ICPTest_804_8 13 12 pdf

ICP Test Report Certification Packet
Company name :
Littelfuse, Inc.
Product Series:
TE Subminiature Fuse
Product #:
804 Series
Issue Date:
August 13, 2012
It is hereby certified by Littelfuse, Inc. that there is neither RoHS (EU Directive 2002/95/EC,
2011/65/EU)-restricted substance nor such use, for materials to be used for unit parts, for
packing/packaging materials, and for additives and the like in the manufacturing processes.
In addition, it is hereby reported to you that the parts and sub-materials, the materials to be used
for unit parts, the packing/packaging materials, and the additives and the like in the manufacturing
processes, are all composed of the following components.
Issued :
<Global EHS Engineer>
(1) Parts, sub-materials and unit parts
This document covers the TE Subminiature Fuse, RoHS-Compliant series products
manufactured by Littelfuse, Inc.
< Raw Materials Used
Please see Table 1
(2) The ICP data on all measurable substances
Please see appropriate pages as identifed in Table 1
Remarks:
Form 585-047 Rev. A
1
2/21/06
Table 1: List of Raw Materials covered by this report
Total Parts
1
2
3
4
5
6
Raw Material Part Number
867-017 (867-002)
910-017 (910-025)
692213
648102
090254
04xxx
Raw Material Description
Socket with Pin
Caps
Solder
Yarn
Sand Filler
Tinned Wire (CuNi44 Sn – Element)
2
Page(s)
3-12
13-21
22-26
27-35
36-42
43-52
Test Report
Applicant:
Littelfuse Philippines Inc.
LIMA Technology Center, Lipa City,
Malvar, Batangas
Number
: TWNC00256913
Date
: May 15, 2012
Sample Description:
One (1) group of submitted samples said to be :
Part Description
: Socket with Pin
Part Number
: 867-002
Date Sample Received
: May 10, 2012
Date Test Started
: May 10, 2012
Test Conducted :
As requested by the applicant, for details please refer to attached pages.
Authorized By:
On Behalf Of Intertek Testing Services
Taiwan Limited
K. Y. Liang
Director
This report shall not be reproduced
except in full, without the written
approval of the laboratory.
Page 1 of 10
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Number:
TWNC00256913
Test Conducted
(Ⅰ) Test Result Summary :
Test Item
Heavy Metal
Cadmium (Cd) content
Lead (Pb) content
Mercury (Hg) content
Chromium VI (Cr6+) content (For Non-Metal
Material)
Chromium VI (Cr6+) content (By Boiling Water
Extraction On Metal) (mg/kg with 50cm2)
Polybrominated Biphenyls (PBBs)
Monobrominated Biphenyls (MonoBB)
Dibrominated Biphenyls (DiBB)
Tribrominated Biphenyls (TriBB)
Tetrabrominated Biphenyls (TetraBB)
Pentabrominated Biphenyls (PentaBB)
Hexabrominated Biphenyls (HexaBB)
Heptabrominated Biphenyls (HeptaBB)
Octabrominated Biphenyls (OctaBB)
Nonabrominated Biphenyls (NonaBB)
Decabrominated Biphenyl (DecaBB)
Polybrominated Diphenyl Ethers (PBDEs)
Monobrominated Diphenyl Ethers (MonoBDE)
Dibrominated Diphenyl Ethers (DiBDE)
Tribrominated Diphenyl Ethers (TriBDE)
Tetrabrominated Diphenyl Ethers (TetraBDE)
Pentabrominated Diphenyl Ethers (PentaBDE)
Hexabrominated Diphenyl Ethers (HexaBDE)
Heptabrominated Diphenyl Ethers (HeptaBDE)
Octabrominated Diphenyl Ethers (OctaBDE)
Nonabrominated Diphenyl Ethers (NonaBDE)
Decabrominated Diphenyl Ether (DecaBDE)
Halogen Content
Fluorine (F)
Chlorine (Cl)
Bromine (Br)
Iodine (I)
(1)
Result (ppm)
(2)
(3)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
--
--
ND
Negative
(< 0.02)(#)
Negative
(< 0.02)(#)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
-----------
-----------
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
-----------
-----------
ND
ND
ND
ND
-----
-----
Page 2 of 10
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Number:
TWNC00256913
Test Conducted
(Ⅰ) Test Result Summary :
Test Item
Phthalates
Di(2-ethylhexyl) Phthalate (DEHP)
Dibutyl Phthalate (DBP)
Benzyl Butyl Phthalate (BBP)
Others
Hexabromocyclododecane (HBCDD)
(1)
Result (ppm)
(2)
(3)
ND
ND
ND
----
----
ND
--
--
Remarks: ppm = Parts per million based on weight of tested sample = mg/kg
ND = Not detected
<
= Less than
mg/kg with 50cm2 = milligram per kilogram with 50 square centimetre
Negative = A negative test result indicated positive observation
was not found at the time of Test.
#
= Due to the insufficient sample area, reduced total sample
surface of 25 cm2 was used and the dilution factor was
adjusted accordingly.
Tested Components:
(1) Black Body Part
(2) Coppery Metal Substrate
(3) Silvery Plating On Metal Pin
Responsibility of Chemist : Irene Chiou / Kevin Liu / Cathy Chen
Date Sample Received
Test Period
: May 10, 2012
: May 10, 2012 To May 14, 2012
(Ⅱ) RoHS Requirement:
Restricted Substances
Cadmium (Cd) Content
Lead (Pb) Content
Mercury (Hg) Content
Chromium VI (Cr6+) Content
Polybrominated Biphenyls (PBBs)
Polybrominated Diphenyl Ehters (PBDEs)
Limits
0.01% (100ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for
homogeneous material.
Page 3 of 10
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Number:
Test Conducted
(Ⅲ) Test Method:
Test Item
TWNC00256913
Test Method
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
Cadmium (Cd)
microwave digestion until the tested
content
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
Lead (Pb) content
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 7, by microwave
Mercury (Hg)
digestion until the tested samples are
content
totally dissolved and determined by
ICP-OES.
With reference to IEC 62321 edition
6+
Chromium VI (Cr )
1.0:2008 in annex C, by alkaline
content (For Nondigestion and determined by UV-Vis
Metal Meterial)
spectrophotometer.
Chromium VI (Cr6+) With reference to IEC 62321 edition
content (By Boiling 1.0:2008 in annex B, by boiling water
Wter Extraction On extraction and determined by UV-Vis
Metal)
Spectrophotometer.
With reference to IEC 62321 edition
1.0:2008 in annex A, by solvent
Polybrominated
extraction and determined by GC-MS and
Biphenyls (PBBs)
further HPLC-DAD confirmation when
necessary.
With reference to IEC 62321 edition
Polybrominated
1.0:2008 in annex A, by solvent
Diphenyl Ethers
extraction and determined by GC-MS and
(PBDEs)
further HPLC-DAD confirmation when
necessary.
With reference to EN 14582:2007 by
Halogen Content
calorimetric bomb with oxygen and
determined by Ion Chromatograph.
With reference to EN 14372: 2004, by
Phthalates
solvent extraction and determined by
GC-MS.
With reference to USEPA 3540C, by
Hexabromocyclodode
solvent extraction and determined by
cane (HBCDD)
GC-MSD.
