J24325-1 Fl_L2 Final Report.pdf

ANALYTICAL REPORT
Job Number: 660-24325-1
Job Description: Raytheon
For:
ARCADIS U.S., Inc.
14055 Riveredge Drive
Suite 400
Tampa, FL 33637
Attention: Mr. Gus Suarez
_____________________________________________
Natalie Tafuni
Project Manager I
[email protected]
07/30/2008
Methods: FDEP, DOH Certification #: E84282, E81005 These test results meet all the requirements of NELAC unless
specified in the case narrative. All questions regarding this test report should be directed to the TestAmerica Project
Manager who signed this test report. The estimated uncertainty associated with these reported results is available upon
request. The results contained in this test report relate only to these samples included herein.
TestAmerica Laboratories, Inc.
TestAmerica Tampa 6712 Benjamin Road, Suite 100, Tampa, FL 33634
Tel (813) 885-7427 Fax (813) 885-7049 www.testamericainc.com
Page 1 of 45
Job Narrative
660-J24325-1
Comments
No additional comments.
Receipt
All samples were received in good condition within temperature requirements.
8260B
Surrogate recovery for the following samples was outside of the upper control limit: 24325-2 and 24325-5. These samples did not contain
any target analytes; therefore, re-extraction and/or re-analysis was not performed.
Page 2 of 45
EXECUTIVE SUMMARY - Detections
Client: ARCADIS U.S., Inc.
Lab Sample ID
Analyte
660-24325-4
Job Number: 660-24325-1
Client Sample ID
Result / Qualifier
Toluene
Units
Method
CP-108 (38'-40')_072808
Toluene
660-24325-6
Reporting
Limit
0.78
I
1.0
ug/L
8260B
0.63
I
1.0
ug/L
8260B
CP-108 (61'-63')_072808
TestAmerica Tampa
Page 3 of 45
METHOD SUMMARY
Client: ARCADIS U.S., Inc.
Description
Job Number: 660-24325-1
Lab Location Method
Preparation Method
Volatile Organic Compounds by GC/MS
Purge-and-Trap
TAL TAM
TAL TAM
SW846 8260B
SW846 5030B
1,4-Dioxane by SIM/Isotopic Dilution
Purge-and-Trap
TAL TAM
TAL TAM
SW846 8260C SIM/ID
SW846 5030B
Matrix
Water
Lab References:
TAL TAM = TestAmerica Tampa
Method References:
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its
Updates.
TestAmerica Tampa
Page 4 of 45
METHOD / ANALYST SUMMARY
Client: ARCADIS U.S., Inc.
Job Number: 660-24325-1
Method
Analyst
SW846 8260B
Carlson, Robyn
RC
SW846 8260C SIM/ID
Carlson, Robyn
RC
TestAmerica Tampa
Page 5 of 45
Analyst ID
SAMPLE SUMMARY
Client: ARCADIS U.S., Inc.
Job Number: 660-24325-1
Date/Time
Sampled
Date/Time
Received
Water
07/28/2008 0000
07/29/2008 0945
Water
Water
Water
Water
Water
Water
Water
Water
07/28/2008
07/28/2008
07/28/2008
07/28/2008
07/28/2008
07/28/2008
07/29/2008
07/29/2008
07/29/2008
07/29/2008
07/29/2008
07/29/2008
07/29/2008
07/29/2008
07/29/2008
07/29/2008
Lab Sample ID
Client Sample ID
Client Matrix
660-24325-1
Trip Blank
(7/28/08)#2_072808
CP-108 (10'-12')_072808
CP-108 (28'-30')_072808
CP-108 (38'-40')_072808
CP-108 (48'-50')_072808
CP-108 (61'-63')_072808
CP-108 (69'-71')_072808
CP-106 (10'-12')_072908
CP-106 (24'-26')_072908
660-24325-2
660-24325-3
660-24325-4
660-24325-5
660-24325-6
660-24325-7
660-24325-8
660-24325-9
TestAmerica Tampa
Page 6 of 45
1122
1151
1230
1258
1434
1519
0808
0830
0945
0945
0945
0945
0945
0945
0945
0945
SAMPLE RESULTS
TestAmerica Tampa
Page 7 of 45
Analytical Data
Client: ARCADIS U.S., Inc.
Job Number: 660-24325-1
Client Sample ID:
Trip Blank (7/28/08)#2_072808
Lab Sample ID:
Client Matrix:
660-24325-1
Water
Date Sampled:
Date Received:
07/28/2008 0000
07/29/2008 0945
8260B Volatile Organic Compounds by GC/MS
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260B
5030B
1.0
07/29/2008 1348
07/29/2008 1348
Analyte
Benzene
Bromobenzene
1,2-Dichlorobenzene
Chlorobromomethane
Dichlorobromomethane
Bromoform
Bromomethane
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
Chlorodibromomethane
1,2-Dibromo-3-Chloropropane
Ethylene Dibromide
Dibromomethane
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
Hexachlorobutadiene
Isopropylbenzene
4-Isopropyltoluene
Methylene Chloride
Naphthalene
N-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
TestAmerica Tampa
Analysis Batch: 660-65433
Result (ug/L)
0.50
0.58
0.44
0.58
0.35
0.58
2.5
0.67
0.63
0.84
0.42
0.63
2.5
0.90
1.0
0.65
0.52
0.34
2.5
0.50
0.41
0.64
0.52
2.5
0.52
0.57
0.45
0.65
0.44
0.52
0.39
0.36
0.31
0.14
0.14
0.44
0.40
0.19
0.69
4.0
2.5
0.59
0.98
0.63
Page 8 of 45
Instrument ID:
BVMH GC/MS
Lab File ID:
1HG2915.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
MDL
0.50
0.58
0.44
0.58
0.35
0.58
2.5
0.67
0.63
0.84
0.42
0.63
2.5
0.90
1.0
0.65
0.52
0.34
2.5
0.50
0.41
0.64
0.52
2.5
0.52
0.57
0.45
0.65
0.44
0.52
0.39
0.36
0.31
0.14
0.14
0.44
0.40
0.19
0.69
4.0
2.5
0.59
0.98
0.63
PQL
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
4.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
5.0
1.0
2.0
1.0
Analytical Data
Client: ARCADIS U.S., Inc.
Job Number: 660-24325-1
Client Sample ID:
Trip Blank (7/28/08)#2_072808
Lab Sample ID:
Client Matrix:
660-24325-1
Water
Date Sampled:
Date Received:
07/28/2008 0000
07/29/2008 0945
8260B Volatile Organic Compounds by GC/MS
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260B
5030B
1.0
07/29/2008 1348
07/29/2008 1348
Analyte
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
o-Xylene
Acetone
2-Butanone (MEK)
4-Methyl-2-pentanone (MIBK)
Carbon disulfide
2-Hexanone
Methyl tert-butyl ether
m-Xylene & p-Xylene
Analysis Batch: 660-65433
Result (ug/L)
0.15
0.50
0.51
0.77
0.58
0.46
0.47
0.50
2.5
0.18
0.86
0.54
0.50
0.50
9.9
8.4
3.8
0.85
4.4
0.44
0.60
Surrogate
Toluene-d8 (Surr)
4-Bromofluorobenzene
Dibromofluoromethane
%Rec
109
97
104
TestAmerica Tampa
Page 9 of 45
Instrument ID:
BVMH GC/MS
Lab File ID:
1HG2915.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
MDL
0.15
0.50
0.51
0.77
0.58
0.46
0.47
0.50
2.5
0.18
0.86
0.54
0.50
0.50
9.9
8.4
3.8
0.85
4.4
0.44
0.60
PQL
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
20
10
10
1.0
10
1.0
2.0
Acceptance Limits
77 - 122
74 - 126
70 - 130
Analytical Data
Client: ARCADIS U.S., Inc.
