ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: Nano2 Fuse Product #: 451-Sn Series Issue Date: December 4, 2012 It is hereby certified by Littelfuse, Inc. that there is neither RoHS (EU Directive 2002/95/EC, 2011/65/EU)-restricted substance nor such use, for materials to be used for unit parts, for packing/packaging materials, and for additives and the like in the manufacturing processes. In addition, it is hereby reported to you that the parts and sub-materials, the materials to be used for unit parts, the packing/packaging materials, and the additives and the like in the manufacturing processes, are all composed of the following components. Issued by: <Global EHS Engineer> (1) Parts, sub-materials and unit parts This document covers the Nano2 Fuse - FA RoHS-Compliant series products manufactured by Littelfuse, Inc. < Raw Materials Used Please see Table 1 (2) The ICP data on all measurable substances Please see appropriate pages as identifed in Table 1 Remarks: Pb (lead) contained in the high temperature melting solder > 85% and is categorized as exempt under section 7a of the RoHS Annex. Form 585-047 Rev. A 1 2/21/06 Table 1: List of Raw Materials covered by this report Total Parts 1 2 3 4 5 6 7 Raw Material Part Number 910-238 Frequenta C221 (909-434) 082xxx 692321 087266 425809 N/A Raw Material Description Cap Body – Ceramic Tube Element- 5% by weight Ag clad Cu Solder Adhesive - RoHS Ink-Black - RoHS Tin 2 Page(s) 3-10 11-34 35-39 40-45 46-55 56-64 65-69 nown ForQueSti PleaseCo TestReport ith sGS No.: CH2O1Z14UEA Date: 2012J02104Page.l ol 24 CERAMTECGMBH 15 D-91207LAUF,GERMANY MULTIFUNCTIONAL CERAMICS LUITPOLDSTRASSE r|| tUi||l]]$t The followlng samplo{a)was/weresubmitted and identified by/on behalfofthe cllent as: SampleDe6ciption Styl€/ltem No. SampleRecejvingDate Testing Period CERAMIC FREQUENTA C22'1 2012t01t30 2012J01|30 TO 201Z O2t04 T€6i Result(s) : Pleasereferto nextpage(s). Conclusion Lead thetestresultsof Cadmium, samples, : Basedontheperfomedtestsonsubmitted limits as setby PBDES comply with the Cr(Vl), PBBS and Mercury, Hexavalent Chromium 2002/95/EC. 2011/65/EU Annexll; recasting RoHSDnective gN|tad ftrltd TestReport Page:2of 24 D e,2012102104 No.:CE/201214846A Llmt t GMBH CERAMTEC LAUF.GERMANY 15D-91207 MULTIFUNCTIONAL CERAMICSLUITPOLDSTMSSE t]||!