ICPTest_373 pdf

ICP Test Report Certification Packet
Company name :
Littelfuse, Inc.
Product Series:
TR5
Product #:
373xxxxxxx
Issue Date:
July 17, 2012
It is hereby certified by Littelfuse, Inc. that there is neither RoHS (EU Directive 2002/95/EC,
2011/65/EU)-restricted substance nor such use, for materials to be used for unit parts, for
packing/packaging materials, and for additives and the like in the manufacturing processes.
In addition, it is hereby reported to you that the parts and sub-materials, the materials to be used
for unit parts, the packing/packaging materials, and the additives and the like in the manufacturing
processes, are all composed of the following components.
Issued by:
<Global EHS Engineer>
(1) Parts, sub-materials and unit parts
This document covers the TR5 RoHS-Compliant series products manufactured by
Littelfuse, Inc.
< Raw Materials Used
Please see Table 1
(2) The ICP data on all measurable substances
Please see appropriate pages as identifed in Table 1
Remarks:.
Form 585-047 Rev. A
1
2/21/06
Table 1: List of Raw Materials covered by this report
Total Parts
Raw Material Part Number
Raw Material Description
Page(s)
1
2
3
4
5
6
7
8
497xxxx
DRKOXXX
DRCUXXX
DRAGXXX
LOZZ194 (692213)
910-016
867-003
009116
Element – 99% Ni
Element – Nickel Plated Wires
Element – Copper & Copper Cladded
Element – Silver Plated wires
Solder
Plastic Cap
Socket
Ceramic Paper
3-9
10-19
20-29
30-39
40-44
45-53
54-63
64-69
2
Validit
nown
ForQues-ti
PleaseCo
Test Report
No. : CE/2011/84958
l
The following sample(s)was/weresubmitted and id€ntifi€d by/on behalf of the client a6:
SampleDescription
Buyer/OderNo.
Date
SampleReceiving
TestingPeriod
TeEtRoault(a)
Page:1of7
Dale: 201111?,01
POLYFILAG
OBERALLMENDSTMSSE2OA,CH-6300ZUG / SWITZERLAND
Ni99.9
+1357
2011t11t25
201Ih1t2510 201II12t01
Pleasereferto nexlpage(s).
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No.I CE/201'1/84958
Page:2ol7
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POLYFILAG
2OA.CH€3OO
OBERALLMENDSTRASSE
ZUG/ SWITZERLAND
Test R6ult{s)
PARTNAMENo,,1
SILVERCOLOREDMETALWIRE
Tost ltem(8)
tlethod
Unit
(Cd)
Cadmium
mg/Kg With referenceto IEC62321:2008and
perfomedby ICP-AES.
mg/Kg A/ithreferenceto IEC62321: 2008and
cerfomedbv ICP-AESmS/kS Withreference
to IEC62321:2008and
pertormed
by ICP-AES.
and
Withreference
to IEC62321:2008
performedby Boilingwaterexkaction
Method.#
Lead (Pb)
Mercury(Hg)
Hexavalent
Chromium
Cr(Vl)
Sum of PBB6
Monobromobiphenyl
Dibromobiphenyl
Tribrcmobiphenyl
Tetrabromobiphenyl
Pentabromobiohenvl
Hexabromobiphenvl
Heptabromobiphenyl
Oclabromobiphenyl
Nonabromobiphenyl
D€cabromobiohenvl
Sum of PBDE8
Monobromodiohenvl
ether
Dibromodiphenyl
ether
Tribromodiphenyl
ether
MDL
Re8ult
No.1
2
n.d.
2
n.o,
2
n.d.
Negative
5
With referenceto IEC 62321: 2008 and
mg/Kg performed
by GC/MS.
5
5
5
5
5
5
5
n.d.
n.d.
n.d.
n.d.
n.o.
n.d.
n.d.
n.d.
n.d.
n.d.
n.o.
n.d.
5
5
5
n.d.
n.d.
n.d.
Tetrabromodiphenylether
5
5
5
Pentabrcmodiohenvl
ether
Hexabromodiphenyl
ether
HeotabromodiDhenvl
ether
n.d-
n.d.
n.d.
ethgr
Octabromodiphenvl
n.o.
ether
Nonabromodiohenvl
n.d.
5
ether
O€cabromodiphenyl
fililnil*
cmpsiy h,:fr 1 rlt lN'i,rl
rh";;*.,6
**d by,h"c".p,
b.gdrcftcromd dlmm6. iba
-]*d*b'h'inkdc.d"
*
il i
tft
it'rrll
.
n.d.
m.ra(s)radsdst b{ 6pod e^ioi b
iL, "",ar,r;ln'
e mid'onorrsbirv
lpoisb98b bcredsndrrsdoe
. : . l . : 1 1f l r : + i 4 . . , , 1 + e t o r t r e e t r e r r s 6 o a r e e tR
t was<oo
TestReport
No. CE/2011/84958
Page:3 of 7
Dale'.2011112101
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POLYFILAG
OBERALLIVENDSTMSSE
2OA,CH$3OOZUG / SWITZERLAND
Test ltem(s)
Halogen
(F)
Halogen-Fluorine
(CASNo.:14762-94-a)
Halogen-Chlorine
(Cl)
(CASNo.:22537-15-1)
(Br)
Halogen-Bromine
(CASNo.:10097-32-2)
Unit
mslkg
toL
Mothod
Withreference
to BS ENMSAZ2007.
Analysis
waspefoamed
by lC.
Halogenlodine(l)
(CAS No.: 14362-44-8)
Result
No.l
50
n.o.
50
n.d.
50
n.d.
50
n.d.
Note:
'1.mg/kg= ppm; 0.1wt%= 1000ppm
2. n.d.= NotDetecled
3. [rDL = l,ilethod
Detection
Limit
4."-"=NotRegulated
(NoUnit)
5. " = Qualitative
analysis
6. # = a. Positivemeansthepresence
of CrVlonthetestedareas
b. Negativemeansthe abs€nc€of CrVlon the testedareas
jn boiling-water-extraction
Thedetected
concentration
solutionis equalor greaterthan0.02mg/kgwith50cm'
testedareas.
l:i!z;li
i: i.tt'
r 1lr . "1 il i r.' -r:'1itli
nysled ro 6 &israrcod r oG or s
fors]sdrcnciom.1doem.itssub]
conpsii rir
1,.
1.!.ij'l'!4'
3@gbitr€lo&cl€d,ndh'3('ffi
'.1 , r.Li- ri:,
l
Fn?,,'tle6lor)ze
Test Report
No. : CE/2011/84958
Page:4 of 7
Da,e :2011112,01
POLYFILAG
OBERALLMENDSTMSSE2OA.CH.63OO
ZUG / SWITZERLAND
tt][]|l[[[]
]l
1) Thesesamples
weredissolved
totallyby pre-conditioning
methodaccording
to belowflowchart.
( Cf' test methodexcluded)
2) Nameof the personwhomademeasurement:
Climbgreat
Yang
3) Nameof the pe6on in cha.geof measurementr
TroyChang
Cutting
/ Preparation
Aciddigestion
by suitable
acid
depended
ondifierent
sample
material
las belowtable)
Add appropriateamountof
digestion
reagent
Heatto appropriate
tgnpe€tu€ to ex€ct
'1) AlkaliFusion
2) HClto dissolve
ICP.AES
DigestionAcid
S1eel,
copper,aluminum,
solder
Aquaregia,HNOs,HCl,HF,H,O,
Gla6s
HNO3/HF
p€lladium,
Gold,platinum,
ceramic Aquaregia
Silver
HNO.I
Plastic
HCI
HrSOr,Hroa HNOg,
Others
Anyacidlo tobldige6tion
1.:.ati
i;llri
abjed ro.ems 3id cofdtoG rof E
throughfilter
Add diphenyl-carbazide
for
SampleMaterial
c o m o , i rt t - , i . r i r l L l { i I r . , r l , J i : n i i !
Cool,filterdigestate
colordevelopment
measurethe absobance
at 540 nm by UV-VIS
1r.rrlri}ll.
Atenoi sdrawiroh.rn'bloior
'ab't
TestReport
No.:CEl20'11184958
Dale:201111i,01
POLYFILAG
OBERALLMENDSTRASSE
2OA,CH€3OO
ZUG/ SWITZERLAND
Page: 5 of 7
lU[uIl||t
[t|]l
PBB/PBDEanalyticalFLOWCHART
'1) l{anEofthepersonwholrEderEaru.enEnt:RofiEnWong
2) lhmeoftheperson
incharge
of nEasurerEnt
TroyChang
Firsttestingprocess----+
process-- Optionalscreen
process - .>
Confinmtion
Screen
analysis
Safipleei€ction/
So* et rnethod
concenkate/Dilute
Extractedsolution
Filter
Analysisby GC/IMS
c o m o a nl ivi i l r / t r i , r L r i ' r , - r l , 1 i , ! n i l i ) : i r r ' l j d i
l?q{!.\.
.,
r'.rll'trl'
mdbaGpJdu€dexeplnig].wbou
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:r,'
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TestReport
No.: CE/2011/84958
Dale:2011h2/01
Page:6 of 7
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POLYFILAG
OBEMLLMENDSTRASSE2OA,CH-6300
ZUG/ SWITZERLAND
AnaMical flow chart of halogen content
'1) Nafi€ of the oerson who arEderEasurernenl Rita Chen
2) Narneofthe person in charg€ of rEasurerEnt: Troy Chang
Sanplepretreatrnent
/ Separatbn
Weighting
andputting
samplein cell
OrygenBombCombustion
/ Ab€orption
Dilution
lo fixedvolunE
AnalysiswasperfonrEdby lC
c o m p . n yn ; , i r r , l r l , ; ! i ' i l r r j J l l ; ' h
rh s @msnr s 'sred by 6e compa
l,.ljf
,ltirllt
psls)6sbd hb red rcPodanioi bs
i 1 ! . . 1 . " .i , r i ' i j ! .