Reporting Limit
2 ppm
2 ppm
2 ppm
1 ppm
0.02
mg/kg with 50cm2
5 ppm
5 ppm
50 ppm
50 ppm
10 ppm
Remark: Reporting limit = Quantitation limit of analyte in sample
Page 4 of 10
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Number:
TWNC00256913
Test Conducted
(Ⅳ) Measurement Flowchart:
Test for Cd/Pb/Hg/Chromium (VI)
Reference Standard:IEC 62321 edition 1.0:2008
Sample preparation
Take sample and immerse into Aqua Regia, start to strip plating layer
Stop the stripping procedure upon color change completely
Take the Aqua solution as plating component and stripped body as substrate component
Cd/Pb/Hg
Cr
Polymers /
electronics
Metal
For different
material, digest
the sample with
*1
appropriate acid
By spot test
Negative
Confirm the tested
samples are
totally dissolved
Make up with
deionized water
6+
*2
Weigh sample
and add
alkaline
solution
Get 50cm2 sample
Definite temp.
extraction
By boiling water
extraction
Cool and filter
the extract
Analyzed by ICP-OES
Make up with deionized water and add
diphenyl-carbazide solution
Remarks:
*1: List of Appropriate Acid:
Material
Polymers
Metals
Electronics
Analyzed by UV-VIS
Acid Added for Digestion
HNO3,HCl,HF,H2O2,H3BO3
HNO3,HCl,HF
HNO3,HCl,H2O2,HBF4
*2: If the result of spot test is positive, Chromium VI would be determined as detected.
Page 5 of 10
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Number:
TWNC00256913
Test Conducted
(Ⅳ) Measurement Flowchart:
Test for Cd/Pb/Hg/Chromium (VI)/PBBS/PBDES Contents
Reference Standard: IEC 62321 edition 1.0:2008
Sample preparation
For non-metal part
For metal part
Take sample and immerse into Aqua Regia, start to strip plating layer
Stop the stripping procedure upon color change completely
Take the Aqua solution as plating component and stripped body as substrate component
Cd/Pb/Hg
Cr
Weigh sample and
add organic solvent
By spot test
Negative
Confirm the tested
samples are
totally dissolved
Make up with
deionized water
PBBs/PBDEs
Polymers /
electronics
Metal
For different
material, digest
the sample with
*1
appropriate acid
6+
Get 50cm2 sample
By boiling water
extraction
*2
Weigh sample
and add
alkaline
solution
By Soxhlet
extraction or
Solvent extraction
Definite temp.
extraction
Cool and filter
the extract
Analyzed by ICP-OES
Concentrate the
extract and make up
with organic
solvent
Analyzed by GC-MSD
Make up with deionized
water and add diphenylcarbazide solution
Remarks:
*1: List of Appropriate Acid:
Material
Polymers
Metals
Electronics
Analyzed by UV-VIS
Acid Added for Digestion
HNO3,HCl,HF,H2O2,H3BO3
HNO3,HCl,HF
HNO3,HCl,H2O2,HBF4
*2: If the result of spot test is positive, Chromium VI would be determined as detected.
Page 6 of 10
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Number:
TWNC00256913
Test Conducted
(Ⅳ) Measurement Flowchart:
Test for Halogen Content
Reference Standard:EN 14582
Sampling/grinding or
cutting
Add absorbent in a
combustion flask &
place weighed sample in
equipment
Fill oxygen into
calorimetric bomb
Ignite then leave the
bomb at room
temperature
Transfer the absorbent
into a volumetric flask
Make up with deionized
water
Analyzed by ion
chromatography
Page 7 of 10
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Number:
TWNC00256913
Test Conducted
(Ⅳ) Measurement Flowchart:
Test For Phthalates Contents
Reference Method: EN 14372: 2004
Sampling/grinding or
cutting
Weigh sample and add
organic solvent
By solvent extraction
Concentrate the extract
and make up with
organic solvent
Analyzed by GC-MSD
Page 8 of 10
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Number:
TWNC00256913
Test Conducted
(Ⅳ) Measurement Flowchart:
Test For Hexabromocyclododecane (HBCDD)
Reference Standard:USEPA 3540C
Sampling/grinding or cutting
Weigh sample and add organic
solvent
By soxhlet extraction
Concentrate the extract and
make up with organic solvent
Analyzed by GC-MSD
End of Report
Page 9 of 10
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Number:
TWNC00256913
Test Conducted
Photo
Page 10 of
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Test Report
Applicant:
Number : TWNC00232331
Littelfuse Philippines Inc.
LIMA Technology Center, Lipa City,
Malvar, Batangas
Date
: Nov 18, 2011
Sample Description:
One (1) group of submitted samples said to be :
Part Description
: TE Caps (same with 910-016 TR Caps)
Part Number
: 910-017
Date Sample Received
: Nov 11, 2011
Date Test Started
: Nov 14, 2011
Test Conducted :
As requested by the applicant, for details please refer to attached pages.
Authorized By:
On Behalf Of Intertek Testing Services
Taiwan Limited
K. Y. Liang
Director
This report shall not be reproduced
except in full, without the written
approval of the laboratory.
Page 1 of 9
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Number : TWNC00232331
Test Conducted
(Ⅰ) Test Result Summary :
Test Item
Result (ppm)
Brown Plastic
Heavy Metal
Cadmium (Cd) content
Lead (Pb) content
Mercury (Hg) content
Chromium VI (Cr6+) content
Polybrominated Biphenyls (PBBs)
Monobrominated Biphenyls (MonoBB)
Dibrominated Biphenyls (DiBB)
Tribrominated Biphenyls (TriBB)
Tetrabrominated Biphenyls (TetraBB)
Pentabrominated Biphenyls (PentaBB)
Hexabrominated Biphenyls (HexaBB)
Heptabrominated Biphenyls (HeptaBB)
Octabrominated Biphenyls (OctaBB)
Nonabrominated Biphenyls (NonaBB)
Decabrominated Biphenyl (DecaBB)
Polybrominated Diphenyl Ethers (PBDEs)
Monobrominated Diphenyl Ethers (MonoBDE)
Dibrominated Diphenyl Ethers (DiBDE)
Tribrominated Diphenyl Ethers (TriBDE)
Tetrabrominated Diphenyl Ethers (TetraBDE)
Pentabrominated Diphenyl Ethers (PentaBDE)
Hexabrominated Diphenyl Ethers (HexaBDE)
Heptabrominated Diphenyl Ethers (HeptaBDE)
Octabrominated Diphenyl Ethers (OctaBDE)
Nonabrominated Diphenyl Ethers (NonaBDE)
Decabrominated Diphenyl Ether (DecaBDE)
Halogen Content
Fluorine (F)
Chlorine (Cl)
Bromine (Br)
Iodine (I)
Phthalates
Di(2-ethylhexyl) Phthalate (DEHP)
Dibutyl Phthalate (DBP)
Benzyl Butyl Phthalate (BBP)
Others
Hexabromocyclododecane (HBCDD)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Remarks: ppm = Parts per million based on weight of tested sample = mg/kg
ND = Not detected
Responsibility of Chemist : Irene Chiou / Kevin Liu / Cathy Chen
Date Sample Received
Test Period
: Nov 11, 2011
: Nov 14, 2011 To Nov 16, 2011
Page 2 of 9
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Test Conducted
(Ⅱ) RoHS Requirement:
Restricted Substances
Cadmium (Cd) Content
Lead (Pb) Content
Mercury (Hg) Content
Chromium VI (Cr6+) Content
Polybrominated Biphenyls (PBBs)
Polybrominated Diphenyl Ehters (PBDEs)
Number : TWNC00232331
Limits
0.01% (100ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for
homogeneous material.
