ICPTest_251L_HF_version_02 06 2013 pdf

ICP Test Report Certification Packet
Company name :
Littelfuse, Inc.
Product Series:
Pico
Product #:
251xxxL Series with low halogen content
Issue Date:
February 6, 2013
It is hereby certified by Littelfuse, Inc. that there is neither RoHS (EU Directive 2002/95/EC,
2011/65/EU)-restricted substance nor such use, for materials to be used for unit parts, for
packing/packaging materials, and for additives and the like in the manufacturing processes.
In addition, it is hereby reported to you that the parts and sub-materials, the materials to be used
for unit parts, the packing/packaging materials, and the additives and the like in the manufacturing
processes, are all composed of the following components.
Issued by:
<Global EHS Engineer>
(1) Parts, sub-materials and unit parts
This document covers the Pico RoHS-Compliant series products manufactured by
Littelfuse, Inc.
＜ Raw Materials Used
Please see Table 1
(2) The ICP data on all measurable substances
Please see appropriate pages as identifed in Table 1
Remarks：
Pb (lead) contained in the high temperature melting solder > 85% and is categorized as
exempt under section 7a of the RoHS Annex.
Form 585-047 Rev. A
1
2/21/06
Table 1: List of Raw Materials covered by this report
Total Parts
1
2
3
4
5
6
7
Raw Material Part Number
910-xxx (910-263/ 910-023)
SIKOR C410 (909-144)
11-0803 (497xxx)
082xxx
082xxx
692320
087229-HF
(Old part number is 087341)
Raw Material Description
Cap and Lead Assembly
Body – Ceramic Tube
Element – Ni42Fe58MCuMAg5%
Element – 5% by weight Ag Clad Cu
Element – 2% Ag plated Cu
Solder
Page(s)
3-7
8-36
37-41
42-46
47-51
52-57
Epoxy Powder
58-67
2
Test Report
Applicant:
Number : TWNC00256249
Littelfuse Philippines Inc.
LIMA Technology Center, Lipa City,
Malvar, Batangas
Date
: May 10, 2012
Sample Description:
One (1) group of submitted samples said to be :
Part Description
: Cap and Lead Assay
Part Number
: 910-023/910-263(910XXX)
Date Sample Received
: May 07, 2012
Date Test Started
: May 09, 2012
Test Conducted :
As requested by the applicant, for details please refer to attached pages.
Authorized By:
On Behalf Of Intertek Testing Services
Taiwan Limited
K. Y. Liang
Director
This report shall not be reproduced
except in full, without the written
approval of the laboratory.
Page 1 of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00256249
Test Conducted
(Ⅰ) Test Result Summary :
Test Item
Heavy Metal
Cadmium (Cd) content
Lead (Pb) content
Mercury (Hg) content
Chromium VI (Cr6+) content (mg/kg with 50cm2)
Test Item
Heavy Metal
Cadmium (Cd) content
Lead (Pb) content
Mercury (Hg) content
Chromium VI (Cr6+) content (mg/kg with 50cm2)
Result (ppm)
(1)
(2)
ND
ND
ND
Negative
(< 0.02)
(#)
ND
55
ND
Negative
(< 0.02)
(#)
Result (ppm)
(3)
(4)
ND
ND
ND
Negative
(< 0.02)
(#)
ND
196
ND
Negative
(< 0.02)
(#)
Remarks: ppm = Parts per million based on weight of tested sample = mg/kg
ND = Not detected
<
= Less than
mg/kg with 50cm2 = milligram per kilogram with 50 square centimetre
Negative = A negative test result indicated positive observation
was not found at the time of Test.
#
= Due to the insufficient sample area, reduced total sample
surface of 10 cm2 was used and the dilution factor was
adjusted accordingly.
Tested Components
(1) Coppery Substrate(Body)
(2) Silvery Plating(Body)
(3) Coppery Substrate(Pin)
(4) Silvery Plating(Pin)
Responsibility of Chemist : Irene Chiou / Kevin Liu / Cathy Chen
Date Sample Received
Test Period
: May 07, 2012
: May 09, 2012 To May 10, 2012
Page 2 of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00256249
Test Conducted
(Ⅱ) RoHS Requirement:
Restricted Substances
Cadmium (Cd) Content
Lead (Pb) Content
Mercury (Hg) Content
Chromium VI (Cr6+) Content
Limits
0.01% (100ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for
homogeneous material.
(Ⅲ) Test Method:
Test Item
Cadmium (Cd)
content
Lead (Pb) content
Mercury (Hg)
content
Chromium VI (Cr6+)
content
Test Method
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 7, by microwave
digestion until the tested samples are
totally dissolved and determined by
ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in annex B, by boiling water
extraction and determined by UV-Vis
Spectrophotometer.
Reporting Limit
2 ppm
2 ppm
2 ppm
0.02
mg/kg with 50cm2
Remark: Reporting limit = Quantitation limit of analyte in sample
Page 3 of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00256249
Test Conducted
(Ⅳ) Measurement Flowchart:
Test for Cd/Pb/Hg/Chromium (VI)
Reference Standard：IEC 62321 edition 1.0:2008
Sample preparation
Take sample and immerse into Aqua Regia, start to strip plating layer
Stop the stripping procedure upon color change completely
Take the Aqua solution as plating component and stripped body as substrate component
Cd/Pb/Hg
Cr
Polymers /
electronics
Metal
For different
material, digest
the sample with
*1
appropriate acid
By spot test
Negative
Confirm the tested
samples are
totally dissolved
Make up with
deionized water
6+
*2
Weigh sample
and add
alkaline
solution
Get 50cm2 sample
Definite temp.
extraction
By boiling water
extraction
Cool and filter
the extract
Analyzed by ICP-OES
Make up with deionized water and add
diphenyl-carbazide solution
Remarks:
*1: List of Appropriate Acid：
Material
Polymers
Metals
Electronics
Analyzed by UV-VIS
Acid Added for Digestion
HNO3,HCl,HF,H2O2,H3BO3
HNO3,HCl,HF
HNO3,HCl,H2O2,HBF4
*2: If the result of spot test is positive, Chromium VI would be determined as detected.
