Test Report. No. CANEC1605546501 Date: 25 Apr 2016 . HANGZHOU SILAN INTEGRATED CIRCUIT CO.,LTD. . NO.308,10TH ROAD,EAST HETZ,HANGZHOU CHINA. . The following sample(s) was/were submitted and identified on behalf of the clients as : DICE . SGS Job No. : CP16-018376 - GZ . Date of Sample Received : . 06 Apr 2016. Testing Period : . 06 Apr 2016 - 21 Apr 2016 . Test Requested : . Selected test(s) as requested by client. . Test Method : . Please refer to next page(s). . Test Results :. Please refer to next page(s). . Signed for and on behalf of SGS-CSTC Standards Technical Services Co., Ltd. Guangzhou Branch. Alkene Liang. Approved Signatory . Almay Gao. Approved Signatory . Page 1 of 26. Test Report. No. CANEC1605546501 Date: 25 Apr 2016 . Page 2 of 26. Test Results :. Test Part Description : . Specimen No.. SN1. SGS Sample ID. CAN16-055465.001 Description. "DICE". Remarks :. (1) 1 mg/kg = 0.0001% . (2) MDL = Method Detection Limit . (3) ND = Not Detected ( < MDL ) . (4) "-" = Not Regulated . SS-00259. Test Method : . (1)With reference to IEC 62321-5:2013, determination of Cadmium by ICP-OES. (2)With reference to IEC 62321-5:2013, determination of Lead by ICP-OES. (3)With reference to IEC 62321-4:2013, determination of Mercury by ICP-OES. (4)With reference to IEC 62321:2008, determination of Hexavalent Chromium by Colorimetric Method using UV-Vis. (5)With reference to IEC 62321-6:2015, determination of PBBs and PBDEs by GC-MS. . Test Item(s). Unit. MDL. 001. Cadmium (Cd) . mg/kg. 2 ND Lead (Pb). mg/kg. 2 ND Mercury (Hg). mg/kg. 2 ND Hexavalent Chromium (CrVI) . mg/kg. 2 ND Sum of PBBs . mg/kg. - ND Monobromobiphenyl . mg/kg. 5 ND Dibromobiphenyl . mg/kg. 5 ND Tribromobiphenyl . mg/kg. 5 ND Tetrabromobiphenyl . mg/kg. 5 ND Pentabromobiphenyl . mg/kg. 5 ND Hexabromobiphenyl . mg/kg. 5 ND Heptabromobiphenyl . mg/kg. 5 ND Octabromobiphenyl . mg/kg. 5 ND Nonabromobiphenyl . mg/kg. 5 ND Decabromobiphenyl . mg/kg. 5 ND Sum of PBDEs . mg/kg. - ND Monobromodiphenyl ether . mg/kg. 5 ND Test Report. No. CANEC1605546501 Date: 25 Apr 2016 . Unit. MDL. 001. Dibromodiphenyl ether . mg/kg. 5 ND Tribromodiphenyl ether . mg/kg. 5 ND Tetrabromodiphenyl ether . mg/kg. 5 ND Pentabromodiphenyl ether . mg/kg. 5 ND Hexabromodiphenyl ether . mg/kg. 5 ND Heptabromodiphenyl ether . mg/kg. 5 ND Octabromodiphenyl ether . mg/kg. 5 ND Nonabromodiphenyl ether . mg/kg. 5 ND Decabromodiphenyl ether . mg/kg. 5 ND Test Item(s). Page 3 of 26. Halogen. Test Method : . With reference to EN 14582: 2007, analysis was performed by Ion Chromatograph (IC). . Test Item(s). Chlorine (Cl). Bromine (Br). Unit. MDL. 001. mg/kg. mg/kg. 50 50 ND ND Asbestos. Test Method : . With reference to NIOSH 9002:1994 and NIOSH 9000:1994, Analysis was performed by PLM and XRD.. Test Item(s). Chrysotile. Amosite. Crocidolite. Anthophyllite . Tremolite. Actinolite. CAS NO. Unit. MDL. 001. 12001-29-5/ 132207-32-0 12172-73-5.. 12001-28-4. 77536-67-5. 77536-68-6. 77536-66-4. % (m/m). % (m/m). % (m/m). % (m/m). % (m/m). % (m/m). 