(Ⅲ) Test Method:
Test Item
Cadmium (Cd) content
Lead (Pb) content
Mercury (Hg) content
Chromium VI (Cr6+)
content
Test Method
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the
tested samples are totally
dissolved and determined by ICPOES.
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the
tested samples are totally
dissolved and determined by ICPOES.
With reference to IEC 62321 edition
1.0:2008 in clause 7, by microwave
digestion until the tested samples
are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in annex C, by alkaline
digestion and determined by UV-Vis
spectrophotometer.
Reporting Limit
2 ppm
2 ppm
2 ppm
1 ppm
Page 3 of 9
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Number : TWNC00232331
Test Conducted
(Ⅲ) Test Method:
Test Item
Test Method
Reporting Limit
With reference to IEC 62321 edition
1.0:2008 in annex A, by solvent
Polybrominated
5 ppm
extraction and determined by GC-MSD
Biphenyls (PBBs)
and further HPLC confirmation when
necessary.
With reference to IEC 62321 edition
Polybrominated
1.0:2008 in annex A, by solvent
5 ppm
Diphenyl Ethers
extraction and determined by GC-MSD
and further HPLC confirmation when
(PBDEs)
necessary.
With reference to EN 14582:2007 by
Halogen Content
50 ppm
calorimetric bomb with oxygen and
determined by ion chromatography
With reference to EN 14372: 2004, by
Phthalates
solvent extraction and determined by
50 ppm
GC-MSD
With reference to USEPA 3540C, by
Hexabromocyclododecane
10 ppm
solvent extraction and determined by
(HBCDD)
GC-MSD
Remark: Reporting limit = Quantitation limit of analyte in sample
Page 4 of 9
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Number : TWNC00232331
Test Conducted
(Ⅳ) Measurement Flowchart:
Test for Cd/Pb/Hg/Chromium (VI)/PBBS/PBDES Contents
Reference Standard: IEC 62321 edition 1.0:2008
Sample preparation
For non-metal part
For metal part
Take sample and immerse into Aqua Regia, start to strip plating layer
Stop the stripping procedure upon color change completely
Take the Aqua solution as plating component and stripped body as substrate component
Cd/Pb/Hg
Cr
Confirm the tested
samples are
totally dissolved
Make up with
deionized water
PBBs/PBDEs
Polymers /
electronics
Metal
For different
material, digest
the sample with
*1
appropriate acid
6+
Weigh sample and
add organic solvent
By spot test
Negative
Get 50cm2 sample
By boiling water
extraction
*2
Weigh sample
and add
alkaline
solution
By Soxhlet
extraction or
Solvent extraction
Definite temp.
extraction
Cool and filter
the extract
Analyzed by ICP-OES
Concentrate the
extract and make up
with organic
solvent
Analyzed by GC-MSD
Make up with deionized
water and add diphenylcarbazide solution
Remarks:
*1: List of Appropriate Acid:
Material
Polymers
Metals
Electronics
Analyzed by UV-VIS
Acid Added for Digestion
HNO3,HCl,HF,H2O2,H3BO3
HNO3,HCl,HF
HNO3,HCl,H2O2,HBF4
*2: If the result of spot test is positive, Chromium VI would be determined as detected.
Page 5 of 9
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Number : TWNC00232331
Test Conducted
(Ⅳ) Measurement Flowchart:
Test for Halogen Content
Reference Standard:EN 14582
Sampling/grinding or
cutting
Add absorbent in a
combustion flask &
place weighed sample in
equipment
Fill oxygen into
calorimetric bomb
Ignite then leave the
flask at room
temperature
Transfer the absorbent
into a volumetric flask
Make up with deionized
water
Analyzed by ion
chromatography
Page 6 of 9
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Number : TWNC00232331
Test Conducted
(Ⅳ) Measurement Flowchart:
Test For Phthalates Contents
Reference Method: EN 14372: 2004
Sampling/grinding or
cutting
Weigh sample and add
organic solvent
By solvent extraction
Concentrate the extract
and make up with
organic solvent
Analyzed by GC-MSD
Page 7 of 9
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Number : TWNC00232331
Test Conducted
(Ⅳ) Measurement Flowchart:
Test For Hexabromocyclododecane (HBCDD)
Reference Standard:USEPA 3540C
Sampling/grinding or cutting
Weigh sample and add organic
solvent
By soxhlet extraction
Concentrate the extract and
make up with organic solvent
Analyzed by GC-MSD
End of Report
Page 8 of 9
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Number : TWNC00232331
Test Conducted
Photo
Page 9 of 9
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Number : TWNC00232330
Test Report
Applicant:
Littelfuse Philippines Inc.
LIMA Technology Center, Lipa City,
Malvar, Batangas
Date
: Nov 18, 2011
Sample Description:
One (1) group of submitted samples said to be :
Part Description
: Solder
Part Number
: 692213
Date Sample Received
: Nov 11, 2011
Date Test Started
: Nov 14, 2011
Test Conducted :
As requested by the applicant, for details please refer to attached pages.
Authorized By:
On Behalf Of Intertek Testing Services
Taiwan Limited
K. Y. Liang
Director
This report shall not be reproduced
except in full, without the written
approval of the laboratory.
Page 1 of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Number : TWNC00232330
Test Conducted
(Ⅰ) Test Result Summary :
Test Item
Heavy Metal
Cadmium (Cd) content
Lead (Pb) content
Mercury (Hg) content
Chromium VI (Cr6+) content (mg/kg with 50cm2)
Result (ppm)
Silvery Metal
ND
92
ND
Negative (< 0.02)
Remarks: ppm = Parts per million based on weight of tested sample = mg/kg
ND = Not detected
<
= Less than
mg/kg with 50cm2 = milligram per kilogram with 50 square centimetre
Negative = A negative test result indicated positive observation
was not found at the time of Test.
Responsibility of Chemist : Irene Chiou / Kevin Liu / Cathy Chen
Date Sample Received
Test Period
: Nov 11, 2011
: Nov 14, 2011 To Nov 17, 2011
(Ⅱ) RoHS Requirement:
Restricted Substances
Cadmium (Cd) Content
Lead (Pb) Content
Mercury (Hg) Content
Chromium VI (Cr6+) Content
Limits
0.01% (100ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for
homogeneous material.
Page 2 of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Number : TWNC00232330
Test Conducted
(Ⅲ) Test Method:
Test Item
Cadmium (Cd)
content
Lead (Pb) content
Mercury (Hg)
content
Chromium VI (Cr6+)
content
Test Method
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 7, by microwave
digestion until the tested samples are
totally dissolved and determined by
ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in annex B, by boiling water
extraction and determined by UV-Vis
spectrophotometer.