End of Report
Page 4 of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00256249
Test Conducted
Photo
Page 5 of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Signaturetid
ForQue
Please
TestRePort
1 of 29
No.: CE/2013/13197D e.2O13lO1l22Page:
GMBH
CERAMTEC
15' 91207LAUF
MULTIFUNKTIONSKEMMIK,LUITPOLDSTRABE
GESCHAFTSBEREICH
Tho following sample(s)wae/weresubmitted and
SampleDescription
No.
Style/ltem
SampleReceivingDate
TestingPeriod
t
lllllllllll
identifiod by/on behalf of the client as:
CERAMIC
stKoR c410
201311114
122
1l14 r o 2013101
20131
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TeBtR€6ult(s)
the test resultsof CaTilt: llf I
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pBBs
complywiththe limitsas setDy
PBDES
and
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Concluslon
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I-AUF
15'e1207
3E$HIFf#R|'",.. MULTTFUNKTT.NSKERAMTK,LuTTPoLD.TMBE
Te3t Result(s)
PARTI'IAMENo.1
CERAMIC
LT.GRAY
MDL
lethod
Unit
R€6ult
Limit
2
No.1
n.d.
oerformedbv ICPAES
mgikg with referenceto lEu bzrz r. uuuo
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2
69
1000
(Hg)
Mercury
mg/Rg With reference to IEU bztz tt zwo 4l
2
n.o.
1000
Fidavater*ctrromiumCr(vt)
mg/Kg With referenceto IEU oz.rz I zuuo
2
n.d.
1000
Ts€tltem(s)
6admiumlcdt
aead(Pb)
mg/Kg ,\rith referenceto lEu bzrzt zvvo 4l
.edormed bv ICP-AES.
Derfomed bY W-VIS
vo
(cns
ptttnatae)
o-i6'fioiisooecyt
No.:267614G0)
phthalate)(cAS
-tNp (Di-rsononyl
No.:28553-124)
(cAs
6NdF (Di-n-octyl
Phthalate)
No.:11744-0)
(cAs No:
S6FlDibutytphthalate)
u-74-2\
sulfonates
F;dluorooc'lane
MetalSalt'Amide)
(PFOS-Acid,
(cAs No.:335€7-1)
FF6A(A
o/o
0.003
n.d.
with €felence to EN rar/2. Arrcrvrl
wa6 oerformed bYGC/MS
0.01
n.d.
With reference to EN l'+r/z ^Irdrvrrr
0.01
n.d.
0.003
n.d.
0.003
n.d.
'10
n.d.
10
n.o.
0.5
n,o.
with reference to EN t45lz. ^tt11'l
,nasDedormedbYGC/MS
wasDerfomedbYGC/MS
%
With referencero EN l'rJZ ^rrcrv'''
sr:s o€rfomed bYGC/MS.
%
With rclelence rc EN r4o''
^r'rt''e
waso€rformedbYGC/MS.
mg/Kg /Vithrcbrencerc un ErA oorw'
AnalysiswasPerfomedbY
ZOO7.
mg/xg with €lerence Io uD EF^ eJrv!
2007.AnalysiswasPerfomedbY
I c/Ms
giphenvts
(pces) mgKg
F6ii6fr!6rinateo
(CASNo.:1336363)
n.d.
ms oerformed bv GC/MS.
No.:8548-7)
dEFiP(Di-(2-€thylheryl)
(CASNo: 117-81-7)
phthalate)
0.003
Wii6EEi6E6€N- 14322.Analysis
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Ptuaute)(ces
100
With relelence ro ur Er^ rF""
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wasPerformed
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method.
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bY
Analysiswas
(PCTs)
fllorinatodNaPf thatene
(PCNs)
Performed
method.
GC/MS.
mg/kg With rclerenceto uD Er^ rlruv
method.Analysi6wasPerformedbY
0.5
Result
No.1
n.d.
5
n.d.
MDL
GC/MS
mg./Kg With retelenceIo ur ErA r*ev
chloro(short
c10-'13,
Alkanes,
method.Analy6iswasPerformedbY
(C'AS
Parafiins)
ChainChlodnated
GC/MS
No.:8553*41)
r I r^ a'
PVC
Analysi9wasPenormeooY
FLAMETest.
(cr5 t'lo: so-ooo) mg/Kg
F6if,EiGfri3e
With reteren@ rc l5u tlzza't\zwe)
100
n.d.
Negative
3
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0.5
n.d.
rc us Er^ o''""
mg/kg Withreierence
fi 6i6me-m'etnytdictrtorodiptenyt
method.AnalysiswasPedormedbY
(Ugilec121)
methane
0.5
n.d.
wilh refelenceto ub Er^ oztue
method.Analysiswas PerfomedbY
GC/MS,
0.5
n.d.
Analvsiswasp€rformedby HPLC/DAD
mgKg With retelenceIo uJ ErA oz' v"
method.AnalysiswasPerformedbY
fi6i6mahyt dibromodiPnenYt
(DBBT)
methane
GC/MS
M6fi
66Eifrlltetrachlorodlpnenylmg/Kg
methane(Ugilec141)
l.lelooen
ffi areiFnjffi(D (cAsNo: I ms/ks
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Limit
|
mg/kg
'
With referenc€to BS EN 14582t2oo7
lC
bY
mgKg AnalysiswasPerformed
mg/Kg
'3
DlNaS4o?'1
t"
wrh
'"f""C
mg/Kg
bYGC/FPD
w€sPedormed
mgKg Analysis
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50
n.d.
50
n.d.
50
n,o-
0.03
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0.03
n.d.
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Test Report
Dale:20131O1t22Page:4of 29
No.: CE12O13/13197
l|r]|||r]
GMBH
CERAMTEC
5' 91207tAUF
MULTIFUNKTIONSKERAMIK'LUITPOLDSTRABE'1
GESCI.TAFTSBEREICH
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method
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Negative
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With referenceto EPA600/R-93i116
method.Analysis'.taspertormedby
StereoMicroscope(SM)' Di6pe6ion
StainingPolarizedLightlMicroscope
(DS-PLM)andX-€Y Diffraction
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Negative
Negative
Negative
%
AZO
Result
3
n.d.
