence to Ll-uE 62 ul_z
3
n.d.
to LFGB82 02-2.
Analysisv/asPerformedbYGC/MS
bYGC/MS
wasPerformed
Analysis
mg/Kg
76-14-2'
uSEPA5o2t
friifrTeferenceto
by
wasperformed
Analysis
m€thod.
GC/MS.
to us EPA5021
reference
Wi--th
by
wasperformecl
Analysis
method-
I
I
n.d.
1
n.o,
1
n,o.
n.d.
to us rPA 5021
Withreference
bY
wasPerformed
Analysis
method.
GC/[/tS.
mg/Kg Wiifr referenceto Us EPA5021
wasPerfomedbY
Analysis
method.
GC/MS.
11 (CASNo.: mg/Kg W lr referenceto US EPA5021
dEloroftuorocarbon-'1
wasPerfomedbY
Analysis
method.
35+56-s)
GC/MS.
(CASNo:
dEiorofluorocarbon-211
422-78-6)
|
,l
GC/MS.
mg/Kg
76-15-3)
12 (CASNo:
dEi6ffuorocarbon-t
7€-12-O)
n.d.
mgikg Withreferenceto uu El'A cul I
method.AnalysiswasPerfomedbY
GC/MS.
to lJb EHAcuzI
mg/kg lwith reference
by
wasperformed
Analysis
lmethod.
tGc/Ms.
Ehffiiil;G;Fo"iI4reI5I-
Group lll
Limlt
Analysiswas per{ormedbYGo/MS
mg/Kg
3 (CnSNo:
dhlc,roftuorocarbon-t
75:72-9)
Result
No.'l
n-d.
Florofluorocarbon-113 (cAs No :
7613-1)
15 (cAs No.:
luoroca6on-1
dFi;mhlorof
MDL
method
Unit
to us EPA5021
Wiihreference
bY
wasPerfomed
Analysis
method.
GC/MS.
to USEPA5021
mg/Kg Withreference
bY
wasPedormed
Analysis
method.
GC/MS.
mg/Kg
1
n.d.
1
n.d.
n.d.
n.d.
Hffigffi"ar+Nffiffisft$r*
Test Report
No.:CE/201214848A Dale:201210i,04 Page:8 of 24
Itl|| [tt]llllullllllll
CERAMTECGMBH
LAUF,GERMANY
15D-91207
CERAMICS LUITPOLDSTMSSE
MULTIFUNCTIONAL
ch-66iG#6on..zitld6-N;
Method
Unit
Test ltem(s)
mg/kg WiifrArence io us EPA5021
method.Analysiswas PerformedbY
GC/MS.
31A2-26-1\
mg/Kg Witlr referenceto uS EPA5021
eh6rofrrrcricarSon--itd5lt;
method.AnalysiswasPerformedbY
2354-06-5)
GC/MS.
+ lcnS No; mg/kg With referenceto ub EPAcuz I
dfri6Eituorocaroon-zt
bY
\r€sPedormed
Analysis
method.
2925s31-0)
GC/MS.
mg/Kg With referenceto uu Ef'A cuz I
uorocarbon-21s(cAsNo:
dfri-rofl
method.Analysis'a/asperformedby
425943-2')
GC/MS.
With referenceto Us El'A buzl
mg/kg
(cAs
:
dhloro-fluoroca$on-216 No
method.AnalysiswasPerformedbY
661-97-2)
GC/MS.
USEPA5021
6frloroiiuqocaro-onrr?ld5l6]mg/Kg Wil[referencetowas
bY
Analysis Performed
method.
422-86-6)
Resuli
i/IDL
'I
No.t
Limlt
n.d.
,!
n.d.
n.o,
1
n,o.
1
n.d.
1
n.d.
cc/Ms.
Ctlcs lChlortnatehYdrocarUon)
(cAs
-J J 2-Tetrachloroethane
No.:630-20€)
i-zTrichloroethane(cAsNo.l
79{0-s)
bY
wasPerformed
Analysis
method.
GC/MS.
m9Kg Wii-reference to Us EPA5021
bY
wasPedormed
Analysis
method.
GC/MS.
to us Et'A euzI
W ithreference
msiks
bY
wasPerformed
Analysis
method.
GC/MS.
mg/Kg with refercnceto u5 El'A cuz I
wasPerfomedbY
Analysis
method.
(CAst''to: z+
ilTdictrtoroettrane
34-3)
mg/Kg with reference10u5 Et'A 5ur t
method.AnalysiswasPerfomedbY
IlEichloroahene (CASNo : 7$
354)
mg/Kg With referenceto us EPA 5uz I
method.Analysiswa6 PedormedbY
GC/MS,
ITIfi;h6roAha"e
71-556)
65I;
.';?l'#f;***e(cAs
l
n.d-
mg/Kg with referenceto u5 Et'A suz I
1
n.d.
1
n.d.
n.d.
GC/MS
n.d.
GC/MS
n.d.
1
ffiil';U#iffiil.friidfr
llr*iffi::i:{!"T$:"5;*H1"']l}rtl#i,,ln,lj,:;i:*t5,fi;i:iH
I;**t*;:t+:rn;nl;'*4"61i"!:i,T:d"t'Ii'r:i:;Fir."xmijxx,;,;"rs;:,i;-'1i."-";';:."x?;"Ji'iiJ
Li,#fl{#i}'li,$;htj,Fj"#fri{ur-.""rt11:i{*li{:#j#jtuJlJ"*fflp"fiiiff.iji#i[ir
1-:*,1**'Ufi};$r"d'lr'':";tr\i"i'ii:lir,ii:it$"I1:i'ri1'iifl'"i#.+ffi*$i
F#ffi$fi{trf:iiir*g#lii{i#F;1rt#m$iii:""*sii::i;*1r,*ri*,,Ht?:""ff;r,m:?i't'.%?
'.wq6siRd
Nvlee
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n",
l:"x'!
TestRePort
No.:CE/20121484&q Date 201202104 Pagel9of 24
rrirL tt||llllulltl]l
GMBH
CERAMTEC
LAUF,GERMANY
15O-91207
CERAMICSLUITPOLDSTMSSE
MULTIFUNCTIONAL
Te6tltem(s)
iliSicntoropropene(ces m r
5m-5e6)
I
irtoL
Method
Unit
lMth-referenceto uS EPA5021
I ms/kg method.
by
lvaspertormed
Analysis
|
GC/MS.
(CASNo:
12,&TrichloroproPane
96-18{)
m9Kg V\tithreferenceto US EPA5021
lZffifrGroeiha#@Sffi:
mg/Kg Wth feference to US EPA 502'l
method.Analysiswas PerfomedbY
GC/MS.
iF-Dichlnopropane (cAS No :
78-87-5)
mg/kg With referenceto uS EPA502'1
method.Analysisv/asperformedby
GC/MS.
m9Kg Wittrreferenceto US EPA5021
wasPe{ormedbY
Analysis
methodGC/MS.
m9Kg Wl h referenceto US EPA5021
method.AnalysiswasPerformedbY
GC/l\,!S.
to USEPA5021
mg/Kg Vvitfrreferenc€
107-062)
iSS6h6ropropaiEldST;
142-28-9)
(cAS No.:
2TEirchloropropane
5*-2U7t
(cAS No :
Cabontetrachloride
56-23-s)
method.AnalysiswasPertormedbY
GC/lVS.
n.d.
'I
n.d.
'I
n.d.
dhlotromett€ne(CASNo : 74-873)
liForchtoroahene (cns No:
15+5S2)
GC/trs.
to USEPA502'l
(cns Ho.: mg/kg Wit eferenc€
Ft goicHc,ropropene
bY
was
1006141-5)
method.Analysis
GC/MS.
