ICPTest_456 pdf

ICP Test Report Certification Packet
Company name :
Littelfuse, Inc.
Product Series:
Nano (Silver or Gold plated)
Product #:
456xxx Series
Issue Date:
May 2, 2012
It is hereby certified by Littelfuse, Inc. that there is neither RoHS (EU Directive
2002/95/EC)-restricted substance nor such use, for materials to be used for unit parts, for
packing/packaging materials, and for additives and the like in the manufacturing processes.
In addition, it is hereby reported to you that the parts and sub-materials, the materials to be used
for unit parts, the packing/packaging materials, and the additives and the like in the manufacturing
processes, are all composed of the following components.
Issued by:
<Global EHS Engineer>
(1) Parts, sub-materials and unit parts
This document covers the Nano RoHS-Compliant series products manufactured by
Littelfuse, Inc.
＜ Raw Materials Used
Please see Table 1
(2) The ICP data on all measurable substances
Please see appropriate pages as identifed in Table 1
Remarks：
Pb (lead) contained in the high temperature melting solder > 85% and is categorized as
exempt under section 7a of the RoHS Annex.
Form 585-047 Rev. A
1
2/21/06
Table 1: List of Raw Materials covered by this report
Total Parts
1
Raw Material Part Number
909-422
Raw Material Description
Body
2
3
4
5
6
7
8
9
910-259 (same as 910-238)
910-554 (same as 910-275)
087266
11-0010 (687xxx)
079xxx
692323
425809
425809
Cap – Silver plated
Cap – Gold plated
Anaerobic Adhesive
Element-Pure Ag1000
Element
Solder
Ink
Ink – RoHS 2
2
Page(s)
3-8
9-12,
13-16
17-21
22-30
31-37
38-42
43-47
48-53
54-56
Test Report
Applicant:
Number : TWNC00233545
Littelfuse Philippines Inc.
LIMA Technology Center, Lipa City,
Malvar, Batangas
Date
: Nov 25, 2011
Sample Description:
One (1) group of submitted samples said to be :
Part Description
: Body
Part Number
: 909-422
Date Sample Received
: Nov 21, 2011
Date Test Started
: Nov 22, 2011
Test Conducted :
As requested by the applicant, for details please refer to attached pages.
Authorized By:
On Behalf Of Intertek Testing Services
Taiwan Limited
K. Y. Liang
Director
This report shall not be reproduced
except in full, without the written
approval of the laboratory.
Page 1 of 6
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00233545
Test Conducted
(Ⅰ) Test Result Summary :
Test Item
Result (ppm)
White Material
Heavy Metal
Cadmium (Cd) content
Lead (Pb) content
Mercury (Hg) content
Chromium VI (Cr6+) content
Polybrominated Biphenyls (PBBs)
Monobrominated Biphenyls (MonoBB)
Dibrominated Biphenyls (DiBB)
Tribrominated Biphenyls (TriBB)
Tetrabrominated Biphenyls (TetraBB)
Pentabrominated Biphenyls (PentaBB)
Hexabrominated Biphenyls (HexaBB)
Heptabrominated Biphenyls (HeptaBB)
Octabrominated Biphenyls (OctaBB)
Nonabrominated Biphenyls (NonaBB)
Decabrominated Biphenyl (DecaBB)
Polybrominated Diphenyl Ethers (PBDEs)
Monobrominated Diphenyl Ethers (MonoBDE)
Dibrominated Diphenyl Ethers (DiBDE)
Tribrominated Diphenyl Ethers (TriBDE)
Tetrabrominated Diphenyl Ethers (TetraBDE)
Pentabrominated Diphenyl Ethers (PentaBDE)
Hexabrominated Diphenyl Ethers (HexaBDE)
Heptabrominated Diphenyl Ethers (HeptaBDE)
Octabrominated Diphenyl Ethers (OctaBDE)
Nonabrominated Diphenyl Ethers (NonaBDE)
Decabrominated Diphenyl Ether (DecaBDE)
Halogen Content
Fluorine (F)
Chlorine (Cl)
Bromine (Br)
Iodine (I)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Remarks: ppm = Parts per million based on weight of tested sample = mg/kg
ND = Not detected
Responsibility of Chemist : Irene Chiou / Kevin Liu / Cathy Chen
Date Sample Received
Test Period
: Nov 21, 2011
: Nov 22, 2011 To Nov 25, 2011
Page 2 of 6
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00233545
Test Conducted
(Ⅱ) RoHS Requirement:
Restricted Substances
Cadmium (Cd) Content
Lead (Pb) Content
Mercury (Hg) Content
Chromium VI (Cr6+) Content
Polybrominated Biphenyls (PBBs)
Polybrominated Diphenyl Ehters (PBDEs)
Limits
0.01% (100ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for
homogeneous material.
(Ⅲ) Test Method:
Test Item
Cadmium (Cd)
content
Lead (Pb) content
Mercury (Hg)
content
Chromium VI (Cr6+)
content
Polybrominated
Biphenyls (PBBs)
Polybrominated
Diphenyl Ethers
(PBDEs)
Halogen Content
Test Method
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 7, by microwave
digestion until the tested samples are
totally dissolved and determined by
ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in annex C, by alkaline
digestion and determined by UV-Vis
spectrophotometer.
With reference to IEC 62321 edition
1.0:2008 in annex A, by solvent
extraction and determined by GC-MSD
and further HPLC confirmation when
necessary.
With reference to IEC 62321 edition
1.0:2008 in annex A, by solvent
extraction and determined by GC-MSD
and further HPLC confirmation when
necessary.