3
n.d.
3
n.d.
3
n.o.
3
n.d.
3
n.d-
3
n.d.
3
n.d.
3
n.d.
mg/Kg wth €telence ro Lr\rD
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anrlvsis was oerformed bY GC/MS
3
n.d.
With relerence ro Lr\rD o. va_''
analvsis was oerformed bY GC/MS
With reterenc€Io Lr\rD 04 uz_z'
3
n.d.
3
n.d.
(cAs No. mgftg Withreferenceto Ll-uE ol uz-z
PHENYL
ij:.4.AMrNoDl
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bY GC/MS
5i-cHLoRo-o-ToLUIDINE
(CASNo.:95€9-2)
(CAS
4}2-NAPHTHYLAMINE
No.:91-59-8)
6jmlNoAzoroLUENE (cAS
No.:97-56-3)
Analvsis vras Performed
mg/kg With reference to LFGb uz.uz-z
Analysis was Perfomed bYGC/MS
mg/Kg Nith €i€rence to LFlto 6z.uz_2.
\nalveis w€s PerformedbY GC/MS
mg/kg y'Vithreference to Ll_Gb 62 ur-z
Analvsiswas Per{omed bYGC/MS
6ilfr tvtiNo-q-NlrnorolueNemg/K9
(CASNo.:99-55-8)
Wiih referenceto LFGB82.(2-2
Analvsis
wasD€rfomedbYGC/MS
(cAsNo.: m9Kg With referenceto Ll-uE !z uz_Z.
TjlF:eHLoRoANlLlNE
Analvsis e€6 PerformedbY GC/MS
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(cAs
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No.:615-05-4)
9):4,4-
drll,tntootpHeuvLl,tEtHArue
mg/Kg With refelence to Ll_uit oz uz-z
Analvsis was PerformedbYGC/MS
mS/kS With reference to LFrrn oz uz-z
Analysis was Perfomed bYGC/MS
(CASNo.: 101-779
(CASNo.:91-941)
mgiKg
iili .a'-omelroxrgerlztotre
(CASNo.:119-904)
-53io-ifi
ernwgevtotne mgKg
ilf
(CASNo.:119-93-7)
oz v._''
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bYGCiMS
Analysis
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Limit
TestRePort
No.: CE/20'1:|/13197Oate 2013101t22Page:5 of 29
!:]
GMBH
CERAMTEC
15' 91207LAUF
MULTIFUNKTIONSKERAMIK,LUITPOLDSTRABE
GESCHAFTSBEREICH
T6t ltem(5)
Unlt
Method
mg/Kg With refelence to Lf(,t dz uz_z
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DIAMINODIPHENYLMETHANE
(CASNo.:838-88-0)
oz uz-z
fitTcREstDlNE (2-METHoxY-mg/kg With reteFnce to LruB
gi,tElHYLeNtLtNo
(cns No.,
120-71-8)
(2iSITTLMETHYLENE-Bls(CAS
No.:
CHLOROANILINE)
101-1441
mg/Kg With retelence to Lrsit oz uz-z
With rclerence to LFutt oz.uz-z
Analvsis wa6 PerformedbYGC/MS'
mg/Kg With Gterenceto Lr(,tt oz.uz-u'
Analvsi6 was PerformedbY GC/MS'
mg/Kg With referenceio LFUE sz uz_Z.
Analvsiswas PerformedbYGC/MS'
mgftg with rcFrence to Lr\tD oz uz-.
Analvsis was DedormedbYGC/MS
mg/Kg With relerence rc LFstt oz.vz_z'
Analvsis was Perfomed bYGC/MS'
IIiZIToLUYLENEDIAMINE mg/kg
LlNE
tdiltTS-TRTMEiHYLANI
t3717-7)
(CASNo.:
@nrstotNe
(cls tto.:so
04-0)
ttT-AMtNoAzoBENZENE
(CAsNo.:60-09-3)
-2j-xYLrD[.lE (cAs No.:956&1)
'AIZEXYLIDINE(cAs No: 8762-7)
3
n.d.
3
n.d.
3
n.d.
Limlt
Analysiswas Per{ormedbYGC/MS
mgKg With referenceto LFUE!z uz_z
Analvsis',!asperformedby Gc/Ms
mg/kg With referencelo LFutt or'uz_z
rzr-21:+Srl.toonntuuelcns
AnalysiswasPerfomedbYGC/MSNo.:139651)
(cAs No.r95- mgKg With referenceto Ll-uE bz uz_z
oLl.JlDlNE
iEj
AnalvsiswasPerformedbYGc/Ms
(CASNo.:95-80-7)
R€6ult
No.t
Analysis wa6 PerformedbYGC/MS
'16):4/A'-oXYDIANILINE
(CAS
No.:10140-4)
53{)
MDL
lrllllllllfll
mg/Kg with referencelo Ll_utt oz,uz-z.
Analvsi6w€sPerformedbYGC/MS'
n.d.
3
n.d.
3
n.d.
3
n.d-
3
n.d.
n.d.
3
n.d.
3
n.d.
3
n.d.
cFc'3 ((;nloror|uorcEaruvrr',
GroupI
lcAs t'to:
Efri-rdtuorocarton-tt
75694)
(CnSuo :
dfi66iluorocarbon-'12
75-71€)
mgKg With retelencerc u! Er^ ou' '
method.AnalysiswasPer{ormedbY
GC/MS.
mg/Kg With lelelencero uD ErA ouz'
method.AnalysiswasP€rformedbY
GC/MS,
n.d.
1
n.d.
sir;r3:i#irr:ryr5's,,"''riirfl{]ii;fim:ilH;,;|f;TTild,j;'li*'ii'flfiffiffi
!#t{iil'i#,;r.r''$*utru,rfu+ii*i'*l+li.+uli*l,pqa+,r*
r:",,,:-.li'i;:;tfri:,ti$f?
ffilla${#}iffiltt}*illffi.Ttrffi"r
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Test Report
Oale :2013101122 P a g e : 6 o f 2 9
No.:CE/2013/'13197
Itr|l[ttl]lll[lll
CERAMTECGMBH
15,91207LAUF
eEsCHliiseEnercFtt/tuLTtFUNKTIoNsKERAMIK,LUITPoLDaTRABE
T€al ltem(s)
Resull
No.1
MDL
Mdhod
Unit
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mg/kg fv n-referenceto US EPA502'1
method.AnalysiswasPerformedbY
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14(CAsNo.: mg/Kg With referenceto US EPA5021
ehbrofluorocalbon-1
wa6PerfomedbY
Analy€is
method.