Limit
n.d.
1
n.d.
1
n.d.
1
n.d.
n.d.
US EPA5021
Eh6roAha'reldsNo-i7toG5 mg/Kg W-rth€ferenceto was
bY
0t oroform(CASNo.:674&3)
No.1
1
wasPerfomedbY
Analysis
method.
GC/tds.
Analysis Performed
method.
GC/MS.
mg/xg Witf' referenceto us EPA5021
wasPerfomedbY
Analysis
method.
GC/MS.
mg/kg With refe.enceto uS EPA5021
wasPedomedbY
Analysis
method.
GCiMS.
mg/kg With referenceto US EPA5021
bY
wasPerformed
Analysis
method.
Result
n.d.
1
n.d.
I
n.d.
n.d.
Perfomed
ilqffirffi**ffiffit$ffiffiffi$*f
TestReport
14848A D€Ile| 20121021c4Page:'i0of24
No.:CE/2012i
t
GMBH
CERAMTEC
LAUF,GERMANY
D.91207
CERAMICSLUITPOLDSTRASSE'15
MULTIFUNCTIONAL
irethod
Unit
Test lt6m(s)
mgKg with .eferenceto IJSEPA5021
bY
wasPertormed
Analy6is
method.
GC/t/ts.
Wilh referenceto US EPA5021
mg/Kg
il,sthyleneChloride(CASNo.:75bY
wasPedormed
Analysis
method.
09-2)
GC/MS.
(cAS No.:127- mg/Kg With referenceto US EPA5021
Tetrachloroethene
method.Analysi6wasPerformedbY
184)
GC/MS.
to uS EPA502'1
Withreference
(CAS
mg/kg
irans-1,2-Dichloroethene
bY
wasPerformed
Analysis
method.
No.:15640-5)
GC/MS.
Wiih referenceto US EPA5021
(CAS
mg/Kg
tran+1,3-DichloroprcPene
bY
wasPerformed
Analysis
method.
No.:10061{2-6)
GC/MS.
to USEPA5021
mg/Kg Withreference
(CASNo.:79Trichloroethylene
bY
wasPerformed
Analysis
method.
016)
GC/[/tS.
MDL
|||! lllllllllllll
Result
No.l
Llmit
n.o.
(CASNo.:
HexacNo,robutadiene
8768-3)
1
n.d.
1
n.d.
1
n.d.
'I
n.d.
n.d-
HCFCa
(Hyd.ochlo.ofluorocarbons)
(CASNo.:75-43-4)
FICFC-21
HcFcr2(cAsNo..7s45€)
(CASNo.:593-7M)
I-ICFC-31
HCFCl2l (CAS No 35414-3)
HCrC-122(CASNo.:3Sl-21-2)
to US EPA5021
mg/xg Withreference
by
v/asperformed
Analysis
method.
GC/MS.
mg/Kg With referenceto US EPA5021
w€sPerfomedbY
Analysis
method.
GC/MS,
to USEPA5021
mg/kg Withreference
bY
waspedormed
method.
Analysis
GC/MS.
to USEPA502'1
mgikg Withreference
bY
wasPerformed
Analysis
method.
GC/MS.
to USEPA5021
mg/Kg Withreference
1
n.d.
1
n.d.
1
n.d.
1
n.d.
n.d.
bY
wasPerfomed
Analysis
method.
GC/MS.
::ifiil:Ji:
:"-"Jl
iiiFd::
T.-lJ"il
il;,#;"i;-,il#;;il#""* ;';ii;;fiffililri
oJ{r rorems andcold i.n6l
'i'"ffi1f#f#;drs:':"#;lt,ilfiiiiir--*1iffi#"i:];:*'{l'j'.:"""#"**;'tu"r.r;;i;.:"r'rl+"u
;;1,;;
; !.b r\
Test Report
No. :CE|201Z14848A O?/le 2O121021c4Page: 11 of 24
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I
GMBH
CERAMTEC
lllll
LAUF,
GERMANY
15D-91207
lrulrtruncrtorunlceRAMtcsLUtrPoLDsrRAssE
Test ltem(s)
(CASNo.:306-83-2)
HCFC-123
HCFCj24 (CAS No.: 2837{94)
Method
Unit
MDL
Result
No.'l
Limit
n.d.
mg/K9 Ftth referenceto Us EPA5021
wasPerfomedbY
Analysis
method.
GC/MS.
mg/Kg Wth referenceto US EPA5021
method.AnalysiswasPerformedbY
n.d.
cc/Ms.
to USEPA5021
mg/Kg Withreferenoe
bY
wasPerfoamed
Analysis
method.
GC/[iS.
to uS EPA5021
Wttr reference
mg/Kl
(CAS
1&9-08-7)
No.:
HCFC-132b
1
n.d.
1
n.d.
mg/Kg Wth feferenceto Us EPA5021
bY
wasPedormed
Analysis
method.
GC/MS.
mg/Kg With referenceto US EPA5021
Analysis
wa6PerfomedbY
method.
GC/MS.
MEKg With refefenceto US EPA502'1
wasperfomedbY
method.
Analysis
GC/MS.
to USEPA5021
m9Kg With.eference
bY
wasperformed
Analy6is
method.
1
n.d.
1
n.d.
to USEPA5021
m9Kg Wth .eference
1
n.d.
t
n.d.
1
n.d.
1
n.d.
HcFCl3l (CASNo.:359-28'4)
bY
wasPerformed
Analysis
method.
GC/MS.
(CASNo.:75-88-7)
HCFC-133a
(CASNo.:1717{04)
HCFC-141b
HCFCI42b (CAS No.: 75643)
(CASNo.:422-26-4)
HCFC-221
n.o.
n.d.
cc/Ms.
HCFC-222(CAS No.: 422-49-l)
(CASNo.r422-526)
HoFC-223
(CASNo.r422-g-8)
HCFC-224
method.Analysiswa6performedbY
GC/MS.
to USEPA502'1
mg/Kg Withreference
wasPerfomedbY
method.
Analysis
GC/MS.
to USEPA5021
m(yKg Withreference
bY
Analysis
wasperformed
method.
GC/l\rs.
(CASNo.:422-56-0)mgftg Withreference
to USEPA5021
HcFC-22sca
bY
waspedormed
Analysi6
method.
GC/MS.
ff ;:,:::;"#-* ffi ;"#;;;;;'"
::J;-1
fii$"lij|*fi;.1,"i;,
*.;*ir#;fiii:11:::
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d i. { , a ' M { s o m . r
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,',+F$t'.#f,it:':'Jd:L&F,i:,'.";"*brt*,i;iti#r.d
TestReport
No. : CE/201214848A Dale: 2012102104Page: 12 ol 24
|l]|||||nl
CEMMTECGMBH
LAUF,GERMANY
15D-91207
CERAMICSLUITPOLOSTRASSE
MULTIFUNCTIOML
T€t ltem(s)
Method
Unit
to USEPA5021
(CASNo.:507-55-1) mg/Kg Wittrreference
HCFG22scb
by
r €s perlormed
Analysis
method.
GC/MS.
to us EPA5021
(cAS No.:431-87-8) mg/Kg W-threference
HCFC-226
MDL
Result
No.t
1
n.d.
I
n.d.
1
n.d-
1
n.d.
lllllI|l
Limlt
method.Analysiswas PerfomedbY
GC/MS.
(CASNo.:421-9+3)
HCFC-231
to IJSEPA5021
mEks Withreference
(CASNo : 460-89-9)
HCFC-232
mg/Kg
bY
wasPerformed
Analysis
method.