0.1 0.1 0.1 0.1 0.1 0.1 Negative Negative Negative Negative Negative Negative Notes :. (1)Negative means the absence of asbestos, Positive means the presence of asbestos. . Test Report. No. CANEC1605546501 Date: 25 Apr 2016 . Page 4 of 26. Element(s). Test Method : . With reference to US EPA Method 3052:1996, analysis was performed by ICP-OES. . Test Item(s). Unit. MDL. 001. Beryllium (Be) . BeO. mg/kg. mg/kg. 5 15 ND ND Notes :. (1) Calculated concentration of BeO is based on the identified Be. . CoCl2 (Cobalt dichloride). Test Method : . With reference to SGS in house method(GZTC CHEM-TOP-099-02), analysis was performed by IC and ICP-OES . Test Item(s). Cobalt Dichloride (CoCl₂) . Unit. MDL. 001. mg/kg. 100 ND Notes :. (1) Results of cobalt dichloride are calculated based on the results of cobalt and chloride. . Polychlorinated Naphthalenes (PCNs). Test Method : . With reference to US EPA 8081B: 2007, analysis was performed by GC-MS . Test Item(s). 1-Chlorinated Naphthalene . 2-Chlorinated Naphthalene . 1,4-Dichlorinated Naphthalene . 1,5-Dichlorinated Naphthalene . 1,2-Dichlorinated Naphthalene . 1,8-Dichlorinated Naphthalene . 1,2,3-Trichlorinated Naphthalene . 1,2,3,4-Tetrachlorinated Naphthalene . 1,2,3,4,6-Pentachlorinated Naphthalene . Octa-chlorinaed Naphthalene . Unit. MDL. 001. mg/kg. mg/kg. mg/kg. mg/kg. mg/kg. mg/kg. mg/kg. mg/kg. mg/kg. mg/kg. 5 5 5 5 5 5 5 5 5 5 ND ND ND ND ND ND ND ND ND ND Test Report. No. CANEC1605546501 Date: 25 Apr 2016 . Page 5 of 26. Organic-Tin compounds. Test Method : . With reference to ISO 17353: 2004 , analysis was performed by GC-MS. . Test Item(s). Tributyl tin (TBT) by weight of Tin . Triphenyl tin (TPhT) by weight of Tin . Tricyclohexyltin (TCyT) by weight of Tin . Trioctyltin (TOT) by weight of Tin . Tripropyltin (TPT) by weight of Tin . Σ of Tri substituted organotin compounds calculated as tin. tin (DBT) by weight of Tin . Dibutyl Dioctyl tin (DOT) by weight of Tin . Unit. MDL. 001. %(w/w). %(w/w). %(w/w). %(w/w). %(w/w). %(w/w). %(w/w). %(w/w). 0.01 0.01 0.01 0.01 0.01 0.01 0.01 ND ND ND ND ND ND ND ND Ozone Depleting Substances (ODS). Test Method : . With reference to US EPA 5021A 2003, Analysis was performed by HS-GC-MS. . Test Item(s). CFC. CFC-11. CFC-12. CFC-13. CFC-111. CFC-112. CFC-112. CFC-113. CFC-113. CFC-114. CFC-114. CFC-115. CFC-211. CFC-212. CFC-213. CFC-214. CFC-215. CFC-215. CAS NO. Unit. MDL. 001. 75-69-4. 75-71-8. 75-72-9. 354-56-3. 76-11-9. 76-12-0. 76-13-1. 354-58-5. 76-14-2. 374-07-2. 76-15-3. 422-78-6. 661-96-1. 1652-89-7. 677-68-9. 1599-41-3. 76-17-5. µg/g. µg/g. µg/g. µg/g. µg/g. µg/g. µg/g. µg/g. µg/g. µg/g. µg/g. µg/g. µg/g. µg/g. µg/g. µg/g. µg/g. 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND Test Report. Test Item(s). CFC-216. CFC-216. CFC-217. Halon. Halon 1211. Halon 1301. Halon 2402. HFC. HFC-23. HFC-32. HFC-41. HFC-43-10mee . HFC-125. HFC-134. HFC-134a. HFC-152a. HFC-143. HFC-143a. HFC-227ea. HFC-236cb. HFC-236ea. HFC-236fa. HFC-245ca. HFC-245fa. HFC-365mfc. PFC. Perfluoromethane . Perfluoroethane . Perfluoropropane . Perfluorobutane . Perfluoropentane . Perfluorohexane . Perfluorocyclobutane . CHC. Carbon tetrachloride . 