76-1+2\
GC/MS.
to Us EPA5021
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Analysis
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13 ICASNo :
Florof luorocarbon-1
76-13-1)
n.d.
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n.d.
1
n.d.
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to us EPA5021
mg/Kg wth referenc€
1 (CASNo :
Chlorofluorocarbon-11
3545e3)
mg/kg With referenceto US EPA5021
method.AnalysiswesPerformedbY
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n.d.
ffiroRuorocaroon-tt 2 (CnSNo:
76-12-0)
to USEPA5021
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n.d.
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Analysis
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bY
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Analysis
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Pedormed
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eFi;-rolhlorofl
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1
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1
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3182-2Cl)
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No: I ms/ks with referenceto us EFAouzI
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method.AnalysiswasPerfomeclbY
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|
GC/MS.
un Er^ ouzI
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Analysis
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I
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No.:CE/201313197 Dale:2013101122Page:7 of 29
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MDL
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ael-97-2)
HCFCs
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R€sult
No.'l
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1
n.d.
1
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Analysis
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m9Kg With €lerenceto us EFAouzI
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Analysis
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mgKg With referenceto us El'A cuz I
FEFElgt(cesNo.:s9+zM)
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GC/MS.
to USEPAs02t
frEFdr7il6esMlasa-145 mgKg Wttr reference
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FEffi-tzz(cesHo.:as+-zl'z) m9Kg Wiitrreference
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Analysis
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(cnsuo.::00-gg-z)
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Analysiswas
1
n.d.
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lmetJtod
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by
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1
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No.: CE/2013/13197Dale:2o13to1122Page:8 of 29
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mg/Kg Witheferenceto us EPA5uzI
R€ult
No.l
1
n.o.
I
n.d.
1
n.d.
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Analysis
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mg/kg Wittrreferenceto US EPA5021
method.Analysisurasper{orm€dby
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mgiKg W-lthref€renceto US EPA5021
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n-d.
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method.
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mgKg WiifErence to us EPA5021
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AnalFiswasPerformed
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mgKg With referenceto us EPAcuz I
bY
wasPedormed
Analy6is
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refelence to ub El'A ouz I
With
msyKg
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method.Analysisurasperformedby
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FEFe-zat
lceSNo.:4zt-91-:1 mg/kg with reference to u5
n.d.
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1
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No.:CE/201313197 Datet2113rc1f22 Page:I of
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-G235(cAsNo.:460-924)
method.AnalysiswasPerformedbY
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No.: CE/2013/13197D.f(e: 2013101122Page: 10of 29
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hydrocarbon)
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method.Analysis,r/asPedormedbY
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(CAsNo :
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71-55€)
lF-Tetrachloroethane(cAs
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34-3)
(CAsNo.: zsiJ5ictriDictrloroettrene
354)
(cnSHo:
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56&5&6)
(CASNo:
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96-18-4)
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107{&2)
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to US ePn SOZI
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method.Analy6iswa6PerfomedbY
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m!yKg Wittr referenceto US EPA5021
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m9Kg w-lthreference
n.d.
1
n.d.
1
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n.d.
n.d.
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method.
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mg/Kg WiifrErenceio UsEPA5021
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No.: CE/2013,/13'197
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mg/Kg Witfrreferenceto US EPA5021
(CASNo :
1.lDi-chloroprcpane
142-28-S)
to Us EPn502t
mg/kg WilFE-ference
1
n.d.
GC/MS.
mg/Kg With referenceto US EPA5021
I
n.d.
1
n.d.
method.AnalysiswasPerformedbY
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78€7-5)
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22Dichloropropane
594-2O-7)
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method.
method-Analysisv€s PerformedbY
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io us EPnso2t
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method.AnalysiswasPerformedbY
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to USEPnS021
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n.d.
(cASNo.:67€6-3)
dfrlorolorm
mgKg With referenceto Us El'A 5uzr
method.Analy8iswasPerfomedbY
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mgKg Wlrreferenceto uS EPA502'l
n.d.
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bY
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method.
cc/Ms.
method-Analysis wa6 Pedomed bY
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uu ErA 3uz I
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mgKg
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GiilZfi6Eiene Prs Ho:tzz184)
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5
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5
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No.:CE/2013i/13197Oetrie:2O13t01122
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Dale: 2o13101D2 Page: 15of 29
No.;CE/2013/13197
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CERAMTECGMBH
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MULTIFUNKTIONSKERAMIK,LUITPOLDSTMBE
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t Nameof the Dersonlvhomademeasurement:
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Page: 16of 29
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No.: CE2013/13197 Dalo 2013101122Page| 23 of 29
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No.:CE/2013/13197
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Test Report
Applicant:
Littelfuse Philippines Inc.
LIMA Technology Center, Lipa City,
Malvar, Batangas
Number
: TWNC00294417
Date
: Jan 17, 2013
Sample Description:
One (1) group of submitted samples said to be :
Part Description
: Ni42Fe58MCuAg5% Element
Part Number
: 497226 (497xxx)
Date Sample Received
: Jan 11, 2013
Date Test Started
: Jan 11, 2013
Test Conducted :
As requested by the applicant, for details please refer to attached pages.
Authorized by:
On Behalf of Intertek Testing Services
Taiwan Limited
K. Y. Liang
Director
*THJ0294417*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C.
全國公證檢驗股份有限公司
11492 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410
Page 1 of 5
Number
: TWNC00294417
Test Conducted
(Ⅰ) Test Result Summary:
Test Item
Unit
Test Method
Result
Silvery
metal wire
RL
ND
2
ND
2
ND
2
Negative
0.02
Heavy Metal
Cadmium (Cd) content
ppm
Lead (Pb) content
ppm
Mercury (Hg) content
ppm
Chromium VI (Cr6+) content
Remarks:
mg/kg
with
50 cm2
With reference to IEC
62321: 2008, by
microwave digestion and
determined by ICP-OES.