GC/MS.
to us EPA5oz1
WllFreference
bY
wasPerformed
Analysis
method.
cc/Ms.
to USEPA5021
(CASNo.:7125-84-0) mgiKg Withreference
HCFC-233
n.o.
(CASNo.:42t94-5)
HCFC-234
wasPeformedbY
Analysis
method.
GC/MS,
mg/Kg Wittrreferenceto US EPA5021
method.Analysi6wasPerformedbY
GC/MS,
n.d.
(CASNo.:460-924)
HCrc-235
tous EPA5021
filEffwitlr reference
by
v/aspedormed
Analysis
lmethod.
tGc/Ms.
(cnst',to:oe0-27-3)| ms/ks Wittrreferenceto US EPA5021
FEFe-z+t
bY
wasPedormed
Analysis
method.
GC/IVS,
referenceto US EPA5021
With
mg/kg
HCFC-242{CAS No.:460-63-9) |
bY
wasPerformed
Analysis
method.
GC/MS.
HoFC-243
{CASNo.:460-69-5) I mg/kg With referenceto US EPA5021
method.AnalysiswasPerformedbY
GC/MS.
mgKg with ieferenceto us EPA5021
HCFC-244
wasPe ormedbY
Analysis
method.
GC/MS.
to USEPA5021
(CASNo.:42141-0)| mg/kg Withreference
HCFG251
1
n.d.
1
n_o.
'I
n.d.
n.d.
1
n.d.
1
n.d.
method.AnalysiswEsPerflrmedbY
GC/MS.
;;;:;;;ilil";;:ffi;;:r#-"r;=n#;','"-ii.{d;diq*""}'"
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TestRePort
No.: CE/2012/14848AOale| 2O12lO2lM Page| 13of 24
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GMBH
CERAMTEC
LAUF,GERMANY
15O-91207
CERAMICSLUITPOLDSTRASSE
MULTIFUNCTIOML
T€6t ltem(s)
method
Unit
FcFdrsZjG5ffi:--5rr5o-:tmg/kg
o us ePn 5ozl
reference
Wi-ith
bY
w€sPerfofmed
Analysis
method.
I
Result
No.t
n.d.
1
n.d.
MOL
GC/MS.
(CASNo.:460-35-5)
HCFC-253
to un Et,AeuzI
mg/Kg Withrel€rence
bY
wasPerformed
Analysis
method.
GC/MS.
us EPAcuz I
FEFozot(cnsNo.:azo-sz-g) m9Kg With referenceto was
Analysis PeformedbY
method.
GC/MS.
Wittrreterenceto US EPn S021
mg/Kg
trcrr--r-6r-@S-M-t:drn5
bY
wasPerformed
Analysis
method.
GC/MS.
With reterenc€to us EFAouzI
mg/Kg
HCFG271(CASNo : 43G55-7)
wasPerfomedbY
Analysis
method.
GC/MS.
Limit
n.o.
1
n-d.
1
n.d.
Note :
= 1000PPm
1. mg/kg= PPmi 0.1M"/o
2. n.d.= NotDetected
Limit
3. MDL= MethodDetec,tion
4."-"=NotRegulated
(NoUnit)
analysis
5. " = Oualitative
/ Positive= Detectable
6. Negative= Undetectable
o/;'
7- Asbestos: Negative= "< 1 0 %o"'Positive= "> 1 0
lnformation: POPS- (EU)757/2010
PFOSRefer€nce
products
or
in s€mi-finished
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PFOSas sub6tances
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artictesoi partsat a levelabove0
'ffi
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ffi
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TestReport
No.: CE/2012/14848ADale: 2012102104Page. 14 ol 24
|r||lllu]llllllllrull
GMBH
CERAMTEC
LAUF,GERMANY
15D-91207
CERAMICSLUITPOLDSTRASSE
MULTIFUNCTIONAL
1 ) Thesesampleswere dissolvedtotallyby
methodaccordingto belowflowchad
preconctiiioning
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2) Nameofthe oersonwho mademeasurementClimbgreal
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3) Nameof the personin chargeof measurementTroy
SampleMeasurement
acid
bYsuitable
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depended
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material
Microw€vedigestionwith
HNO3/HCVHF
amountof
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digestion
Heatto appropnate
temperaturcto exract
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HCltodissolve
f or
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ICP-AES
sampleMaterial
solder
Steel,copper,aluminum,
throughfilter
DigestionAcid
Aqua regia,HNO3,HCl,HF,HrO,
HNO3/HF
Glass
ceram|c Aquaregia
Gold,platinum,
Palladium,
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colordevelopment
measurethe abaorbance
at 540nm by UV'VIS
ffiiu+mmtrlrffi
ffiffiffiffit#mt#*ffi
ot 24
No.:CE/2012y14848ADale:2012/02104 Page:15
Test Report
CERAMTECGMBH
LAUF,GERMANY
15D-9'1207
CERAMICS LUITPOLDSTMSSE
MULTIFUNCTIONAL
n|| lltrlllllu
lll!
procedure
Analytical f,ow chart of Soxhlet extraction (LC/MS)
I
r
RomanWong
Nameofthe pe6on who mademeasurement:
Trovchang
t'iil; ;i ih; ;;*"" inchargeof measurement
'
I
I Te3tltems:PFOS/PFOABenzotriazole
iiff,iii:t:,1:ll":i#iili:l{ii.t}}f:::f$i:f-liTtri't"j;i:i];nffi#'ffi*'
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Page 16of 24
No.: CEl201214848A Dale:201,2tO2lO4
TestRePort
||]m||
GMBH
CERAMTEC
LAUF,GERMANY
15D.91207
CERAMICSLUITPOLDSTRASSE
MULTIFUNCTIONAL
|||mlll|I
Chlorinated Flame retardant analytical flow chart
BarryTseng
1) Nameof thepe6onwhomademeasurement:
Troychang
2) Nameof thepersonin chargeof measurement:
USEPA3540
USEPA8270D'
method:
I Reference
Mirex,Ce MCCP
PCNS,PCTS,
r Testltems:PCBS,
' ' * * * * - ; ' : : "/,I
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No.: CEi2O'1214848ADale:201i,02104 Page: 17ol 24
TestRePort
GMBH
CERAMTEC
LAUF,GERMANY
15D.9'1207
CERAMICSLUITPOLDSTMSSE
MULTIFUNCTIONAL
|l|[[
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ltll
of PVc in matorial
Analyslsflowcharttor determinatlon
r
r
GinnyChen
Nameof thepersonwhomademeasurement
TroyChang
Nameof thepersonin chargeof measufement:
Samplepre-treatment
SampleanalyzedbYFTIR
of C-Clbonding
check wave-number
ie
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Page' 18ol24
No.: CE/201214848ADaI.e:2O12tO2104
GMBH
CERAMTEC
't5
LAUF,GERMANY
CERAMICSLUITPOLDSTRASSED-91207
MULTIFUNCTIONAL
Analyticalflow chartof Soxhlotertraction(Gc/Ms)procedure
RomanWong
r
Nameofthe pe6onwhomademeasufemenl
Troychang
r
Nameof thebersonin chargeof measurement
' DBBT'
'
'
[T6st ltems: Phthalato' BenzotdazoleHBCDD NP
comPounds
)
OrganicphosPhorus
Dah
:lt*t
r
";
r rfilliflrllllrlll
Test Report