Job Number: 660-24325-1
Client Sample ID:
CP-108 (10'-12')_072808
Lab Sample ID:
Client Matrix:
660-24325-2
Water
Date Sampled:
Date Received:
07/28/2008 1122
07/29/2008 0945
8260B Volatile Organic Compounds by GC/MS
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260B
5030B
1.0
07/29/2008 1609
07/29/2008 1609
Analyte
Benzene
Bromobenzene
1,2-Dichlorobenzene
Chlorobromomethane
Dichlorobromomethane
Bromoform
Bromomethane
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
Chlorodibromomethane
1,2-Dibromo-3-Chloropropane
Ethylene Dibromide
Dibromomethane
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
Hexachlorobutadiene
Isopropylbenzene
4-Isopropyltoluene
Methylene Chloride
Naphthalene
N-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
TestAmerica Tampa
Analysis Batch: 660-65433
Result (ug/L)
0.50
0.58
0.44
0.58
0.35
0.58
2.5
0.67
0.63
0.84
0.42
0.63
2.5
0.90
1.0
0.65
0.52
0.34
2.5
0.50
0.41
0.64
0.52
2.5
0.52
0.57
0.45
0.65
0.44
0.52
0.39
0.36
0.31
0.14
0.14
0.44
0.40
0.19
0.69
4.0
2.5
0.59
0.98
0.63
Page 10 of 45
Instrument ID:
BVMH GC/MS
Lab File ID:
1HG2922.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
MDL
0.50
0.58
0.44
0.58
0.35
0.58
2.5
0.67
0.63
0.84
0.42
0.63
2.5
0.90
1.0
0.65
0.52
0.34
2.5
0.50
0.41
0.64
0.52
2.5
0.52
0.57
0.45
0.65
0.44
0.52
0.39
0.36
0.31
0.14
0.14
0.44
0.40
0.19
0.69
4.0
2.5
0.59
0.98
0.63
PQL
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
4.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
5.0
1.0
2.0
1.0
Analytical Data
Client: ARCADIS U.S., Inc.
Job Number: 660-24325-1
Client Sample ID:
CP-108 (10'-12')_072808
Lab Sample ID:
Client Matrix:
660-24325-2
Water
Date Sampled:
Date Received:
07/28/2008 1122
07/29/2008 0945
8260B Volatile Organic Compounds by GC/MS
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260B
5030B
1.0
07/29/2008 1609
07/29/2008 1609
Analyte
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
o-Xylene
Acetone
2-Butanone (MEK)
4-Methyl-2-pentanone (MIBK)
Carbon disulfide
2-Hexanone
Methyl tert-butyl ether
m-Xylene & p-Xylene
Surrogate
Toluene-d8 (Surr)
4-Bromofluorobenzene
Dibromofluoromethane
TestAmerica Tampa
Analysis Batch: 660-65433
Result (ug/L)
0.15
0.50
0.51
0.77
0.58
0.46
0.47
0.50
2.5
0.18
0.86
0.54
0.50
0.50
9.9
8.4
3.8
0.85
4.4
0.44
0.60
%Rec
129
111
121
Page 11 of 45
Instrument ID:
BVMH GC/MS
Lab File ID:
1HG2922.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
J1
MDL
0.15
0.50
0.51
0.77
0.58
0.46
0.47
0.50
2.5
0.18
0.86
0.54
0.50
0.50
9.9
8.4
3.8
0.85
4.4
0.44
0.60
PQL
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
20
10
10
1.0
10
1.0
2.0
Acceptance Limits
77 - 122
74 - 126
70 - 130
Analytical Data
Client: ARCADIS U.S., Inc.
Job Number: 660-24325-1
Client Sample ID:
CP-108 (28'-30')_072808
Lab Sample ID:
Client Matrix:
660-24325-3
Water
Date Sampled:
Date Received:
07/28/2008 1151
07/29/2008 0945
8260B Volatile Organic Compounds by GC/MS
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260B
5030B
1.0
07/29/2008 1750
07/29/2008 1750
Analyte
Benzene
Bromobenzene
1,2-Dichlorobenzene
Chlorobromomethane
Dichlorobromomethane
Bromoform
Bromomethane
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
Chlorodibromomethane
1,2-Dibromo-3-Chloropropane
Ethylene Dibromide
Dibromomethane
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
Hexachlorobutadiene
Isopropylbenzene
4-Isopropyltoluene
Methylene Chloride
Naphthalene
N-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
TestAmerica Tampa
Analysis Batch: 660-65433
Result (ug/L)
0.50
0.58
0.44
0.58
0.35
0.58
2.5
0.67
0.63
0.84
0.42
0.63
2.5
0.90
1.0
0.65
0.52
0.34
2.5
0.50
0.41
0.64
0.52
2.5
0.52
0.57
0.45
0.65
0.44
0.52
0.39
0.36
0.31
0.14
0.14
0.44
0.40
0.19
0.69
4.0
2.5
0.59
0.98
0.63
Page 12 of 45
Instrument ID:
BVMH GC/MS
Lab File ID:
1HG2927.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
MDL
0.50
0.58
0.44
0.58
0.35
0.58
2.5
0.67
0.63
0.84
0.42
0.63
2.5
0.90
1.0
0.65
0.52
0.34
2.5
0.50
0.41
0.64
0.52
2.5
0.52
0.57
0.45
0.65
0.44
0.52
0.39
0.36
0.31
0.14
0.14
0.44
0.40
0.19
0.69
4.0
2.5
0.59
0.98
0.63
PQL
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
4.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
5.0
1.0
2.0
1.0
Analytical Data
Client: ARCADIS U.S., Inc.