Reporting Limit
2 ppm
2 ppm
2 ppm
0.02
mg/kg with 50cm2
Remark: Reporting limit = Quantitation limit of analyte in sample
Page 3 of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Test Conducted
(Ⅳ) Measurement Flowchart:
Test for Cd/Pb/Hg/Chromium (VI)
Reference Standard:IEC 62321 edition 1.0:2008
Number : TWNC00232330
Sample preparation
Take sample and immerse into Aqua Regia, start to strip plating layer
Stop the stripping procedure upon color change completely
Take the Aqua solution as plating component and stripped body as substrate component
Cd/Pb/Hg
Cr
Polymers /
electronics
Metal
For different
material, digest
the sample with
*1
appropriate acid
By spot test
Negative
Confirm the tested
samples are
totally dissolved
Make up with
deionized water
6+
*2
Weigh sample
and add
alkaline
solution
Get 50cm2 sample
Definite temp.
extraction
By boiling water
extraction
Cool and filter
the extract
Analyzed by ICP-OES
Make up with deionized water and add
diphenyl-carbazide solution
Remarks:
*1: List of Appropriate Acid:
Material
Polymers
Metals
Electronics
Analyzed by UV-VIS
Acid Added for Digestion
HNO3,HCl,HF,H2O2,H3BO3
HNO3,HCl,HF
HNO3,HCl,H2O2,HBF4
*2: If the result of spot test is positive, Chromium VI would be determined as detected.
End of Report
Page 4 of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Number : TWNC00232330
Test Conducted
Photo
Page 5 of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Intertek Testing Services Ltd., Shanghai
TFH Division
Block B, Jinling Business Square,No.801 Yi Shan Road,
Shanghai, China, 200233
Tel: +86 21 6120 6565
Fax: +86 21 6127 9740
www.intertek.com
www.intertek.com.cn
China Toll-Free: 800 999 1338
TEST REPORT
APPLICANT: LITTELFUSE,INC.
800 E. NORTHWEST HWY
ATTN: A. CESISTA/ K. BACILA
NUMBER: SHAH00276230
DATE: AUG 24, 2011
SAMPLE DESCRIPTION:
One(1) submitted sample said to be :White yarn.
Part Description
: Yarn.
Part Number
: 648102.
Date Sample Received
: Aug.18, 2011.
Date Test Started
: Aug.18, 2011.
***********************************************************************
TESTS CONDUCTED:
AS REQUESTED BY THE APPLICANT, FOR DETAILS REFER TO ATTACHED PAGE(S)
***********************************************************************
TO BE CONTINUED
PREPARED AND CHECKED BY:
FOR INTERTEK TESTING SERVICES
LTD., SHANGHAI
AUTHORIZED BY:
FOR INTERTEK TESTING SERVICES
LTD., SHANGHAI
MYRA LV
CHEMICAL LAB SENIOR MANAGER
STEPHEN TSANG
GENERAL MANAGER
PAGE 1 OF 9
Intertek Testing Services Ltd., Shanghai
TFH Division
Block B, Jinling Business Square,No.801 Yi Shan Road,
Shanghai, China, 200233
Tel: +86 21 6120 6565
Fax: +86 21 6127 9740
www.intertek.com
www.intertek.com.cn
China Toll-Free: 800 999 1338
TEST REPORT
NUMBER: SHAH00276230
TESTS CONDUCTED
1
(I) Test Result Summary :
Testing Item
Halogen Content
Fluorine (F)
Chlorine (Cl)
Bromine (Br)
Iodine (I)
Result (ppm)
ND
ND
ND
ND
Remarks: ppm = Parts per million = mg/kg
ND = Not detected
Responsibility Of Chemist : Ken He
(II) Test Method:
Testing Item
Testing Method
With reference to EN 14582:2007 by
Halogen
combustion flask with oxygen and
Content
determined by ion chromatography
Reporting Limit
50 ppm
Remark: Reporting limit = Quantitation limit of analyte in sample
***********************************************************************
TO BE CONTINUED
PAGE 2 OF 9
Intertek Testing Services Ltd., Shanghai
TFH Division
Block B, Jinling Business Square,No.801 Yi Shan Road,
Shanghai, China, 200233
Tel: +86 21 6120 6565
Fax: +86 21 6127 9740
www.intertek.com
www.intertek.com.cn
China Toll-Free: 800 999 1338
TEST REPORT
NUMBER: SHAH00276230
TESTS CONDUCTED
(III) Measurement Flowchart:
Test For Halogen Content
Reference Standard: EN 14582
sampling/grinding or
cutting
add absorbent in a
combustion flask &
place weighed sample in
equipment
fill the combustion
flask with oxygen
ignite then leave the
flask at room
temperature
transfer the absorbent
into a volumetric flask
make up with deionized
water
analyzed by ion
chromatography
***********************************************************************
TO BE CONTINUED
PAGE 3 OF 9
Intertek Testing Services Ltd., Shanghai
TFH Division
Block B, Jinling Business Square,No.801 Yi Shan Road,
Shanghai, China, 200233
Tel: +86 21 6120 6565
Fax: +86 21 6127 9740
www.intertek.com
www.intertek.com.cn
China Toll-Free: 800 999 1338
TEST REPORT
NUMBER: SHAH00276230
TESTS CONDUCTED
2
(I) Test Result Summary :
Testing Item
Heavy Metal
Cadmium (Cd) content
Lead (Pb) content
Mercury (Hg) content
Chromium VI (Cr6+) content
Polybrominated Biphenyls (PBBs)
Monobrominated Biphenyls (MonoBB)
Dibrominated Biphenyls (DiBB)
Tribrominated Biphenyls (TriBB)
Tetrabrominated Biphenyls (TetraBB)
Pentabrominated Biphenyls (PentaBB)
Hexabrominated Biphenyls (HexaBB)
Heptabrominated Biphenyls (HeptaBB)
Octabrominated Biphenyls (OctaBB)
Nonabrominated Biphenyls (NonaBB)
Decabrominated Biphenyl (DecaBB)
Polybrominated Diphenyl Ethers (PBDEs)
Monobrominated Diphenyl Ethers (MonoBDE)
Dibrominated Diphenyl Ethers (DiBDE)
Tribrominated Diphenyl Ethers (TriBDE)
Tetrabrominated Diphenyl Ethers (TetraBDE)
Pentabrominated Diphenyl Ethers (PentaBDE)
Hexabrominated Diphenyl Ethers (HexaBDE)
Heptabrominated Diphenyl Ethers (HeptaBDE)
Octabrominated Diphenyl Ethers (OctaBDE)
Nonabrominated Diphenyl Ethers (NonaBDE)
Decabrominated Diphenyl Ether (DecaBDE)
Result (ppm)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Remarks: ppm = Parts per million = mg/kg
ND = Not detected
Responsibility Of Chemist : Dent Fang / Ken He
***********************************************************************
TO BE CONTINUED
PAGE 4 OF 9
Intertek Testing Services Ltd., Shanghai
TFH Division
Block B, Jinling Business Square,No.801 Yi Shan Road,
Shanghai, China, 200233
Tel: +86 21 6120 6565
Fax: +86 21 6127 9740
www.intertek.com
www.intertek.com.cn
China Toll-Free: 800 999 1338
TEST REPORT
NUMBER: SHAH00276230
TESTS CONDUCTED
(II) RoHS Requirement:
Restricted Substances
Cadmium (Cd) Content
Lead (Pb) Content
Mercury (Hg) Content
Chromium VI (Cr6+) Content
Polybrominated Biphenyls (PBBs)
Polybrominated Diphenyl Ehters (PBDEs)
Limits
0.01% (100ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
The above limits were quoted from 2002/95/EC and amendment
2005/618/EC for homogeneous material.