No.: CE/201214848ADate.2012102104Page: 19ol 24
CERAMTECGMBH
LAUF,GERMANY
15D-91207
CERAMICS LUITPOLDSTRASSE
IIULTIFUNCTIONAL
[||il
ltI
lltlrl
contenl
Analytlcalflowchartof Organic_Tln
I
I
GinnyChen
Nameof thepersonwhomademeasurementl
TroyChang
per6on
of
measurement:
in charge
Nameof the
Data
g-$EjtrE$i*1ggery$1.i'j'$;*f,ri
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TestReport
No.ICE/2012/14848ADate:2012t02n4 Page:20ot 24
GMBH
CERAIVTEC
LAUF'GERMANY
15D-91207
CERAMICSLUITPOLDSTRASSE
MULTIFUNCTIONAL
Analytical flow chart of halogen content
'1) Name
Ritachen
ofthepe6onwhomademeasurement
TroyChang
ofmeasurement:
incharge
2) Nameoftheperson
/ Separation
Samoleoretreatment
Weightingand puting samplein cell
/ Ab6orption
OrygenBombCombustion
to fixedvolume
Dilution
bYlC
wasPerfonned
Analysis
ffie,=#flffi
[1 [ttllllllulllllll]
Test RePort
No.:CE2O1Z14848A Date 2012102104Page:21o124
GMBH
CERAMTEC
LAUF,GERMANY
15D.91207
CERAMICSLUITPOLDSTMSSE
MULTIFUNCTIONAL
|r l ||||l]lllllllllil
Analysisf,ow chartfor determinationof Asbestos
VictorKao
1) Nameof thepe6onwhomademeasurement
WendyWei
|ncnaQeof measurement
2) Nameofthe P€rson
( Reference
method:EPA600/R-93/1161
Asbestosidenlificaljonby dispersion
lightmicrcscopy
polarizEtion
staining
Asbestov
Containing
Asbestos/
Notcontaining
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No.: CE/2012148484 Date.2O1ZO2|04Page| 22 oI24
Test Report
CERAMTECGMBH
15 D.91207LAUF,GERMANY
CERAMICS LUITPOLDSTRASSE
MULTIFUNCTIONAL
t
r
Lrtflnm
ffrlllt
Analyticalllow chan
Romanwong
Nameof thepersonwhomademeasurement
TroyChang
Nameof thepersonin chargeof measurement
TBBP'A'bls)
( Testlterns:PBB/PBOE,
_ '>
proc€ss
prccess___' Conlimation
---_-' Optionalscre€n
process
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s*i.rv:ry'q$e::::iiflUiii.::F:[':::]tr:#fi,#:THi:iirji:'iii]fflffi"#
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t;]fi;iltuy
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Test Report
No.:CE/201214848A
Dale.2O1ZO2J04 Page| 23 of 24
t[l llllllll[ml1l
CERAMTECGMBH
GERMANY
LAUF'
15D-91207
ceRAMtcsLUlrPoLDsrMssE
ir-riiiiiur.rirroNnL
Analyticalflow chartofvolatileorganiccompounds(VOcs)
: ChunWu
I
Nameof thepersonwhomademeasu€ment
: ShinjyhChen
!
Nameofthe personin chargeof measurement
( Refefence
method: us EPA5021)
Samplepretreatment
TakesampleandPutit into
glasswarc.
headspace
ffi
#ffi
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TestReport
No.: CE/201214848ADale:2012to2104Page| 24 ol24
l
GMBH
CERAMTEC
'15
LAUF.GERMANY
CERAMICSLUITPOLDSTMSSE D.91207
MULTIFUNCTIONAL
t The tesied sample / part i3 marked by an a ow if its shown on the photo'
|||ti|l llI|illllll
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giffi*rffiffi
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Validi
nown
ForQueEll
PleaseCo
Test Report
No.: CEl2011184955
Datet20'1111201
POLYFILAG
OBERALLMENDSTMSSE2OA,CH€3OOZUG / SWITZERLAND
ithscs
Page:'l of 7
ll]uttfi
[[m
Thefollowingsample(s)wa3/weresubmitledand identitiedby/onbehalfof the clientas:
SampleDesciption
Buyer/OrderNo.
SampleReceiving
Date
TestingPeriod
Ni42Fe58MCuMAgs%
11-0803
2011t11t25
2011t11t25'l O 2011I 1'J01
T€stResult(s)
Pleasereferto nextpage(s).
(NW4E
f,lmdiorrd
Or.rlcd l,.bor|b.t - Trlpd
ps(31i€ded rhs ied rcpod eiior be
cwpanye
!,
rt
rr-ri'f.,ri,il]ilntlli ir ].ri
iiil-:i I
ny tublsd b b Gene6 coideoB d se
1,.
|.lrrrr?!t!:.
dbis r aiy'Iha cohpantssoo r69onsbiI s b r ct'odaddrhs dodm
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f: lFt
. ,;,i+ @610?)ree
14 | + 8610r)2ee
ry
(w ar.on
TestReport
No.: CE/201
1/84955
Page:2of 7
Dale: 2111/12t01
POLYFILAG
OBERALLI\4ENDSTMSSE
2OA,CH63OO
ZUG/ SWITZERLAND
lm[tmlrltttll
Test Reault{s}
PARTNAMENo.1
SILVERCOLOREDI'ETAL WIRE (INCLUDINGTHE PLATINGLAYER)
T66l ltem(s)
Unit
Cadmium(Cd)
Method
mSikS Witheferenceto tEC62321:2008and
perfom€dby lCPdES.
mgKg Withreference
to IEC62321:2008and
perfomedby ICP-AES.
mg/Kg Withreference
to IEC62321:2008and
pe.formed
by ICP-AES.
Withreferenc€
to IEC6232'1:
2008and
performed
by Boilingwaterextraction
M€thod.#
Lead (Pb)
(Hg)
Mercury
Hexavalent
Chromium
Cr(Vl)
Sumof PBB9
l\4onobromobiphenyl
Dibromobiphenyl
Tribromobiphenyl
Tetrabromobiphenyl
MDL
2
R6sult
No.l
n.o.
2
2
n.d.
Negative
n.d.
n.d.
n.d.
n.d.
n.d.
n.d.
n.d.
n.d.
n,d,
n.o.
5
5
5
Pentabromobiphenyl
Hexabromobiphenyl
Heptabromobiphenyl
Octabromobiphenyl
Nonabromobiphenyl
Decabromobiphenyl
Sumof PBOE3
Monobromodiphenyl
ether
5
mgikg
Withreference
to IEC62321:2008and
per{ormedby GC/lrS.
DibromodiDhenvl
ether
TribromodiDhenvl
ether
Tetrabromodiphenyl
ether
PentabromodiDh9nvl
ether
Hexabromodiohenvl
ether
Heplabro.nodiphenylether
5
5
n.d.
n,o.
5
5
5
n.d.
n.d.
n.d.
n.d.
5
n.o.
n.d.
5
5
5
Octabromodiphenvl
ether
NonabaomodiDhenvl
ether
n.d.
n.d.
n.d.
Decabromodiohenvl
ether
c o m o a n yi r r l ! /
tu.f-]i'
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n,o,
I
:.i
i
^r!.l;li,
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aidllr edd'on $@3 d
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iidbe€pduedexeptniur*6oq
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TestReport
No.: CFJ2011184955
Page:3 of 7
Dale:2O11h21O1
POLYFIL
AG
OBEMLLMENDSTRASSE
2OA,CH-6300ZUG/ SWITZERLAND
Testltem(s)
Halogen
Halogen-Fluorine
(F)
(CASNo.:14762-9+8)
Halogen.chlorine
(Cl)
(CASNo.:22537-15-1)
Halogen-Bromine
(Br)
(CASNo.:10097-32-2)
Unit
lrethod
With refe.enc€to BS EN 14582].2007
.
mg/Kg
Analysis
wasperformod
by lC.