With reference to EN 14582:2007 by
calorimetric bomb with oxygen and
determined by ion chromatography
Reporting Limit
2 ppm
2 ppm
2 ppm
1 ppm
5 ppm
5 ppm
50 ppm
Remark: Reporting limit = Quantitation limit of analyte in sample
Page 3 of 6
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00233545
Test Conducted
(Ⅳ) Measurement Flowchart:
Test for Cd/Pb/Hg/Chromium (VI)/PBBS/PBDES Contents
Reference Standard: IEC 62321 edition 1.0:2008
Sample preparation
For non-metal part
For metal part
Take sample and immerse into Aqua Regia, start to strip plating layer
Stop the stripping procedure upon color change completely
Take the Aqua solution as plating component and stripped body as substrate component
Cd/Pb/Hg
Cr
Weigh sample and
add organic solvent
By spot test
Negative
Confirm the tested
samples are
totally dissolved
Make up with
deionized water
PBBs/PBDEs
Polymers /
electronics
Metal
For different
material, digest
the sample with
*1
appropriate acid
6+
Get 50cm2 sample
By boiling water
extraction
*2
Weigh sample
and add
alkaline
solution
By Soxhlet
extraction or
Solvent extraction
Definite temp.
extraction
Cool and filter
the extract
Analyzed by ICP-OES
Concentrate the
extract and make up
with organic
solvent
Analyzed by GC-MSD
Make up with deionized
water and add diphenylcarbazide solution
Analyzed by UV-VIS
Remarks:
*1: List of Appropriate Acid：
Material
Polymers
Metals
Electronics
Acid Added for Digestion
HNO3,HCl,HF,H2O2,H3BO3
HNO3,HCl,HF
HNO3,HCl,H2O2,HBF4
*2: If the result of spot test is positive, Chromium VI would be determined as detected.
Page 4 of 6
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00233545
Test Conducted
(Ⅳ) Measurement Flowchart:
Test for Halogen Content
Reference Standard：EN 14582
Sampling/grinding or
cutting
Add absorbent in a
combustion flask &
place weighed sample in
equipment
Fill oxygen into
calorimetric bomb
Ignite then leave the
flask at room
temperature
Transfer the absorbent
into a volumetric flask
Make up with deionized
water
Analyzed by ion
chromatography
End of Report
Page 5 of 6
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00233545
Test Conducted
Photo
Page 6 of 6
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
scs
Test Report
No.:LB12-01094C
March5, 2012
Page1 of 4
LTTTELFUSE
PHtLS.,tNC.
LimaTech Center,SEZ,
Lipa,Malvar,Batangas
The followingsample(s)was/veere
submittedand identifiedbylonbehaltol the clientas:
ProductName
Cap 910-259/ Base
SGSSamplgNumber
LB12-01094.004
RecelvedDate
FebrJary21,2012
Test PerlormingDate
F€bruary
21,20121o
March5,2012
T6sl Perlormed
SGS Philippines
subcontracted
the testingot sampte(s)
setecl€dby
applicantwithfollowingresults
Test Requested
Selectedtest(s)as requested
by client.
Test llethod
Pleaserelerto nextpage(s).
Ted n6sult(5)
Pleaserefer1onextpage(s).
C,oncluslon
Basedon the perfomedtestson submittedsample(s),
the resultsof
Lead,Cadmium,Hexavalent
chromiumand l\,,lercury
complywith
lhe RoHSDnective2002/95/EC
and iis subsequeniamendments.
This reportwillbekepl on filefor six monthsfromthe dateol issue.
Signedfor and on behaltol
INC.
SGSPHILIPPINES,
I'EDEN L. PENEYHA
LaboraloryOperalions Manager
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SGS
Test Report
No.:LB12'01094C
Page2 ol4
March5.2012
: LB11-01094.004
SampleNumber
metal
of silvercolored
PhyslcalDas€ription : Basematerial
Item/ BatchNumb€r : fl/A
RoHSDlreclive2002/95/EC
Tesl ltem(s)
unit
(Cd)
Cadmium
mg/Kg
Lead(Pb)
MEKg
(Hg)
Mercury
mg/Kg
C(Vl)
Hexavalent
Chromium
Itothod
IEC62321:2008application
of modifieddigestionby
surlaceetchingand
perfomedby ICP-AES.
withreference
to lEc 62321:
2008andperfomedby
Boiling
waterextraction
Method.#
iIDL
n6sult
2
2
ND
'|19
2
ND
Negative
Nole :
1 mg/kg= ppm ; 0.1wt%= lOOOppm
2. ND = Not Detected
3. MDL = lllethodDet€ctionLimit
4. " = Oualitative
analysis(NoUnit)
5. # = a. Posilivemeansthe presenceol CrVlon the testedareas
b. Negativemeansthe.absenceof CrVlon the testedareas
solulionis equalorgrealerthan0 02 mg/kg
in boiling-water'extraction
The detecGdconcentration
with 50 cm2lesleda€as.
6. Analyseswere subcontractedto SGS Taiwan,Ltd
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TestReport
No.:LB12-01094C
March
5,2012
Page 3 of 4
ATALYSISFLOWCHARTOFHEAVYMETALS
Pb, cd, Hg
Negalive
A d d i n q1 , 5 lor
diph€nylcalbazide
Adding1.5the prssenceo, Cl6+.
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SGS
Test Report
No.:LB12-010S4C
March5, 2012
Page4 of 4
SamplePhoto (As Becaived):
LB12-01094.004
,
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...End
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Test Heport
No.:1812-01094A
March5, 2012
Page1 ot 4
INC.
LITTELFUSEPHII..S.,
LimaTech Center,SEz,
Lipa,Malvar,Batangas
bylonbehalfof theclientas:
andidentilied
The followingsample(s)was/were submitled
ProductName
Cap910'259/ Plaling
SGSSampleNumbel
L812,01094.002
RecelvedDate
Fehtuary21, 2012
Test PerformingDate
21, 2012to lllarch5, 2012
February
T€st Perfurmed
by
selected
lheteslingol sample(s)
subconlracted
SGSPhilippines
results
wilhfollowing
applicant
Te€t Requested
byclient.
teg(s)asrequested
Selecled
Test Method
Pleaserelerto nextPage(s)
Tqrt R.eult(s)
Pleaserefer10nextpage(s).
conclugion
theresultsof
sample(s)'
testsonsubmitted
Basedontheperlormed
complywlth
andl\rercury
Hexavalent
chromium
Lead,Cadmium,
amendments
anditssubsequent
2oo2l95/Eo
theRoHSDkective
This repodwill be kept on filelor six monthsfromthe dale of issue'
Signedlor and on behalfol
INC.