1,1,1-trichloroethane . Others. Sulphur Hexafluoride - SF₆ . No. CANEC1605546501 Date: 25 Apr 2016 . CAS NO. Unit. MDL. 001. 661-97-2. 1652-80-8. 422-86-6. µg/g. µg/g. µg/g. 0.1 0.1 0.1 ND ND ND 353-59-3. 75-63-8. 124-73-2. µg/g. µg/g. µg/g. 0.1 0.1 0.1 ND ND ND 75-46-7. 75-10-5. 593-53-3. -. 354-33-6. 359-35-3. 811-97-2. 75-37-6. 420-46-2. 430-66-0. -. -. 431-63-0. 690-39-1. 679-86-7. -. -. µg/g. µg/g. µg/g. µg/g. µg/g. µg/g. µg/g. µg/g. µg/g. µg/g. µg/g. µg/g. µg/g. µg/g. µg/g. µg/g. µg/g. 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 75-73-0. 76-16-4. 76-19-7. 355-25-9. 678-26-2. 355-42-0. 115-25-3. µg/g. µg/g. µg/g. µg/g. µg/g. µg/g. µg/g. 0.1 0.1 0.1 0.1 0.1 0.1 0.1 ND ND ND ND ND ND ND 56-23-5. 71-55-6. µg/g. µg/g. 0.1 0.1 ND ND 2551-62-4. µg/g. 0.1 ND Page 6 of 26. Test Report. No. CANEC1605546501 Date: 25 Apr 2016 . Page 7 of 26. Perchlorate. Test Method : . With reference to SGS In-house method (GZTC CHEM-TOP-224-01), analysis was performed by LC-MSMS.. Test Item(s). Perchlorate. Unit. MDL. 001. µg/kg. 5 ND Formaldehyde. Test Method : . In-house method (GZTC-CHEM-TOP-059-03),analysis was performed by UV-Vis. . Test Item(s). Unit. Formaldehyde . g/kg. MDL. 001. 0.02 ND Commission Decision 2011/135/EU (previously restricted under 2010/153/EU and 2009/251/EC) – Dimethyl fumarate(DMF). Test Method : . SGS Inhouse method (GZTC CHEM-TOP-095), analysis was performed by GC-MS. . Test Item(s). Limit. Dimethyl fumarate(DMF) . Comment. 0.1 Unit. mg/kg. MDL. 001. 0.1 ND PASS Notes :. (1) The maximum permissible limit is quoted from the document EU Directive 2011/135/EU (previously restricted under 2010/153/EU and 2009/251/EC) . Polyvinyl chloride (PVC). Test Method : . SGS in house method (GZTC CHEM-TOP-066), analysis was performed by FTIR. . Test Item(s). CAS NO. PVC. 9002-86-2. Notes :. (1) Negative=Undetectable,Positive=Detectable . Unit. - MDL. 001. - Negative Test Report. No. CANEC1605546501 Date: 25 Apr 2016 . Page 8 of 26. SCCP (Short chained chlorinated paraffins). Test Method : . With reference to US EPA 3550C: 2007, analysis was performed by GC-ECD. . Test Item(s). Short Chained Chlorinated Paraffin (SCCP) . Unit. MDL. 001. mg/kg. 50 ND Notes :. (1) The result of SCCP is confirmed by GC-MS(NCI). . Polychlorinated Terphenyls (PCTs). Test Method : . With reference to US EPA 8082A: 2007, analysis was performed by GC-MS . Test Item(s). Aroclor 5432 . Aroclor 5442 . Aroclor 5460 . Unit. MDL. 001. mg/kg. mg/kg. mg/kg. 5 5 5 ND ND ND Hexabromocyclododecane (HBCDD). Test Method : . With reference to EPA 3550C:2007, analysis was performed by GC-MS. . Test Item(s). Unit. Hexabromocyclododecane (HBCDD) and all major diastereoisomers identified (α-HBCDD, β-HBCDD, γ-HBCDD) . MDL. 10. ND. Unit. %(w/w). %(w/w). %(w/w). %(w/w). MDL. 0.003. 0.003. 0.003. 0.010. 001. ND. ND. ND. ND. %(w/w). 0.003. ND. mg/kg. 001. Phthalates Content. Test Method : . With reference to EN14372: 2004. Analysis was performed by GC-MS. . Test Item(s). Dibutyl Phthalate (DBP) . Benzylbutyl Phthalate (BBP) . Bis(2-ethylhexyl) Phthalate (DEHP) . Diisononyl Phthalate (DINP) . Di-n-octyl Phthalate (DNOP) . CAS NO. 84-74-2. 