Halogen-lodine
(l)
(CAS No.: 14362-4,4-8)
|l]rl||l]
MDL
t[]||n
Result
No.1
50
n.d.
50
n.d-
50
n.d.
50
n.o.
NoteI
1. mg/kg= ppm; 0.1wt%= 1000ppm
2. n.d.= NotDetected
3. [4DL= MethodDetection
Limit
4."-"=NotRegulated
5. " = Qualitative
(NoUnit)
analysis
=
6. # a. Positivemeansthe presenceof CrVlon the testedareas
b. Negativemeansthe abgenceof CrVlon the testedareas
Thedetected
concentration
in boiling-wEter€xtraction
6olution
is equalor greaterthanO.O2
mg/kgwithS0cm,
testedareas.
7. The6ample(s)
was^rereanalyzed
on behalfoftheapplicant
as mixingsamplein onetesting.Theaboveresult(s)
was^^€re
onlygiv€nas theinformality
vaue.
c m e a i ya r | 1 l l r ' r d 1 1 ' t , r , i i l l , n r 4 L . i . r 1
iirl4li
r3G)rssrd rh I r€d'+on €nnd e '
ir'r'r Nlttll\.
tfi r:li {:/:rFi4,t;r+s6Frtreer7e r}s6Or)xerr
Ewar.on
Test Report
No.: CEl2011/84955
Paget 4 of 7
Dale:2011h2101
POLYFILAG
OBERALLMENDSTMSSE2OA,CH-6300ZUG / SWITZERLAND
t[| tl
rrr ]l
'1) Thesesamples
! €re dissolved
totallyby prcconditioning
methodaccording
to belowflowchart.
( Cf' test methode(cluded)
yang
2) Nameof the personwfiomademeasurement:
Climbgle€t
3) Nameof the personin chargeof measurement:
TroyChang
Cutling/ Preparation
Aciddigestion
by suitable
acid
dependedon differentsample
matedal(as belodtable)
Add appropriateamountof
digestion
reagent
Heatto eppropriate
temp€ratueto extract
Cool, filter digestate
1) AlkaliFusion
2) HCltodissolve
ICP-AES
throughfilter
AdddiphenyFcarbazide
for
SampleMaterial
colordevelopment
DigestionAcid
Steel,copper,aluminum,
solder
Aqua regia,HNO3,HCl,HF,HrO,
Glass
HNO/HF
measure the absorbance
Gold,platinum,palladium,ceramic
Aqua regia
at 540 nm by UV-VIS
Silver
HNOs
Plastic
H,SOI, H'O', HNO3,HCI
Others
Anyacidtototaldigestion
rlrlt
c f f i o . n yB : . 1
t-f
i,l'irl!
!,i
i,.t'l
lii]]irl)
! rd4krzE,
'r
1rItihl-
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r ;r
+1 r rtLtri,ni+ s6 orrree
Test Report
No.: CE/2011/84955
POLYFILAG
OBEMLLMENDSTRASSE2OA,CH€3OO
ZUG/ SWITZERLAND
|t
PBB/PBDEanalyticalFLOW CHART
1) Name
of theperson
whorEdenEasurer€nt:
RormnWong
2) Mrneof theperson
incharge
of fipasurenEnt:
TroyChang
Firsttestingprocess----+
Optional
screenprocess---process - .>
Confifination
Scfeenanalysis
Sanpleextractiort
So*rlet nEthod
ConcedtratdDilute
Extractedsolution
Filter
Analysisby GCiMS
kriue Relp-l1
c o m p a n yG i ! I
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riit!-l
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rary rh,ComFnys30eGspdisb
r1l6b
Page:5 of 7
Date| 2011h2t01
bddnraidrbsdoem
be
r |l t[]
]l
TestReport
No.: CE/2011/84955
Page:6 of 7
Date 2011,1|:]01
POLYFILAG
OBERALLIVENDSTRASSE
2OA,CH$3OO
ZUG/ SWITZERLAND
rt][]|l
rtl[]ll
Analltical flow chart of halogen content
1) Narneofthe pe6on who rcde fiEasurenEnt:Rita Chen
2) Narneof the person in charge of rEasureient: Troy Chang
SaftplepretreatnEnt/ Separatbn
Weightiryandputting
sanplein cell
OrygenBombConbustion
/ Ahsorption
Dilution
to fixedvolunE
AnalysiswasperforfiEdby lC
cdnp,iy til ,il irl,rlli'i
r l r r r j r J ,n j r l ; .
{i!-rL\
.,, tF
Th s dofuneil 6 'sued h' 6e c onpa
$bjed b tens &d cdidrrois rof E
I
mp31s)rsded nE bd rcpod.aiioi b
r1",1."inr'!.!.
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6 drtun ro be rmlarioi o, abit
Test Report
No.: CE/2011/84955
Page.7of 7
Dai.e| 2O11112J01
POLYFIL
AG
OBEMLLMENDSTMSSE
2OA,CH{3OOZUG/ SWITZERLAND
][|l
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' Thetsgtedsample,/pa is ma*ed by an
anow if ifs shownon the photo..
" Endof Repod*'
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+€ {/F + **t rt ;* d,*birl. / $i r1'
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perforned by tCP-r{XS,
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*+
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6 2 3 2 1 . 2 i A B a n d p e r f o r m e db y
B o iI i n s s a t e r e x t . a c t i o n M € t h o d . #
}fr.+B**
sulfonates
/ Perrruo.oocrane
nglka
(PF!S-Acid. Uetal salt
t+us
EPA3540C:1996tii, 'lil
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/ t r i t h r e f e r e n c e t o u s E P A3 5 4 0 c
1 9 9 6n € t h o d f o r P F o SC o . l e . l .
Analysis was perlorned by tClMS.
an+6.(J+) / PFoA(cAsNo.: 3356?
r)
++US EPA3540c:l996tt!,
,Xtl
&Eif 1{r*{,*fl an+d(n) }f
/ w i t h r e f e t e n c € t o U S E P A3 5 4 0 C
1 9 9 6e e t h o d f o r P F O AC o n t e n t .
Analysis was perfofned by rc/MS.
i j :i :r l , ]. r : . a i i . ; ; r t i ]
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Test Report
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ELSCHUKOM
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87, D-98669 !'EIISDORF, GERMAIr\
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( U n it )
( R e s u1 t )
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/ uonobronobiphenyt
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qA#tri
/ Dib.onobipltenyl
/ T r i b r o n o b ip h e n y l
/ T e t r a b r 6 n o bLo h e n v l
I*#Xi
/ P e n t a b r o n o br o h e n ! I
/ Hexabronobiphenyl
?!4$it
+iASf
/ H e p r a b . o n o bpi h e . y 1
^itrfi A / o.rabronobipheDyl
/ Nonabromobipheryt
4)qS*
/ D e c a b r o n o bpih e n y t
+;ASf
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t*AS.t&t"
-;ASf!{
/ M o n o b r o n o dD
i hehvl ether
=-r[#*e
:;A#+a{
/ D i b r o n o d ip h e n y l e t h e r
/ ' l r i b r o d o d i p } e n v l er h e .
B,*SiFa*
/ Tet ra6.onodi phe.vl erher
i;*Sxad
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/ P e . r a b r o m o dDi h € " v l e t h e r
/ H e a a b r o n o dpih e r v t e r h e r
-k;A#Xa{
/ H e p t a b r o m o d iD h € n v l e t h e r
,\;*SXa{
/ o c r a b r o n o dD
i he.vl ether
,L;i#*e
i henvl etler
i N o n a b r o m o dD
+&#ii4
/ D € c a b r o n o d i D h e n velt h e r
623211
zoo$iiF, ,tfu|aE
+8dlf :*d,&jrl. / $ith rererence
ro IEC 62321:?008 and perforned
by rc/MS.
