ICPTest_217XP_1 08 2013 pdf

ICP Test Report Certification Packet
Company name :
Littelfuse, Inc.
Product Series:
5x20 Cartridge Fuse
Product #:
217P Series
Issue Date:
January 8, 2013
It is hereby certified by Littelfuse, Inc. that there is neither RoHS (EU Directive 2002/95/EC,
2011/65/EU)-restricted substance nor such use, for materials to be used for unit parts, for
packing/packaging materials, and for additives and the like in the manufacturing processes.
In addition, it is hereby reported to you that the parts and sub-materials, the materials to be used
for unit parts, the packing/packaging materials, and the additives and the like in the manufacturing
processes, are all composed of the following components.
Issued by:
<Global EHS Engineer>
(1) Parts, sub-materials and unit parts
This document covers the 5x20 Fuse Rohs-Compliant series products manufactured by
Littelfuse, Inc.
＜ Raw Materials Used
Please see Table 1
(2) The ICP data on all measurable substances
Please see appropriate pages as identifed in Table 1
Remarks：
Form 585-047 Rev. A
1
2/21/06
Table 1: List of Raw Materials covered by this report
Total Parts
1
2
3
4
5
6
7
Raw Material Part Number
C910541
C910510
C909543
082xxx
687xxx
YTW206 (692529)
YTW102 (692535-002)
8
3M-3779-PG (087244)
9
EP608 (087335)
10
030204
11
934-077 (C030208)
12
13
14
15
16
17
18
19
20
C030210
425901
425902
425903
425904
425906
425907
425909
425913
Raw Material Description
Cap
Cap
Body – Soda Lime Glass
Element - Ag Plated Wires
Element – Copper Cladded Wires
Solder
Solder
HMA (RoHS
& Halogens)
Glue (RoHS
& Halogens)
Overcap (Cap base & plating)
Overcap (Cap wire base & plating)
Overcap (Cap base & plating)
Overcap (Cap wire base & plating)
Overcap (Cap base & plating)
Overcap (Cap wire base & plating)
Ink - Red
Ink - Black
Ink - Yellow
Ink - Blue
Ink - Brown
Ink - Green
Ink - Grey
Ink - Pale Blue
2
Page(s)
3-6
3-6
7-11
12-21
22-31
32-36
37-41
42-48
49-60
61-64
61-64
61-64
65-75
76-86
87-97
98-108
109-119
120-130
131-141
142-152
AOV"BPFS,U
TESTREPORT
R02
NO.:4002R12100802+1
Dare:ocr.10,2012
Customer:SuzhouFuHongElectronjc
InduslrialCo.,
Lld.
XIANGCHENG
DlsTRlCT,
SUZHOU,
CHINA
Addres!:NO.89WEIDUROAD,WANGTINGTOWN,
to
be
Reporton ths submitreds.mplesald
S.mplename:CoppeJ,shell
Mod€h/
Item/LoiNo.:/
Metarlal:/,
Buyer: / ,
Suppli€r:/
Samplorecaivsdd.te: Ocl.08.2012
1o'O4r'10,
2012
Testinsperiod:Ffomoct os,20!€
'\l
'
. . ,,
E9S!.s-Ecs!ed9!f
samplein
Chrcmium
contentin thesubmitled
& Hexavalent
As specifiedby dient, to determineihe Lead,cadmlun, Mercury
accordancewith Dircctive2002/95/EC{RoHS).
Ec!!!s-ee$9!.:
instrumeni I\4QL
Measunng
Testingltem
(cd)
Cadmium
(Hg)
[4ercury
IEC62321:2008,s€ction9
|EC62321:
2008,seclionI
7
lEc 623212008,seclron
Chromum(Cr\rl)
IEC623212008AnnexB
Lead(Pb)
ICP€ES
2-'nglkg
ICP-OES
2 mg/kg
tcP-oEs
2 mg/kg
0.02m9/k9'
Ieq
r 0.02mg/kgreE|sto theMQLofsampleextfaction
liquid
SsElcge!:
Decision
ol 18 Aug 2005
of commission
withthe requirements
-whentesledas speci{i€d
samplecomplied
the submitted
2005/618/Ec
noiiliedunderdocument
2002/95/Ec
Directjve
amending
ILS,PLEASEREFERTOTHE FOLLOWNGPAGE(S)***
signedlor andon behalfof
Brcncn
Co.,Ltd,Kunshan
Technology
Shenzhen
AOVTesling
We-r k] n
**n*"oor,
/blfil
caeateaaer:
LiTingting,Maggie
ooo,',*or44.
Ylan Qi, lrickey
Chemic€lTestDirecror
S I t E N 2 H E NA O V T f S I I N G T € C H N O I , O 6 YC O . , I " T O . K U N S N ABNR A N C T I
,
/// \ Noll ne
Ja,t 7tt) 9€'t'o
AOV'*F#S,[
TESTREPORT
NO.:4002R121008024-1
R02
Oate:Od.10,2012
1. To Determiney'.ead,
C€dmium
Contenli(Metalsubslrate)
I*redby (y'a04*
Weighihe sampleinto
Add ihe digestionsolulionithe
vesselis heatedunlilthe sample
AddHrOruntilthe
sampleis clear
nlter;washed
and
Cooling
thevess€|,
Rlled
wat€r.
10themarkwithdistill€d
To Dete
sulit€le)
Content i|retb.r
. \ .
The sampleis digestedin the
Weighihe sample
microwaveovenfollowinga specific
decomposrlonprogram
Tested
by lcP-oES
Coolingthe vessel,tiltei washedand
filledlothe maiKwilh dislilledwater.
ChromiumContenl(boiling-wat€F€xtlaclion):([4etalEubstrate)
Takethe (50i5) cm,
samplein the beaker.
Heat50 mLof Olwaterin
thebe6ker
to boilingfor 1o
F;;1.-
lhe sample,
andcool
Remove
thebeak€rto roomtemperature,
anddo thecolorreaction
Testthe samplesolutionand lhe 0.02
ng/kg standardsolltion by uv-vls.
BSANCH
lCCINOLOGYCO.,LTD.KUNSIIAN
SH€NZH€NAOVTESTITIG
(:
Hotlrne
'tL)0700 8600
nov'Bpf,F,il
TESTREPORT
NO.:
4002R121008024-1R02
Daie:Ocl.10,
2012
5. TooetemineHexavalenl
Chromium
Contonlin colorlessand coloredchromatecoatingon metats:iPtating)
_
.. -i\
: va'hu't'
lfthe lest resultis positive,
the sample is consideredto
havehexavalent
chmmium
Place
1-5
Boiling- water- extraotion
procedu€shallbe usedto
and the 0.02 mg/kg
lflhee is interference
or it is hardto decide
whetherlhesamplehavelhe hexavalent
5.2Boiling-wateF
enradion
Remove
thesample,
andcool
thebeaker
lo roomtemperalure,
anddolhe colorreaction
Heat50 mlof Dlwaier in the
samplein thebeaker.
beakerto boilingfor 10 min
Testtnesamplesolution
andlhe0.02
mg/kgstandadsolulion
by UV-VIS.
SampleDelcriptlon:
Code
1-1
SampleDescndion
Substrate
Plating
Te3tR63ulb:
Unit
RoHSLimit
Lead(Pb)
msfts
1000
N.D.
10
(Cd)
Cadmium
Merorry(Hg)
mg/K9
N.D.
ms/Kg
100
1000
N.D,
N.O.
N.D.
Chromium
{Crl,ll)
m9/kg
1000
Negative
Negative
s8€NZh€N AOVT€SrtNGTECHNOlOSYCO,,tTD,TUNSHAI!
ARANCH
,.r
Ho t l i ne
.100700B6a0
nov'F"Ff"qn
TESTREPORT
No.:A002R1210o602:L1
R02
-ThenewRoHSdircclive
2011/6tEU,on Jul.21,2011comeintoforc€,onJan.03,2013lheformalimplementation,
Direclive
repealed
2002r'95/EC
simultaneously.
ahallbe
Sp€cimens,
whichr€Slested
lo detemineLead,Cadmium
havebeendissolved
andMercury
Content,
completely,
-mg/kg=ppm ,
-N.D.=not
i",,,,,,
( The iested sample
resultis uncertain
or
neoatve.,
-"The te8t is bas€d on lhe followins d!!{mplifi:
maybe cannot stand lor the physical lrdh 6t s€r
Coppershell
SH€NZII
AFANCH
AOVTIST|n|GTECHNOIOCVCO.,ITD.KUNSHAN
Ho t l i ne
400 /00 8600
No.CANEC1207912201 Date:26Jun2012
TestReport
Page '1of 5
CO''LTD
ELEIVENT
XIAMENLICHUNELECTRONIC
DISTRICT,XIAI\,IEN''FUJIAN,P.R'C
WESTRD.,361O22,JIMEI
42_2XINGLIN
SODALIMEGLASS
The followjngsample(s)was/weresubmittedand identifiedon b€halfof the ctiens as:
- Xl\,1
xrvtl390111gEC
'18Jun2012
18 Jun2012- 26 Jun2012
Selectedtest(s)as requestedby client
SGS Job No. :
Date of Sample Received :
TestingPeiod :
Test Requested :
Pleasereferto nextPage(s).
Pleasereferto nextPage(s)
thgresultsof Lead'
samples,
testsonsubmitted
Basedontheperformed
(PBB)'
biphenyls
Polybrominated
chromium,
Hexavalent
Cadmium,
I\rercury,
RoHS
by
as
set
limits
with
the
(PBDE)
comply
ethers
diphenyl
PolybrominateO
200295/EC
Annexll; rec€sting
2011/65/EU
Direc{ive
Test Method :
Test Results :
C,onclusion:
Signedfof and on behalfof
scs-csrc Ltd.
ApprovedSignatory
:ffitili":;r,:1"'),i:;'"""ft1u1!'irlil"l'.:".-".:"^:;-:*;r::r"';',:""*i:::l;l,l:
iiiiirii$ii:iii:l+*tij'"$:ff.+#.,;1]:ii::T;.^.Ji{,*isi"iilj:ilii:{fiIj
isGs96s9f
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Ettt*eB*+tl&*C1e3!
sqeco6
' lgsdm@t{sd
rie20ls2075rl3
|
ml:\'0633 {6-201s?it55ss
Mombo.olth€SGSGroup(SGSSA)
lls-20)@075r13 @'i
510'63 i rs6-20ier56666
TestReport
No.oANEC1207912201
Date:26Jun2012
Page 2 of 5
Test Results:
Test PartDescriotion:
D€sc.l$ion
SGSSamplolD
Sp€dmonNo.
Transparentglasstube
CAN12'079122.001
1
Remarl..s:
(1)1 mg/kg=1 PPm=00001%
Limat
(2)MDL= MethodDetection
( < MDL)
(3)ND= NotDetected
(4) "-" = Po1P"n''"t"d
RoHSOit€dhe 2011,/66/EU
to IEC62321:2008
Testlvethod: with reference
bv ICP"OES
(1)Determination
ofCadmium
of Leadby ICP-OES.
(2)Determination
by ICP'OES'
of l\rercury
(3)Determination
MethodusingIJV-Vis'
by Colorjmetric
Chromium
of Hexavalent
(4)Determination
contentby GC-I\'S
of PBBS/ PBDES
(5) Determination
Test ltem(s)
Cadmium(Cd)
Lead(Pb)
Mercury(Hg)
Chromium(CrVl)
Hexavalent
Sumof PBBS
MonobrcmobiPhenyl
DibromobiPhenyl
Tnbromobiphenyl
TetrabromobiPhenYl
PentabromobiPhenYl
Hexabromobiphenyl
HeptabromobiPhenyl
OctabromobiPhenyl
Nonabromobiphenyl
DecabromobiPhenYl
Sumof PBDES
ether
Monobromodiphenyl
t!!i!
100
1,000
1,000
1,000
1,000
1,000
Unit
MO!
2
mg/kg
2
mg/kg
2
mg/kg
2
mg/kg
mgKg
5
mg/kg
5
mg/kg
5
mdkg
5
mg/kg
5
mg/kg
5
mS^(S
5
mg/kg
5
mg/kg
5
mS-ftS
5
mgikg
mg/Kg
5
mS/kg
001
ND
229
ND
ND
ND
ND
NO
NO
ND
ND
ND
ND
ND
ND
ND
ND
ND
+iifr
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TestReport
No. CANEC120791220'l
titri!
Test ltem(s)
ether
Dibromodiphenyl
ethet
Tribromodiphenyl
ether
Tetrabromodiphenyl
ether
PentabromodiphenYl
ether
Hexabromodiphenyl
elher
HeptabromodiPhenyl
ether
OctabromodiPhenyl
ether
Nonabromodiphenyl
ether
DecabromodiPhenyl
Notes:
Date:26 Jun 2012
udt
MDL
mg/Kg
5
5
5
5
5
5
5
5
5
ms,ks
mg/Kg
mg/Kg
mg/Kg
mg/kg
mg/Kg
mgK9
mg/Kg
Page 3 of 5
091
N
N
D
D
ND
ND
ND
ND
NO
ND
ND
Annexll
2011/65/Eu'
permissible
limitis quotedfromthedirective
(1)Themaximum
iiilttll$jf*:nii.l,irJg'fr*fiiq*ts**efti#*
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ATTACHMENTS
Page4 of5
Date:26Jun2012
No.CANEC12O7S12201
RoHS T€sting Flow Chart
'1)Nameof thepersonwhomadetesting:
BellaWang/ CuteyYu
AdamsYu/ RyanYang
of
testing:
in
charge
of
the
2t Name
berson
to belowflowchaft
methodaccording
dissolfu totallybypre-conditioning
ii in."" Lroriti
"tt"
excluded)
(cf' and PbBs/PBDEs
test method
SamplePreParation
SampleMeasurement
PBBS/PBDE8
Pb/Cd/Hg
Aciddigestionwith
rnicrowave/hotplate
Conc€ntration/
Dilutionof extraction
solution
1) AlkaliFusion/
DryAshing
to
Acid
2)
dissolve
Positive
and
Filtration
pH adjustment
'1,$
Adding
diphenyloarbazide
@lor
for
development
1,5Adding
diphenylcarbazide
color
for
development
color
red
A
the
indicates
presence of CF*
n€cessary,
I
with
confirm
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No.CANEC1207912201
Datet26 Jun2012
Page 5 of 5
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/ ' l r i b r o d o d i p } e n v l er h e .
B,*SiFa*
/ Tet ra6.onodi phe.vl erher
i;*Sxad
'r*S*a*
/ P e . r a b r o m o dDi h € " v l e t h e r
/ H e a a b r o n o dpih e r v t e r h e r
-k;A#Xa{
/ H e p t a b r o m o d iD h € n v l e t h e r
,\;*SXa{
/ o c r a b r o n o dD
i he.vl ether
,L;i#*e
i henvl etler
i N o n a b r o m o dD
+&#ii4
/ D € c a b r o n o d i D h e n velt h e r
623211
zoo$iiF, ,tfu|aE
+8dlf :*d,&jrl. / $ith rererence
ro IEC 62321:?008 and perforned
by rc/MS.
5
5
5
5
5
5
5
5
5
5
5
5
5
5
a* / s"l.s."
(fr.) / Halogen-Floo.ine(F) (c{s
6*
No.: 14?6?_94-8)
(5.) / Haloeen-chlo.ine (cl) (cAs
6*
! o . : 2 2 5 3 71- 5 - r )
& * ( * ) / H a l o r e n - B r o n i n e( B r ) ( c A S
l{o.: 10097-32-2)
50
ng/18
vx&+8fr
ltBs vt r4s82:2007,
50
/ sirh reference to Bs EN
{r}*t.
I 4 5 8 2 r 2 0 0 7A. n a l y si s v a s
50
(I) (cAS
6fr (dU / Halocen-lodine
No.: 14362-44-8)
conFiv;"
r 1 llu.,[r'r,
l: i/irr.r I i.tl
lt!,lr'i
oyglbredbb6ai.'alcondloisds
50
hrr.(s) rssbd rh s resr €pon ennd
lLr Lt[]!.
iq
3pdJb't}6lobc€da^dhsdocu
b
r**
,illt,rl
EIE{I
/ su! of PBtss
t*t**'ts
:14#*
:i*#f'
(Iethod)
ro
l ]tl|
]t
,F{a+E+
ff6(No.)
Test Report
: CE/2012l10835
aBlJzr.)
. 20L2/ot/71 Ftk(pare) : 1 of r0
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ELEKTROSCHUTZ(oVPO|iENTU\]BAU
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87, D,98669 VEITSDORF.GERVIIY
[]tl||t][]tI|
fiii(N.t.):
l . m g l k g: p p m ;0 . | w t %= l o o o p p n
2 _ n _ d . = N o r D e t e c t e d( * . t A r r )
3 - M D L: M e t l o d D e t e c t i o n L i r i i ( r l t l A ; { t s 1 8 1 6 )
4. '- = Not R"sulated (Sli,+&.6)
5 . r ' = Q u a t i t a t i v e a n a L y s i s( N o u n i t ) _ € , B r ) * f ( * + & )
6. #:
a . P o s i t i v e b e a ! s t l e p . e s e n c eo f C r V t o n t h e r € s t e d a r e a s
(po s i t i ve *,F rq,lit E q.tF jq r{ ,r{l rS)
b . N e g a t i v e n e a n s t h e a b s e n c eo f C i V I o n r h € r e s t e d a . e a s
( Nesat i ve i nr::tl*, E 4 t.tA ).14 'r1l1g )
T h e d e t e c t e dc o h c e n r r a t i o ni n b o i l ] n a - e a r € r - e x r r a c t i o sno l u t i o n i s € q u a l o r g r € a r e r t h a b 0 . 0 2
m A l k gw i t h
50 cn: tested ar.a". / li6;i{XA>0.02
nslka *iih 50 cm, (tested
z. tte.i,tlS{r.'Af
;F./.**isArxl:{,, *E+titi,sA,tt:ri}:+.Tftt 4 +1Erll+-ttlt aiAE.
(The sanples sas/were analyzed on behalf of the atfricant
! e s u l t s w a s / w e r eo n l y g i v e n a s r t e i n f o . n a t i t y v a l u e , )
PFos++*d,(R"f
Inf orlation)'
"'.o"€
(1) riitrrf rTfi.'|tsld.&n,r+r+4rrf,
as mixing sanpre in one resrine.
The above
!A+ 2oo6trzztEa (Di rect iae 2006/t2ztw)
d.Ee,Ed,rlE*tla+,i6d.n,+0.
005%.
(May not be placed on the market o. used as a sDbstance o. consrituent
€qual io or nigh€r than 0.005 % by nass.)
of prepararrons
(2rtit{ttX4n&*fi&}.ei+d."%d.6s{.*{r1+;1!i*€1+}aX*Jt+ApFosi.4t?J*fi}.e.t&r€t6€};l4pFosEE
,i.&+,i!d.i,ifo.r%,6*r&€d.4{tti.4rf. {,RprrsaAt*f + 6E*;Ad.Ji;Aruc/.,.
(Maynot be placed on ihe na.k€t in seni-linisned prodocts or articles, or pa.ts rhereof, if
ure
c o n c e n t . a t i o n o f P F O Si s e q u a t r o o r h i g h e . t h a n 0 . 1 % b y n a s s c a l c ! l a t e d s i t h r e f e r e n c e t o t l e n a s s o f
s t . u c t u r a l i y o . f r i c . o s t r u c r u r a l l y d i s r i n . r p a r r s t ! a i c o n t a i n P F o . so r , f o . r e x r i t e s o r o t h e . c o a r e d
naterials,
if thc anoun! of PFOSis equal to o. hiahcr than Ug/nr of thc coated nateriat.)
c o m p a ityr : ; r , r ; : i r l , , ; - f i t . r l J r . n i r r , . r , , t i i
Ltlttr
1i., r".l,r!/,)!
ont andub'n ihsh b orc en'3,ns
-.4ttr
- ! . ! , , : r r i r l l i - I. c i e o a F i
-:.r ;::rlnti,,;i+46iDr,ssr7
l
,rla#+
TestReport
ft,q(No.) : cE/20r2lr0835
E S ( D a t e ) : 2 0 1 2 1 0 1 / 1 1F * . ( p a s € ) : 5 o r l 0
EI-SCHIXOi,I
ELEKTRO€CHUIZKNTPONENTENMU
CVBH
GEIIERBESTInSSE
87, D 98669 IEIT,SDORF.GERILUY
tl&4!t(styl./I
[t[t
t.' N".)
(B-1) 101. 014
-silver
plated coFpe.{tre-Cu. Ag - - %
(B-2) 101. 0131. - - - - -pure silve. sire-Ag l()()()
( B - 3 ) 1 0 1 . 0 1 2 3 . 0- - - - s i l v e r
platcd purest nickct vire-Ni99.98%. AgI%
-silve.-copper alloy plated cotpe. clad vire-Elcon D,
(B-4) 10r,0182.0 - -silver
(B 5) 101.0120.0
p l a t e d c o n s t a n t a nw i i € - C u N i 4 4 , A A S %
( B - 6 ) 1 0 1 . 0 1 5 1 . 0- - - - c o p p e r - n i c k e t 4 4 a l l o y s v e r p l a r e d s i . e - c u N i 4 4 ,
c o D o a n tv l r I t ! . , r - N ' | , r " l : l , i l l l i
:. ! 1 1:;!1,1\
p sG)rssr€drh s€d Gpon€ind e
rlllrillrl.
