ICPTest_215XEP_04 13 2013 pdf

ICP Test Report Certification Packet
Company name :
Littelfuse, Inc.
Product Series:
5x20 Fuse
Product #:
215xxxXEP
Issue Date:
April 13, 2013
It is hereby certified by Littelfuse, Inc. that there is neither RoHS (EU Directive 2002/95/EC,
2011/65/EU)-restricted substance nor such use, for materials to be used for unit parts, for
packing/packaging materials, and for additives and the like in the manufacturing processes.
In addition, it is hereby reported to you that the parts and sub-materials, the materials to be used
for unit parts, the packing/packaging materials, and the additives and the like in the manufacturing
processes, are all composed of the following components.
Issued by:
<Global EHS Specialist >
(1) Parts, sub-materials and unit parts
This document covers the 5x20 Fuse RoHS-Compliant series products manufactured by
Littelfuse, Inc.
< Raw Materials Used
Please see Table 1
(2) The ICP data on all measurable substances
Please see appropriate pages as identifed in Table 1
Remarks:
Form 585-047 Rev. A
1
2/21/06
Table 1: List of Raw Materials covered by this report
Total
Parts
2
Raw Material Part
Number
030204, 934-077,
C030210, 934-079
C910510, 910-555
(replaced 910-553)
3
4
5
910-556
692529
692539-002
Cap
Solder
Solder
6
909532/ 909-449
Body
7
11-0595 (082xxx-001)
57-61
8
9
082xxx-001
0042xx
Ag-Cu Sn Plated (687xxx-001)
Element –
Cu99.9MSn(082xxx)
Tin plated Wire
10
11
12
12
648118
648901
195116
087355
Yarn – GLZZXXX-6481XX
Yarn
Flux_Chlorinated
Glue
72-78
79-85
86-98
99-102
13
091250/ 091251
Sand
103-109
1
Raw Material Description
Page(s)
Overcap
3-6
Cap
7-10
11-17
18-22
23-27
28-56
Rating(s)
All Amps
2
62-65
66-71
0.125-0.8Amps &
1-6.3Amps
8,10-16, 20 &
25Amps
0.125-0.8Amps
1-25Amps
0.125-0.8Amps/
1-25Amps
0.125-0.250/
4-12Amps
0.315-0.8, 15, 16,
20 & 25Amps
1-3.15Amps
0.125 &
0.160Amps
0.2-0.8Amps
0.2-0.8Amps
0.125-0.8Amps
0.125 & 0.160,
0.5-0.8Amps/
1-25Amps
AOV"BPFS,U
TESTREPORT
R02
NO.:4002R12100802+1
Dare:ocr.10,2012
Customer:SuzhouFuHongElectronjc
InduslrialCo.,
Lld.
XIANGCHENG
DlsTRlCT,
SUZHOU,
CHINA
Addres!:NO.89WEIDUROAD,WANGTINGTOWN,
to
be
Reporton ths submitreds.mplesald
S.mplename:CoppeJ,shell
Mod€h/
Item/LoiNo.:/
Metarlal:/,
Buyer: / ,
Suppli€r:/
Samplorecaivsdd.te: Ocl.08.2012
1o'O4r'10,
2012
Testinsperiod:Ffomoct os,20!€
'\l
'
. . ,,
E9S!.s-Ecs!ed9!f
samplein
Chrcmium
contentin thesubmitled
& Hexavalent
As specifiedby dient, to determineihe Lead,cadmlun, Mercury
accordancewith Dircctive2002/95/EC{RoHS).
Ec!!!s-ee$9!.:
instrumeni I\4QL
Measunng
Testingltem
(cd)
Cadmium
(Hg)
[4ercury
IEC62321:2008,s€ction9
|EC62321:
2008,seclionI
7
lEc 623212008,seclron
Chromum(Cr\rl)
IEC623212008AnnexB
Lead(Pb)
ICP€ES
2-'nglkg
ICP-OES
2 mg/kg
tcP-oEs
2 mg/kg
0.02m9/k9'
Ieq
r 0.02mg/kgreE|sto theMQLofsampleextfaction
liquid
SsElcge!:
Decision
ol 18 Aug 2005
of commission
-whentesledas speci{i€d
withthe requirements
samplecomplied
the submitted
2005/618/Ec
noiiliedunderdocument
2002/95/Ec
Directjve
amending
ILS,PLEASEREFERTOTHE FOLLOWNGPAGE(S)***
signedlor andon behalfof
Brcncn
Co.,Ltd,Kunshan
Technology
Shenzhen
AOVTesling
We-r k] n
**n*"oor,
/blfil
caeateaaer:
LiTingting,Maggie
ooo,',*or44.
Ylan Qi, lrickey
Chemic€lTestDirecror
S I t E N 2 H E NA O V T f S I I N G T € C H N O I , O 6 YC O . , I " T O . K U N S N ABNR A N C T I
,
/// \ Noll ne
Ja,t 7tt) 9€'t'o
AOV'*F#S,[
TESTREPORT
NO.:4002R121008024-1
R02
Oate:Od.10,2012
1. To Determiney'.ead,
C€dmium
Contenli(Metalsubslrate)
I*redby (y'a04*
Weighihe sampleinto
Add ihe digestionsolulionithe
vesselis heatedunlilthe sample
AddHrOruntilthe
sampleis clear
nlter;washed
and
Cooling
thevess€|,
Rlled
wat€r.
10themarkwithdistill€d
To Dete
sulit€le)
Content i|retb.r
. \ .
The sampleis digestedin the
Weighihe sample
microwaveovenfollowinga specific
decomposrlonprogram
Tested
by lcP-oES
Coolingthe vessel,tiltei washedand
filledlothe maiKwilh dislilledwater.
ChromiumContenl(boiling-wat€F€xtlaclion):([4etalEubstrate)
Takethe (50i5) cm,
samplein the beaker.
Heat50 mLof Olwaterin
thebe6ker
to boilingfor 1o
F;;1.-
lhe sample,
andcool
Remove
thebeak€rto roomtemperature,
anddo thecolorreaction
Testthe samplesolutionand lhe 0.02
ng/kg standardsolltion by uv-vls.
BSANCH
lCCINOLOGYCO.,LTD.KUNSIIAN
SH€NZH€NAOVTESTITIG
(:
Hotlrne
'tL)0700 8600
nov'Bpf,F,il
TESTREPORT
NO.:
4002R121008024-1R02
Daie:Ocl.10,
2012
5. TooetemineHexavalenl
Chromium
Contonlin colorlessand coloredchromatecoatingon metats:iPtating)
_
.. -i\
: va'hu't'
lfthe lest resultis positive,
the sample is consideredto
havehexavalent
chmmium
Place
1-5
Boiling- water- extraotion
procedu€shallbe usedto
and the 0.02 mg/kg
lflhee is interference
or it is hardto decide
whetherlhesamplehavelhe hexavalent
5.2Boiling-wateF
enradion
Remove
thesample,
andcool
thebeaker
lo roomtemperalure,
anddolhe colorreaction
Heat50 mlof Dlwaier in the
samplein thebeaker.
beakerto boilingfor 10 min
Testtnesamplesolution
andlhe0.02
mg/kgstandadsolulion
by UV-VIS.
SampleDelcriptlon:
Code
1-1
SampleDescndion
Substrate
Plating
Te3tR63ulb:
Unit
RoHSLimit
Lead(Pb)
msfts
1000
N.D.
10
(Cd)
Cadmium
Merorry(Hg)
mg/K9
N.D.
ms/Kg
100
1000
N.D,
N.O.
N.D.
Chromium
{Crl,ll)
m9/kg
1000
Negative
Negative
s8€NZh€N AOVT€SrtNGTECHNOlOSYCO,,tTD,TUNSHAI!
ARANCH
,.r
Ho t l i ne
.100700B6a0
nov'F"Ff"qn
TESTREPORT
No.:A002R1210o602:L1
R02
-ThenewRoHSdircclive
2011/6tEU,on Jul.21,2011comeintoforc€,onJan.03,2013lheformalimplementation,
Direclive
2002r'95/EC
simultaneously.
ahallbe repealed
Sp€cimens,
whichr€Slested
lo detemineLead,Cadmium
havebeendissolved
andMercury
Content,
completely,
-mg/kg=ppm ,
-N.D.=not
i",,,,,,
( The iested sample
resultis uncertain
or
neoatve.,
-"The te8t is bas€d on lhe followins d!!{mplifi:
maybe cannot stand lor the physical lrdh 6t s€r
Coppershell
SH€NZII
AFANCH
AOVTIST|n|GTECHNOIOCVCO.,ITD.KUNSHAN
Ho t l i ne
400 /00 8600
a
GTI#,ffiffi,H
TestReport
ageI of4
ReportNo. RLSZE0o1492l00002
Applicart
Address
CO.'LTD
DONGGUANCITY XNHAI METALPRODUCTS
'ST
COMMUI"IIry
I
WEIMING ROAD HENGZENGAV.XINAN
TOWN DONGGUANCITY GUANGDONGPROVINCE
GAN
by/onthe
The following samplqs) and samPleinformttion wavwere submitt€drnd id
behaHof the client
BASEOFCAP
SampleName
BRASSH65
Materidl
SampleReceivedDate Nov.16,2012
Nov. 16,2012to Nov. 19,2012
TestingPeriod
As specifiedby client,to testLead(Pb),Cadrnium(Cd),
T€st Requ€st€d
Hexavalent Chromium(Cr(Vl)) in the submitted sample(s).
T€st Method
Ed.l Sec.9
IEC62121:2008
IEC612r:2008Ed.l S€.9
Ed.t Sec-7
IEc 62321:2008
Ed.l AnnexB
IEC62121:2C108
Pleasereferio the following page(s).
Test Result(s)
Di.d
!y
picL L
Ddc
Appt@dR
$6i.d
Cdlldi€Iffi
Nov. 19,
No. I 033098
ttu4!.