SGSPHILIPPINES,
i,EDEN L. PENEYRA
LaboratoryOperationsManager
'ffi
'ffi
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sGs
TestReport
No.:1812-01094A
PaOe2 ol 4
Llarch5, 2012
: LB11-01094.002
SampleNumber
PhygicalDescriplion : Platinglayerot siMercolored
metal
Itom/ BalchNumbor
RoHS Dlrectlve 2002/95/EC
Test ltem(s)
(tu)
Cadmium
Lead(Pb)
(Hg)
Mercury
Unlt
Method
MDL
Rg€ult
mgKg
m9Kg
mg/kg
IEC62321:2006application
ol modifieddigestionby
surfaceetchingand
performedby ICP-AES.
2
2
ND
18
NO
HexavalentChromiumC(Vl)
wilh reference
to lEc 62321:
2008andperformedby
Boiling
waterextraction
Method.#
Negalive
Nole :
1 . mdks=ppm; 0.1M%=1000ppm
2. ND= NotDetected
Limit
3. MDL= MethodDetection
(NoUnit)
analysis
4. " = Qualitative
meansthepresence
ot CrVlonthetestedareas
5. # = a. Positive
b. Negativemoansthe absenceof CrVlonlhe testedareas
is equalorgreaterthan
0.02mg/kg
Thedetected
concentration
in boiling-waterexlraction
solulion
with50 cm,testedarcas.
to SGSTaiwan,Ltd
6. Analys€sweresubcontracled
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No.:LB12-01094A
Page3 of 4
March5,2012
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March5,2012
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Number : TWNC00233554
Test Report
Applicant:
Littelfuse Philippines Inc.
LIMA Technology Center, Lipa City,
Malvar, Batangas
Date
: Nov 24, 2011
Sample Description:
One (1) group of submitted samples said to be :
Part Description
: Cap
Part Number
: 910-275 / 910-554
Date Sample Received
: Nov 21, 2011
Date Test Started
: Nov 23, 2011
Test Conducted :
As requested by the applicant, for details please refer to attached pages.
Authorized By:
On Behalf Of Intertek Testing Services
Taiwan Limited
K. Y. Liang
Director
This report shall not be reproduced
except in full, without the written
approval of the laboratory.
Page 1 of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
៮ᶑ៲减ㄨ惝䜧ᖃⶏ峖៲᩾
114 ᩶ᦝ⒈៭㓜ᧆ㫤៏呵 423 䳥 8 ゙
Tel: (+886-2) 6602-2888Η2797-8885ʳ Fax: (+886-2) 6602-2400Η6602-2401
Number : TWNC00233554
Test Conducted
(Ⅰ) Test Result Summary :
Result (ppm)
(1)
(2)
Test Item
Heavy Metal
Cadmium (Cd) content
Lead (Pb) content
Mercury (Hg) content
Chromium VI (Cr6+) content (mg/kg with 50cm2)
ND
ND
ND
Negative
(< 0.02)
ND
ND
ND
Negative
(< 0.02)
Remarks: ppm = Parts per million based on weight of tested sample = mg/kg
ND = Not detected
<
= Less than
mg/kg with 50cm2 = milligram per kilogram with 50 square centimetre
Negative = A negative test result indicated positive observation
was not found at the time of Test.
Tested Components
(1) Brown Metal Base Material
(2) Golden Plating Layer
Responsibility of Chemist : Irene Chiou / Kevin Liu
Date Sample Received
Test Period
: Nov 21, 2011
: Nov 23, 2011 To Nov 24, 2011
(Ⅱ) RoHS Requirement:
Restricted Substances
Cadmium (Cd) Content
Lead (Pb) Content
Mercury (Hg) Content
Chromium VI (Cr6+) Content
Limits
0.01% (100ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for
homogeneous material.
Page 2 of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00233554
Test Conducted
(Ⅲ) Test Method:
Test Item
Cadmium (Cd)
content
Lead (Pb) content
Mercury (Hg)
content
Chromium VI (Cr6+)
content
Test Method
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 7, by microwave
digestion until the tested samples are
totally dissolved and determined by
ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in annex B, by boiling water
extraction and determined by UV-Vis
spectrophotometer.
Reporting Limit
2 ppm
2 ppm
2 ppm
0.02
mg/kg with 50cm2
Remark: Reporting limit = Quantitation limit of analyte in sample
Page 3 of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00233554
Test Conducted
(Ⅳ) Measurement Flowchart:
Test for Cd/Pb/Hg/Chromium (VI)
Reference Standard：IEC 62321 edition 1.0:2008
Sample preparation
Take sample and immerse into Aqua Regia, start to strip plating layer
Stop the stripping procedure upon color change completely
Take the Aqua solution as plating component and stripped body as substrate component
Cd/Pb/Hg
Cr
Polymers /
electronics
Metal
For different
material, digest
the sample with
*1
appropriate acid
By spot test
Negative
Confirm the tested
samples are
totally dissolved
Make up with
deionized water
6+
*2
Weigh sample
and add
alkaline
solution
Get 50cm2 sample
Definite temp.
extraction
By boiling water
extraction
Cool and filter
the extract
Analyzed by ICP-OES
Make up with deionized water and add
diphenyl-carbazide solution
Remarks:
*1: List of Appropriate Acid：
Material
Polymers
Metals
Electronics
Analyzed by UV-VIS
Acid Added for Digestion
HNO3,HCl,HF,H2O2,H3BO3
HNO3,HCl,HF
HNO3,HCl,H2O2,HBF4
*2: If the result of spot test is positive, Chromium VI would be determined as detected.