!
ont 3nd*ii'n rh. hrs or c €nr s 'ns
ri.:l,;l-":Iq:j1
tl|
|||ll
,fl-d,#+
Test Report
f i { 5 ( N o . ) : C E l 2 0 1 2 l l o s 3 s E S ( D a r e ): 2 o t z l 0 r / t t F # ( p a s € ) :
ELSCHUI{OM
ELEKTROSCHUTZKOMPONENTENBAU
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8?, D 98669 WILSDoII, CERMA\Y
6
0 f l 0
[l|[]|l
r) ll?cr,-F $,EEn zI*1+ ' *.& aia*t+
. ( *1' j&d *tt *hrl. ) / Thes€samDtes
!,€€
d€sotuedrolrrryby p.e-condrumhgmethooaccodinglo betN nowchad. cP re€tmethodexcludeo
2) r.lri^l:
yang
$e ! / Naheotlneps6onwhomadenEsuremed:ctimbgreal
3) ir'13{I i ^ : tl4* / Nameof the pe6on in chargeormeasu€m€nlrTroychans
tr*. {rtt*s
/curing. p€galaton
iqr{.&,cf ! / sdde MeasuEmenl
&lf;F n l*'.g6tt{ f, 6 }xn!trai&it,tirt /LoeTt
4rt/!inlt n.i'la{&,aib /
4,;) /Acid dig€slion by suitabte acid dependedon
dtrerenlsahdemaledat{asbetowiable)
MiorcMve digestion with HNO3/HC|/HF
,"rl4rOf jit& jt.li,lilt +
C( / H€i to appropriate
1)
2)
f [*a{*4+*it{rtc
/ AlkaliF6ion
/HCltod$d€
/ rcP,aEs
f!911L / samdeMatedal
51eel,@pper,allnirum, solder
&ltgti
ta{*tt
;filt&AJlfi / DiqesL|onAcd
-t+, 4la{,!lt, nn*, el,,k /
Aa@ reoia. HNO' HCl. HF. H,O,
rra{,Inc / HNoJftF
A, J6,€, nit /
Gold,olalinum,
Dalladium,
ceramic
,i(f rf 7h-ir,g t.rLrlf,.' I
irl#B*i{Aftrcnm 6id
rti!€ /HNOr
&E / Plaslic
4?,*i&8tt$ / coot,
fherdigestate
lhrough
liher
*d, t{"*,
s!t, td / H,so. Ho,. HNorhcl
,! \'efi*1eti*l+
/ Anyacldlo lotaldig€Gtion
j i i r i r +
r i l , i ,
! . r 1 r . t p . l i , . 1 , i f i ' ! ! l .
rhcdddneiiAs€dbysgcompa^ys!b4d{ob6ai..a|condloi3ds
ab6o6anceat a/ronmby
UV-VIS
t]n]l
,F{a*R+
Test Report
iEIS(No.) : cE/2012l10835
E rr?(Dare) : 2012l01/11 F&(P,s")
ELSCHUKOMELEI$ROSCHUTZKOIIPONENTENB,qU
GMBH
CETERBESTRA.SSE87, D-98669 VEIISDORF, CER[{AI\'Y
t ttt*/t
rtt+4+f
l
*,aE / PBB/PBDE
anatyticat
FLOWCHART
a }l{,/\l
I a_i9*, / Nameoftheperson
whomademeasuremenl:
RomanWonq
r,$Ji( frt ^ : &+le / Nam€of thepersonIn chargeof measurement
TrcyCha;g
n^ ld,ElF / Firstlestry proce.s------------f
....,---.
prccess
€*,E&*€F / OptionalscE€n
-. -,t
*{.€,S / Confimation
orccess
:l
Scre€n
analysis
/ ,, rfi+rt
I
I
sample
erlraclion
*s+*/
Soxhlet
melhod6i,+tx;*
Concentrale/Dilute
Enractedsoluiion
+tri{ rira/ifi#
Filter/ +S.i{'E.d
Analysis
byGC/MS
/ fr"ian&f ie*,+&
*irl+
c o m D a n +! " , I
rirr,,: i;
r. lJ: ?.lria 1.:-!i
-j!,AlrI
3u!,0db'.ms,idcoidsdislolE
pslsl bdad h€rad cpod€nnorb3
i.,.-l:r311.!
|
|
t
l||tI
l
rF{-d,+E+
Test Report
f t 1 4 ( N o . ) , C E / 2 0 r 2 l 1 0 8 3 5E S ( D a r . ) , 2 o l 2 l l ] t / t t
F&{prse)
EI.SCHUI(OM
ELEI{TROSCHUTZ(OMA)NENTENB,{U
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87, D 98669 \,'EIT-SDoRF.GEf,Vl}IY
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I
Il]tIltt][||||[|!
/ Analyticalflowchartof halogencontent
jtli{,l.F : gi',g* / Naneof thepersonwhomademe€surement:
RitaChen
jrl:i,A ll, : #,*e / Nameof thepersonin cbargeof measurement:
TroyChang
*+E &t&.'sl'I
Analysis
wE6perfomedby lC
.Iir
Th s ddfuh.il
s '$u€d bl ft
np61s) rssbd fu bn cpod €nnor b
i.'.iiri:llr
it
Li
ii'!r]-l
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c om
3 l b j e d b ] e m s a i d c o i d l o n s f o r E A t a ^ l o n 6 d d n l o f t ] m l a t o n d s b l t y
.;.: r.r- i.1-]ii1
r,r+ s6iorre
rD r+ s6 Lo?lrrenr
wwslon
ilts,#+
TestReport
it4(No. ) : cE/2012l10835 AS(Dare) : 201210r/tr
F*.(pase) : 9 of lo
E-SCHUKOM
EI-E(TROSCHUTZKO]\IIONENTEN&{U
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87, D-98669 VEIISDORF, CERMA]\ry
tI|fll|t][taf,
*Ji+n+fin€n /
Analyticalflow chartofSoxhtetextraction(LC/MS)procedure
r
r
i A/-F : ij!9*y / Nameofthe personwhomademeesuementRcmanWong
t4j:{, q i,\ : tF'.*4 / Nameof the personin chargeof measurement:
TroyChang
( rd8,{ a : Afi.+n*.n/Afi.+rt(*)
, **.:4i{bA4,
Test ltems: PFOS/PFOA. Benzotriazole)
*{*
cmpanyr:i r , tr 'ri_ll i ,r'"'ll:l ill+
r. r i rtirril: .
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TestReport
fi6(N". ) , c-E/2072/10a35
Es(Date) : 2tr2/ar/r1
E*@aEe) : r0 of t0
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8?, D.98669 WII-SDOTF,GERVA}Y
trlt[tl
+ ffifi tr'6*t*i
' Fl* ftfrfl*lt,rlz{tsi
(The tested sanple / part is narked bt an arror if
ir's
1083s
10835
** lE+344.(E"d of Report) ++
i:. j:r.i | ,.tll
itt: I
c d h p , i in r . i ' , r , " r i l ' i , ,
rhsdoarudE 3s!sdbyhe.omp,^yeqedb G6erydcodromor s
+ *ri.*irr !r. i r,.
l6en,a r,p.
'
..
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${i'
t
shorn on rhe photo.)
fl|||trr
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Please
,Ffff,*r+
i B 4 q ( N o ). : C E / 2 0 1 2 l 1 0 8 3 6
Test Report
Efi(Date):2012l0r/11 q l t ( P a s e ) : 1 o f 1 0
E-SCqIKOI,IELE](TRqSCHUTZKOI,IIININTENBAU
GMBH
GEIERBESTIAS,SE
87, D-98669 \aEILSDOnr, CrnUrry
t(Ttjd,&sfi &*r,t&,
ide!tified
-eAfP +*trE*P **iT
by/o! behalf oI the clie!t
D€s-ipt ion)
*.gZt*(sanple
iS.S4*,(StyLe/Iten No.)
,FE g(coontry of orisin)
&+ A S (s,'pl. Receivins Date)
,rli{S Fl(res t ins Pe.iod)
irli*
rr|||l|rl[[ttf,]l!
jF(rest Resurts)
,
(Th€ fol Iori!t
6aDples eas/rere
6uboi t t€d and
as) :
COPPERCLAD & COPPERNLTO] WTRIS
(PLEASE
RFERTo PAGE5)
fi++XsA.
(GER
A},Y)
ftg
20L2/0L/04
2 0 L 20/L/ 0 1 ' , l O2 n r 2 / O Ir r/
;t4.T-E
(Ple"'e rerer .o nex, rasc")
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i *frreir 'i*lj:r
,. rrl
,t 1,1
',1i
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iird
r
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,
p€(3)€iad rb66d rcpod €iidb'
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,r||H,*E+
ier6(No.) : cEl2012l10836 A S ( D a t e ) : 2 0 1 2 l o l l r l
Test Report
F*.(Pace) : z or to
i||lr[t
ET.SCHIJKOM
ELEKTROSCIUTZKOMPONENTENB,{U
CVBH
GENERBESfiNSSE
87, D.98669 VEILSDORF,GEL\LAIY
t :ll**.(Te.t
xl l{S&
R e . t rt t . )
(PAlr Nr'uE) No.l :
'e,i fiaee&,a&
(a4b?) (*16*) (lrxEDALLcoroRMErAL
$rRE
(INCLUDING
THEPLATINGL{YM) (T6 TYPES)
)
j0d,Zlt
+.fn
,r'l$,f E
(U!i t)
$
(uethod)
+ + r E r6. z s z rz:o o 8 t * , , 1 6 4 *
A€{4 +*4t,t,;*d,&,tl. / $irh
/ cadniun (cd)
( R e s u lt )
(lDL)
No.l
2
reference to IEC 62321: 2008 and
perlorned by ICP-AIS.
,5
+*rDt 6232L'2oo8ttA, ,r(&,6F
r
A{*AA44I{*&A:.1.
r e f e r € n c € t o I E C 6 2 3 2 r : 2 0 0 8"i,n
and
/ Lead ( Pb)
perforf,ed by ICP-nnS.
4+Is. 6232rt2008rii. /,*Bl4
/ {i ih
+€tF+*4i{r*'ft*xl.
*. / vercury (Es)
2
reference to IEc 62321: 2008 and
pe.forn€d by ICP-A!S.
++tgc 6232r.2oo9fit, r/)k,Y"4
7i'llr& / nexavalentchroniun cr(vI)
4.i*lt;Fl. / rith ref€rence to IEc
62321: ?008and perfor0€d by
BoiI inE water extraction Merhod,#
An+R&*
sulfonat€s
4+us EPA35.10C,1996ti4, 'Xr{
/ Perrluoroocta.e
h.t 44f, ;*A,if :rlAfl.*R tt&+E.
( P F O S - A ci d , M e r a l S a l t
/ Iilh referen.e 16 us EPA 3540C:
1 9 9 6 n e t h o d f o r P F o SC o n t e n t .
Analysis sas perforned by LCINS,
ift+d.(14)
/ PFoA(cAsNo.: 33s-6?-
4+US EPA35a0c:l996tii,
,)(t{
4fr.+c(J*)n&
iEafi J{:*.t*,tairl
1)
/ s i t h r e f e r e n c e t o U S E P A3 5 . { 0 c
1 9 9 6n e t h o d f o r P F O AC o n t e n t .
Analysis vas perforned by tClMS.
c o m o a n+vj l 1 / n r l , r r , f ' | , 1 , i : 1 f i l r ,
r.I ltri{::
ny ssbled io b GeneG cond[dns d se
on|yandw$|.lhelmcolc6i|sns
bi€d rh s €d €Podennd e
PrsG)
- _',1 r!t!,.!'
s*
t*{t j{
f;Ed
l0
Nun[ll|
,fl.d,+E+
Test Report
lE*r(No-) : CE/2012/108s6
ES(Dare) : 2012101/11 F&(pase)
ELSCHUKOIELEKTROGCHUTZLOVPoNU,ITINtsAU
G[tsH
GEWERBESTMSSE
8?, D-98669 VEIISDoRF,CERMANry
jnd,{ E
+'fs
I|lt|||||N ||[l
j{nt*
(Unit)
t ilt**#
-iAlfi;F
:AS*
€;ESX
t;9#E
'i;A#*.
/ Sut of PBBS
/ M o r o b r o n o bpih e n y l
/ D i b r o n o b ir h e n y r
/ T ri b r o n o b
rphcnyl
/ Tetrabronobiphenyl
/ P € n t a b ! o m o bDi h e n Iv
/ H e x a b ! o m o b i p h eLn y
-Lill$*
/ H e p t a b r o n o b ip h e n y l
:iAlft*
tthlt j{
fi E,it
(rDL)
/ o c t a b r o m o bpi h e n y l
bh e n y l
, , , L A S * ' / N o n a b r o n oi p
/
D
e
c
a
b
r
o
m
o
biphenyl
iA$t
:AS8d
++r!x 6232t,zoo9tit, ,\^lBE
*f&,/lf*A.Axl. / x,ithr€r€.€n€e
p ih e n y l e t h e r
/ Monobronod
/ D i b r o m o d i p h e n€y(Lh € .
:i*d86d
/ T r i b r o n o d i o h e n vI e r h e r
qAdSEt
/ T e r r a b r o n o d , p h € neytlh € r
/ P e n t a b r o n o d i D n e r v€l t h € r
A;&l$ri6{
^;&ISliAC
t,Flfi;.a*
^*lSX.6t
/ octab.onod
/ Nodabfonod
**#XEn
/ o"catronoa
5
5
5
5
5
5
5
5
5
5
5
/ H e x a b r o n o d io b e n v l e t h e r
/ Heolab.ooodi lh€nvl ethe.
,L*SXAt
air
to IEC 62321. 2008a,d p€.lorhed
by GC/MS.
/ suo of PBDES
t ttfltlltrfr
No.l
5
5
5
5
5
5
5
5
^tA#f
-_A#Xi4
$*
(Resul t )
/ Halo..n
(fl.) / Halose!_Fluori.e
6*
N o .: 1 4 7 6 2 - 9 4 - 8 )
(F) (cAs
(fi") / Haloser-chlorine (cl) (c'{s
6*
!o.: 22537-15-1)
(;i) / Halos€.-Bronine(Br) (cAs
&l
N o . : 1 0 0 9 73 2 2 )
(4t) / Halogen-lodin€(l)
6*
50
r,lrt+,gff
4+Bs ENr4582:2007,
ag/(t
50
/ I[ith .efe.ence io Bs EN
&r)fi.
1 4 5 8 |22 0 0 ? .A n a l y s i s{ a s
(cAs
50
No.: 14362-44-8)
c o m D a n; "v, r 1 r i | l , f _ a { l , r . r r , , Jnt i j l r : r ] . 2 j i
ii!.fli,
r . 1rr rrlJLl.
r i r : ' I l l l ) . : l : , i l t . , i + s 6 i o n r * r 7 e r + s 6 o r ) r e e r rv t u { r @ h
t
n{'d,#+
TestReport
frq(No-) : cE/201?/10836 g i ! ( D a i e ) : 2 0 r 2 l o r l r l F * . ( P a r e ) ; 4 o f l o
EISCHIJXOI'{
ELEKTROSCHUTZKO\{PONEI\'TENBAU
GYBI]
GEWERBESTRASSE
8?, D-98669 VEIT,SDoRF,GERMANry
lllIrIlrl||||u[tl|l
fiii(Note):
1. nglkg = ppni 0.lwt% = 100oppn
z. n.d. = Nor D"t.cr.d (*.ifA)
3 . M D L= M e t t r o dD € r e c t i o n L i n i r ( t t i l F x l E f B l & )
' : Nor Resulated (**ei'.ii.)
,t.
.
.
=
5.
Qualitaiive analysis (No u.ir) €,I4r)tt(*+dn)
6, # =
a. Posjlive
(Posi t i
b,
"e*. +;r{ 3t E &,1i,rl t{ ,r.ll r8)
Negative
(Nesa
ti
Eeais the Fresence of CrVI on rhe tested areas
neans the
absence of
C.VI
on rhe
iesied
areas
"€e + iri:;l E ii. i1A trlt{ '\fiJ} )
The d€tected concentration in boiling-water-ext.action solutibn is equal or sreate. th:n 0.02 bglkg with
50 cm, tested areas. / lii)*i{,i,8=0.02
malks sith 50 cm, (tested areas)
7. *l s 0t,nl?i,t.
A+ + if ^*,i,E 6tFl:lt' *r+ f ftliEe;il*,3*
+rri.a4f&r!
+-titr 616s.
(The satuples sas/{€re anaiyzed on b e h a l f o f l h e a f p l i c a n t a s n i x i n s s a m p l €i n o n e t e s t i n g . T h € a b o v e
r e s u l i s w a s / w e r eo n l y g i v e n a s t h e i n f o r n a l i l y v a l u € . )
PrOs++itfi.(Refer."ce Inforiatior)
(Directive 2006/122lEc)
. lE+ 2006/122/FL
(1) :**r( 6irE,ai4-Ld..n,s :ar+*lrf d.Ec.Er\rl**r*a++{.i'i+o. 00s%.
(Maynot be placed on ihe oarket or used as a srbstanceor constituent of preparations in a €onc€ntratioi
€qu,l io or !igher lhan 0.005 % by nass.)
(2,t hY4q&*fr*rii+d.sd.fi"%4.*#r{+r 1kr5e+rExfirt4ApFosltti€,*+6-La&.rElt€_LitSPFlsg&
i.lA+,Ad.ri^0.1%,d,1&& A,t+!-&6,*,9,t'*Isos.arts't f + Al+Ad.d,Arus/".
(May.ot be placed on th€ narke! in seni finished products or a.ticles, or paris rh€reof, if the
concentration of PIOS is equal to or hiab€r than 0.1 % by nass calculated *ith r€ference to the nass of
s t r u c t u . a l l y o . n i c r o s t r u c t u r a 1 Ly d i s t i n c t p a r r s r h a t c o n t a i n P F 0 6 o r , f o ! t € x t i l e s o r o t h e . c o a t e d
naterials,
i f t b e a m o u n t o t P F O Si s e q u a l t o o r h i s h c r t h a n l U s / n : o f i h € c o a i e d n a t e r i a l . )
c o m o a n4v , r / t r , , t - i ' : , 1 " : i : ! n l r r i
, I
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t A , 4 ( N " . ) c, E / 2 0 L 2 / t A A 3 6
E&(Date):20I2l0r/11
FjR(P:se):5ofro
tl|
ELSCIIUKON
ELEKTROSCHUVKO]{PONENTEN&CU
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t e o N o .)
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( c - 1 ) 1 0 1 . 0 1 7 7 .o ( c - 2 ) 1 0 1 _0 1 8 3 . 0 ( c - 3 ) 1 0 1 . 0 1 ? 2 .0 ( c - 4 )r 0 r . 0 r 8 r . 0
( c - 5 ) 1 0 1 . 0 1 3 2 -. ( c - 6 ) 1 0 1 . 0 1 3 1 . 0(c-?) 101.01?1.0
( c - 8 ) 1 0 1 . 0 1 3 s -. ( c - 9 ) r 0 1 . 0 1 5 7 .0 ( c - 1 0 ) 1 0 1 . 0 1 3 6 -. (c-11) 101-- 064. ( c - r 2 ) 1 0 1 . 0 1 6 6 -. ( c - 1 3 ) 1 0 1 . 0 1 s 8 -. ( c - 1 4 ) 1 0 1 . 0 1 6 1 -. ( c - 1 5 ) 1 0 1 . 0 1 5 5O
.
( c - 1 6 ) 1 0 1 . 0 1 2 8 0. -
cdpaiy:
copper tin alloy wire CuSn6
copper cLad{ire - Elcon 30
coppcr cLad steel wire - Elcon F
copper clad iron-nick€l-alloy si.e
Elcon D
silve. copper alloy wire
AgC!50
silver copper alLoy wi.e Agcugo
.opper vire
Cu99.9%
silver copper alloy wire Ag72Cu28
copper-zinc-alloy
wire C u 8 0Z n 2 0
.il'er copnerallo/ ri-F A g 4 5 C L 5 5( A g a L 5 5 )
-
copper plared, brass plared sp.ing-steel wire silver copperalloy sire
A 8 c u 7 0( E l c u 7 0 )
silv€r coppe. alloy vire
ANu80 (Elcu8o)
oxyaenfr€€ copper vire
OF Cu
copper-,in.-alloy
vi.e
C!70 Zn30 (Vs 70)
tungsten Furiry uire
lV
1 1lt r-ll i,,r i;.llilr'i 1!.I11 1ir..l:
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Climbg€atYang
3) ,Ilit I t ^ . t[4* / Nam€of the personin chaqe of measuRent Trry Chans
tri{ ' {I*i*.s /Cutins.Pl€ aBlion
idnt*stl
/ Sample
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f.f,1. Fl*e $tl f ,6,x,af 6lriG lifi lt (:{'T,i.
ti) /Acid digstion by suilableaciddepeded on
direren!ssmde maiedal(as belowlable)
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ftt6(No.) : cE/2012l10836 E S ( D u t " ) , 2 o l 2 l 0 1 / 1 1 F * . ( p a s e ) : z o r r 0
ET,SCIIUKOMELEK'|RGSCHUTZKOMPONENTENMU
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anaryticat
. ,|l:{,,i.F I 44ry / Nameoltheperson$ho mademeasurement
RomanWong
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T'oyChang
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prcc€ss
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RitaChen
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AS(Date):2012l01/ll
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r
I
ic|l:{ -F: Ai4# / Nameof theperconwhomademeasurement
RomanWong
tll*,Atl.:
tiBF / Nameof thepersonin chargeof measurement:Trcy
Chang
( ls'{ E: AE+H,*.t/An+*(s)' *it:4i{E6&
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T€stReport
No.SHAEC1216714738
Page1 ol5
Date:25 Sep 2012
CO.,LTD
MATERIAL
SOLDERING&BRAZING
ASIAGENERAL
ZHEJIANG
CHINA
PROVINCE'
CIry' ZHEJIANG,
HANGZHOU
PARK,SANDUN,
XIHUINDUSTRIAL
SoLDER
The following 6ample(s)was/were submittedand identifiedon behalf of the clients as : LEAD-FREE
WIRE
Dateof Sampl€Received:
TestingPeriod:
TestR€quested:
- SH
sP12-028285
YTW2O6
sno.3Ag0.7ouce
21 Sep2012
21 s,ep2012- 25 SeP2012
Selectedtest(s)as requestedby client
TestMethod:
Pleasereferto nextPage(s)
T€stResulb:
:
Condusion
Pleasereferto nextPage(s).