(S*)Co-Lrt
cottonNlol{
c!!rnE rEslrNgINrEtNAlloNAl
comot.r4lc6ti D755,33tSii'ra
lc
Rcvicr€d by
Eofi,li LinNlti{ Zfla BD'a ru Dntrrt
cdmplsrn1E ft sll- .orip s ll@cx'e
Glnfdd&Chil
@4 0 0 - 0 7 8 E . 3 ! 3
ftn
I F_}'H.mryl
GTI
TestRePort
Page2 of4
ReportNo. R1S2E001492100002
T€rr R€rrlt(sl
Testedltem(s)
Lead(Pb)
Cadmium(Cd)
Mercury(Hg)
Chromium(cr(v l))
Hexavalent
TestedSample/PartD€scriptioD
Note:
Result
13 mgllg
N.D.
N.D,
Negative
Metalbase
totally testedfor Lead,Cadmium'
ry.
The samplehad bdendi,csolved
=
-MDL MethodDetectionLinit
-N.D. = Not Detected(<MDL )
-mg/kg= pptn= PartsPermillion
in
boiling
-Negative= Abs€nceofC(VD , the detectedC(VI) concentration
samplesurface a used.
extractionsolutionis lessthan0 02 mg/kgwith 5ocm'?
cl{ra[ trt t T t t a Gr N l a l N A l l o l l A l c o l P o l a l l o l
I cal] 0755.331t81700 corpls'nl E mtrl con! r'ilG)cl ced cr)ri
0 0 , 6 7t 8 - 3 3 l
E-fla FJrE.',{e'r
':.
o
GTIF_i,H"m,m
TestReport
ReportNo RIS2E001492100002
Page3 of4
Test Process
1. Lmd(Pb),Cadmiun(cd)
2, Mercury(Hg)
Weigh saraple ed place it m a
microwave digE'stionves sel
Chromiun(C(Vl))
3. Hexavalent
Sdecl a test sallplc
m.aswing about 50t5cnf
AElyred
ty UV-V1s
cottolallofl
ctuTtt t!st| o rNlElrlaltoNAL
.4mcirrrtt.l' ren c'n
E_m6r
0755-!36S:7i0 Compi:r.r
conormLnrcrll
@.iif;".,,,
a
GTI#,mffi,^)#
TestReport
ReportNo. RLS2E001492100002
Pag. 4 of 4
Photo(s)of the sample(s)
*** End of rcport***
Thetestaeportis effectiveonly with bothsignatueandsp€cializedstamp.Theresult(s shownin this
report refer only to the sarnple(s)tested.Without written approvalof CTI, this
can't be
reDroduced
exceDtin full.
c c N l a E t a i r | N G t N l E R N A l t o l t Acl o l t o l ^ r i o N
n l- r 3 r l c o n p i a' u r d c I N e nc o m
C o m o r a rcnar r r0 7 5 5 - 3 3 6 8 1 1 0 0 C o m p l s r E
E nra,, .,'ii,.
i.fliLd
O;';;,;",,,.,,
a
GTI#,HMJ"M
TestReport
ReportNo. RLSZE001492I0O00I
PageI of3
DONGGUANCITY XINHAI METAL PRODUCTSCO.,LD
I 'ST WEIMING ROAD HENGZENGAV.XINAN COMMLINITY
TOWN DONGGUANCITY CUANGDONGPROVINCE
Applicant
Address
by/on the
The following samplqs) and sampleinformatiotr was/weresubmittedand
behalfof the client
SILVERCOLORPLATINGOF CAP
SampleName
El€ctrolyticNickel
Material
SampleReceivedDate Nov.16;2012
Nov. 16,2012to Nov. 19,2012
TestingPeriod
As specifledby client,to testLead(Pb),Cadmium(cd),
T€st Requested
HexavalentChrcmium(Cr(Vl)) in the subrnittedsample(s).
Test Mothod
T€st Itein(s)
Ed.t
Ref€rto IEc 62321:2008
Ed.l
R€ferto IEc 62321:2008
Refe.to IEC62321
:2008Ed.I
IEC62321:2008
Ed.l AnnexB
Pleasereferto thefollowing page(s).
T€stResul(s)
elc
lliod
Rrvi.&dby
by
teic.l
Cd!f!di!
I@bd
Nov. 19,
D&
4rt ov.dty
(Sedd
No. I 1033098
ltu|gr.
Co-bf
Ea8wdbtil
Zoc Bs'-
Cu-fiL.& 6na
ToDitti:t'
cotPol^lloll
cItlrE ra5TrN6,NlEtNArroNl!
codpLi hr cari 0 7 55-l3li I I / i)0
c ompldril E-fi3r1I cohpia rl@cl' ce.l .ofr
E 03
!{4?.r
rcfl in n
a
.a00.6tt6-!ll
o
GTIlt.)m.ffiirm
TestReport
Page2 of3
ReportNo. RLSzE001492l0000l
Test€dSample/Prrt Desc ption
Not€:
silvery plating
The wasb€dplrtirg had beondissolv€dtotally test€dfor Lead,
Mercury.
-MDL = MethodDetectionLimit
-N.D. = Not Detected(<MDL )
-mg/kg: pprn= partspermillion
-Negative= Absenceof C(VI) , thedetectedC(VI) concenbation
in
boilingwater
used.
extmctionsolutionis lesslhan0.02mg,&gwith 50cm2sarnplesurface
Test Process
l.
Lead(Pb),Crdmium(Cd)' Mercury(Hg)
Selecl a lesl sample
'n.asurmg aboul 50c!rf
2. Il€xaval€ntChrornium(C(VD)
Selecl a !€st samplc
mlasuring aboui 50t5ctrf
A)alyr.d by UV-VIS
c I f { r R l T E s l t r Gr N T l l N A l r O N A lC O I P O R A T I O f i
r ^m
l a r lc a m !r . l l . l d , c e n . o t
c r l l 0 7 5 53 3 6 8 1 7 0 0 C o m p L EE
Complsrn
E-nn mio@q' r:.n ..n
@4 0 0 - r 1 3 !! 1 3
o
GTI#-),m.ffi^'Y!
TestReport
ReportNo. RLSZE00I492I00001
P€e3of3
Photo(s)ofthe sample(s)
+** End of repon***
Thet€strcport is elfectiveonty with bothsignatureandspecializedstamp.The
report ref€r only to the samplds) test€d.Witlod witten apProvalof CTl, this
reorcducedexceotin full.
cot?olAIloN
ct,{nt f tlfltG rNIElr{ArrotrAt
canro aLnlcair !f55-3308r fao
lompla'nl E m$l coc'piii rlrc].l' ce1l c.rr
shownin this
can't be
,a
a00-6188.133
T€stReport
No.SHAEC1216714738
Page1 ol5
Date:25 Sep 2012
CO.,LTD
MATERIAL
SOLDERING&BRAZING
ASIAGENERAL
ZHEJIANG
CHINA
PROVINCE'
CIry' ZHEJIANG,
HANGZHOU
PARK,SANDUN,
XIHUINDUSTRIAL
SoLDER
The following 6ample(s)was/were submittedand identifiedon behalf of the clients as : LEAD-FREE
WIRE
Dateof Sampl€Received:
TestingPeriod:
TestR€quested:
- SH
sP12-028285
YTW2O6
sno.3Ag0.7ouce
21 Sep2012
21 s,ep2012- 25 SeP2012
Selectedtest(s)as requestedby client
TestMethod:
Pleasereferto nextPage(s)
T€stResulb:
:
Condusion
Pleasereferto nextPage(s).
Baa€don the perfomedtestson submittedsamples'the resultsof Lead'
(PBB)'
biphenyls
chomium,Polybrorninated
Hexavalent
I\rercury,
Cadmium,
RoHS
by
limits
as
set
with
the
diphenylethe6 (PBDE)comply
Polybrominated
200295/EC
Annexll; recasting
2011/65/EU
Di.ective
SGSJobNo.:
PartNo.(PN) :
Compositlon:
Signed for and on b€half of
scs-csTc Ltd.
/Qv''
.n#ffiffi
Fan Jingiie,JJ
Approved Signatory
irmr
r* u-ra
-td *vot
tirtDafi$EE|ihtltrorr
il.t.|.*f,Ertr€€.lt$l
rmrr.t.t t*
zxtao
ll@3
tErEl@llitldt6!E{ti"clt06t'9
Kr(,-tt)Eaffi
xr.c+rti el
iLnlirotllt
ffior*ofr
1j!ltorSOSOtbt4 (aGS8A)
T€6tReport
No.SHAEC1216714734
Date:25 Sep2012
Page2 o15
TestResults:
;
TestPertDe€criotion
S@rn6n No,
1
D6ctiptioi
SGSSampl€lD
wire
SHA12-167147.035Silvery
Rgmarks:
(1)1 mg/kg=I PPm=00001%
Limit
(2)MDL= MethodDeteclion
(3) ND = NotD€teded( < lrDL )
(4) '-' = NotRegulated
RoHSDllBdivs201l/85/EU
Test Llethod
with referenceto lEc 62321:2008
(1)Determination
of cadmiumby ICP-oEs.
(2) Dete.mination
of Leadby ICP-oEs
(3) Determination
of Mercrlryby ICP-OES.
(4) Determination
Chromiumby Spottest/ Colorimetricl\,ethodusingUV-Vis
of Hexavalent
(5)Detemination
by GC-[IS.