With reference to IEC
62321: 2008, by
microwave digestion and
determined by ICP-OES.
With reference to IEC
62321: 2008, by
microwave digestion and
determined by ICP-OES.
With reference to IEC
62321: 2008, by boiling
water extraction and
determined by UV-Vis
Spectrophotometer.
ppm = parts per million based on weight of tested sample = mg/kg
ND
= Not detected
RL
= Reporting Limit, Quantitation limit of analyte in sample
mg/kg with 50cm2 = milligram per kilogram with 50 square centimeter
Negative = A negative test result indicated positive observation was not
found at the time of Test. When the spot test showed a negative
result, the boiling water extraction procedure shall be used to
verify the result.
Responsibility of Chemist:
Date Sample Received
Test Period
Kevin Liu/ Irene Chiou
: Jan 11, 2013
: Jan 11, 2013 To Jan 15, 2013
(Ⅱ) RoHS Limits:
Restricted Substances
Limits
Cadmium (Cd) content
Lead (Pb) content
Mercury (Hg) content
Chromium VI (Cr6+) content
0.01% (100ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
The above limits were quoted from Annex II of 2011/65/EU for homogeneous material.
*THJ0294417*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C.
全國公證檢驗股份有限公司
11492 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410
Page 2 of 5
Number
: TWNC00294417
Test Conducted
(Ⅳ) Measurement Flowchart:
Test For Cd/Pb/Hg/Chromium (VI)
Reference Standard：IEC 62321 edition 1.0:2008
Sampling/grinding or cutting
Cd/Pb/Hg
Cr
6+
Polymers /
Electronics
Metal
For different
material, digest
the sample with
*1
appropriate acid
By spot test
Negative
Confirm the tested
samples are
totally dissolved
Make up with
deionized water
*2
Weigh sample
and add
alkaline
solution
Get 50cm2 sample
Definite temp.
extraction
Boiling water
extraction
Cool and filter
the extract
Analyzed by ICP-OES
Make up with deionized
water and add diphenylcarbazide solution
Analyzed by UV-VIS
*THJ0294417*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C.
全國公證檢驗股份有限公司
11492 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410
Page 3 of 5
Number
: TWNC00294417
Test Conducted
Remarks:
*1: List of Appropriate Acid：
Material
Acid Added for Digestion
Polymers
HNO3,HCl,HF,H2O2,H3BO3
Metals
HNO3,HCl,HF
Electronics
HNO3,HCl,H2O2,HBF4
*2: If the result of spot test is positive, Chromium VI would be determined as
detected.
End of Report
This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a
recommendation for any particular course of action. Intertek does not accept a duty of care or any other responsibility to any person other than
the Client in respect of this report and only accepts liability to the Client insofar as is expressly contained in the terms and conditions
governing Intertek's provision of services to you. Intertek makes no warranties or representations either express or implied with respect to this
report save as provided for in those terms and conditions. We have aimed to conduct the Review on a diligent and careful basis and we do not
accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by statute or otherwise, except in
the event of our gross negligence or wilful misconduct.
*THJ0294417*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C.
全國公證檢驗股份有限公司
11492 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410
Page 4 of 5
Number
: TWNC00294417
Test Conducted
Photo
*THJ0294417*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C.
全國公證檢驗股份有限公司
11492 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410
Page 5 of 5
Test Report
Applicant:
Number : TWNC00249177
Littelfuse Philippines Inc.
LIMA Technology Center, Lipa City,
Malvar, Batangas
Date
: Mar 26, 2012
Sample Description:
One (1) group of submitted samples said to be :
Part Description
: Silver Clad Cu Wire with 5% Ag
Part Number
: 082xxx(082375)
Date Sample Received
: Mar 22, 2012
Date Test Started
: Mar 22, 2012
Test Conducted :
As requested by the applicant, for details please refer to attached pages.
Authorized By:
On Behalf Of Intertek Testing Services
Taiwan Limited
K. Y. Liang
Director
This report shall not be reproduced
except in full, without the written
approval of the laboratory.
Page 1 of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00249177
Test Conducted
(Ⅰ) Test Result Summary :
Test Item
Heavy Metal
Cadmium (Cd) content
Lead (Pb) content
Mercury (Hg) content
Chromium VI (Cr6+) content (mg/kg with 50cm2)
Remarks: ppm =
ND =
<
=
mg/kg
Result (ppm)
Silvery Wire
ND
ND
ND
Negative (< 0.02)
Parts per million based on weight of tested sample = mg/kg
Not detected
Less than
with 50cm2 = milligram per kilogram with 50 square centimetre
Responsibility of Chemist : Irene Chiou / Kevin Liu / Cathy Chen
Date Sample Received
Test Period
: Mar 22, 2012
: Mar 22, 2012 To Mar 26, 2012
(Ⅱ) RoHS Requirement:
Restricted Substances
Cadmium (Cd) Content
Lead (Pb) Content
Mercury (Hg) Content
Chromium VI (Cr6+) Content
Limits
0.01% (100ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for
homogeneous material.
Page 2 of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00249177
Test Conducted
(Ⅲ) Test Method:
Test Item
Cadmium (Cd)
content
Lead (Pb) content
Mercury (Hg)
content
Chromium VI (Cr6+)
content
Test Method
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 7, by microwave
digestion until the tested samples are
totally dissolved and determined by
ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in annex B, by boiling water
extraction and determined by UV-Vis
Spectrophotometer.