5
5
5
5
5
5
5
5
5
5
5
5
5
5
a* / s"l.s."
(fr.) / Halogen-Floo.ine(F) (c{s
6*
No.: 14?6?_94-8)
(5.) / Haloeen-chlo.ine (cl) (cAs
6*
! o . : 2 2 5 3 71- 5 - r )
& * ( * ) / H a l o r e n - B r o n i n e( B r ) ( c A S
l{o.: 10097-32-2)
50
ng/18
vx&+8fr
ltBs vt r4s82:2007,
50
/ sirh reference to Bs EN
{r}*t.
I 4 5 8 2 r 2 0 0 7A. n a l y si s v a s
50
(I) (cAS
6fr (dU / Halocen-lodine
No.: 14362-44-8)
conFiv;"
r 1 llu.,[r'r,
l: i/irr.r I i.tl
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oyglbredbb6ai.'alcondloisds
50
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iq
3pdJb't}6lobc€da^dhsdocu
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(Iethod)
ro
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Test Report
: CE/2012l10835
aBlJzr.)
. 20L2/ot/71 Ftk(pare) : 1 of r0
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2 _ n _ d . = N o r D e t e c t e d( * . t A r r )
3 - M D L: M e t l o d D e t e c t i o n L i r i i ( r l t l A ; { t s 1 8 1 6 )
4. '- = Not R"sulated (Sli,+&.6)
5 . r ' = Q u a t i t a t i v e a n a L y s i s( N o u n i t ) _ € , B r ) * f ( * + & )
6. #:
a . P o s i t i v e b e a ! s t l e p . e s e n c eo f C r V t o n t h e r € s t e d a r e a s
(po s i t i ve *,F rq,lit E q.tF jq r{ ,r{l rS)
b . N e g a t i v e n e a n s t h e a b s e n c eo f C i V I o n r h € r e s t e d a . e a s
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T h e d e t e c t e dc o h c e n r r a t i o ni n b o i l ] n a - e a r € r - e x r r a c t i o sno l u t i o n i s € q u a l o r g r € a r e r t h a b 0 . 0 2
m A l k gw i t h
50 cn: tested ar.a". / li6;i{XA>0.02
nslka *iih 50 cm, (tested
z. tte.i,tlS{r.'Af
;F./.**isArxl:{,, *E+titi,sA,tt:ri}:+.Tftt 4 +1Erll+-ttlt aiAE.
(The sanples sas/were analyzed on behalf of the atfricant
! e s u l t s w a s / w e r eo n l y g i v e n a s r t e i n f o . n a t i t y v a l u e , )
PFos++*d,(R"f
Inf orlation)'
"'.o"€
(1) riitrrf rTfi.'|tsld.&n,r+r+4rrf,
as mixing sanpre in one resrine.
The above
!A+ 2oo6trzztEa (Di rect iae 2006/t2ztw)
d.Ee,Ed,rlE*tla+,i6d.n,+0.
005%.
(May not be placed on the market o. used as a sDbstance o. consrituent
€qual io or nigh€r than 0.005 % by nass.)
of prepararrons
(2rtit{ttX4n&*fi&}.ei+d."%d.6s{.*{r1+;1!i*€1+}aX*Jt+ApFosi.4t?J*fi}.e.t&r€t6€};l4pFosEE
,i.&+,i!d.i,ifo.r%,6*r&€d.4{tti.4rf. {,RprrsaAt*f + 6E*;Ad.Ji;Aruc/.,.
(Maynot be placed on ihe na.k€t in seni-linisned prodocts or articles, or pa.ts rhereof, if
ure
c o n c e n t . a t i o n o f P F O Si s e q u a t r o o r h i g h e . t h a n 0 . 1 % b y n a s s c a l c ! l a t e d s i t h r e f e r e n c e t o t l e n a s s o f
s t . u c t u r a l i y o . f r i c . o s t r u c r u r a l l y d i s r i n . r p a r r s t ! a i c o n t a i n P F o . so r , f o . r e x r i t e s o r o t h e . c o a r e d
naterials,
if thc anoun! of PFOSis equal to o. hiahcr than Ug/nr of thc coated nateriat.)
c o m p a ityr : ; r , r ; : i r l , , ; - f i t . r l J r . n i r r , . r , , t i i
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ft,q(No.) : cE/20r2lr0835
E S ( D a t e ) : 2 0 1 2 1 0 1 / 1 1F * . ( p a s € ) : 5 o r l 0
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87, D 98669 IEIT,SDORF.GERILUY
tl&4!t(styl./I
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(B-1) 101. 014
-silver
plated coFpe.{tre-Cu. Ag - - %
(B-2) 101. 0131. - - - - -pure silve. sire-Ag l()()()
( B - 3 ) 1 0 1 . 0 1 2 3 . 0- - - - s i l v e r
platcd purest nickct vire-Ni99.98%. AgI%
-silve.-copper alloy plated cotpe. clad vire-Elcon D,
(B-4) 10r,0182.0 - -silver
(B 5) 101.0120.0
p l a t e d c o n s t a n t a nw i i € - C u N i 4 4 , A A S %
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ELSCHUI{OM
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3) ir'13{I i ^ : tl4* / Nameof the pe6on in chargeormeasu€m€nlrTroychans
tr*. {rtt*s
/curing. p€galaton
iqr{.&,cf ! / sdde MeasuEmenl
&lf;F n l*'.g6tt{ f, 6 }xn!trai&it,tirt /LoeTt
4rt/!inlt n.i'la{&,aib /
4,;) /Acid dig€slion by suitabte acid dependedon
dtrerenlsahdemaledat{asbetowiable)
MiorcMve digestion with HNO3/HC|/HF
,"rl4rOf jit& jt.li,lilt +
C( / H€i to appropriate
1)
2)
f [*a{*4+*it{rtc
/ AlkaliF6ion
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Aa@ reoia. HNO' HCl. HF. H,O,
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A, J6,€, nit /
Gold,olalinum,
Dalladium,
ceramic
,i(f rf 7h-ir,g t.rLrlf,.' I
irl#B*i{Aftrcnm 6id
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4?,*i&8tt$ / coot,
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rhcdddneiiAs€dbysgcompa^ys!b4d{ob6ai..a|condloi3ds
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t]n]l
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Test Report
iEIS(No.) : cE/2012l10835
E rr?(Dare) : 2012l01/11 F&(P,s")
ELSCHUKOMELEI$ROSCHUTZKOIIPONENTENB,qU
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a }l{,/\l
I a_i9*, / Nameoftheperson
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RomanWonq
r,$Ji( frt ^ : &+le / Nam€of thepersonIn chargeof measurement
TrcyCha;g
n^ ld,ElF / Firstlestry proce.s------------f
....,---.