PBBS
i
PBoES
of
Limit
100
1000
1000
Test ltem{s)
Cadmium(Cd)
Lead (Pb)
Mercuryfig)
HexavalentChromium(Ci(VD)
UlE
mdkg
ms/kg
ms/kS
mS.ftS
mS/kS
mdkg
mdkS
mSikS
mdks
ms/kg
mg/kg
mdkS
msikg
mdks
mgftS
mg/KS
1000
-
Sumof PBBS
Monobromobiphenyl
Dibromobiphenyl
Tribromobiph€nyl
Tetrabrornobiphenyl
PentabromobiPhenYl
He/€bromobiphenyl
HeptabromobiPhenyl
Octabromobiphenyl
NonabromobiPhenyl
DecabromobiPhenYl
SumoI PBDES
ether
Monobromodiphenyl
1m0
-
5
5
s
5
5
5
5
5
5
5
5
ND
50
ND
N€gative
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ffi
ffiffi:ffi
g"fff
###f
rffi
!#,g;"EHT*
*,Hffi
ffi Stift
Ufi
*lvl*sm.1m*ts""nr*
#ffi*,rx*$'#'ffi
Ij*tffi
b D.r. na co{d6
;;bii*hEni-.6fr
l\rDL
2
2
2
o
Sffi*ff
d tbtk
*r I
r6tr.{.)r-H
tt-ErrlFYasft.cxd|lt.9|dlcrn
+l -l|.*tr[lt|fte||6+l
zfrlr3
lr:2@
tElEF{lF6tl
rd€6+1)6r.@
Hit!-2l164@raa it{&aFl@
(8cgs )
lr.nD.t o1$.8GgOrouP
Tes{Report
No. SHAEC1216714738
Test ltem(s)
Dibromodiphenylether
Tribromodiphenyl
ether
Tetrabromodiphenyl
ether
Pentabromodiphenyl
elher
Hexabromodiphenyl
ether
Heptabromodiphenyl
ether
Oc-tabromodiphenyl
ether
Nonabro.nodiphenyl
ether
D€cabromodiphenyl
ether
thi!
Date:25Sep2012
UdT
MDt
mdkS
mdkS
mdkS
mdkg
mS/kg
mSikS
mg/kg
mS/kS
mgkg
5
5
5
5
5
5
5
5
5
Page3 of 5
@
ND
ND
ND
NO
ND
ND
ND
ND
ND
Notes :
(1) The maximumpermissiblelimitis quotedfromdiredive2011/65/EU,
Annexll
(2) ospot{est:
Negative = Absence of Cr(Vl) coating, Positive= Presenceof Cr(Vl) coating;
CIhe tested sample should be fudher verifed by boiling-waterextractionmethodif the spot test result
is Negative or cannot be confirmed.)
oBoiling-wateFextraction:
Negative = Ahsence of Cr(Vl) coating
Positive = Pesence of Cr(Vl) coating;the detectedconcentrationin boiling-water-ext€ctionsolution is
equal or greater than 0.02 mgl(q with 50 cm'zsample surtace area.
For corrosion protectioncoatingson metals: Informationon storage conditionsand producliondate of
the tested sample is unavailableand thus results of Cr(Vl) representstatus of lhe sample at the time
of testing.
t'ilt,b.aYrbto
+1
drchrbrd,Swaon
!e3a
I ErE{O-Zr)OtrOO
raEFaFffiTl
*FA)ala@!.a |{j{l.?J)6r@
M.m!.rorh.scsGtuc(acgs
)
TestReport
No.SHAEC1216714734
Page 4 of 5
Date:25 S€p2012
ATTACHMENTS
RoHSTe€tingFlowChart
xu
Xiao/Gary
Wang/Allen
JanShi/Yoyo
1) Nameof the personwhomadetesting:
Xu/LindaLi
'
2i Nameof thebersonin chargeof testing:JeffZhang/George
chart.(Cf
to berowflow
accorcting
6'ypre-condit-roningherhod
totarry
aissoried
iiiii,"i !!rir!!,i.
testmethodexcluded)
andPBBdPBDES
SamplePrcparation
SampleMeasurement
Pbrcd,Hg
PB86fPBDE8
Acid digestionwith
microw€ve/hotplate
Concentration/
Dilutionof extraclion
solution
'1)AlkaliFusion/
DryAshing
2) Acidto dissolve
Adding1,s
diphenylcarbazide
for color
development
A red color
indicatesthe
presence
of cP'.
neceas€ry,
confirmwith
tr
'l';-;Ltidbd$rffi'd6.h*lhE.,nrdri*6
tilairl$gYb.rto dErloat4ltrtracnr 20(43
a|lM
fl..tjt.*Iqldl|6els+l
rEtEFzr)0tac53 rE&&4lrsa
l+{a-a)dlqaa rtjF.?1)6@
$6nb.fol th.ao6 GlDlD{8oas )
TestReport
No.SHAECl2'16714738
Date:25 Sep2012
Page5 of 5
Samplephoto:
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TestReport
No. SHAEC1216714749
Date:25 Sep2012
Page1of 5
ZHEJIANG
ASIAGENERAL
SOLDERING&BRAZING
I.iIATERIAL
CO.,LTD
XIHUINDUSTRIAL
PARK,SANDUN,HANGZHOU
CITY,ZHEJIANG,
PROVINCE,
CHINA
The followingsample(s)was/weresubmittedand identifiedon behalfof the clientsas : LEAD-FREESOLDER
WIRE
SGSJobNo.:
PartNo.(P/N):
Composition
:
Dateof SampleReceived:
TestingPeriodI
- SH
sP12-028285
(692535-002)
YTW'102
TestRequestedI
Selecledtest(s)as requestedby client.
Test l\relhod:
Pleasereferto nextpage(s).
Pleas€referto nextpage(s).
Basedon the performedtesb on submitteds€mples,th€ resultsof Lead,
(PBB),
biphenyls
cfiromium,
Polybrominated
Meroiry,Cadmium,
Hexavalent
(PBDE)
withthelimitsas setby RoHS
comply
Polybrominated
diphenylethers
200295/EC.
Annexll; rec€sting
Directive
2011/65/EtJ
Sn2.ocuRE
21 Sep2012
21 Sep2012- 25 Sep2012
T€stResults:
:
Condusion
Signed for and on bohalf of
SGgCSTC Ltd.
.,/1,-
,rt*{'""^
FanJinqjie,JJ
ApprovedSignatory
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(SGssA)
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TastReport
No.SHAECl216714749
Date:25Sep2012
Page2 of 5
TestResulb:
TestPartDescriotion:
Sp6dr|on No.
1
SGSSamplolD
Dgcriptio.l
SHA12-167147.042
Silvery
wire
Rema*s:
(1)1 mg/ks=1 PPm=0.0001%
(2) lrDL = LlethodDeteclionLimit
(3) ND= NotDetected( < IVDL)
(4)'-" = 1o1q*r,","d
RoHSDlrB.dv€2011/55iEU
TestMethod: Withreferenceto IEC62321:2008
(1)Determination
of Cadmium
by ICP-OES.
(2) Determination
of Leadby ICP-OES.
(3) Determin€tion
of l\rercuryby ICP-OES.
(4) Deteminationof Hexavalent
Chromiumby Spottest/ Colorimetric
MethodusingUV-Vis.
(5)Detemination
of PBBS/ PBDES
by GC-[IS.
Testltem(s)
Limit unit
100 msfts
1000 mdkg
Cadmium(Cd)
Lead (Pb)
Merd.iry(Hg)
(C(Vl))
Hexavalent
Chromium
Sumof PBBS
Monobromobiphenyl
Dibromobiphenyl
Tribromobiphenyl
Tetrabromobiphenyl
Penlabromobiphenyl
Hexabmmobiphenyl
Heptabromobiphenyl
Octabromobiphenyl
Nonabromobiphenyl
Decabromobiphenyl
Sumof PBDES
Monobromodiphenyl
ether
,o:o *1*
1000
_
1000
-
mdlQ
ms,/KS
mg/Kg
mg/Kg
mgxs
mg/Kg
ms/Kg
msfts
mg/Kg
mgKg
mgKg
mg/kg
mg/Kg
MDt
2
@2
N
D
2
1
n
2
o
-
N
D
Negative
N
D
5
5
5
5
5
5
5
5
5
5
-
N
N
N
N
N
N
N
N
N
N
N
D
D
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D
D
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D
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D
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TestReport
No.SHAECl2'16714749
T6stltem(s)
Dibromodiphenyl
ether
Tribrcmodiphenyl
elher
Tetrabromodiphenyl
ether
Pentabohodiphenyl
ether
Hexabrcmodiphenyl
ether
Heptabromodiphenyl
ether
Oclabromodiphenyl
ether
Nonabromodiphenyl
ether
Decabromodiphenyl
ether
thi!
Date:25Sep2012
llil
MDt
mg/kS
mg/kg
mSikS
mg/kg
mg/kg
mg/kg
mg/kg
mg/kS
mg/kg
5
5
5
5
5
5
5
5
5
Page3 of 5
g2
ND
ND
ND
ND
ND
ND
ND
ND
ND
Notes :
(1) The maximumpermissible
limitis quotedfromdiroclive2011/65/EU,
Annexll
(2)
"spot-test:=
Negative Absence of Cr(Vl) coating, Positive= Presenceof Cr(Vl) coatingi
(The tested sample should be further verified by boiling-wateFextractionmethod if the spot test result
is Negativeor cannot be confirmed.)
oBoiling-wateFext€c{on:
Negative = Abs€nc€ of Cr(Vl) coating
Positive = Presenceof Cr(Vl) coalingt the detectedconcentrationanboiling-water-extractionsolution is
equal or gre€ter than 0.02 mg/kg wilh 50 cm':sample surface area,
For corosion protectioncoatingson melals: Informationon storage conditionsand productiondate of
the tested sample is unavailableand thus results of Cr(Vl) representstatus of the sample at the time
of testing.