'ndom^ioroiaidluisdclon $uord
iidbe6pd!€dai6plniu]qho'
'.1 . :: ji
::r,ii{
jl + e6ior)rs !^
r+ $61orre tt
@r a*on
TestReport
No.: CE/2011/84958
Page:7of 7
Dale| 201111201
POLYFILAG
OBERALLMENDSTMSSE2OA.CH.63OO
ZUG / SWITZERLAND
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r Thetestedsample/ part is mafted by an arow if ifs shownon the photo.*
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(u€thod)
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6€*,.8+,t+l,t,;*d,if;rl. / witn
2
ref€ren.e to IEC 62321: 2008 and
perforned by IcP-ArS.
tB / Lead (Pb)
++IFt 6232r.2oo8tt*, r,,(64*E,
A€*,ft+&4}'t *&lttFl. / {i rh
r e l e r e n c e t o l l c 6 2 3 2 r : 2 0 0 8a n d
pe.fo.ned by ICP-AES.
;ft. / Ye.cury(Hsr
dg/kg
++rrx 6232r,2oo8t*. ,r 6/B*t
A€4.&+*4t,tr*d,Ht4l. / {i rb
.eferen.e ro IEC 62321: 2008 and
perfo.ned by ICP-AES.
:r{li}
/ t t e x a v a t e n tc h r o n i u n c r ( v I )
+*rEc 6232rt2008r)*, tt,ht+
/ xith reference io lEc
{tti*xi.
62321: 2008a.d perforbed by
B o iI i n e w a t e . e x t r a c t i o nV e r n o d . #
/ Pe.rluoroocrane
An+H,*6
s u l f o n a t e s ( P F O 6 - A C i d!,e r a l S a l r
'tE,F*tf*d.*xi 4fr.+n&!teE
10
/ {ith reference to US EPA 3540C
1 9 9 6 m e t h o d t o r P F O , SC o n r e n r .
Ahalysis was pe.forned by tClMS.
en+&(J*)
r)
/ PFoA(cAsNo.: 335-6?-
a+Us EPA3540c:l996tt!,
,Xtt
t0
lEEit f *d.*irtafi.+e(At) 5c
/ l 4 i r h r e f e r e n c e t o u s E P A3 5 4 0 c
1 9 9 6 n e r h o d f o r P F O AC o n t e a l .
Analysis nas perfo.hed by LCl S.
coipaiy nrlr,i
tt,.,:-H'i,,1
ir.l/f
,i
i
.tl
llq:t:.
pbG) rad€d rh s les rero( eind
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ELSCHUKOM
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GEWERBESTRASSE
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r|d,t €
+ls
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/
/
-:.-;ASS /
@i A l f i i t /
/
.'';*Sit
:i*#it
s*
(Re6ul t)
No.1
v o n o b r o n o' pbh e n ty
DibroEobiphenyl
T r i b r o n o b ip h e n y l
T€trabfooob
P € nr a b r o m o bp, h e n vI
nill$*
/ H e x a b r o m o bpi h e . y l
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tilt*t&+
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*+rFf 6232r.2oo\lir, tlR,*aE
itd,/€z*d,iFjrl. / rcit! .ererence
to IE€ 6232r: 2008and Perforaed
by rc/MS.
/ sld of PBDEs
-,ASA&.
/ M o n o b . o n o d , D h e nev rl h e r
i-tA$*!t
/ D i b r o n o d i D h e n ' re t h e r
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/ T . i b r o m o dDi h e n v l e t l e r
@A'sEi{
/ T e L r a b r o m o d , D h e hev rt h e r
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/ P e n t a b . o n o dDi h € n v re t h e r
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/ H € x . b r o n o d i p h e . v re r h e .
+;i#X6d
/ H e p t a b . o n o dpi h e n y t e t h e r
,\'i*Sitd
i henvl ether
/ o c t a b r o n o dp
p
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/ N o n a b r o n o d ih e n y l € t h e r
/ D e . , b r o a o d i p h e n ev trh e .
+AS*&
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if
( n ) / B a l o s € n - F l u o r i n (€F ) ( c s
6*
No.: 1.{762-9,t-8)
cl) (cAs
& * ( n ) / H a l o s e . - c n l o r i n( e
N o . : 2 2 5 3 71-5 -1 )
(Br) (cAs
&f (*) / Haroren-Bronine
No.: r0097-32-2)
( 4 ) / H a l o g e n - I o d i n €( l )
6f
:{o.: 14362-44-8)
50
mg/Rg
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to Bs EN
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1 4 5 8 2 : 2 0 0A7n. a l y s i sw a s
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]||1tI|a |||[[ll|t
fiii(Note):
l . m g / k g: p p n ; 0 . l q t % = 1 0 0 0 p p o
? . n . d . : N o r D e t € c t " d( , t . * * )
3 . U D L= M e r h o dD e r € c t i o n L i n i r ( t > * 1 H i t , l E f R f t )
4. - : Not R"s"lared G*4,+tld)
5. .*: Qualirative anatysis (No u"it) A,ErI# (.S(F.ta)
6 . # = a . P o s i t i v € n e a n s t h e p . e s e n c eo f C r V I o n l h e r e s r e d a r e a s
(p" i t i ,. *.,F r{lit E d,{A,rl4i 1!jt )
"
b. N€sative neans the abse.ce of CrVI on rhe tested a.eas
{ Nesat i veA i irl :{ E$ *1A trl:{ 7rll rt)
T h e d e t e . t e d c o n c e n r r a t i o hi . h o i l i n g - v z r e r - e x t . a c r i o ns o t u t i o n i s e q u a l o r
ar€atef than0.02 nslka,ith
50 cn: tesr€d areas. / AA,iitl,{>o.02
ns/ks wjth S0 cnz (rested areas)
?. **.t"ii,rliite*A+"=f,./.**EAinl,"lt,*[+f6trieAxj:t***.Tjt*.4+lEr{+_+iq6{1+!.
(The sanples was/{ere analyzed on hehalr or the apprica!t
r e s u l t s w a s / w e r €o n L y g i v e D a s r h € i n t o r n a l i t y v a l ! e . )
Pm4*it*.(Retetence
as niring
sanple in one restihg.
The above
InlorDation) | !A+ 2oo6/r22tvE(Directi,e 2006/122lEc)
(1) l*1r,t{arrr.,ittrisr{&n,r!st*ttf {.ae,Erir}etr*.a++d.i,ao.
005%.
(May not be placed on the narket or !sed as a substance or constituent
€qual to or Iigher than 0.005 % 6y nass.)
of trepararrons
(2)t*4trx4rrfli+fr&rai+d.s4.A,%{.4#i+:1p**4}an#*,,4dpFos-tr.4x!-}*6}a&rEr6i€,r.it4pFos€!
,iA+'ild,i,t!o.1%, n,Ar$"s*.*{UtS.#rf , j' *prcsirfi*& lt f A9S:i[d.)i,Arugr.z.
(Maynot be placed on the marker in seni-linished producls o. arricles, or parrs
rhereof, if the
c o n c e n t r a t i o n o f P F o s i s e q l a l t o o r h i g h e r t t a n 0 . 1 % b v n a s s c a l c u r a t e d w i r h r e f e r € n c e r o t h e m a s so f
s t r u c t u r a l l y o r n i c r o s t r u c t u r a l l y d i s t i n c t p a . t s t t r a t c o n r a i r P F O So r , f o r t € x t i l e s o r o t t e . c o a r e d
natefials,
if the anornt of PFIS is equal io or highe. rhan ljrgln: of the coated naterial.)
cmcant i:)
I i,
:!-ll i,r.l,i.ll,n
lt!tr:i.
l
,.t!
ThAdoorcn6ss€dbyhe.omp,.,9qedbb6'rc.a|codioisols
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Test Report
i t 4 ( N " . ) , cE/20t2/taa3?
$\Date) : 2012/0r/r\
F*(pzse)
ET.SCHUXOM
ELEKTROSCHUTZKOMPONENTENBAU
GMBH
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8?, D-98669 WII-SDORF, GBMA\Y
t[] [ttt]
*[S4it(styr€/rten No.)
( D - 1 ) 1 0 1- - 2 2 8 . 0 ' - t u n g s t e n- t i n n e d E i . e t V ,S n
( D - 2) r 0 1 . 0 1 2 6 . -0 qr, Ni
tungsten purity, nickel pLatedrire
( D - 3 ) r 0 1 . 0 1 2 t . 0- _
corp€f - nickel {1 anoy (cotrsranran) sire
cuNi.tl
( D - 4 )r 0 r . 0 1 2 4 . 0 - - copp€r-!ickel zinc-attoy
vire (NSl8) - CuNi18Zn20
( D - 5 )1 0 r . 0 1 2 7 . 0 - - -_
copper - nickel -alLoy sire
cuNi 2
( D - 6 )l 0 l . 0 1 2 90. - - - copper - nickel -alloy
rire
ClNi 12
( D - 7 )1 0 1 . 0 1 7 4 .- 0 - coppe. - nrcket -a]]oy
wire
CuNi 6
( D - 8 )1 0 1 . 0 r 7 5 . 0 - copper - nickel -attoy
wire
CuNi 22
( D - 9 )r 0 r . 0 r 7 8 . 0- - - iron - nickel -attoy sire
FeNi36(rivar)
( D - 1 0 r) 0 r . 0 1 ? 5 . 0- - - copper - nanganese- nickel -alloy
vire
CuMnt2Ni
compada
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GMBH
GEWERBESTMSSE
87, D 98669 VEII.SDoRF, GIRUANry
1l
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2) i.Jt{.^ I : it41* / Nameof the personwrD mademeasu€menl:Ctimbs@tyang
3) jrl{ I ir'. : *4rr+ / Narneortle p€€on in .hargeof medurernern:T.oychang
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Microuave
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Acd
r*, I{*, I.n, n*.*, tnn /
S€el.copp€r,
aluminum,
solder
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r/* ,f *, a l,ra/..,t$.,t
,4*'.sAkAs0 nmr!'{
4i{ q{.'t {&, i* / H:so.,H,o,,HNotr.