Job Number: 660-24325-1
Client Sample ID:
CP-108 (28'-30')_072808
Lab Sample ID:
Client Matrix:
660-24325-3
Water
Date Sampled:
Date Received:
07/28/2008 1151
07/29/2008 0945
8260B Volatile Organic Compounds by GC/MS
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260B
5030B
1.0
07/29/2008 1750
07/29/2008 1750
Analyte
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
o-Xylene
Acetone
2-Butanone (MEK)
4-Methyl-2-pentanone (MIBK)
Carbon disulfide
2-Hexanone
Methyl tert-butyl ether
m-Xylene & p-Xylene
Surrogate
Toluene-d8 (Surr)
4-Bromofluorobenzene
Dibromofluoromethane
TestAmerica Tampa
Analysis Batch: 660-65433
Result (ug/L)
0.15
0.50
0.51
0.77
0.58
0.46
0.47
0.50
2.5
0.18
0.86
0.54
0.50
0.50
9.9
8.4
3.8
0.85
4.4
0.44
0.60
%Rec
111
99
107
Page 13 of 45
Instrument ID:
BVMH GC/MS
Lab File ID:
1HG2927.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
MDL
0.15
0.50
0.51
0.77
0.58
0.46
0.47
0.50
2.5
0.18
0.86
0.54
0.50
0.50
9.9
8.4
3.8
0.85
4.4
0.44
0.60
PQL
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
20
10
10
1.0
10
1.0
2.0
Acceptance Limits
77 - 122
74 - 126
70 - 130
Analytical Data
Client: ARCADIS U.S., Inc.
Job Number: 660-24325-1
Client Sample ID:
CP-108 (38'-40')_072808
Lab Sample ID:
Client Matrix:
660-24325-4
Water
Date Sampled:
Date Received:
07/28/2008 1230
07/29/2008 0945
8260B Volatile Organic Compounds by GC/MS
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260B
5030B
1.0
07/29/2008 1730
07/29/2008 1730
Analyte
Benzene
Bromobenzene
1,2-Dichlorobenzene
Chlorobromomethane
Dichlorobromomethane
Bromoform
Bromomethane
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
Chlorodibromomethane
1,2-Dibromo-3-Chloropropane
Ethylene Dibromide
Dibromomethane
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
Hexachlorobutadiene
Isopropylbenzene
4-Isopropyltoluene
Methylene Chloride
Naphthalene
N-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
TestAmerica Tampa
Analysis Batch: 660-65433
Result (ug/L)
0.50
0.58
0.44
0.58
0.35
0.58
2.5
0.67
0.63
0.84
0.42
0.63
2.5
0.90
1.0
0.65
0.52
0.34
2.5
0.50
0.41
0.64
0.52
2.5
0.52
0.57
0.45
0.65
0.44
0.52
0.39
0.36
0.31
0.14
0.14
0.44
0.40
0.19
0.69
4.0
2.5
0.59
0.98
0.63
Page 14 of 45
Instrument ID:
BVMH GC/MS
Lab File ID:
1HG2926.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
MDL
0.50
0.58
0.44
0.58
0.35
0.58
2.5
0.67
0.63
0.84
0.42
0.63
2.5
0.90
1.0
0.65
0.52
0.34
2.5
0.50
0.41
0.64
0.52
2.5
0.52
0.57
0.45
0.65
0.44
0.52
0.39
0.36
0.31
0.14
0.14
0.44
0.40
0.19
0.69
4.0
2.5
0.59
0.98
0.63
PQL
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
4.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
5.0
1.0
2.0
1.0
Analytical Data
Client: ARCADIS U.S., Inc.
Job Number: 660-24325-1
Client Sample ID:
CP-108 (38'-40')_072808
Lab Sample ID:
Client Matrix:
660-24325-4
Water
Date Sampled:
Date Received:
07/28/2008 1230
07/29/2008 0945
8260B Volatile Organic Compounds by GC/MS
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260B
5030B
1.0
07/29/2008 1730
07/29/2008 1730
Analyte
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
o-Xylene
Acetone
2-Butanone (MEK)
4-Methyl-2-pentanone (MIBK)
Carbon disulfide
2-Hexanone
Methyl tert-butyl ether
m-Xylene & p-Xylene
Surrogate
Toluene-d8 (Surr)
4-Bromofluorobenzene
Dibromofluoromethane
TestAmerica Tampa
Analysis Batch: 660-65433
Result (ug/L)
0.15
0.50
0.78
0.77
0.58
0.46
0.47
0.50
2.5
0.18
0.86
0.54
0.50
0.50
9.9
8.4
3.8
0.85
4.4
0.44
0.60
%Rec
116
100
110
Page 15 of 45
Instrument ID:
BVMH GC/MS
Lab File ID:
1HG2926.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
U
U
I
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
MDL
0.15
0.50
0.51
0.77
0.58
0.46
0.47
0.50
2.5
0.18
0.86
0.54
0.50
0.50
9.9
8.4
3.8
0.85
4.4
0.44
0.60
PQL
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
20
10
10
1.0
10
1.0
2.0
Acceptance Limits
77 - 122
74 - 126
70 - 130
Analytical Data
Client: ARCADIS U.S., Inc.
Job Number: 660-24325-1
Client Sample ID:
CP-108 (48'-50')_072808
Lab Sample ID:
Client Matrix:
660-24325-5
Water
Date Sampled:
Date Received:
07/28/2008 1258
07/29/2008 0945
8260B Volatile Organic Compounds by GC/MS
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260B
5030B
1.0
07/29/2008 1710
07/29/2008 1710
Analyte
Benzene
Bromobenzene
1,2-Dichlorobenzene
Chlorobromomethane
Dichlorobromomethane
Bromoform
Bromomethane
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
Chlorodibromomethane
1,2-Dibromo-3-Chloropropane
Ethylene Dibromide
Dibromomethane
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
Hexachlorobutadiene
Isopropylbenzene
4-Isopropyltoluene
Methylene Chloride
Naphthalene
N-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
TestAmerica Tampa
Analysis Batch: 660-65433
Result (ug/L)
0.50
0.58
0.44
0.58
0.35
0.58
2.5
0.67
0.63
0.84
0.42
0.63
2.5
0.90
1.0
0.65
0.52
0.34
2.5
0.50
0.41
0.64
0.52
2.5
0.52
0.57
0.45
0.65
0.44
0.52
0.39
0.36
0.31
0.14
0.14
0.44
0.40
0.19
0.69
4.0
2.5
0.59
0.98
0.63
Page 16 of 45
Instrument ID:
BVMH GC/MS
Lab File ID:
1HG2925.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
MDL
0.50
0.58
0.44
0.58
0.35
0.58
2.5
0.67
0.63
0.84
0.42
0.63
2.5
0.90
1.0
0.65
0.52
0.34
2.5
0.50
0.41
0.64
0.52
2.5
0.52
0.57
0.45
0.65
0.44
0.52
0.39
0.36
0.31
0.14
0.14
0.44
0.40
0.19
0.69
4.0
2.5
0.59
0.98
0.63
PQL
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
4.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
5.0
1.0
2.0
1.0
Analytical Data
Client: ARCADIS U.S., Inc.