Baa€don the perfomedtestson submittedsamples'the resultsof Lead'
(PBB)'
biphenyls
chomium,Polybrorninated
Hexavalent
I\rercury,
Cadmium,
RoHS
by
limits
as
set
with
the
diphenylethe6 (PBDE)comply
Polybrominated
200295/EC
Annexll; recasting
2011/65/EU
Di.ective
SGSJobNo.:
PartNo.(PN) :
Compositlon:
Signed for and on b€half of
scs-csTc Ltd.
/Qv''
.n#ffiffi
Fan Jingiie,JJ
Approved Signatory
irmr
r* u-ra
-td *vot
tirtDafi$EE|ihtltrorr
il.t.|.*f,Ertr€€.lt$l
rmrr.t.t t*
zxtao
ll@3
tErEl@llitldt6!E{ti"clt06t'9
Kr(,-tt)Eaffi
xr.c+rti el
iLnlirotllt
ffior*ofr
1j!ltorSOSOtbt4 (aGS8A)
T€6tReport
No.SHAEC1216714734
Date:25 Sep2012
Page2 o15
TestResults:
;
TestPertDe€criotion
S@rn6n No,
1
D6ctiptioi
SGSSampl€lD
wire
SHA12-167147.035Silvery
Rgmarks:
(1)1 mg/kg=I PPm=00001%
Limit
(2)MDL= MethodDeteclion
(3) ND = NotD€teded( < lrDL )
(4) '-' = NotRegulated
RoHSDllBdivs201l/85/EU
Test Llethod
with referenceto lEc 62321:2008
(1)Determination
of cadmiumby ICP-oEs.
(2) Dete.mination
of Leadby ICP-oEs
(3) Determination
of Mercrlryby ICP-OES.
(4) Determination
Chromiumby Spottest/ Colorimetricl\,ethodusingUV-Vis
of Hexavalent
by GC-[IS.
(5)Detemination
PBBS
i
PBoES
of
Limit
100
1000
1000
Test ltem{s)
Cadmium(Cd)
Lead (Pb)
Mercuryfig)
HexavalentChromium(Ci(VD)
UlE
mdkg
ms/kg
ms/kS
mS.ftS
mS/kS
mdkg
mdkS
mSikS
mdks
ms/kg
mg/kg
mdkS
msikg
mdks
mgftS
mg/KS
1000
-
Sumof PBBS
Monobromobiphenyl
Dibromobiphenyl
Tribromobiph€nyl
Tetrabrornobiphenyl
PentabromobiPhenYl
He/€bromobiphenyl
HeptabromobiPhenyl
Octabromobiphenyl
NonabromobiPhenyl
DecabromobiPhenYl
SumoI PBDES
ether
Monobromodiphenyl
1m0
-
5
5
s
5
5
5
5
5
5
5
5
ND
50
ND
N€gative
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ffi
ffiffi:ffi
g"fff
###f
rffi
!#,g;"EHT*
*,Hffi
ffi Stift
Ufi
*lvl*sm.1m*ts""nr*
#ffi*,rx*$'#'ffi
Ij*tffi
b D.r. na co{d6
;;bii*hEni-.6fr
l\rDL
2
2
2
o
Sffi*ff
d tbtk
*r I
r6tr.{.)r-H
tt-ErrlFYasft.cxd|lt.9|dlcrn
+l -l|.*tr[lt|fte||6+l
zfrlr3
lr:2@
tElEF{lF6tl
rd€6+1)6r.@
Hit!-2l164@raa it{&aFl@
(8cgs )
lr.nD.t o1$.8GgOrouP
Tes{Report
No. SHAEC1216714738
Test ltem(s)
Dibromodiphenylether
Tribromodiphenyl
ether
Tetrabromodiphenyl
ether
Pentabromodiphenyl
elher
Hexabromodiphenyl
ether
Heptabromodiphenyl
ether
Oc-tabromodiphenyl
ether
Nonabro.nodiphenyl
ether
D€cabromodiphenyl
ether
thi!
Date:25Sep2012
UdT
MDt
mdkS
mdkS
mdkS
mdkg
mS/kg
mSikS
mg/kg
mS/kS
mgkg
5
5
5
5
5
5
5
5
5
Page3 of 5
@
ND
ND
ND
NO
ND
ND
ND
ND
ND
Notes :
(1) The maximumpermissiblelimitis quotedfromdiredive2011/65/EU,
Annexll
(2) ospot{est:
Negative = Absence of Cr(Vl) coating, Positive= Presenceof Cr(Vl) coating;
CIhe tested sample should be fudher verifed by boiling-waterextractionmethodif the spot test result
is Negative or cannot be confirmed.)
oBoiling-wateFextraction:
Negative = Ahsence of Cr(Vl) coating
Positive = Pesence of Cr(Vl) coating;the detectedconcentrationin boiling-water-ext€ctionsolution is
equal or greater than 0.02 mgl(q with 50 cm'zsample surtace area.
For corrosion protectioncoatingson metals: Informationon storage conditionsand producliondate of
the tested sample is unavailableand thus results of Cr(Vl) representstatus of lhe sample at the time
of testing.
t'ilt,b.aYrbto
+1
drchrbrd,Swaon
!e3a
I ErE{O-Zr)OtrOO
raEFaFffiTl
*FA)ala@!.a |{j{l.?J)6r@
M.m!.rorh.scsGtuc(acgs
)
TestReport
No.SHAEC1216714734
Page 4 of 5
Date:25 S€p2012
ATTACHMENTS
RoHSTe€tingFlowChart
xu
Xiao/Gary
Wang/Allen
JanShi/Yoyo
1) Nameof the personwhomadetesting:
Xu/LindaLi
'
2i Nameof thebersonin chargeof testing:JeffZhang/George
chart.(Cf
to berowflow
accorcting
6'ypre-condit-roningherhod
totarry
aissoried
iiiii,"i !!rir!!,i.
testmethodexcluded)
andPBBdPBDES
SamplePrcparation
SampleMeasurement
Pbrcd,Hg
PB86fPBDE8
Acid digestionwith
microw€ve/hotplate
Concentration/
Dilutionof extraclion
solution
'1)AlkaliFusion/
DryAshing
2) Acidto dissolve
Adding1,s
diphenylcarbazide
for color
development
A red color
indicatesthe
presence
of cP'.
neceas€ry,
confirmwith
tr
'l';-;Ltidbd$rffi'd6.h*lhE.,nrdri*6
tilairl$gYb.rto dErloat4ltrtracnr 20(43
a|lM
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rEtEFzr)0tac53 rE&&4lrsa
l+{a-a)dlqaa rtjF.?1)6@
$6nb.fol th.ao6 GlDlD{8oas )
TestReport
No.SHAECl2'16714738
Date:25 Sep2012
Page5 of 5
Samplephoto:
sHA12-167147.035
SGSauthenticato
the photoon originalreportonly
'* Endof Report""
(d-l!r.
.Dor
-iibhihr.ldcn.h,
'|l!!a|i!!{l|ddbd'
,td.lwb|||d4ded
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tr.tl.*tr6l||,|rF|6r+l
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ll: @3
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.,9d'rt.l.-
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TestReport
No. SHAEC1216714749
Date:25 Sep2012
Page1of 5
ZHEJIANG
ASIAGENERAL
SOLDERING&BRAZING
I.iIATERIAL
CO.,LTD
XIHUINDUSTRIAL
PARK,SANDUN,HANGZHOU
CITY,ZHEJIANG,
PROVINCE,
CHINA
The followingsample(s)was/weresubmittedand identifiedon behalfof the clientsas : LEAD-FREESOLDER
WIRE
SGSJobNo.:
PartNo.(P/N):
Composition
:
Dateof SampleReceived:
TestingPeriodI
- SH
sP12-028285
(692535-002)
YTW'102
TestRequestedI
Selecledtest(s)as requestedby client.
Test l\relhod:
Pleasereferto nextpage(s).
Pleas€referto nextpage(s).
Basedon the performedtesb on submitteds€mples,th€ resultsof Lead,
(PBB),
biphenyls
cfiromium,
Polybrominated
Meroiry,Cadmium,
Hexavalent
(PBDE)
withthelimitsas setby RoHS
comply
Polybrominated
diphenylethers
200295/EC.
Annexll; rec€sting
Directive
2011/65/EtJ
Sn2.ocuRE
21 Sep2012
21 Sep2012- 25 Sep2012
T€stResults:
:
Condusion
Signed for and on bohalf of
SGgCSTC Ltd.
.,/1,-
,rt*{'""^
FanJinqjie,JJ
ApprovedSignatory
H,
',E
l.db&o-d
cdd|{d. orswI6
frqiiffi*#r"r#H'ffil'ft1#l'l'Id*i,ffi
t.Uiltrar|$&r,lrnllq,gldicti!
*l '.tf. *ir8l'lraast3rtll
@
ar:M
M6t{rm
tEl€(S{1)t1{q60 l6lE(E-llF{S't9
Hljfi.2l)614&r04rl!(s-n)$5d83''q9dmFdl
(SGssA)
Momlarolth. SGsGloup
TastReport
No.SHAECl216714749
Date:25Sep2012
Page2 of 5
TestResulb:
TestPartDescriotion:
Sp6dr|on No.
1
SGSSamplolD
Dgcriptio.l
SHA12-167147.042
Silvery
wire
Rema*s:
(1)1 mg/ks=1 PPm=0.0001%
(2) lrDL = LlethodDeteclionLimit
(3) ND= NotDetected( < IVDL)
(4)'-" = 1o1q*r,","d
RoHSDlrB.dv€2011/55iEU
TestMethod: Withreferenceto IEC62321:2008
(1)Determination
of Cadmium
by ICP-OES.
(2) Determination
of Leadby ICP-OES.
(3) Determin€tion
of l\rercuryby ICP-OES.
(4) Deteminationof Hexavalent
Chromiumby Spottest/ Colorimetric
MethodusingUV-Vis.
(5)Detemination
of PBBS/ PBDES
by GC-[IS.
Testltem(s)
Limit unit
100 msfts
1000 mdkg
Cadmium(Cd)
Lead (Pb)
Merd.iry(Hg)
(C(Vl))
Hexavalent
Chromium
Sumof PBBS
Monobromobiphenyl
Dibromobiphenyl
Tribromobiphenyl
Tetrabromobiphenyl
Penlabromobiphenyl
Hexabmmobiphenyl
Heptabromobiphenyl
Octabromobiphenyl
Nonabromobiphenyl
Decabromobiphenyl
Sumof PBDES
Monobromodiphenyl
ether
,o:o *1*
1000
_
1000
-
mdlQ
ms,/KS
mg/Kg
mg/Kg
mgxs
mg/Kg
ms/Kg
msfts
mg/Kg
mgKg
mgKg
mg/kg
mg/Kg
MDt
2
@2
N
D
2
1
n
2
o
-
N
D
Negative
N
D
5
5
5
5
5
5
5
5
5
5
-
N
N
N
N
N
N
N
N
N
N
N
D
D
D
D
D
D
D
D
D
D
D
5
N
D
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TestReport
No.SHAECl2'16714749
T6stltem(s)
Dibromodiphenyl
ether
Tribrcmodiphenyl
elher
Tetrabromodiphenyl
ether
Pentabohodiphenyl
ether
Hexabrcmodiphenyl
ether
Heptabromodiphenyl
ether
Oclabromodiphenyl
ether
Nonabromodiphenyl
ether
Decabromodiphenyl
ether
thi!
Date:25Sep2012
llil
MDt
mg/kS
mg/kg
mSikS
mg/kg
mg/kg
mg/kg
mg/kg
mg/kS
mg/kg
5
5
5
5
5
5
5
5
5
Page3 of 5
g2
ND
ND
ND
ND
ND
ND
ND
ND
ND
Notes :
(1) The maximumpermissible
limitis quotedfromdiroclive2011/65/EU,
Annexll
(2)
"spot-test:=
Negative Absence of Cr(Vl) coating, Positive= Presenceof Cr(Vl) coatingi
(The tested sample should be further verified by boiling-wateFextractionmethod if the spot test result
is Negativeor cannot be confirmed.)
oBoiling-wateFext€c{on:
Negative = Abs€nc€ of Cr(Vl) coating
Positive = Presenceof Cr(Vl) coalingt the detectedconcentrationanboiling-water-extractionsolution is
equal or gre€ter than 0.02 mg/kg wilh 50 cm':sample surface area,
For corosion protectioncoatingson melals: Informationon storage conditionsand productiondate of
the tested sample is unavailableand thus results of Cr(Vl) representstatus of the sample at the time
of testing.
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T€€tReport
No.SHAEC121671474S
Date:25 Sep 2012
Page 4 of 5
ATTACHMENTS
RoHSTestingFlowChart
1) Nameof the personwho madetesting:Jan Shi/YoyoWangy'Aen Xiaor'caryXu
2) Nameof the personin chargeof testing:Jeff ZhangJceorge
Xd LindaLi
3) Thesesamples
wereda66olved
totallyby preconditioning
methodaccording
to betowflowchad.(Cf'
andPBBS,/PBDES
testmethodexcluded)
Sample
I\reasurement
Pb/CdrHg
PBB8/PBDEs
Nonmetallic
mateial
Concentration/
Dilution
of extraction
solution
1)AlkaliFusion/
DryAshing
2) Acjdto dissolve
Adding1,5diphenylcabazide
for color
development
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A red color
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necessary,
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Test Repori
Page5 of 5
Date: 25 Sep 20 12
No.SHAEC1216714749
Samplephoto:
sHAl2-167147.042
repodonly
thephotoonoriginal
SGSauthenticate
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TestReport
No.TSNEC1200272601
Date:09Apr2012
Page 1 of I
BEIJINGHYSTICNEW MATERIALSCO,,LTD.
5 SHUANGYUAN
ROAD,BADACHUHIGH.TECH
ZONE,BEIJING,
100041,
cHtNA
Thefollowing
sample(s)
was^^/ere
submitted
andidentified
onbehalfof thectientsas : EpOXyADHESTVE
- TJ
SGSJobNo.:
TP12-004950
l\rodelNo.:
Dateof SampleReceived:
EP6O8
3l Mat2012
31Mat2012- 09 Apt2012
Selecledtest(s)as requestedby client.
TestingPeriod:
TestRequested:
TestMethod:
Pleasereferto nextpage(s).
Pleasereferto nextpage(s).
TestResults:
Basedontheperfomedtesb onsubmitted
samples,
theresutts
of Lead,
Mercury,
Cadmium,
Hexavalent
chromium,
Polybrominated
(PBB),
biphenyts
Polybrominated
diphenyl
ethers(PBDE)
complywiththelimitsas setby RoHS
Directive
2011/65/EU
Annexll; recasting
2002/95/EC.
Conclusion
i
Signedforandon behalfof
scs-csTcLtd.
O\
N6'(
AimyWang
ApprovedSignatory
rh!do.!n'lt6!.d5ylh.con!.iy
'id !' .drdoi r.i,.; dsr..d 't.,.h
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I iis
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rloA,Ti.njn china3ol4s7 r 13t2?66233000
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M e m b e rrohl.S G S G o l p { S GSSA I
Te€tReport
No.TSNEC1200272601
Date: 09 Apr 20 12
Page2 ol8
TestResults:
TestPartDescription:
Sp€d.n€nNo.
SGSSsmplelD
D€6criplion
1
TSN12-002726.001ivory-white
paste
Remarks:
(1)1mg/kg=1 ppm= 0.0001%
(2)IIDL = MethodDetection
Limit
(3)ND= NotDeteded( < MDL)
(4)"-' = 1o1q"nu,","o
RoHSDirodive201t/66/EU
TestMethod: Withreference
to |EC62321:2008
(1)Determination
ofCadmium
by tCP-OES.
(2)Determination
of Leadby ICP-OES.
(3)Detemination
of l,rercury
by ICP-OES.
(4)Determination
of Hexavalent
Chrcmium
byColo metricMethodusingUV-Vis
(5)Detemination
of PBBS/ PBDES
contentby GC-MS.
Test ltem(s)
Cadmium(Cd)
Lead(Pb)
lllercury (Hg)
(Cr(Vl))
Hexavalent
Chromium
Sumof PBBS
Ivlonobromobiphenyl
Dibromobiphenyl
Tribromobiphenyl
Tetrabromobiphenyl
Pentabromobiphenyl
Hexabromobiphenyl
Heptabromobiphenyl
Oclabromobiphenyl
Nonabromobiphenyl
Decabromobiphenyl
Sumof PBDES
Monobromodiphenyl
ether
;trvdGhFo&de,sr,E^rh.;d.i@br.^
tr' bt6$n;tonl!N{h'i
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i'ci't6rr.nE
i DaDbh" -d d e
h,q!aoit"
tinit
Ud!
100
1000
1000
1000
1000
'
-
mg/kg
mS/kS
mS/KS
mS/kS
mdks
mg/Kg
mg/Kg
mg/Kg
mg-fts
mgKg
mgKS
ms/Ks
mg/kg
mgKg
m9x9
ms/ks
mg/Kg
1000
-
{1d".'db.
MDt
0p1
2
2
2
2
-
N
N
N
N
N
5
5
5
5
5
5
5
5
5
5
N
N
N
N
N
N
N
N
N
N
5
O
D
D
D
D
D
D
D
D
D
D
D
D
D
D
ND
N
D
t r rd r . 6i1rir h 6do.vnld d.d
rc'rdn dr s.iod.d'
f,nqc'i!9s@r
| 0G42529s29
2aBA80CC
sGs MadsioiNc.41.Tho slh AvenueTEoA,llanin,chiM 1l}a57 I 136
s sss.f'[email protected]
s F . *lriE*fitrtte8lit641Cscs*l
ffll: 300457I {3f2r66?8806l1e2?26&12
Membero,rbeSGSGroup(SGSSA)
TestReport
No.TSNEC1200272601
Tost ltem(s)
Dibromodiphenyl
elher
Tdbromodiphenyl
elher
Telrab.omodiphenylether
Pentabromodiphenyl
elh€r
Hexabromodiphenyl
ether
Heptabromodiphenyl
ether
Octabromodiphenyl
ether
Nonabromodiphenyl
ether
Decabromodiphenyl
elher
trd!
Date:09Apr2012
udt
MDt
@1
ms/Kg
mg/Kg
mS/kS
ms/Ks
mg/kg
mg/Kg
m9KS
mgKs
mgKs
5
5
5
5
5
5
5
5
5
ND
ND
ND
ND
ND
ND
ND
ND
ND
Page3 of 8
Notes:
(1)Themaximum
permissibte
limitis quotedfromdirective
2011/65/EU.
Annexlt.
Horebrpmocrrdododecane
THBCDD)
Testlvlethod
: Withreference
to IEC62321:2008,
anatysis
wasp€rfomedby GC-N4S.
T€stltem(s)
Hexabromocyclododecane
(HBCDD)
Ulit
MDI
pp1
mgKg
10
ND
Notes:
(1)Reference
Information:
Diredive2011/6S/EU
recasting
RoHSdirective
200?J9S/EC:
Hexabromocydododec€ne
(HBCDD)
is considered
as a priority
forriskevaluation
andsubstance
restriclion.
Phthalatss
Testl\Iethod: Withreference
to EN14372:2004,
anatysis
wasperformed
by co-tvts.
Test ltem(s)
DibutylPhthalate
(DBP)
B€nzylbutylPhthalate(BBP)
(DEHP)
Bis (2-elhylhexyD
Phthalale
Notes :
!d!
MDt
%(w4,,/) 0.003
%(ww) 0.003
%(Ww) 0.003
0p1
ND
ND
ND
(1)Reference
Infomation:
Directive
2011/65/EU
recasting
RoHSdirective
200295/EC:
phthaiate
Bis(2-ethylhexyl)
(DEHP),
Butylbenzytphthatate
(BBP)andoibutytphthatate
(DBp)are
considered
as a pdority
forriskevaluation
andsubslance
restiction.
l6yh.cofr'm'sb]kl]ot6.n'd
':Rcg*
scsMa^tion,No.4l.Tnb5lh Av€ns€',lEoa,Iaiti.chie 3&457 I i3t,21d5233,t0t
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TestReport
No.TSNEC1200272601
Date:09Apr2012
Page 4 of I
Resultshownis of the total weight of wet sample
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Menberolrh. SGSGrow ISGSSAl
SGSTest ReDort
No.TSNEC1200272601
Date:09 Apr 2012
Page 5 of 8
ATTACHMENTS
cd/Pb/Hg/Cf'lPBB5&PBOES Flow Chart
Aer0nWang/Jason
Li/AngellYao
1 )Nameoflhe personwho madetesling:
percon
in chargeoftesting:
CindyYin/RelZhu
2) Nameofthe
tolallyby pre-condilioning
melhodaccording
to
3) Thssesampleswsrs dissolved
belowllowchari.(C16*
andPBBS/PBDES
testmelhodexcluded)
Preparation
Sample
lVeasuremenl
Sample
PEB'PEDE5
Fb/Cd/Hg
Sample
solvent
Aciddigestion
wilh
micrcwave/holplale
reagent
Addingdigestion
Heatingio 9tF95'C for
extraction
Concentralion/
Dilution
ofextraction
s0iuIt0n
Solution
ResiduB
Filtralion
andpH
adjustmenl
I
1)AkaliFusion
DryAshing
2) Acid to
dissolve
ill;l,ffi;i;lii'#:;'
i i
i;
;ii;
Adding1,5'
fo!
diphenylcarbazide
coloidevelopment
i;;;;i'-,iiiliir
ii'iiii;'";l;;n
*aro 1t:.,.trere1"l:,11e191191':ll1"l:11*:::::L:11.,1:1:":i:YlTi
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rn!