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/ any acid1ototaldigBtion
,!^l+ttrt4taa*
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4re.! R* / HNO,1-iF
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lhrough
fner
i
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.
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TestReport
*(Date) : 2012101/11 q*(p,s")
ETSCHUKOM
ELE(TROSCHUI'ZXONPONENTENBAU
GVBH
CEIERBESTRASSE
87, D-98669 VEILSDORF,GERVJ}.IY
t *d*/
||ll[tutflru ||[rl
r *4+&+&jft,'E||
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anatyticat
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r
,Q;{ A t \ r tACq / Nameofthe peEon rl cha€e ofmeasurcmentT.oy Cha;g
t rtrl3ttr+ / FirsttBling proc6s ------t
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pro@ss-. -.t
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I
I
t 7 0 t L 0
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{ltr;++J
soxhrer
method*{+qqi
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I
concentrate/Dilute
Extractedsotution
+clRri*/it6
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Analysis
byGC/[4S
/ {rtB&fi.{*d.+tr
p31stbsrad rh6 rad GPon €f ml be
rysub]dlobGe^e6cdidsonsds
l:,]'i+..:ir&l0rl2sr
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lE6(No.) : cEl2012lr0837 E * ( D a t e ) : 2 0 1 2 l o r / 1 1 F * ( p , e " )
EI,SCHU(OM ELE(IROSCHIITZKOMPONENTEN&{U
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87,
D 98669 \'EI[SDORF,
tt+fi*#f
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chartof hatogon
content
I
jllt[LF : *.S,* /Nameoftheperson
whomademeasurement
RitaChen
I
jllt\, F l-l. : tits4 / Nameof thepeFonin chargeof measurcment:
TroyChang
e+8fr16,ifr t
Analysis
wasperformed
by lC
||||l[![]|ll
fi{s,+E+
Test Report
!t4(No.)
: cD/2012l10837
ES(Date) : 2012l01/11 Ftk(p,s") : 9 of to
ELSCHU(OM
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87, D-98669 T'EILSDORF,CER\LA\Y
lt]
*Ji+n(+ft*,af /
Analytical flow chart of Soxhletextraction(LC/ltS) procedure
r
r
;{:t/-F : .-i-!9d / Narneof the personwhomademeasurement:
Rofian Wong .
x{fi I l',,i' : ,i,*R / Nameof thepersonin chargeof measurement:
TroyChang
( d,t E: A;.+ti,4rUAE+&(*) ' *&:4t{bA&
Test ltems: PFO9PFOA. Benzotriazole)
*4
comp.i,fj: irl,!iii
rrr:rl,ltrrl,i .ai
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1,,.,lrilrtt.
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9: i:'ii] ,,* + 86lor)re
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|||lIttt
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lE6(No.) : CEl2012lr0S37 E * ( D a r e ) : 2 0 r 2 l 0 1 / 1 1 F j k ( p a s e ) : r 0 o f l 0
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10837
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Efi(Date):2012l0r/11 q l t ( P a s e ) : 1 o f 1 0
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GMBH
GEIERBESTIAS,SE
87, D-98669 \aEILSDOnr, CrnUrry
t(Ttjd,&sfi &*r,t&,
ide!tified
-eAfP +*trE*P **iT
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D€s-ipt ion)
*.gZt*(sanple
iS.S4*,(StyLe/Iten No.)
,FE g(coontry of orisin)
&+ A S (s,'pl. Receivins Date)
,rli{S Fl(res t ins Pe.iod)
irli*
rr|||l|rl[[ttf,]l!
jF(rest Resurts)
,
(Th€ fol Iori!t
6aDples eas/rere
6uboi t t€d and
as) :
COPPERCLAD & COPPERNLTO] WTRIS
(PLEASE
RFERTo PAGE5)
fi++XsA.
(GER
A},Y)
ftg
20L2/0L/04
2 0 L 20/L/ 0 1 ' , l O2 n r 2 / O Ir r/
;t4.T-E
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i *frreir 'i*lj:r
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Test Report
F*.(Pace) : z or to
i||lr[t
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87, D.98669 VEILSDORF,GEL\LAIY
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(PAlr Nr'uE) No.l :
'e,i fiaee&,a&
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$rRE
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THEPLATINGL{YM) (T6 TYPES)
)
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( R e s u lt )
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No.l
2
reference to IEC 62321: 2008 and
perlorned by ICP-AIS.
,5
+*rDt 6232L'2oo8ttA, ,r(&,6F
r
A{*AA44I{*&A:.1.
r e f e r € n c € t o I E C 6 2 3 2 r : 2 0 0 8"i,n
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perforf,ed by ICP-nnS.
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/ {i ih
+€tF+*4i{r*'ft*xl.
*. / vercury (Es)
2
reference to IEc 62321: 2008 and
pe.forn€d by ICP-A!S.
++tgc 6232r.2oo9fit, r/)k,Y"4
7i'llr& / nexavalentchroniun cr(vI)
4.i*lt;Fl. / rith ref€rence to IEc
62321: ?008and perfor0€d by
BoiI inE water extraction Merhod,#
An+R&*
sulfonat€s
4+us EPA35.10C,1996ti4, 'Xr{
/ Perrluoroocta.e
h.t 44f, ;*A,if :rlAfl.*R tt&+E.
( P F O S - A ci d , M e r a l S a l t
/ Iilh referen.e 16 us EPA 3540C:
1 9 9 6 n e t h o d f o r P F o SC o n t e n t .
Analysis sas perforned by LCINS,
ift+d.(14)
/ PFoA(cAsNo.: 33s-6?-
4+US EPA35a0c:l996tii,
,)(t{
4fr.+c(J*)n&
iEafi J{:*.t*,tairl
1)
/ s i t h r e f e r e n c e t o U S E P A3 5 . { 0 c
1 9 9 6n e t h o d f o r P F O AC o n t e n t .
Analysis vas perforned by tClMS.
c o m o a n+vj l 1 / n r l , r r , f ' | , 1 , i : 1 f i l r ,
r.I ltri{::
ny ssbled io b GeneG cond[dns d se
on|yandw$|.lhelmcolc6i|sns
bi€d rh s €d €Podennd e
PrsG)
- _',1 r!t!,.!'
s*
t*{t j{
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l0
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,fl.d,+E+
Test Report
lE*r(No-) : CE/2012/108s6
ES(Dare) : 2012101/11 F&(pase)
ELSCHUKOIELEKTROGCHUTZLOVPoNU,ITINtsAU
G[tsH
GEWERBESTMSSE
8?, D-98669 VEIISDoRF,CERMANry
jnd,{ E
+'fs
I|lt|||||N ||[l
j{nt*
(Unit)
t ilt**#
-iAlfi;F
:AS*
€;ESX
t;9#E
'i;A#*.
/ Sut of PBBS
/ M o r o b r o n o bpih e n y l
/ D i b r o n o b ir h e n y r
/ T ri b r o n o b
rphcnyl
/ Tetrabronobiphenyl
/ P € n t a b ! o m o bDi h e n Iv
/ H e x a b ! o m o b i p h eLn y
-Lill$*
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e
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r
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o
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/ Monobronod
/ D i b r o m o d i p h e n€y(Lh € .
:i*d86d
/ T r i b r o n o d i o h e n vI e r h e r
qAdSEt
/ T e r r a b r o n o d , p h € neytlh € r
/ P e n t a b r o n o d i D n e r v€l t h € r
A;&l$ri6{
^;&ISliAC
t,Flfi;.a*
^*lSX.6t
/ octab.onod
/ Nodabfonod
**#XEn
/ o"catronoa
5
5
5
5
5
5
5
5
5
5
5
/ H e x a b r o n o d io b e n v l e t h e r
/ Heolab.ooodi lh€nvl ethe.
,L*SXAt
air
to IEC 62321. 2008a,d p€.lorhed
by GC/MS.
/ suo of PBDES
t ttfltlltrfr
No.l
5
5
5
5
5
5
5
5
^tA#f
-_A#Xi4
$*
(Resul t )
/ Halo..n
(fl.) / Halose!_Fluori.e
6*
N o .: 1 4 7 6 2 - 9 4 - 8 )
(F) (cAs
(fi") / Haloser-chlorine (cl) (c'{s
6*
!o.: 22537-15-1)
(;i) / Halos€.-Bronine(Br) (cAs
&l
N o . : 1 0 0 9 73 2 2 )
(4t) / Halogen-lodin€(l)
6*
50
r,lrt+,gff
4+Bs ENr4582:2007,
ag/(t
50
/ I[ith .efe.ence io Bs EN
&r)fi.
1 4 5 8 |22 0 0 ? .A n a l y s i s{ a s
(cAs
50
No.: 14362-44-8)
c o m D a n; "v, r 1 r i | l , f _ a { l , r . r r , , Jnt i j l r : r ] . 2 j i
ii!.fli,
r . 1rr rrlJLl.
r i r : ' I l l l ) . : l : , i l t . , i + s 6 i o n r * r 7 e r + s 6 o r ) r e e r rv t u { r @ h
t
n{'d,#+
TestReport
frq(No-) : cE/201?/10836 g i ! ( D a i e ) : 2 0 r 2 l o r l r l F * . ( P a r e ) ; 4 o f l o
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8?, D-98669 VEIT,SDoRF,GERMANry
lllIrIlrl||||u[tl|l
fiii(Note):
1. nglkg = ppni 0.lwt% = 100oppn
z. n.d. = Nor D"t.cr.d (*.ifA)
3 . M D L= M e t t r o dD € r e c t i o n L i n i r ( t t i l F x l E f B l & )
' : Nor Resulated (**ei'.ii.)
,t.
.
.
=
5.