Reporting Limit
2 ppm
2 ppm
2 ppm
0.02
mg/kg with 50cm2
Remark: Reporting limit = Quantitation limit of analyte in sample
Page 3 of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00249177
Test Conducted
(Ⅳ) Measurement Flowchart:
Test For Cd/Pb/Hg/Chromium (VI)
Reference Standard：IEC 62321 edition 1.0:2008
Sampling/grinding or cutting
Cd/Pb/Hg
Cr
Polymers /
Electronics
Metal
For different
material, digest
the sample with
*1
appropriate acid
By spot test
Negative
Confirm the tested
samples are
totally dissolved
Make up with
deionized water
6+
*2
Weigh sample
and add
alkaline
solution
Get 50cm2 sample
Definite temp.
extraction
Boiling water
extraction
Cool and filter
the extract
Analyzed by ICP-OES
Make up with deionized
water and add diphenylcarbazide solution
Remarks:
*1: List Of Appropriate Acid：
Material
Polymers
Metals
Electronics
Analyzed by UV-VIS
Acid Added For Digestion
HNO3,HCl,HF,H2O2,H3BO3
HNO3,HCl,HF
HNO3,HCl,H2O2,HBF4
*2: If the result of spot test is positive, Chromium VI would be determined as detected.
End of Report
Page 4 of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00249177
Test Conducted
Photo
Page 5 of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Test Report
Applicant:
Number : TWNC00249178
Littelfuse Philippines Inc.
LIMA Technology Center, Lipa City,
Malvar, Batangas
Date
: Mar 26, 2012
Sample Description:
One (1) group of submitted samples said to be :
Part Description
: Silver Clad Cu Wire with 2% Ag
Part Number
: 082xxx(082684)
Date Sample Received
: Mar 22, 2012
Date Test Started
: Mar 22, 2012
Test Conducted :
As requested by the applicant, for details please refer to attached pages.
Authorized By:
On Behalf Of Intertek Testing Services
Taiwan Limited
K. Y. Liang
Director
This report shall not be reproduced
except in full, without the written
approval of the laboratory.
Page 1 of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00249178
Test Conducted
(Ⅰ) Test Result Summary :
Test Item
Heavy Metal
Cadmium (Cd) content
Lead (Pb) content
Mercury (Hg) content
Chromium VI (Cr6+) content (mg/kg with 50cm2)
Remarks: ppm =
ND =
<
=
mg/kg
Result (ppm)
Silvery Wire
ND
ND
ND
Negative (< 0.02)
Parts per million based on weight of tested sample = mg/kg
Not detected
Less than
with 50cm2 = milligram per kilogram with 50 square centimetre
Responsibility of Chemist : Irene Chiou / Kevin Liu / Cathy Chen
Date Sample Received
Test Period
: Mar 22, 2012
: Mar 22, 2012 To Mar 26, 2012
(Ⅱ) RoHS Requirement:
Restricted Substances
Cadmium (Cd) Content
Lead (Pb) Content
Mercury (Hg) Content
Chromium VI (Cr6+) Content
Limits
0.01% (100ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for
homogeneous material.
Page 2 of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00249178
Test Conducted
(Ⅲ) Test Method:
Test Item
Cadmium (Cd)
content
Lead (Pb) content
Mercury (Hg)
content
Chromium VI (Cr6+)
content
Test Method
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 7, by microwave
digestion until the tested samples are
totally dissolved and determined by
ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in annex B, by boiling water
extraction and determined by UV-Vis
Spectrophotometer.
Reporting Limit
2 ppm
2 ppm
2 ppm
0.02
mg/kg with 50cm2
Remark: Reporting limit = Quantitation limit of analyte in sample
Page 3 of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00249178
Test Conducted
(Ⅳ) Measurement Flowchart:
Test For Cd/Pb/Hg/Chromium (VI)
Reference Standard：IEC 62321 edition 1.0:2008
Sampling/grinding or cutting
Cd/Pb/Hg
Cr
Polymers /
Electronics
Metal
For different
material, digest
the sample with
*1
appropriate acid
By spot test
Negative
Confirm the tested
samples are
totally dissolved
Make up with
deionized water
6+
*2
Weigh sample
and add
alkaline
solution
Get 50cm2 sample
Definite temp.
extraction
Boiling water
extraction
Cool and filter
the extract
Analyzed by ICP-OES
Make up with deionized
water and add diphenylcarbazide solution
Remarks:
*1: List Of Appropriate Acid：
Material
Polymers
Metals
Electronics
Analyzed by UV-VIS
Acid Added For Digestion
HNO3,HCl,HF,H2O2,H3BO3
HNO3,HCl,HF
HNO3,HCl,H2O2,HBF4
*2: If the result of spot test is positive, Chromium VI would be determined as detected.
End of Report
Page 4 of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00249178
Test Conducted
Photo
Page 5 of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00294413
Test Report
Applicant:
Littelfuse Philippines Inc.
LIMA Technology Center, Lipa City,
Malvar, Batangas
Date
: Jan 17, 2013
Sample Description:
One (1) group of submitted samples said to be :
Part Description
: Solder
Part Number
: 692320
Date Sample Received
: Jan 11, 2013
Date Test Started
: Jan 11, 2013
Test Conducted :
As requested by the applicant, for details please refer to attached pages.
Authorized by:
On Behalf of Intertek Testing Services
Taiwan Limited
K. Y. Liang
Director
*THJ0294413*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C.
全國公證檢驗股份有限公司
11492 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410
Page 1 of 6
Number : TWNC00294413
Test Conducted
(Ⅰ) Test Result Summary:
Test Item
Unit
Test Method
Result
Silvery
metal
RL
ND
2
882771
2
ND
2
Negative
0.02
Heavy Metal
Cadmium (Cd) content
ppm
Lead (Pb) content
ppm
Mercury (Hg) content
ppm
Chromium VI (Cr6+) content
Remarks:
mg/kg
with
50 cm2
With reference to IEC
62321: 2008, by
microwave digestion and
determined by ICP-OES.
With reference to IEC
62321: 2008, by
microwave digestion and
determined by ICP-OES.
With reference to IEC
62321: 2008, by
microwave digestion and
determined by ICP-OES.
With reference to IEC
62321: 2008, by boiling
water extraction and
determined by UV-Vis
Spectrophotometer.
ppm = parts per million based on weight of tested sample = mg/kg
ND
= Not detected
RL
= Reporting Limit, Quantitation limit of analyte in sample
mg/kg with 50cm2 = milligram per kilogram with 50 square centimeter
Negative = A negative test result indicated positive observation was not
found at the time of Test. When the spot test showed a negative
result, the boiling water extraction procedure shall be used to
verify the result.