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+F.*Ffislit$*x&8tEt!
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M e m b e r o , l nSeC SG r o u p( S G SS A )
TestReport
No.TSNEC1200272601
Date:09 Apr 2012
Page6 ofB
ATTACHMENTS
HECDD Tosting Flow Chaft
'l) Nameofthe perconwho made
testing:MarineSun
2) Namsoflhe personin chargeoftestingr
RexZhu
Sample
cutting/preparation
Sample
measurement
Solvenlexhaction
ConcBntraliodDilution
h'iii
d*,n'n.&ij'd
Liliiiiiidin'ii
b i.rrs
riirul6d t'.ry. tbi"6p.^,! -h..ts*,',
uf,.dr
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Mebberolrh6scs Grouo(SGSSAI
TestReport
No.TSNEC1200272601
Date:09Apr2012
Page7 of I
ATTACHMENTS
Phthalde Testng Floli, chaft
1) Namsoflhe pelsonwho madelestingiMaina Sun
2) Nameofthe personin chargeoftesling:RsxZhu
Solvenlexhaclion
ution
Concentralion/Dil
Fihralion
i,ffi{{ftf#,fii#jja!:i;'}'.f:rir""
lirid+
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tl:300457 lls6'4)652$ffi
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Mbfrberoilh6
SGs6roup{SGs5A)
TestReport
No.TSNEC1200272601
Date:09 Apr2012
Page 8 of 8
Samplephoto:
TSN12-002726.001
the photoon originalrepoionly
SGS authenticate
'*. End of Report'-
l#;tr$#,Ii.1i;;iffi
$:l:S,e*',#l+-*I*fiini,iil'*t";l*l'";*i#;fi
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Mehboror$€ scs GbuP (SGSSA)
TestReport
No.TSNEC1200272602
Date:09Apr2012
Page1 of 4
BEIJINGHYSTICNEWIVATERIALS
CO,,LTD,
ROAD,BADACHUHIGH.TECHZONE,BEIJING.
5 SHUANGYUAN
100041,
cHtNA
The followingsample(6)wasirere submittedand identifiedon behalfofthe clientsas : EPOXYADHESIVE
- TJ
TP12-004950
SGSJobNo.:
lvodelNo.:
Dateof SampleReceived
TestingPedod:
EP6O8
31 Mat2012
31 Mat 2012- 0g Apt2012
Test Requested:
Selecledtest(s)as requestedby client.
Testlvlethod:
Pleasereferto nextpage(s).
Pleasereferto nextpage(s).
TestResults:
Signedfor and on behalfof
scs-csTcLtd.
o*) N-(
AimyWang
ApprovedSignatory
fi:id;:ifillll'.i.i ;i;i;l
;:i ;;i;;:;;;;";;;;;
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M€mb€rol
TestRemrt
No.TSNEC1200272602
Date:09 Apr20'l2
Page2 of 4
TestResults:
TestPartDescdption:
Spodm€i No.
1
SGSSamplelD
D€6cription
TSN12-002726.002ivorv-whiteDaste
Remarks:
0 )1 m g / k g = 1 p p m = 0 . 0 0 0 1 %
(2)[,lDL = lllethod DetectionLimit
(3)ND = Not Detected( < IVIDL)
(4) '!" = Not Regulated
Halogen
(lC).
performed
by lonChromatograph
TestMethod: Withreferenceto EN 14582:2007,analysiswas
Testltem(s)
(F)
Fluorine
Chlorine(Cl)
(Br)
Bromine
(l)
lodine
u!j!
mg/(9
mgKs
mg/Kg
mg/kg
MDt
O@
50
50
50
50
57
7557
ND
NO
Result shown is of the total weight of wet sample
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TestReport
Dater09Apr2012
No.TSNEC1200272602
Page 3 of 4
ATTACHMENTS
HalogenTestingFlow Chad
Angell
Yao
whomadetesling:
1)Nameofthepercon
Rsx
Zhu
psrson
in
charge
oflesling:
ofthe
2) Name
Samplecutting/preparation
measuremsnl
Sample
in oxygenbomb
Combuslion
Dissolv€d
inan absorption
by ion
Analyzed
Do!ble
chromatography.
if
conlimby otherinslruments,
nacessaty
;L"iliiliiii'i]'i;;fi"
"r'irni"
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iictn ' ..*.u-.
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dha'o
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a
tb b cl sr sd s Bdo;'""d 6s Tl
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r {!fn|65?33001
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r€6'2a66a!0of
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e S O r o !l P
S G Ss A )
TestReport
Date:09 Apr 2012
No.TSNEC1200272602
Page4 of 4
Samplephoto:
TSNl2-002726.002
SGS authenticatethe photo on odginal report only
'*" End of Report""'
'";';;;;
:'l:i,:irul;r,ii*,:-';l',1^:r$:T:,'st'""i:;:TffH3,il,iw*';ilS[i::ilii--k*.li,Jji#l*in:
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Momb€rot
l\OV'BF.F.q,A
TESTREPORT
NO.:4002R121008024-2R02
Oate:Oct.1
0,2012
Cuslomer: SuzhouFuHongElectronicIndustriatCo.,
16.
Addr6s: NO.89 \/ElDU ROAD,WANGTINGTOVIN,XTANGCHENG
DISTR|CI SUZHOU.CHINA
Repod on the submltted samrl€ said to be
sample name: Leadwife coppershell
Modol:/
Itefi/Lot Io.: /
Matonal:/
Buyen/
Supplier:/,
lilanufacturE:/-f
.
_
- i
Samplerecelveddate:
Gq
2012 :
_08,
:
t*,tn o"n.o,t.. o".;;,,013
"."r.-,.,,613,
1
,]
i
&glirs-Bgsccsgq
As specifedby dienl,to determine
the L€ad,Cadrium,l,tercury
& tiexayabntChrcmium
conle in the6ubmitted
samptein
accodance
withDirective
2OO2I95/EC
{RoHS).
j
Testino method:
Testingltem
Lead(Pb)
IEC62321:2008.
sectionI
cadmium(Cd)
IEC62321:2008,
s€ction9
(Hg)
[,lercury
IEC62321r2008,
s€ction7
(CrM)
Chromium
IEC62321:2008,AnnexB
Measufing
instrument ,MQL
rcP-oEs
a!gag
tcP-oEs
rcP-oEs
2 mg/kg
2 mg/kg
0.02mg/kg*
lsq
j 0.02mg/tg rctursto the MQL olsampleexlractionliquid.
Conclu3ion:
-\ryhentested as specifiedlhe submiliedsamplecompriedwith th€ requircmentsof commissionD€cisionof 18 Aug 2005
amendingDircctive2002/95/ECnotiliedunderdocum€nt2005/618/EC.
."*FOR
FURTHERDETAILS,PLEASEREFERTOT
Sign€dior and on behallol
ShenzhenAOVTestingTechnology
Co., Ltd,Kunshan8ran6h
Walbn
A?1
ea"arc"a"r,
YuanQi, l,lickey
LiTingting,Maggie
Chemical Test Direclor
OrO."*0r44
Technical
Di€clor
LabManager
STIENZIIEN
AOVTE$Tl'{GI€CHI!OLOGYCO,.I.TD,KUNSHAN
BRANCI]
(,10",'ll,,u*
l\ov"BF,?sn
TESTREPORT
NO.:A0O2R12100802+2R02
D a t eO c i . 1 0 , 2 0 1 2
T63l Flow:
L
ToDetemine/lead,
CldmiumContent(Metalsubstrale)
lestedbY
L7.^otq,
Add the digestionsolulionjthe
vess€lis heateduntilthesample
Coolingthe vessel,fiitei washedand
fllledlo the mafKwith distilledwaler.
-*".irl,"*J
"r,to,"t|,
The sampleis digestedin the
Addlhe digestion
soluUon,
close
lhemicrowave
vessel.
micrcwaveoventollowinga specinc
progrcm.
deoomposilion
Coolingthe vessel,frller;washedand
filled to the maft wilh dislilled waler.
Remove
lhe sample,
andcool
thebeak€rlo roomtemperature,
anddo thecolorreaclion
-].f----
Testthe samplesolulionand ihe 0.02
mg/kgslandardsolutionby uv-vls.
(Plating)
nrte,.washedand
______-l
l_____*p;-r, f;;-1
"*rn
rilledlo$e markwithDlwaler
I
I
ON
EANCH
ShENZH€N
A O VI 6 S T I I { GT ' C N O I O G YC O . . I T D . X U N S H A
' Hotlrne
40a 7008600
/\OV"BF#,HN
TESTREPORT
NO.iA002R121008024-2R02
O a t e : O c l 1 02 0 1 2
coalingon metals:(Plating)
in colorless
andcolorcdchromate
Hexavalent
Chromium
Content
5. ToDeiermine
r e s t ebd'v : l )
^,
L/A^U,4.
(
5.1Spotlesl
lf thelestresultis posiiive,
lo
ihesampleis considered
chromium
havehexavalenl
Place
1-5
Boiling- water-
lf the testreslrlt
extracton
procedurcshall be us€d to
and the 0.02 mg/kg
lltherc is intederenceor it is had to decide
whetherlhesamplehavethe hexavalent
water-enractron
5.2Boilin9Removethe sample,and cool
Takethe (50i5)cm2
Heat50 ml ol Dl walerin the
samplein the beaker.
beak€rto boilinglof 10 min
the beakerto rcomtemperalu€,
and do the colorrcaolion
Sample Doscripilon:
Code
Sample Desc{iplion
Leadwire Plating
Unit
Code
coppershellsubslfate
CoppershellPlatng
24
Result
RoHSLimit
2-3
N.O
Lead{Pb)
(Cd)
Cadmium
mg/l(g
1000
N.D.
N.D.
N.D.
mg/k9
100
N.D.
N.D.
N.D,
N.D.
(Hg)
Meroury
mg/kg
1000
N.D.
N.D.
N.D,
ND.
Chromum(Crl'I)
mg/K9
1000
Negalive
Negalrve
Negaliv€
Negative
S N € $ Z H E NA O V I : S T I N G T € C N O I O G Y C O ' ' I T D . X U N S I l A NB B A N C I I
f l;"')l;**
TESTREPORT
oare:oct.10,2012
NO.:A0O2R12100802+2R02
-:fh€newRoHSdi€ctive2011/65/EU,
Direcliv€
on Jul.21,2011comeinloforce,on Jan.03,2013thsformalimplementation,
simultaneously200295/EC
ahallbe repeal€d
Sp€cimens,whichggqeted to d€temineLead,CadmiumandMercuryconient havebeendissolvedcompletelv.
-mg/Kg=ppm
ceofC_rl\,I)l
if"veiry/y6hetp ttef.li
v
meresr{.q!.be/rurTr
--The iest is bas€don the following
maybecannotstandfor the physicaltruth
-Photois included
ii'iffyiT-''
lhe spot test result is uncertainor
*'q:*
eachpadis unifom.Theteslrcsult
Leadwir€ coppershell
"'End of Repod""
SRANCIi
CO.,ITDKUNSHAN
AOVrlsrr'tc IECNl'lO!OeY
sHEI\tZH:ir
r.r i35.1J:55i0eo0o Fd.3F1t?55roEr$
hrr ,w.d{.di'
Fodrdo 1r.r00
/, Hotlrne
I , 400 7008600
NUMBER: SH
TEST REPORT
APPLICANT:
ATT
LITTELFUSE,INC.
800 E. NORTHWEST HWY
N:
A.DIVIETRO/D.UNTIEDT
DATE:
AH00346635
OCT 29, 2012
SAMPLE DESCRIPTION:
ONE (1) SUBMITTED SAMPLE SAID TO BE RED INK.
PART DESCRIPTION
: INK-RED.
PART NUMBER
: 425901.
DATE SAMPLE RECEIVED
: OCTOBER.19, 2012.
DATE TEST STARTED
: OCTOBER.19, 2012.
*****************************************************************************************************************************************************
TESTS CONDUCTED:
AS REQUESTED BY THE APPLICANT, FOR DETAILS REFER TO ATTACHED PAGE(S)
*****************************************************************************************************************************************************
TO BE CONTINUED
AUTHORIZED BY：
FOR INTERTEK TESTING SERVICES
LTD., SHANGHAI
JACOB LIN
GENERAL MANAGER
PAGE 1 OF 11
Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233
Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
NUMBER: SH
TEST REPORT
AH00346635
TESTS CONDUCTED
1(
Ⅰ) Test Result Summary :
Testing Item
Result (ppm)
Heavy Metal
Cadmium (Cd) content
Lead (Pb) content
Mercury (Hg) content
6+
Chromium VI (Cr ) content
Polybrominated Biphenyls (PBBs)
Monobrominated Biphenyls (MonoBB)
Dibrominated Biphenyls (DiBB)
Tribrominated Biphenyls (TriBB)
Tetrabrominated Biphenyls (TetraBB)
Pentabrominated Biphenyls (PentaBB)
Hexabrominated Biphenyls (HexaBB)
Heptabrominated Biphenyls (HeptaBB)
Octabrominated Biphenyls (OctaBB)
Nonabrominated Biphenyls (NonaBB)
Decabrominated Biphenyl (DecaBB)
Polybrominated Diphenyl Ethers (PBDEs)
Monobrominated Diphenyl Ethers (MonoBDE)
Dibrominated Diphenyl Ethers (DiBDE)
Tribrominated Diphenyl Ethers (TriBDE)
Tetrabrominated Diphenyl Ethers (TetraBDE)
Pentabrominated Diphenyl Ethers (PentaBDE)
Hexabrominated Diphenyl Ethers (HexaBDE)
Heptabrominated Diphenyl Ethers (HeptaBDE)
Octabrominated Diphenyl Ethers (OctaBDE)
Nonabrominated Diphenyl Ethers (NonaBDE)
Decabrominated Diphenyl Ether (DecaBDE)
(Ⅲ) Test Method:
Testing Item T
Cadmium (Cd) content
Lead (Pb) content
Mercury (Hg) content
6+
Chromium VI (Cr ) content
Polybrominated Biphenyls
(PBBs)
Polybrominated Diphenyl
Ethers (PBDEs)
esting Method R
With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10,
by microwave digestion until the tested samples are totally
dissolved and determined by ICP-OES.
With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10,
by microwave digestion until the tested samples are totally
dissolved and determined by ICP-OES.
With reference to IEC 62321 edition 1.0:2008 in clause 7, by
microwave digestion until the tested samples are totally
dissolved and determined by ICP-OES.
With reference to IEC 62321 edition 1.0:2008 in annex C, by
alkaline digestion and determined by UV-Vis spectrophotometer.
With reference to IEC 62321 edition 1.0:2008 in annex A, by
solvent extraction and determined by GC-MSD and further
HPLC confirmation when necessary.
With reference to IEC 62321 edition 1.0:2008 in annex A, by
solvent extraction and determined by GC-MSD and further
HPLC confirmation when necessary.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
eporting Limit
2 ppm
2 ppm
2 ppm
1 ppm
5 ppm
5 ppm
Remark:
Reporting limit = Quantitation limit of analyte in sample
**************************************************************************************************************************************************
TO BE CONTINUED
PAGE 2 OF 11
Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233
Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
NUMBER: SH
TEST REPORT
AH00346635
TESTS CONDUCTED
(Ⅳ) Measurement Flowchart:
Test For Cd/Pb/Hg/Chromium (VI)/PBBs/PBDEs Contents
Reference Standard: IEC 62321 edition 1.0:2008
sampling/grinding or cutting
Cr6+
Cd/Pb/Hg
metal
weigh sample and
for different
material, digest
the sample with
confirm the tested
samples are totally
dissolved
spot test
negative*2
No
PBBs/PBDEs
polymers /
electronics
weigh sample
and add
organic
weigh sample
and add
alkaline
solution
get 50cm2
samples
definite
temp.
boiling water
extraction
cool and
filter the
extract
soxhlet
extraction or
solvent
extraction
make up with
deionized water
concentrate
the extract
and make up
with organic
analyzed by ICP-OES
make up with deionized
water and add diphenylcarbazide solution
analyzed by GCMSD
analyzed by UV-VIS
REMARKS:
*1: List of appropriate acid：
Material
Polymers
Metals HNO
Electronics H
Acid added for digestion
HNO3,HCl,HF,H2O2,H3BO3
3,HCl,HF
NO3,HCl,H2O2,HBF4
*2: If the result of spot test is positive, Chromium VI would be determined as detected.
**************************************************************************************************************************************************
TO BE CONTINUED
PAGE 3 OF 11
Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233
Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
NUMBER: SH
TEST REPORT
AH00346635
TESTS CONDUCTED
2(
Ⅰ) Test Result Summary :
Testing Item
Halogen Content
Fluorine (F)
Chlorine (Cl)
Bromine (Br)
Iodine (I)
Remarks:
ND
ppm
ND
1000
ND
ND
= Parts per million = mg/kg
=
Not detected
Responsibility Of Chemist
(Ⅲ) Test Method:
Testing Item T
Halogen Content
Result (ppm)
: Leaf Liu
esting Method R
With reference to EN 14582:2007 by combustion flask with
oxygen and determined by ion chromatography
eporting Limit
50 ppm
Remark:
Reporting limit = Quantitation limit of analyte in sample
**************************************************************************************************************************************************
TO BE CONTINUED
PAGE 4 OF 11
Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233
Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
NUMBER: SH
TEST REPORT
AH00346635
TESTS CONDUCTED
(Ⅳ) Measurement Flowchart:
Test For Halogen Content
Reference Standard： EN 14582
sampling/grinding or
cutting
add absorbent in a
combustion flask &
place weighed sample in
equipment
fill the combustion
flask with oxygen
ignite then leave the
flask at room
temperature
transfer the absorbent
into a volumetric flask
make up with deionized
water
analyzed by ion
chromatography
**************************************************************************************************************************************************
TO BE CONTINUED
PAGE 5 OF 11
Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233
Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
NUMBER: SH
TEST REPORT
AH00346635
TESTS CONDUCTED
3
(A) TEST RESULT SUMMARY:
TESTING ITEM R
HBCD (HEXABROMOCYCLODODECANE)
ESULT(ppm)
ND
REMARKS:
ppm = PARTS PER MILLION = mg/kg
ND = NOT DETECTED
(B) TEST METHOD :
TESTING ITEM TE
STING METHOD
REPORTING
LIMIT
WITH REFERENCE TO USEPA 3540C, BY
SOLVENT EXTRACTION AND DETERMINED
10 ppm
BY GC/MS
**************************************************************************************************************************************************
TO BE CONTINUED
HBCD (HEXABROMOCYCLODODECANE)
PAGE 6 OF 11
Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233
Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
NUMBER: SH
TEST REPORT
AH00346635
TESTS CONDUCTED
MEASUREMENT FLOWCHART:
TEST FOR HBCD (HEXABROMOCYCLODODECANE) CONTENT
WEIGH SAMPLE AND PLACE
INTO A THIMBLE
SOXHLET EXTRACTION WITH
ORGANIC SOLVENT
CONCENTRATE THE EXTRACT
TRANSFER THE EXTRACT
INTO A VOLUMETRIC FLASK
MAKE UP WITH ORGANIC
SOLVENT
ANALYZE BY GC-MSD
**************************************************************************************************************************************************
TO BE CONTINUED
PAGE 7 OF 11
Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233
Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
NUMBER: SH
TEST REPORT
AH00346635
TESTS CONDUCTED
4 PHT
HALATE CONTENT TEST
WITH REFERENCE TO EN14372, BY GAS CHROMATOGRAPHY-MASS SPECTROMETRY (GC-MS) ANALYSIS.
TESTED COMPOUND R
ESULT (%,W/W)
DIBUTYL PHTHALATE (DBP)
DI(2-ETHYL HEXYL) PHTHALATE(DEHP)
BENZYL BUTYL PHTHALATE (BBP)
SUM OF THREE PHTHALATES
ND
ND
ND
ND
LIMIT(%,W/W)
(MAX.)
------0.1
REMARK：THE ABOVE LIMIT WAS QUOTED ACCORDING TO ANNEX XVII ITEMS 51 & 52 OF THE REACH
REGULATION (EC) NO. 1907/2006 & AMENDENT NO.552/2009 FOR PHTHALATE CONTENT IN TOYS
AND CHILDREN CARE ARTICLES.
DETECTION LIMIT = 0.01%(W/W)
ND = NOT DETECTED
5 PHT
HALATE CONTENT TEST
WITH REFERENCE TO CPSC-CH-C1001-09.3, BY GAS CHROMATOGRAPHY-MASS SPECTROMETRY (GC-MS)
ANALYSIS.
TESTED COMPOUND R
ESULT (%,W/W)
DI-BUTYL PHTHALATE (DBP)
DI(2-ETHYL HEXYL) PHTHALATE(DEHP)
BENZYL BUTYL PHTHALATE (BBP)
ND
ND
ND
LIMIT(%,W/W)
(MAX.)