Qualitaiive analysis (No u.ir) €,I4r)tt(*+dn)
6, # =
a. Posjlive
(Posi t i
b,
"e*. +;r{ 3t E &,1i,rl t{ ,r.ll r8)
Negative
(Nesa
ti
Eeais the Fresence of CrVI on rhe tested areas
neans the
absence of
C.VI
on rhe
iesied
areas
"€e + iri:;l E ii. i1A trlt{ '\fiJ} )
The d€tected concentration in boiling-water-ext.action solutibn is equal or sreate. th:n 0.02 bglkg with
50 cm, tested areas. / lii)*i{,i,8=0.02
malks sith 50 cm, (tested areas)
7. *l s 0t,nl?i,t.
A+ + if ^*,i,E 6tFl:lt' *r+ f ftliEe;il*,3*
+rri.a4f&r!
+-titr 616s.
(The satuples sas/{€re anaiyzed on b e h a l f o f l h e a f p l i c a n t a s n i x i n s s a m p l €i n o n e t e s t i n g . T h € a b o v e
r e s u l i s w a s / w e r eo n l y g i v e n a s t h e i n f o r n a l i l y v a l u € . )
PrOs++itfi.(Refer."ce Inforiatior)
(Directive 2006/122lEc)
. lE+ 2006/122/FL
(1) :**r( 6irE,ai4-Ld..n,s :ar+*lrf d.Ec.Er\rl**r*a++{.i'i+o. 00s%.
(Maynot be placed on ihe oarket or used as a srbstanceor constituent of preparations in a €onc€ntratioi
€qu,l io or !igher lhan 0.005 % by nass.)
(2,t hY4q&*fr*rii+d.sd.fi"%4.*#r{+r 1kr5e+rExfirt4ApFosltti€,*+6-La&.rElt€_LitSPFlsg&
i.lA+,Ad.ri^0.1%,d,1&& A,t+!-&6,*,9,t'*Isos.arts't f + Al+Ad.d,Arus/".
(May.ot be placed on th€ narke! in seni finished products or a.ticles, or paris rh€reof, if the
concentration of PIOS is equal to or hiab€r than 0.1 % by nass calculated *ith r€ference to the nass of
s t r u c t u . a l l y o . n i c r o s t r u c t u r a 1 Ly d i s t i n c t p a r r s r h a t c o n t a i n P F 0 6 o r , f o ! t € x t i l e s o r o t h e . c o a t e d
naterials,
i f t b e a m o u n t o t P F O Si s e q u a l t o o r h i s h c r t h a n l U s / n : o f i h € c o a i e d n a t e r i a l . )
c o m o a n4v , r / t r , , t - i ' : , 1 " : i : ! n l r r i
, I
l6m..1.Fi
r r _ i ir ? r r 1 , , r
;:r:*r..:i+s6Fanerrre,'s
nl'd,+E+
TestReport
t A , 4 ( N " . ) c, E / 2 0 L 2 / t A A 3 6
E&(Date):20I2l0r/11
FjR(P:se):5ofro
tl|
ELSCIIUKON
ELEKTROSCHUVKO]{PONENTEN&CU
CMBH
CMERBESTi.ASSE
8?, D-98669 WII,SDORF, GER\{A\Y
t e o N o .)
*.S4ft(styre/l
( c - 1 ) 1 0 1 . 0 1 7 7 .o ( c - 2 ) 1 0 1 _0 1 8 3 . 0 ( c - 3 ) 1 0 1 . 0 1 ? 2 .0 ( c - 4 )r 0 r . 0 r 8 r . 0
( c - 5 ) 1 0 1 . 0 1 3 2 -. ( c - 6 ) 1 0 1 . 0 1 3 1 . 0(c-?) 101.01?1.0
( c - 8 ) 1 0 1 . 0 1 3 s -. ( c - 9 ) r 0 1 . 0 1 5 7 .0 ( c - 1 0 ) 1 0 1 . 0 1 3 6 -. (c-11) 101-- 064. ( c - r 2 ) 1 0 1 . 0 1 6 6 -. ( c - 1 3 ) 1 0 1 . 0 1 s 8 -. ( c - 1 4 ) 1 0 1 . 0 1 6 1 -. ( c - 1 5 ) 1 0 1 . 0 1 5 5O
.
( c - 1 6 ) 1 0 1 . 0 1 2 8 0. -
cdpaiy:
copper tin alloy wire CuSn6
copper cLad{ire - Elcon 30
coppcr cLad steel wire - Elcon F
copper clad iron-nick€l-alloy si.e
Elcon D
silve. copper alloy wire
AgC!50
silver copper alLoy wi.e Agcugo
.opper vire
Cu99.9%
silver copper alloy wire Ag72Cu28
copper-zinc-alloy
wire C u 8 0Z n 2 0
.il'er copnerallo/ ri-F A g 4 5 C L 5 5( A g a L 5 5 )
-
copper plared, brass plared sp.ing-steel wire silver copperalloy sire
A 8 c u 7 0( E l c u 7 0 )
silv€r coppe. alloy vire
ANu80 (Elcu8o)
oxyaenfr€€ copper vire
OF Cu
copper-,in.-alloy
vi.e
C!70 Zn30 (Vs 70)
tungsten Furiry uire
lV
1 1lt r-ll i,,r i;.llilr'i 1!.I11 1ir..l:
DyabPdlob6ela|cofuldi3bis
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tN ntlnl
:r.,.,,rift,y.
-:,r r:r:*!t..:i1+s60,r,,errt
FST, Cu -%
scs
,n{-d,*E+
Test Report
!tr6(No.) : cE/2012l108s6 E S ( D a t e ) : 2 0 1 2 l 0 1 / 1 1 q r & . ( P a s e ) : 6 o f 1 0
||l| [ttn]t
DI-SCHLTI(OI\4
ELEKTRO6CHUTZI<OIIR}NENTEI{BAU
OVBH
GEWE&BESTRASSE
87. D 98669 VEII^SDoRF,CEL\IAI\ry
r) *{itrTil,i{!Ezi*?+
' fsEe}:tsfl.(
trliJ$)}lilttilArl. ) / TtEsesamde ree
dissolv€dlotallyby pE{onditioningmelhodaccording
!o belowiow chan. ( cP bst methodexcluded)
2) jd :l\',,.I : t} 4.L / N6meorthe personwhomademeasuremsntr
Climbg€atYang
3) ,Ilit I t ^ . t[4* / Nam€of the personin chaqe of measuRent Trry Chans
tri{ ' {I*i*.s /Cutins.Pl€ aBlion
idnt*stl
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Measu€menl
f.f,1. Fl*e $tl f ,6,x,af 6lriG lifi lt (:{'T,i.
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direren!ssmde maiedal(as belowlable)
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Micro'i/avedigeslion wilh HNOy'HCUHF
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/ HCllo di$ol',€
irlLAitllt
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Acd
.t,t, diaa,taa, &,*.at,,tl"t /
/add
'tX,l/.-q t +,k).ltr't
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,! \1t1T.{4:
i
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rrii ).?rl;r
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?,:|6tl
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*
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Test Report
ftt6(No.) : cE/2012l10836 E S ( D u t " ) , 2 o l 2 l 0 1 / 1 1 F * . ( p a s e ) : z o r r 0
ET,SCIIUKOMELEK'|RGSCHUTZKOMPONENTENMU
GMBq
GEWERBESTTSSE 87. D-98669 \,'EII-SDOXF. GERV,q\Y
t*t*/
t i**tl,*+&fiaf
tl|
/ PBB/PBDE
FLOWCHART
anaryticat
. ,|l:{,,i.F I 44ry / Nameoltheperson$ho mademeasurement
RomanWong
. t'l*i F 1,,- : 'f,+q / Nameof lhep€rconin cnaeeof measufement
T'oyChang
t\,ilil{rr
/ FiFltsiing prccess----------.f
...----.
prcc€ss
*f.E&&44 / Oplionalscrcen
- . -.>
4t{AF /Cmfimalion
Dro.ess
.rrrrrtrrrrrrrrr..r
Scre€nanalysis
/ tSriif
Sampleexlraolion+l&+S.l
Soxhlet
merhodi *.+tdi*
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Enracledsolulion
+Rn,ilB/ri#
Filter/ +S.i{€,8
Analysis
byGc/lvfs/ RleE&f.'*&.+&
*+r**
c o m p a ndy
rli ,l,l L i'!
,.'r.l:lirili
r:.r
r
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pe{3)€jed rh s r€d GFn €i.or be
.rr
.r!l!!!.
tI || flttt]l
,41'd,*E+
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fi,6(r".),
CE/2012/1aa36 E r q ( D a r e: ,2 0 1 2 / 0 r / r r F i H . t p a B :e8) o r t 0
EISCIIUKOM
ELEKTROGCHUTZI{OIIPONENTENB,{U
GMBH
GEtrERBESTRASSE
8?. D-98669 WII.SDORF. CXRMANry
f f'+fit€f,
t
I
trffLntI| Ilrtfll
/ Analyticalflou,chartof halogencontent
,!13t,\F : ttg* / Nameofthepersonwhomademeesurement:
RitaChen
tr!3t,€ l,\ : 'Fr$4 / Nameof thepersonin chargeof measu€ment:
TroyChang
*a & frFr}+trI
Analysiswasperformedby lC
compair:iiritt!
j!-ll'ilrl
i|i,itrr.
i..liii
l}!.ri.
prsG)rared rh s€dr4o^6.^d
r.r.|rllii.r
spoisbtV €roGc
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Test Report
€i6(No. ) : CE/20t2lr0836
AS(Date):2012l01/ll
FlR(Pase)ieofto
rtl |lll
ET-SCHUI{OM
ELEI{TROSCHUTZ(OMPONENTENMU
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87. D 98669 VEILSDORF.GE&\!AIY
*{+F}frfi4cf
/
Analyticalflow chartof So)drletextraction(LC/MS)procedure
r
I
ic|l:{ -F: Ai4# / Nameof theperconwhomademeasurement
RomanWong
tll*,Atl.:
tiBF / Nameof thepersonin chargeof measurement:Trcy
Chang
( ls'{ E: AE+H,*.t/An+*(s)' *it:4i{E6&
Te6tltems: PFOS/PFOA' Benzotriazolo)
Itfr i Data
c o m p a n y . r 1. , l 1 l L r i : , r l , 1 1 i: | r r l .