Responsibility of Chemist:
Date Sample Received
Test Period
Kevin Liu/ Irene Chiou
: Jan 11, 2013
: Jan 11, 2013 To Jan 16, 2013
*THJ0294413*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C.
全國公證檢驗股份有限公司
11492 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410
Page 2 of 6
Number : TWNC00294413
Test Conducted
(Ⅱ) RoHS Limits:
Restricted Substances
Limits
Cadmium (Cd) content
Lead (Pb) content
Mercury (Hg) content
Chromium VI (Cr6+) content
0.01% (100ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
The above limits were quoted from Annex II of 2011/65/EU for homogeneous material.
*THJ0294413*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C.
全國公證檢驗股份有限公司
11492 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410
Page 3 of 6
Number : TWNC00294413
Test Conducted
(Ⅲ) Measurement Flowchart:
Test For Cd/Pb/Hg/Chromium (VI)
Reference Standard：IEC 62321 edition 1.0:2008
Sampling/grinding or cutting
Cd/Pb/Hg
Cr
6+
Polymers /
Electronics
Metal
For different
material, digest
the sample with
*1
appropriate acid
By spot test
Negative
Confirm the tested
samples are
totally dissolved
Make up with
deionized water
*2
Weigh sample
and add
alkaline
solution
Get 50cm2 sample
Definite temp.
extraction
Boiling water
extraction
Cool and filter
the extract
Analyzed by ICP-OES
Make up with deionized
water and add diphenylcarbazide solution
Analyzed by UV-VIS
*THJ0294413*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C.
全國公證檢驗股份有限公司
11492 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410
Page 4 of 6
Number : TWNC00294413
Test Conducted
Remarks:
*1: List of Appropriate Acid：
Acid Added for Digestion
Material
Polymers
HNO3,HCl,HF,H2O2,H3BO3
Metals
HNO3,HCl,HF
Electronics
HNO3,HCl,H2O2,HBF4
*2: If the result of spot test is positive, Chromium VI would be determined as
detected.
End of Report
This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a
recommendation for any particular course of action. Intertek does not accept a duty of care or any other responsibility to any person other than
the Client in respect of this report and only accepts liability to the Client insofar as is expressly contained in the terms and conditions
governing Intertek's provision of services to you. Intertek makes no warranties or representations either express or implied with respect to this
report save as provided for in those terms and conditions. We have aimed to conduct the Review on a diligent and careful basis and we do not
accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by statute or otherwise, except in
the event of our gross negligence or wilful misconduct.
*THJ0294413*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C.
全國公證檢驗股份有限公司
11492 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410
Page 5 of 6
Number : TWNC00294413
Test Conducted
Photo
*THJ0294413*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C.
全國公證檢驗股份有限公司
11492 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410
Page 6 of 6
Test Report
Applicant:
Number : TWNC00289666
Littelfuse Philippines Inc.
LIMA Technology Center, Lipa City,
Malvar, Batangas
Date
: Dec 13, 2012
Sample Description:
One (1) group of submitted samples said to be :
Part Description
: Epoxy Powder - Green HF
(Old part number is 087341)
Part Number
: 087229-HF
Date Sample Received
: Dec 06, 2012
Date Test Started
: Dec 06, 2012
Test Conducted :
As requested by the applicant, for details please refer to attached pages.
Authorized By:
On Behalf Of Intertek Testing Services
Taiwan Limited
K. Y. Liang
Director
*THJ0289666*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C.
全國公證檢驗股份有限公司
11492 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410
Page 1 of 10
Number : TWNC00289666
Test Conducted
(Ⅰ) Test Result Summary :
Result (ppm)
Green powder
Test Item
Heavy Metal
Cadmium (Cd) content
Lead (Pb) content
Mercury (Hg) content
Chromium VI (Cr6+) content
Polybrominated Biphenyls (PBBs)
Monobrominated Biphenyls (MonoBB)
Dibrominated Biphenyls (DiBB)
Tribrominated Biphenyls (TriBB)
Tetrabrominated Biphenyls (TetraBB)
Pentabrominated Biphenyls (PentaBB)
Hexabrominated Biphenyls (HexaBB)
Heptabrominated Biphenyls (HeptaBB)
Octabrominated Biphenyls (OctaBB)
Nonabrominated Biphenyls (NonaBB)
Decabrominated Biphenyl (DecaBB)
Polybrominated Diphenyl Ethers (PBDEs)
Monobrominated Diphenyl Ethers (MonoBDE)
Dibrominated Diphenyl Ethers (DiBDE)
Tribrominated Diphenyl Ethers (TriBDE)
Tetrabrominated Diphenyl Ethers (TetraBDE)
Pentabrominated Diphenyl Ethers (PentaBDE)
Hexabrominated Diphenyl Ethers (HexaBDE)
Heptabrominated Diphenyl Ethers (HeptaBDE)
Octabrominated Diphenyl Ethers (OctaBDE)
Nonabrominated Diphenyl Ethers (NonaBDE)
Decabrominated Diphenyl Ether (DecaBDE)
Halogen Content
Fluorine (F)
Chlorine (Cl)
Bromine (Br)
Iodine (I)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
323
ND
ND
*THJ0289666*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C.
全國公證檢驗股份有限公司
11492 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410
Page 2 of 10
Number : TWNC00289666
Test Conducted
(Ⅰ) Test Result Summary :
Result (ppm)
Green powder
Test Item
Phthalates
Di(2-ethylhexyl) Phthalate (DEHP)
Dibutyl Phthalate (DBP)
Benzyl Butyl Phthalate (BBP)
Others
Hexabromocyclododecane (HBCDD)
ND
ND
ND
ND
Remarks: ppm = Parts per million based on weight of tested sample = mg/kg
ND = Not detected
Responsibility of Chemist : Irene Chiou / Kevin Liu / Cathy Chen
Date Sample Received
Test Period
: Dec 06, 2012
: Dec 06, 2012 to Dec 11, 2012
(Ⅱ) RoHS Limits:
Restricted Substances
Cadmium (Cd) Content
Lead (Pb) Content
Mercury (Hg) Content
Chromium VI (Cr6+) Content
Polybrominated Biphenyls (PBBs)
Polybrominated Diphenyl Ehters (PBDEs)
Limits
0.01% (100ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
The above limits were quoted from Annex II of 2011/65/EU for homogeneous
material.