Job Number: 660-24325-1
Client Sample ID:
CP-108 (48'-50')_072808
Lab Sample ID:
Client Matrix:
660-24325-5
Water
Date Sampled:
Date Received:
07/28/2008 1258
07/29/2008 0945
8260B Volatile Organic Compounds by GC/MS
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260B
5030B
1.0
07/29/2008 1710
07/29/2008 1710
Analyte
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
o-Xylene
Acetone
2-Butanone (MEK)
4-Methyl-2-pentanone (MIBK)
Carbon disulfide
2-Hexanone
Methyl tert-butyl ether
m-Xylene & p-Xylene
Surrogate
Toluene-d8 (Surr)
4-Bromofluorobenzene
Dibromofluoromethane
TestAmerica Tampa
Analysis Batch: 660-65433
Result (ug/L)
0.15
0.50
0.51
0.77
0.58
0.46
0.47
0.50
2.5
0.18
0.86
0.54
0.50
0.50
9.9
8.4
3.8
0.85
4.4
0.44
0.60
%Rec
128
112
122
Page 17 of 45
Instrument ID:
BVMH GC/MS
Lab File ID:
1HG2925.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
J1
MDL
0.15
0.50
0.51
0.77
0.58
0.46
0.47
0.50
2.5
0.18
0.86
0.54
0.50
0.50
9.9
8.4
3.8
0.85
4.4
0.44
0.60
PQL
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
20
10
10
1.0
10
1.0
2.0
Acceptance Limits
77 - 122
74 - 126
70 - 130
Analytical Data
Client: ARCADIS U.S., Inc.
Job Number: 660-24325-1
Client Sample ID:
CP-108 (61'-63')_072808
Lab Sample ID:
Client Matrix:
660-24325-6
Water
Date Sampled:
Date Received:
07/28/2008 1434
07/29/2008 0945
8260B Volatile Organic Compounds by GC/MS
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260B
5030B
1.0
07/29/2008 1650
07/29/2008 1650
Analyte
Benzene
Bromobenzene
1,2-Dichlorobenzene
Chlorobromomethane
Dichlorobromomethane
Bromoform
Bromomethane
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
Chlorodibromomethane
1,2-Dibromo-3-Chloropropane
Ethylene Dibromide
Dibromomethane
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
Hexachlorobutadiene
Isopropylbenzene
4-Isopropyltoluene
Methylene Chloride
Naphthalene
N-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
TestAmerica Tampa
Analysis Batch: 660-65433
Result (ug/L)
0.50
0.58
0.44
0.58
0.35
0.58
2.5
0.67
0.63
0.84
0.42
0.63
2.5
0.90
1.0
0.65
0.52
0.34
2.5
0.50
0.41
0.64
0.52
2.5
0.52
0.57
0.45
0.65
0.44
0.52
0.39
0.36
0.31
0.14
0.14
0.44
0.40
0.19
0.69
4.0
2.5
0.59
0.98
0.63
Page 18 of 45
Instrument ID:
BVMH GC/MS
Lab File ID:
1HG2924.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
MDL
0.50
0.58
0.44
0.58
0.35
0.58
2.5
0.67
0.63
0.84
0.42
0.63
2.5
0.90
1.0
0.65
0.52
0.34
2.5
0.50
0.41
0.64
0.52
2.5
0.52
0.57
0.45
0.65
0.44
0.52
0.39
0.36
0.31
0.14
0.14
0.44
0.40
0.19
0.69
4.0
2.5
0.59
0.98
0.63
PQL
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
4.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
5.0
1.0
2.0
1.0
Analytical Data
Client: ARCADIS U.S., Inc.
Job Number: 660-24325-1
Client Sample ID:
CP-108 (61'-63')_072808
Lab Sample ID:
Client Matrix:
660-24325-6
Water
Date Sampled:
Date Received:
07/28/2008 1434
07/29/2008 0945
8260B Volatile Organic Compounds by GC/MS
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260B
5030B
1.0
07/29/2008 1650
07/29/2008 1650
Analyte
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
o-Xylene
Acetone
2-Butanone (MEK)
4-Methyl-2-pentanone (MIBK)
Carbon disulfide
2-Hexanone
Methyl tert-butyl ether
m-Xylene & p-Xylene
Surrogate
Toluene-d8 (Surr)
4-Bromofluorobenzene
Dibromofluoromethane
TestAmerica Tampa
Analysis Batch: 660-65433
Result (ug/L)
0.15
0.50
0.63
0.77
0.58
0.46
0.47
0.50
2.5
0.18
0.86
0.54
0.50
0.50
9.9
8.4
3.8
0.85
4.4
0.44
0.60
%Rec
121
104
118
Page 19 of 45
Instrument ID:
BVMH GC/MS
Lab File ID:
1HG2924.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
U
U
I
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
MDL
0.15
0.50
0.51
0.77
0.58
0.46
0.47
0.50
2.5
0.18
0.86
0.54
0.50
0.50
9.9
8.4
3.8
0.85
4.4
0.44
0.60
PQL
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
20
10
10
1.0
10
1.0
2.0
Acceptance Limits
77 - 122
74 - 126
70 - 130
Analytical Data
Client: ARCADIS U.S., Inc.
Job Number: 660-24325-1
Client Sample ID:
CP-108 (69'-71')_072808
Lab Sample ID:
Client Matrix:
660-24325-7
Water
Date Sampled:
Date Received:
07/28/2008 1519
07/29/2008 0945
8260B Volatile Organic Compounds by GC/MS
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260B
5030B
1.0
07/29/2008 1629
07/29/2008 1629
Analyte
Benzene
Bromobenzene
1,2-Dichlorobenzene
Chlorobromomethane
Dichlorobromomethane
Bromoform
Bromomethane
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
Chlorodibromomethane
1,2-Dibromo-3-Chloropropane
Ethylene Dibromide
Dibromomethane
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
Hexachlorobutadiene
Isopropylbenzene
4-Isopropyltoluene
Methylene Chloride
Naphthalene
N-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
TestAmerica Tampa
Analysis Batch: 660-65433
Result (ug/L)
0.50
0.58
0.44
0.58
0.35
0.58
2.5
0.67
0.63
0.84
0.42
0.63
2.5
0.90
1.0
0.65
0.52
0.34
2.5
0.50
0.41
0.64
0.52
2.5
0.52
0.57
0.45
0.65
0.44
0.52
0.39
0.36
0.31
0.14
0.14
0.44
0.40
0.19
0.69
4.0
2.5
0.59
0.98
0.63
Page 20 of 45
Instrument ID:
BVMH GC/MS
Lab File ID:
1HG2923.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
MDL
0.50
0.58
0.44
0.58
0.35
0.58
2.5
0.67
0.63
0.84
0.42
0.63
2.5
0.90
1.0
0.65
0.52
0.34
2.5
0.50
0.41
0.64
0.52
2.5
0.52
0.57
0.45
0.65
0.44
0.52
0.39
0.36
0.31
0.14
0.14
0.44
0.40
0.19
0.69
4.0
2.5
0.59
0.98
0.63
PQL
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
4.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
5.0
1.0
2.0
1.0
Analytical Data
Client: ARCADIS U.S., Inc.