|r] Test ReBult{s} PARTllAMENo.1 : CREAI, CERAMIC mg/Kg With referenc€to IEC62321: 2008and 2 Result No.t n.o, to IEC62321:2008and mgKg Withreference pedormed by ICP-AES. to IEC62321:2008and (Hg) mg/Kg Withreference lllercury oenotmeo Dvtut -AEn, mg/Kg Witheferenceto IEC62321:2008and Cr(Vl) Chromium Hexavalent per{ormedby UV-VIS. (PCBS) m9Kg With referenceto US EPA3540c Biphenyls Polychlorinated bY Analysis wasperlormed method. (CASNo.:133+363) GC/MS. to Us EPA3540c mgKg Withreference Terphenyls Polychlorinated bY Analysis wa6performed method. (PCTs) 2 n.d. 1000 2 n_o. 1000 2 n.d. 1000 Test ltem(s) Cadmium(Cd) Unit Method Lead(Pb) MDL n.d. 0.5 n.d. 5 n.d. 0.01 n.d. 10 n.d. 10 n.d. 3 n.d. GC/[rS. to USEPA3540C mS/kS Withreference wasperformed by method. Analy6is GC/tMS. o/. to USEPA3g0C Withreference Alkanes,C1G13,chloro(short wasperformedbY Analysi6 (CAS method. Paraffins) ChainChlorinated GC/MS. No.:85535-44-8) to Us EPA3540c: m9Kg Withreference Perfluorooctanesulfonates 1996methodfor PFOSContent. (PFOS-Acid, MetalSalt,Amide) wasperfomedby LC/MS. Analysis to USEPA3540C: mg/Kg Withreference PFOA(CASNo.:335€7-1) '1996methodfor PFOAContent. bYLC/MS. Analysis wa6performed Naphthalene Polychlorinated (PCNs) ormaldehyde(CAS No.: 50-00-0) mg/kg With reference to ISO 17226-1(200A). Analysiswas perfomed by HPLC/DAD PVC performed bYFTIRand Analysiswas Test, FLAME Negative Limit 100 TestReport No.: CE/20'1214846ADale:201202104 Page 3 of 24 r ]lfltl|fl [tu||llll CERAMTEC GMBH 15D-91207 LAUF,GERMANY CERAMICSLUITPOLDSTMSSE I\4ULTIFUNCTIOML Testltem(s) Mothod Unit Analysis to EN 14372. Withreference ,nasperformedby GC/MS. % Witheferenceto EN 14372.Analysis lva6per{ormedby GC/MS. ok to EN 14372.Analysis Withreference DIDP(Di-isodecylphthalate)(CAS wasperformed by GC/MS. No.:26761-40-0) o/o Withreference to EN14372.Analysis DINP(Di-isononylphthalate)(CAS per{ormed was by GC/irS. No.r2855312-0) to EN 14372.Analysis phthalate) % With reference (cAS (Di-n-octyl DNOP performed by GC/MS. was 11744-0) No.: to EN14372.Analysis (CASNo.: % Withreference DBP(Dibutylphthalate) \ras performedby GC/MS. u-74-2) mg/Kg With referencetb US EPA8270D dibromodiphenyl Monomethyl bY Analysis \rasperformed method. methane(DBBT) GC/MS. mg/Kg With referenceio US EPA8270D dichlorodiphenyl Monomethyl by Analysis wasperformed method. methane(Ugilecl21) (CAS BBP(Benzylbdyl phthalate) No.:8568-4 DEHP(Di-(2-ethylheryD phthalate) (cAs No.:117-81-7) % MDL Result No.1 0.003 n.d. 0.003 n.d. 0.01 0.01 n.d. 0.003 n.d. 0.003 n.d. 0.5 n.d. 0.5 n.d. 0.5 n.o. 0.03 n.d. 0.03 n.d. I n.d. cc/Ms. tetrachlorodiPhenYl mg/Kg With referenceto US EPA8270D lronomethyl wasperfomedbY method. Analysis methane(Ugilec141) GC/MS. compounds Organic.tln TnbutylTin(TBT) Tin (TphT) Triphenyl 3. mg/kg Wth referenceto DIN38407-1 perfomed bY GC/FPD. was Analysis 3. mg/kg ul,/ithreferenceto DIN38407-1 by GC/FPDwasperformed Analysis Halons to l-JSEPA5021 (CASNo.:353-59-3) m9Kg Withreference Halon-1211 bY Analysis wasperformed method. GC/MS. mg/Kg With referenceto US EPA5021 (CASNo.:7563-8) Haion-1301 