.t
i lt{.rl
prsG) rar6d rh s led @od 6ind
!t ,.r .rrtrl.
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Test Report
: CE/2012l10836
Es(Date) , 2012l01/11F{(page)
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87, D-98669'IIEIISDORF,CE!.T{Ar\Y
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by ICP-,ES.
terforaed
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: 2008t&,'r€E*4
++ lEx.62321
+€ {/F + **t rt ;* d,*birl. / $i r1'
reference to IEC 62321: ?008 and
perforned by tCP-r{XS,
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++ \F: 62321.2OO8li*, t)a.,fr
*+
/ with fefe.€n€e ro IEc
RliAtll.
6 2 3 2 1 . 2 i A B a n d p e r f o r m e db y
B o iI i n s s a t e r e x t . a c t i o n M € t h o d . #
}fr.+B**
sulfonates
/ Perrruo.oocrane
nglka
(PF!S-Acid. Uetal salt
t+us
EPA3540C:1996tii, 'lil
IO
iE,9*f1[-r*&}f,4
an+,t,4*69'
/ t r i t h r e f e r e n c e t o u s E P A3 5 4 0 c
1 9 9 6n € t h o d f o r P F o SC o . l e . l .
Analysis was perlorned by tClMS.
an+6.(J+) / PFoA(cAsNo.: 3356?
r)
++US EPA3540c:l996tt!,
,Xtl
&Eif 1{r*{,*fl an+d(n) }f
/ w i t h r e f e t e n c € t o U S E P A3 5 4 0 C
1 9 9 6e e t h o d f o r P F O AC o n t e n t .
Analysis was perfofned by rc/MS.
i j :i :r l , ]. r : . a i i . ; ; r t i ]
c o n o a .t y r r , : 1 r 1 , ri!' _, r r l - J n
iy $qd rob cene6cdidroc d s
onlysndwibinlh.imlsoic€nls'ns
pelsr reded rhE bd rcpod Enid be
1, . r, rjr,!*.
l0
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No,1
rfla+E+
ft4(No.) : cE/20I2lr0835
Test Report
E J q ( D a r :e2)0 t 2 l 0 t
E * . t e , B " ,/ 3 . r
ELSCHUKOM
ELEKTROSCHUTZKONPONENTENBAU
CMBq
GMERBESTRASSE
87, D-98669 !'EIISDORF, GERMAIr\
d{t
E
lll
+4o
,{fi,t*
( U n it )
( R e s u1 t )
(IDL)
No.l
/ uonobronobiphenyt
:;Ad*
qA#tri
/ Dib.onobipltenyl
/ T r i b r o n o b ip h e n y l
/ T e t r a b r 6 n o bLo h e n v l
I*#Xi
/ P e n t a b r o n o br o h e n ! I
/ Hexabronobiphenyl
?!4$it
+iASf
/ H e p r a b . o n o bpi h e . y 1
^itrfi A / o.rabronobipheDyl
/ Nonabromobipheryt
4)qS*
/ D e c a b r o n o bpih e n y t
+;ASf
*trEc
/ suo of PBDES
t*AS.t&t"
-;ASf!{
/ M o n o b r o n o dD
i hehvl ether
=-r[#*e
:;A#+a{
/ D i b r o n o d ip h e n y l e t h e r
/ ' l r i b r o d o d i p } e n v l er h e .
B,*SiFa*
/ Tet ra6.onodi phe.vl erher
i;*Sxad
'r*S*a*
/ P e . r a b r o m o dDi h € " v l e t h e r
/ H e a a b r o n o dpih e r v t e r h e r
-k;A#Xa{
/ H e p t a b r o m o d iD h € n v l e t h e r
,\;*SXa{
/ o c r a b r o n o dD
i he.vl ether
,L;i#*e
i henvl etler
i N o n a b r o m o dD
+&#ii4
/ D € c a b r o n o d i D h e n velt h e r
623211
zoo$iiF, ,tfu|aE
+8dlf :*d,&jrl. / $ith rererence
ro IEC 62321:?008 and perforned
by rc/MS.
5
5
5
5
5
5
5
5
5
5
5
5
5
5
a* / s"l.s."
(fr.) / Halogen-Floo.ine(F) (c{s
6*
No.: 14?6?_94-8)
(5.) / Haloeen-chlo.ine (cl) (cAs
6*
! o . : 2 2 5 3 71- 5 - r )
& * ( * ) / H a l o r e n - B r o n i n e( B r ) ( c A S
l{o.: 10097-32-2)
50
ng/18
vx&+8fr
ltBs vt r4s82:2007,
50
/ sirh reference to Bs EN
{r}*t.
I 4 5 8 2 r 2 0 0 7A. n a l y si s v a s
50
(I) (cAS
6fr (dU / Halocen-lodine
No.: 14362-44-8)
conFiv;"
r 1 llu.,[r'r,
l: i/irr.r I i.tl
lt!,lr'i
oyglbredbb6ai.'alcondloisds
50
hrr.(s) rssbd rh s resr €pon ennd
lLr Lt[]!.
iq
3pdJb't}6lobc€da^dhsdocu
b
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,illt,rl
EIE{I
/ su! of PBtss
t*t**'ts
:14#*
:i*#f'
(Iethod)
ro
l ]tl|
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,F{a+E+
ff6(No.)
Test Report
: CE/2012l10835
aBlJzr.)
. 20L2/ot/71 Ftk(pare) : 1 of r0
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87, D,98669 VEITSDORF.GERVIIY
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fiii(N.t.):
l . m g l k g: p p m ;0 . | w t %= l o o o p p n
2 _ n _ d . = N o r D e t e c t e d( * . t A r r )
3 - M D L: M e t l o d D e t e c t i o n L i r i i ( r l t l A ; { t s 1 8 1 6 )
4. '- = Not R"sulated (Sli,+&.6)
5 . r ' = Q u a t i t a t i v e a n a L y s i s( N o u n i t ) _ € , B r ) * f ( * + & )
6. #:
a . P o s i t i v e b e a ! s t l e p . e s e n c eo f C r V t o n t h e r € s t e d a r e a s
(po s i t i ve *,F rq,lit E q.tF jq r{ ,r{l rS)
b . N e g a t i v e n e a n s t h e a b s e n c eo f C i V I o n r h € r e s t e d a . e a s
( Nesat i ve i nr::tl*, E 4 t.tA ).14 'r1l1g )
T h e d e t e c t e dc o h c e n r r a t i o ni n b o i l ] n a - e a r € r - e x r r a c t i o sno l u t i o n i s € q u a l o r g r € a r e r t h a b 0 . 0 2
m A l k gw i t h
50 cn: tested ar.a". / li6;i{XA>0.02
nslka *iih 50 cm, (tested
z. tte.i,tlS{r.'Af
;F./.**isArxl:{,, *E+titi,sA,tt:ri}:+.Tftt 4 +1Erll+-ttlt aiAE.
(The sanples sas/were analyzed on behalf of the atfricant
! e s u l t s w a s / w e r eo n l y g i v e n a s r t e i n f o . n a t i t y v a l u e , )
PFos++*d,(R"f
Inf orlation)'
"'.o"€
(1) riitrrf rTfi.'|tsld.&n,r+r+4rrf,
as mixing sanpre in one resrine.
The above
!A+ 2oo6trzztEa (Di rect iae 2006/t2ztw)
d.Ee,Ed,rlE*tla+,i6d.n,+0.
005%.
(May not be placed on the market o. used as a sDbstance o. consrituent
€qual io or nigh€r than 0.005 % by nass.)
of prepararrons
(2rtit{ttX4n&*fi&}.ei+d."%d.6s{.*{r1+;1!i*€1+}aX*Jt+ApFosi.4t?J*fi}.e.t&r€t6€};l4pFosEE
,i.&+,i!d.i,ifo.r%,6*r&€d.4{tti.4rf. {,RprrsaAt*f + 6E*;Ad.Ji;Aruc/.,.
(Maynot be placed on ihe na.k€t in seni-linisned prodocts or articles, or pa.ts rhereof, if
ure
c o n c e n t . a t i o n o f P F O Si s e q u a t r o o r h i g h e . t h a n 0 . 1 % b y n a s s c a l c ! l a t e d s i t h r e f e r e n c e t o t l e n a s s o f
s t . u c t u r a l i y o . f r i c . o s t r u c r u r a l l y d i s r i n . r p a r r s t ! a i c o n t a i n P F o . so r , f o . r e x r i t e s o r o t h e . c o a r e d
naterials,
if thc anoun! of PFOSis equal to o. hiahcr than Ug/nr of thc coated nateriat.)
c o m p a ityr : ; r , r ; : i r l , , ; - f i t . r l J r . n i r r , . r , , t i i
Ltlttr
1i., r".l,r!/,)!
ont andub'n ihsh b orc en'3,ns
-.4ttr
- ! . ! , , : r r i r l l i - I. c i e o a F i
-:.r ;::rlnti,,;i+46iDr,ssr7
l
,rla#+
TestReport
ft,q(No.) : cE/20r2lr0835
E S ( D a t e ) : 2 0 1 2 1 0 1 / 1 1F * . ( p a s € ) : 5 o r l 0
EI-SCHIXOi,I
ELEKTRO€CHUIZKNTPONENTENMU
CVBH
GEIIERBESTInSSE
87, D 98669 IEIT,SDORF.GERILUY
tl&4!t(styl./I
[t[t
t.' N".)