Job Number: 660-24325-1
Client Sample ID:
CP-108 (69'-71')_072808
Lab Sample ID:
Client Matrix:
660-24325-7
Water
Date Sampled:
Date Received:
07/28/2008 1519
07/29/2008 0945
8260B Volatile Organic Compounds by GC/MS
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260B
5030B
1.0
07/29/2008 1629
07/29/2008 1629
Analyte
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
o-Xylene
Acetone
2-Butanone (MEK)
4-Methyl-2-pentanone (MIBK)
Carbon disulfide
2-Hexanone
Methyl tert-butyl ether
m-Xylene & p-Xylene
Surrogate
Toluene-d8 (Surr)
4-Bromofluorobenzene
Dibromofluoromethane
TestAmerica Tampa
Analysis Batch: 660-65433
Result (ug/L)
0.15
0.50
0.51
0.77
0.58
0.46
0.47
0.50
2.5
0.18
0.86
0.54
0.50
0.50
9.9
8.4
3.8
0.85
4.4
0.44
0.60
%Rec
113
99
107
Page 21 of 45
Instrument ID:
BVMH GC/MS
Lab File ID:
1HG2923.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
MDL
0.15
0.50
0.51
0.77
0.58
0.46
0.47
0.50
2.5
0.18
0.86
0.54
0.50
0.50
9.9
8.4
3.8
0.85
4.4
0.44
0.60
PQL
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
20
10
10
1.0
10
1.0
2.0
Acceptance Limits
77 - 122
74 - 126
70 - 130
Analytical Data
Client: ARCADIS U.S., Inc.
Job Number: 660-24325-1
Client Sample ID:
CP-106 (10'-12')_072908
Lab Sample ID:
Client Matrix:
660-24325-8
Water
Date Sampled:
Date Received:
07/29/2008 0808
07/29/2008 0945
8260B Volatile Organic Compounds by GC/MS
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260B
5030B
1.0
07/29/2008 1811
07/29/2008 1811
Analyte
Benzene
Bromobenzene
1,2-Dichlorobenzene
Chlorobromomethane
Dichlorobromomethane
Bromoform
Bromomethane
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
Chlorodibromomethane
1,2-Dibromo-3-Chloropropane
Ethylene Dibromide
Dibromomethane
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
Hexachlorobutadiene
Isopropylbenzene
4-Isopropyltoluene
Methylene Chloride
Naphthalene
N-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
TestAmerica Tampa
Analysis Batch: 660-65433
Result (ug/L)
0.50
0.58
0.44
0.58
0.35
0.58
2.5
0.67
0.63
0.84
0.42
0.63
2.5
0.90
1.0
0.65
0.52
0.34
2.5
0.50
0.41
0.64
0.52
2.5
0.52
0.57
0.45
0.65
0.44
0.52
0.39
0.36
0.31
0.14
0.14
0.44
0.40
0.19
0.69
4.0
2.5
0.59
0.98
0.63
Page 22 of 45
Instrument ID:
BVMH GC/MS
Lab File ID:
1HG2928.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
MDL
0.50
0.58
0.44
0.58
0.35
0.58
2.5
0.67
0.63
0.84
0.42
0.63
2.5
0.90
1.0
0.65
0.52
0.34
2.5
0.50
0.41
0.64
0.52
2.5
0.52
0.57
0.45
0.65
0.44
0.52
0.39
0.36
0.31
0.14
0.14
0.44
0.40
0.19
0.69
4.0
2.5
0.59
0.98
0.63
PQL
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
4.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
5.0
1.0
2.0
1.0
Analytical Data
Client: ARCADIS U.S., Inc.
Job Number: 660-24325-1
Client Sample ID:
CP-106 (10'-12')_072908
Lab Sample ID:
Client Matrix:
660-24325-8
Water
Date Sampled:
Date Received:
07/29/2008 0808
07/29/2008 0945
8260B Volatile Organic Compounds by GC/MS
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260B
5030B
1.0
07/29/2008 1811
07/29/2008 1811
Analyte
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
o-Xylene
Acetone
2-Butanone (MEK)
4-Methyl-2-pentanone (MIBK)
Carbon disulfide
2-Hexanone
Methyl tert-butyl ether
m-Xylene & p-Xylene
Surrogate
Toluene-d8 (Surr)
4-Bromofluorobenzene
Dibromofluoromethane
TestAmerica Tampa
Analysis Batch: 660-65433
Result (ug/L)
0.15
0.50
0.51
0.77
0.58
0.46
0.47
0.50
2.5
0.18
0.86
0.54
0.50
0.50
9.9
8.4
3.8
0.85
4.4
0.44
0.60
%Rec
114
102
111
Page 23 of 45
Instrument ID:
BVMH GC/MS
Lab File ID:
1HG2928.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
MDL
0.15
0.50
0.51
0.77
0.58
0.46
0.47
0.50
2.5
0.18
0.86
0.54
0.50
0.50
9.9
8.4
3.8
0.85
4.4
0.44
0.60
PQL
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
20
10
10
1.0
10
1.0
2.0
Acceptance Limits
77 - 122
74 - 126
70 - 130
Analytical Data
Client: ARCADIS U.S., Inc.
Job Number: 660-24325-1
Client Sample ID:
CP-106 (24'-26')_072908
Lab Sample ID:
Client Matrix:
660-24325-9
Water
Date Sampled:
Date Received:
07/29/2008 0830
07/29/2008 0945
8260B Volatile Organic Compounds by GC/MS
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260B
5030B
1.0
07/29/2008 1831
07/29/2008 1831
Analyte
Benzene
Bromobenzene
1,2-Dichlorobenzene
Chlorobromomethane
Dichlorobromomethane
Bromoform
Bromomethane
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
Chlorodibromomethane
1,2-Dibromo-3-Chloropropane
Ethylene Dibromide
Dibromomethane
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
Hexachlorobutadiene
Isopropylbenzene
4-Isopropyltoluene
Methylene Chloride
Naphthalene
N-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
TestAmerica Tampa
Analysis Batch: 660-65433
Result (ug/L)
0.50
0.58
0.44
0.58
0.35
0.58
2.5
0.67
0.63
0.84
0.42
0.63
2.5
0.90
1.0
0.65
0.52
0.34
2.5
0.50
0.41
0.64
0.52
2.5
0.52
0.57
0.45
0.65
0.44
0.52
0.39
0.36
0.31
0.14
0.14
0.44
0.40
0.19
0.69
4.0
2.5
0.59
0.98
0.63
Page 24 of 45
Instrument ID:
BVMH GC/MS
Lab File ID:
1HG2929.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
MDL
0.50
0.58
0.44
0.58
0.35
0.58
2.5
0.67
0.63
0.84
0.42
0.63
2.5
0.90
1.0
0.65
0.52
0.34
2.5
0.50
0.41
0.64
0.52
2.5
0.52
0.57
0.45
0.65
0.44
0.52
0.39
0.36
0.31
0.14
0.14
0.44
0.40
0.19
0.69
4.0
2.5
0.59
0.98
0.63
PQL
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
4.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
5.0
1.0
2.0
1.0
Analytical Data
Client: ARCADIS U.S., Inc.