prccess
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-. -,t
*{.€,S / Confimation
orccess
:l
Scre€n
analysis
/ ,, rfi+rt
I
I
sample
erlraclion
*s+*/
Soxhlet
melhod6i,+tx;*
Concentrale/Dilute
Enractedsoluiion
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Analysis
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Test Report
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F&{prse)
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jtli{,l.F : gi',g* / Naneof thepersonwhomademe€surement:
RitaChen
jrl:i,A ll, : #,*e / Nameof thepersonin cbargeof measurement:
TroyChang
*+E &t&.'sl'I
Analysis
wE6perfomedby lC
.Iir
Th s ddfuh.il
s '$u€d bl ft
np61s) rssbd fu bn cpod €nnor b
i.'.iiri:llr
it
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.;.: r.r- i.1-]ii1
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TestReport
it4(No. ) : cE/2012l10835 AS(Dare) : 201210r/tr
F*.(pase) : 9 of lo
E-SCHUKOM
EI-E(TROSCHUTZKO]\IIONENTEN&{U
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*Ji+n+fin€n /
Analyticalflow chartofSoxhtetextraction(LC/MS)procedure
r
r
i A/-F : ij!9*y / Nameofthe personwhomademeesuementRcmanWong
t4j:{, q i,\ : tF'.*4 / Nameof the personin chargeof measurement:
TroyChang
( rd8,{ a : Afi.+n*.n/Afi.+rt(*)
, **.:4i{bA4,
Test ltems: PFOS/PFOA. Benzotriazole)
*{*
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fi6(N". ) , c-E/2072/10a35
Es(Date) : 2tr2/ar/r1
E*@aEe) : r0 of t0
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8?, D.98669 WII-SDOTF,GERVA}Y
trlt[tl
+ ffifi tr'6*t*i
' Fl* ftfrfl*lt,rlz{tsi
(The tested sanple / part is narked bt an arror if
ir's
1083s
10835
** lE+344.(E"d of Report) ++
i:. j:r.i | ,.tll
itt: I
c d h p , i in r . i ' , r , " r i l ' i , ,
rhsdoarudE 3s!sdbyhe.omp,^yeqedb G6erydcodromor s
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fl|||trr
TWNCo0240906
TeaE R€DoTt
Applicant:
T i 1-f6l
l,'ca
Dhilinhirae
Jan 79, 20!2
Th.
LIMA Technologry Center,
Lipa
CiEy,
one (1) sroup
of submitsted samples said to be :
'Solder
Part Nu.arber
| 692320
DaEe Sample Received
I Ja'r 16, 2012
Datse Tests Started
. JaIr 16, 2412
TesE Conducled :
As requestsed by Lhe applicanE,
Authorized
or
Il-hF
Taiwan
!
for
deEails
please
refer
to attached
paqres,
By:
o.
.rta_tFt
'Tesriro
Services
Liinited
shall nol be reproduced
This report
except in fu1l, wilhout the written
approval of the laboratory.
IntertekTesting ServlcesTaiwanLtd.
8F., No. 423, RuiguangRd., NeihuOistdct,Taipel 114, Taiwan R O C.
tEA*&&&6E FAA
1145ltfi^*EH,6B423 S8||
rerr(+886'2)6€02-28882797-8885Fax (+88F2)6602-24006602_2401
Nunber
: TWNC00240906
Conducted
Test Result
Summary :
TesL Item
Result
(ppm)
Silvery
Metal
E6avy X€tel
cadmium (cd) content
ND
T,ead (Pb) content
(Hg) conLent
Mercury
Chromium VI (Cr6 ) conlen-
92'72',73
ND
lng/kg wilh
50cm')
NeqraEive (< 0.02 )
based on weights of tesLed sample = mg/kg
Remarks: ppm = Parls per million
ND = Not' detected
= Less than
<
per kilogram witsh 50 square centsimetre
mg/ks wiLh 5ocm'1= millisram
observaLion
=
indicaLed positive
test
result
A
negatsive
Negatsive
was nots found at lhe tsiine of Test.
Responsibility
of Chemist
Date Sample Received
Tests Perlod
(tr)
: Irene
Chiou / Kevin Liu
I Ja 16, 20L2
: L T a n1 6 , 2 0 1 2 T o J a n 1 9 , 2 0 1 2
RoHS Requirements:
Substances
Restrrcted
(cd)
ConEent
cadnd unl
Lead
(Pb)
0 . 0 1 * (1 0 o p p m )
0.1t (100oppm)
0.1t (100oppm)
0.1t (t00oppm)
Content
(Eg) ConLent
Mercury
Chromium vr tCr6t) Conlent
The above limitss were quotsed from 2AO2/95/EC and amendnent 2OO5/6lA/EC tor
homogeneous material,
PaEre 2 of
htenek T€tlng Servic* Taiwan Ltd.
Rd.,NeihuDistnclTaiper'll4 TaiwanR o C
8F , No 423,Ruiguang
4EaB*fr&6€&AE
114alhft^*Efl)t*423is|l
Tel:r+88e2)e6o2'2888 27974885 Fax (+88G2)6602-24006602_2401
5
Numlcer : 1\^1NC00240906
Tests Conducted
( I I I ) Test Metshod:
Cadrnium (Cd)
Lead (Pb) conlent
Mercury (Hs)
chromiun vr
(cr5*)
(mg/k€'witsh 50cm')
Remark:
ReporEingr
Tests Method
With reference to IEC 62321 edition
1.0r2008 in clause 8/9/10, by
lhe tested
nricrowawe digest.ion until
samples are Lotalfy dissolved and
deterndned by ICP-OES.
jgiLh reference to IEC 62321 ediLion
1.0:2008 in cLause 8/9/10, by
tshe testsed
microwave digestsion until
dissolved and
samples are totally
deLeimi'led by ICP-OES.
llith reference to IEC 62321 edition
1.0:2008 in clause 7r by microitave
Cigestsion unLil Ehe tested samples are
dissolved and delermined by
totally
TCP-OES.
With reference lo IEC 62321 ediEion
1.0:2008 in annex B, bY boilinq water
and determined by W-vis
extraction
limit
= Quantitalion
limit
of
analvte
in
lntertek T€tlng Service3 Taiwan Ltd.
Rd.,NeihuDi{nd, Taipei114 TaiwanR.Oc
8f., No.423,Ruiguang
EEAE*R&6€EAE
114elLfi ^xE*)tlg423i0||
, 2?974885Fax:(+88&2)
6602_2401
6602-2400
6602-28a8
Tel:(+88e2)
Reportins
1,imit
2 ppm
2 ppm
2 ppm
0.02
mgr/kg witsh 5ocm'z
sample
Numloer : TWNCo0240906
TesL Conducted
(IV) Measurdent
Florchari::
Test For Cd/Pb/HSlChxomlum (VI)
Reference SLandaid: rEC 6232a ediLion
sartplirs/grlldins
applolliate
contim
Malyzed
1.0:2008
or cultins
acid't
lhe
tesied
bY IcP
ols
Make up witn
calbazide
"li
List
d€ionized
solution
Of Applopliate
Acid
Added
Fof
Digestion
lNor Hc1, HF,H,O) HIBOr
ENO3.lIC1,HF
HNOr HCl, E)O, nBF.
*2:
If
the lesu1t
of
spot test
is posiEive,
Chronim
VI would L'e detennined
aE detected'
End of
Report
Page
Inte(€k Testing Se.vicesTalwan Ltd.
Taipei114,Taiwan,R O C.
Rd.,NeihuOistncl,
8F.,No.423,Ruiguang
EEAE**&6EEAA
1146ltfifrflEHrfB423 r 8|
6602-2400
6@2-2'101
27sru885 Fsx(+88€'2)
T€li(+846'2)
6602-2884
4 of
5
Nunilcer : T!']Nc00240906
TesE Conductsed
Photo
IntertekT€tlng servic* TaiwanLtd.
8F., No. 423, RuiguangRd., NeihuOistriol.Taipei 114, Taiwan,R O C.
6daa&&&6€'F'
E
114altfifrfl[Hr69423 s 8l
66022',101
6602_2400
Fa( (+8a6-2)
faroa€6-2tefo2'28f€2J97_3835
Test Report
Applicant:
Number : TWNC00236189
Littelfuse, Philippines Inc.
