Test Report. No. SHAEC1514782501 Date: 31 Jul 2015 . Page 1 of 19. CHANG CHUN PLASTICS CO.,LTD 、CHANG CHUN SB(CHANG SHU)CO.,LTD . NO.8，CHUNG HWA ROAD,HSINCHU INDUSTRIAL DISTRICT,TAIWAN 、CHANGCHUN RD.,RIVERSIDE INDUSTRIAL PARK,CHANGSHU ECONOMIC DEVELOPMENT ZONE,JIANGSU,CHINA . . The following sample(s) was/were submitted and identified on behalf of the clients as : Epoxy Molding Compound for semiconductor . SGS Job No. : SP15-025120 - SUZ . Model No. :. EME-1200. Client Ref. Information : . EME-1100、EME-2100、EME-2500、EME-5000N、EME-5000VR、EME-5051 S、EME-5500F、EME-5500FL、EME-5500FR、EME-5961、EME-220L、EC-1 1、EC-12、ER100、ER200、EME-2050、EME-1250. Date of Sample Received : . 27 Jul 2015. Testing Period : . 27 Jul 2015 - 30 Jul 2015 . Test Requested : . Selected test(s) as requested by client. . Test Method : . Please refer to next page(s). . Test Results :. Please refer to next page(s). . Conclusion :. Based on the performed tests on submitted sample(s), the results of Lead, Mercury, Cadmium, Hexavalent chromium, Polybrominated biphenyls (PBBs), Polybrominated diphenyl ethers (PBDEs) and Phthalates such as Bis(2-ethylhexyl) phthalate (DEHP), Butyl benzyl phthalate (BBP), Dibutyl phthalate (DBP) and Diisobutyl phthalate (DIBP) comply with the limits as set by RoHS Directive (EU) 2015/863 amending Annex II to Directive 2011/65/EU. . When tested as specified, Dimethyl fumarate(DMF) content of the submitted sample comply with Commission Regulation (EU) No 412/2012 and Entry 61 of Annex XVII of REACH Regulation (EC) No 1907/2006 . Signed for and on behalf of SGS-CSTC Standards Technical Services (Shanghai) Co., Ltd.. Marry Ma. Approved Signatory . Test Report. No. SHAEC1514782501 Date: 31 Jul 2015 . Page 2 of 19. Test Results :. Test Part Description : . Specimen No.. SN1. SGS Sample ID. SHA15-147825.001 Description. Black powder. Remarks :. (1) 1 mg/kg = 0.0001% . (2) MDL = Method Detection Limit . (3) ND = Not Detected ( < MDL ) . (4) "-" = Not Regulated . RoHS Directive (EU) 2015/863 amending Annex II to Directive 2011/65/EU. Test Method : . (1) With reference to IEC 62321-5:2013, determination of Cadmium by ICP-OES. (2) With reference to IEC 62321-5:2013, determination of Lead by ICP-OES. (3) With reference to IEC 62321-4:2013, determination of Mercury by ICP-OES. (4) With reference to IEC 62321:2008, determination of Hexavalent Chromium by Colorimetric Method using UV-Vis. (5) With reference to IEC 62321-6:2015, determination of PBBs and PBDEs by GC-MS. (6) With reference to IEC 62321-8 (111/321/CD), determination of phthalates by GC-MS. . Limit. Unit. MDL. 001. Cadmium (Cd) . 100 mg/kg. 2 ND Lead (Pb). 1000 mg/kg. 2 ND Mercury (Hg). 1000 mg/kg. 2 ND Hexavalent Chromium (Cr(VI)) . 1000 mg/kg. 2 ND Sum of PBBs . 1000 mg/kg. - ND Monobromobiphenyl . - mg/kg. 5 ND Dibromobiphenyl . - mg/kg. 5 ND Tribromobiphenyl . - mg/kg. 5 ND Tetrabromobiphenyl . - mg/kg. 5 ND Pentabromobiphenyl . - mg/kg. 5 ND Hexabromobiphenyl . - mg/kg. 5 ND Heptabromobiphenyl . - mg/kg. 5 ND Octabromobiphenyl . - mg/kg. 5 ND Nonabromobiphenyl . - mg/kg. 5 ND Decabromobiphenyl . - mg/kg. 5 ND 1000 mg/kg. - ND Test Item(s). Sum of PBDEs . Test Report. No. SHAEC1514782501 Date: 31 Jul 2015 . Limit. Unit. MDL. 001. Monobromodiphenyl ether . - mg/kg. 5 ND Dibromodiphenyl ether . - mg/kg. 5 ND Tribromodiphenyl ether . - mg/kg. 5 ND Tetrabromodiphenyl ether . - mg/kg. 5 ND Pentabromodiphenyl ether . - mg/kg. 5 ND Hexabromodiphenyl ether . - mg/kg. 5 ND Heptabromodiphenyl ether . - mg/kg. 5 ND Octabromodiphenyl ether . - mg/kg. 5 ND Nonabromodiphenyl ether . - mg/kg. 5 ND Decabromodiphenyl ether . - mg/kg. 5 ND Di-butyl Phthalate (DBP) . 