Job Number: 660-24325-1
Client Sample ID:
CP-106 (24'-26')_072908
Lab Sample ID:
Client Matrix:
660-24325-9
Water
Date Sampled:
Date Received:
07/29/2008 0830
07/29/2008 0945
8260B Volatile Organic Compounds by GC/MS
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260B
5030B
1.0
07/29/2008 1831
07/29/2008 1831
Analyte
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
o-Xylene
Acetone
2-Butanone (MEK)
4-Methyl-2-pentanone (MIBK)
Carbon disulfide
2-Hexanone
Methyl tert-butyl ether
m-Xylene & p-Xylene
Surrogate
Toluene-d8 (Surr)
4-Bromofluorobenzene
Dibromofluoromethane
TestAmerica Tampa
Analysis Batch: 660-65433
Result (ug/L)
0.15
0.50
0.51
0.77
0.58
0.46
0.47
0.50
2.5
0.18
0.86
0.54
0.50
0.50
9.9
8.4
3.8
0.85
4.4
0.44
0.60
%Rec
116
102
116
Page 25 of 45
Instrument ID:
BVMH GC/MS
Lab File ID:
1HG2929.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
MDL
0.15
0.50
0.51
0.77
0.58
0.46
0.47
0.50
2.5
0.18
0.86
0.54
0.50
0.50
9.9
8.4
3.8
0.85
4.4
0.44
0.60
PQL
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
20
10
10
1.0
10
1.0
2.0
Acceptance Limits
77 - 122
74 - 126
70 - 130
Analytical Data
Client: ARCADIS U.S., Inc.
Job Number: 660-24325-1
Client Sample ID:
Trip Blank (7/28/08)#2_072808
Lab Sample ID:
Client Matrix:
660-24325-1
Water
Date Sampled:
Date Received:
07/28/2008 0000
07/29/2008 0945
8260C SIM/ID 1,4-Dioxane by SIM/Isotopic Dilution
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260C SIM/ID
5030B
1.0
07/29/2008 1348
07/29/2008 1348
Analyte
1,4-Dioxane
TestAmerica Tampa
Analysis Batch: 660-65431
Result (ug/L)
0.54
Page 26 of 45
Instrument ID:
BVMH GC/MS
Lab File ID:
1HG2915.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
U
MDL
0.54
PQL
1.0
Analytical Data
Client: ARCADIS U.S., Inc.
Job Number: 660-24325-1
Client Sample ID:
CP-108 (10'-12')_072808
Lab Sample ID:
Client Matrix:
660-24325-2
Water
Date Sampled:
Date Received:
07/28/2008 1122
07/29/2008 0945
8260C SIM/ID 1,4-Dioxane by SIM/Isotopic Dilution
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260C SIM/ID
5030B
1.0
07/29/2008 1609
07/29/2008 1609
Analyte
1,4-Dioxane
TestAmerica Tampa
Analysis Batch: 660-65431
Result (ug/L)
0.54
Page 27 of 45
Instrument ID:
BVMH GC/MS
Lab File ID:
1HG2922.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
U
MDL
0.54
PQL
1.0
Analytical Data
Client: ARCADIS U.S., Inc.
Job Number: 660-24325-1
Client Sample ID:
CP-108 (28'-30')_072808
Lab Sample ID:
Client Matrix:
660-24325-3
Water
Date Sampled:
Date Received:
07/28/2008 1151
07/29/2008 0945
8260C SIM/ID 1,4-Dioxane by SIM/Isotopic Dilution
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260C SIM/ID
5030B
1.0
07/29/2008 1750
07/29/2008 1750
Analyte
1,4-Dioxane
TestAmerica Tampa
Analysis Batch: 660-65431
Result (ug/L)
0.54
Page 28 of 45
Instrument ID:
BVMH GC/MS
Lab File ID:
1HG2927.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
U
MDL
0.54
PQL
1.0
Analytical Data
Client: ARCADIS U.S., Inc.
Job Number: 660-24325-1
Client Sample ID:
CP-108 (38'-40')_072808
Lab Sample ID:
Client Matrix:
660-24325-4
Water
Date Sampled:
Date Received:
07/28/2008 1230
07/29/2008 0945
8260C SIM/ID 1,4-Dioxane by SIM/Isotopic Dilution
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260C SIM/ID
5030B
1.0
07/29/2008 1730
07/29/2008 1730
Analyte
1,4-Dioxane
TestAmerica Tampa
Analysis Batch: 660-65431
Result (ug/L)
0.54
Page 29 of 45
Instrument ID:
BVMH GC/MS
Lab File ID:
1HG2926.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
U
MDL
0.54
PQL
1.0
Analytical Data
Client: ARCADIS U.S., Inc.
Job Number: 660-24325-1
Client Sample ID:
CP-108 (48'-50')_072808
Lab Sample ID:
Client Matrix:
660-24325-5
Water
Date Sampled:
Date Received:
07/28/2008 1258
07/29/2008 0945
8260C SIM/ID 1,4-Dioxane by SIM/Isotopic Dilution
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260C SIM/ID
5030B
1.0
07/29/2008 1710
07/29/2008 1710
Analyte
1,4-Dioxane
TestAmerica Tampa
Analysis Batch: 660-65431
Result (ug/L)
0.54
Page 30 of 45
Instrument ID:
BVMH GC/MS
Lab File ID:
1HG2925.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
U
MDL
0.54
PQL
1.0
Analytical Data
Client: ARCADIS U.S., Inc.
Job Number: 660-24325-1
Client Sample ID:
CP-108 (61'-63')_072808
Lab Sample ID:
Client Matrix:
660-24325-6
Water
Date Sampled:
Date Received:
07/28/2008 1434
07/29/2008 0945
8260C SIM/ID 1,4-Dioxane by SIM/Isotopic Dilution
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260C SIM/ID
5030B
1.0
07/29/2008 1650
07/29/2008 1650
Analyte
1,4-Dioxane
TestAmerica Tampa
Analysis Batch: 660-65431
Result (ug/L)
0.54
Page 31 of 45
Instrument ID:
BVMH GC/MS
Lab File ID:
1HG2924.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
U
MDL
0.54
PQL
1.0
Analytical Data
Client: ARCADIS U.S., Inc.
Job Number: 660-24325-1
Client Sample ID:
CP-108 (69'-71')_072808
Lab Sample ID:
Client Matrix:
660-24325-7
Water
Date Sampled:
Date Received:
07/28/2008 1519
07/29/2008 0945
8260C SIM/ID 1,4-Dioxane by SIM/Isotopic Dilution
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260C SIM/ID
5030B
1.0
07/29/2008 1629
07/29/2008 1629
Analyte
1,4-Dioxane
TestAmerica Tampa
Analysis Batch: 660-65431
Result (ug/L)
0.54
Page 32 of 45
Instrument ID:
BVMH GC/MS
Lab File ID:
1HG2923.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
U
MDL
0.54
PQL
1.0
Analytical Data
Client: ARCADIS U.S., Inc.
Job Number: 660-24325-1
Client Sample ID:
CP-106 (10'-12')_072908
Lab Sample ID:
Client Matrix:
660-24325-8
Water
Date Sampled:
Date Received:
07/29/2008 0808
07/29/2008 0945
8260C SIM/ID 1,4-Dioxane by SIM/Isotopic Dilution
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260C SIM/ID
5030B
1.0
07/29/2008 1811
07/29/2008 1811
Analyte
1,4-Dioxane
TestAmerica Tampa
Analysis Batch: 660-65431
Result (ug/L)
0.54
Page 33 of 45
Instrument ID:
BVMH GC/MS
Lab File ID:
1HG2928.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
U
MDL
0.54
PQL
1.0
Analytical Data
Client: ARCADIS U.S., Inc.