85-68-7. 117-81-7. 28553-12-0 / 68515-48-0. 117-84-0. Test Report. No. CANEC1605546501 Test Item(s). Diisodecyl Phthalate (DIDP) . Diisobutyl Phthalate (DIBP) . Di-n-hexyl Phthalate (DnHP) . 1,2-Benzenedicarboxylic acid, di-C6-8-branched alkyl esters, C7-rich (DIHP) . 1,2-Benzenedicarboxylic acid, di-C7-11-branched and linear alkyl esters (DHNUP) . Bis(2-methoxyethyl) Phthalate (DMEP) . Diisopentyl Phthalate (DIPP) . n-pentyl Isopentyl Phthalate (nPIPP) . Di-n-pentyl Phthalate (DnPP) . 1,2-Benzenedicarboxylic acid, dipentyl ester, branched and linear (DPP) . 1,2-Benzenedicarboxylic acid, dihexyl ester branched and linear (DHP) . Date: 25 Apr 2016 . CAS NO. Unit. Page 9 of 26. MDL. 001. 26761-40-0 / 68515-49-1. 84-69-5. %(w/w). 0.010. ND. %(w/w). 0.003. ND. 84-75-3. %(w/w). 0.003. ND. 71888-89-6. %(w/w). 0.010. ND. 68515-42-4. %(w/w). 0.010. ND. 117-82-8. %(w/w). 0.003. ND. 605-50-5. %(w/w). 0.003. ND. 776297-69-9 . %(w/w). 0.003. ND. 131-18-0. %(w/w). 0.003. ND. 84777-06-0. %(w/w). 0.010. ND. 68515-50-4. %(w/w). 0.010. ND. Polychlorinated Biphenyls (PCBs). Test Method : . With reference to US EPA 8082A: 2007, analysis was performed by GC-MS . CAS NO. Unit. 2,4,4’-Trichlorobiphenyl (PCB 28) . Test Item(s). 7012-37-5. mg/kg. 2,2’,5,5’-Tetrachloro-biphenyl (PCB 52) . 35693-99-3. mg/kg. 2,2’,4,5,5’-Pentachloro-biphenyl (PCB 101) . 37680-73-2. mg/kg. 2,3’,4,4’,5-Pentachlorobiphenyl (PCB 118) . 31508-00-6. mg/kg. 2,2’3,4,4’,5’-Hexachloro-biphenyl (PCB 138) . 35065-28-2. mg/kg. 2,2’,4,4’,5,5’-Hexachloro-biphenyl (PCB 153) . 35065-27-1. mg/kg. 2,2’,3,4,4’,5,5’-Heptachlorobiphenyl (PCB 180) . 35065-29-3. mg/kg. MDL. 0.5. 0.5. 0.5. 0.5. 0.5. 0.5. 0.5. 001. ND. ND. ND. ND. ND. ND. ND. PFOA & PFOS (Perfluorooctanoic acid & Perfluorooctane sulfonates). Test Method : . With reference to CEN/TS15968:2010, analysis was performed by LC-MS. . Test Item(s). Perfluoroctanoic acid (PFOA) . Perfluorooctane Sulfonates (PFOS)^ . CAS NO. Unit. 335-67-1. mg/kg. -. mg/kg. MDL. 10. 10. 001. ND. ND. Notes :. ^ PFOS refer to Perfluorooctanesulfonic acid and its derivatives including Perfluoroctanesulfonic acid, Test Report. No. CANEC1605546501 Date: 25 Apr 2016 . Page 10 of 26. Perfluoroctane sulfonamide, N-Methylperfluoroctane sulfonamide, N-Ethylperfluoroctane sulfonamide, N-Methylperfluoroctane sulfonamidoethanol and N-Ethylperfluoroctane sulfonamidoethanol. . Polycyclic Aromatic Hydrocarbons (PAHs). Test Method : . With reference to AfPS GS 2014:01 PAK, analysis was performed by GC-MS. . CAS NO. Unit. Benzo(a)anthracene(BaA) . Test Item(s). 56-55-3. mg/kg. Chrysene(CHR) . 218-01-9. mg/kg. Benzo(b)fluoranthene(BbF) . 205-99-2. mg/kg. Benzo(j)fluoranthene(BjF) . 205-82-3. mg/kg. Benzo(k)fluoranthene(BkF) . 207-08-9. mg/kg. Benzo(a)pyrene(BaP) . 50-32-8. mg/kg. Benzo(e)pyrene(BeP) . 192-97-2. mg/kg. Dibenzo(a,h)anthracene(DBA) . 53-70-3. mg/kg. MDL. 0.1. 0.1. 0.1. 0.1. 0.1. 0.1. 0.1. 0.1. 