End of Report
Page 4 of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00233554
Test Conducted
Photo
Page 5 of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00233529
Test Report
Applicant:
Littelfuse Philippines Inc.
LIMA Technology Center, Lipa City,
Malvar, Batangas
Date
: Nov 25, 2011
Sample Description:
One (1) group of submitted samples said to be :
Part Description
: Anaerobic Adhesive
Part Number
: 087266
Date Sample Received
: Nov 21, 2011
Date Test Started
: Nov 22, 2011
Test Conducted :
As requested by the applicant, for details please refer to attached pages.
Authorized By:
On Behalf Of Intertek Testing Services
Taiwan Limited
K. Y. Liang
Director
This report shall not be reproduced
except in full, without the written
approval of the laboratory.
Page 1 of 9
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00233529
Test Conducted
(Ⅰ) Test Result Summary :
Test Item
Result (ppm)
Green Liquid
Heavy Metal
Cadmium (Cd) content
Lead (Pb) content
Mercury (Hg) content
Chromium VI (Cr6+) content
Polybrominated Biphenyls (PBBs)
Monobrominated Biphenyls (MonoBB)
Dibrominated Biphenyls (DiBB)
Tribrominated Biphenyls (TriBB)
Tetrabrominated Biphenyls (TetraBB)
Pentabrominated Biphenyls (PentaBB)
Hexabrominated Biphenyls (HexaBB)
Heptabrominated Biphenyls (HeptaBB)
Octabrominated Biphenyls (OctaBB)
Nonabrominated Biphenyls (NonaBB)
Decabrominated Biphenyl (DecaBB)
Polybrominated Diphenyl Ethers (PBDEs)
Monobrominated Diphenyl Ethers (MonoBDE)
Dibrominated Diphenyl Ethers (DiBDE)
Tribrominated Diphenyl Ethers (TriBDE)
Tetrabrominated Diphenyl Ethers (TetraBDE)
Pentabrominated Diphenyl Ethers (PentaBDE)
Hexabrominated Diphenyl Ethers (HexaBDE)
Heptabrominated Diphenyl Ethers (HeptaBDE)
Octabrominated Diphenyl Ethers (OctaBDE)
Nonabrominated Diphenyl Ethers (NonaBDE)
Decabrominated Diphenyl Ether (DecaBDE)
Halogen Content
Fluorine (F)
Chlorine (Cl)
Bromine (Br)
Iodine (I)
Phthalates
Di(2-ethylhexyl) Phthalate (DEHP)
Dibutyl Phthalate (DBP)
Benzyl Butyl Phthalate (BBP)
Others
Hexabromocyclododecane (HBCDD)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Remarks: ppm = Parts per million based on wet weight of tested sample =
mg/kg
ND = Not detected
Responsibility of Chemist : Irene Chiou / Kevin Liu / Cathy Chen
Date Sample Received
Test Period
: Nov 21, 2011
: Nov 22, 2011 To Nov 24, 2011
Page 2 of 9
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00233529
Test Conducted
(Ⅱ) RoHS Requirement:
Restricted Substances
Cadmium (Cd) Content
Lead (Pb) Content
Mercury (Hg) Content
Chromium VI (Cr6+) Content
Polybrominated Biphenyls (PBBs)
Polybrominated Diphenyl Ehters (PBDEs)
Limits
0.01% (100ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for
homogeneous material.
(Ⅲ) Test Method:
Test Item
Test Method
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
Cadmium (Cd) content microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
Lead (Pb) content
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 7, by microwave
Mercury (Hg) content digestion until the tested samples
are totally dissolved and determined
by ICP-OES.
With reference to IEC 62321 edition
Chromium VI (Cr6+)
1.0:2008 in annex C, by alkaline
content
digestion and determined by UV-Vis
spectrophotometer.
With reference to IEC 62321 edition
1.0:2008 in annex A, by solvent
Polybrominated
extraction and determined by GC-MSD
Biphenyls (PBBs)
and further HPLC confirmation when
necessary.
Reporting Limit
2 ppm
2 ppm
2 ppm
1 ppm
5 ppm
Page 3 of 9
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00233529
Test Conducted
(Ⅲ) Test Method:
Test Item
Test Method
With reference to IEC 62321 edition
1.0:2008 in annex A, by solvent
Polybrominated
Diphenyl Ethers
extraction and determined by GC-MSD
(PBDEs)
and further HPLC confirmation when
necessary.
With reference to EN 14582:2007 by
Halogen Content
calorimetric bomb with oxygen and
determined by ion chromatography
With reference to EN 14372: 2004, by
Phthalates
solvent extraction and determined by
GC-MSD
With reference to USEPA 3540C, by
Hexabromocyclododecane
solvent extraction and determined by
(HBCDD)
GC-MSD
Reporting Limit
5 ppm
50 ppm
50 ppm
10 ppm
Remark: Reporting limit = Quantitation limit of analyte in sample
Page 4 of 9
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00233529
Test Conducted
(Ⅳ) Measurement Flowchart:
Test for Cd/Pb/Hg/Chromium (VI)/PBBS/PBDES Contents
Reference Standard: IEC 62321 edition 1.0:2008
Sample preparation
For non-metal part
For metal part
Take sample and immerse into Aqua Regia, start to strip plating layer
Stop the stripping procedure upon color change completely
Take the Aqua solution as plating component and stripped body as substrate component
Cd/Pb/Hg
Cr
Confirm the tested
samples are
totally dissolved
Make up with
deionized water
PBBs/PBDEs
Polymers /
electronics
Metal
For different
material, digest
the sample with
*1
appropriate acid
6+
Weigh sample and
add organic solvent
By spot test
Negative
Get 50cm2 sample
By boiling water
extraction
*2
Weigh sample
and add
alkaline
solution
By Soxhlet
extraction or
Solvent extraction
Definite temp.
extraction
Cool and filter
the extract
Analyzed by ICP-OES
Concentrate the
extract and make up
with organic
solvent
Analyzed by GC-MSD
Make up with deionized
water and add diphenylcarbazide solution
Analyzed by UV-VIS
Remarks:
*1: List of Appropriate Acid：
Material
Polymers
Metals
Electronics
Acid Added for Digestion
HNO3,HCl,HF,H2O2,H3BO3
HNO3,HCl,HF
HNO3,HCl,H2O2,HBF4
*2: If the result of spot test is positive, Chromium VI would be determined as detected.