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T€€tReport
No.SHAEC121671474S
Date:25 Sep 2012
Page 4 of 5
ATTACHMENTS
RoHSTestingFlowChart
1) Nameof the personwho madetesting:Jan Shi/YoyoWangy'Aen Xiaor'caryXu
2) Nameof the personin chargeof testing:Jeff ZhangJceorge
Xd LindaLi
3) Thesesamples
wereda66olved
totallyby preconditioning
methodaccording
to betowflowchad.(Cf'
andPBBS,/PBDES
testmethodexcluded)
Sample
I\reasurement
Pb/CdrHg
PBB8/PBDEs
Nonmetallic
mateial
Concentration/
Dilution
of extraction
solution
1)AlkaliFusion/
DryAshing
2) Acjdto dissolve
Adding1,5diphenylcabazide
for color
development
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for color
development
A red color
indicates
the
presenceof Cr6'.
necessary,
confirmwith
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Test Repori
No.SHAEC1216714749
Date: 25 Sep 20 12
Page5 of 5
Samplephoto:
sHAl2-167147.042
repodonly
thephotoonoriginal
SGSauthenticate
'"' Endof Reporl"*
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Test Report
Applicant:
Number:
ELSCHUKOM ELEKTROSCHUTZKOMPONENTENBAU
GMBH
GEWERBESTRASSE 87,D-98669 VEILSDORF,
GERMANY
Date:
SHAH0036227401
JAN 18, 2013
Sample Description:
Two(2) pieces of submitted samples said to be :
(1) Mixed all kinds of metal substrates.
(2) Mixed all kinds of plating layers.
Item Name
: Silver Plated & Pure Silver Wires.
Item No.
: (B-1) 101.014 -. ---– silver plated copper wire – Cu, Ag--%
(B-2) 101.0131.---– pure silver wire – Ag 1000
(B-3) 101.0123.0--– silver plated purest nickel wire – Ni99.98%, Ag1%
(B-4) 101.0182.0--– silver-copper alloy plated copper plated iron nickel alloy wire
– ElconD, AgCu5%
(B-5) 101.0120.0--– silver plated constantan wire – CuNi44, Ag5%
(B-6) 101.0151.0--– silver plated copper - nickel 44 alloy wire
– CuNi44, Ag10%
(B-7) 1050--31.-------– pure silver strips – Ag 1000 pure
Country Of Origin
: Germany.
************************************************************************************************************************************************************
Tests Conducted:
As requested by the applicant, for details refer to attached page(s).
************************************************************************************************************************************************************
To Be Continued
Authorized by:
For intertek testing services Ltd., Shanghai
Jacob Lin
General Manager
Page 1 Of 5
Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233
Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
Test Report
Number:
SHAH0036227401
Tests Conducted
(A) Test result of RoHS Directive:
Result
Testing item
(1)
Cadmium (Cd) content (mg/kg)
ND
Lead (Pb) content (mg/kg)
ND
Mercury (Hg) content (mg/kg)
6+
Chromium2(VI)(Cr ) result (by boiling water extraction on metal) (mg/kg
with 50cm )
ND
ND
Result
Testing item
(2)
Cadmium (Cd) content (mg/kg) /Plating
ND
Lead (Pb) content (mg/kg) /Plating
ND
Mercury (Hg) content (mg/kg) /Plating
ND
6+
Chromium2(VI)(Cr ) result (by boiling water extraction on metal) (mg/kg
with 50cm ) /Plating
ND
2
Remark:mg/kg with 50cm = milligram per kilogram with 50 square centimeter
ND = not detected
(B) RoHS Requirement:
Restricted substances
Cadmium (Cd)
Lead (Pb)
Mercury (Hg)
6+
Chromium (VI) (Cr )
Limits
0.01% (100 mg/kg)
0.1% (1000 mg/kg)
0.1% (1000 mg/kg)
0.1% (1000 mg/kg)
The above limits were quoted from RoHS Directive 2011/65/EU for homogeneous material.
(C) Test method:
Testing item
Cadmium (Cd) content
Lead (Pb) content
Mercury (Hg) content
6+
Chromium (VI) (Cr ) content (for
metal)
Testing method
With reference to IEC 62321 Edition 1.0: 2008, by acid
digestion until the tested sample was totally dissolved, and
determined by ICP-OES.
With reference to IEC 62321 Edition 1.0: 2008, by acid
digestion until the tested sample was totally dissolved, and
determined by ICP-OES.
With reference to IEC 62321 Edition 1.0: 2008, by acid
digestion until the tested sample was totally dissolved, and
determined by ICP-OES.
With reference to IEC 62321 Edition 1.0: 2008, by boiling
water extraction and determined by UV-VIS
Spectrophotometer.
Reporting limit
2 mg/kg
2 mg/kg
2 mg/kg
2
0.02mg/kg with 50cm
(in testing solution)
Date sample received: Jan.14, 2013
Testing period: Jan.14, 2013 To Jan.17, 2013
************************************************************************************************************************************************************
To Be Continued
Page 2 Of 5
Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233
Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
Test Report
Number:
SHAH0036227401
Tests Conducted
(D) Measurement flowchart:
Test for Cd/Pb/Hg/Cr (VI)/PBBs/PBDEs contents
Reference standard: IEC 62321 Edition 1.0: 2008
Sampling/grinding or cutting
Cr
Cd/Pb/Hg
Metal
Weigh sample and for
different material, digest
the sample with
*1
appropriate acid
Positive
No
Confirm the tested
samples are totally
dissolved
Yes
Polymers /
electronics
PBBs/PBDEs
Weigh sample
and add alkaline
solution
Spot test
Get 50cm
samples
6+
Weigh sample and
add organic
solvent
*2
Definite temp.
Extraction
2
Boiling water
extraction
Soxhlet extraction
or
Solvent extraction
Cool and filter the
extract
Concentrate the
extract and make
up with organic
solvent
Make up with
deionized water
Analyzed by ICP-OES
Make up with deionized water
and add diphenyl-carbazide
solution
Analyzed by GC-MSD
Analyzed by UV-VIS
Remarks:
*1: list of appropriate acid:
Material
Polymers
Metals
Electronics
Acid added for digestion
HNO3,HCL,HF,H2O2,H3BO3
HNO3,HCL,HF
HNO3,HCL,H2O2,HBF4
*2: If the result of spot test is positive, Chromium VI would be determined as detected.
************************************************************************************************************************************************************
To Be Continued
Page 3 Of 5
Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233
Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
Test Report
Number:
SHAH0036227401
Tests Conducted
************************************************************************************************************************************************************
To Be Continued
Page 4 Of 5
Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233
Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
Test Report
Number:
SHAH0036227401
Tests Conducted
************************************************************************************************************************************************************
End Of Report
This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a recommendation for any particular
course of action. Intertek does not accept a duty of care or any other responsibility to any person other than the Client in respect of this report and only accepts liability
to the Client insofar as is expressly contained in the terms and conditions governing Intertek's provision of services to you. Intertek makes no warranties or
representations either express or implied with respect to this report save as provided for in those terms and conditions. We have aimed to conduct the Review on a
diligent and careful basis and we do not accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by statute or otherwise,
except in the event of our gross negligence or wilful misconduct.
Page 5 Of 5
Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233
Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
Test Report
Applicant:
Number:
LITTELFUSE,INC.
800 E. NORTHWEST HWY
A.DIVIETRO/D.UNTIEDT
Attn:
Date:
SHAH00361401
JAN 16, 2013
Sample Description:
One (1) submitted sample said to be Grey Wire.
Item Name
: Wire Tin Plated Cu.
Part No.
: Element.
************************************************************************************************************************************************************
Tests Conducted:
As requested by the applicant, for details refer to attached page(s).
************************************************************************************************************************************************************
To be continued
Authorized by:
For intertek testing services Ltd., Shanghai
Jacob Lin
General Manager
Page 1 Of 4
Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233
Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
Test Report
SHAH00361401
Number:
Tests Conducted
(Ⅰ) Test Result Summary:
Result (ppm)
(1)
Testing Item
Heavy Metal
Cadmium (Cd) content
Lead (Pb) content
Mercury (Hg) content
6+
2
Chromium VI (Cr ) content (mg/kg With 50cm )
ND
ND
ND
Negative (< 0.02)
Testing Item
Result (ppm)
(2)
Heavy Metal
Cadmium (Cd) content / Plating
Lead (Pb) content / Plating
Mercury (Hg) content / Plating
6+
2
Chromium VI (Cr ) content (mg/kg With 50cm ) / Plating
ND
60
ND
Negative (< 0.02)
Remarks: ppm = parts per million = mg/kg
ND = not detected
2
@ = Due to the insufficient sample area, reduced total sample surface of 10 cm was used and the dilution factor
was adjusted
accordingly.
2
mg/kg with 50cm = milligram per kilogram with 50 square centimetre
Tested components:
(1)Substrate.
(2)Plating.
Responsibility of Chemist: Dent Fang / Ken He
(Ⅱ) RoHS Requirement:
Restricted substances
Cadmium (Cd) Content
Lead (Pb) Content
Mercury (Hg) Content
6+
Chromium VI (Cr ) Content
Polybrominated Biphenyls (PBBs)
Polybrominated Diphenyl Ethers (PBDEs)
Limits
0.01% (100ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
The above limits were quoted from RoHS Directive 2011/65/EU for homogeneous material.
(Ⅲ) Test Method:
Testing item
Cadmium (Cd) content
Lead (Pb) content
Mercury (Hg) content
6+
Chromium VI (Cr ) content
Testing method
With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by
microwave digestion until the tested samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by
microwave digestion until the tested samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition 1.0:2008 in clause 7, by microwave
digestion until the tested samples are totally dissolved and determined
by ICP-OES.
With reference to IEC 62321 edition 1.0:2008 in Annex B, by boiling
water extraction and determined by UV-VIS Spectrophotometer.
Reporting limit
2 ppm
2 ppm
2 ppm
0.02
2
mg/kg with 50cm
Remark:Reporting limit = Quantitation limit of analyze in sample
Date Sample Received:Jan.9, 2013
Testing Period:Jan.9, 2013 to Jan.14, 2013
************************************************************************************************************************************************************
To be continued
Page 2 Of 4
Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233
Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
Test Report
Number:
SHAH00361401
Tests Conducted
(Ⅳ) MEASUREMENT FLOWCHART:
Test for Cd/ Pb/ Hg/Cr (VI)/ PBBs/PBDEs contents
Reference standard: IEC 62321 edition 1.0:2008
Sampling/grinding or cutting
Cr
Cd/Pb/Hg
Metal
Weigh sample and for
different material,
digest the sample with
*1
appropriate acid
No
Get 50cm
samples
Yes
Weigh sample and
add organic
solvent
*2
Soxhlet extraction
or
Solvent extraction
Cool and filter the
extract
Make up with deionized
water and add Diphenylcarbazide solution
Analyzed by ICP-OES
PBBs/PBDEs
Definite temp.