Job Number: 660-24325-1
Client Sample ID:
CP-106 (24'-26')_072908
Lab Sample ID:
Client Matrix:
660-24325-9
Water
Date Sampled:
Date Received:
07/29/2008 0830
07/29/2008 0945
8260C SIM/ID 1,4-Dioxane by SIM/Isotopic Dilution
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260C SIM/ID
5030B
1.0
07/29/2008 1831
07/29/2008 1831
Analyte
1,4-Dioxane
TestAmerica Tampa
Analysis Batch: 660-65431
Result (ug/L)
0.54
Page 34 of 45
Instrument ID:
BVMH GC/MS
Lab File ID:
1HG2929.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
Qualifier
U
MDL
0.54
PQL
1.0
DATA REPORTING QUALIFIERS
Client: ARCADIS U.S., Inc.
Lab Section
Job Number: 660-24325-1
Qualifier
Description
J1
Estimated value; value may not be accurate. Surrogate
recovery outside of criteria.
U
Indicates that the compound was analyzed for but not
detected.
I
The reported value is between the laboratory method
detection limit and the laboratory practical quantitation limit.
GC/MS VOA
TestAmerica Tampa
Page 35 of 45
QUALITY CONTROL RESULTS
TestAmerica Tampa
Page 36 of 45
Quality Control Results
Client: ARCADIS U.S., Inc.
Job Number: 660-24325-1
Surrogate Recovery Report
8260B Volatile Organic Compounds by GC/MS
Client Matrix: Water
TOL
%Rec
BFB
%Rec
DBFM
%Rec
109
97
104
111
121
111
99
107
116
100
110
128J1
112
122
121
104
118
113
99
107
114
102
111
116
102
116
MB 660-65433/3
112
100
106
LCS 660-65433/1
110
96
104
LCSD 660-65433/2
113
97
104
660-24324-A-1 MS
109
93
108
660-24324-B-1 MSD
109
91
107
Lab Sample ID
Client Sample ID
660-24325-1
Trip Blank
(7/28/08)#2_072808
CP-108
(10'-12')_072808
CP-108
(28'-30')_072808
CP-108
(38'-40')_072808
CP-108
(48'-50')_072808
CP-108
(61'-63')_072808
CP-108
(69'-71')_072808
CP-106
(10'-12')_072908
CP-106
(24'-26')_072908
660-24325-2
660-24325-3
660-24325-4
660-24325-5
660-24325-6
660-24325-7
660-24325-8
660-24325-9
Surrogate
TOL = Toluene-d8 (Surr)
BFB = 4-Bromofluorobenzene
DBFM = Dibromofluoromethane
129J1
Acceptance Limits
77-122
74-126
70-130
TestAmerica Tampa
Page 37 of 45
Quality Control Results
Client: ARCADIS U.S., Inc.
Job Number: 660-24325-1
Method Blank - Batch: 660-65433
Lab Sample ID:
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
MB 660-65433/3
Water
1.0
07/29/2008 1227
07/29/2008 1227
Method: 8260B
Preparation: 5030B
Analysis Batch: 660-65433
Prep Batch: N/A
Units: ug/L
Instrument ID: BVMH GC/MS
Lab File ID:
1HG2911.D
Initial Weight/Volume: 5 mL
Final Weight/Volume: 5 mL
Analyte
Result
Qual
MDL
PQL
Benzene
Bromobenzene
1,2-Dichlorobenzene
Chlorobromomethane
Dichlorobromomethane
Bromoform
Bromomethane
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
Chlorodibromomethane
1,2-Dibromo-3-Chloropropane
Ethylene Dibromide
Dibromomethane
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
Hexachlorobutadiene
Isopropylbenzene
4-Isopropyltoluene
Methylene Chloride
Naphthalene
0.50
0.58
0.44
0.58
0.35
0.58
2.5
0.67
0.63
0.84
0.42
0.63
2.5
0.90
1.0
0.65
0.52
0.34
2.5
0.50
0.41
0.64
0.52
2.5
0.52
0.57
0.45
0.65
0.44
0.52
0.39
0.36
0.31
0.14
0.14
0.44
0.40
0.19
0.69
4.0
2.5
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
0.50
0.58
0.44
0.58
0.35
0.58
2.5
0.67
0.63
0.84
0.42
0.63
2.5
0.90
1.0
0.65
0.52
0.34
2.5
0.50
0.41
0.64
0.52
2.5
0.52
0.57
0.45
0.65
0.44
0.52
0.39
0.36
0.31
0.14
0.14
0.44
0.40
0.19
0.69
4.0
2.5
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
4.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
5.0
Calculations are performed before rounding to avoid round-off errors in calculated results.
TestAmerica Tampa
Page 38 of 45
Quality Control Results
Client: ARCADIS U.S., Inc.
Job Number: 660-24325-1
Method Blank - Batch: 660-65433
Lab Sample ID:
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
MB 660-65433/3
Water
1.0
07/29/2008 1227
07/29/2008 1227
Method: 8260B
Preparation: 5030B
Analysis Batch: 660-65433
Prep Batch: N/A
Units: ug/L
Instrument ID: BVMH GC/MS
Lab File ID:
1HG2911.D
Initial Weight/Volume: 5 mL
Final Weight/Volume: 5 mL
Analyte
Result
Qual
MDL
PQL
N-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
o-Xylene
Acetone
2-Butanone (MEK)
4-Methyl-2-pentanone (MIBK)
Carbon disulfide
2-Hexanone
Methyl tert-butyl ether
m-Xylene & p-Xylene
0.59
0.98
0.63
0.15
0.50
0.51
0.77
0.58
0.46
0.47
0.50
2.5
0.18
0.86
0.54
0.50
0.50
9.9
8.4
3.8
0.85
4.4
0.44
0.60
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
0.59
0.98
0.63
0.15
0.50
0.51
0.77
0.58
0.46
0.47
0.50
2.5
0.18
0.86
0.54
0.50
0.50
9.9
8.4
3.8
0.85
4.4
0.44
0.60
1.0
2.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
20
10
10
1.0
10
1.0
2.0
Surrogate
Toluene-d8 (Surr)
4-Bromofluorobenzene
Dibromofluoromethane
% Rec
Acceptance Limits
112
100
106
77 - 122
74 - 126
70 - 130
Calculations are performed before rounding to avoid round-off errors in calculated results.
TestAmerica Tampa
Page 39 of 45
Quality Control Results
Client: ARCADIS U.S., Inc.