Page 5 of 9
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00233529
Test Conducted
(Ⅳ) Measurement Flowchart:
Test for Halogen Content
Reference Standard：EN 14582
Sampling/grinding or
cutting
Add absorbent in a
combustion flask &
place weighed sample in
equipment
Fill oxygen into
calorimetric bomb
Ignite then leave the
flask at room
temperature
Transfer the absorbent
into a volumetric flask
Make up with deionized
water
Analyzed by ion
chromatography
Page 6 of 9
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00233529
Test Conducted
(Ⅳ) Measurement Flowchart:
Test For Phthalates Contents
Reference Method: EN 14372: 2004
Sampling/grinding or
cutting
Weigh sample and add
organic solvent
By solvent extraction
Concentrate the extract
and make up with
organic solvent
Analyzed by GC-MSD
Page 7 of 9
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00233529
Test Conducted
(Ⅳ) Measurement Flowchart:
Test For Hexabromocyclododecane (HBCDD)
Reference Standard：USEPA 3540C
Sampling/grinding or cutting
Weigh sample and add organic
solvent
By soxhlet extraction
Concentrate the extract and
make up with organic solvent
Analyzed by GC-MSD
End of Report
Page 8 of 9
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00233529
Test Conducted
Photo
Page 9 of 9
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
nown
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Mercury(Hg)
Cr(Vl)
Hexavalent
Chromium
to IEC62321r2008and
Withreference
mg/Kg
perfomedby ICP-AES.
mS/kS
2
2
Withr€fefence
to IEC62321:2008and
perfomedby Boilingwaterext€ction
Method.#
Rs6ult
l.lo.l
n.d.
n.d.
n.o,
Negative
n.o.
Sumof PBB3
Monobromobiphenyl
Dibromobiphenyl
Tribromobiphenyl
5
5
5
Tetrabromobiphenyl
Pentabromobiphenyl
Hexabromobiphenyl
Hoptabro.nobiphenyl
Octabromobiphenyl
Nonabromobiphenyl
Decabromobiphenyl
Sumof PBDES
ether
Monobromodiphenyl
ether
Dibromodiphenyl
ether
Tribromodiphenyl
Tetrabromodiphenyl
ether
5
2008and
Withreference
to IEC6232'1r
mg/Kg perfomed
by GC/MS.
5
5
5
5
5
5
n.d-
n.d.
n_o,
n.d.
n.d.
n.d.
n.d.
n.d.
n-o.
n.d.
n.d.
n.o.
n.d.
n.d.
5
5
5
Pentabromodiphenyl
ether
ether
Hexabromodiphenyl
ether
Heptabrornodiphenyl
ether
Octabromodiphenyl
5
5
ether
Nonabromodiphenyl
n.d.
n.d.
n.d.
n.d.
n.d.
n.d.
n.d.
ether
Decabromodiphenyl
sGrrsdd rhs rd @d €n@lb €
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Test Report
No.: CEl201'1/84940
Page:3 of 7
Dale: 2O11112J01
rl
POLYFILAG
OBERALLMENDSTMSSE2OA,CH€3OOZUG / SWITZERLAND
T€t lt.m(s)
Halogen
(F)
Halogen-Fluorine
(CASNo.:14762-9+8)
(Cl)
Halogen-Chlorin€
(CASNo.:22537-15-1)
(Br)
Halogen-Bromine
(CASNo.:10097-32-2)
(l)
Halogen-lodine
(CASNo.:14362.44-8)
Unit
mg/Kg
Method
With referenceto BS EN ASAZ2007.
wasperfomedby lC.
Analysis
[IDL
[|||llt[l]t
Result
No.1
50
n.o,
50
n.d.
50
n-d.
50
n.d.
Note :
1. mg/kg= ppm i 0.1M%= 1000ppm
2. n.d. = Not Det€cted
Limit
3. MDL= MethodDeteclion
4."-"=NotRegulated
analysis(NoUnit)
5. " = Qualitative
6. # = a. Positivemeansthe presenceof ClVl on the testedareas
b. Negativemeansthe absenceof OVI on the testedareas
solutionis equalor grcatefthan0.02mg/kgwith 50 cm'z
The de'tectedconcent€tionin boiling-watea-extraction
testedareas.
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ostra
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Test Report
No.: CE/2011/84940
Page:4 ol7
Dale.201111i,01
||t] tlt
POLYFILAG
OBERALLMENDSTRASSE
2OA,CH63OOZUG / SWTZERLAND
trlll
methodaccording
to belowflowchart.