*THJ0289666*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C.
全國公證檢驗股份有限公司
11492 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410
Page 3 of 10
Number : TWNC00289666
Test Conducted
(Ⅲ) Test Method:
Test Item
Reporting Limit
Test Method
With reference to IEC 62321
edition 1.0:2008 in clause 8/9/10,
by microwave digestion until the
Cadmium (Cd) content
2 ppm
tested samples are totally
dissolved and determined by ICPOES.
With reference to IEC 62321
edition 1.0:2008 in clause 8/9/10,
by microwave digestion until the
Lead (Pb) content
2 ppm
tested samples are totally
dissolved and determined by ICPOES.
With reference to IEC 62321
edition 1.0:2008 in clause 7, by
microwave digestion until the
Mercury (Hg) content
2 ppm
tested samples are totally
dissolved and determined by ICPOES.
With reference to IEC 62321 edition
Chromium VI (Cr6+)
1.0:2008 in annex C, by alkaline
1 ppm
content
digestion and determined by UV-Vis
spectrophotometer.
With reference to IEC 62321
edition 1.0:2008 in annex A, by
Polybrominated
5 ppm
solvent extraction and determined
Biphenyls (PBBs)
by GC-MS and further HPLC-DAD
confirmation when necessary.
With reference to IEC 62321
edition 1.0:2008 in annex A, by
Polybrominated Diphenyl
5 ppm
solvent extraction and determined
Ethers (PBDEs)
by GC-MS and further HPLC-DAD
confirmation when necessary.
*THJ0289666*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C.
全國公證檢驗股份有限公司
11492 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410
Page 4 of 10
Number : TWNC00289666
Test Conducted
(Ⅲ) Test Method:
Test Item
Test Method
With reference to EN 14582:2007 by
Halogen Content
calorimetric bomb with oxygen and
determined by Ion Chromatograph.
With reference to EN 14372: 2004,
Phthalates
by solvent extraction and
determined by GC-MS.
With reference to USEPA 3540C, by
Hexabromocyclododecane
solvent extraction and determined
(HBCDD)
by GC-MS.
Reporting Limit
50 ppm
50 ppm
10 ppm
Remark: Reporting limit = Quantitation limit of analyte in sample
*THJ0289666*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C.
全國公證檢驗股份有限公司
11492 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410
Page 5 of 10
Number : TWNC00289666
Test Conducted
(Ⅳ) Measurement Flowchart:
Test for Cd/Pb/Hg/Chromium (VI)/PBBS/PBDES Contents
Reference Standard: IEC 62321 edition 1.0:2008
Sample preparation
For non-metal part
For metal part
Take sample and immerse into Aqua Regia, start to strip plating layer
Stop the stripping procedure upon color change completely
Take the Aqua solution as plating component and stripped body as substrate component
PBBs/PBDEs
Weigh sample and
add organic solvent
By Soxhlet
extraction or
Solvent extraction
Concentrate the
extract and make up
with organic
solvent
Cr
6+
Substrate
Cd/Pb/Hg
Weigh sample
and add
alkaline
solution
For different
material, digest
the sample with
*1
appropriate acid
Plating
Cr
6+
By spot test
Definite temp.
extraction
Cool and filter
the extract
Confirm the tested
samples are
totally dissolved
Negative
*2
Get 50cm2 sample
Make up with
deionized water
By boiling water
extraction
Analyzed by ICP-OES
Analyzed by GC-MSD
Make up with deionized
water and add
diphenyl-carbazide
solution
Remarks:
*1: List of Appropriate Acid：
Material
Polymers
Metals
Electronics
Analyzed by UV-VIS
Acid Added for Digestion
HNO3,HCl,HF,H2O2,H3BO3
HNO3,HCl,HF
HNO3,HCl,H2O2,HBF4
*2: If the result of spot test is positive, Chromium VI would be determined as detected.
*THJ0289666*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C.
全國公證檢驗股份有限公司
11492 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410
Page 6 of 10
Number : TWNC00289666
Test Conducted
(Ⅳ) Measurement Flowchart:
Test for Halogen Content
Reference Standard：EN 14582
Sampling/grinding or
cutting
Add absorbent in a
combustion flask &
place weighed sample in
equipment
Fill oxygen into
calorimetric bomb
Ignite then leave the
bomb at room
temperature
Transfer the absorbent
into a volumetric flask
Make up with deionized
water
Analyzed by ion
chromatography
*THJ0289666*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C.
全國公證檢驗股份有限公司
11492 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410
Page 7 of 10
Number : TWNC00289666
Test Conducted
(Ⅳ) Measurement Flowchart:
Test For Phthalates Contents
Reference Method: EN 14372: 2004
Sampling/grinding or
cutting
Weigh sample and add
organic solvent
By solvent extraction
Concentrate the extract
and make up with
organic solvent
Analyzed by GC-MSD
*THJ0289666*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C.
全國公證檢驗股份有限公司
11492 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410
Page 8 of 10
Number : TWNC00289666
Test Conducted
(Ⅳ) Measurement Flowchart:
Test For Hexabromocyclododecane (HBCDD)
Reference Standard：USEPA 3540C
Sampling/grinding or cutting
Weigh sample and add
organic solvent
By soxhlet extraction
Concentrate the extract and
make up with organic solvent
Analyzed by GC-MSD
End of Report
This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a
recommendation for any particular course of action. Intertek does not accept a duty of care or any other responsibility to any person other than
the Client in respect of this report and only accepts liability to the Client insofar as is expressly contained in the terms and conditions
governing Intertek's provision of services to you. Intertek makes no warranties or representations either express or implied with respect to this
report save as provided for in those terms and conditions. We have aimed to conduct the Review on a diligent and careful basis and we do not
accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by statute or otherwise, except in
the event of our gross negligence or wilful misconduct.
*THJ0289666*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C.
全國公證檢驗股份有限公司
11492 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410
Page 9 of 10
Number : TWNC00289666
Test Conducted
Photo
*THJ0289666*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C.
全國公證檢驗股份有限公司
11492 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410
Page 10 of 10