Job Number: 660-24325-1
Lab Control Spike/
Lab Control Spike Duplicate Recovery Report - Batch: 660-65433
Method: 8260B
Preparation: 5030B
LCS Lab Sample ID: LCS 660-65433/1
Client Matrix:
Water
Dilution:
1.0
07/29/2008 1127
Date Analyzed:
07/29/2008 1127
Date Prepared:
Analysis Batch: 660-65433
Prep Batch: N/A
Units: ug/L
Instrument ID: BVMH GC/MS
Lab File ID:
1HG2908.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
LCSD Lab Sample ID: LCSD 660-65433/2
Client Matrix:
Water
Dilution:
1.0
07/29/2008 1147
Date Analyzed:
07/29/2008 1147
Date Prepared:
Analysis Batch: 660-65433
Prep Batch: N/A
Units: ug/L
Instrument ID:
BVMH GC/MS
Lab File ID:
1HG2909.D
Initial Weight/Volume: 5 mL
Final Weight/Volume: 5 mL
Analyte
LCS
Benzene
Chlorobenzene
1,1-Dichloroethene
Toluene
Trichloroethene
108
109
114
108
110
% Rec.
LCSD
103
105
107
105
103
Limit
RPD
RPD Limit
62 - 135
72 - 127
46 - 147
68 - 131
56 - 143
5
4
6
2
7
37
22
30
33
35
Calculations are performed before rounding to avoid round-off errors in calculated results.
TestAmerica Tampa
Page 40 of 45
LCS Qual LCSD Qual
Quality Control Results
Client: ARCADIS U.S., Inc.
Job Number: 660-24325-1
Matrix Spike/
Matrix Spike Duplicate Recovery Report - Batch: 660-65433
Method: 8260B
Preparation: 5030B
MS Lab Sample ID:
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
660-24324-A-1 MS
Water
1.0
07/29/2008 2012
07/29/2008 2012
Analysis Batch: 660-65433
Prep Batch: N/A
Instrument ID: BVMH GC/MS
Lab File ID:
1HG2934.D
Initial Weight/Volume: 5 mL
Final Weight/Volume: 5 mL
MSD Lab Sample ID:
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
660-24324-B-1 MSD
Water
1.0
07/29/2008 2032
07/29/2008 2032
Analysis Batch: 660-65433
Prep Batch: N/A
Instrument ID: BVMH GC/MS
Lab File ID:
1HG2935.D
Initial Weight/Volume: 5 mL
Final Weight/Volume: 5 mL
Analyte
MS
Benzene
Chlorobenzene
1,1-Dichloroethene
Toluene
Trichloroethene
111
108
116
107
117
% Rec.
MSD
111
108
112
108
115
Limit
RPD
RPD Limit
62 - 135
72 - 127
46 - 147
68 - 131
56 - 143
0
0
3
1
1
37
22
30
33
35
Calculations are performed before rounding to avoid round-off errors in calculated results.
TestAmerica Tampa
Page 41 of 45
MS Qual MSD Qual
Quality Control Results
Client: ARCADIS U.S., Inc.
Job Number: 660-24325-1
Method Blank - Batch: 660-65431
Lab Sample ID:
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
MB 660-65431/3
Water
1.0
07/29/2008 1227
07/29/2008 1227
Method: 8260C SIM/ID
Preparation: 5030B
Analysis Batch: 660-65431
Prep Batch: N/A
Units: ug/L
Instrument ID: BVMH GC/MS
Lab File ID:
1HG2911.D
Initial Weight/Volume: 5 mL
Final Weight/Volume: 5 mL
Analyte
Result
Qual
MDL
PQL
1,4-Dioxane
0.54
U
0.54
1.0
Lab Control Spike/
Lab Control Spike Duplicate Recovery Report - Batch: 660-65431
Method: 8260C SIM/ID
Preparation: 5030B
LCS Lab Sample ID: LCS 660-65431/1
Client Matrix:
Water
Dilution:
1.0
07/29/2008 1127
Date Analyzed:
07/29/2008 1127
Date Prepared:
Analysis Batch: 660-65431
Prep Batch: N/A
Units: ug/L
Instrument ID: BVMH GC/MS
Lab File ID:
1HG2908.D
Initial Weight/Volume:
5 mL
Final Weight/Volume:
5 mL
LCSD Lab Sample ID: LCSD 660-65431/2
Client Matrix:
Water
Dilution:
1.0
07/29/2008 1147
Date Analyzed:
07/29/2008 1147
Date Prepared:
Analysis Batch: 660-65431
Prep Batch: N/A
Units: ug/L
Instrument ID:
BVMH GC/MS
Lab File ID:
1HG2909.D
Initial Weight/Volume: 5 mL
Final Weight/Volume: 5 mL
Analyte
LCS
% Rec.
LCSD
1,4-Dioxane
113
85
Limit
RPD
RPD Limit
50 - 150
28
50
Calculations are performed before rounding to avoid round-off errors in calculated results.
TestAmerica Tampa
Page 42 of 45
LCS Qual LCSD Qual
Quality Control Results
Client: ARCADIS U.S., Inc.
Job Number: 660-24325-1
Matrix Spike/
Matrix Spike Duplicate Recovery Report - Batch: 660-65431
Method: 8260C SIM/ID
Preparation: 5030B
MS Lab Sample ID:
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
660-24324-A-1 MS
Water
1.0
07/29/2008 2012
07/29/2008 2012
Analysis Batch: 660-65431
Prep Batch: N/A
Instrument ID: BVMH GC/MS
Lab File ID:
1HG2934.D
Initial Weight/Volume: 5 mL
Final Weight/Volume: 5 mL
MSD Lab Sample ID:
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
660-24324-B-1 MSD
Water
1.0
07/29/2008 2032
07/29/2008 2032
Analysis Batch: 660-65431
Prep Batch: N/A
Instrument ID: BVMH GC/MS
Lab File ID:
1HG2935.D
Initial Weight/Volume: 5 mL
Final Weight/Volume: 5 mL
Analyte
MS
1,4-Dioxane
110
% Rec.
MSD
110
Limit
RPD
RPD Limit
50 - 150
0
50
Calculations are performed before rounding to avoid round-off errors in calculated results.
TestAmerica Tampa
Page 43 of 45
MS Qual MSD Qual
Page 44 of 45
Login Sample Receipt Check List
Client: ARCADIS U.S., Inc.
Job Number: 660-24325-1
Login Number: 24325
Creator: Volz, Charles
List Number: 1
List Source: TestAmerica Tampa
Question
T / F/ NA
Radioactivity either was not measured or, if measured, is at or below
background
The cooler's custody seal, if present, is intact.
N/A
The cooler or samples do not appear to have been compromised or
tampered with.
Samples were received on ice.
Cooler Temperature is acceptable.
True
Cooler Temperature is recorded.
COC is present.
COC is filled out in ink and legible.
COC is filled out with all pertinent information.
There are no discrepancies between the sample IDs on the containers and
the COC.
Samples are received within Holding Time.
Sample containers have legible labels.
Containers are not broken or leaking.
True
True
True
True
True
Sample collection date/times are provided.
Appropriate sample containers are used.
Sample bottles are completely filled.
There is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
VOA sample vials do not have headspace or bubble is <6mm (1/4") in
diameter.
If necessary, staff have been informed of any short hold time or quick TAT
needs
Multiphasic samples are not present.
Samples do not require splitting or compositing.
True
True
True
True
TestAmerica Tampa
Comment
N/A
True
True
True
True
True
True
True
True
True
Page 45 of 45
3 Degrees.CU-04