method.AnalysiswasPerformedbY GC/MS. to USEPA5021 (CASNo.:124-73-2) m9Kg Withreference Halon-2402 bY wasPedormed Analysis method. GC/t!ts. n-d. n.d. 4r:' r:2.J1.3!.101!ic ,1-3.3.9_19'l*:t l?:L rrY :-s!,11 ur]r}il Limit scs TestReport No.I CE2012/14846AOalet2UA1ZU Paget4of 24 |l] CEMMTECGMBH 15D.91207LAUF,GERMANY LUITPOLDSTMSSE I,ULTIFUNCTIONAL CERAIVICS unit T€6t ltem(s) method MDL |lfl Result No.'l Haloqen mg/Kg Withreferenceto BS EN 1458212007. (F) (CASNo.: Halogen-Fluorine 14762-94-A) (cl) (cAs No.: Halogen-Chlorine 22537-15-11 (Br)(CASNo.: Halogen-Bromine 10097-32-2) by lC. Analysis wasperformed . mgKg With referenceto BS EN 1458212007 Analysis wasperformed by lC. . mg/Kg With referenceto BS EN 14582:2007 Analysis wasperformed by lC. . mg/Kg With referenceto BS EN 14582.2007 wasperformed by lC. Analysis Halogenlodine(l) (CAS No.: 1436244-8) Asbestos (CASNo.:77536-66-4) Actinolite % (CASNo.:12172-73-5) Amosite (CASNo.:n 53&67 Anthophyllite (CASNo.r12001-29-5) Chrysotile % Crocidolite(CASNo.: 12001-284\ o/o (CASNo.:77536€8S) Tremolite % com€n{ , t ll r+: :,il 9: Ltr Withreference to EPA600/R-93/116 wasperformed by method. Analysis SM.PLII andXRD. with reference to EPA600/R-93/116 method.Analysiswasperformedby SM,PLMandXRD. Withreference to EPA600/R-93/116 Analysis wasperformed by method. SI/| PLMand)(RD. With referenceto EPA600/R-93/1 16 by method. Analysis wasperformed SM,PL[, andXRD. Withreference to EPA600/R-93/116 method. Analysis wasperfomedby Sl,l,PLMandXRD. With referenceto EPA600/R-93n16 method. Analysis wasperformed by SM.PLl andXRD. {lj i :-: rh s ddcumm s 'suad by ihe comoanvslhrd b 's cenedrCmdiotrsdr Sede pdtrd ovedeatava'she i d'c'or '$$ de *seF 50 n.d. 50 n.d. 50 n.d. 50 n.d. 'I Negative I Negative 'I Negative 1 Negative Negative Negative ]|lt]t Limit TestReport No.: CE/2012i 148464 Dale:201ZO2|M Page:5of24 n] CEMMTECGMBH 15D-9'I207 LAUF,GERI,|ANY LUITPOLDSTRASSE MULTIFUNCTIONALCERAI/!ICS Tost ltefi(s) Method Unit Sumof PBB6 Monobromobiphenyl Dibromobiphenyl MDL 5 fdbromobiphenyl Tetrabromobiphenyl Pentabrcmobiphenyl Hex€bromobiphenyl Heptabromobiphenyl Oclabromobiphenyl Nonabromobiphenyl Decabromobiphenyl Sumof PBDE3 Monobromodiphenyl ether Dibromodiphenyl ether €ther f ribromodiphenyl Tetrabromodiphenyl ether ether Pentabromodiphenyl Hexabromodiphenyl ether Heptabromodiphenyl ether ether Octabromodiphenyl Nonabromodiphenyl eth€r Decabromodiphenyl ether Withreference to IEC62321:2008and m9Kg perfomed by GC/MS. 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 Result No.'l n,o, mg/Kg with referenceto LFGB82.02-2. 