Extraction
2
Boiling water
extraction
Make up with
deionized water
Polymers /
electronics
Weigh sample
and add alkaline
solution
Spot test
Negative
Confirm the tested
samples are totally
dissolved
6+
Concentrate the
extract and make
up with organic
solvent
Analyzed by GC-MSD
Analyzed by UV-VIS
REMARKS:
*1: LIST OF APPROPRIATE ACID:
MATERIAL
Polymers
Metals
Electronics
ACID ADDED FOR DIGESTION
HNO3,HCl,HF,H2O2,H3BO3
HNO3,HCL,HF
HNO3,HCL,H2O2,HBF4
*2: IF THE RESULT OF SPOT TEST IS POSITIVE, CHROMIUM (VI) WOULD BE DETERMINED AS DETECTED.
************************************************************************************************************************************************************
To be continued
Page 3 Of 4
Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233
Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
Test Report
Number:
SHAH00361401
Tests Conducted
***********************************************************************************************************************************************************
End of report
This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a recommendation for any particular
course of action. Intertek does not accept a duty of care or any other responsibility to any person other than the Client in respect of this report and only accepts liability
to the Client insofar as is expressly contained in the terms and conditions governing Intertek's provision of services to you. Intertek makes no warranties or
representations either express or implied with respect to this report save as provided for in those terms and conditions. We have aimed to conduct the Review on a
diligent and careful basis and we do not accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by statute or otherwise,
except in the event of our gross negligence or wilful misconduct.
Page 4 Of 4
Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233
Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
Number : TWNC00294415
Test Report
Applicant:
Littelfuse Philippines Inc.
LIMA Technology Center, Lipa City,
Malvar, Batangas
Date
: Jan 17, 2013
Sample Description:
One (1) group of submitted samples said to be :
Part Description
: Tin plated Elcon Wire Element
Part Number
: 0042xx/ 0063x
Date Sample Received
: Jan 11, 2013
Date Test Started
: Jan 11, 2013
Test Conducted :
As requested by the applicant, for details please refer to attached pages.
Authorized by:
On Behalf of Intertek Testing Services
Taiwan Limited
K. Y. Liang
Director
*THJ0294415*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C.
全國公證檢驗股份有限公司
11492 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410
Page 1 of 6
Number : TWNC00294415
Test Conducted
(Ⅰ) Test Result Summary:
Test Item
Unit
Result
Test Method
RL
(1)
(2)
ND
ND
2
ND
248
2
ND
ND
2
Negative
Negative
0.02
Heavy Metal
Cadmium (Cd) content
ppm
Lead (Pb) content
ppm
Mercury (Hg) content
ppm
Chromium VI (Cr6+) content
Remarks:
mg/kg
with
50 cm2
With reference to IEC
62321: 2008, by
microwave digestion and
determined by ICP-OES.
With reference to IEC
62321: 2008, by
microwave digestion and
determined by ICP-OES.
With reference to IEC
62321: 2008, by
microwave digestion and
determined by ICP-OES.
With reference to IEC
62321: 2008, by boiling
water extraction and
determined by UV-Vis
Spectrophotometer.
ppm = parts per million based on weight of tested sample = mg/kg
ND
= Not detected
RL
= Reporting Limit, Quantitation limit of analyte in sample
mg/kg with 50cm2 = milligram per kilogram with 50 square centimeter
Negative = A negative test result indicated positive observation was not
found at the time of Test. When the spot test showed a negative
result, the boiling water extraction procedure shall be used to
verify the result.
Tested Components
(1) Coppery metal wire base material
(2) Silvery plating layer
Responsibility of Chemist:
Date Sample Received
Test Period
Kevin Liu/ Irene Chiou
: Jan 11, 2013
: Jan 11, 2013 To Jan 15, 2013
*THJ0294415*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C.
全國公證檢驗股份有限公司
11492 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410
Page 2 of 6
Number : TWNC00294415
Test Conducted
(Ⅱ) RoHS Limits:
Restricted Substances
Limits
Cadmium (Cd) content
Lead (Pb) content
Mercury (Hg) content
Chromium VI (Cr6+) content
0.01% (100ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
The above limits were quoted from Annex II of 2011/65/EU for homogeneous material.
*THJ0294415*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C.
全國公證檢驗股份有限公司
11492 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410
Page 3 of 6
Number : TWNC00294415
Test Conducted
(Ⅲ) Measurement Flowchart:
Test For Cd/Pb/Hg/Chromium (VI)
Reference Standard:IEC 62321 edition 1.0:2008
Sample preparation
Take sample and immerse into Aqua Regia, start to strip plating layer
Stop the stripping procedure upon color change completely
Take the Aqua solution as plating component and stripped body as substrate component
Cd/Pb/Hg
Substrate
For different
material, digest
the sample with
*1
appropriate acid
Cr
6+
By spot test
Confirm the tested
samples are
totally dissolved
Make up with
deionized water
Plating
Negative
*2
Get 50cm2 sample
By boiling water
extraction
Analyzed by ICP-OES
Make up with deionized water and add
diphenyl-carbazide solution
Analyzed by UV-VIS
*THJ0294415*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C.
全國公證檢驗股份有限公司
11492 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410
Page 4 of 6
Number : TWNC00294415
Test Conducted
Remarks:
*1: List Of Appropriate Acid:
Material
Polymers
Metals
Electronics
Acid Added For Digestion
HNO3,HCl,HF,H2O2,H3BO3
HNO3,HCl,HF
HNO3,HCl,H2O2,HBF4
*2: If the result of spot test is positive, Chromium VI would be determined as detected.
End of Report
This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a
recommendation for any particular course of action. Intertek does not accept a duty of care or any other responsibility to any person other than
the Client in respect of this report and only accepts liability to the Client insofar as is expressly contained in the terms and conditions
governing Intertek's provision of services to you. Intertek makes no warranties or representations either express or implied with respect to this
report save as provided for in those terms and conditions. We have aimed to conduct the Review on a diligent and careful basis and we do not
accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by statute or otherwise, except in
the event of our gross negligence or wilful misconduct.
*THJ0294415*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C.
全國公證檢驗股份有限公司
11492 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410
Page 5 of 6
Number : TWNC00294415
Test Conducted
Photo
*THJ0294415*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C.
全國公證檢驗股份有限公司
11492 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410
Page 6 of 6
Test Report
Applicant:
Number : TWNC00286464
Littelfuse Philippines Inc.
LIMA Technology Center, Lipa City,
Malvar, Batangas
Date
: Nov 22, 2012
Sample Description:
One (1) group of submitted samples said to be :
Part Description
: Yarn
Part Number
: 648118_648119_648120 (6481xxx_GLZZxxx)
Date Sample Received
: Nov 15, 2012
Date Test Started
: Nov 16, 2012
Test Conducted :
As requested by the applicant, for details please refer to attached pages.
Authorized By:
On Behalf Of Intertek Testing Services
Taiwan Limited
K. Y. Liang
Director
*THJ0286464*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410
Page 1 of 7
Number : TWNC00286464
Test Conducted
(Ⅰ) Test Result Summary :
Result (ppm)
White Yarn
Test Item
Heavy Metal
Cadmium (Cd) content
Lead (Pb) content
Mercury (Hg) content
Chromium VI (Cr6+) content
Polybrominated Biphenyls (PBBs)
Monobrominated Biphenyls (MonoBB)
Dibrominated Biphenyls (DiBB)
Tribrominated Biphenyls (TriBB)
Tetrabrominated Biphenyls (TetraBB)
Pentabrominated Biphenyls (PentaBB)
Hexabrominated Biphenyls (HexaBB)
Heptabrominated Biphenyls (HeptaBB)
Octabrominated Biphenyls (OctaBB)
Nonabrominated Biphenyls (NonaBB)
Decabrominated Biphenyl (DecaBB)
Polybrominated Diphenyl Ethers (PBDEs)
Monobrominated Diphenyl Ethers (MonoBDE)
Dibrominated Diphenyl Ethers (DiBDE)
Tribrominated Diphenyl Ethers (TriBDE)
Tetrabrominated Diphenyl Ethers (TetraBDE)
Pentabrominated Diphenyl Ethers (PentaBDE)
Hexabrominated Diphenyl Ethers (HexaBDE)
Heptabrominated Diphenyl Ethers (HeptaBDE)
Octabrominated Diphenyl Ethers (OctaBDE)
Nonabrominated Diphenyl Ethers (NonaBDE)
Decabrominated Diphenyl Ether (DecaBDE)
Halogen Content
Fluorine (F)
Chlorine (Cl)
Bromine (Br)
Iodine (I)
ND
14
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Remarks: ppm = Parts per million based on weight of tested sample = mg/kg
ND = Not detected
Responsibility of Chemist : Irene Chiou / Kevin Liu / Cathy Chen
Date Sample Received
Test Period
: Nov 15, 2012
: Nov 16, 2012 To Nov 21, 2012
*THJ0286464*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410
Page 2 of 7
Number : TWNC00286464
Test Conducted
(Ⅱ) RoHS Limits:
Restricted Substances
Cadmium (Cd) Content
Lead (Pb) Content
Mercury (Hg) Content
Chromium VI (Cr6+) Content
Polybrominated Biphenyls (PBBs)
Polybrominated Diphenyl Ehters (PBDEs)
Limits
0.01% (100ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
The above limits were quoted from Annex II of 2011/65/EU for homogeneous
material.