001. ND. ND. ND. ND. ND. ND. ND. ND. Substances in the Candidate List of SVHC. Test Method : . SGS In House method-GZTC CHEM-TOP-092-01, SGS In House method-GZTC CHEM-TOP-092-02, Analyzed by ICP-OES&GC-MS. . Test Item(s). Diarsenic pentaoxide* . CAS NO. 1303-28-2. Unit. %(w/w). MDL. 0.005. 001. 0.125. Diarsenic trioxide* . 1327-53-3. %(w/w). 0.005. 0.108. Boric acid*. 10043-35-3, 11113-50-1. 1303-96-4, 1330-43-4, 12179-04-3. 12267-73-1. %(w/w). 0.005. ND. %(w/w). 0.005. ND. %(w/w). 0.005. ND. 140-66-9. %(w/w). 0.050. ND. Trixylyl phosphate . 25155-23-1. %(w/w). 0.050. ND. 2-(2H-Benzotriazol-2-yl)-4,6-ditertpentylphenol (UV-328) . 25973-55-1. %(w/w). 0.050. ND. 2-benzotriazol-2-yl-4,6-di-tert-butylphenol (UV-320) . 3846-71-7. %(w/w). 0.050. ND. Bis(2-methoxyethyl) ether . 111-96-6. %(w/w). 0.050. ND. N,N-dimethylacetamide . 127-19-5. %(w/w). 0.050. ND. 1,2-dimethoxyethane; ethylene glycol dimethyl ether (EGDME). 110-71-4. %(w/w). 0.050. ND. Disodium tetraborate, anhydrous* . Tetraboron disodium heptaoxide, hydrate* . 4-(1,1,3,3-tetramethylbutyl)phenol . Test Report. No. CANEC1605546501 Test Item(s). Date: 25 Apr 2016 . Page 11 of 26. CAS NO. Unit. 2-Ethylhexyl 10-ethyl-4,4-dioctyl-7-oxo-8-oxa-3,5-dithia-4-stannatetrad ecanoate; DOTE . 15571-58-1. %(w/w). 0.050. MDL. ND. 001. Reaction mass of 2-ethylhexyl 10-ethyl-4,4-dioctyl-7-oxo-8-oxa-3,5-dithia-4-stannatetrad ecanoate & 2-ethylhexyl 10-ethyl-4-[[2[(2-ethylhexyl)oxy]-2-oxoethyl]thio]-4-octyl-7-oxo-8-oxa-3, 5-dithia-4-stannatetradecanoate (reaction mass of DOTE & MOTE). -. %(w/w). 0.050. ND. Notes :. 1. Calculated concentration of Diarsenic pentaoxide,Diarsenic trioxide are based on the arsenic by ICP OES.Calculated concentration of boric acid, disodium tetraborate, anhydrous and tetraboron disodium heptaoxide, hydrate are based on the total/water extractive boron and sodium by ICP OES. . Benzotriazole UV Absorbant. Test Method : . With reference to US EPA 3550C: 2007, analysis was performed by GC-MS. . Test Item(s). 2(3,5-Di-tert-butyl-2-hydroxyphen yl) benzotriazole (UV-320) . CAS NO. Unit. MDL. 001. 3846-71-7. mg/kg. 5 ND Azo Dyes. Test Method : . With reference to EN 14362-1 :2012 - Analysis was conducted with GC-MS/HPLC-DAD. Determination of 4-aminoazobenzene (CAS No.:60-09-3) – EN 14362-3:2012; with the use of Gas Chromatography – Mass Spectrometry (GC-MS) . CAS NO. Unit. MDL. 001. 4-Aminobiphenyl . 92-67-1. mg/kg. 5 ND Benzidine. 92-87-5. mg/kg. 5 ND Test Item(s). Test Report. No. CANEC1605546501 Date: 25 Apr 2016 . CAS NO. Unit. MDL. 001. 4-chloro-o-toluidine . 95-69-2. mg/kg. 5 ND 2-naphthylamine . 91-59-8. mg/kg. 5 ND o-aminoazotoluene . 97-56-3. mg/kg. 5 ND 5-nitro-o-toluidine / 2-Amino-4-nitrotoluene . 99-55-8. mg/kg. 5 ND 4-chloroaniline . 106-47-8. mg/kg. 5 ND 4-methoxy-m-phenylenediamine / 2,4-Diaminoanisole . 615-05-4. mg/kg. 5 ND 4,4’-diaminodiphenylmethane . 101-77-9. mg/kg. 5 ND 3,3’-dichlorobenzidine . 91-94-1. mg/kg. 5 ND 3.3’-dimethoxybenzidine . 119-90-4. mg/kg. 5 ND 3,3’-dimethylbenzidine . 119-93-7. mg/kg. 5 ND 3,3'-Dimethyl-4,4'-diaminodiphe nylmethane / 4,4'-methylenedi-o-toluidine . 838-88-0. mg/kg. 5 ND p-cresidine. 120-71-8. mg/kg. 5 ND 4,4’-methylene-bis(2-chloroaniline) . 