(B-1) 101. 014
-silver
plated coFpe.{tre-Cu. Ag - - %
(B-2) 101. 0131. - - - - -pure silve. sire-Ag l()()()
( B - 3 ) 1 0 1 . 0 1 2 3 . 0- - - - s i l v e r
platcd purest nickct vire-Ni99.98%. AgI%
-silve.-copper alloy plated cotpe. clad vire-Elcon D,
(B-4) 10r,0182.0 - -silver
(B 5) 101.0120.0
p l a t e d c o n s t a n t a nw i i € - C u N i 4 4 , A A S %
( B - 6 ) 1 0 1 . 0 1 5 1 . 0- - - - c o p p e r - n i c k e t 4 4 a l l o y s v e r p l a r e d s i . e - c u N i 4 4 ,
c o D o a n tv l r I t ! . , r - N ' | , r " l : l , i l l l i
:. ! 1 1:;!1,1\
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Test Report
f i { 5 ( N o . ) : C E l 2 0 1 2 l l o s 3 s E S ( D a r e ): 2 o t z l 0 r / t t F # ( p a s € ) :
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3) ir'13{I i ^ : tl4* / Nameof the pe6on in chargeormeasu€m€nlrTroychans
tr*. {rtt*s
/curing. p€galaton
iqr{.&,cf ! / sdde MeasuEmenl
&lf;F n l*'.g6tt{ f, 6 }xn!trai&it,tirt /LoeTt
4rt/!inlt n.i'la{&,aib /
4,;) /Acid dig€slion by suitabte acid dependedon
dtrerenlsahdemaledat{asbetowiable)
MiorcMve digestion with HNO3/HC|/HF
,"rl4rOf jit& jt.li,lilt +
C( / H€i to appropriate
1)
2)
f [*a{*4+*it{rtc
/ AlkaliF6ion
/HCltod$d€
/ rcP,aEs
f!911L / samdeMatedal
51eel,@pper,allnirum, solder
&ltgti
ta{*tt
;filt&AJlfi / DiqesL|onAcd
-t+, 4la{,!lt, nn*, el,,k /
Aa@ reoia. HNO' HCl. HF. H,O,
rra{,Inc / HNoJftF
A, J6,€, nit /
Gold,olalinum,
Dalladium,
ceramic
,i(f rf 7h-ir,g t.rLrlf,.' I
irl#B*i{Aftrcnm 6id
rti!€ /HNOr
&E / Plaslic
4?,*i&8tt$ / coot,
fherdigestate
lhrough
liher
*d, t{"*,
s!t, td / H,so. Ho,. HNorhcl
,! \'efi*1eti*l+
/ Anyacldlo lotaldig€Gtion
j i i r i r +
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Number : TWNC00232330
Test Report
Applicant:
Littelfuse Philippines Inc.
LIMA Technology Center, Lipa City,
Malvar, Batangas
Date
: Nov 18, 2011
Sample Description:
One (1) group of submitted samples said to be :
Part Description
: Solder
Part Number
: 692213
Date Sample Received
: Nov 11, 2011
Date Test Started
: Nov 14, 2011
Test Conducted :
As requested by the applicant, for details please refer to attached pages.
Authorized By:
On Behalf Of Intertek Testing Services
Taiwan Limited
K. Y. Liang
Director
This report shall not be reproduced
except in full, without the written
approval of the laboratory.
Page 1 of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Number : TWNC00232330
Test Conducted
(Ⅰ) Test Result Summary :
Test Item
Heavy Metal
Cadmium (Cd) content
Lead (Pb) content
Mercury (Hg) content
Chromium VI (Cr6+) content (mg/kg with 50cm2)
Result (ppm)
Silvery Metal
ND
92
ND
Negative (< 0.02)
Remarks: ppm = Parts per million based on weight of tested sample = mg/kg
ND = Not detected
<
= Less than
mg/kg with 50cm2 = milligram per kilogram with 50 square centimetre
Negative = A negative test result indicated positive observation
was not found at the time of Test.
Responsibility of Chemist : Irene Chiou / Kevin Liu / Cathy Chen
Date Sample Received
Test Period
: Nov 11, 2011
: Nov 14, 2011 To Nov 17, 2011
(Ⅱ) RoHS Requirement:
Restricted Substances
Cadmium (Cd) Content
Lead (Pb) Content
Mercury (Hg) Content
Chromium VI (Cr6+) Content
Limits
0.01% (100ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for
homogeneous material.
Page 2 of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Number : TWNC00232330
Test Conducted
(Ⅲ) Test Method:
Test Item
Cadmium (Cd)
content
Lead (Pb) content
Mercury (Hg)
content
Chromium VI (Cr6+)
content
Test Method
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 7, by microwave
digestion until the tested samples are
totally dissolved and determined by
ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in annex B, by boiling water
extraction and determined by UV-Vis
spectrophotometer.
Reporting Limit
2 ppm
2 ppm
2 ppm
0.02
mg/kg with 50cm2
Remark: Reporting limit = Quantitation limit of analyte in sample
Page 3 of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Number : TWNC00232330
Test Conducted
(Ⅳ) Measurement Flowchart:
Test for Cd/Pb/Hg/Chromium (VI)
Reference Standard:IEC 62321 edition 1.0:2008
Sample preparation
Take sample and immerse into Aqua Regia, start to strip plating layer
Stop the stripping procedure upon color change completely
Take the Aqua solution as plating component and stripped body as substrate component
Cd/Pb/Hg
Cr
Polymers /
electronics
Metal
For different
material, digest
the sample with
*1
appropriate acid
By spot test
Negative
Confirm the tested
samples are
totally dissolved
Make up with
deionized water
6+
*2
Weigh sample
and add
alkaline
solution
Get 50cm2 sample
Definite temp.
extraction
By boiling water
extraction
Cool and filter
the extract
Analyzed by ICP-OES
Make up with deionized water and add
diphenyl-carbazide solution
Remarks:
*1: List of Appropriate Acid:
Material
Polymers
Metals
Electronics
Analyzed by UV-VIS
Acid Added for Digestion
HNO3,HCl,HF,H2O2,H3BO3
HNO3,HCl,HF
HNO3,HCl,H2O2,HBF4
*2: If the result of spot test is positive, Chromium VI would be determined as detected.
End of Report
Page 4 of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Number : TWNC00232330
Test Conducted
Photo
Page 5 of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Test Report
Applicant:
Number : TWNC00232331
Littelfuse Philippines Inc.
LIMA Technology Center, Lipa City,
Malvar, Batangas
Date
: Nov 18, 2011
Sample Description:
One (1) group of submitted samples said to be :
Part Description
: TE Caps (same with 910-016 TR Caps)
Part Number
: 910-017
Date Sample Received
: Nov 11, 2011
Date Test Started
: Nov 14, 2011
Test Conducted :
As requested by the applicant, for details please refer to attached pages.
Authorized By:
On Behalf Of Intertek Testing Services
Taiwan Limited
K. Y. Liang
Director
This report shall not be reproduced
except in full, without the written
approval of the laboratory.
Page 1 of 9
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Number : TWNC00232331
Test Conducted
(Ⅰ) Test Result Summary :
Test Item
Result (ppm)
Brown Plastic
Heavy Metal
Cadmium (Cd) content
Lead (Pb) content
Mercury (Hg) content
Chromium VI (Cr6+) content
Polybrominated Biphenyls (PBBs)
Monobrominated Biphenyls (MonoBB)
Dibrominated Biphenyls (DiBB)
Tribrominated Biphenyls (TriBB)
Tetrabrominated Biphenyls (TetraBB)
Pentabrominated Biphenyls (PentaBB)
Hexabrominated Biphenyls (HexaBB)
Heptabrominated Biphenyls (HeptaBB)
Octabrominated Biphenyls (OctaBB)
Nonabrominated Biphenyls (NonaBB)
Decabrominated Biphenyl (DecaBB)
Polybrominated Diphenyl Ethers (PBDEs)
Monobrominated Diphenyl Ethers (MonoBDE)
Dibrominated Diphenyl Ethers (DiBDE)
Tribrominated Diphenyl Ethers (TriBDE)
Tetrabrominated Diphenyl Ethers (TetraBDE)
Pentabrominated Diphenyl Ethers (PentaBDE)
Hexabrominated Diphenyl Ethers (HexaBDE)
Heptabrominated Diphenyl Ethers (HeptaBDE)
Octabrominated Diphenyl Ethers (OctaBDE)
Nonabrominated Diphenyl Ethers (NonaBDE)
Decabrominated Diphenyl Ether (DecaBDE)
Halogen Content
Fluorine (F)
Chlorine (Cl)
Bromine (Br)
Iodine (I)
Phthalates
Di(2-ethylhexyl) Phthalate (DEHP)
Dibutyl Phthalate (DBP)
Benzyl Butyl Phthalate (BBP)
Others
Hexabromocyclododecane (HBCDD)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Remarks: ppm = Parts per million based on weight of tested sample = mg/kg
ND = Not detected
Responsibility of Chemist : Irene Chiou / Kevin Liu / Cathy Chen
Date Sample Received
Test Period
: Nov 11, 2011
: Nov 14, 2011 To Nov 16, 2011
Page 2 of 9
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Test Conducted
(Ⅱ) RoHS Requirement:
Restricted Substances
Cadmium (Cd) Content
Lead (Pb) Content
Mercury (Hg) Content
Chromium VI (Cr6+) Content
Polybrominated Biphenyls (PBBs)
Polybrominated Diphenyl Ehters (PBDEs)
Number : TWNC00232331
Limits
0.01% (100ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for
homogeneous material.
(Ⅲ) Test Method:
Test Item
Cadmium (Cd) content
Lead (Pb) content
Mercury (Hg) content
Chromium VI (Cr6+)
content
Test Method
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the
tested samples are totally
dissolved and determined by ICPOES.
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the
tested samples are totally
dissolved and determined by ICPOES.
With reference to IEC 62321 edition
1.0:2008 in clause 7, by microwave
digestion until the tested samples
are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in annex C, by alkaline
digestion and determined by UV-Vis
spectrophotometer.
Reporting Limit
2 ppm
2 ppm
2 ppm
1 ppm
Page 3 of 9
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Number : TWNC00232331
Test Conducted
(Ⅲ) Test Method:
Test Item
Test Method
Reporting Limit
With reference to IEC 62321 edition
1.0:2008 in annex A, by solvent
Polybrominated
5 ppm
extraction and determined by GC-MSD
Biphenyls (PBBs)
and further HPLC confirmation when
necessary.