0.1
0.1
0.1
REMARK：THE ABOVE LIMIT WAS QUOTED ACCORDING TO US CONSUMER PRODUCT SAFETY
IMPROVEMENT ACT 2008 & AMENDMENT H.R.2715 FOR PROHIBITION ON SALE OF CERTAIN
PRODUCTS CONTAINING SPECIFIED PHTHALATES.
DETECTION LIMIT = 0.01%(W/W)
ND = NOT DETECTED
DATE SAMPLE RECEIVED : OCT.19, 2012
TESTING PERIOD : OCT.19, 2012 TO OCT.23, 2012
**************************************************************************************************************************************************
TO BE CONTINUED
PAGE 8 OF 11
Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233
Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
NUMBER: SH
TEST REPORT
AH00346635
TESTS CONDUCTED
MEASUREMENT FLOWCHART:
TEST FOR PHTHALATES CONTENTS (EN14372)
WEIGH SAMPLE AND
PLACE IN A THIMBLE
EXTRACTED BY SOXHLET
EXTRACTION WITH
ORGANIC SOLVENT
CONCENTRATE THE
EXTRACT
Transfer the extract
into a volumetric
flask
MAKE UP WITH ORGANIC
SOLVENT
ANALYZE BY GC-MSD
**************************************************************************************************************************************************
TO BE CONTINUED
PAGE 9 OF 11
Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233
Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
NUMBER: SH
TEST REPORT
AH00346635
TESTS CONDUCTED
MEASUREMENT FLOWCHART:
TEST FOR PHTHALATES CONTENTS (CPSC-CH-C1001-09.3)
WEIGH SAMPLE AND
PLACE IN A THIMBLE
EXTRACTED WITH
ORGANIC SOLVENT BY
ULTRASONIC WATER
BATH
ANALYZE BY GC-MSD
**************************************************************************************************************************************************
TO BE CONTINUED
PAGE 10 OF 11
Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233
Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
TEST REPORT
NUMBER: SH
AH00346635
TESTS CONDUCTED
**************************************************************************************************************************************************
END OF REPORT
This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a recommendation for any particular
course of action. Intertek does not accept a duty of care or any other responsibility to any person other than the Client in respect of this report and only accepts liability
to the Client insofar as is expressly contained in the terms and conditions governing Intertek's provision of services to you. Intertek makes no warranties or
representations either express or implied with respect to this report save as provided for in those terms and conditions. We have aimed to conduct the Review on a
diligent and careful basis and we do not accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by statute or otherwise,
except in the event of our gross negligence or wilful misconduct.
PAGE 11 OF 11
Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233
Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
NUMBER: SH
TEST REPORT
APPLICANT:
ATT
LITTELFUSE,INC.
800 E. NORTHWEST HWY
N:
A.DIVIETRO/D.UNTIEDT
DATE:
AH00345635
OCT 29, 2012
SAMPLE DESCRIPTION:
ONE (1) SUBMITTED SAMPLE SAID TO BE BLACK INK.
PART DESCRIPTION
: INK-BLACK.
PART NUMBER
: 425902.
DATE SAMPLE RECEIVED
: OCTOBER.15, 2012.
DATE TEST STARTED
: OCTOBER.15, 2012.
**************************************************************************************************************************************************
TESTS CONDUCTED:
AS REQUESTED BY THE APPLICANT, FOR DETAILS REFER TO ATTACHED PAGE(S)
**************************************************************************************************************************************************
TO BE CONTINUED
AUTHORIZED BY：
FOR INTERTEK TESTING SERVICES
LTD., SHANGHAI
JACOB LIN
GENERAL MANAGER
PAGE 1 OF 11
Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233
Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
NUMBER: SH
TEST REPORT
AH00345635
TESTS CONDUCTED
1(
Ⅰ) Test Result Summary :
Testing Item
Result (ppm)
Heavy Metal
Cadmium (Cd) content
Lead (Pb) content
Mercury (Hg) content
6+
Chromium VI (Cr ) content
Polybrominated Biphenyls (PBBs)
Monobrominated Biphenyls (MonoBB)
Dibrominated Biphenyls (DiBB)
Tribrominated Biphenyls (TriBB)
Tetrabrominated Biphenyls (TetraBB)
Pentabrominated Biphenyls (PentaBB)
Hexabrominated Biphenyls (HexaBB)
Heptabrominated Biphenyls (HeptaBB)
Octabrominated Biphenyls (OctaBB)
Nonabrominated Biphenyls (NonaBB)
Decabrominated Biphenyl (DecaBB)
Polybrominated Diphenyl Ethers (PBDEs)
Monobrominated Diphenyl Ethers (MonoBDE)
Dibrominated Diphenyl Ethers (DiBDE)
Tribrominated Diphenyl Ethers (TriBDE)
Tetrabrominated Diphenyl Ethers (TetraBDE)
Pentabrominated Diphenyl Ethers (PentaBDE)
Hexabrominated Diphenyl Ethers (HexaBDE)
Heptabrominated Diphenyl Ethers (HeptaBDE)
Octabrominated Diphenyl Ethers (OctaBDE)
Nonabrominated Diphenyl Ethers (NonaBDE)
Decabrominated Diphenyl Ether (DecaBDE)
(Ⅲ) Test Method:
Testing Item T
Cadmium (Cd) content
Lead (Pb) content
Mercury (Hg) content
6+
Chromium VI (Cr ) content
Polybrominated Biphenyls
(PBBs)
Polybrominated Diphenyl
Ethers (PBDEs)
esting Method R
With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10,
by microwave digestion until the tested samples are totally
dissolved and determined by ICP-OES.
With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10,
by microwave digestion until the tested samples are totally
dissolved and determined by ICP-OES.
With reference to IEC 62321 edition 1.0:2008 in clause 7, by
microwave digestion until the tested samples are totally
dissolved and determined by ICP-OES.
With reference to IEC 62321 edition 1.0:2008 in annex C, by
alkaline digestion and determined by UV-Vis spectrophotometer.
With reference to IEC 62321 edition 1.0:2008 in annex A, by
solvent extraction and determined by GC-MSD and further
HPLC confirmation when necessary.
With reference to IEC 62321 edition 1.0:2008 in annex A, by
solvent extraction and determined by GC-MSD and further
HPLC confirmation when necessary.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
eporting Limit
2 ppm
2 ppm
2 ppm
1 ppm
5 ppm
5 ppm
Remark:
Reporting limit = Quantitation limit of analyte in sample
**************************************************************************************************************************************************
TO BE CONTINUED
PAGE 2 OF 11
Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233
Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
NUMBER: SH
TEST REPORT
AH00345635
TESTS CONDUCTED
(Ⅳ) Measurement Flowchart:
Test For Cd/Pb/Hg/Chromium (VI)/PBBs/PBDEs Contents
Reference Standard: IEC 62321 edition 1.0:2008
sampling/grinding or cutting
Cr6+
Cd/Pb/Hg
metal
weigh sample and
for different
material, digest
the sample with
confirm the tested
samples are totally
dissolved
spot test
negative*2
No
PBBs/PBDEs
polymers /
electronics
weigh sample
and add
organic
weigh sample
and add
alkaline
solution
get 50cm2
samples
definite
temp.
boiling water
extraction
cool and
filter the
extract
soxhlet
extraction or
solvent
extraction
make up with
deionized water
concentrate
the extract
and make up
with organic
analyzed by ICP-OES
make up with deionized
water and add diphenylcarbazide solution
analyzed by GCMSD
analyzed by UV-VIS
REMARKS:
*1: List of appropriate acid：
Material
Polymers
Metals HNO
Electronics H
Acid added for digestion
HNO3,HCl,HF,H2O2,H3BO3
3,HCl,HF
NO3,HCl,H2O2,HBF4
*2: If the result of spot test is positive, Chromium VI would be determined as detected.
**************************************************************************************************************************************************
TO BE CONTINUED
PAGE 3 OF 11
Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233
Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
NUMBER: SH
TEST REPORT
AH00345635
TESTS CONDUCTED
2(
Ⅰ) Test Result Summary :
Testing Item
Halogen Content
Fluorine (F)
Chlorine (Cl)
Bromine (Br)
Iodine (I)
Result (ppm)
ND
150
ND
ND
Remarks:
ppm = Parts per million = mg/kg
ND
=
Not detected
Responsibility Of Chemist :
(Ⅲ) Test Method:
Testing Item T
Halogen Content
Leaf Liu
esting Method R
With reference to EN 14582:2007 by combustion flask with
oxygen and determined by ion chromatography
eporting Limit
50 ppm
Remark:
Reporting limit = Quantitation limit of analyte in sample
**************************************************************************************************************************************************
TO BE CONTINUED
PAGE 4 OF 11
Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233
Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
NUMBER: SH
TEST REPORT
AH00345635
TESTS CONDUCTED
(Ⅳ) Measurement Flowchart:
Test For Halogen Content
Reference Standard： EN 14582
sampling/grinding or
cutting
add absorbent in a
combustion flask &
place weighed sample in
equipment
fill the combustion
flask with oxygen
ignite then leave the
flask at room
temperature
transfer the absorbent
into a volumetric flask
make up with deionized
water
analyzed by ion
chromatography
**************************************************************************************************************************************************
TO BE CONTINUED
PAGE 5 OF 11
Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233
Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
NUMBER: SH
TEST REPORT
AH00345635
TESTS CONDUCTED
3
(A) TEST RESULT SUMMARY:
TESTING ITEM R
HBCD (HEXABROMOCYCLODODECANE)
ESULT(ppm)
ND
REMARKS:
ppm = PARTS PER MILLION = mg/kg
ND = NOT DETECTED
(B) TEST METHOD :
TESTING ITEM TE
STING METHOD
REPORTING
LIMIT
WITH REFERENCE TO USEPA 3540C, BY
SOLVENT EXTRACTION AND DETERMINED
10 ppm
BY GC/MS
**************************************************************************************************************************************************
TO BE CONTINUED
HBCD (HEXABROMOCYCLODODECANE)
PAGE 6 OF 11
Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233
Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
NUMBER: SH
TEST REPORT
AH00345635
TESTS CONDUCTED
MEASUREMENT FLOWCHART:
TEST FOR HBCD (HEXABROMOCYCLODODECANE) CONTENT
WEIGH SAMPLE AND PLACE
INTO A THIMBLE
SOXHLET EXTRACTION WITH
ORGANIC SOLVENT
CONCENTRATE THE EXTRACT
TRANSFER THE EXTRACT
INTO A VOLUMETRIC FLASK
MAKE UP WITH ORGANIC
SOLVENT
ANALYZE BY GC-MSD
**************************************************************************************************************************************************
TO BE CONTINUED
PAGE 7 OF 11
Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233
Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
NUMBER: SH
TEST REPORT
AH00345635
TESTS CONDUCTED
4 PHT
HALATE CONTENT TEST
WITH REFERENCE TO EN14372, BY GAS CHROMATOGRAPHY-MASS SPECTROMETRY (GC-MS) ANALYSIS.
TESTED COMPOUND R
ESULT (%,W/W)
DIBUTYL PHTHALATE (DBP)
DI(2-ETHYL HEXYL) PHTHALATE(DEHP)
BENZYL BUTYL PHTHALATE (BBP)
SUM OF THREE PHTHALATES
ND
ND
ND
ND
LIMIT(%,W/W)
(MAX.)
------0.1
REMARK：THE ABOVE LIMIT WAS QUOTED ACCORDING TO ANNEX XVII ITEMS 51 & 52 OF THE REACH
REGULATION (EC) NO. 1907/2006 & AMENDENT NO.552/2009 FOR PHTHALATE CONTENT IN TOYS
AND CHILDREN CARE ARTICLES.
DETECTION LIMIT = 0.01%(W/W)
ND = NOT DETECTED
5 PHT
HALATE CONTENT TEST
WITH REFERENCE TO CPSC-CH-C1001-09.3, BY GAS CHROMATOGRAPHY-MASS SPECTROMETRY (GC-MS)
ANALYSIS.
TESTED COMPOUND R
ESULT (%,W/W)
DI-BUTYL PHTHALATE (DBP)
DI(2-ETHYL HEXYL) PHTHALATE(DEHP)
BENZYL BUTYL PHTHALATE (BBP)
ND
ND
ND
LIMIT(%,W/W)
(MAX.)
0.1
0.1
0.1
REMARK：THE ABOVE LIMIT WAS QUOTED ACCORDING TO US CONSUMER PRODUCT SAFETY
IMPROVEMENT ACT 2008 & AMENDMENT H.R.2715 FOR PROHIBITION ON SALE OF CERTAIN
PRODUCTS CONTAINING SPECIFIED PHTHALATES.
DETECTION LIMIT = 0.01%(W/W)
ND = NOT DETECTED
DATE SAMPLE RECEIVED: OCT.15, 2012
TESTING PERIOD : OCT.15, 2012 TO OCT.18, 2012
**************************************************************************************************************************************************
TO BE CONTINUED
PAGE 8 OF 11
Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233
Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
NUMBER: SH
TEST REPORT
AH00345635
TESTS CONDUCTED
MEASUREMENT FLOWCHART:
TEST FOR PHTHALATES CONTENTS (EN14372)
WEIGH SAMPLE AND
PLACE IN A THIMBLE
EXTRACTED BY SOXHLET
EXTRACTION WITH
ORGANIC SOLVENT
CONCENTRATE THE
EXTRACT
Transfer the extract
into a volumetric
flask
MAKE UP WITH ORGANIC
SOLVENT
ANALYZE BY GC-MSD
**************************************************************************************************************************************************
TO BE CONTINUED
PAGE 9 OF 11
Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233
Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
NUMBER: SH
TEST REPORT
AH00345635
TESTS CONDUCTED
MEASUREMENT FLOWCHART:
TEST FOR PHTHALATES CONTENTS (CPSC-CH-C1001-09.3)
Weigh sample and
place in a tube
Extracted with
organic solvent by
ultrasonic water
bath
Analyze by GC-MSD
**************************************************************************************************************************************************
TO BE CONTINUED
PAGE 10 OF 11
Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233
Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
TEST REPORT
NUMBER: SH
AH00345635
TESTS CONDUCTED
**************************************************************************************************************************************************
END OF REPORT
This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to
be a recommendation for any particular course of action. Intertek does not accept a duty of care or any other responsibility to any
person other than the Client in respect of this report and only accepts liability to the Client insofar as is expressly contained in the
terms and conditions governing Intertek's provision of services to you. Intertek makes no warranties or representations either
express or implied with respect to this report save as provided for in those terms and conditions. We have aimed to conduct the
Review on a diligent and careful basis and we do not accept any liability to you for any loss arising out of or in connection with this
report, in contract, tort, by statute or otherwise, except in the event of our gross negligence or wilful misconduct.
PAGE 11 OF 11
Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233
Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
NUMBER: SH
TEST REPORT
APPLICANT:
AT
LITTELFUSE,INC.
800 E. NORTHWEST HWY
TN:
A.DIVIETRO/D.UNTIEDT
DATE:
AH00345662
OCT 26, 2012
SAMPLE DESCRIPTION:
ONE (1) SUBMITTED SAMPLE SAID TO BE YELLOW INK.
PART DESCRIPTION
: INK-YELLOW.
PART NUMBER
: 425903.
DATE SAMPLE RECEIVED
: OCTOBER.15, 2012.
DATE TEST STARTED
: OCTOBER.15, 2012.
**************************************************************************************************************************************************
TESTS CONDUCTED:
AS REQUESTED BY THE APPLICANT, FOR DETAILS REFER TO ATTACHED PAGE(S)
**************************************************************************************************************************************************
TO BE CONTINUED
AUTHORIZED BY：
FOR INTERTEK TESTING SERVICES
LTD., SHANGHAI
JACOB LIN
GENERAL MANAGER
PAGE 1 OF 11
Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233
Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
NUMBER: SH
TEST REPORT
AH00345662
TESTS CONDUCTED
1(
Ⅰ) Test Result Summary :
Testing Item
Result (ppm)
Heavy Metal
Cadmium (Cd) content
Lead (Pb) content
Mercury (Hg) content
6+
Chromium VI (Cr ) content
Polybrominated Biphenyls (PBBs)
Monobrominated Biphenyls (MonoBB)
Dibrominated Biphenyls (DiBB)
Tribrominated Biphenyls (TriBB)
Tetrabrominated Biphenyls (TetraBB)
Pentabrominated Biphenyls (PentaBB)
Hexabrominated Biphenyls (HexaBB)
Heptabrominated Biphenyls (HeptaBB)
Octabrominated Biphenyls (OctaBB)
Nonabrominated Biphenyls (NonaBB)
Decabrominated Biphenyl (DecaBB)
Polybrominated Diphenyl Ethers (PBDEs)
Monobrominated Diphenyl Ethers (MonoBDE)
Dibrominated Diphenyl Ethers (DiBDE)
Tribrominated Diphenyl Ethers (TriBDE)
Tetrabrominated Diphenyl Ethers (TetraBDE)
Pentabrominated Diphenyl Ethers (PentaBDE)
Hexabrominated Diphenyl Ethers (HexaBDE)
Heptabrominated Diphenyl Ethers (HeptaBDE)
Octabrominated Diphenyl Ethers (OctaBDE)
Nonabrominated Diphenyl Ethers (NonaBDE)
Decabrominated Diphenyl Ether (DecaBDE)
(Ⅲ) Test Method:
Testing Item T
Cadmium (Cd) content
Lead (Pb) content
Mercury (Hg) content
6+
Chromium VI (Cr ) content
Polybrominated Biphenyls
(PBBs)
Polybrominated Diphenyl
Ethers (PBDEs)
esting Method R
With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10,
by microwave digestion until the tested samples are totally
dissolved and determined by ICP-OES.
With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10,
by microwave digestion until the tested samples are totally
dissolved and determined by ICP-OES.
With reference to IEC 62321 edition 1.0:2008 in clause 7, by
microwave digestion until the tested samples are totally
dissolved and determined by ICP-OES.
With reference to IEC 62321 edition 1.0:2008 in annex C, by
alkaline digestion and determined by UV-Vis spectrophotometer.
With reference to IEC 62321 edition 1.0:2008 in annex A, by
solvent extraction and determined by GC-MSD and further
HPLC confirmation when necessary.
With reference to IEC 62321 edition 1.0:2008 in annex A, by
solvent extraction and determined by GC-MSD and further
HPLC confirmation when necessary.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
eporting Limit
2 ppm
2 ppm
2 ppm
1 ppm
5 ppm
5 ppm
Remark:
Reporting limit = Quantitation limit of analyte in sample
**************************************************************************************************************************************************
TO BE CONTINUED
PAGE 2 OF 11
Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233
Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
NUMBER: SH
TEST REPORT
AH00345662
TESTS CONDUCTED
(Ⅳ) Measurement Flowchart:
Test For Cd/Pb/Hg/Chromium (VI)/PBBs/PBDEs Contents
Reference Standard: IEC 62321 edition 1.0:2008
sampling/grinding or cutting
Cr6+
Cd/Pb/Hg
metal
weigh sample and
for different
material, digest
the sample with
confirm the tested
samples are totally
dissolved
spot test
negative*2
No
PBBs/PBDEs
polymers /
electronics
weigh sample
and add
organic
weigh sample
and add
alkaline
solution
get 50cm2
samples
definite
temp.
boiling water
extraction
cool and
filter the
extract
soxhlet
extraction or
solvent
extraction
make up with
deionized water
concentrate
the extract
and make up
with organic
analyzed by ICP-OES
make up with deionized
water and add diphenylcarbazide solution
analyzed by GCMSD
analyzed by UV-VIS
REMARKS:
*1: List of appropriate acid：
Material
Polymers
Metals HNO
Electronics H
Acid added for digestion
HNO3,HCl,HF,H2O2,H3BO3
3,HCl,HF
NO3,HCl,H2O2,HBF4
*2: If the result of spot test is positive, Chromium VI would be determined as detected.
**************************************************************************************************************************************************
TO BE CONTINUED
PAGE 3 OF 11
Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233
Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
NUMBER: SH
TEST REPORT
AH00345662
TESTS CONDUCTED
2(
Ⅰ) Test Result Summary :
Testing Item
Halogen Content
Fluorine (F)
Chlorine (Cl)
Bromine (Br)
Iodine (I)
Remarks:
N
ppm
ND
7400
ND
ND
= Parts per million = mg/kg
=
D
Not detected
Responsibility Of Chemist :
(Ⅲ) Test Method:
Testing Item T
Halogen Content
Result (ppm)
Leaf Liu
esting Method R
With reference to EN 14582:2007 by combustion flask with
oxygen and determined by ion chromatography
eporting Limit
50 ppm
Remark:
Reporting limit = Quantitation limit of analyte in sample
**************************************************************************************************************************************************
TO BE CONTINUED
PAGE 4 OF 11
Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233
Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
NUMBER: SH
TEST REPORT
AH00345662
TESTS CONDUCTED
(Ⅳ) Measurement Flowchart:
Test For Halogen Content
Reference Standard： EN 14582
sampling/grinding or
cutting
add absorbent in a
combustion flask &
place weighed sample in
equipment
fill the combustion
flask with oxygen
ignite then leave the
flask at room
temperature
transfer the absorbent
into a volumetric flask
make up with deionized
water
analyzed by ion
chromatography
**************************************************************************************************************************************************
TO BE CONTINUED
PAGE 5 OF 11
Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233
Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
NUMBER: SH
TEST REPORT
AH00345662
TESTS CONDUCTED
3
(A) TEST RESULT SUMMARY:
TESTING ITEM R
HBCD (HEXABROMOCYCLODODECANE)
ESULT(ppm)
ND
REMARKS:
ppm = PARTS PER MILLION = mg/kg
ND = NOT DETECTED
(B) TEST METHOD :
TESTING ITEM T
ESTING METHOD
REPORTING
LIMIT
WITH REFERENCE TO USEPA 3540C, BY
SOLVENT EXTRACTION AND DETERMINED
10 ppm
BY GC/MS
**************************************************************************************************************************************************
TO BE CONTINUED
HBCD (HEXABROMOCYCLODODECANE)
PAGE 6 OF 11
Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233
Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
NUMBER: SH
TEST REPORT
AH00345662
TESTS CONDUCTED
MEASUREMENT FLOWCHART:
TEST FOR HBCD (HEXABROMOCYCLODODECANE) CONTENT
WEIGH SAMPLE AND PLACE
INTO A THIMBLE
SOXHLET EXTRACTION WITH
ORGANIC SOLVENT
CONCENTRATE THE EXTRACT
TRANSFER THE EXTRACT
INTO A VOLUMETRIC FLASK
MAKE UP WITH ORGANIC
SOLVENT
ANALYZE BY GC-MSD
**************************************************************************************************************************************************
TO BE CONTINUED
PAGE 7 OF 11
Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233
Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
NUMBER: SH
TEST REPORT
AH00345662
TESTS CONDUCTED
4
PHTHALATE CONTENT TEST
WITH REFERENCE TO EN14372, BY GAS CHROMATOGRAPHY-MASS SPECTROMETRY (GC-MS) ANALYSIS.