(Ⅲ) Test Method:
Test Item
Cadmium (Cd)
content
Lead (Pb) content
Mercury (Hg)
content
Chromium VI (Cr6+)
content
Test Method
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 7, by microwave
digestion until the tested samples
are totally dissolved and determined
by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in annex C, by alkaline
digestion and determined by UV-Vis
spectrophotometer.
Reporting Limit
*THJ0286464*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410
2 ppm
2 ppm
2 ppm
1 ppm
Page 3 of 7
Number : TWNC00286464
Test Conducted
(Ⅲ) Test Method:
Test Item
Polybrominated
Biphenyls (PBBs)
Polybrominated
Diphenyl Ethers
(PBDEs)
Halogen Content
Test Method
With reference to IEC 62321 edition
1.0:2008 in annex A, by solvent
extraction and determined by GC-MS
and further HPLC-DAD confirmation
when necessary.
With reference to IEC 62321 edition
1.0:2008 in annex A, by solvent
extraction and determined by GC-MS
and further HPLC-DAD confirmation
when necessary.
With reference to EN 14582:2007 by
calorimetric bomb with oxygen and
determined by Ion Chromatograph.
Reporting Limit
5 ppm
5 ppm
50 ppm
Remark: Reporting limit = Quantitation limit of analyte in sample
*THJ0286464*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410
Page 4 of 7
Number : TWNC00286464
Test Conducted
(Ⅳ) Measurement Flowchart:
Test for Cd/Pb/Hg/Chromium (VI)/PBBS/PBDES Contents
Reference Standard: IEC 62321 edition 1.0:2008
Sample preparation
For non-metal part
For metal part
Take sample and immerse into Aqua Regia, start to strip plating layer
Stop the stripping procedure upon color change completely
Take the Aqua solution as plating component and stripped body as substrate component
PBBs/PBDEs
Weigh sample and
add organic solvent
By Soxhlet
extraction or
Solvent extraction
Concentrate the
extract and make up
with organic
solvent
Cr
6+
Substrate
Cd/Pb/Hg
Weigh sample
and add
alkaline
solution
For different
material, digest
the sample with
*1
appropriate acid
Plating
Cr
6+
By spot test
Definite temp.
extraction
Cool and filter
the extract
Confirm the tested
samples are
totally dissolved
Negative
Get 50cm2 sample
Make up with
deionized water
By boiling water
extraction
Analyzed by ICP-OES
Analyzed by GC-MSD
Remarks:
*1: List of Appropriate Acid:
Material
Polymers
Metals
Electronics
*2
Make up with deionized
water and add
diphenyl-carbazide
solution
Analyzed by UV-VIS
Acid Added for Digestion
HNO3,HCl,HF,H2O2,H3BO3
HNO3,HCl,HF
HNO3,HCl,H2O2,HBF4
*2: If the result of spot test is positive, Chromium VI would be determined as detected.
*THJ0286464*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410
Page 5 of 7
Number : TWNC00286464
Test Conducted
(Ⅳ) Measurement Flowchart:
Test for Halogen Content
Reference Standard:EN 14582
Sampling/grinding or
cutting
Add absorbent in a
combustion flask &
place weighed sample in
equipment
Fill oxygen into
calorimetric bomb
Ignite then leave the
bomb at room
temperature
Transfer the absorbent
into a volumetric flask
Make up with deionized
water
Analyzed by ion
chromatography
End of Report
This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a
recommendation for any particular course of action. Intertek does not accept a duty of care or any other responsibility to any person other than
the Client in respect of this report and only accepts liability to the Client insofar as is expressly contained in the terms and conditions
governing Intertek's provision of services to you. Intertek makes no warranties or representations either express or implied with respect to this
report save as provided for in those terms and conditions. We have aimed to conduct the Review on a diligent and careful basis and we do not
accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by statute or otherwise, except in
the event of our gross negligence or wilful misconduct.
*THJ0286464*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410
Page 6 of 7
Number : TWNC00286464
Test Conducted
Photo
*THJ0286464*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410
Page 7 of 7
Test Report
Applicant:
Number:
LITTELFUSE,INC.
800 E. NORTHWEST HWY
A.DIVIETRO/D.UNTIEDT
Attn:
Date:
SHAH00361375
JAN 16, 2013
Sample Description:
One(1) submitted sample said to be White Yarn.
Item Name
: Glass Yarn.
Part No.
: 648901.
************************************************************************************************************************************************************
Tests Conducted:
As requested by the applicant, for details refer to attached page(s).
************************************************************************************************************************************************************
To Be Continued
Authorized by:
For intertek testing services Ltd., Shanghai
Jacob Lin
General Manager
Page 1 Of 7
Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233
Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
Test Report
Number:
SHAH00361375
Tests Conducted
1
(Ⅰ) Test Result Summary:
Testing Item
Heavy Metal
Cadmium (Cd) content
Lead (Pb) content
Mercury (Hg) content
6+
Chromium VI (Cr ) content
Polybrominated Biphenyls (PBBs)
Monobrominated Biphenyls (MonoBB)
Dibrominated Biphenyls (DiBB)
Tribrominated Biphenyls (TriBB)
Tetrabrominated Biphenyls (TetraBB)
Pentabrominated Biphenyls (PentaBB)
Hexabrominated Biphenyls (HexaBB)
Heptabrominated Biphenyls (HeptaBB)
Octabrominated Biphenyls (OctaBB)
Nonabrominated Biphenyls (NonaBB)
Decabrominated Biphenyl (DecaBB)
Polybrominated Diphenyl Ethers (PBDEs)
Monobrominated Diphenyl Ethers (MonoBDE)
Dibrominated Diphenyl Ethers (DiBDE)
Tribrominated Diphenyl Ethers (TriBDE)
Tetrabrominated Diphenyl Ethers (TetraBDE)
Pentabrominated Diphenyl Ethers (PentaBDE)
Hexabrominated Diphenyl Ethers (HexaBDE)
Heptabrominated Diphenyl Ethers (HeptaBDE)
Octabrominated Diphenyl Ethers (OctaBDE)
Nonabrominated Diphenyl Ethers (NonaBDE)
Decabrominated Diphenyl Ether (DecaBDE)
Result (ppm)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Remarks:ppm = parts per million = mg/kg
ND = not detected
Responsibility of Chemist: Dent Fang / Leaf Liu
(Ⅱ) RoHS Requirement:
Restricted substances
Cadmium (Cd) Content
Lead (Pb) Content
Mercury (Hg) Content
6+
Chromium VI (Cr ) Content
Polybrominated Biphenyls (PBBs)
Polybrominated Diphenyl Ethers (PBDEs)
Limits
0.01% (100ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
The above limits were quoted from RoHS Directive 2011/65/EU for homogeneous material.
************************************************************************************************************************************************************
To Be Continued
Page 2 Of 7
Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233
Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
Test Report
Number:
SHAH00361375
Tests Conducted
(Ⅲ) Test Method:
Testing item
Cadmium (Cd) content
Lead (Pb) content
Mercury (Hg) content
6+
Chromium VI (Cr ) content
Polybrominated Biphenyls
(PBBs)
Polybrominated Diphenyl
Ethers (PBDEs)
Testing method
With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by
microwave digestion until the tested samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by
microwave digestion until the tested samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition 1.0:2008 in clause 7, by microwave
digestion until the tested samples are totally dissolved and determined
by ICP-OES.
With reference to IEC 62321 edition 1.0:2008 in annex C, by alkaline
digestion and determined by UV-VIS Spectrophotometer.
With reference to IEC 62321 edition 1.0:2008 in Annex A, by solvent
extraction and determined by GC-MSD and further HPLC confirmation
when necessary.
With reference to IEC 62321 edition 1.0:2008 in Annex A, by solvent
extraction and determined by GC-MSD and further HPLC confirmation
when necessary.
Reporting limit
2 ppm
2 ppm
2 ppm
1 ppm
5 ppm
5 ppm
Remark:Reporting limit = Quantitation limit of analyze in sample
************************************************************************************************************************************************************
To Be Continued
Page 3 Of 7
Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233
Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
Test Report
Number:
SHAH00361375
Tests Conducted
(Ⅳ) MEASUREMENT FLOWCHART:
Test for Cd/ Pb/ Hg/Cr (VI)/ PBBs/PBDEs contents
Reference standard: IEC 62321 edition 1.0:2008
Sampling/grinding or cutting
Cr
Cd/Pb/Hg
Metal
Weigh sample and for
different material,
digest the sample with
*1
appropriate acid
No
Get 50cm
samples
Yes
Weigh sample and
add organic
solvent
*2
Soxhlet extraction
or
Solvent extraction
Cool and filter the
extract
Make up with deionized
water and add Diphenylcarbazide solution
Analyzed by ICP-OES
PBBs/PBDEs
Definite temp.
Extraction
2
Boiling water
extraction
Make up with
deionized water
Polymers /
electronics
Weigh sample
and add alkaline
solution
Spot test
Negative
Confirm the tested
samples are totally
dissolved
6+
Concentrate the
extract and make
up with organic
solvent
Analyzed by GC-MSD
Analyzed by UV-VIS
REMARKS:
*1: LIST OF APPROPRIATE ACID:
MATERIAL
Polymers
Metals
Electronics
ACID ADDED FOR DIGESTION
HNO3,HCl,HF,H2O2,H3BO3
HNO3,HCL,HF
HNO3,HCL,H2O2,HBF4
*2: IF THE RESULT OF SPOT TEST IS POSITIVE, CHROMIUM (VI) WOULD BE DETERMINED AS DETECTED.