With reference to IEC 62321 edition
Polybrominated
1.0:2008 in annex A, by solvent
5 ppm
Diphenyl Ethers
extraction and determined by GC-MSD
and further HPLC confirmation when
(PBDEs)
necessary.
With reference to EN 14582:2007 by
Halogen Content
50 ppm
calorimetric bomb with oxygen and
determined by ion chromatography
With reference to EN 14372: 2004, by
Phthalates
solvent extraction and determined by
50 ppm
GC-MSD
With reference to USEPA 3540C, by
Hexabromocyclododecane
10 ppm
solvent extraction and determined by
(HBCDD)
GC-MSD
Remark: Reporting limit = Quantitation limit of analyte in sample
Page 4 of 9
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Number : TWNC00232331
Test Conducted
(Ⅳ) Measurement Flowchart:
Test for Cd/Pb/Hg/Chromium (VI)/PBBS/PBDES Contents
Reference Standard: IEC 62321 edition 1.0:2008
Sample preparation
For non-metal part
For metal part
Take sample and immerse into Aqua Regia, start to strip plating layer
Stop the stripping procedure upon color change completely
Take the Aqua solution as plating component and stripped body as substrate component
Cd/Pb/Hg
Cr
Confirm the tested
samples are
totally dissolved
Make up with
deionized water
PBBs/PBDEs
Polymers /
electronics
Metal
For different
material, digest
the sample with
*1
appropriate acid
6+
Weigh sample and
add organic solvent
By spot test
Negative
Get 50cm2 sample
By boiling water
extraction
*2
Weigh sample
and add
alkaline
solution
By Soxhlet
extraction or
Solvent extraction
Definite temp.
extraction
Cool and filter
the extract
Analyzed by ICP-OES
Concentrate the
extract and make up
with organic
solvent
Analyzed by GC-MSD
Make up with deionized
water and add diphenylcarbazide solution
Remarks:
*1: List of Appropriate Acid:
Material
Polymers
Metals
Electronics
Analyzed by UV-VIS
Acid Added for Digestion
HNO3,HCl,HF,H2O2,H3BO3
HNO3,HCl,HF
HNO3,HCl,H2O2,HBF4
*2: If the result of spot test is positive, Chromium VI would be determined as detected.
Page 5 of 9
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Number : TWNC00232331
Test Conducted
(Ⅳ) Measurement Flowchart:
Test for Halogen Content
Reference Standard:EN 14582
Sampling/grinding or
cutting
Add absorbent in a
combustion flask &
place weighed sample in
equipment
Fill oxygen into
calorimetric bomb
Ignite then leave the
flask at room
temperature
Transfer the absorbent
into a volumetric flask
Make up with deionized
water
Analyzed by ion
chromatography
Page 6 of 9
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Number : TWNC00232331
Test Conducted
(Ⅳ) Measurement Flowchart:
Test For Phthalates Contents
Reference Method: EN 14372: 2004
Sampling/grinding or
cutting
Weigh sample and add
organic solvent
By solvent extraction
Concentrate the extract
and make up with
organic solvent
Analyzed by GC-MSD
Page 7 of 9
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Number : TWNC00232331
Test Conducted
(Ⅳ) Measurement Flowchart:
Test For Hexabromocyclododecane (HBCDD)
Reference Standard:USEPA 3540C
Sampling/grinding or cutting
Weigh sample and add organic
solvent
By soxhlet extraction
Concentrate the extract and
make up with organic solvent
Analyzed by GC-MSD
End of Report
Page 8 of 9
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Number : TWNC00232331
Test Conducted
Photo
Page 9 of 9
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Test Report
Applicant:
Littelfuse Philippines Inc.
LIMA Technology Center, Lipa City,
Malvar, Batangas
Number
: TWNC00256914
Date
: May 15, 2012
Sample Description:
One (1) group of submitted samples said to be :
Part Description
: Socket with Pin
Part Number
: 867-003
Date Sample Received
: May 10, 2012
Date Test Started
: May 10, 2012
Test Conducted :
As requested by the applicant, for details please refer to attached pages.
Authorized By:
On Behalf Of Intertek Testing Services
Taiwan Limited
K. Y. Liang
Director
This report shall not be reproduced
except in full, without the written
approval of the laboratory.
Page 1 of 10
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Number:
TWNC00256914
Test Conducted
(Ⅰ) Test Result Summary :
Test Item
Heavy Metal
Cadmium (Cd) content
Lead (Pb) content
Mercury (Hg) content
Chromium VI (Cr6+) content (For Non-Metal
Material)
Chromium VI (Cr6+) content (By Boiling Water
Extraction On Metal) (mg/kg with 50cm2)
Polybrominated Biphenyls (PBBs)
Monobrominated Biphenyls (MonoBB)
Dibrominated Biphenyls (DiBB)
Tribrominated Biphenyls (TriBB)
Tetrabrominated Biphenyls (TetraBB)
Pentabrominated Biphenyls (PentaBB)
Hexabrominated Biphenyls (HexaBB)
Heptabrominated Biphenyls (HeptaBB)
Octabrominated Biphenyls (OctaBB)
Nonabrominated Biphenyls (NonaBB)
Decabrominated Biphenyl (DecaBB)
Polybrominated Diphenyl Ethers (PBDEs)
Monobrominated Diphenyl Ethers (MonoBDE)
Dibrominated Diphenyl Ethers (DiBDE)
Tribrominated Diphenyl Ethers (TriBDE)
Tetrabrominated Diphenyl Ethers (TetraBDE)
Pentabrominated Diphenyl Ethers (PentaBDE)
Hexabrominated Diphenyl Ethers (HexaBDE)
Heptabrominated Diphenyl Ethers (HeptaBDE)
Octabrominated Diphenyl Ethers (OctaBDE)
Nonabrominated Diphenyl Ethers (NonaBDE)
Decabrominated Diphenyl Ether (DecaBDE)
Halogen Content
Fluorine (F)
Chlorine (Cl)
Bromine (Br)
Iodine (I)
(1)
Result (ppm)
(2)
(3)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
--
--
ND
Negative
(< 0.02)(#)
Negative
(< 0.02)(#)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
-----------
-----------
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
-----------
-----------
ND
ND
ND
ND
-----
-----
Page 2 of 10
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Number:
TWNC00256914
Test Conducted
(Ⅰ) Test Result Summary :
Test Item
(1)
Result (ppm)
(2)
(3)
ND
ND
ND
----
----
ND
--
--
Phthalates
Di(2-ethylhexyl) Phthalate (DEHP)
Dibutyl Phthalate (DBP)
Benzyl Butyl Phthalate (BBP)
Others
Hexabromocyclododecane (HBCDD)
Remarks: ppm = Parts per million based on weight of tested sample = mg/kg
ND = Not detected
<
= Less than
mg/kg with 50cm2 = milligram per kilogram with 50 square centimetre
Negative = A negative test result indicated positive observation
was not found at the time of Test.
#
= Due to the insufficient sample area, reduced total sample
surface of 25 cm2 was used and the dilution factor was
adjusted accordingly.
Tested Components:
(1) Black Body Part
(2) Coppery Metal Substrate
(3) Silvery Plating On Metal Pin
Responsibility of Chemist : Irene Chiou / Kevin Liu / Cathy Chen
Date Sample Received
Test Period
: May 10, 2012
: May 10, 2012 To May 14, 2012
(Ⅱ) RoHS Requirement:
Restricted Substances
Cadmium (Cd) Content
Lead (Pb) Content
Mercury (Hg) Content
Chromium VI (Cr6+) Content
Polybrominated Biphenyls (PBBs)
Polybrominated Diphenyl Ehters (PBDEs)
Limits
0.01% (100ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for
homogeneous material.
Page 3 of 10
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Number:
Test Conducted
(Ⅲ) Test Method:
Test Item
TWNC00256914
Test Method
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
Cadmium (Cd)
microwave digestion until the tested
content
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
Lead (Pb) content
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 7, by microwave
Mercury (Hg)
digestion until the tested samples are
content
totally dissolved and determined by
ICP-OES.
Chromium VI (Cr6+) With reference to IEC 62321 edition
content (For Non1.0:2008 in annex C, by alkaline
Metal Extraction On digestion and determined by UV-Vis
Metal)
spectrophotometer.
Chromium VI (Cr6+) With reference to IEC 62321 edition
content (By Boiling 1.0:2008 in annex B, by boiling water
Water Extraction On extraction and determined by UV-Vis
Metal)
Spectrophotometer.
With reference to IEC 62321 edition
1.0:2008 in annex A, by solvent
Polybrominated
extraction and determined by GC-MS and
Biphenyls (PBBs)
further HPLC-DAD confirmation when
necessary.
With reference to IEC 62321 edition
Polybrominated
1.0:2008 in annex A, by solvent
Diphenyl Ethers
extraction and determined by GC-MS and
(PBDEs)
further HPLC-DAD confirmation when
necessary.
With reference to EN 14582:2007 by
Halogen Content
calorimetric bomb with oxygen and
determined by Ion Chromatograph.
With reference to EN 14372: 2004, by
Phthalates
solvent extraction and determined by
GC-MS.
With reference to USEPA 3540C, by
Hexabromocyclodode
solvent extraction and determined by
cane (HBCDD)
GC-MSD.