(III) Test Method:
Testing Item
Testing Method
Reporting
Limit
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
Cadmium (Cd)
microwave digestion until the
2 ppm
content
tested samples are totally
dissolved and determined by ICPOES.
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the
Lead (Pb) content
2 ppm
tested samples are totally
dissolved and determined by ICPOES.
With reference to IEC 62321 edition
1.0:2008 in clause 7, by microwave
Mercury (Hg)
digestion until the tested samples
2 ppm
content
are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
Chromium VI (Cr6+) 1.0:2008 in annex C, by alkaline
1 ppm
content
digestion and determined by UV-Vis
spectrophotometer.
***********************************************************************
TO BE CONTINUED
PAGE 5 OF 9
Intertek Testing Services Ltd., Shanghai
TFH Division
Block B, Jinling Business Square,No.801 Yi Shan Road,
Shanghai, China, 200233
Tel: +86 21 6120 6565
Fax: +86 21 6127 9740
www.intertek.com
www.intertek.com.cn
China Toll-Free: 800 999 1338
TEST REPORT
NUMBER: SHAH00276230
TESTS CONDUCTED
Testing Item
Polybrominated
Biphenyls (PBBs)
Polybrominated
Diphenyl Ethers
(PBDEs)
Testing Method
With reference to IEC 62321 edition
1.0:2008 in annex A, by solvent
extraction and determined by GC-MSD
and further HPLC confirmation when
necessary.
With reference to IEC 62321 edition
1.0:2008 in annex A, by solvent
extraction and determined by GC-MSD
and further HPLC confirmation when
necessary.
Reporting
Limit
5 ppm
5 ppm
Remark: Reporting limit = Quantitation limit of analyte in sample
Date Sample Received : AUG.18, 2011
Testing Period : AUG.18, 2011 TO AUG.23, 2011
***********************************************************************
TO BE CONTINUED
PAGE 6 OF 9
Intertek Testing Services Ltd., Shanghai
TFH Division
Block B, Jinling Business Square,No.801 Yi Shan Road,
Shanghai, China, 200233
Tel: +86 21 6120 6565
Fax: +86 21 6127 9740
www.intertek.com
www.intertek.com.cn
China Toll-Free: 800 999 1338
TEST REPORT
NUMBER: SHAH00276230
TESTS CONDUCTED
(IV) Measurement Flowchart:
Test For Cd/Pb/Hg/Chromium (VI)/PBBs/PBDEs Contents
Reference Standard: IEC 62321 edition 1.0:2008
sampling/grinding or cutting
Cr6+
Cd/Pb/Hg
metal
weigh sample and
for different
material, digest
the sample with
confirm the tested
samples are totally
dissolved
spot test
negative*2
No
polymers /
electronics
weigh sample
and add
alkaline
solution
get 50cm2
samples
definite
temp.
boiling water
extraction
cool and
filter the
extract
PBBs/PBDEs
weigh sample
and add
organic
soxhlet
extraction or
solvent
extraction
make up with
deionized water
analyzed by ICP-OES
make up with deionized
water and add diphenylcarbazide solution
concentrate
the extract
and make up
with organic
analyzed by GCMSD
analyzed by UV-VIS
***********************************************************************
TO BE CONTINUED
PAGE 7 OF 9
Intertek Testing Services Ltd., Shanghai
TFH Division
Block B, Jinling Business Square,No.801 Yi Shan Road,
Shanghai, China, 200233
Tel: +86 21 6120 6565
Fax: +86 21 6127 9740
www.intertek.com
www.intertek.com.cn
China Toll-Free: 800 999 1338
TEST REPORT
NUMBER: SHAH00276230
TESTS CONDUCTED
REMARKS:
*1: List of appropriate acid:
Material
Acid added for digestion
Polymers
HNO3,HCl,HF,H2O2,H3BO3
Metals
HNO3,HCl,HF
Electronics
HNO3,HCl,H2O2,HBF4
*2: If the result of spot test is positive, Chromium VI would be
determined as detected.
***********************************************************************
TO BE CONTINUED
PAGE 8 OF 9
Intertek Testing Services Ltd., Shanghai
TFH Division
Block B, Jinling Business Square,No.801 Yi Shan Road,
Shanghai, China, 200233
Tel: +86 21 6120 6565
Fax: +86 21 6127 9740
www.intertek.com
www.intertek.com.cn
China Toll-Free: 800 999 1338
TEST REPORT
NUMBER: SHAH00276230
TESTS CONDUCTED
***********************************************************************
END OF REPORT
PAGE 9 OF 9
Test Report
Applicant:
Number : TWNC00217908
Littelfuse, S.A. de C.V.
Blvd. Fausto Z. Martinez #1800
Col. Magisterio Seccion 38 C.P.
26070 Piedra Negras, Coahuila,
Mexico
Date
: Aug 03, 2011
Sample Description:
One (1) group of submitted samples said to be :
Part Description
: Filler
Part Number
: 090254
Date Sample Received
: Jul 27, 2011
Date Test Started
: Jul 27, 2011
Test Conducted :
As requested by the applicant, for details please refer to attached pages.
Authorized By:
On Behalf Of Intertek Testing Services
Taiwan Limited
K. Y. Liang
Director
This report shall not be reproduced
except in full, without the written
approval of the laboratory.
Page 1 of 7
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Number : TWNC00217908
Test Conducted
(Ⅰ) Test Result Summary :
Test Item
Result (ppm)
Yellow Crystals
Heavy Metal
Cadmium (Cd) content
Lead (Pb) content
Mercury (Hg) content
Chromium VI (Cr6+) content
Polybrominated Biphenyls (PBBs)
Monobrominated Biphenyls (MonoBB)
Dibrominated Biphenyls (DiBB)
Tribrominated Biphenyls (TriBB)
Tetrabrominated Biphenyls (TetraBB)
Pentabrominated Biphenyls (PentaBB)
Hexabrominated Biphenyls (HexaBB)
Heptabrominated Biphenyls (HeptaBB)
Octabrominated Biphenyls (OctaBB)
Nonabrominated Biphenyls (NonaBB)
Decabrominated Biphenyl (DecaBB)
Polybrominated Diphenyl Ethers (PBDEs)
Monobrominated Diphenyl Ethers (MonoBDE)
Dibrominated Diphenyl Ethers (DiBDE)
Tribrominated Diphenyl Ethers (TriBDE)
Tetrabrominated Diphenyl Ethers (TetraBDE)
Pentabrominated Diphenyl Ethers (PentaBDE)
Hexabrominated Diphenyl Ethers (HexaBDE)
Heptabrominated Diphenyl Ethers (HeptaBDE)
Octabrominated Diphenyl Ethers (OctaBDE)
Nonabrominated Diphenyl Ethers (NonaBDE)
Decabrominated Diphenyl Ether (DecaBDE)
Halogen Content
Fluorine (F)
Chlorine (Cl)
Bromine (Br)
Iodine (I)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Remarks: ppm = Parts per million based on weight of tested sample = mg/kg
ND = Not detected
Responsibility of Chemist : Irene Chiou / Kevin Liu / Cathy Chen
Date Sample Received
Test Period
: Jul 27, 2011
: Jul 27, 2011 To Aug 02, 2011
Page 2 of 7
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Test Conducted
(Ⅱ) RoHS Requirement:
Restricted Substances
Cadmium (Cd) Content
Lead (Pb) Content
Mercury (Hg) Content
Chromium VI (Cr6+) Content
Polybrominated Biphenyls (PBBs)
Polybrominated Diphenyl Ehters (PBDEs)
Number : TWNC00217908
Limits
0.01% (100ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for
homogeneous material.