************************************************************************************************************************************************************
To Be Continued
Page 4 Of 7
Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233
Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
Test Report
Number:
SHAH00361375
Tests Conducted
2
Halogen content
(Ⅰ) Test result summary:
Testing item
Fluorine (F)
Chlorine (Cl)
Bromine (Br)
Result (ppm)
350
150
ND
Iodine (I)
ND
Remarks:ppm = parts per million = mg/kg
ND = Not detected
Responsibility of chemist:Grave Wang
(Ⅱ) Test method:
Testing item
Halogen content
Testing method
Reporting limit
With reference to EN 14582:2007 by combustion flask with oxygen
and determined by ion chromatography
50 ppm
Remark:Reporting limit = quantitation limit of analyte in sample
Date sample received:Jan.8, 2013
Testing period:Jan.8, 2013 To Jan.14, 2013
************************************************************************************************************************************************************
To Be Continued
Page 5 Of 7
Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233
Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
Test Report
Number:
SHAH00361375
Tests Conducted
(Ⅲ) MEASUREMENT FLOWCHART:
Test for halogen content
REFERENCE STANDARD:EN 14582
Sampling/grinding or cutting
Add absorbent in a combustion flask &
place weighed sample in equipment
Fill the combustion flask with oxygen
Ignite then leave the flask at room
temperature
Transfer the absorbent into a volumetric
flask
Make up with deionized water
Analyzed by ion chromatography
************************************************************************************************************************************************************
To Be Continued
Page 6 Of 7
Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233
Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
Test Report
Number:
SHAH00361375
Tests Conducted
************************************************************************************************************************************************************
End Of Report
This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a recommendation for any particular
course of action. Intertek does not accept a duty of care or any other responsibility to any person other than the Client in respect of this report and only accepts liability
to the Client insofar as is expressly contained in the terms and conditions governing Intertek's provision of services to you. Intertek makes no warranties or
representations either express or implied with respect to this report save as provided for in those terms and conditions. We have aimed to conduct the Review on a
diligent and careful basis and we do not accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by statute or otherwise,
except in the event of our gross negligence or wilful misconduct.
Page 7 Of 7
Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233
Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
Test Report
Applicant:
Number:
LITTELFUSE,INC.
800 E. NORTHWEST HWY
A.DIVIETRO/D.UNTIEDT
Attn:
Date:
SHAH00361371
JAN 16, 2013
Sample Description:
One(1) submitted sample said to be Brown Liquid.
Item Name
: Solder Flux BC310.
Part No.
: 195116.
************************************************************************************************************************************************************
Tests Conducted:
As requested by the applicant, for details refer to attached page(s).
************************************************************************************************************************************************************
Authorized by:
For intertek testing services Ltd., Shanghai
Jacob Lin
General Manager
Page 1 Of 13
Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233
Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
Test Report
Number:
SHAH00361371
Tests Conducted
1
(Ⅰ) Test Result Summary:
Testing Item
Heavy Metal
Cadmium (Cd) content
Lead (Pb) content
Mercury (Hg) content
6+
Chromium VI (Cr ) content
Polybrominated Biphenyls (PBBs)
Monobrominated Biphenyls (MonoBB)
Dibrominated Biphenyls (DiBB)
Tribrominated Biphenyls (TriBB)
Tetrabrominated Biphenyls (TetraBB)
Pentabrominated Biphenyls (PentaBB)
Hexabrominated Biphenyls (HexaBB)
Heptabrominated Biphenyls (HeptaBB)
Octabrominated Biphenyls (OctaBB)
Nonabrominated Biphenyls (NonaBB)
Decabrominated Biphenyl (DecaBB)
Polybrominated Diphenyl Ethers (PBDEs)
Monobrominated Diphenyl Ethers (MonoBDE)
Dibrominated Diphenyl Ethers (DiBDE)
Tribrominated Diphenyl Ethers (TriBDE)
Tetrabrominated Diphenyl Ethers (TetraBDE)
Pentabrominated Diphenyl Ethers (PentaBDE)
Hexabrominated Diphenyl Ethers (HexaBDE)
Heptabrominated Diphenyl Ethers (HeptaBDE)
Octabrominated Diphenyl Ethers (OctaBDE)
Nonabrominated Diphenyl Ethers (NonaBDE)
Decabrominated Diphenyl Ether (DecaBDE)
Result (ppm)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Remarks:ppm = parts per million = mg/kg
ND = not detected
Responsibility of Chemist: Dent Fang / Leaf Liu
(Ⅱ) RoHS Requirement:
Restricted substances
Cadmium (Cd) Content
Lead (Pb) Content
Mercury (Hg) Content
6+
Chromium VI (Cr ) Content
Polybrominated Biphenyls (PBBs)
Polybrominated Diphenyl Ethers (PBDEs)
Limits
0.01% (100ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
The above limits were quoted from RoHS Directive 2011/65/EU for homogeneous material.
************************************************************************************************************************************************************
To Be Continued
Page 2 Of 13
Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233
Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
Test Report
Number:
SHAH00361371
Tests Conducted
(Ⅲ) Test Method:
Testing item
Cadmium (Cd) content
Lead (Pb) content
Mercury (Hg) content
6+
Chromium VI (Cr ) content
Polybrominated Biphenyls
(PBBs)
Polybrominated Diphenyl
Ethers (PBDEs)
Testing method
With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by
microwave digestion until the tested samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by
microwave digestion until the tested samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition 1.0:2008 in clause 7, by microwave
digestion until the tested samples are totally dissolved and determined
by ICP-OES.
With reference to IEC 62321 edition 1.0:2008 in annex C, by alkaline
digestion and determined by UV-VIS Spectrophotometer.
With reference to IEC 62321 edition 1.0:2008 in Annex A, by solvent
extraction and determined by GC-MSD and further HPLC confirmation
when necessary.
With reference to IEC 62321 edition 1.0:2008 in Annex A, by solvent
extraction and determined by GC-MSD and further HPLC confirmation
when necessary.
Reporting limit
2 ppm
2 ppm
2 ppm
1 ppm
5 ppm
5 ppm
Remark:Reporting limit = Quantitation limit of analyze in sample
************************************************************************************************************************************************************
To Be Continued
Page 3 Of 13
Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233
Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
Test Report
Number:
SHAH00361371
Tests Conducted
(Ⅳ) MEASUREMENT FLOWCHART:
Test for Cd/ Pb/ Hg/Cr (VI)/ PBBs/PBDEs contents
Reference standard: IEC 62321 edition 1.0:2008
Sampling/grinding or cutting
Cr
Cd/Pb/Hg
Metal
Weigh sample and for
different material,
digest the sample with
*1
appropriate acid
No
Get 50cm
samples
Yes
Weigh sample and
add organic
solvent
*2
Soxhlet extraction
or
Solvent extraction
Cool and filter the
extract
Make up with deionized
water and add Diphenylcarbazide solution
Analyzed by ICP-OES
PBBs/PBDEs
Definite temp.
Extraction
2
Boiling water
extraction
Make up with
deionized water
Polymers /
electronics
Weigh sample
and add alkaline
solution
Spot test
Negative
Confirm the tested
samples are totally
dissolved
6+
Concentrate the
extract and make
up with organic
solvent
Analyzed by GC-MSD
Analyzed by UV-VIS
REMARKS:
*1: LIST OF APPROPRIATE ACID:
MATERIAL
Polymers
Metals
Electronics
ACID ADDED FOR DIGESTION
HNO3,HCl,HF,H2O2,H3BO3
HNO3,HCL,HF
HNO3,HCL,H2O2,HBF4
*2: IF THE RESULT OF SPOT TEST IS POSITIVE, CHROMIUM (VI) WOULD BE DETERMINED AS DETECTED.
************************************************************************************************************************************************************
To Be Continued
Page 4 Of 13
Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233
Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
Test Report
Number:
SHAH00361371
Tests Conducted
2
Halogen content
(Ⅰ) Test result summary:
Testing item
Fluorine (F)
Chlorine (Cl)
Bromine (Br)
Result (ppm)
ND
1000
ND
Iodine (I)
ND
Remarks:ppm = parts per million = mg/kg
ND = Not detected
Responsibility of chemist:Grave Wang
(Ⅱ) Test method:
Testing item
Halogen content
Testing method
Reporting limit
With reference to EN 14582:2007 by combustion flask with oxygen
and determined by ion chromatography
50 ppm
Remark:Reporting limit = quantitation limit of analyte in sample
************************************************************************************************************************************************************
To Be Continued
Page 5 Of 13
Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233
Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
Test Report
Number:
SHAH00361371
Tests Conducted
(Ⅲ) MEASUREMENT FLOWCHART:
Test for halogen content
REFERENCE STANDARD:EN 14582
Sampling/grinding or cutting
Add absorbent in a combustion flask &
place weighed sample in equipment
Fill the combustion flask with oxygen
Ignite then leave the flask at room
temperature
Transfer the absorbent into a volumetric
flask
Make up with deionized water
Analyzed by ion chromatography
************************************************************************************************************************************************************
To Be Continued
Page 6 Of 13
Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233
Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
Test Report
SHAH00361371
Number:
Tests Conducted
3
HBCDD content
(Ⅰ)Test result summary:
Testing item
Result (ppm)
HBCDD (hexabromocyclododecane)
ND
Remarks:ppm = parts per million = mg/kg
ND = Not detected
(Ⅱ) Test method:
Testing item
Testing method
Reporting limit
HBCDD (hexabromocyclododecane)
With reference to US EPA 3540C, by solvent
extraction and determined by GC-MS
10 ppm
*****************************************************************************************************************************************************
To Be Continued
Page 7 Of 13
Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233
Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
Test Report
Number:
SHAH00361371
Tests Conducted
Measurement flowchart:
Test for HBCDD (hexabromocyclododecane) content
Weigh sample and place into a thimble
Soxhlet extraction with organic solvent
Concentrate the extract
Transfer the extract into a volumetric flask
Make up with organic solvent
Analyze by GC-MS
*****************************************************************************************************************************************************
To Be Continued
Page 8 Of 13
Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233
Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
Test Report
Number:
SHAH00361371
Tests Conducted
4
Phthalate content test
With reference to EN 14372, by Gas Chromatography-Mass Spectrometry (GC-MS) analysis.
Tested compound
Result (%,w/w)
Di-butyl phthalate (DBP)
Di(2-ethyl hexyl) phthalate(DEHP)
Benzyl butyl phthalate (BBP)
Sum of three phthalates
ND
ND
ND
ND
Limit(%,w/w)
(MAX.)