1) Thesesamples
weredissolved
totallyby pretonditioning
( Cr- test methodexcluded)
Yang
Climbgreat
2) Nameofthe personwhom€demeasurernent:
TroyChang
3) Nameof thepersonin chargeof measu.ement:
Cutting/ Preparation
acid
Aciddigestion
by suitable
dependedon difierentsample
material{a8belowtable)
Addappropiateamountof
digestion
reagent
Heatto appropriate
t€rnperatureto exttact
1) AlkaliFusion
2) HCltodi6solve
ICP.AES
Add diphenyl-carbazidef or
colordevelopment
Dige*ionAcid
S€mpleMaterial
solder
Steel,copper,aluminum,
Aqua €gia, HNO3,HCl,HF,HrO,
Gla6s
HNO3/HF
measurethe absotbance
Gold,platinum,palladium,ceramic
Aqua fegia
at 5,10nm by W-VIS
Silver
HNOg
Plastic
HrSO4,
HrOr,HNq, HCI
Others
Anyacidtototaldigestion
ipsGlb{d rh s rd reD.d
€nid b
cmtsry alrrjllr!I. iri.if::l.r{iji;;i-\Jl*, i*"f.inF*}ri1'r:\, +j'an fn:/tE+'
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rFrl|ri 14610r)re
TestReport
No.: CE/2011/84940
Dale.2011hZO1
[fir
POLYFILAG
ZUG/ SWITZERLAND
2OA,CH€3OO
OBERALLMENDSTRASSE
PBBIPBDE analyticalFLow CHART
Wong
1) l.lade of the personwhonEderBasurerEnl Rornan
2) l{anE of the personin chargeof nEasurenEntTroyChang
Fi6t te6tingprocess------'
Optional
screenprocess---.
proce6s - .>
Confinmtion
Screenanalysis
i..........1..........
Sanplee)draction/
So*rlet d€thod
ConcentratdDilute
Extractedsoftlion
v
Filter
Analysisby GC/MS
csF
nirhsl6itspdBlsrdvroibsamprqtbd€d
i;:Jret4i..!ril'j!.;!1{t,; jiilni:rEi,l-,1llri+ttr^1\i=fl:''
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Page:5 of 7
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TestReport
No.:CE/2011/84940
Date:.2011h21j
POLYFIL
AG
OBERALLMENDSTRASSE
2OA,CH-6300
ZUG/ SWITZERLAND
Analyticalflow chartof halogencontent
'1) tlarneof theperson
whorEde rEasurerpnt:RitaChen
2) lLarE of the personin chaee of fiEa6urefl€nt:TroyChang
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Weigtrting
andputting
sarple in cell
OrygenBombCombustion
/ Ab6orption
Dilution
to fixedvolufl€
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Pagei 6 of 7
lm[r[
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TestReport
No.: CE/2011/84940
Page:7 ol7
Date:2011h2J01
f][Ilrt]tlltttt!
POLYFIL
AG
2OA,CH-6300
ZUG/ SWITZERLAND
OBERALLMENDSTMSSE
' Thetestedsample/ part ls markedby an anow if its shownon tho photo.'
'* Endof Report
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Dtre
Test Report
Applicant:
Number : TWNC00237228
Littelfuse Philippines Inc.
LIMA Technology Center, Lipa City,
Malvar, Batangas
Date
: Jan 05, 2012
Sample Description:
One (1) group of submitted samples said to be :
Part Description
: Element (Silver Strip Sn Plated)
Part Number
: 079026
Date Sample Received
: Dec 15, 2011
Date Test Started
: Jan 03, 2012
Test Conducted :
As requested by the applicant, for details please refer to attached pages.
Authorized By:
On Behalf Of Intertek Testing Services
Taiwan Limited
K. Y. Liang
Director
This report shall not be reproduced
except in full, without the written
approval of the laboratory.
Page 1 of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00237228
Test Conducted
(Ⅰ) Test Result Summary :
Test Item
Heavy Metal
Cadmium (Cd) content
Lead (Pb) content
Mercury (Hg) content
Chromium VI (Cr6+) content (mg/kg with 50cm2)
Result (ppm)
Silvery Metal
ND
ND
ND
Negative (< 0.02)
Remarks: ppm = Parts per million based on weight of tested sample = mg/kg
ND = Not detected
<
= Less than
mg/kg with 50cm2 = milligram per kilogram with 50 square centimetre
Negative = A negative test result indicated positive observation
was not found at the time of Test.
Responsibility of Chemist : Irene Chiou / Kevin Liu
Date Sample Received
Test Period
: Dec 15, 2011
: Jan 03, 2012 To Jan 05, 2012
(Ⅱ) RoHS Requirement:
Restricted Substances
Cadmium (Cd) Content
Lead (Pb) Content
Mercury (Hg) Content
Chromium VI (Cr6+) Content
Limits
0.01% (100ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for
homogeneous material.
Page 2 of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00237228
Test Conducted
(Ⅲ) Test Method:
Test Item
Cadmium (Cd)
content
Lead (Pb) content
Mercury (Hg)
content
Chromium VI (Cr6+)
content
Test Method
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 7, by microwave
digestion until the tested samples are
totally dissolved and determined by
ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in annex B, by boiling water
extraction and determined by UV-Vis
spectrophotometer.
Reporting Limit
2 ppm
2 ppm
2 ppm
0.02
mg/kg with 50cm2
Remark: Reporting limit = Quantitation limit of analyte in sample
Page 3 of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00237228
Test Conducted
(Ⅳ) Measurement Flowchart:
Test for Cd/Pb/Hg/Chromium (VI)
Reference Standard：IEC 62321 edition 1.0:2008
Sample preparation
Take sample and immerse into Aqua Regia, start to strip plating layer
Stop the stripping procedure upon color change completely
Take the Aqua solution as plating component and stripped body as substrate component
Cd/Pb/Hg
Cr
Polymers /
electronics
Metal
For different
material, digest
the sample with
*1
appropriate acid
By spot test
Negative
Confirm the tested
samples are
totally dissolved
Make up with
deionized water
Analyzed by ICP-OES
6+
*2
Weigh sample
and add
alkaline
solution
Get 50cm2 sample
Definite temp.
extraction
By boiling water
extraction
Cool and filter
the extract
Make up with deionized water and add
diphenyl-carbazide solution
Analyzed by UV-VIS
Remarks:
*1: List of Appropriate Acid：
Acid Added for Digestion
Material
Polymers
HNO3,HCl,HF,H2O2,H3BO3
Metals
HNO3,HCl,HF
Electronics
HNO3,HCl,H2O2,HBF4
*2: If the result of spot test is positive, Chromium VI would be determined as detected.