Reporting Limit
2 ppm
2 ppm
2 ppm
1 ppm
0.02
mg/kg with 50cm2
5 ppm
5 ppm
50 ppm
50 ppm
10 ppm
Remark: Reporting limit = Quantitation limit of analyte in sample
Page 4 of 10
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Number:
TWNC00256914
Test Conducted
(Ⅳ) Measurement Flowchart:
Test for Cd/Pb/Hg/Chromium (VI)
Reference Standard:IEC 62321 edition 1.0:2008
Sample preparation
Take sample and immerse into Aqua Regia, start to strip plating layer
Stop the stripping procedure upon color change completely
Take the Aqua solution as plating component and stripped body as substrate component
Cd/Pb/Hg
Cr
Polymers /
electronics
Metal
For different
material, digest
the sample with
*1
appropriate acid
By spot test
Negative
Confirm the tested
samples are
totally dissolved
Make up with
deionized water
6+
*2
Weigh sample
and add
alkaline
solution
Get 50cm2 sample
Definite temp.
extraction
By boiling water
extraction
Cool and filter
the extract
Analyzed by ICP-OES
Make up with deionized water and add
diphenyl-carbazide solution
Remarks:
*1: List of Appropriate Acid:
Material
Polymers
Metals
Electronics
Analyzed by UV-VIS
Acid Added for Digestion
HNO3,HCl,HF,H2O2,H3BO3
HNO3,HCl,HF
HNO3,HCl,H2O2,HBF4
*2: If the result of spot test is positive, Chromium VI would be determined as detected.
Page 5 of 10
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Number:
TWNC00256914
Test Conducted
(Ⅳ) Measurement Flowchart:
Test for Cd/Pb/Hg/Chromium (VI)/PBBS/PBDES Contents
Reference Standard: IEC 62321 edition 1.0:2008
Sample preparation
For non-metal part
For metal part
Take sample and immerse into Aqua Regia, start to strip plating layer
Stop the stripping procedure upon color change completely
Take the Aqua solution as plating component and stripped body as substrate component
Cd/Pb/Hg
Cr
Weigh sample and
add organic solvent
By spot test
Negative
Confirm the tested
samples are
totally dissolved
Make up with
deionized water
PBBs/PBDEs
Polymers /
electronics
Metal
For different
material, digest
the sample with
*1
appropriate acid
6+
Get 50cm2 sample
By boiling water
extraction
*2
Weigh sample
and add
alkaline
solution
By Soxhlet
extraction or
Solvent extraction
Definite temp.
extraction
Cool and filter
the extract
Analyzed by ICP-OES
Concentrate the
extract and make up
with organic
solvent
Analyzed by GC-MSD
Make up with deionized
water and add diphenylcarbazide solution
Analyzed by UV-VIS
Remarks:
*1: List of Appropriate Acid:
Material
Polymers
Metals
Electronics
Acid Added for Digestion
HNO3,HCl,HF,H2O2,H3BO3
HNO3,HCl,HF
HNO3,HCl,H2O2,HBF4
*2: If the result of spot test is positive, Chromium VI would be determined as detected.
Page 6 of 10
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Number:
TWNC00256914
Test Conducted
(Ⅳ) Measurement Flowchart:
Test for Halogen Content
Reference Standard:EN 14582
Sampling/grinding or
cutting
Add absorbent in a
combustion flask &
place weighed sample in
equipment
Fill oxygen into
calorimetric bomb
Ignite then leave the
bomb at room
temperature
Transfer the absorbent
into a volumetric flask
Make up with deionized
water
Analyzed by ion
chromatography
Page 7 of 10
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Number:
TWNC00256914
Test Conducted
(Ⅳ) Measurement Flowchart:
Test For Phthalates Contents
Reference Method: EN 14372: 2004
Sampling/grinding or
cutting
Weigh sample and add
organic solvent
By solvent extraction
Concentrate the extract
and make up with
organic solvent
Analyzed by GC-MSD
Page 8 of 10
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Number:
TWNC00256914
Test Conducted
(Ⅳ) Measurement Flowchart:
Test For Hexabromocyclododecane (HBCDD)
Reference Standard:USEPA 3540C
Sampling/grinding or cutting
Weigh sample and add organic
solvent
By soxhlet extraction
Concentrate the extract and
make up with organic solvent
Analyzed by GC-MSD
End of Report
Page 9 of 10
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Number:
TWNC00256914
Test Conducted
Photo
Page 10 of
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Number : TWNC00232333
Test Report
Applicant:
Littelfuse Philippines Inc.
LIMA Technology Center, Lipa City,
Malvar, Batangas
Date
: Nov 18, 2011
Sample Description:
One (1) group of submitted samples said to be :
Part Description
: Ceramic Paper
Part Number
: 009116
Date Sample Received
: Nov 11, 2011
Date Test Started
: Nov 14, 2011
Test Conducted :
As requested by the applicant, for details please refer to attached pages.
Authorized By:
On Behalf Of Intertek Testing Services
Taiwan Limited
K. Y. Liang
Director
This report shall not be reproduced
except in full, without the written
approval of the laboratory.
Page 1 of 6
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Number : TWNC00232333
Test Conducted
(Ⅰ) Test Result Summary :
Test Item
Result (ppm)
White Material
Heavy Metal
Cadmium (Cd) content
Lead (Pb) content
Mercury (Hg) content
Chromium VI (Cr6+) content
Polybrominated Biphenyls (PBBs)
Monobrominated Biphenyls (MonoBB)
Dibrominated Biphenyls (DiBB)
Tribrominated Biphenyls (TriBB)
Tetrabrominated Biphenyls (TetraBB)
Pentabrominated Biphenyls (PentaBB)
Hexabrominated Biphenyls (HexaBB)
Heptabrominated Biphenyls (HeptaBB)
Octabrominated Biphenyls (OctaBB)
Nonabrominated Biphenyls (NonaBB)
Decabrominated Biphenyl (DecaBB)
Polybrominated Diphenyl Ethers (PBDEs)
Monobrominated Diphenyl Ethers (MonoBDE)
Dibrominated Diphenyl Ethers (DiBDE)
Tribrominated Diphenyl Ethers (TriBDE)
Tetrabrominated Diphenyl Ethers (TetraBDE)
Pentabrominated Diphenyl Ethers (PentaBDE)
Hexabrominated Diphenyl Ethers (HexaBDE)
Heptabrominated Diphenyl Ethers (HeptaBDE)
Octabrominated Diphenyl Ethers (OctaBDE)
Nonabrominated Diphenyl Ethers (NonaBDE)
Decabrominated Diphenyl Ether (DecaBDE)
Halogen Content
Fluorine (F)
Chlorine (Cl)
Bromine (Br)
Iodine (I)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Remarks: ppm = Parts per million based on weight of tested sample = mg/kg
ND = Not detected
Responsibility of Chemist : Irene Chiou / Kevin Liu / Cathy Chen
Date Sample Received
Test Period
: Nov 11, 2011
: Nov 14, 2011 To Nov 16, 2011
Page 2 of 6
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Test Conducted
(Ⅱ) RoHS Requirement:
Restricted Substances
Cadmium (Cd) Content
Lead (Pb) Content
Mercury (Hg) Content
Chromium VI (Cr6+) Content
Polybrominated Biphenyls (PBBs)
Polybrominated Diphenyl Ehters (PBDEs)
Number : TWNC00232333
Limits
0.01% (100ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for
homogeneous material.
(Ⅲ) Test Method:
Test Item
Cadmium (Cd)
content
Lead (Pb) content
Mercury (Hg)
content
Chromium VI (Cr6+)
content
Polybrominated
Biphenyls (PBBs)
Polybrominated
Diphenyl Ethers
(PBDEs)
Halogen Content
Test Method
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 7, by microwave
digestion until the tested samples are
totally dissolved and determined by
ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in annex C, by alkaline
digestion and determined by UV-Vis
spectrophotometer.
With reference to IEC 62321 edition
1.0:2008 in annex A, by solvent
extraction and determined by GC-MSD
and further HPLC confirmation when
necessary.
With reference to IEC 62321 edition
1.0:2008 in annex A, by solvent
extraction and determined by GC-MSD
and further HPLC confirmation when
necessary.
With reference to EN 14582:2007 by
calorimetric bomb with oxygen and
determined by ion chromatography
Reporting Limit
2 ppm
2 ppm
2 ppm
1 ppm
5 ppm
5 ppm
50 ppm
Remark: Reporting limit = Quantitation limit of analyte in sample
Page 3 of 6
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Number : TWNC00232333
Test Conducted
(Ⅳ) Measurement Flowchart:
Test for Cd/Pb/Hg/Chromium (VI)/PBBS/PBDES Contents
Reference Standard: IEC 62321 edition 1.0:2008
Sample preparation
For non-metal part
For metal part
Take sample and immerse into Aqua Regia, start to strip plating layer
Stop the stripping procedure upon color change completely
Take the Aqua solution as plating component and stripped body as substrate component
Cd/Pb/Hg
Cr
Confirm the tested
samples are
totally dissolved
Make up with
deionized water
PBBs/PBDEs
Polymers /
electronics
Metal
For different
material, digest
the sample with
*1
appropriate acid
6+
Weigh sample and
add organic solvent
By spot test
Negative
Get 50cm2 sample
By boiling water
extraction
*2
Weigh sample
and add
alkaline
solution
By Soxhlet
extraction or
Solvent extraction
Definite temp.
extraction
Cool and filter
the extract
Analyzed by ICP-OES
Concentrate the
extract and make up
with organic
solvent
Analyzed by GC-MSD
Make up with deionized
water and add diphenylcarbazide solution
Remarks:
*1: List of Appropriate Acid:
Material
Polymers
Metals
Electronics
Analyzed by UV-VIS
Acid Added for Digestion
HNO3,HCl,HF,H2O2,H3BO3
HNO3,HCl,HF
HNO3,HCl,H2O2,HBF4
*2: If the result of spot test is positive, Chromium VI would be determined as detected.
Page 4 of 6
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Number : TWNC00232333
Test Conducted
(Ⅳ) Measurement Flowchart:
Test for Halogen Content
Reference Standard:EN 14582
Sampling/grinding or
cutting
Add absorbent in a
combustion flask &
place weighed sample in
equipment
Fill oxygen into
calorimetric bomb
Ignite then leave the
flask at room
temperature
Transfer the absorbent
into a volumetric flask
Make up with deionized
water
Analyzed by ion
chromatography
End of Report
Page 5 of 6
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Number : TWNC00232333
Test Conducted
Photo
Page 6 of 6
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401