(Ⅲ) Test Method:
Test Item
Cadmium (Cd)
content
Lead (Pb) content
Mercury (Hg)
content
Chromium VI (Cr6+)
content
Test Method
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 7, by microwave
digestion until the tested samples are
totally dissolved and determined by
ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in annex C, by alkaline
digestion and determined by UV-Vis
spectrophotometer.
Reporting Limit
2 ppm
2 ppm
2 ppm
1 ppm
Page 3 of 7
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Test Conducted
(Ⅲ) Test Method:
Test Item
Polybrominated
Biphenyls (PBBs)
Polybrominated
Diphenyl Ethers
(PBDEs)
Halogen Content
Number : TWNC00217908
Test Method
With reference to IEC 62321 edition
1.0:2008 in annex A, by solvent
extraction and determined by GC-MSD
and further HPLC confirmation when
necessary.
With reference to IEC 62321 edition
1.0:2008 in annex A, by solvent
extraction and determined by GC-MSD
and further HPLC confirmation when
necessary.
With reference to EN 14582:2007 by
calorimetric bomb with oxygen and
determined by ion chromatography
Reporting Limit
5 ppm
5 ppm
50 ppm
Remark: Reporting limit = Quantitation limit of analyte in sample
Page 4 of 7
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Number : TWNC00217908
Test Conducted
(Ⅳ) Measurement Flowchart:
Test for Cd/Pb/Hg/Chromium (VI)/PBBS/PBDES Contents
Reference Standard: IEC 62321 edition 1.0:2008
Sample preparation
For non-metal part
For metal part
Take sample and immerse into Aqua Regia, start to strip plating layer
Stop the stripping procedure upon color change completely
Take the Aqua solution as plating component and stripped body as substrate component
Cd/Pb/Hg
Cr
Confirm the tested
samples are
totally dissolved
Make up with
deionized water
PBBs/PBDEs
Polymers /
electronics
Metal
For different
material, digest
the sample with
*1
appropriate acid
6+
Weigh sample and
add organic solvent
By spot test
Negative
Get 50cm2 sample
By boiling water
extraction
*2
Weigh sample
and add
alkaline
solution
By Soxhlet
extraction or
Solvent extraction
Definite temp.
extraction
Cool and filter
the extract
Analyzed by ICP-OES
Concentrate the
extract and make up
with organic
solvent
Analyzed by GC-MSD
Make up with deionized
water and add diphenylcarbazide solution
Remarks:
*1: List of Appropriate Acid:
Material
Polymers
Metals
Electronics
Analyzed by UV-VIS
Acid Added for Digestion
HNO3,HCl,HF,H2O2,H3BO3
HNO3,HCl,HF
HNO3,HCl,H2O2,HBF4
*2: If the result of spot test is positive, Chromium VI would be determined as detected.
Page 5 of 7
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Number : TWNC00217908
Test Conducted
(Ⅳ) Measurement Flowchart:
Test for Halogen Content
Reference Standard:EN 14582
Sampling/grinding or
cutting
Add absorbent in a
combustion flask &
place weighed sample in
equipment
Fill oxygen into
calorimetric bomb
Ignite then leave the
flask at room
temperature
Transfer the absorbent
into a volumetric flask
Make up with deionized
water
Analyzed by ion
chromatography
End of Report
Page 6 of 7
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Number : TWNC00217908
Test Conducted
Photo
Page 7 of 7
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
,Fl|s,#+
fitq(No.)
TestReport
: cE/2Q\2/ roa34
E *(Dare)
: 2ai.2/a1/1z
Validit
nown
ForQuegll
Plea€eCo
ithscs
F*.(page) : l o f l 0
ELSCHI'{Oi' ELEKTROSChUTZ(OVPONEMENBAU
CVBH
GEI'ERBESTMSSE 87, D-98669 VEILSMRF. GERVANT
trTi{*&efi*8P
idetrtifi€d
bylo!
't*,
!eb.lf
IlIttfllfltflI
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of the clienr
TINNED VIRES
:Il:{,JklE1(resri ir Pe'i od)
20L2/I/4
Results)
:
s a n pI e s r a 6 / r e r e
subdi t ted and
as) :
&S3+*(s..pl. Descriptio.)
11"9"4fi(sryl€/I temNo.)
,FA El(corntry of o.isin)
{i?t A lq (sanpI e ReceivinsDate)
trl*,*+(Test
(The fol lovina
1E+445F (Pr-EAsE
REFER
To PAGE
5)
(cERrl,{N"f)
€El
2012/t1
/
:* {,T-F
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( P r e d . er e I € r r o n e x r p a s P , )
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itIS(N6. ) : cE/2012l10834
qs(DaLe): uol2lot/tl
n*(pa8e) : 2 oI r0
ELSCIIU(OTI
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87, D 98669 \'EIISMRF, CERN,{IY
idLg*(Test
llfllflNl[lttutl
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;FJiT4,'i (PARTNANE)NO.1 :
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No.1
++IEc 62321t2008rt1, ,r(&Alt
A€*4+**f
tE;*d,i*,r|. / nitr'
.eference ro IEC 62321: 2008 aid
perforned by ICP-A'S.
tE / r.ad (Pb)
2oo8tti, /64*
++rFE 62321,,
A€*,.f +*+lrt r*A*,!i. / wirh
68
.efer€nce ro IEC 6?321: 2008 and
by ICP-AXS.
perforn€d
*. / vercury (Hs)
2008t:1, ,xdA**
t-+rFN 623211
A€t.6+*4trb*Al*,r,.
/ lvith
ref€renc€ ro IEC 62321: 2008 and
by ICP AXS.
perforn€d
n1!r$
/ Hexaralentchro6iun cr(vl)
t-trFr
62321:2oo$rit , ,]lih'K+
/ iri rh ief erence to tEc
*.*l*;rl.
6 2 3 2 1 , 2 0 0 Aa n d p e r f o r n e d b y
B oi t i n s ' a i € r € x t r a c t i o n l t e t h o d . #
An+B,*&
/ Perfl uo!ooctane
s u l f o n a t e s ( P F O S - A C i dv, e t a l s a l r ,
4+us EPA3510c,1996rii, ,(ri
l0
rE,?ffl(+dis;r'lafi.+Edda*.
/ Sit! reference io US EPA 3540C:
1 9 9 6 n e t h o d l o r P F O SC o ! r e n r ,
Analysis vas pe.fo.ned by tClMS.
an+6(r4)
/ PFoA(cAsNo.: 335-6?-
4+us EPA3b1oc,r996til,
,x,t
t0
€,?{ f, rt&l*,fl }n+d.(r*) 6t
1)
/ r / i t h r e f e f e n c e i o u s E P A3 5 1 0 c
1 9 9 6n c t h o d f o r P F o Ac o n t e n t .