TESTED COMPOUND RESULT
(%,W/W)
DIBUTYL PHTHALATE (DBP)
DI(2-ETHYL HEXYL) PHTHALATE(DEHP)
BENZYL BUTYL PHTHALATE (BBP)
SUM OF THREE PHTHALATES
ND
ND
ND
ND
LIMIT(%,W/W)
(MAX.)
------0.1
REMARK：THE ABOVE LIMIT WAS QUOTED ACCORDING TO ANNEX XVII ITEMS 51 & 52 OF THE REACH
REGULATION (EC) NO. 1907/2006 & AMENDENT NO.552/2009 FOR PHTHALATE CONTENT IN TOYS
AND CHILDREN CARE ARTICLES.
DETECTION LIMIT = 0.01%(W/W)
ND = NOT DETECTED
5
PHTHALATE CONTENT TEST
WITH REFERENCE TO CPSC-CH-C1001-09.3, BY GAS CHROMATOGRAPHY-MASS SPECTROMETRY (GC-MS)
ANALYSIS.
TESTED COMPOUND RESULT
DI-BUTYL PHTHALATE (DBP)
DI(2-ETHYL HEXYL) PHTHALATE(DEHP)
BENZYL BUTYL PHTHALATE (BBP)
(%,W/W)
ND
ND
ND
LIMIT(%,W/W)
(MAX.)
0.1
0.1
0.1
REMARK：THE ABOVE LIMIT WAS QUOTED ACCORDING TO US CONSUMER PRODUCT SAFETY
IMPROVEMENT ACT 2008 & AMENDMENT H.R.2715 FOR PROHIBITION ON SALE OF CERTAIN
PRODUCTS CONTAINING SPECIFIED PHTHALATES.
DETECTION LIMIT = 0.01%(W/W)
ND = NOT DETECTED
DATE SAMPLE RECEIVED: OCT.15, 2012
TESTING PERIOD : OCT.15, 2012 TO OCT.19, 2012
**************************************************************************************************************************************************
TO BE CONTINUED
PAGE 8 OF 11
Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233
Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
NUMBER: SH
TEST REPORT
AH00345662
TESTS CONDUCTED
MEASUREMENT FLOWCHART:
TEST FOR PHTHALATES CONTENTS (EN14372)
WEIGH SAMPLE AND
PLACE IN A THIMBLE
EXTRACTED BY SOXHLET
EXTRACTION WITH
ORGANIC SOLVENT
CONCENTRATE THE
EXTRACT
Transfer the extract
into a volumetric
flask
MAKE UP WITH ORGANIC
SOLVENT
ANALYZE BY GC-MSD
**************************************************************************************************************************************************
TO BE CONTINUED
PAGE 9 OF 11
Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233
Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
NUMBER: SH
TEST REPORT
AH00345662
TESTS CONDUCTED
MEASUREMENT FLOWCHART:
TEST FOR PHTHALATES CONTENTS (CPSC-CH-C1001-09.3)
Weigh sample and
place in a tube
Extracted with bath
organic solvent by
w\trasonic water
Analyze by GC-MSD
**************************************************************************************************************************************************
TO BE CONTINUED
PAGE 10 OF 11
Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233
Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
TEST REPORT
NUMBER: SH
AH00345662
TESTS CONDUCTED
**************************************************************************************************************************************************
END OF REPORT
This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a recommendation for any particular
course of action. Intertek does not accept a duty of care or any other responsibility to any person other than the Client in respect of this report and only accepts liability
to the Client insofar as is expressly contained in the terms and conditions governing Intertek's provision of services to you. Intertek makes no warranties or
representations either express or implied with respect to this report save as provided for in those terms and conditions. We have aimed to conduct the Review on a
diligent and careful basis and we do not accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by statute or otherwise,
except in the event of our gross negligence or wilful misconduct.
PAGE 11 OF 11
Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233
Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
NUMBER: SH
TEST REPORT
APPLICANT:
AT
LITTELFUSE,INC.
800 E. NORTHWEST HWY
TN:
A.DIVIETRO/D.UNTIEDT
DATE:
AH00345415
OCT 26, 2012
SAMPLE DESCRIPTION:
ONE (1) SUBMITTED SAMPLE SAID TO BE BLUE INK.
PART DESCRIPTION
: INK-BLUE.
PART NUMBER
: 425904.
DATE SAMPLE RECEIVED
: OCTOBER.15, 2012.
DATE TEST STARTED
: OCTOBER.15, 2012.
******************************************************************************************************************************************************
TESTS CONDUCTED:
AS REQUESTED BY THE APPLICANT, FOR DETAILS REFER TO ATTACHED PAGE(S)
******************************************************************************************************************************************************
TO BE CONTINUED
AUTHORIZED BY：
FOR INTERTEK TESTING SERVICES
LTD., SHANGHAI
JACOB LIN
GENERAL MANAGER
PAGE 1 OF 11
Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233
Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
NUMBER: SH
TEST REPORT
AH00345415
TESTS CONDUCTED
1(
Ⅰ) Test Result Summary :
Testing Item
Result (ppm)
Heavy Metal
Cadmium (Cd) content
Lead (Pb) content
Mercury (Hg) content
6+
Chromium VI (Cr ) content
Polybrominated Biphenyls (PBBs)
Monobrominated Biphenyls (MonoBB)
Dibrominated Biphenyls (DiBB)
Tribrominated Biphenyls (TriBB)
Tetrabrominated Biphenyls (TetraBB)
Pentabrominated Biphenyls (PentaBB)
Hexabrominated Biphenyls (HexaBB)
Heptabrominated Biphenyls (HeptaBB)
Octabrominated Biphenyls (OctaBB)
Nonabrominated Biphenyls (NonaBB)
Decabrominated Biphenyl (DecaBB)
Polybrominated Diphenyl Ethers (PBDEs)
Monobrominated Diphenyl Ethers (MonoBDE)
Dibrominated Diphenyl Ethers (DiBDE)
Tribrominated Diphenyl Ethers (TriBDE)
Tetrabrominated Diphenyl Ethers (TetraBDE)
Pentabrominated Diphenyl Ethers (PentaBDE)
Hexabrominated Diphenyl Ethers (HexaBDE)
Heptabrominated Diphenyl Ethers (HeptaBDE)
Octabrominated Diphenyl Ethers (OctaBDE)
Nonabrominated Diphenyl Ethers (NonaBDE)
Decabrominated Diphenyl Ether (DecaBDE)
(Ⅲ) Test Method:
Testing Item T
Cadmium (Cd) content
Lead (Pb) content
Mercury (Hg) content
6+
Chromium VI (Cr ) content
Polybrominated Biphenyls
(PBBs)
Polybrominated Diphenyl
Ethers (PBDEs)
esting Method R
With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10,
by microwave digestion until the tested samples are totally
dissolved and determined by ICP-OES.
With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10,
by microwave digestion until the tested samples are totally
dissolved and determined by ICP-OES.
With reference to IEC 62321 edition 1.0:2008 in clause 7, by
microwave digestion until the tested samples are totally
dissolved and determined by ICP-OES.
With reference to IEC 62321 edition 1.0:2008 in annex C, by
alkaline digestion and determined by UV-Vis spectrophotometer.
With reference to IEC 62321 edition 1.0:2008 in annex A, by
solvent extraction and determined by GC-MSD and further
HPLC confirmation when necessary.
With reference to IEC 62321 edition 1.0:2008 in annex A, by
solvent extraction and determined by GC-MSD and further
HPLC confirmation when necessary.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
eporting Limit
2 ppm
2 ppm
2 ppm
1 ppm
5 ppm
5 ppm
Remark:
Reporting limit = Quantitation limit of analyte in sample
******************************************************************************************************************************************************
TO BE CONTINUED
PAGE 2 OF 11
Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233
Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
NUMBER: SH
TEST REPORT
AH00345415
TESTS CONDUCTED
(Ⅳ) Measurement Flowchart:
Test For Cd/Pb/Hg/Chromium (VI)/PBBs/PBDEs Contents
Reference Standard: IEC 62321 edition 1.0:2008
sampling/grinding or cutting
Cr6+
Cd/Pb/Hg
metal
weigh sample and
for different
material, digest
the sample with
confirm the tested
samples are totally
dissolved
spot test
negative*2
No
PBBs/PBDEs
polymers /
electronics
weigh sample
and add
organic
weigh sample
and add
alkaline
solution
get 50cm2
samples
definite
temp.
boiling water
extraction
cool and
filter the
extract
soxhlet
extraction or
solvent
extraction
make up with
deionized water
concentrate
the extract
and make up
with organic
analyzed by ICP-OES
make up with deionized
water and add diphenylcarbazide solution
analyzed by GCMSD
analyzed by UV-VIS
REMARKS:
*1: List of appropriate acid：
Material
Polymers
Metals HNO
Electronics H
Acid added for digestion
HNO3,HCl,HF,H2O2,H3BO3
3,HCl,HF
NO3,HCl,H2O2,HBF4
*2: If the result of spot test is positive, Chromium VI would be determined as detected.
************************************************************************************************************************************************************
TO BE CONTINUED
PAGE 3 OF 11
Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233
Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
NUMBER: SH
TEST REPORT
AH00345415
TESTS CONDUCTED
2(
Ⅰ) Test Result Summary :
Testing Item
Halogen Content
Fluorine (F)
Chlorine (Cl)
Bromine (Br)
Iodine (I)
Remarks:
N
ppm
ND
600
ND
ND
= Parts per million = mg/kg
=
D
Not detected
Responsibility Of Chemist
(Ⅲ) Test Method:
Testing Item T
Halogen Content
Result (ppm)
: Leaf Liu
esting Method R
With reference to EN 14582:2007 by combustion flask with
oxygen and determined by ion chromatography
eporting Limit
50 ppm
Remark:
Reporting limit = Quantitation limit of analyte in sample
************************************************************************************************************************************************************
TO BE CONTINUED
PAGE 4 OF 11
Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233
Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
NUMBER: SH
TEST REPORT
AH00345415
TESTS CONDUCTED
(Ⅳ) Measurement Flowchart:
Test For Halogen Content
Reference Standard： EN 14582
sampling/grinding or
cutting
add absorbent in a
combustion flask &
place weighed sample in
equipment
fill the combustion
flask with oxygen
ignite then leave the
flask at room
temperature
transfer the absorbent
into a volumetric flask
make up with deionized
water
analyzed by ion
chromatography
************************************************************************************************************************************************************
TO BE CONTINUED
PAGE 5 OF 11
Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233
Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
NUMBER: SH
TEST REPORT
AH00345415
TESTS CONDUCTED
3
(A) TEST RESULT SUMMARY:
TESTING ITEM R
HBCD (HEXABROMOCYCLODODECANE)
ESULT(ppm)
ND
REMARKS:
ppm = PARTS PER MILLION = mg/kg
ND = NOT DETECTED
(B) TEST METHOD :
TESTING ITEM T
ESTING METHOD
REPORTING
LIMIT
WITH REFERENCE TO USEPA 3540C, BY SOLVENT
10 ppm
EXTRACTION AND DETERMINED BY GC/MS
************************************************************************************************************************************************************
TO BE CONTINUED
HBCD (HEXABROMOCYCLODODECANE)
PAGE 6 OF 11
Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233
Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
NUMBER: SH
TEST REPORT
AH00345415
TESTS CONDUCTED
MEASUREMENT FLOWCHART:
TEST FOR HBCD (HEXABROMOCYCLODODECANE) CONTENT
WEIGH SAMPLE AND PLACE
INTO A THIMBLE
SOXHLET EXTRACTION WITH
ORGANIC SOLVENT
CONCENTRATE THE EXTRACT
TRANSFER THE EXTRACT
INTO A VOLUMETRIC FLASK
MAKE UP WITH ORGANIC
SOLVENT
ANALYZE BY GC-MSD
************************************************************************************************************************************************************
TO BE CONTINUED
PAGE 7 OF 11
Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233
Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
NUMBER: SH
TEST REPORT
AH00345415
TESTS CONDUCTED
4
PHTHALATE CONTENT TEST
WITH REFERENCE TO EN14372, BY GAS CHROMATOGRAPHY-MASS SPECTROMETRY (GC-MS) ANALYSIS.
TESTED COMPOUND RESULT
(%,W/W)
DIBUTYL PHTHALATE (DBP)
DI(2-ETHYL HEXYL) PHTHALATE(DEHP)
BENZYL BUTYL PHTHALATE (BBP)
SUM OF THREE PHTHALATES
ND
ND
ND
ND
LIMIT(%,W/W)
(MAX.)
------0.1
REMARK：THE ABOVE LIMIT WAS QUOTED ACCORDING TO ANNEX XVII ITEMS 51 & 52 OF THE REACH
REGULATION (EC) NO. 1907/2006 & AMENDENT NO.552/2009 FOR PHTHALATE CONTENT IN TOYS
AND CHILDREN CARE ARTICLES.
DETECTION LIMIT = 0.01%(W/W)
ND = NOT DETECTED
5
PHTHALATE CONTENT TEST
WITH REFERENCE TO CPSC-CH-C1001-09.3, BY GAS CHROMATOGRAPHY-MASS SPECTROMETRY (GC-MS)
ANALYSIS.
TESTED COMPOUND RESULT
DI-BUTYL PHTHALATE (DBP)
DI(2-ETHYL HEXYL) PHTHALATE(DEHP)
BENZYL BUTYL PHTHALATE (BBP)
(%,W/W)
ND
ND
ND
LIMIT(%,W/W)
(MAX.)
0.1
0.1
0.1
REMARK：THE ABOVE LIMIT WAS QUOTED ACCORDING TO US CONSUMER PRODUCT SAFETY
IMPROVEMENT ACT 2008 FOR PROHIBITION ON SALE OF CERTAIN PRODUCTS CONTAINING
SPECIFIED PHTHALATES.
DETECTION LIMIT = 0.01%(W/W)
ND = NOT DETECTED
************************************************************************************************************************************************************
TO BE CONTINUED
PAGE 8 OF 11
Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233
Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
NUMBER: SH
TEST REPORT
AH00345415
TESTS CONDUCTED
MEASUREMENT FLOWCHART:
TEST FOR PHTHALATES CONTENTS (EN14372)
WEIGH SAMPLE AND
PLACE IN A THIMBLE
EXTRACTED BY SOXHLET
EXTRACTION WITH
ORGANIC SOLVENT
CONCENTRATE THE
EXTRACT
Transfer the extract
into a volumetric
flask
MAKE UP WITH ORGANIC
SOLVENT
ANALYZE BY GC-MSD
************************************************************************************************************************************************************
TO BE CONTINUED
PAGE 9 OF 11
Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233
Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
NUMBER: SH
TEST REPORT
AH00345415
TESTS CONDUCTED
MEASUREMENT FLOWCHART:
TEST FOR PHTHALATES CONTENTS (CPSC-CH-C1001-09.3)
WEIGH SAMPLE AND
PLACE IN A TUBE
EXTRACTED WITH
ORGANIC SOLVENT BY
ULTRASONIC WATER
BATH
ANALYZE BY GC-MSD
************************************************************************************************************************************************************
TO BE CONTINUED
PAGE 10 OF 11
Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233
Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
TEST REPORT
NUMBER: SH
AH00345415
TESTS CONDUCTED
************************************************************************************************************************************************************
END OF REPORT
This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a recommendation for any particular
course of action. Intertek does not accept a duty of care or any other responsibility to any person other than the Client in respect of this report and only accepts liability
to the Client insofar as is expressly contained in the terms and conditions governing Intertek's provision of services to you. Intertek makes no warranties or
representations either express or implied with respect to this report save as provided for in those terms and conditions. We have aimed to conduct the Review on a
diligent and careful basis and we do not accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by statute or otherwise,
except in the event of our gross negligence or wilful misconduct.
PAGE 11 OF 11
Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233
Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
NUMBER: SH
TEST REPORT
APPLICANT:
AT
LITTELFUSE,INC.
800 E. NORTHWEST HWY
TN:
A.DIVIETRO/D.UNTIEDT
DATE:
AH00345432
OCT 29, 2012
SAMPLE DESCRIPTION:
ONE (1) SUBMITTED SAMPLE SAID TO BE BROWN INK.
PART DESCRIPTION
: INK-BROWN.
PART NUMBER
: 425906.
DATE SAMPLE RECEIVED
: OCTOBER.15, 2012.
DATE TEST STARTED
: OCTOBER.15, 2012.
*****************************************************************************************************************************************************
TESTS CONDUCTED:
AS REQUESTED BY THE APPLICANT, FOR DETAILS REFER TO ATTACHED PAGE(S)
*****************************************************************************************************************************************************
TO BE CONTINUED
AUTHORIZED BY：
FOR INTERTEK TESTING SERVICES
LTD., SHANGHAI
JACOB LIN
GENERAL MANAGER
PAGE 1 OF 11
Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233
Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
NUMBER: SH
TEST REPORT
AH00345432
TESTS CONDUCTED
1 ( Ⅰ) Test Result Summary :
Testing Item
Result (ppm)
Heavy Metal
Cadmium (Cd) content
Lead (Pb) content
Mercury (Hg) content
6+
Chromium VI (Cr ) content
Polybrominated Biphenyls (PBBs)
Monobrominated Biphenyls (MonoBB)
Dibrominated Biphenyls (DiBB)
Tribrominated Biphenyls (TriBB)
Tetrabrominated Biphenyls (TetraBB)
Pentabrominated Biphenyls (PentaBB)
Hexabrominated Biphenyls (HexaBB)
Heptabrominated Biphenyls (HeptaBB)
Octabrominated Biphenyls (OctaBB)
Nonabrominated Biphenyls (NonaBB)
Decabrominated Biphenyl (DecaBB)
Polybrominated Diphenyl Ethers (PBDEs)
Monobrominated Diphenyl Ethers (MonoBDE)
Dibrominated Diphenyl Ethers (DiBDE)
Tribrominated Diphenyl Ethers (TriBDE)
Tetrabrominated Diphenyl Ethers (TetraBDE)
Pentabrominated Diphenyl Ethers (PentaBDE)
Hexabrominated Diphenyl Ethers (HexaBDE)
Heptabrominated Diphenyl Ethers (HeptaBDE)
Octabrominated Diphenyl Ethers (OctaBDE)
Nonabrominated Diphenyl Ethers (NonaBDE)
Decabrominated Diphenyl Ether (DecaBDE)
(Ⅲ) Test Method:
Testing Item T
Cadmium (Cd) content
Lead (Pb) content
Mercury (Hg) content
6+
Chromium VI (Cr ) content
Polybrominated Biphenyls
(PBBs)
Polybrominated Diphenyl
Ethers (PBDEs)
esting Method R
With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10,
by microwave digestion until the tested samples are totally
dissolved and determined by ICP-OES.
With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10,
by microwave digestion until the tested samples are totally
dissolved and determined by ICP-OES.
With reference to IEC 62321 edition 1.0:2008 in clause 7, by
microwave digestion until the tested samples are totally
dissolved and determined by ICP-OES.
With reference to IEC 62321 edition 1.0:2008 in annex C, by
alkaline digestion and determined by UV-Vis spectrophotometer.
With reference to IEC 62321 edition 1.0:2008 in annex A, by
solvent extraction and determined by GC-MSD and further
HPLC confirmation when necessary.
With reference to IEC 62321 edition 1.0:2008 in annex A, by
solvent extraction and determined by GC-MSD and further
HPLC confirmation when necessary.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
eporting Limit
2 ppm
2 ppm
2 ppm
1 ppm
5 ppm
5 ppm
Remark:
Reporting limit = Quantitation limit of analyte in sample
*****************************************************************************************************************************************************
TO BE CONTINUED
PAGE 2 OF 11
Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233
Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
NUMBER: SH
TEST REPORT
AH00345432
TESTS CONDUCTED
(Ⅳ) Measurement Flowchart:
Test For Cd/Pb/Hg/Chromium (VI)/PBBs/PBDEs Contents
Reference Standard: IEC 62321 edition 1.0:2008
sampling/grinding or cutting
Cr6+
Cd/Pb/Hg
metal
weigh sample and
for different
material, digest
the sample with
confirm the tested
samples are totally
dissolved
spot test
negative*2
No
PBBs/PBDEs
polymers /
electronics
weigh sample
and add
organic
weigh sample
and add
alkaline
solution
get 50cm2
samples
definite
temp.
boiling water
extraction
cool and
filter the
extract
soxhlet
extraction or
solvent
extraction
make up with
deionized water
concentrate
the extract
and make up
with organic
analyzed by ICP-OES
make up with deionized
water and add diphenylcarbazide solution
analyzed by GCMSD
analyzed by UV-VIS
REMARKS:
*1: List of appropriate acid：
Material
Polymers
Metals HNO
Electronics H
Acid added for digestion
HNO3,HCl,HF,H2O2,H3BO3
3,HCl,HF
NO3,HCl,H2O2,HBF4
*2: If the result of spot test is positive, Chromium VI would be determined as detected.