End of Report
Page 4 of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00237228
Test Conducted
Photo
Page 5 of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Test Report
Applicant:
Number : TWNC00233558
Littelfuse Philippines Inc.
LIMA Technology Center, Lipa City,
Malvar, Batangas
Date
: Nov 25, 2011
Sample Description:
One (1) group of submitted samples said to be :
Part Description
: Solder (Pb above 85%)
Part Number
: 692323
Date Sample Received
: Nov 21, 2011
Date Test Started
: Nov 22, 2011
Test Conducted :
As requested by the applicant, for details please refer to attached pages.
Authorized By:
On Behalf Of Intertek Testing Services
Taiwan Limited
K. Y. Liang
Director
This report shall not be reproduced
except in full, without the written
approval of the laboratory.
Page 1 of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00233558
Test Conducted
(Ⅰ) Test Result Summary :
Test Item
Heavy Metal
Cadmium (Cd) content
Lead (Pb) content
Mercury (Hg) content
Chromium VI (Cr6+) content (mg/kg with 50cm2)
Result (ppm)
Grey Metal
ND
896353
ND
Negative (< 0.02)
Remarks: ppm = Parts per million based on weight of tested sample = mg/kg
ND = Not detected
<
= Less than
mg/kg with 50cm2 = milligram per kilogram with 50 square centimetre
Negative = A negative test result indicated positive observation
was not found at the time of Test.
Responsibility of Chemist : Irene Chiou / Kevin Liu
Date Sample Received
Test Period
: Nov 21, 2011
: Nov 22, 2011 To Nov 25, 2011
(Ⅱ) RoHS Requirement:
Restricted Substances
Cadmium (Cd) Content
Lead (Pb) Content
Mercury (Hg) Content
Chromium VI (Cr6+) Content
Limits
0.01% (100ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for
homogeneous material.
Page 2 of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00233558
Test Conducted
(Ⅲ) Test Method:
Test Item
Cadmium (Cd)
content
Lead (Pb) content
Mercury (Hg)
content
Chromium VI (Cr6+)
content
Test Method
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 7, by microwave
digestion until the tested samples are
totally dissolved and determined by
ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in annex B, by boiling water
extraction and determined by UV-Vis
spectrophotometer.
Reporting Limit
2 ppm
2 ppm
2 ppm
0.02
mg/kg with 50cm2
Remark: Reporting limit = Quantitation limit of analyte in sample
Page 3 of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00233558
Test Conducted
(Ⅳ) Measurement Flowchart:
Test for Cd/Pb/Hg/Chromium (VI)
Reference Standard：IEC 62321 edition 1.0:2008
Sample preparation
Take sample and immerse into Aqua Regia, start to strip plating layer
Stop the stripping procedure upon color change completely
Take the Aqua solution as plating component and stripped body as substrate component
Cd/Pb/Hg
Cr
Metal
For different
material, digest
the sample with
*1
appropriate acid
By spot test
Negative
Confirm the tested
samples are
totally dissolved
Make up with
deionized water
*2
6+
Polymers /
electronics
Weigh sample
and add
alkaline
solution
Get 50cm2 sample
Definite temp.
extraction
By boiling water
extraction
Cool and filter
the extract
Analyzed by ICP-OES
Make up with deionized water and add
diphenyl-carbazide solution
Remarks:
*1: List of Appropriate Acid：
Material
Polymers
Metals
Electronics
Analyzed by UV-VIS
Acid Added for Digestion
HNO3,HCl,HF,H2O2,H3BO3
HNO3,HCl,HF
HNO3,HCl,H2O2,HBF4
*2: If the result of spot test is positive, Chromium VI would be determined as detected.
End of Report
Page 4 of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00233558
Test Conducted
Photo
Page 5 of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Test Report
Applicant:
Number : TWNC00253636
Littelfuse Philippines Inc.
LIMA Technology Center, Lipa City,
Malvar, Batangas
Date
: Apr 24, 2012
Sample Description:
One (1) group of submitted samples said to be :
Part Description
: Black Ink
Part Number
: 425809
Date Sample Received
: Apr 19, 2012
Date Test Started
: Apr 19, 2012
Test Conducted :
As requested by the applicant, for details please refer to attached pages.
Authorized By:
On Behalf Of Intertek Testing Services
Taiwan Limited
K. Y. Liang
Director
This report shall not be reproduced
except in full, without the written
approval of the laboratory.