Analysis {as peiforned 6y rc/MS.
ri
comranY
I i
lrr'lr'i
i ,.'irl;l nii
:
rysub]dlo6cene6cdd|to^3ds
rr,u :.i t:r rirJr,,r.s6Lo?rrq
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rfla#+
TestReport
*4(No. ) : cE/2012l10834
a&(Date) : 20r2/or/r2
F*.(par€) : 3 of ro
E-scllUKOIl ELE(TROSCHUTZI(oIPONENTEN&{U
GItsH
CEWE&BESTRASSE
87, D 98669 VEITSDoRF, GERII,AI\'Y
*litit E
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h
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+41F. 62321.2aa9t)*, ,)rfulaE
-*d,&xi. / rt/ith.ererenc€
fid,/f
ro IEC 62321.2008 and p€rforned
by CC/MS-
/ suo of PBDEg
ttlt*r|trfr
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/
/
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/ H € x a b r o n o d i D h e n v Le t h e r
ether
D i b r o n o d i D h e n r le t h e r
IribroaodiDlenvl ether
T e t r a b r o m o d i p h e neyt h
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P e nr a b r o m o doi h e n v l e t h e r
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/ o c t a b r o m o d i D h e n vel t h e r
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No.:14762-91-8)
&+ (S,) / Halosen-chlorine (cl) (cAS
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(;*) / Halogen-Brosi.e(8.) (cAs
6*
{o.: r0097-32-2)
& * ( 4 ) / H a l o s € n - I o d i n (eI ) ( c a s
!o.: 14362-44-8)
50
n8/k8
,/,*L+Ett
++Bs ENr4FB2,?!Jo7,
50
r ,litt' ref €rence to BS s*
&i*1.
I 4 5 8 2 : 2 0 0 7A. n a l y s i ss a s
50
50
nPb(s) bdad *€ ra$ Gpod enior b
.r
r . , l r . , r i
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1. , . ! l 1r r . : r ,
rh s dofumeil ts 'sued 6y $e co6p'
9 u b j . c l l o ] € m s 6 i d c o i d l o n s i o r E A h e f r o n € d a w i l o h s ] m { d o n d : b l l y
! idr( d zoiq N?!riiF clr tiiwd r]i : r!rt r r!
r:{i!.l,rrh}s6iorr,
fi|fi,+r+
TestReport
*€(No. ) : cE/2012l10834
AA\Date) : 20r2/0r/r2
Fg.(pase) : a of 10
E-sCIruIOU ELB<TROSCHUTZKOIIPOIIENTINB,{U
GMBH
GESERBESTRASSE
87, D-98669 VEItsDoRF, GIRMANry
tI|||l||lt][trt|l!
f,li(Note):
r . n s l k 8: P p n ;0 . l n t %: 1 0 0 0 P P n
2 . n . d . = N o r D e t e c r e (d, f t . A * )
3. MDL= MerhodDere.rionLioit (t*.l*tFltsfE.ti)
4. '-' : Noi Res'1.r.d (**n*.i4.)
5 . . . : Q u a l i r a t i v ea n a l y s i s( N oU n i t ) . t , E r > r 4 G R + A )
6. #:
a . P o s i r i v e m e a n s r b e p r e s € n c eo f C r V I o n t h e t e s r e d a r e 2 s
(posi r i vei.6n,l:d, E&jA ;Flr|l ,r.ll J} )
b. Nesative means th€ abs€nce of C.VI on tle
( Negar i veA + jr,l:i, E }{ ^.fi '4lr,j ,rllj*
tesred areas
)
T l e d € t e c t e dc o d c e n t . a t i o ni n 6 . i r i n s _ q a r e r - e x t r a c i i o sn o l u r i o n i s e q u a Lo r g r e a t e . t h a r o , o 2 o g l k g w i t h
s0 csr tesred ar"a", / it8ii;AA=o.02
na/ks uiih 50 cm?(tested areas)
7- *tsiitrl:{€I,'A
f ;6^*,tEAtslit
' lE*f tli&A)rl:t}: *.ir1ti.4 f tEfl+-+iJ{ t.l+&.
(Tn€ sanples vas/sere analyzed on b€nalf of rhe applicanl
resulls sas/-€re only giv€n as rh€ info.naliry value.)
as nixing
sanple i.
one resring.
Tle above
8. ttr)*E+4c.f\2orzlor
/ rrir'tt *gcE/20t2/tos3l&+.
( T h i s r e p o r t s ! p e r s e d e s t h e p r e v i o r s d d . u D e n tb e a r i n g r h e r e s r r e p o r t n u m b e rC E / 2 0 1 2 l 1 0 8 3v4h i . h v a s
i s s u € do n 2 0 1 2 l 0 1 / 1 1 . )
Plost+
fin (R.f.'.nce
InJoraa!ion) | )A+ 2006/r22/M (Dltecrirc
2oo6/t22/w,
(r) Ji&( 4;rfl +t4_Ld.&n r{.++**rlfd.aeflrt+€g;ia+,a*.rJi+o. oo5%.
(May not be placed on rhe oarket or used as a substaace or constituent
equal to or higher than 0.005 % hy hass.)
of Dreparaiions in a conc€n!ra!ion
(2r r hy4rr &*fi 8!at+d.s{.ff tr"d.4b4; 1Rri+t+}3EH*.4{ pFoss49€-.r*fi}a&hii€}g4pFos6i
j'*.P!osAA}.{tf f 5g+,i4,*.ji'ifrug/.r.
,tA++t A,Ao.t%, fi,rt,{'sd.*{tt$*rtr,
(Nay not be Placed on rh€ narket in seEi-finished products or arricles, or parts rh€reof, if the
conc€n1.ation of PFOSis equal to of hiChe. than 0.1 % by nass calculared virh r€ference to the nass oI
s t r u c t u r a l l y o . m i c r o s t r u c t u r a l l y d i s t i d c i p a ! t s t h a t c o n t a i n P F O So r , f o r t € x t i l e s o r o t l e r c o a t e d
naterials,
if
the a'iount of PIOS is equal to or Iigher
cmoanyr:fr111r! Lll i.,ri,j.,lnlr.i i: i.tri
li,,!,Ll\
i.r
than 1Ug/n? of the coated nareriaL.)
4.r ir,rtr,,!.
fil-d,+E+
it6(No.)
Test Report
: cEl2012lI0834
Aq(Date)
, 2012/01/12
ELSCI1UKOM
ELEKTROSCHU']'ZKONPONENTENBAU
CMBH
GEIERBESTRASSE
8?, D-98669 \'EILSDORF, CETMI\Y
tlB4lt
: 5 of t0
F]R(p,s")
t||uI|
(siyle/ I !€n No.)