LIMA Technology Center, Lipa City,
Malvar, Batangas
Date
: Dec 13, 2011
Sample Description:
One (1) group of submitted samples said to be :
Part Description
: Epoxy Poweder Green HF
Part Number
: 087341
Date Sample Received
: Dec 08, 2011
Date Test Started
: Dec 08, 2011
Test Conducted :
As requested by the applicant, for details please refer to attached pages.
Authorized By:
On Behalf Of Intertek Testing Services
Taiwan Limited
K. Y. Liang
Director
This report shall not be reproduced
except in full, without the written
approval of the laboratory.
Page 1 of 9
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00236189
Test Conducted
(Ⅰ) Test Result Summary :
Test Item
Result (ppm)
Green Powder
Heavy Metal
Cadmium (Cd) content
Lead (Pb) content
Mercury (Hg) content
Chromium VI (Cr6+) content
Polybrominated Biphenyls (PBBs)
Monobrominated Biphenyls (MonoBB)
Dibrominated Biphenyls (DiBB)
Tribrominated Biphenyls (TriBB)
Tetrabrominated Biphenyls (TetraBB)
Pentabrominated Biphenyls (PentaBB)
Hexabrominated Biphenyls (HexaBB)
Heptabrominated Biphenyls (HeptaBB)
Octabrominated Biphenyls (OctaBB)
Nonabrominated Biphenyls (NonaBB)
Decabrominated Biphenyl (DecaBB)
Polybrominated Diphenyl Ethers (PBDEs)
Monobrominated Diphenyl Ethers (MonoBDE)
Dibrominated Diphenyl Ethers (DiBDE)
Tribrominated Diphenyl Ethers (TriBDE)
Tetrabrominated Diphenyl Ethers (TetraBDE)
Pentabrominated Diphenyl Ethers (PentaBDE)
Hexabrominated Diphenyl Ethers (HexaBDE)
Heptabrominated Diphenyl Ethers (HeptaBDE)
Octabrominated Diphenyl Ethers (OctaBDE)
Nonabrominated Diphenyl Ethers (NonaBDE)
Decabrominated Diphenyl Ether (DecaBDE)
Halogen Content
Fluorine (F)
Chlorine (Cl)
Bromine (Br)
Iodine (I)
Phthalates
Di(2-ethylhexyl) Phthalate (DEHP)
Dibutyl Phthalate (DBP)
Benzyl Butyl Phthalate (BBP)
Others
Hexabromocyclododecane (HBCDD)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
405
ND
ND
ND
ND
ND
ND
Remarks: ppm = Parts per million based on weight of tested sample = mg/kg
ND = Not detected
Responsibility of Chemist : Irene Chiou / Kevin Liu / Cathy Chen
Date Sample Received
Test Period
: Dec 08, 2011
: Dec 08, 2011 To Dec 12, 2011
Page 2 of 9
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00236189
Test Conducted
(Ⅱ) RoHS Requirement:
Restricted Substances
Cadmium (Cd) Content
Lead (Pb) Content
Mercury (Hg) Content
Chromium VI (Cr6+) Content
Polybrominated Biphenyls (PBBs)
Polybrominated Diphenyl Ehters (PBDEs)
Limits
0.01% (100ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for
homogeneous material.
(Ⅲ) Test Method:
Test Item
Test Method
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
Cadmium (Cd) content microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
Lead (Pb) content
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 7, by microwave
Mercury (Hg) content digestion until the tested samples
are totally dissolved and determined
by ICP-OES.
With reference to IEC 62321 edition
Chromium VI (Cr6+)
1.0:2008 in annex C, by alkaline
content
digestion and determined by UV-Vis
spectrophotometer.
With reference to IEC 62321 edition
1.0:2008 in annex A, by solvent
Polybrominated
extraction and determined by GC-MSD
Biphenyls (PBBs)
and further HPLC confirmation when
necessary.
With reference to IEC 62321 edition
Polybrominated
1.0:2008 in annex A, by solvent
Diphenyl Ethers
extraction and determined by GC-MSD
(PBDEs)
and further HPLC confirmation when
necessary.
Reporting Limit
2 ppm
2 ppm
2 ppm
1 ppm
5 ppm
5 ppm
Page 3 of 9
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00236189
Test Conducted
(Ⅲ) Test Method:
Test Item
Test Method
With reference to EN 14582:2007 by
Halogen Content
calorimetric bomb with oxygen and
determined by ion chromatography
With reference to EN 14372: 2004, by
Phthalates
solvent extraction and determined by
GC-MSD
With reference to USEPA 3540C, by
Hexabromocyclododecane
solvent extraction and determined by
(HBCDD)
GC-MSD
Reporting Limit
50 ppm
50 ppm
10 ppm
Remark: Reporting limit = Quantitation limit of analyte in sample
Page 4 of 9
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00236189
Test Conducted
(Ⅳ) Measurement Flowchart:
Test for Cd/Pb/Hg/Chromium (VI)/PBBS/PBDES Contents
Reference Standard: IEC 62321 edition 1.0:2008
Sample preparation
For non-metal part
For metal part
Take sample and immerse into Aqua Regia, start to strip plating layer
Stop the stripping procedure upon color change completely
Take the Aqua solution as plating component and stripped body as substrate component
Cd/Pb/Hg
Cr
Weigh sample and
add organic solvent
By spot test
Negative
Confirm the tested
samples are
totally dissolved
Make up with
deionized water
PBBs/PBDEs
Polymers /
electronics
Metal
For different
material, digest
the sample with
*1
appropriate acid
6+
Get 50cm2 sample
By boiling water
extraction
*2
Weigh sample
and add
alkaline
solution
By Soxhlet
extraction or
Solvent extraction
Definite temp.
extraction
Cool and filter
the extract
Analyzed by ICP-OES
Concentrate the
extract and make up
with organic
solvent
Analyzed by GC-MSD
Make up with deionized
water and add diphenylcarbazide solution
Remarks:
*1: List of Appropriate Acid：
Material
Polymers
Metals
Electronics
Analyzed by UV-VIS
Acid Added for Digestion
HNO3,HCl,HF,H2O2,H3BO3
HNO3,HCl,HF
HNO3,HCl,H2O2,HBF4
*2: If the result of spot test is positive, Chromium VI would be determined as detected.
Page 5 of 9
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00236189
Test Conducted
(Ⅳ) Measurement Flowchart:
Test for Halogen Content
Reference Standard：EN 14582
Sampling/grinding or
cutting
Add absorbent in a
combustion flask &
place weighed sample in
equipment
Fill oxygen into
calorimetric bomb
Ignite then leave the
flask at room
temperature
Transfer the absorbent
into a volumetric flask
Make up with deionized
water
Analyzed by ion
chromatography
Page 6 of 9
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00236189
Test Conducted
(Ⅳ) Measurement Flowchart:
Test For Phthalates Contents
Reference Method: EN 14372: 2004
Sampling/grinding or
cutting
Weigh sample and add
organic solvent
By solvent extraction
Concentrate the extract
and make up with
organic solvent
Analyzed by GC-MSD
Page 7 of 9
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00236189
Test Conducted
(Ⅳ) Measurement Flowchart:
Test For Hexabromocyclododecane (HBCDD)
Reference Standard：USEPA 3540C
Sampling/grinding or cutting
Weigh sample and add organic
solvent
By soxhlet extraction
Concentrate the extract and
make up with organic solvent
Analyzed by GC-MSD
End of Report
Page 8 of 9
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00236189
Test Conducted
Photo
Page 9 of 9
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401