------0.1
Remark:The above limit was quoted according to Annex XVII items 51 & 52 of the REACH regulation (EC)
NO.1907/2006 & Amendment NO.552/2009 for phthalate content in toys and children care articles.
Detection limit = 0.01%(w/w)
ND = Not detected
*****************************************************************************************************************************************************
To Be Continued
Page 9 Of 13
Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233
Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
Test Report
Number:
SHAH00361371
Tests Conducted
Measurement flowchart:
Test for phthalate content
Weigh sample and place in a
thimble
Extracted by soxhlet extraction
with organic solvent
Concentrate the extract
TRANSFER THE EXTRACT
INTO A VOLUMETRIC FLASK
Make up with organic solvent
Analyze by GC-MS
*****************************************************************************************************************************************************
To Be Continued
Page 10 Of 13
Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233
Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
Test Report
Number:
SHAH00361371
Tests Conducted
5
PHTHALATE CONTENT TEST
WITH REFERENCE TO CPSC-CH-C1001-09.3, BY GAS CHROMATOGRAPHY-MASS SPECTROMETRY (GC-MS)
ANALYSIS.
TESTED COMPOUND
RESULT (%,W/W)
DI-BUTYL PHTHALATE (DBP)
DI(2-ETHYL HEXYL) PHTHALATE(DEHP)
BENZYL BUTYL PHTHALATE (BBP)
REMARK:
ND
ND
ND
LIMIT(%,W/W)
(MAX.)
0.1
0.1
0.1
DETECTION LIMIT = 0.01%(W/W)
ND = NOT DETECTED
DATE SAMPLE RECEIVED:JAN.8, 2013
TESTING PERIOD:JAN.8, 2013 TO JAN.11, 2013
*****************************************************************************************************************************************************
To Be Continued
Page 11 Of 13
Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233
Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
Test Report
Number:
SHAH00361371
Tests Conducted
MEASUREMENT FLOWCHART
TEST FOR PHTHALATE CONTENT
Weigh sample and place in a
thimble
Extracted by soxhlet extraction
with organic solvent
Concentrate the extract
TRANSFER THE EXTRACT
INTO A VOLUMETRIC FLASK
Make up with organic solvent
Analyze by GC-MS
*****************************************************************************************************************************************************
To Be Continued
Page 12 Of 13
Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233
Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
Test Report
Number:
SHAH00361371
Tests Conducted
*****************************************************************************************************************************************************
End Of Report
This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a recommendation for any particular
course of action. Intertek does not accept a duty of care or any other responsibility to any person other than the Client in respect of this report and only accepts liability
to the Client insofar as is expressly contained in the terms and conditions governing Intertek's provision of services to you. Intertek makes no warranties or
representations either express or implied with respect to this report save as provided for in those terms and conditions. We have aimed to conduct the Review on a
diligent and careful basis and we do not accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by statute or otherwise,
except in the event of our gross negligence or wilful misconduct.
Page 13 Of 13
Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233
Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
Test Report
Applicant:
Number : TWNC00282886
Littelfuse Philippines Inc.
LIMA Technology Center, Lipa City,
Malvar, Batangas
Date
: Oct 31, 2012
Sample Description:
One (1) group of submitted samples said to be :
Part Description
: sand
Part Number
: 091250
Date Sample Received
: Oct 24, 2012
Date Test Started
: Oct 25, 2012
Test Conducted :
As requested by the applicant, for details please refer to attached pages.
Authorized By:
On Behalf Of Intertek Testing Services
Taiwan Limited
K. Y. Liang
Director
*THJ0282886*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410
Page 1 of 7
Number : TWNC00282886
Test Conducted
(Ⅰ) Test Result Summary :
Result (ppm)
Submitted Samples
Test Item
Heavy Metal
Cadmium (Cd) content
Lead (Pb) content
Mercury (Hg) content
Chromium VI (Cr6+) content
Polybrominated Biphenyls (PBBs)
Monobrominated Biphenyls (MonoBB)
Dibrominated Biphenyls (DiBB)
Tribrominated Biphenyls (TriBB)
Tetrabrominated Biphenyls (TetraBB)
Pentabrominated Biphenyls (PentaBB)
Hexabrominated Biphenyls (HexaBB)
Heptabrominated Biphenyls (HeptaBB)
Octabrominated Biphenyls (OctaBB)
Nonabrominated Biphenyls (NonaBB)
Decabrominated Biphenyl (DecaBB)
Polybrominated Diphenyl Ethers (PBDEs)
Monobrominated Diphenyl Ethers (MonoBDE)
Dibrominated Diphenyl Ethers (DiBDE)
Tribrominated Diphenyl Ethers (TriBDE)
Tetrabrominated Diphenyl Ethers (TetraBDE)
Pentabrominated Diphenyl Ethers (PentaBDE)
Hexabrominated Diphenyl Ethers (HexaBDE)
Heptabrominated Diphenyl Ethers (HeptaBDE)
Octabrominated Diphenyl Ethers (OctaBDE)
Nonabrominated Diphenyl Ethers (NonaBDE)
Decabrominated Diphenyl Ether (DecaBDE)
Halogen Content
Fluorine (F)
Chlorine (Cl)
Bromine (Br)
Iodine (I)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Remarks: ppm = Parts per million based on weight of tested sample = mg/kg
ND = Not detected
Responsibility of Chemist : Irene Chiou / Kevin Liu / Cathy Chen
Date Sample Received
Test Period
: Oct 24, 2012
: Oct 25, 2012 To Oct 30, 2012
*THJ0282886*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410
Page 2 of 7
Number : TWNC00282886
Test Conducted
(Ⅱ) RoHS Limits:
Restricted Substances
Cadmium (Cd) Content
Lead (Pb) Content
Mercury (Hg) Content
Chromium VI (Cr6+) Content
Polybrominated Biphenyls (PBBs)
Polybrominated Diphenyl Ehters (PBDEs)
Limits
0.01% (100ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
The above limits were quoted from Annex II of 2011/65/EU for homogeneous
material.
(Ⅲ) Test Method:
Test Item
Cadmium (Cd)
content
Lead (Pb) content
Mercury (Hg)
content
Chromium VI (Cr6+)
content
Test Method
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 7, by microwave
digestion until the tested samples
are totally dissolved and determined
by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in annex C, by alkaline
digestion and determined by UV-Vis
spectrophotometer.
Reporting Limit
*THJ0282886*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410
2 ppm
2 ppm
2 ppm
1 ppm
Page 3 of 7
Number : TWNC00282886
Test Conducted
(Ⅲ) Test Method:
Test Item
Polybrominated
Biphenyls (PBBs)
Polybrominated
Diphenyl Ethers
(PBDEs)
Halogen Content
Test Method
With reference to IEC 62321 edition
1.0:2008 in annex A, by solvent
extraction and determined by GC-MS
and further HPLC-DAD confirmation
when necessary.
With reference to IEC 62321 edition
1.0:2008 in annex A, by solvent
extraction and determined by GC-MS
and further HPLC-DAD confirmation
when necessary.
With reference to EN 14582:2007 by
calorimetric bomb with oxygen and
determined by Ion Chromatograph.
Reporting Limit
5 ppm
5 ppm
50 ppm
Remark: Reporting limit = Quantitation limit of analyte in sample
*THJ0282886*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410
Page 4 of 7
Number : TWNC00282886
Test Conducted
(Ⅳ) Measurement Flowchart:
Test for Cd/Pb/Hg/Chromium (VI)/PBBS/PBDES Contents
Reference Standard: IEC 62321 edition 1.0:2008
Sample preparation
For non-metal part
For metal part
Take sample and immerse into Aqua Regia, start to strip plating layer
Stop the stripping procedure upon color change completely
Take the Aqua solution as plating component and stripped body as substrate component
Cd/Pb/Hg
Cr
Confirm the tested
samples are
totally dissolved
Make up with
deionized water
PBBs/PBDEs
Polymers /
electronics
Metal
For different
material, digest
the sample with
*1
appropriate acid
6+
Weigh sample and
add organic solvent
By spot test
Negative
Get 50cm2 sample
By boiling water
extraction
*2
Weigh sample
and add
alkaline
solution
By Soxhlet
extraction or
Solvent extraction
Definite temp.
extraction
Cool and filter
the extract
Analyzed by ICP-OES
Concentrate the
extract and make up
with organic
solvent
Analyzed by GC-MSD
Make up with deionized
water and add diphenylcarbazide solution
Remarks:
*1: List of Appropriate Acid:
Material
Polymers
Metals
Electronics
Analyzed by UV-VIS
Acid Added for Digestion
HNO3,HCl,HF,H2O2,H3BO3
HNO3,HCl,HF
HNO3,HCl,H2O2,HBF4
*2: If the result of spot test is positive, Chromium VI would be determined as detected.
*THJ0282886*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410
Page 5 of 7
Number : TWNC00282886
Test Conducted
(Ⅳ) Measurement Flowchart:
Test for Halogen Content
Reference Standard:EN 14582
Sampling/grinding or
cutting
Add absorbent in a
combustion flask &
place weighed sample in
equipment
Fill oxygen into
calorimetric bomb
Ignite then leave the
bomb at room
temperature
Transfer the absorbent
into a volumetric flask
Make up with deionized
water
Analyzed by ion
chromatography
End of Report
This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a
recommendation for any particular course of action. Intertek does not accept a duty of care or any other responsibility to any person other than
the Client in respect of this report and only accepts liability to the Client insofar as is expressly contained in the terms and conditions
governing Intertek's provision of services to you. Intertek makes no warranties or representations either express or implied with respect to this
report save as provided for in those terms and conditions. We have aimed to conduct the Review on a diligent and careful basis and we do not
accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by
statute or otherwise, except in the event of our gross negligence or wilful misconduct.
*THJ0282886*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410
Page 6 of 7
Number : TWNC00282886
Test Conducted
Photo
*THJ0282886*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410
Page 7 of 7