(A-1) 101 - - 2?1.0 - - - -tinned copperwi.e-Cu, Sn %
(A-2) 101 - - 283. 0 - - - -tinned.opper clad wire-El.on 30, Sn - - %
- - -tinned copper clad wirc-Elcon F, Sn - -%
(A-3) 101 272.0_
_
(A-4) 101
281. 0 - - - -tinned copper clad wi.e-ElconD, sn - - %
(A-5) 101(A-6) 101 (A-?) l0l _
(A-8) I0l -
- 221,.0 - - - 24-. O - - - 257,0
- - 232. 0
-
(A-9) 101 - -234.0(A-10) 10r- - 255. (A-11) 101- - 229. (A_12) 101- - 235. (A-13) r01 - 23r. (A-14)r01
cmpaiy;,.
r,
llr'r:
-rinned
-tinned
-rinned
- - -ti.n€d
- -
-tinned
- - - -tinned
- - - -tinned
- - - -tinned
236.----
i
-tinned
: ,l.lj,lilr+
copper nickel alloy ui.e-CuNi{4, Sn - -%
s i l v e r p i a t e d c o p p € rF i r e - c ! ,
As--%, sn -- %
brass vire-Ct802n20, Sn - - %
silver copper aitoy vir€-Ascu50, Sn
%
s i l v e r c o p p e r a L L o yw i r € - A s c u g o , s n - - % ( E l c u g o , s i
coppe. zinc aLloy pire-Cu702n30, Sn - - %
c o p p € r n i c k e l a L L o yr i r e - C ! N i 1 2 , S n - - ,
%)
s i l v € r . o p p e r a L L o yv i r e - A g 7 2 c u 2 8 , s n - - ,
- %
wire-A81000, sn
sitver
- t i n n e d s i t v e r c o p p e ra l l o y
r.ril
-
l+!r,]].
"ire
P]BG)bsbd rh 3 bi cPod €nnd e
r 4, L|\i.
poigb't}6lobcl€daodhsdgm
A s 4 5 c u 5 5s. n -
- % ( A g c u s 5S, n )
]||lr]|lt
,Ff'd,*E+
Test Report
itS(No. ) : cE/2Or2l10834 a*(Date) : 2ar2/a1/L2 F*(P.8.)
EI-SCHLXOM
ELEKTROSCHUTZ.(OVPOMNTENBAU
CVBII
GEFMBESTMSSE87, D-98669 VEIT^SDORF,
GEL\!AIry
|r []t
. ( ilt jtjrt i{t* ff + ) / Thes€sampt€€
illi,rTdt )i.a tr ai*r+ ' tls e,tt*tt
we€
dissolvEdlolalt by pHonditioning methodaccoftting10betM no/r ch€rt. ( CP testm€thodexcluded)
4 ir, d^ I : lr.Ett / Nameof the pe6onwio ftade m€surement ctimbs€aryans
3) )rlll fi I ^ : tl,l|^ / Nameorthe p€Bonin chaBeol measu€mentTroyChans
. Peporation
/ Cutting
t{.'1.*{*.9
dq$slil
/ sampleMe*uemenr
fti{ r E*.s n{ { 6,} !! f,.0 *i3li,I &(r,T*.
rf +) / rdd dtg€slion
bysuitaueaciddep€nded
d
(asbetowtabte)
diffe€ntsamplsmateriat
d &/I &/i. s.*at&tit ib /
Micwve digestian
wnhHNoJHct/HF
j!ti l{ it +
,, t*4iitE&
+. / Heatro appropnab
1) &8fi;4 /AlkaliFudon
2) i*t8t+ / HCllodissoh€
rgrt'rst*,*+*4.Jt,rlfl
*.sltrf
/ ICP-AES
/ sampleMatedal
S1eel.coooer.aluminum.solder
/ Cool,
AftlirQ*{'s
nllel digeclaleomugh liher
/ oiqestion
Add
tXib*&&t
.at! sr!, !at, i.f.*, !*.+ /
Aquareqia,
HNOrBCl,HF,H,O,
e\*eilf,e
/Add
/ HNO:,/HF
4&,1Rt
/*tlX-a A,kk1+t't
tl*eatta 54onmAt4
Gold.Dlatinum,
Dalladium.
c6'dmic
.t&, ttr.+, drn, 4.t / HzsorH:o, HNo:,HCI
rF\4+t;r&7?aa4
4atedb16Geie€rcodroisot
| Anyacidlo lotal dbestion
s
3polgb'ty6lo'9c'd'ddh6e!
ab6dban@ al 540 nm by
UV.VIS
fllr
,t{'d,+E+
Test Report
it4(No. ) : CE/2012lr0834 A * ( D a r e )
. 2072/07/t2
F*(P.g.)
ET.SCHU(OM
ELH(TRG5CHU1'ZKOMA)NEMENBAU
GI{BH
GEAERBESTI.ASSE
87, D.98669 VEILSDORF.GERVAIY
t*i+/
tmrum tlltmr
/ PBB/PBDE
analytlcal
FLOwCHART
t*i&g,.&*,€ll
r ;il$r'.t : 4iir# / Nameoflh€peEonwhomademeasurcment:
RomanWong
r FIE\A l/\ : 'E-** / Nameof thepersonin chaEeof measurement
TroyChang
---------+
?r^,rli{fll / Firsttestingproc€€s
1ti*la$*€,+ / oplional
sc€[email protected].
SrS{1,l / ConfnnalionDrcGs - . - .)
Sc.eenanalys's/ir$
"+4
I
I
Sampleext€c1ionSa;+*.-/
Soxhleimethod*1.++t*
Concenvate/Dilute
Extracl€dsolution
sfrR;i*ffif
Filter/ +F enli&
Analysis
by GCAIS/ *,IAEf|ii'*it+4
c o m e a !n: v
',1,
r. 1i)rr.l
,arr,:.
.rii
i:!l-li,
p3(s)bsradrb s rad Gponeniorb
,.r,'r\l!.
|
|
rl|a*E+
Test Report
*tq(No.) : cEl2012/lo83a A*$are)
| 2.r12/or/r2 q&(pase) : 8
ELSCIIU(OMELEKTROSCHUTZKOMPONENTENBAU
CMBH
CEIERBESTRASSE
8?, D-98669 I'EIISDORF, GERM,{NY
f *+*tr;t€f
I
I
"f
l0
lflmf]t
/ Analyticalflow chadof hatogencontent
irl-J,/.F : tt,g+ / Narneof thepe6:onwhomademeasurement
RitaChen
lll$A t,t. : Ji.*q / Nameof thepersonin chargeof measurement:
TroyChang
*+nfr6N{r I
Analysiswasperformedby IC
c o m r att u , . ) ) i , t . , , t I
t'r,, r.:jr
i r l r : l ir
1 .'
ir'rl
Thsfume.ls'$uedby6ecompani9b]edlo'BGenelaco|dtoisds!8lolac3sftalWsgscom[em
abnron 6 dawi ro rh. miaioi or abit
suq6d ro r.ms aid coid$o.s ro, E
!hds(D|7omN4'!pd(ur!w!i/N
lttlfil
,t{-d#+
TestReport
itt6(Yo. ) : cE/20r2/r0834
*(D"r")
, 2or2/ot/12
FjF.(pase): 9 or to
ELSCHUKOM
ELE(TROSCHUTZKONPONENTENBAU
GMBH
GEi'ERBESIIASSE87, D-98669 IIEII,SDORF, GRMA\Y
lfll[l]
*{+F)ffX,ar
/
Analyticalflow chat of 50)6tetextraction(LC/MS)procedu.e
r
r
i{l- F : ff 41, / Nameof the personwho mademe€surement:
RomanWong
fl:{A t,\ : tFr'34 / Nameof thepersonin chargeof measurementt
TroyChang
(rdn,iE: aF.+*,*rn/an+t(*), **:"+fitb+& /
Test ltem3: PFOS/PFOA ' Benzotriazole)
,tf
' r _ l l r , . ri r l / : r f i i r . ! 7 i l f r r t )
!bG) r8*d
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