101-14-4. mg/kg. 5 ND 4,4’-oxydianiline . 101-80-4. mg/kg. 5 ND Test Item(s). Page 12 of 26. Test Report. No. CANEC1605546501 Date: 25 Apr 2016 . Test Item(s). CAS NO. Unit. MDL. 001. 4,4’-thiodianiline . 139-65-1. mg/kg. 5 ND o-toluidine. 95-53-4. mg/kg. 5 ND 4-methyl-m-phenylenediamine / 2,4-Toluylendiamine . 95-80-7. mg/kg. 5 ND 2,4,5-trimethylaniline . 137-17-7. mg/kg. 5 ND 4-aminoazobenzene . 60-09-3. mg/kg. 5 ND O-Anisidine. 90-04-0. mg/kg. 5 ND 2,4-Xylidine. 95-68-1. mg/kg. 5 ND 2,6-Xylidine. 87-62-7. mg/kg. 5 ND Page 13 of 26. Notes :. (1)The EN 14362-1 methods will enable further cleavage of 4-aminoazobenzene to non-forbidden amines: aniline and 1,4-phenylenediamine, therefore, the test method of EN14362-3:2012 was employed to verify the presence of 4-aminoazobenzene. . Flame retardant(s). Test Method : . With reference to US EPA Method 3550C:2007 and US EPA Method 8270D: 2007, analysis was performed by GC-MS, HPLC-DAD/MS. . Test Item(s). Tris(1,3-dichloro-2-propyl) Phosphate(TDCPP) . CAS NO. Unit. MDL. 001. 13674-87-8. mg/kg. 5 ND Test Report. Test Item(s). Tris(1-chloro-2-propyl) Phosphate (TCPP) . Tris(2-chloroethyl) Phosphate(TCEP) . No. CANEC1605546501 Date: 25 Apr 2016 . CAS NO. Unit. MDL. 001. 13674-84-5. mg/kg. 5 ND 115-96-8. mg/kg. 5 ND Page 14 of 26. Benzenamine,N-phenyl-,Reaction Products with Styrene and 2,4,4-Trimethylpentene. Test Method : . With reference to EPA method 3550C:2007 & EPA method 8270D:2007, analysis was performed by GC-MS.. Test Item(s). Benzenamine,N-phenyl-,Reactio n Products with Styrene and 2,4,4-Trimethylpentene (BNST) . CAS NO. Unit. MDL. 001. 68921-45-9. mg/kg. 10 ND Notes :. The result of BNST is quantified by one of BNST components . Test Report. No. CANEC1605546501 Date: 25 Apr 2016 . Page 15 of 26. ATTACHMENTS Pb/Cd/Hg/Cr6+/PBBs/PBDEs Testing Flow Chart 1) Name of the person who made testing: Bruce Xiao / Sunny Hu 2) Name of the person in charge of testing: Bella Wang / Cutey Yu 3) These samples were dissolved totally by pre-conditioning method according to below flow chart (Cr6+ and PBBs/PBDEs test method excluded ). Sample Preparation Sample Measurement Pb/Cd/Hg Acid digestion with microwave/ hotplate Sample solvent extraction Filtration Concentration/ Dilution of extraction solution Solution Residue Filtration 1) Alkali Fusion / Dry Ashing 2) Acid to dissolve ICP-OES/AAS DATA Cr6+ PBBs/PBDEs GC-MS DATA Nonmetallic material Metallic material Adding digestion reagent Boiling water extraction Heating to 90~95℃ for extraction Filtration and pH adjustment Adding 1,5diphenylcarbazide for color development UV-Vis DATA Adding 1,5diphenylcarbazide for color development UV-Vis DATA Test Report. No. CANEC1605546501 ATTACHMENTS Phthalates Testing Flow Chart 1) Name of the person who made testing: Sunny Hu 2) Name of the person in charge of testing: Cutey Yu Sample cutting / preparation Sample Measurem ent Solvent extraction Concentration/Dilution Filtration GC-MS DATA Date: 25 Apr 2016 . Page 16 of 26. Test Report. No. CANEC1605546501 ATTACHMENTS HBCDD Testing Flow Chart 