Page 1 of 9
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00253636
Test Conducted
(Ⅰ) Test Result Summary :
Test Item
Heavy Metal
Cadmium (Cd) content
Lead (Pb) content
Mercury (Hg) content
Chromium VI (Cr6+) content
Polybrominated Biphenyls (PBBs)
Monobrominated Biphenyls (MonoBB)
Dibrominated Biphenyls (DiBB)
Tribrominated Biphenyls (TriBB)
Tetrabrominated Biphenyls (TetraBB)
Pentabrominated Biphenyls (PentaBB)
Hexabrominated Biphenyls (HexaBB)
Heptabrominated Biphenyls (HeptaBB)
Octabrominated Biphenyls (OctaBB)
Nonabrominated Biphenyls (NonaBB)
Decabrominated Biphenyl (DecaBB)
Polybrominated Diphenyl Ethers (PBDEs)
Monobrominated Diphenyl Ethers (MonoBDE)
Dibrominated Diphenyl Ethers (DiBDE)
Tribrominated Diphenyl Ethers (TriBDE)
Tetrabrominated Diphenyl Ethers (TetraBDE)
Pentabrominated Diphenyl Ethers (PentaBDE)
Hexabrominated Diphenyl Ethers (HexaBDE)
Heptabrominated Diphenyl Ethers (HeptaBDE)
Octabrominated Diphenyl Ethers (OctaBDE)
Nonabrominated Diphenyl Ethers (NonaBDE)
Decabrominated Diphenyl Ether (DecaBDE)
Result (ppm)
Black Paste
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Page 2 of 9
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00253636
Test Conducted
(Ⅰ) Test Result Summary :
Test Item
Result (ppm)
Black Paste
Halogen Content
Fluorine (F)
Chlorine (Cl)
Bromine (Br)
Iodine (I)
Phthalates
Di(2-ethylhexyl) Phthalate (DEHP)
Dibutyl Phthalate (DBP)
Benzyl Butyl Phthalate (BBP)
Others
Hexabromocyclododecane (HBCDD)
ND
610
ND
ND
ND
ND
ND
ND
Remarks: ppm = Parts per million based on wet weight of tested sample =
mg/kg
ND = Not detected
Responsibility of Chemist : Irene Chiou / Kevin Liu / Cathy Chen
Date Sample Received
Test Period
: Apr 19, 2012
: Apr 19, 2012 To Apr 24, 2012
(Ⅱ) RoHS Requirement:
Restricted Substances
Cadmium (Cd) Content
Lead (Pb) Content
Mercury (Hg) Content
Chromium VI (Cr6+) Content
Polybrominated Biphenyls (PBBs)
Polybrominated Diphenyl Ehters (PBDEs)
Limits
0.01% (100ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for
homogeneous material.
Page 3 of 9
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00253636
Test Conducted
(Ⅲ) Test Method:
Test Item
Test Method
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
Cadmium (Cd) content
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
Lead (Pb) content
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 7, by microwave
Mercury (Hg) content
digestion until the tested samples
are totally dissolved and determined
by ICP-OES.
With reference to IEC 62321 edition
Chromium VI (Cr6+)
1.0:2008 in annex C, by alkaline
content
digestion and determined by UV-Vis
spectrophotometer.
With reference to IEC 62321 edition
1.0:2008 in annex A, by solvent
Polybrominated
extraction and determined by GC-MS
Biphenyls (PBBs)
and further HPLC-DAD confirmation
when necessary.
With reference to IEC 62321 edition
Polybrominated
1.0:2008 in annex A, by solvent
Diphenyl Ethers
extraction and determined by GC-MS
(PBDEs)
and further HPLC-DAD confirmation
when necessary.
With reference to EN 14582:2007 by
Halogen Content
calorimetric bomb with oxygen and
determined by Ion Chromatograph.
With reference to EN 14372: 2004, by
Phthalates
solvent extraction and determined by
GC-MS.
With reference to USEPA 3540C, by
Hexabromocyclododecane
solvent extraction and determined by
(HBCDD)
GC-MSD.
Reporting Limit
2 ppm
2 ppm
2 ppm
1 ppm
5 ppm
5 ppm
50 ppm
10 ppm
10 ppm
Remark: Reporting limit = Quantitation limit of analyte in sample
Page 4 of 9
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00253636
Test Conducted
(Ⅳ) Measurement Flowchart:
Test for Cd/Pb/Hg/Chromium (VI)/PBBS/PBDES Contents
Reference Standard: IEC 62321 edition 1.0:2008
Sample preparation
For non-metal part
For metal part
Take sample and immerse into Aqua Regia, start to strip plating layer
Stop the stripping procedure upon color change completely
Take the Aqua solution as plating component and stripped body as substrate component
Cd/Pb/Hg
Cr
Weigh sample and
add organic solvent
By spot test
Negative
Confirm the tested
samples are
totally dissolved
Make up with
deionized water
PBBs/PBDEs
Polymers /
electronics
Metal
For different
material, digest
the sample with
*1
appropriate acid
6+
Get 50cm2 sample
By boiling water
extraction
*2
Weigh sample
and add
alkaline
solution
By Soxhlet
extraction or
Solvent extraction
Definite temp.
extraction
Cool and filter
the extract
Analyzed by ICP-OES
Concentrate the
extract and make up
with organic
solvent
Analyzed by GC-MSD
Make up with deionized
water and add diphenylcarbazide solution
Analyzed by UV-VIS
Remarks:
*1: List of Appropriate Acid：
Acid Added for Digestion
Material
Polymers
HNO3,HCl,HF,H2O2,H3BO3
Metals
HNO3,HCl,HF
Electronics
HNO3,HCl,H2O2,HBF4
*2: If the result of spot test is positive, Chromium VI would be determined as detected.
Page 5 of 9
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00253636
Test Conducted
(Ⅳ) Measurement Flowchart:
Test for Halogen Content
Reference Standard：EN 14582
Sampling/grinding or
cutting
Add absorbent in a
combustion flask &
place weighed sample in
equipment
Fill oxygen into
calorimetric bomb
Ignite then leave the
bomb at room
temperature
Transfer the absorbent
into a volumetric flask
Make up with deionized
water
Analyzed by ion
chromatography
Page 6 of 9
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00253636
Test Conducted
(Ⅳ) Measurement Flowchart:
Test For Phthalates Contents
Reference Method: EN 14372: 2004
Sampling/grinding or
cutting
Weigh sample and add
organic solvent
By solvent extraction
Concentrate the extract
and make up with
organic solvent
Analyzed by GC-MSD
Page 7 of 9
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00253636
Test Conducted
(Ⅳ) Measurement Flowchart:
Test For Hexabromocyclododecane (HBCDD)
Reference Standard：USEPA 3540C
Sampling/grinding or cutting
Weigh sample and add organic
solvent
By soxhlet extraction
Concentrate the extract and
make up with organic solvent
Analyzed by GC-MSD
End of Report
Page 8 of 9
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00253636
Test Conducted
Photo
Page 9 of 9
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401