*****************************************************************************************************************************************************
TO BE CONTINUED
PAGE 3 OF 11
Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233
Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
NUMBER: SH
TEST REPORT
AH00345432
TESTS CONDUCTED
2(
Ⅰ) Test Result Summary :
Testing Item
Halogen Content
Fluorine (F)
Chlorine (Cl)
Bromine (Br)
Iodine (I)
Remarks:
N
ppm
ND
8600
ND
ND
= Parts per million = mg/kg
=
D
Not detected
Responsibility Of Chemist
(Ⅲ) Test Method:
Testing Item T
Halogen Content
Result (ppm)
: Leaf Liu
esting Method R
With reference to EN 14582:2007 by combustion flask with
oxygen and determined by ion chromatography
eporting Limit
50 ppm
Remark:
Reporting limit = Quantitation limit of analyte in sample
*****************************************************************************************************************************************************
TO BE CONTINUED
PAGE 4 OF 11
Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233
Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
NUMBER: SH
TEST REPORT
AH00345432
TESTS CONDUCTED
(Ⅳ) Measurement Flowchart:
Test For Halogen Content
Reference Standard： EN 14582
sampling/grinding or
cutting
add absorbent in a
combustion flask &
place weighed sample in
equipment
fill the combustion
flask with oxygen
ignite then leave the
flask at room
temperature
transfer the absorbent
into a volumetric flask
make up with deionized
water
analyzed by ion
chromatography
*****************************************************************************************************************************************************
TO BE CONTINUED
PAGE 5 OF 11
Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233
Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
NUMBER: SH
TEST REPORT
AH00345432
TESTS CONDUCTED
3
(A) TEST RESULT SUMMARY:
TESTING ITEM R
ESULT(ppm)
HBCD (HEXABROMOCYCLODODECANE)
ND
REMARKS:
ppm = PARTS PER MILLION = mg/kg
ND = NOT DETECTED
(B) TEST METHOD :
TESTING ITEM T
ESTING METHOD
REPORTING
LIMIT
WITH REFERENCE TO USEPA 3540C, BY
HBCD (HEXABROMOCYCLODODECANE) SOLVENT EXTRACTION AND DETERMINED
10 ppm
BY GC/MS
*****************************************************************************************************************************************************
TO BE CONTINUED
PAGE 6 OF 11
Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233
Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
NUMBER: SH
TEST REPORT
AH00345432
TESTS CONDUCTED
MEASUREMENT FLOWCHART:
TEST FOR HBCD (HEXABROMOCYCLODODECANE) CONTENT
WEIGH SAMPLE AND PLACE
INTO A THIMBLE
SOXHLET EXTRACTION WITH
ORGANIC SOLVENT
CONCENTRATE THE EXTRACT
TRANSFER THE EXTRACT
INTO A VOLUMETRIC FLASK
MAKE UP WITH ORGANIC
SOLVENT
ANALYZE BY GC-MSD
*****************************************************************************************************************************************************
TO BE CONTINUED
PAGE 7 OF 11
Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233
Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
NUMBER: SH
TEST REPORT
AH00345432
TESTS CONDUCTED
4
PHTHALATE CONTENT TEST
WITH REFERENCE TO EN14372, BY GAS CHROMATOGRAPHY-MASS SPECTROMETRY (GC-MS) ANALYSIS.
TESTED COMPOUND RESULT
(%,W/W)
DIBUTYL PHTHALATE (DBP)
DI(2-ETHYL HEXYL) PHTHALATE(DEHP)
BENZYL BUTYL PHTHALATE (BBP)
ND
ND
ND
LIMIT(%,W/W)
(MAX.)
-------
SUM OF THREE PHTHALATES
ND
0.1
REMARK： THE ABOVE LIMIT WAS QUOTED ACCORDING TO ANNEX XVII ITEMS 51 & 52 OF THE REACH
REGULATION (EC) NO. 1907/2006 & AMENDENT NO.552/2009 (FORMERLY KNOWN AS
DIRECTIVE 2005/84/EC) FOR PHTHALATE CONTENT IN TOYS AND CHILDREN CARE ARTICLES.
DETECTION LIMIT = 0.01%(W/W)
ND = NOT DETECTED
5
PHTHALATE CONTENT TEST
WITH REFERENCE TO CPSC-CH-C1001-09.3, BY GAS CHROMATOGRAPHY-MASS SPECTROMETRY (GC-MS)
ANALYSIS.
TESTED COMPOUND RESULT
DI-BUTYL PHTHALATE (DBP)
DI(2-ETHYL HEXYL) PHTHALATE(DEHP)
BENZYL BUTYL PHTHALATE (BBP)
REMARK：
(%,W/W)
ND
ND
ND
LIMIT(%,W/W)
(MAX.)
0.1
0.1
0.1
THE ABOVE LIMIT WAS QUOTED ACCORDING TO US CONSUMER PRODUCT SAFETY
IMPROVEMENT ACT 2008 FOR PROHIBITION ON SALE OF CERTAIN PRODUCTS CONTAINING
SPECIFIED PHTHALATES.
DETECTION LIMIT = 0.01%(W/W)
ND = NOT DETECTED
DATE SAMPLE RECEIVED：OCT.15, 2012
TESTING PERIOD：OCT.15, 2012 TO OCT.23, 2012
*****************************************************************************************************************************************************
TO BE CONTINUED
PAGE 8 OF 11
Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233
Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
NUMBER: SH
TEST REPORT
AH00345432
TESTS CONDUCTED
MEASUREMENT FLOWCHART:
TEST FOR PHTHALATES CONTENTS (EN14372)
Weigh sample and
place in a thimble
Extracted by Soxhlet
extraction with
organic solvent
Concentrate the
extract
Transfer the extract
into a volumetric
flask
Make up with organic
solvent
Analyze by GC-MSD
*****************************************************************************************************************************************************
TO BE CONTINUED
PAGE 9 OF 11
Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233
Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
NUMBER: SH
TEST REPORT
AH00345432
TESTS CONDUCTED
MEASUREMENT FLOWCHART:
TEST FOR PHTHALATES CONTENTS (CPSC-CH-C1001-09.3)
Weigh sample and
place in a tube
Extracted with
organic solvent by
ultrasonic water
bath
Analyze by GC-MSD
*****************************************************************************************************************************************************
TO BE CONTINUED
PAGE 10 OF 11
Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233
Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
TEST REPORT
NUMBER: SH
AH00345432
TESTS CONDUCTED
*****************************************************************************************************************************************************
END OF REPORT
This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a recommendation for any particular
course of action. Intertek does not accept a duty of care or any other responsibility to any person other than the Client in respect of this report and only accepts liability
to the Client insofar as is expressly contained in the terms and conditions governing Intertek's provision of services to you. Intertek makes no warranties or
representations either express or implied with respect to this report save as provided for in those terms and conditions. We have aimed to conduct the Review on a
diligent and careful basis and we do not accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by statute or otherwise,
except in the event of our gross negligence or wilful misconduct.
PAGE 11 OF 11
Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233
Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
NUMBER: SH
TEST REPORT
APPLICANT:
ATT
LITTELFUSE,INC.
800 E. NORTHWEST HWY
N:
A.DIVIETRO/D.UNTIEDT
DATE:
AH00345639
OCT 29, 2012
SAMPLE DESCRIPTION:
ONE (1) SUBMITTED SAMPLE SAID TO BE GREEN INK.
PART DESCRIPTION
: INK-GREEN.
PART NUMBER
: 425907.
DATE SAMPLE RECEIVED
: OCTOBER.15, 2012.
DATE TEST STARTED
: OCTOBER.15, 2012.
**************************************************************************************************************************************************
TESTS CONDUCTED:
AS REQUESTED BY THE APPLICANT, FOR DETAILS REFER TO ATTACHED PAGE(S)
**************************************************************************************************************************************************
TO BE CONTINUED
AUTHORIZED BY：
FOR INTERTEK TESTING SERVICES
LTD., SHANGHAI
JACOB LIN
GENERAL MANAGER
PAGE 1 OF 11
Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233
Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
NUMBER: SH
TEST REPORT
AH00345639
TESTS CONDUCTED
1(
Ⅰ) Test Result Summary :
Testing Item
Result (ppm)
Heavy Metal
Cadmium (Cd) content
Lead (Pb) content
Mercury (Hg) content
6+
Chromium VI (Cr ) content
Polybrominated Biphenyls (PBBs)
Monobrominated Biphenyls (MonoBB)
Dibrominated Biphenyls (DiBB)
Tribrominated Biphenyls (TriBB)
Tetrabrominated Biphenyls (TetraBB)
Pentabrominated Biphenyls (PentaBB)
Hexabrominated Biphenyls (HexaBB)
Heptabrominated Biphenyls (HeptaBB)
Octabrominated Biphenyls (OctaBB)
Nonabrominated Biphenyls (NonaBB)
Decabrominated Biphenyl (DecaBB)
Polybrominated Diphenyl Ethers (PBDEs)
Monobrominated Diphenyl Ethers (MonoBDE)
Dibrominated Diphenyl Ethers (DiBDE)
Tribrominated Diphenyl Ethers (TriBDE)
Tetrabrominated Diphenyl Ethers (TetraBDE)
Pentabrominated Diphenyl Ethers (PentaBDE)
Hexabrominated Diphenyl Ethers (HexaBDE)
Heptabrominated Diphenyl Ethers (HeptaBDE)
Octabrominated Diphenyl Ethers (OctaBDE)
Nonabrominated Diphenyl Ethers (NonaBDE)
Decabrominated Diphenyl Ether (DecaBDE)
(Ⅲ) Test Method:
Testing Item T
Cadmium (Cd) content
Lead (Pb) content
Mercury (Hg) content
6+
Chromium VI (Cr ) content
Polybrominated Biphenyls
(PBBs)
Polybrominated Diphenyl
Ethers (PBDEs)
esting Method R
With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10,
by microwave digestion until the tested samples are totally
dissolved and determined by ICP-OES.
With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10,
by microwave digestion until the tested samples are totally
dissolved and determined by ICP-OES.
With reference to IEC 62321 edition 1.0:2008 in clause 7, by
microwave digestion until the tested samples are totally
dissolved and determined by ICP-OES.
With reference to IEC 62321 edition 1.0:2008 in annex C, by
alkaline digestion and determined by UV-Vis spectrophotometer.
With reference to IEC 62321 edition 1.0:2008 in annex A, by
solvent extraction and determined by GC-MSD and further
HPLC confirmation when necessary.
With reference to IEC 62321 edition 1.0:2008 in annex A, by
solvent extraction and determined by GC-MSD and further
HPLC confirmation when necessary.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
eporting Limit
2 ppm
2 ppm
2 ppm
1 ppm
5 ppm
5 ppm
Remark:
Reporting limit = Quantitation limit of analyte in sample
**************************************************************************************************************************************************
TO BE CONTINUED
PAGE 2 OF 11
Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233
Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
NUMBER: SH
TEST REPORT
AH00345639
TESTS CONDUCTED
(Ⅳ) Measurement Flowchart:
Test For Cd/Pb/Hg/Chromium (VI)/PBBs/PBDEs Contents
Reference Standard: IEC 62321 edition 1.0:2008
sampling/grinding or cutting
Cr6+
Cd/Pb/Hg
metal
weigh sample and
for different
material, digest
the sample with
confirm the tested
samples are totally
dissolved
spot test
negative*2
No
PBBs/PBDEs
polymers /
electronics
weigh sample
and add
organic
weigh sample
and add
alkaline
solution
get 50cm2
samples
definite
temp.
boiling water
extraction
cool and
filter the
extract
soxhlet
extraction or
solvent
extraction
make up with
deionized water
concentrate
the extract
and make up
with organic
analyzed by ICP-OES
make up with deionized
water and add diphenylcarbazide solution
analyzed by GCMSD
analyzed by UV-VIS
REMARKS:
*1: List of appropriate acid：
Material
Polymers
Metals HNO
Electronics H
Acid added for digestion
HNO3,HCl,HF,H2O2,H3BO3
3,HCl,HF
NO3,HCl,H2O2,HBF4
*2: If the result of spot test is positive, Chromium VI would be determined as detected.
**************************************************************************************************************************************************
TO BE CONTINUED
PAGE 3 OF 11
Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233
Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
NUMBER: SH
TEST REPORT
AH00345639
TESTS CONDUCTED
2
(Ⅰ) Test Result Summary :
Testing Item
Halogen Content
Fluorine (F)
Chlorine (Cl)
Bromine (Br)
Iodine (I)
Remarks:
ND
ppm
200
650
ND
ND
= Parts per million = mg/kg
=
Not detected
Responsibility Of Chemist
(Ⅲ) Test Method:
Testing Item T
Halogen Content
Result (ppm)
: Leaf Liu
esting Method R
With reference to EN 14582:2007 by combustion flask with
oxygen and determined by ion chromatography
eporting Limit
50 ppm
Remark:
Reporting limit = Quantitation limit of analyte in sample
**************************************************************************************************************************************************
TO BE CONTINUED
PAGE 4 OF 11
Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233
Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
NUMBER: SH
TEST REPORT
AH00345639
TESTS CONDUCTED
(Ⅳ) Measurement Flowchart:
Test For Halogen Content
Reference Standard： EN 14582
sampling/grinding or
cutting
add absorbent in a
combustion flask &
place weighed sample in
equipment
fill the combustion
flask with oxygen
ignite then leave the
flask at room
temperature
transfer the absorbent
into a volumetric flask
make up with deionized
water
analyzed by ion
chromatography
**************************************************************************************************************************************************
TO BE CONTINUED
PAGE 5 OF 11
Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233
Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
NUMBER: SH
TEST REPORT
AH00345639
TESTS CONDUCTED
3
(A) TEST RESULT SUMMARY:
TESTING ITEM R
HBCD (HEXABROMOCYCLODODECANE)
ESULT(ppm)
ND
REMARKS:
ppm = PARTS PER MILLION = mg/kg
ND = NOT DETECTED
(B) TEST METHOD :
TESTING ITEM TE
STING METHOD
REPORTING
LIMIT
WITH REFERENCE TO USEPA 3540C, BY
SOLVENT EXTRACTION AND DETERMINED
10 ppm
BY GC/MS
**************************************************************************************************************************************************
TO BE CONTINUED
HBCD (HEXABROMOCYCLODODECANE)
PAGE 6 OF 11
Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233
Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
NUMBER: SH
TEST REPORT
AH00345639
TESTS CONDUCTED
MEASUREMENT FLOWCHART:
TEST FOR HBCD (HEXABROMOCYCLODODECANE) CONTENT
WEIGH SAMPLE AND PLACE
INTO A THIMBLE
SOXHLET EXTRACTION WITH
ORGANIC SOLVENT
CONCENTRATE THE EXTRACT
TRANSFER THE EXTRACT
INTO A VOLUMETRIC FLASK
MAKE UP WITH ORGANIC
SOLVENT
ANALYZE BY GC-MSD
**************************************************************************************************************************************************
TO BE CONTINUED
PAGE 7 OF 11
Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233
Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
NUMBER: SH
TEST REPORT
AH00345639
TESTS CONDUCTED
4 PHT
HALATE CONTENT TEST
WITH REFERENCE TO EN14372, BY GAS CHROMATOGRAPHY-MASS SPECTROMETRY (GC-MS) ANALYSIS.
TESTED COMPOUND R
ESULT (%,W/W)
DIBUTYL PHTHALATE (DBP)
DI(2-ETHYL HEXYL) PHTHALATE(DEHP)
BENZYL BUTYL PHTHALATE (BBP)
SUM OF THREE PHTHALATES
ND
ND
ND
ND
LIMIT(%,W/W)
(MAX.)
------0.1
REMARK：THE ABOVE LIMIT WAS QUOTED ACCORDING TO ANNEX XVII ITEMS 51 & 52 OF THE REACH
REGULATION (EC) NO. 1907/2006 & AMENDENT NO.552/2009 FOR PHTHALATE CONTENT IN TOYS
AND CHILDREN CARE ARTICLES.
DETECTION LIMIT = 0.01%(W/W)
ND = NOT DETECTED
5 PHT
HALATE CONTENT TEST
WITH REFERENCE TO CPSC-CH-C1001-09.3, BY GAS CHROMATOGRAPHY-MASS SPECTROMETRY (GC-MS)
ANALYSIS.
TESTED COMPOUND R
ESULT (%,W/W)
DI-BUTYL PHTHALATE (DBP)
DI(2-ETHYL HEXYL) PHTHALATE(DEHP)
BENZYL BUTYL PHTHALATE (BBP)
ND
ND
ND
LIMIT(%,W/W)
(MAX.)
0.1
0.1
0.1
REMARK：THE ABOVE LIMIT WAS QUOTED ACCORDING TO US CONSUMER PRODUCT SAFETY
IMPROVEMENT ACT 2008 & AMENDMENT H.R.2715 FOR PROHIBITION ON SALE OF CERTAIN
PRODUCTS CONTAINING SPECIFIED PHTHALATES.
DETECTION LIMIT = 0.01%(W/W)
ND = NOT DETECTED
DATE SAMPLE RECEIVED : OCT.15, 2012
TESTING PERIOD : OCT.15, 2012 TO OCT.18, 2012
**************************************************************************************************************************************************
TO BE CONTINUED
PAGE 8 OF 11
Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233
Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
NUMBER: SH
TEST REPORT
AH00345639
TESTS CONDUCTED
MEASUREMENT FLOWCHART:
TEST FOR PHTHALATES CONTENTS (EN14372)
WEIGH SAMPLE AND
PLACE IN A THIMBLE
EXTRACTED BY SOXHLET
EXTRACTION WITH
ORGANIC SOLVENT
CONCENTRATE THE
EXTRACT
Transfer the extract
into a volumetric
flask
MAKE UP WITH ORGANIC
SOLVENT
ANALYZE BY GC-MSD
**************************************************************************************************************************************************
TO BE CONTINUED
PAGE 9 OF 11
Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233
Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
NUMBER: SH
TEST REPORT
AH00345639
TESTS CONDUCTED
MEASUREMENT FLOWCHART:
TEST FOR PHTHALATES CONTENTS (CPSC-CH-C1001-09.3)
Weigh sample and
place in a tube
Extracted with
organic solvent by
ultrasonic water
bath
Analyze by GC-MSD
**************************************************************************************************************************************************
TO BE CONTINUED
PAGE 10 OF 11
Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233
Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
TEST REPORT
NUMBER: SH
AH00345639
TESTS CONDUCTED
**************************************************************************************************************************************************
END OF REPORT
This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a recommendation for any particular
course of action. Intertek does not accept a duty of care or any other responsibility to any person other than the Client in respect of this report and only accepts liability
to the Client insofar as is expressly contained in the terms and conditions governing Intertek's provision of services to you. Intertek makes no warranties or
representations either express or implied with respect to this report save as provided for in those terms and conditions. We have aimed to conduct the Review on a
diligent and careful basis and we do not accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by statute or otherwise,
except in the event of our gross negligence or wilful misconduct.
PAGE 11 OF 11
Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233
Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
NUMBER: SH
TEST REPORT
APPLICANT:
AT
LITTELFUSE,INC.
800 E. NORTHWEST HWY
TN:
A.DIVIETRO/D.UNTIEDT
DATE:
AH00345659
OCT 26, 2012
SAMPLE DESCRIPTION:
ONE (1) SUBMITTED SAMPLE SAID TO BE:GREY INK.
PART DESCRIPTION
: INK-GREY.
PART NUMBER
: 425909.
DATE SAMPLE RECEIVED
: OCTOBER.15, 2012.
DATE TEST STARTED
: OCTOBER.15, 2012.
******************************************************************************************************************************************************
TESTS CONDUCTED:
AS REQUESTED BY THE APPLICANT, FOR DETAILS REFER TO ATTACHED PAGE(S)
******************************************************************************************************************************************************
TO BE CONTINUED
AUTHORIZED BY：
FOR INTERTEK TESTING SERVICES
LTD., SHANGHAI
JACOB LIN
GENERAL MANAGER
PAGE 1 OF 11
Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233
Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
NUMBER: SH
TEST REPORT
AH00345659
TESTS CONDUCTED
1 ( Ⅰ) Test Result Summary :
Testing Item
Result (ppm)
Heavy Metal
Cadmium (Cd) content
Lead (Pb) content
Mercury (Hg) content
6+
Chromium VI (Cr ) content
Polybrominated Biphenyls (PBBs)
Monobrominated Biphenyls (MonoBB)
Dibrominated Biphenyls (DiBB)
Tribrominated Biphenyls (TriBB)
Tetrabrominated Biphenyls (TetraBB)
Pentabrominated Biphenyls (PentaBB)
Hexabrominated Biphenyls (HexaBB)
Heptabrominated Biphenyls (HeptaBB)
Octabrominated Biphenyls (OctaBB)
Nonabrominated Biphenyls (NonaBB)
Decabrominated Biphenyl (DecaBB)
Polybrominated Diphenyl Ethers (PBDEs)
Monobrominated Diphenyl Ethers (MonoBDE)
Dibrominated Diphenyl Ethers (DiBDE)
Tribrominated Diphenyl Ethers (TriBDE)
Tetrabrominated Diphenyl Ethers (TetraBDE)
Pentabrominated Diphenyl Ethers (PentaBDE)
Hexabrominated Diphenyl Ethers (HexaBDE)
Heptabrominated Diphenyl Ethers (HeptaBDE)
Octabrominated Diphenyl Ethers (OctaBDE)
Nonabrominated Diphenyl Ethers (NonaBDE)
Decabrominated Diphenyl Ether (DecaBDE)
(Ⅲ) Test Method:
Testing Item T
Cadmium (Cd) content
Lead (Pb) content
Mercury (Hg) content
6+
Chromium VI (Cr ) content
Polybrominated Biphenyls
(PBBs)
Polybrominated Diphenyl
Ethers (PBDEs)
esting Method R
With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10,
by microwave digestion until the tested samples are totally
dissolved and determined by ICP-OES.