1) Name of the person who made testing: Sunny Hu 2) Name of the person in charge of testing: Cutey Yu Sample cutting / preparation Sample Measurement Solvent extraction Concentration/Dilution Filtration GC-MS DATA Date: 25 Apr 2016 . Page 17 of 26. Test Report. No. CANEC1605546501 ATTACHMENTS SCCP/MCCP Testing Flow Chart 1) Name of the person who made testing: Alison Zhang 2) Name of the person in charge of testing: Cutey Yu Sample cutting / preparation Sample Measurement Solvent extraction Concentration Clean-Up Filtration GC-ECD DATA Date: 25 Apr 2016 . Page 18 of 26. Test Report. No. CANEC1605546501 Date: 25 Apr 2016 . ATTACHMENTS PFOA / PFOS Testing Flow Chart 1) Name of the person who made testing: Zhihong Wang 2) Name of the person in charge of testing: Cutey Yu Sample cutting / preparation Sample Measurement Solvent extraction Concentration/Dilution Filtration LC-MS DATA Page 19 of 26. Test Report. No. CANEC1605546501 ATTACHMENTS Dimethyl Fumarate Testing Flow Chart 1) Name of the person who made testing: Sunny Hu 2) Name of the person in charge of testing: Cutey Yu Sample cutting / preparation Sample Measurement Solvent extraction Concentration/Dilution Filtration GC-MS DATA Date: 25 Apr 2016 . Page 20 of 26. Test Report. No. CANEC1605546501 ATTACHMENTS PAHs Testing Flow Chart 1) Name of the person who made testing: Sunny Hu 2) Name of the person in charge of testing: Cutey Yu Sample cutting / preparation Sample Measurement Solvent extraction Concentration/Dilution Filtration GC-MS DATA Date: 25 Apr 2016 . Page 21 of 26. Test Report. No. CANEC1605546501 ATTACHMENTS PVC Testing Flow Chart 1) Name of the person who made testing: Alison Zhang 2) Name of the person in charge of testing: Cutey Yu Sample cutting/preparation FTIR Check wave -number of C-Cl bonding DATA Date: 25 Apr 2016 . Page 22 of 26. Test Report. No. CANEC1605546501 Date: 25 Apr 2016 . ATTACHMENTS Halogen Testing Flow Chart 1) Name of the person who made testing: Hanming Xiao 2) Name of the person in charge of testing: Bella Wang Sample cutting / preparation Sample Measur ement Combustion in oxygen bomb Dissolved in an absorption solution Filtration Analyzed by ion chromatography. Double confirm by other instruments, if necessary DATA Page 23 of 26. Test Report. No. CANEC1605546501 ATTACHMENTS Elementary Testing Flow Chart 1) Name of the person who made testing : Bruce Xiao 2) Name of the person in charge of testing : Bella Wang Sample cutting / preparation Sample Measurement Acid digestion Filtration Solution ICP-OES/AAS DATA Date: 25 Apr 2016 . Page 24 of 26. Test Report. No. CANEC1605546501 ATTACHMENTS SVHC Testing Flow Chart 1) Name of the person who made testing: Martin He / Alison Zhang 2) Name of the person in charge of testing: Cutey Yu Sample cutting/prepar ation Sample measurement Sample Pretreatment Instrumental Analysis DATA Date: 25 Apr 2016 . Page 25 of 26. Test Report. No. CANEC1605546501 Date: 25 Apr 2016 . Sample photo: . CANEC1605546501 CAN16-055465.001 . SGS authenticate the photo on original report only . *** End of Report *** . Page 26 of 26.