1000 mg/kg. 30 ND Benzyl Butyl Phthalate (BBP) . 1000 mg/kg. 30 ND Di-2-Ethyl Hexyl Phthalate (DEHP) . 1000 mg/kg. 30 ND Diisobutyl Phthalates (DIBP) . 1000 mg/kg. 30 ND Test Item(s). Page 3 of 19. Notes :. (1) The maximum permissible limit is quoted from RoHS Directive (EU) 2015/863. . Halogen. Test Method : . With reference to EN 14582: 2007, analysis was performed by Ion Chromatograph (IC). . Test Item(s). Fluorine (F). Chlorine (Cl). Bromine (Br). Iodine (I). Unit. MDL. 001. mg/kg. mg/kg. mg/kg. mg/kg. 50 50 50 50 ND 110 8866 ND Element(s). Test Method : . With reference to US EPA 3052:1996, analysis was performed by ICP-OES. . Test Item(s). Unit. MDL. 001. Nickel (Ni). Phosphorus (P) . Antimony (Sb) . Beryllium (Be) . mg/kg. mg/kg. mg/kg. mg/kg. 5 20 10 5 ND ND 8139 ND Test Report. No. SHAEC1514782501 Date: 31 Jul 2015 . Page 4 of 19. Polychlorinated Naphthalenes (PCNs). Test Method : . With reference to US EPA 8081B: 2007, analysis was performed by GC-MS . Test Item(s). 2-Chlorinated Naphthalene . 1,4-Dichlorinated Naphthalene . 1,5-Dichlorinated Naphthalene . 1,2-Dichlorinated Naphthalene . 1,8-Dichlorinated Naphthalene . 1,2,3-Trichlorinated Naphthalene . 1,2,3,4-Tetrachlorinated Naphthalene . 1,2,3,4,6-Pentachlorinated Naphthalene . Octa-chlorinaed Naphthalene . 1-Chlorinated Naphthalene . Unit. MDL. 001. mg/kg. mg/kg. mg/kg. mg/kg. mg/kg. mg/kg. mg/kg. mg/kg. mg/kg. mg/kg. 5 5 5 5 5 5 5 5 5 5 ND ND ND ND ND ND ND ND ND ND Short Chained Chlorinated Paraffin (SCCP). Test Method : . With reference to US EPA 3550C: 2007, analysis was performed by GC-ECD / GC-NCl-MS. . Test Item(s). Short Chained Chlorinated Paraffin (SCCP) (C10-C13). Unit. MDL. 001. mg/kg. 50 ND Hexabromocyclododecane (HBCDD). Test Method : . Determination of HBCDD by GC-MS based on IEC 62321:2008. . Test Item(s). Unit. Hexabromocyclododecane (HBCDD) . mg/kg. MDL. 001. 10 ND Notes :. (1) Reference Information: Directive 2011/65/EU recasting RoHS directive 2002/95/EC: Hexabromocyclododecane (HBCDD) is considered as a priority for risk evaluation and substance restriction. . Test Report. No. SHAEC1514782501 Date: 31 Jul 2015 . Page 5 of 19. Commission Regulation (EU) No 412/2012 and Entry 61 of Annex XVII of REACH Regulation (EC) No 1907/2006 - Dimethyl fumarate(DMF). Test Method : . Solvent extraction, analysis was performed by GC-MS. . Test Item(s). Dimethyl fumarate(DMF) . Limit. 0.1 Unit. MDL. 001. 0.1 ND mg/kg. Polychlorinated Terphenyls (PCTs). Test Method : . With reference to US EPA 8082A: 2007, analysis was performed by GC-MS . Test Item(s). Aroclor 5432 . Aroclor 5442 . Unit. MDL. 001. mg/kg. mg/kg. 5 5 ND ND Polychlorinated Biphenyls (PCBs). Test Method : . With reference to US EPA 8082A: 2007, analysis was performed by GC-MS . CAS NO. Unit. 2,4,4’-Trichlorobiphenyl (PCB 28) . Test Item(s). 7012-37-5. mg/kg. 2,2’,5,5’-Tetrachloro-biphenyl (PCB 52) . 35693-99-3. mg/kg. 2,2’,4,5,5’-Pentachloro-biphenyl (PCB 101) . 37680-73-2. mg/kg. 2,3’,4,4’,5-Pentachlorobiphenyl (PCB 118) . 31508-00-6. mg/kg. 2,2’,3,4,4’,5’-Hexachloro-biphenyl (PCB 138) . 35065-28-2. mg/kg. 2,2’,4,4’,5,5’-Hexachloro-biphenyl (PCB 153) . 35065-27-1. mg/kg. 2,2’,3,4,4’,5,5’-Heptachlorobiphenyl (PCB 180) . 35065-29-3. mg/kg. MDL. 0.5. 0.5. 0.5. 0.5. 0.5. 0.5. 0.5. 001. ND. ND. ND. ND. ND. ND. ND. MDL. 001. ND. ND. ND. Phthalates. Test Method : . With reference to EN 14372:2004, analysis was performed by GC-MS. . Test Item(s). CAS NO. Dibutyl Phthalate (DBP) . 84-74-2. Benzylbutyl Phthalate (BBP) . 85-68-7. Bis-(2-ethylhexyl) Phthalate (DEHP) . 117-81-7. Unit. %. %. %. 0.003. 0.003. 0.003. Test Report. Test Item(s). Diisononyl Phthalate (DINP) . Di-n-octyl Phthalate (DNOP) . No. SHAEC1514782501 Date: 31 Jul 2015 . CAS NO. 28553-12-0 /68515-48-0. 117-84-0. Page 6 of 19. Unit. %. 0.01. MDL. 001. ND. %. 0.003. ND. 26761-40-0 /68515-49-1. 131-11-3. %. 0.01. ND. %. 0.003. ND. Diethyl Phthalate (DEP) . 84-66-2. %. 0.003. ND. Diisobutyl Phthalate (DIBP) . 84-69-5. %. 0.003. ND. Di-n-pentyl Phthalates (DnPP) . 131-18-0. %. 0.003. ND. Dicyclohexyl Phthalate (DCHP) . 84-61-7. %. 0.003. ND. Diphenyl Phthalate (DPhP) . 84-62-8. %. 0.003. ND. Dibenzyl Phthalate (DBzP) . 523-31-9. %. 0.003. ND. Diisooctyl Phthalate (DiOP) . 27554-26-3. %. 0.01. ND. Dipropyl Phthalate (DPrP) . 131-16-8. %. 0.003. ND. Dinonyl Phthalate (DNP) . 84-76-4. %. 0.003. ND. Di-n-hexyl Phthalate (DnHP) . 84-75-3. %. 0.003. ND. Diisodecyl Phthalate (DIDP) . Dimethyl Phthalate (DMP) . Notes :. (1) DBP,BBP,DEHP Reference information: Entry 51 of Regulation (EC) No 552/2009 amending Annex XVII of REACH Regulation (EC) No 1907/2006 (previously restricted under Directive 2005/84/EC): i) Shall not be used as substances or in mixtures, in concentrations greater than 0,1 % by weight of the plasticised material, in toys and childcare articles. ii) Toys and childcare articles containing these phthalates in a concentration greater than 0.1 % by weight of the plasticised material shall not be placed on the market. Please refer to Regulation (EC) No 552/2009 to get more detail information DINP, DNOP, DIDP Reference information: Entry 52 of Regulation (EC) No 552/2009 amending Annex XVII of REACH Regulation (EC) No 1907/2006 (previously restricted under Directive 2005/84/EC). i) Shall not be used as substances or in mixtures, in concentrations greater than 0.1 % by weight of the plasticised material, in toys and childcare articles which can be placed in the mouth by children. ii) Such toys and childcare articles containing these phthalates in a concentration greater than 0.1 % by weight of the plasticised material shall not be placed on the market. Please refer to Regulation (EC) No 552/2009 to get more detail information . PFOS (Perfluorooctane Sulfonates) and PFOA (Perfluorooctanoic Acid). Test Method : . With reference to US EPA 3550C: 2007, analysis was performed by HPLC-MS. . Test Item(s). Perfluorooctane Sulfonates (PFOS) and related Acid,Metal Salt and Amide . Limit. 10. Unit. mg/kg. MDL. 10. 001. ND. Test Report. No. SHAEC1514782501 Test Item(s). Perfluorooctanoic Acid (PFOA) . Date: 31 Jul 2015 . Limit. - Unit. mg/kg. Page 7 of 19. MDL. 10. 001. ND. Notes :. Max. limit specified by commission regulation (EU) No. 757/2010 amending regulation (EC) No 850/2004.. Polycyclic aromatic hydrocarbons (PAHs). Test Method : . With reference to ZEK 01.4-08 of German ZLS and its amendments, analysis was performed by GC-MS.. Test Item(s). Sum of 18 PAHs . Naphthalene(NAP) . Acenaphthylene(ANY) . Acenaphthene(ANA) . Fluorene(FLU) . Phenanthrene(PHE) . Anthracene(ANT) . Fluoranthene(FLT) . Pyrene(PYR) . Benzo(a)anthracene(BaA) . Chrysene(CHR) . Benzo(b)fluoranthene(BbF) and Benzo(j)fluoranthene(BjF) . Benzo(k)fluoranthene(BkF) . Benzo(a)pyrene(BaP) . Benzo(e)pyrene(BeP) . Indeno(1,2,3-c,d)pyrene(IPY) . Dibenzo(a,h)anthracene(DBA) . Benzo(g,h,i)perylene(BPE) . Unit. mg/kg. mg/kg. mg/kg. mg/kg. mg/kg. mg/kg. mg/kg. mg/kg. mg/kg. mg/kg. mg/kg. mg/kg. mg/kg. mg/kg. mg/kg. mg/kg. mg/kg. mg/kg. MDL. 0.1. 0.1. 0.1. 0.1. 0.1. 0.1. 0.1. 0.1. 0.1. 0.1. 0.1. 0.1. 0.1. 0.1. 0.1. 0.1. 0.1. 001. ND. ND. ND. ND. ND. ND. ND. ND. ND. ND. ND. ND. ND. ND. ND. ND. ND. ND. Notes :. Above 8 PAHs(BaA,CHR,BbF,BjF.BkF,BeP,BaP,DBA) are listed in Commission Regulation (EU) No 1272/2013 amending Annex XVII to Regulation (EC) No 1907/2006. (1) In order to protect the health of consumers from the risk arising from exposure to PAHs in articles, limits on the PAH content in the accessible plastic or rubber parts of articles should be set, and the placing on the market of articles containing any of the PAHs in concentrations greater than 1 mg/kg in those parts should be prohibited. (2) Taking into account the vulnerability of children a lower limit value should be established. Therefore the placing on the market of toys and childcare articles, containing any of the PAHs in concentrations Test Report. No. SHAEC1514782501 Date: 31 Jul 2015 . Page 8 of 19. greater than 0,5 mg/kg in their accessible plastic or rubber parts, should be prohibited. Remark: The German committee on Product Safety (AfPS) adopted a new PAHs document on August 4, 2014, which was taken into account by the GS certification bodies for the certification process of the GS mark. The previously valid PAK-document (ZEK 01.4-08, English version) was repealed on June 30, 2015. . Test Report. No. SHAEC1514782501 Date: 31 Jul 2015 . Page 9 of 19. ATTACHMENTS RoHS Testing Flow Chart 1) Name of the person who made testing: Bob Zhang/Gary Xu/Zengzhen Zhu/Sunny Qin 2) Name of the person in charge of testing: Jan Shi/Summer Jin/Jessy Huang/Stone Chen 3) These samples were dissolved totally by pre-conditioning method according to below flow chart. 6+ (Cr and PBBs/PBDEs test method excluded) Sample Preparation Sample Measurement Pb/Cd/Hg Acid digestion with microwave/ hotplate Sample solvent extraction Filtration Concentration/ Dilution of extraction solution Solution + Cr6 PBBs/PBDEs Nonmetallic material Adding digestion reagent Residue GC/MS Heating to 90~95℃ for extraction Filtration and pH adjustment DATA ICP-OES/AAS DATA Positive Spot test Negative Filtration 1) Alkali Fusion / Dry Ashing 2) Acid to dissolve Metallic material Adding 1,5diphenylcarbazide for color development UV-Vis DATA Boiling water extraction Adding 1,5diphenylcarbazide for color development A red color indicates the 6+ presence of Cr . If necessary, confirm with UVVis. DATA Test Report. No. SHAEC1514782501 Date: 31 Jul 2015 . ATTACHMENTS Phthalates Testing Flow Chart 1) Name of the person who made testing: Sherlock Gao 2) Name of the person in charge of testing: Myra Ma Sample cutting/preparation Sample measurement Solvent extraction Concentration/Dilution Filtration GC-MS DATA Page 10 of 19. Test Report. No. SHAEC1514782501 Date: 31 Jul 2015 . ATTACHMENTS HBCDD Testing Flow Chart 1) Name of the person who made testing: Gary Xu 2) Name of the person in charge of testing: Jessy Huang Sample cutting/preparation Sample measurement Solvent extraction Concentration/Dilution Filtration GC-MS DATA Page 11 of 19. Test Report. No. SHAEC1514782501 Date: 31 Jul 2015 . ATTACHMENTS PCB/ PCT/ PCN Testing Flow Chart 1) Name of the person who made testing: Brin Feng 2) Name of the person in charge of testing: Chaven Lian Sample cutting/preparation Sample measurement Solvent extraction Concentration/Dilution Filtration GC-MS DATA Page 12 of 19. Test Report. No. SHAEC1514782501 Date: 31 Jul 2015 . ATTACHMENTS Elements Testing Flow Chart 1) Name of the person who made testing: Bob Zhang/Sunny Qin 2) Name of the person in charge of testing: Summer Jin/Jan Shi Sample cutting/preparation Sample measurement Acid digestion Filtration Solution ICP-OES/AAS DATA Page 13 of 19. Test Report. No. SHAEC1514782501 Date: 31 Jul 2015 . ATTACHMENTS PFOS/PFOA Testing Flow Chart 1) Name of the person who made testing: Jane Yang 2) Name of the person in charge of testing: Myra Ma Sample cutting/preparation Sample measurement Solvent extraction Concentration/Dilution Filtration LC-MS DATA Page 14 of 19. Test Report. No. SHAEC1514782501 Date: 31 Jul 2015 . ATTACHMENTS PAHs Testing Flow Chart 1) Name of the person who made testing: Lisa Duan 2) Name of the person in charge of testing: Myra ma Sample cutting/preparation Sample measurement Solvent extraction Concentration/Dilution Filtration GC-MS DATA Page 15 of 19. Test Report. No. SHAEC1514782501 Date: 31 Jul 2015 . ATTACHMENTS SCCP Testing Flow Chart 1) Name of the person who made testing: Brin Feng 2) Name of the person in charge of testing: Chaven Lian Sample cutting/preparation Sample measurement Solvent extraction Concentration Clean-up Filtration GC-ECD/ GC-NCI-MS DATA Page 16 of 19. Test Report. No. SHAEC1514782501 Date: 31 Jul 2015 . ATTACHMENTS Halogen Testing (oxygen bomb) Flow Chart 1) Name of the person who made testing: Sisily Yin 2) Name of the person in charge of testing: Linda Li Sample cutting/preparation Sample measurement Combustion in oxygen bomb Dissolved in an absorption solution Filtration Analyzed by ion chromatography. Double confirm by other instruments, if necessary DATA Page 17 of 19. Test Report. No. SHAEC1514782501 Date: 31 Jul 2015 . ATTACHMENTS DMF (Dimethyl fumarate) Testing Flow Chart 1) Name of the person who made testing: Lisa Duan 2) Name of the person in charge of testing: Jessy Huang Sample cutting/preparation Sample measurement Solvent extraction Concentration/Dilution Filtration GC-MS DATA Page 18 of 19. Test Report. No. SHAEC1514782501 Date: 31 Jul 2015 . Sample photo: . SHAEC1514782501 SHA15-147825.001 . SGS authenticate the photo on original report only . *** End of Report *** . Page 19 of 19.