With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10,
by microwave digestion until the tested samples are totally
dissolved and determined by ICP-OES.
With reference to IEC 62321 edition 1.0:2008 in clause 7, by
microwave digestion until the tested samples are totally
dissolved and determined by ICP-OES.
With reference to IEC 62321 edition 1.0:2008 in annex C, by
alkaline digestion and determined by UV-Vis spectrophotometer.
With reference to IEC 62321 edition 1.0:2008 in annex A, by
solvent extraction and determined by GC-MSD and further
HPLC confirmation when necessary.
With reference to IEC 62321 edition 1.0:2008 in annex A, by
solvent extraction and determined by GC-MSD and further
HPLC confirmation when necessary.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
eporting Limit
2 ppm
2 ppm
2 ppm
1 ppm
5 ppm
5 ppm
Remark:
Reporting limit = Quantitation limit of analyte in sample
******************************************************************************************************************************************************
TO BE CONTINUED
PAGE 2 OF 11
Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233
Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
NUMBER: SH
TEST REPORT
AH00345659
TESTS CONDUCTED
(Ⅳ) Measurement Flowchart:
Test For Cd/Pb/Hg/Chromium (VI)/PBBs/PBDEs Contents
Reference Standard: IEC 62321 edition 1.0:2008
sampling/grinding or cutting
Cr6+
Cd/Pb/Hg
metal
weigh sample and
for different
material, digest
the sample with
confirm the tested
samples are totally
dissolved
spot test
negative*2
No
PBBs/PBDEs
polymers /
electronics
weigh sample
and add
organic
weigh sample
and add
alkaline
solution
get 50cm2
samples
definite
temp.
boiling water
extraction
cool and
filter the
extract
soxhlet
extraction or
solvent
extraction
make up with
deionized water
concentrate
the extract
and make up
with organic
analyzed by ICP-OES
make up with deionized
water and add diphenylcarbazide solution
analyzed by GCMSD
analyzed by UV-VIS
REMARKS:
*1: List of appropriate acid：
Material
Polymers
Metals HNO
Electronics H
Acid added for digestion
HNO3,HCl,HF,H2O2,H3BO3
3,HCl,HF
NO3,HCl,H2O2,HBF4
*2: If the result of spot test is positive, Chromium VI would be determined as detected.
************************************************************************************************************************************************************
TO BE CONTINUED
PAGE 3 OF 11
Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233
Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
NUMBER: SH
TEST REPORT
AH00345659
TESTS CONDUCTED
2(
Ⅰ) Test Result Summary :
Testing Item
Halogen Content
Fluorine (F)
Chlorine (Cl)
Bromine (Br)
Iodine (I)
Remarks:
N
ppm
ND
ND
ND
ND
= Parts per million based on weight of tested sample = mg/kg
=
D
Not detected
Responsibility Of Chemist
(Ⅲ) Test Method:
Testing Item T
Halogen Content
Result (ppm)
: Ken He
esting Method R
With reference to EN 14582:2007 by combustion flask with
oxygen and determined by ion chromatography
eporting Limit
50 ppm
Remark:
Reporting limit = Quantitation limit of analyte in sample
************************************************************************************************************************************************************
TO BE CONTINUED
PAGE 4 OF 11
Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233
Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
NUMBER: SH
TEST REPORT
AH00345659
TESTS CONDUCTED
(Ⅳ) Measurement Flowchart:
Test For Halogen Content
Reference Standard： EN 14582
sampling/grinding or
cutting
add absorbent in a
combustion flask &
place weighed sample in
equipment
fill the combustion
flask with oxygen
ignite then leave the
flask at room
temperature
transfer the absorbent
into a volumetric flask
make up with deionized
water
analyzed by ion
chromatography
************************************************************************************************************************************************************
TO BE CONTINUED
PAGE 5 OF 11
Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233
Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
NUMBER: SH
TEST REPORT
AH00345659
TESTS CONDUCTED
3 (A) TEST RESULT SUMMARY:
TESTING ITEM R
HBCD (HEXABROMOCYCLODODECANE)
ESULT(ppm)
ND
REMARKS:
ppm = PARTS PER MILLION = mg/kg
ND = NOT DETECTED
(B) TEST METHOD :
TESTING ITEM T
ESTING METHOD
REPORTING
LIMIT
WITH REFERENCE TO USEPA 3540C, BY SOLVENT
10 ppm
EXTRACTION AND DETERMINED BY GC/MS
************************************************************************************************************************************************************
TO BE CONTINUED
HBCD (HEXABROMOCYCLODODECANE)
PAGE 6 OF 11
Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233
Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
NUMBER: SH
TEST REPORT
AH00345659
TESTS CONDUCTED
MEASUREMENT FLOWCHART:
TEST FOR HBCD (HEXABROMOCYCLODODECANE) CONTENT
WEIGH SAMPLE AND PLACE
INTO A THIMBLE
SOXHLET EXTRACTION WITH
ORGANIC SOLVENT
CONCENTRATE THE EXTRACT
TRANSFER THE EXTRACT
INTO A VOLUMETRIC FLASK
MAKE UP WITH ORGANIC
SOLVENT
ANALYZE BY GC-MSD
************************************************************************************************************************************************************
TO BE CONTINUED
PAGE 7 OF 11
Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233
Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
NUMBER: SH
TEST REPORT
AH00345659
TESTS CONDUCTED
4
PHTHALATE CONTENT TEST
WITH REFERENCE TO EN14372, BY GAS CHROMATOGRAPHY-MASS SPECTROMETRY (GC-MS) ANALYSIS.
TESTED COMPOUND RESULT
(%,W/W)
DIBUTYL PHTHALATE (DBP)
DI(2-ETHYL HEXYL) PHTHALATE(DEHP)
BENZYL BUTYL PHTHALATE (BBP)
SUM OF THREE PHTHALATES
ND
ND
ND
ND
LIMIT(%,W/W)
(MAX.)
------0.1
REMARK：THE ABOVE LIMIT WAS QUOTED ACCORDING TO ANNEX XVII ITEMS 51 & 52 OF THE REACH
REGULATION (EC) NO. 1907/2006 & AMENDENT NO.552/2009 FOR PHTHALATE CONTENT IN TOYS
AND CHILDREN CARE ARTICLES.
DETECTION LIMIT = 0.01%(W/W)
ND = NOT DETECTED
5
PHTHALATE CONTENT TEST
WITH REFERENCE TO CPSC-CH-C1001-09.3, BY GAS CHROMATOGRAPHY-MASS SPECTROMETRY (GC-MS)
ANALYSIS.
TESTED COMPOUND RESULT
DI-BUTYL PHTHALATE (DBP)
DI(2-ETHYL HEXYL) PHTHALATE(DEHP)
BENZYL BUTYL PHTHALATE (BBP)
(%,W/W)
ND
ND
ND
LIMIT(%,W/W)
(MAX.)
0.1
0.1
0.1
REMARK：THE ABOVE LIMIT WAS QUOTED ACCORDING TO US CONSUMER PRODUCT SAFETY
IMPROVEMENT ACT 2008 FOR PROHIBITION ON SALE OF CERTAIN PRODUCTS CONTAINING
SPECIFIED PHTHALATES.
DETECTION LIMIT = 0.01%(W/W)
ND = NOT DETECTED
************************************************************************************************************************************************************
TO BE CONTINUED
PAGE 8 OF 11
Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233
Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
NUMBER: SH
TEST REPORT
AH00345659
TESTS CONDUCTED
MEASUREMENT FLOWCHART:
TEST FOR PHTHALATES CONTENTS (EN14372)
WEIGH SAMPLE AND
PLACE IN A THIMBLE
EXTRACTED BY SOXHLET
EXTRACTION WITH
ORGANIC SOLVENT
CONCENTRATE THE
EXTRACT
Transfer the extract
into a volumetric
flask
MAKE UP WITH ORGANIC
SOLVENT
ANALYZE BY GC-MSD
************************************************************************************************************************************************************
TO BE CONTINUED
PAGE 9 OF 11
Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233
Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
NUMBER: SH
TEST REPORT
AH00345659
TESTS CONDUCTED
MEASUREMENT FLOWCHART:
TEST FOR PHTHALATES CONTENTS (CPSC-CH-C1001-09.3)
WEIGH SAMPLE AND
PLACE IN A TUBE
EXTRACTED WITH
ORGANIC SOLVENT BY
ULTRASONIC WATER
BATH
ANALYZE BY GC-MSD
************************************************************************************************************************************************************
TO BE CONTINUED
PAGE 10 OF 11
Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233
Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
TEST REPORT
NUMBER: SH
AH00345659
TESTS CONDUCTED
************************************************************************************************************************************************************
END OF REPORT
This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a recommendation for any particular
course of action. Intertek does not accept a duty of care or any other responsibility to any person other than the Client in respect of this report and only accepts liability
to the Client insofar as is expressly contained in the terms and conditions governing Intertek's provision of services to you. Intertek makes no warranties or
representations either express or implied with respect to this report save as provided for in those terms and conditions. We have aimed to conduct the Review on a
diligent and careful basis and we do not accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by statute or otherwise,
except in the event of our gross negligence or wilful misconduct.
PAGE 11 OF 11
Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233
Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
NUMBER: SH
TEST REPORT
APPLICANT:
ATT
LITTELFUSE,INC.
800 E. NORTHWEST HWY
N:
A.DIVIETRO/D.UNTIEDT
DATE:
AH00345657
OCT 29, 2012
SAMPLE DESCRIPTION:
ONE (1) SUBMITTED SAMPLE SAID TO BE PALE BLUE INK.
PART DESCRIPTION
: INK-PALE BLUE.
PART NUMBER
: 425913.
DATE SAMPLE RECEIVED
: OCTOBER.15, 2012.
DATE TEST STARTED
: OCTOBER.15, 2012.
**************************************************************************************************************************************************
TESTS CONDUCTED:
AS REQUESTED BY THE APPLICANT, FOR DETAILS REFER TO ATTACHED PAGE(S)
**************************************************************************************************************************************************
TO BE CONTINUED
AUTHORIZED BY：
FOR INTERTEK TESTING SERVICES
LTD., SHANGHAI
JACOB LIN
GENERAL MANAGER
PAGE 1 OF 11
Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233
Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
NUMBER: SH
TEST REPORT
AH00345657
TESTS CONDUCTED
1(
Ⅰ) Test Result Summary :
Testing Item
Result (ppm)
Heavy Metal
Cadmium (Cd) content
Lead (Pb) content
Mercury (Hg) content
6+
Chromium VI (Cr ) content
Polybrominated Biphenyls (PBBs)
Monobrominated Biphenyls (MonoBB)
Dibrominated Biphenyls (DiBB)
Tribrominated Biphenyls (TriBB)
Tetrabrominated Biphenyls (TetraBB)
Pentabrominated Biphenyls (PentaBB)
Hexabrominated Biphenyls (HexaBB)
Heptabrominated Biphenyls (HeptaBB)
Octabrominated Biphenyls (OctaBB)
Nonabrominated Biphenyls (NonaBB)
Decabrominated Biphenyl (DecaBB)
Polybrominated Diphenyl Ethers (PBDEs)
Monobrominated Diphenyl Ethers (MonoBDE)
Dibrominated Diphenyl Ethers (DiBDE)
Tribrominated Diphenyl Ethers (TriBDE)
Tetrabrominated Diphenyl Ethers (TetraBDE)
Pentabrominated Diphenyl Ethers (PentaBDE)
Hexabrominated Diphenyl Ethers (HexaBDE)
Heptabrominated Diphenyl Ethers (HeptaBDE)
Octabrominated Diphenyl Ethers (OctaBDE)
Nonabrominated Diphenyl Ethers (NonaBDE)
Decabrominated Diphenyl Ether (DecaBDE)
(Ⅲ) Test Method:
Testing Item T
Cadmium (Cd) content
Lead (Pb) content
Mercury (Hg) content
6+
Chromium VI (Cr ) content
Polybrominated Biphenyls
(PBBs)
Polybrominated Diphenyl
Ethers (PBDEs)
esting Method R
With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10,
by microwave digestion until the tested samples are totally
dissolved and determined by ICP-OES.
With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10,
by microwave digestion until the tested samples are totally
dissolved and determined by ICP-OES.
With reference to IEC 62321 edition 1.0:2008 in clause 7, by
microwave digestion until the tested samples are totally
dissolved and determined by ICP-OES.
With reference to IEC 62321 edition 1.0:2008 in annex C, by
alkaline digestion and determined by UV-Vis spectrophotometer.
With reference to IEC 62321 edition 1.0:2008 in annex A, by
solvent extraction and determined by GC-MSD and further
HPLC confirmation when necessary.
With reference to IEC 62321 edition 1.0:2008 in annex A, by
solvent extraction and determined by GC-MSD and further
HPLC confirmation when necessary.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
eporting Limit
2 ppm
2 ppm
2 ppm
1 ppm
5 ppm
5 ppm
Remark:
Reporting limit = Quantitation limit of analyte in sample
**************************************************************************************************************************************************
TO BE CONTINUED
PAGE 2 OF 11
Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233
Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
NUMBER: SH
TEST REPORT
AH00345657
TESTS CONDUCTED
(Ⅳ) Measurement Flowchart:
Test For Cd/Pb/Hg/Chromium (VI)/PBBs/PBDEs Contents
Reference Standard: IEC 62321 edition 1.0:2008
sampling/grinding or cutting
Cr6+
Cd/Pb/Hg
metal
weigh sample and
for different
material, digest
the sample with
confirm the tested
samples are totally
dissolved
spot test
negative*2
No
PBBs/PBDEs
polymers /
electronics
weigh sample
and add
organic
weigh sample
and add
alkaline
solution
get 50cm2
samples
definite
temp.
boiling water
extraction
cool and
filter the
extract
soxhlet
extraction or
solvent
extraction
make up with
deionized water
concentrate
the extract
and make up
with organic
analyzed by ICP-OES
make up with deionized
water and add diphenylcarbazide solution
analyzed by GCMSD
analyzed by UV-VIS
REMARKS:
*1: List of appropriate acid：
Material
Polymers
Metals HNO
Electronics H
Acid added for digestion
HNO3,HCl,HF,H2O2,H3BO3
3,HCl,HF
NO3,HCl,H2O2,HBF4
*2: If the result of spot test is positive, Chromium VI would be determined as detected.
**************************************************************************************************************************************************
TO BE CONTINUED
PAGE 3 OF 11
Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233
Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
NUMBER: SH
TEST REPORT
AH00345657
TESTS CONDUCTED
2(
Ⅰ) Test Result Summary :
Testing Item
Halogen Content
Fluorine (F)
Chlorine (Cl)
Bromine (Br)
Iodine (I)
Remarks:
ND
ppm
ND
ND
ND
ND
= Parts per million = mg/kg
=
Not detected
Responsibility Of Chemist
(Ⅲ) Test Method:
Testing Item T
Halogen Content
Result (ppm)
: Leaf Liu
esting Method R
With reference to EN 14582:2007 by combustion flask with
oxygen and determined by ion chromatography
eporting Limit
50 ppm
Remark:
Reporting limit = Quantitation limit of analyte in sample
**************************************************************************************************************************************************
TO BE CONTINUED
PAGE 4 OF 11
Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233
Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
NUMBER: SH
TEST REPORT
AH00345657
TESTS CONDUCTED
(Ⅳ) Measurement Flowchart:
Test For Halogen Content
Reference Standard： EN 14582
sampling/grinding or
cutting
add absorbent in a
combustion flask &
place weighed sample in
equipment
fill the combustion
flask with oxygen
ignite then leave the
flask at room
temperature
transfer the absorbent
into a volumetric flask
make up with deionized
water
analyzed by ion
chromatography
**************************************************************************************************************************************************
TO BE CONTINUED
PAGE 5 OF 11
Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233
Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
NUMBER: SH
TEST REPORT
AH00345657
TESTS CONDUCTED
3
(A) TEST RESULT SUMMARY:
TESTING ITEM R
HBCD (HEXABROMOCYCLODODECANE)
ESULT(ppm)
ND
REMARKS:
ppm = PARTS PER MILLION = mg/kg
ND = NOT DETECTED
(B) TEST METHOD :
TESTING ITEM TE
STING METHOD
REPORTING
LIMIT
WITH REFERENCE TO USEPA 3540C, BY
SOLVENT EXTRACTION AND DETERMINED
10 ppm
BY GC/MS
**************************************************************************************************************************************************
TO BE CONTINUED
HBCD (HEXABROMOCYCLODODECANE)
PAGE 6 OF 11
Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233
Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
NUMBER: SH
TEST REPORT
AH00345657
TESTS CONDUCTED
MEASUREMENT FLOWCHART:
TEST FOR HBCD (HEXABROMOCYCLODODECANE) CONTENT
WEIGH SAMPLE AND PLACE
INTO A THIMBLE
SOXHLET EXTRACTION WITH
ORGANIC SOLVENT
CONCENTRATE THE EXTRACT
TRANSFER THE EXTRACT
INTO A VOLUMETRIC FLASK
MAKE UP WITH ORGANIC
SOLVENT
ANALYZE BY GC-MSD
**************************************************************************************************************************************************
TO BE CONTINUED
PAGE 7 OF 11
Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233
Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
NUMBER: SH
TEST REPORT
AH00345657
TESTS CONDUCTED
4 PHT
HALATE CONTENT TEST
WITH REFERENCE TO EN14372, BY GAS CHROMATOGRAPHY-MASS SPECTROMETRY (GC-MS) ANALYSIS.
TESTED COMPOUND R
ESULT (%,W/W)
DIBUTYL PHTHALATE (DBP)
DI(2-ETHYL HEXYL) PHTHALATE(DEHP)
BENZYL BUTYL PHTHALATE (BBP)
SUM OF THREE PHTHALATES
ND
ND
ND
ND
LIMIT(%,W/W)
(MAX.)
------0.1
REMARK：THE ABOVE LIMIT WAS QUOTED ACCORDING TO ANNEX XVII ITEMS 51 & 52 OF THE REACH
REGULATION (EC) NO. 1907/2006 & AMENDENT NO.552/2009 FOR PHTHALATE CONTENT IN TOYS
AND CHILDREN CARE ARTICLES.
DETECTION LIMIT = 0.01%(W/W)
ND = NOT DETECTED
5 PHT
HALATE CONTENT TEST
WITH REFERENCE TO CPSC-CH-C1001-09.3, BY GAS CHROMATOGRAPHY-MASS SPECTROMETRY (GC-MS)
ANALYSIS.
TESTED COMPOUND R
ESULT (%,W/W)
DI-BUTYL PHTHALATE (DBP)
DI(2-ETHYL HEXYL) PHTHALATE(DEHP)
BENZYL BUTYL PHTHALATE (BBP)
ND
ND
ND
LIMIT(%,W/W)
(MAX.)
0.1
0.1
0.1
REMARK：THE ABOVE LIMIT WAS QUOTED ACCORDING TO US CONSUMER PRODUCT SAFETY
IMPROVEMENT ACT 2008 & AMENDMENT H.R.2715 FOR PROHIBITION ON SALE OF CERTAIN
PRODUCTS CONTAINING SPECIFIED PHTHALATES.
DETECTION LIMIT = 0.01%(W/W)
ND = NOT DETECTED
DATE SAMPLE RECEIVED : OCT.15, 2012
TESTING PERIOD : OCT.15, 2012 TO OCT.19, 2012
**************************************************************************************************************************************************
TO BE CONTINUED
PAGE 8 OF 11
Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233
Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
NUMBER: SH
TEST REPORT
AH00345657
TESTS CONDUCTED
MEASUREMENT FLOWCHART:
TEST FOR PHTHALATES CONTENTS (EN14372)
WEIGH SAMPLE AND
PLACE IN A THIMBLE
EXTRACTED BY SOXHLET
EXTRACTION WITH
ORGANIC SOLVENT
CONCENTRATE THE
EXTRACT
Transfer the extract
into a volumetric
flask
MAKE UP WITH ORGANIC
SOLVENT
ANALYZE BY GC-MSD
**************************************************************************************************************************************************
TO BE CONTINUED
PAGE 9 OF 11
Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233
Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
NUMBER: SH
TEST REPORT
AH00345657
TESTS CONDUCTED
MEASUREMENT FLOWCHART:
TEST FOR PHTHALATES CONTENTS (CPSC-CH-C1001-09.3)
Weigh sample and
place in a tube
Extracted with
organic solvent by
ultrasonic water
bath
Analyze by GC-MSD
**************************************************************************************************************************************************
TO BE CONTINUED
PAGE 10 OF 11
Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233
Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
TEST REPORT
NUMBER: SH
AH00345657
TESTS CONDUCTED
**************************************************************************************************************************************************
END OF REPORT
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course of action. Intertek does not accept a duty of care or any other responsibility to any person other than the Client in respect of this report and only accepts liability
to the Client insofar as is expressly contained in the terms and conditions governing Intertek's provision of services to you. Intertek makes no warranties or
representations either express or implied with respect to this report save as provided for in those terms and conditions. We have aimed to conduct the Review on a
diligent and careful basis and we do not accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by statute or otherwise,
except in the event of our gross negligence or wilful misconduct.
PAGE 11 OF 11
Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233
Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn