ICP Test Report Certification Packet
Company name :
Littelfuse, Inc.
Product Series:
250V UMF SB
Product #:
465xxx Series
Issue Date:
May 7, 2012
It is hereby certified by Littelfuse, Inc. that there is neither RoHS (EU Directive
2002/95/EC)-restricted substance nor such use, for materials to be used for unit parts, for
packing/packaging materials, and for additives and the like in the manufacturing processes.
In addition, it is hereby reported to you that the parts and sub-materials, the materials to be used
for unit parts, the packing/packaging materials, and the additives and the like in the manufacturing
processes, are all composed of the following components.
Issued by:
<Global EHS Engineer >
(1) Parts, sub-materials and unit parts
This document covers the 250V UMF SB RoHS-Compliant series products manufactured
by Littelfuse, Inc.
＜ Raw Materials Used
Please see Table 1
(2) The ICP data on all measurable substances
Please see appropriate pages as identifed in Table 1
Remarks：
Pb (lead) contained in the high temperature melting solder > 85% and is categorized as
exempt under section 7a of the RoHS Annex.
Form 585-047 Rev. A
1
2/21/06
Table 1: List of Raw Materials covered by this report
Total Parts
1
2
3
4
5
6
7
8
Raw Material Part Number
910-261
909-423
082xxx-001
082xxx-001
692323
648112-00x
425809
425809
Raw Material Description
Cap (Metal)
Body
Element – Cu99.9MSn
Element - Cu CDA102 Sn Plated
Solder
Yarn
Ink – RoHS 6 & Halogens
Ink – RoHS 2
2
Page(s)
3-7
8-13
14-20
21-25
26-30
31-36
37-45
37-45
Test Report
Applicant:
Number : TWNC00233552
Littelfuse Philippines Inc.
LIMA Technology Center, Lipa City,
Malvar, Batangas
Date
: Nov 24, 2011
Sample Description:
One (1) group of submitted samples said to be :
Part Description
: Cap
Part Number
: 910-261
Date Sample Received
: Nov 21, 2011
Date Test Started
: Nov 23, 2011
Test Conducted :
As requested by the applicant, for details please refer to attached pages.
Authorized By:
On Behalf Of Intertek Testing Services
Taiwan Limited
K. Y. Liang
Director
This report shall not be reproduced
except in full, without the written
approval of the laboratory.
Page 1 of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00233552
Test Conducted
(Ⅰ) Test Result Summary :
Result (ppm)
(1)
(2)
Test Item
Heavy Metal
Cadmium (Cd) content
Lead (Pb) content
Mercury (Hg) content
Chromium VI (Cr6+) content (mg/kg with 50cm2)
7
9
ND
Negative
(< 0.02)
ND
ND
ND
Negative
(< 0.02)
Remarks: ppm = Parts per million based on weight of tested sample = mg/kg
ND = Not detected
<
= Less than
mg/kg with 50cm2 = milligram per kilogram with 50 square centimetre
Negative = A negative test result indicated positive observation
was not found at the time of Test.
Tested Components
(1) Dark Brown Metal Base Material
(2) Silvery Plating Layer
Responsibility of Chemist : Irene Chiou / Kevin Liu
Date Sample Received
Test Period
: Nov 21, 2011
: Nov 23, 2011 To Nov 24, 2011
(Ⅱ) RoHS Requirement:
Restricted Substances
Cadmium (Cd) Content
Lead (Pb) Content
Mercury (Hg) Content
Chromium VI (Cr6+) Content
Limits
0.01% (100ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for
homogeneous material.
Page 2 of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00233552
Test Conducted
(Ⅲ) Test Method:
Test Item
Cadmium (Cd)
content
Lead (Pb) content
Mercury (Hg)
content
Chromium VI (Cr6+)
content
Test Method
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 7, by microwave
digestion until the tested samples are
totally dissolved and determined by
ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in annex B, by boiling water
extraction and determined by UV-Vis
spectrophotometer.
Reporting Limit
2 ppm
2 ppm
2 ppm
0.02
mg/kg with 50cm2
Remark: Reporting limit = Quantitation limit of analyte in sample
Page 3 of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00233552
Test Conducted
(Ⅳ) Measurement Flowchart:
Test for Cd/Pb/Hg/Chromium (VI)
Reference Standard：IEC 62321 edition 1.0:2008
Sample preparation
Take sample and immerse into Aqua Regia, start to strip plating layer
Stop the stripping procedure upon color change completely
Take the Aqua solution as plating component and stripped body as substrate component
Cd/Pb/Hg
Cr
Polymers /
electronics
Metal
For different
material, digest
the sample with
*1
appropriate acid
By spot test
Negative
Confirm the tested
samples are
totally dissolved
Make up with
deionized water
6+
*2
Weigh sample
and add
alkaline
solution
Get 50cm2 sample
Definite temp.
extraction
By boiling water
extraction
Cool and filter
the extract
Analyzed by ICP-OES
Make up with deionized water and add
diphenyl-carbazide solution
Remarks:
*1: List of Appropriate Acid：
Material
Polymers
Metals
Electronics
Analyzed by UV-VIS
Acid Added for Digestion
HNO3,HCl,HF,H2O2,H3BO3
HNO3,HCl,HF
HNO3,HCl,H2O2,HBF4
*2: If the result of spot test is positive, Chromium VI would be determined as detected.
End of Report
Page 4 of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00233552
Test Conducted
Photo
Page 5 of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Test Report
Applicant:
Number : TWNC00233547
Littelfuse Philippines Inc.
LIMA Technology Center, Lipa City,
Malvar, Batangas
Date
: Nov 28, 2011
Sample Description:
One (1) group of submitted samples said to be :
Part Description
: Body
Part Number
: 909-423
Date Sample Received
: Nov 21, 2011
Date Test Started
: Nov 22, 2011
Test Conducted :
As requested by the applicant, for details please refer to attached pages.
Authorized By:
On Behalf Of Intertek Testing Services
Taiwan Limited
K. Y. Liang
Director
This report shall not be reproduced
except in full, without the written
approval of the laboratory.
Page 1 of 6
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00233547
Test Conducted
(Ⅰ) Test Result Summary :
Test Item
Result (ppm)
Grey Material
Heavy Metal
Cadmium (Cd) content
Lead (Pb) content
Mercury (Hg) content
Chromium VI (Cr6+) content
Polybrominated Biphenyls (PBBs)
Monobrominated Biphenyls (MonoBB)
Dibrominated Biphenyls (DiBB)
Tribrominated Biphenyls (TriBB)
Tetrabrominated Biphenyls (TetraBB)
Pentabrominated Biphenyls (PentaBB)
Hexabrominated Biphenyls (HexaBB)
Heptabrominated Biphenyls (HeptaBB)
Octabrominated Biphenyls (OctaBB)
Nonabrominated Biphenyls (NonaBB)
Decabrominated Biphenyl (DecaBB)
Polybrominated Diphenyl Ethers (PBDEs)
Monobrominated Diphenyl Ethers (MonoBDE)
Dibrominated Diphenyl Ethers (DiBDE)
Tribrominated Diphenyl Ethers (TriBDE)
Tetrabrominated Diphenyl Ethers (TetraBDE)
Pentabrominated Diphenyl Ethers (PentaBDE)
Hexabrominated Diphenyl Ethers (HexaBDE)
Heptabrominated Diphenyl Ethers (HeptaBDE)
Octabrominated Diphenyl Ethers (OctaBDE)
Nonabrominated Diphenyl Ethers (NonaBDE)
Decabrominated Diphenyl Ether (DecaBDE)
Halogen Content
Fluorine (F)
Chlorine (Cl)
Bromine (Br)
Iodine (I)
ND
34
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Remarks: ppm = Parts per million based on weight of tested sample = mg/kg
ND = Not detected
Responsibility of Chemist : Irene Chiou / Kevin Liu / Cathy Chen
Date Sample Received
Test Period
: Nov 21, 2011
: Nov 22, 2011 To Nov 25, 2011
Page 2 of 6
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00233547
Test Conducted
(Ⅱ) RoHS Requirement:
Restricted Substances
Cadmium (Cd) Content
Lead (Pb) Content
Mercury (Hg) Content
Chromium VI (Cr6+) Content
Polybrominated Biphenyls (PBBs)
Polybrominated Diphenyl Ehters (PBDEs)
Limits
0.01% (100ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for
homogeneous material.
(Ⅲ) Test Method:
Test Item
Cadmium (Cd)
content
Lead (Pb) content
Mercury (Hg)
content
Chromium VI (Cr6+)
content
Polybrominated
Biphenyls (PBBs)
Polybrominated
Diphenyl Ethers
(PBDEs)
Halogen Content
Test Method
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 7, by microwave
digestion until the tested samples are
totally dissolved and determined by
ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in annex C, by alkaline
digestion and determined by UV-Vis
spectrophotometer.
With reference to IEC 62321 edition
1.0:2008 in annex A, by solvent
extraction and determined by GC-MSD
and further HPLC confirmation when
necessary.
With reference to IEC 62321 edition
1.0:2008 in annex A, by solvent
extraction and determined by GC-MSD
and further HPLC confirmation when
necessary.
With reference to EN 14582:2007 by
calorimetric bomb with oxygen and
determined by ion chromatography
Reporting Limit
2 ppm
2 ppm
2 ppm
1 ppm
5 ppm
5 ppm
50 ppm
Remark: Reporting limit = Quantitation limit of analyte in sample
Page 3 of 6
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00233547
Test Conducted
(Ⅳ) Measurement Flowchart:
Test for Cd/Pb/Hg/Chromium (VI)/PBBS/PBDES Contents
Reference Standard: IEC 62321 edition 1.0:2008
Sample preparation
For non-metal part
For metal part
Take sample and immerse into Aqua Regia, start to strip plating layer
Stop the stripping procedure upon color change completely
Take the Aqua solution as plating component and stripped body as substrate component
Cd/Pb/Hg
Cr
Confirm the tested
samples are
totally dissolved
Make up with
deionized water
PBBs/PBDEs
Polymers /
electronics
Metal
For different
material, digest
the sample with
*1
appropriate acid
6+
Weigh sample and
add organic solvent
By spot test
Negative
Get 50cm2 sample
By boiling water
extraction
*2
Weigh sample
and add
alkaline
solution
By Soxhlet
extraction or
Solvent extraction
Definite temp.
extraction
Cool and filter
the extract
Analyzed by ICP-OES
Concentrate the
extract and make up
with organic
solvent
Analyzed by GC-MSD
Make up with deionized
water and add diphenylcarbazide solution
Remarks:
*1: List of Appropriate Acid：
Material
Polymers
Metals
Electronics
Analyzed by UV-VIS
Acid Added for Digestion
HNO3,HCl,HF,H2O2,H3BO3
HNO3,HCl,HF
HNO3,HCl,H2O2,HBF4
*2: If the result of spot test is positive, Chromium VI would be determined as detected.
Page 4 of 6
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00233547
Test Conducted
(Ⅳ) Measurement Flowchart:
Test for Halogen Content
Reference Standard：EN 14582
Sampling/grinding or
cutting
Add absorbent in a
combustion flask &
place weighed sample in
equipment
Fill oxygen into
calorimetric bomb
Ignite then leave the
flask at room
temperature
Transfer the absorbent
into a volumetric flask
Make up with deionized
water
Analyzed by ion
chromatography
End of Report
Page 5 of 6
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00233547
Test Conducted
Photo
Page 6 of 6
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
scs
Validit
ForQueSti
PleaseCo
I
TestReport
No.: CE/2011/84950
D e | 2011112101
POLYFIL
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OBERALLMENDSTMSSE
2OA,CH€3OO
ZUG/ SWITZERLAND
Cu99.9MSn
'1'14595
lest Result(a)
Plea6e efer to next page(s).
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Thefollowingsample(s)was/w6resubmittedand identifiedby/onbehalfoftheclientas:
S€mpleDescription
Buyer/OrderNo.
SampleReceiving
Date
TestingPeriod
nown
b
TestReport
No.:CE/2011/84950
Page'.2of 7
Dale:2O114ZO1
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POLYFILAG
OBERALLI\4ENDSTRASSE
2OA,CH63OO
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I]
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T66i R.6ultls)
THE PLATINGLAYER)
SILVERCOLOREDMETALWIRE(INCLUDING
PART t.lAME No.1
Unit
Te3t lt6m(s)
Cadmium(Cd)
Lead(Pb)
MDL
Method
mg/Kg
reterence
to IEC62321r
2008and
mgKg With
perfomed
Mercury(Hg)
byICP-AES.
mS/kS
Hexavalent
Chromium
Cr(Vl)
Withreference
to IEC62321:2008and
pedormedby Boiling\r€terext€ction
Method.#
Sum of PBBS
Monobromobiphenyl
5
5
5
5
Dibromobiphenyl
Tribromobiphenyl
Tetrabromobiphenyl
Pontabromobiphenyl
Hexabrcmobiphenyl
Heptabromobiphenyl
Octabromobiphenyl
Nonabrornobiphenyl
Dec€bromobiphenyl
Sumof PBOEa
Withreference
to IEC62321:2008and
mgikS perfomed
by GC/MS.
5
5
5
n.o.
n.d.
n.d.
n.d.
n.d.
n.d.
5
5
Pentabromodiphenyl
ether
Hexabrcmodiohenvl
ether
Heptabromodiphenyl
ether
Octabromodiphenyl
ether
5
5
Nonabromodiphenyl
ether
5
5
Decabromodiphenyl
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Test Report
No.: CE/2011/84950
Page:3 of 7
Date| 2011h21O1
POLYFILAG
2OA,CH€3OOZUG / SWITZERLAND
OBERALLMENDSTRASSE
Test ltem(s)
Halogen
(F)
Halogen-Fluorine
(CASNo.:14762-94-8)
(Cl)
HalogenChlodne
(CASNo.:22537-1s1)
(Br)
Halogen-Brcmine
(CASNo.r10097-32-2)
(l)
Halogen-lodine
(CASNo.i14362-44-8)
Unit
mg/Kg
tl]tIlltltfltttlt
method
Withreference
to BSEN M5A2,2007.
Analysiswasperfomedby lC.
MDL
Result
No.1
50
n,o,
50
n.d.
50
n.d.
50
n.d.
Note :
1. mg/kg= ppm : 0.1wf/6= 1o00ppm
2. n.d.= NotDetected
3. MDL= MethodDetection
Limit
4-"-"=NotRegulaled
(Nounit)
analysis
5. '" = Qualitative
6. # = a. Positivemeansthe presenceof CrVlon the testedareas
b. Negativemgansthe absenceof C l on the testedareas
Thedgteci€dconcentration
in boiling-lvater-ext€ction
solutionis equalorgreaterthan
0.02mg/kgwith50 cm,
testedareas.
7. Thesample(€)
was/wer6
analyzed
on behalfoftheapplicant
as mixingsamplein onetesting.Theaboveresult(s)
was^^/€re
onlygiv€nas theinformality
value.
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es
Test Report
No.: CE201'1/84950
OaL .2011h2,01
Pager4
POLYFILAG
2OA,CH63OOZUG / SWITZERLAND
OBERALLMENDSTRASSE
methodaccordingto belo\/ flo /
1) Thesesample6were
da66olved
totallyby pre-conditioning
aCf' test methodexcluded)
Climbg€atYang
Nameof the pe6onwho mademeasurement:
TroyChang
3) Nameofthe pe6onin chargeof measurement:
acid
Aciddigestion
by suitable
dependedon difierentsample
mderial (as belo\, iable)
Micro\ravedigestionwith
HNO/HCVHF
Heatto appropriat€
to e,\tract
temperature
1) AlkaliFusion
2) HCltodissolve
Cool,filterdigestate
filter
through
ICP-AES
SampleMaterial
Dige€tionAcid
sold€r
S1eel,
copper,aluminum,
Aqua regia,HNO3,HCl,HF,HrO,
Glass
HNO3/HF
cold, platinum,palladium,ceramic
Aqua regia
Silver
HNO3
Plastic
H2SO1,HrOr,HNq, HCI
Othe.s
Anyacidto totraldigestion
ii. irei,.or if *q
at 540 nm by UV-VIS
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TestReport
Page:5 of 7
Oale'.201lh2lo1
No.: CE2011184950
tl
POLYFILAG
2OA,CH43OO
ZUG/ SWITZERLAND
OBERALLI\4ENDSTRASSE
PBB/PBDEanalyticalFLOWcHART
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TestReport
No.: CE/2011/84950
Daie | 2011h21O1
POLYFILAG
2OA.CH-6300ZUG/ SWITZERLAND
OBERALLMENDSTRASSE
Analyticalflow chartof halogencontent
RitaChen
1) Nameof thep€rsonwholmde rneasuredEntr
2) llan€ of the personin chargeof nEasurerEdt:Troy Chang
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Page:6 of 7
Test Report
No.: CE/2011/84950
Paget 7 of 7
D€te 2011h2101
POLYFILAG
OBEMLLMENDSTRASSE2OA,CH63OOZUG / SWITZERLAND
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TestReport
No.TSNEC1110357903
Date:26 Oct 2011
Page1of 5
TIANJINBAIRUIJIEWELDINGIJATERIALCO.,LTD.
NO.38,BAOYUAN
ROAD,EASTZONEOF JINNANDEVELPOPMENT
ZONE,JINNAN
DISTRICT,TIANJIN
CHINA
The followingsample(s)was^/vere
submittedand identifiedon behatfof the clientsas : TIN-COATEDCOppER
WIRE
TP11-0021
84- TJ
Cu
210d2011
21ocl2011-26 ccl2011
SGSJobNo.:
Composition
:
DateofSampl€Received
:
TestingPeriod:
TestRequested:
Selectedtest(s)as requestedby client.
TestMethod:
Pleasereferto nextpage(s).
TestResulb:
Pleasereferto nextpage(s).
Basedonthe performedtestson submittedsamples,the resultsof Lead,
I\rercury,
Cadmium,
Hexavalent
chromium,
Polybrominated
(pBB),
biphenyls
Polybrominated
diphenyl
ethe6(PBDE)
compty
withthelimitsas setby RoHS
Directive
2011l65/EtJ
Annexll; recasting
2002/95/EC.
Conclusion
:
Signedfor and on behalfof
scs-csTcLtd.
;@ReabecaZhou
ApprovedSignatory
ku. m qEr or rr.dd.
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s 5$r.b€!F.M
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couD{sossA)
TestReport
No.TSNEC1110357903 Date:26oct 2011
Page2 of 5
TestResulb:
TestPadDescriotion
:
SpodmenNo.
I
SGSSamdelD
D6.*iptbn
TSN1l -103579.002 sjtverymetatwire
Remal}6 :
(1)I mgftg=l PPm=0.0001%
(2)MDL= lrethodDetedionLimit
(3) ND = NotDetecled( < MDL)
(4)'-" = NotRegulated
RoHSIDllEdive201I,/8AEU
Testllethod : Withreferenceto IEC6232't:2008
(1)Determination
of Cadmium
by tCp-OES.
(2)Detemination
of Leadby |CP-OES.
(3)Determination
of [,lefcury
by tCp-OES.
(4) Deteminationof Hexavalent
Chromiumby Spottest/ Colorimetric
MethodusingUV-Vis.
(5)Determination
of PBBS/ pBDEsby GC-MS.
Test ltem(s)
Cadmium(Cd)
Lead(Pb)
lllercury (Hg)
Hexavalent
(C(Vl))
Chromium
Monobromobiphenyl
Dibromobiphenyl
Tribromobiphenyl
Tetrabromobiphenyl
Pentabromobiphenyl
Heptabromobiphenyl
Octabromobiphenyl
Nonabromobiphenyl
Decabromobiphenyl
Sumof PBOES
Monobromodiphenyl
ether
tjDj!
10O
1,000
1,000
Unit
mS/Kg
ms/Ks
mg/kg
1,000
_
-
mg/kg
mg/Kg
mg/Kg
mg/Kg
mg/xg
mg/(g
ms/Kg
mg/Kg
mgks
mdks
mgKg
msu4a
mgKg
1,000
-
lo.d [email protected]
b r.m d
i.d
fiMii-h.rnt
fiMr$hrnt
td Fehi
tuhro'csrr
'iffia
hcdr 0thr
0rhr dsm.d
tmr
tr dnd
MDt
2
2
2
C
@
5
5
5
5
5
5
5
5
5
5
-
N
D
N
D
N
D
Negative
ND
N
D
N
D
N
D
N
D
N
D
N
D
N
D
N
D
N
D
N
D
N
D
5
N
I tri,_rr!!,colrr!.'nt
h.l
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rhoi
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rrd
*r
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.,!ecu!rt!!1!!!i. diiii&
ii ddni b-i'.lFnria.|d
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t
dBr,.-
.
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fl.tlrilttitllflt*tlrrts€s*!
D
3&at
ttr3o$r
r (s.22t6623gm
r 1&24A4562
| (e2a62sd l(*-?a5@
. .6jir'.OF@
M€nb6'orrh6scs o,o!p (sos sAj
TestReport
No.TSNEC1110357903 DaIe:26 Od 2O11
Tesl ltem(s)
Dibromodiphenyl
olher
Tdbromodiphenyt
elher
Tetrabromodiphenyl
ether
Penlabromodiphenyl
ether
Hexabromodiphenyl
elher
Heptabromodiphenyl
ethe.
Oclabromodiphenyl
ether
Nonabromodiphenyl
ether
Decabromodjphenyl
ether
ti!r!
UlI
MDL
pe
5
5
5
5
5
5
5
5
5
ND
ND
ND
ND
ND
NO
ND
ND
ND
mg/rg
ms/kg
ms/k9
mgKs
mgKg
mg/rg
mgftg
mg/Kg
mg/Kg
Page3 of 5
Notes :
(1)The maximumpermissible
timitis quotedfromdirective2011/65/ElJ.
Annex .
(2) o spot-test:
Negative= AbsenceofCr(Vl) coating,positive= presenceofC(Vt) coating;
The tested sample should be further verified by boiling-wEter-€xtraction
method ifthe spot test resutt as
Negativeor c€nnotbe confimed,
o Boiling-wateFextraction:
Negative= Absenceof Cr(Vl)coaling; positive= presenceof C(Vt) coating
The detecledconcentration
in boiling-watef-extraction
solutionis equalorgreaterthan0.02mg/kgwith 50
cm2samplesurfacearea.
For conosionprotectioncoatingson metals:Information
on stofageconditionsand productiondateofthe
testedsampleis unavailable
andthus resultsof Cr(VI)representstatusof the sampteat the time of
testing
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Memb.rorth.SGSG@rISOSSAl
TestReport
No.TSNEC1110357903
Date:26Oct2011
Page4 of 5
ATTASHMENTS
cdpb/t{g/cl./FBBs&pBDEr TcsdngFtow c-h.It
'l) Name
oflh6 porconwhomadstesiing:
yeo
AaronWang/Jeson
Li/Angell
2) Nameofthe psrsonin chargeoftesting:Cindyyin,/Rsx
Zhu
3) Thssesamplss
wer8dissolved
iotelly
by prs-condilionjng
method
according
to bslowflowchad
(Cf* endPBBs/PBDEs
iesl rnethod
excluded)
Sample
Preparation
SamplelVeasurBmeil
Acid digeBlion
w'th
micrc,,rave/
hotplale
Sample
solv€nt
extraclion
N€gative
ConcenlraliorV
Dilution
ofexlraciion
s0lution
Boiling
water
Bxllacl,on
Adding1,5diphenylcarbazid€
for
colord9velopmenl
1)Alkali
Fusion
/
0ryAshing
2) Acid to
dissolve
_{
dlld
ll .d
by b. 6@y
&q.o
'o in c.tu.'
Aredcolorindicalgs
thepresence
ofCre.
lf necessary,
conlifm
cod 16. d e
rbc.iF.ri
sh '6pdMn
cunxbrN'6ed.|dbryd!
bb
I scs u.nrio,r{orar.Th.5|| Avru1ED4Tt rth,chkEsas,
| +!::!$'et!11!g!Ili41!!9!*!
!!i9erl
,{6s.jbrhirqq
I {a_2216*w I F,r?r5295252
|p&.e!ry r(!:a,5ry9
[{olnb.rotrhsSGSGrolD(SOSSA)
TestReport
No.TSNEC1110357903
Date:26 oct 2011
Page5 of 5
Sample photo:
TSN11-103579.002
SGSauthentic€tethe
photoonoriginal
reporlonly
'" Endof Report-.
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Test Report
Applicant:
Number : TWNC00233558
Littelfuse Philippines Inc.
LIMA Technology Center, Lipa City,
Malvar, Batangas
Date
: Nov 25, 2011
Sample Description:
One (1) group of submitted samples said to be :
Part Description
: Solder (Pb above 85%)
Part Number
: 692323
Date Sample Received
: Nov 21, 2011
Date Test Started
: Nov 22, 2011
Test Conducted :
As requested by the applicant, for details please refer to attached pages.
Authorized By:
On Behalf Of Intertek Testing Services
Taiwan Limited
K. Y. Liang
Director
This report shall not be reproduced
except in full, without the written
approval of the laboratory.
Page 1 of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00233558
Test Conducted
(Ⅰ) Test Result Summary :
Test Item
Heavy Metal
Cadmium (Cd) content
Lead (Pb) content
Mercury (Hg) content
Chromium VI (Cr6+) content (mg/kg with 50cm2)
Result (ppm)
Grey Metal
ND
896353
ND
Negative (< 0.02)
Remarks: ppm = Parts per million based on weight of tested sample = mg/kg
ND = Not detected
<
= Less than
mg/kg with 50cm2 = milligram per kilogram with 50 square centimetre
Negative = A negative test result indicated positive observation
was not found at the time of Test.
Responsibility of Chemist : Irene Chiou / Kevin Liu
Date Sample Received
Test Period
: Nov 21, 2011
: Nov 22, 2011 To Nov 25, 2011
(Ⅱ) RoHS Requirement:
Restricted Substances
Cadmium (Cd) Content
Lead (Pb) Content
Mercury (Hg) Content
Chromium VI (Cr6+) Content
Limits
0.01% (100ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for
homogeneous material.
Page 2 of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00233558
Test Conducted
(Ⅲ) Test Method:
Test Item
Cadmium (Cd)
content
Lead (Pb) content
Mercury (Hg)
content
Chromium VI (Cr6+)
content
Test Method
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 7, by microwave
digestion until the tested samples are
totally dissolved and determined by
ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in annex B, by boiling water
extraction and determined by UV-Vis
spectrophotometer.
Reporting Limit
2 ppm
2 ppm
2 ppm
0.02
mg/kg with 50cm2
Remark: Reporting limit = Quantitation limit of analyte in sample
Page 3 of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00233558
Test Conducted
(Ⅳ) Measurement Flowchart:
Test for Cd/Pb/Hg/Chromium (VI)
Reference Standard：IEC 62321 edition 1.0:2008
Sample preparation
Take sample and immerse into Aqua Regia, start to strip plating layer
Stop the stripping procedure upon color change completely
Take the Aqua solution as plating component and stripped body as substrate component
Cd/Pb/Hg
Cr
Metal
For different
material, digest
the sample with
*1
appropriate acid
By spot test
Negative
Confirm the tested
samples are
totally dissolved
Make up with
deionized water
*2
6+
Polymers /
electronics
Weigh sample
and add
alkaline
solution
Get 50cm2 sample
Definite temp.
extraction
By boiling water
extraction
Cool and filter
the extract
Analyzed by ICP-OES
Make up with deionized water and add
diphenyl-carbazide solution
Remarks:
*1: List of Appropriate Acid：
Material
Polymers
Metals
Electronics
Analyzed by UV-VIS
Acid Added for Digestion
HNO3,HCl,HF,H2O2,H3BO3
HNO3,HCl,HF
HNO3,HCl,H2O2,HBF4
*2: If the result of spot test is positive, Chromium VI would be determined as detected.
End of Report
Page 4 of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00233558
Test Conducted
Photo
Page 5 of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Test Report
Applicant:
Number : TWNC00233543
Littelfuse Philippines Inc.
LIMA Technology Center, Lipa City,
Malvar, Batangas
Date
: Nov 25, 2011
Sample Description:
One (1) group of submitted samples said to be :
Part Description
: Yarn
Part Number
: 648112-002
Date Sample Received
: Nov 21, 2011
Date Test Started
: Nov 22, 2011
Test Conducted :
As requested by the applicant, for details please refer to attached pages.
Authorized By:
On Behalf Of Intertek Testing Services
Taiwan Limited
K. Y. Liang
Director
This report shall not be reproduced
except in full, without the written
approval of the laboratory.
Page 1 of 6
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00233543
Test Conducted
(Ⅰ) Test Result Summary :
Test Item
Result (ppm)
White Yarn
Heavy Metal
Cadmium (Cd) content
Lead (Pb) content
Mercury (Hg) content
Chromium VI (Cr6+) content
Polybrominated Biphenyls (PBBs)
Monobrominated Biphenyls (MonoBB)
Dibrominated Biphenyls (DiBB)
Tribrominated Biphenyls (TriBB)
Tetrabrominated Biphenyls (TetraBB)
Pentabrominated Biphenyls (PentaBB)
Hexabrominated Biphenyls (HexaBB)
Heptabrominated Biphenyls (HeptaBB)
Octabrominated Biphenyls (OctaBB)
Nonabrominated Biphenyls (NonaBB)
Decabrominated Biphenyl (DecaBB)
Polybrominated Diphenyl Ethers (PBDEs)
Monobrominated Diphenyl Ethers (MonoBDE)
Dibrominated Diphenyl Ethers (DiBDE)
Tribrominated Diphenyl Ethers (TriBDE)
Tetrabrominated Diphenyl Ethers (TetraBDE)
Pentabrominated Diphenyl Ethers (PentaBDE)
Hexabrominated Diphenyl Ethers (HexaBDE)
Heptabrominated Diphenyl Ethers (HeptaBDE)
Octabrominated Diphenyl Ethers (OctaBDE)
Nonabrominated Diphenyl Ethers (NonaBDE)
Decabrominated Diphenyl Ether (DecaBDE)
Halogen Content
Fluorine (F)
Chlorine (Cl)
Bromine (Br)
Iodine (I)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
571
ND
ND
Remarks: ppm = Parts per million based on weight of tested sample = mg/kg
ND = Not detected
Responsibility of Chemist : Irene Chiou / Kevin Liu / Cathy Chen
Date Sample Received
Test Period
: Nov 21, 2011
: Nov 22, 2011 To Nov 25, 2011
Page 2 of 6
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00233543
Test Conducted
(Ⅱ) RoHS Requirement:
Restricted Substances
Cadmium (Cd) Content
Lead (Pb) Content
Mercury (Hg) Content
Chromium VI (Cr6+) Content
Polybrominated Biphenyls (PBBs)
Polybrominated Diphenyl Ehters (PBDEs)
Limits
0.01% (100ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for
homogeneous material.
(Ⅲ) Test Method:
Test Item
Cadmium (Cd)
content
Lead (Pb) content
Mercury (Hg)
content
Chromium VI (Cr6+)
content
Polybrominated
Biphenyls (PBBs)
Polybrominated
Diphenyl Ethers
(PBDEs)
Halogen Content
Test Method
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 7, by microwave
digestion until the tested samples are
totally dissolved and determined by
ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in annex C, by alkaline
digestion and determined by UV-Vis
spectrophotometer.
With reference to IEC 62321 edition
1.0:2008 in annex A, by solvent
extraction and determined by GC-MSD
and further HPLC confirmation when
necessary.
With reference to IEC 62321 edition
1.0:2008 in annex A, by solvent
extraction and determined by GC-MSD
and further HPLC confirmation when
necessary.
With reference to EN 14582:2007 by
calorimetric bomb with oxygen and
determined by ion chromatography
Reporting Limit
2 ppm
2 ppm
2 ppm
1 ppm
5 ppm
5 ppm
50 ppm
Remark: Reporting limit = Quantitation limit of analyte in sample
Page 3 of 6
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00233543
Test Conducted
(Ⅳ) Measurement Flowchart:
Test for Cd/Pb/Hg/Chromium (VI)/PBBS/PBDES Contents
Reference Standard: IEC 62321 edition 1.0:2008
Sample preparation
For non-metal part
For metal part
Take sample and immerse into Aqua Regia, start to strip plating layer
Stop the stripping procedure upon color change completely
Take the Aqua solution as plating component and stripped body as substrate component
Cd/Pb/Hg
Cr
Confirm the tested
samples are
totally dissolved
Make up with
deionized water
PBBs/PBDEs
Polymers /
electronics
Metal
For different
material, digest
the sample with
*1
appropriate acid
6+
Weigh sample and
add organic solvent
By spot test
Negative
Get 50cm2 sample
By boiling water
extraction
*2
Weigh sample
and add
alkaline
solution
By Soxhlet
extraction or
Solvent extraction
Definite temp.
extraction
Cool and filter
the extract
Analyzed by ICP-OES
Concentrate the
extract and make up
with organic
solvent
Analyzed by GC-MSD
Make up with deionized
water and add diphenylcarbazide solution
Analyzed by UV-VIS
Remarks:
*1: List of Appropriate Acid：
Material
Polymers
Metals
Electronics
Acid Added for Digestion
HNO3,HCl,HF,H2O2,H3BO3
HNO3,HCl,HF
HNO3,HCl,H2O2,HBF4
*2: If the result of spot test is positive, Chromium VI would be determined as detected.
Page 4 of 6
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00233543
Test Conducted
(Ⅳ) Measurement Flowchart:
Test for Halogen Content
Reference Standard：EN 14582
Sampling/grinding or
cutting
Add absorbent in a
combustion flask &
place weighed sample in
equipment
Fill oxygen into
calorimetric bomb
Ignite then leave the
flask at room
temperature
Transfer the absorbent
into a volumetric flask
Make up with deionized
water
Analyzed by ion
chromatography
End of Report
Page 5 of 6
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00233543
Test Conducted
Photo
Page 6 of 6
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Test Report
Applicant:
Number : TWNC00253636
Littelfuse Philippines Inc.
LIMA Technology Center, Lipa City,
Malvar, Batangas
Date
: Apr 24, 2012
Sample Description:
One (1) group of submitted samples said to be :
Part Description
: Black Ink
Part Number
: 425809
Date Sample Received
: Apr 19, 2012
Date Test Started
: Apr 19, 2012
Test Conducted :
As requested by the applicant, for details please refer to attached pages.
Authorized By:
On Behalf Of Intertek Testing Services
Taiwan Limited
K. Y. Liang
Director
This report shall not be reproduced
except in full, without the written
approval of the laboratory.
Page 1 of 9
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00253636
Test Conducted
(Ⅰ) Test Result Summary :
Test Item
Heavy Metal
Cadmium (Cd) content
Lead (Pb) content
Mercury (Hg) content
Chromium VI (Cr6+) content
Polybrominated Biphenyls (PBBs)
Monobrominated Biphenyls (MonoBB)
Dibrominated Biphenyls (DiBB)
Tribrominated Biphenyls (TriBB)
Tetrabrominated Biphenyls (TetraBB)
Pentabrominated Biphenyls (PentaBB)
Hexabrominated Biphenyls (HexaBB)
Heptabrominated Biphenyls (HeptaBB)
Octabrominated Biphenyls (OctaBB)
Nonabrominated Biphenyls (NonaBB)
Decabrominated Biphenyl (DecaBB)
Polybrominated Diphenyl Ethers (PBDEs)
Monobrominated Diphenyl Ethers (MonoBDE)
Dibrominated Diphenyl Ethers (DiBDE)
Tribrominated Diphenyl Ethers (TriBDE)
Tetrabrominated Diphenyl Ethers (TetraBDE)
Pentabrominated Diphenyl Ethers (PentaBDE)
Hexabrominated Diphenyl Ethers (HexaBDE)
Heptabrominated Diphenyl Ethers (HeptaBDE)
Octabrominated Diphenyl Ethers (OctaBDE)
Nonabrominated Diphenyl Ethers (NonaBDE)
Decabrominated Diphenyl Ether (DecaBDE)
Result (ppm)
Black Paste
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Page 2 of 9
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00253636
Test Conducted
(Ⅰ) Test Result Summary :
Test Item
Result (ppm)
Black Paste
Halogen Content
Fluorine (F)
Chlorine (Cl)
Bromine (Br)
Iodine (I)
Phthalates
Di(2-ethylhexyl) Phthalate (DEHP)
Dibutyl Phthalate (DBP)
Benzyl Butyl Phthalate (BBP)
Others
Hexabromocyclododecane (HBCDD)
ND
610
ND
ND
ND
ND
ND
ND
Remarks: ppm = Parts per million based on wet weight of tested sample =
mg/kg
ND = Not detected
Responsibility of Chemist : Irene Chiou / Kevin Liu / Cathy Chen
Date Sample Received
Test Period
: Apr 19, 2012
: Apr 19, 2012 To Apr 24, 2012
(Ⅱ) RoHS Requirement:
Restricted Substances
Cadmium (Cd) Content
Lead (Pb) Content
Mercury (Hg) Content
Chromium VI (Cr6+) Content
Polybrominated Biphenyls (PBBs)
Polybrominated Diphenyl Ehters (PBDEs)
Limits
0.01% (100ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for
homogeneous material.
Page 3 of 9
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00253636
Test Conducted
(Ⅲ) Test Method:
Test Item
Test Method
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
Cadmium (Cd) content
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
Lead (Pb) content
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 7, by microwave
Mercury (Hg) content
digestion until the tested samples
are totally dissolved and determined
by ICP-OES.
With reference to IEC 62321 edition
Chromium VI (Cr6+)
1.0:2008 in annex C, by alkaline
content
digestion and determined by UV-Vis
spectrophotometer.
With reference to IEC 62321 edition
1.0:2008 in annex A, by solvent
Polybrominated
extraction and determined by GC-MS
Biphenyls (PBBs)
and further HPLC-DAD confirmation
when necessary.
With reference to IEC 62321 edition
Polybrominated
1.0:2008 in annex A, by solvent
Diphenyl Ethers
extraction and determined by GC-MS
(PBDEs)
and further HPLC-DAD confirmation
when necessary.
With reference to EN 14582:2007 by
Halogen Content
calorimetric bomb with oxygen and
determined by Ion Chromatograph.
With reference to EN 14372: 2004, by
Phthalates
solvent extraction and determined by
GC-MS.
With reference to USEPA 3540C, by
Hexabromocyclododecane
solvent extraction and determined by
(HBCDD)
GC-MSD.
Reporting Limit
2 ppm
2 ppm
2 ppm
1 ppm
5 ppm
5 ppm
50 ppm
10 ppm
10 ppm
Remark: Reporting limit = Quantitation limit of analyte in sample
Page 4 of 9
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00253636
Test Conducted
(Ⅳ) Measurement Flowchart:
Test for Cd/Pb/Hg/Chromium (VI)/PBBS/PBDES Contents
Reference Standard: IEC 62321 edition 1.0:2008
Sample preparation
For non-metal part
For metal part
Take sample and immerse into Aqua Regia, start to strip plating layer
Stop the stripping procedure upon color change completely
Take the Aqua solution as plating component and stripped body as substrate component
Cd/Pb/Hg
Cr
Weigh sample and
add organic solvent
By spot test
Negative
Confirm the tested
samples are
totally dissolved
Make up with
deionized water
PBBs/PBDEs
Polymers /
electronics
Metal
For different
material, digest
the sample with
*1
appropriate acid
6+
Get 50cm2 sample
By boiling water
extraction
*2
Weigh sample
and add
alkaline
solution
By Soxhlet
extraction or
Solvent extraction
Definite temp.
extraction
Cool and filter
the extract
Analyzed by ICP-OES
Concentrate the
extract and make up
with organic
solvent
Analyzed by GC-MSD
Make up with deionized
water and add diphenylcarbazide solution
Analyzed by UV-VIS
Remarks:
*1: List of Appropriate Acid：
Acid Added for Digestion
Material
Polymers
HNO3,HCl,HF,H2O2,H3BO3
Metals
HNO3,HCl,HF
Electronics
HNO3,HCl,H2O2,HBF4
*2: If the result of spot test is positive, Chromium VI would be determined as detected.
Page 5 of 9
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00253636
Test Conducted
(Ⅳ) Measurement Flowchart:
Test for Halogen Content
Reference Standard：EN 14582
Sampling/grinding or
cutting
Add absorbent in a
combustion flask &
place weighed sample in
equipment
Fill oxygen into
calorimetric bomb
Ignite then leave the
bomb at room
temperature
Transfer the absorbent
into a volumetric flask
Make up with deionized
water
Analyzed by ion
chromatography
Page 6 of 9
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00253636
Test Conducted
(Ⅳ) Measurement Flowchart:
Test For Phthalates Contents
Reference Method: EN 14372: 2004
Sampling/grinding or
cutting
Weigh sample and add
organic solvent
By solvent extraction
Concentrate the extract
and make up with
organic solvent
Analyzed by GC-MSD
Page 7 of 9
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00253636
Test Conducted
(Ⅳ) Measurement Flowchart:
Test For Hexabromocyclododecane (HBCDD)
Reference Standard：USEPA 3540C
Sampling/grinding or cutting
Weigh sample and add organic
solvent
By soxhlet extraction
Concentrate the extract and
make up with organic solvent
Analyzed by GC-MSD
End of Report
Page 8 of 9
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00253636
Test Conducted
Photo
Page 9 of 9
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401