3): 4-CHLORO-O-TOLUIDINE (CAS No.: 9569-2) Analysiswas p€rfomed by GC/MS. (CAS 4): 2-NAPHTHYLAMINE mg/kg with reference to LFGB82.02-2. wasperformed by GC/MS. No.:9'l-59-8) Analysis 5): O-A[4INOMOTOLUENE(CAS mg/Kg Withreference to LFGB82.02-2. Analysis wasperformed by GC/MS. No.: 97-56-3) , 1 / - ' i - . - j _ r r d I'jr sdidionbsFsdstidbsrsf.tuy codp.ny 6y uiaurhodzei!5 b6r of. roee,y or birstct on or me onient o hoderorth€ doamenrtadusedh Limit 1000 n.d. n.d. n.d. n.o. n.dn.d. n.d. n.d. n.o. n.dn.d. n.d. n.d. n.d. n-d. 5 5 n.d. n.d. n.d. n.o. n.d. n.d. 3 n.d. 3 n.d. ,zo '1):4-AMINODIPHENYL (CASNo.: mg/Kg Withreference to LFGB82.02-2. 9247-1) Analysis w€sperformed by GC/MS(CASNo.i92-87- mg/kg Withreference 2rlBENZIOINE to LFGB82.02-2. Analysis wasperformed by GC/IVS. tlllfllllllll n.o. 3 n.d. 3 n-d. 1000 Test Report Pase : 6of24 o^e.2o12tozo4 No'cEt2o1z14u6A ll CERAMTEC GMBH LAUF,GERI'ANY 15D.91207 CERAMICSLUITPOLDSTRASSE MULTIFUNCTTONAL [alllllll[llllu!! 3 Result No.l n.d. 3 n.d. 3 n.d. 3 n.d. '10): 3,3'-DICHLOROBENZIDINE mg/Kg With refefenceto LFGB82.02-2. Analysiswas perfomed by GC/MS. (CASNo.:91-94-1) 3 n.o. to LFGB82.02-2. mg/Kg Withreference 11):3,3'-DIMETHOXYBENZIDINE by GC/MS. wasperformed Analysis (CASNo.:119-90{) to LFGB82.02-2. 12):3,3'-DIMETHYLBENZIDINEmsyKg Withreference bYGC/MS. Analysis wa6performed (CASNo.:119-93-7) 3 n.d. 3 n.d- mg/Kg With referenceto LFGB82.02-2. 13): 3,3'-DlMETHYL4,4Analysiswas performedby GC/MS. DIAMINODIPHENYLMETHANE (CAS No.: 838€8-0) 3 n.d. Test ltem(s) Unit MDL Method to LFGB82.02-2. mg/Kg Withreference 6):2.AMlNO-4-NITROTOLUENE by GC/l\rS. Analysis waspertormed (CASNo.:99-s5-8) to LFGB 82.02-2. (CAs With reference No.: mg/Kg 7): P4HLORoANILINE performed by GC/MS. Analysis wBs 106-47-8) to LFGB82.02-2. (CAS mg/Kg with reference 8):2,+DIAIVINOANISOLE wasperformed by GC/MS. Analysis No.:615-054) LFGB 82.02-2. With reference to m9Kg 9):4,4Analysiswas performedby GC/I\IS. DIAIVINODIPHENYLMETHANE (CASNo.:101-77-9) (2-METHoXY- mg/Kg Withreference to LFGB82.02-2. 14):P-CRESIDINE by GC/MS. (CASNo.: Analysis wasperformed s-ITETHYLANILINE) 120-71-a) '15)r4,4'-METHYLENE-B|Sto LFGB82.02-2. (2mgKg Withreference pertormed was bYGC/lrS. Analysis (CASNo.: CHLOROANILINE) 101-144) (CAS to LFGB82.02-2. mg/Kg Withreference 16):4,4-OXYDIANILINE performed bYGC/MS. was Analysis 101-80{) No.: '17):4,4'-THIODIANILINE to LFGB82.02-2. (CAS mg/Kg with reference by GC/MS. wasperformed Analysis No.:139€5-1) n.d. 3 n.o. 3 n.d. 3 n.d. mg/kg With referenceto LFGB82.02-2. Analysiswas performedbYGC/IVS. 3 n.d. to LFGB82.02-2. 19):2,+TOLUYLENEDIAIVINE mg/Kg Withreference bYGC/MS. Analysis $/asperformed (CASNo.r95€G7) to LFGB82.02-2. 20)r2,4,5.TRllVETHYLANlLlNEmgkg Withreference Analysis$rasperformedbYGC/MS. (CASNo.:137-17-7) to LFGB82.02-2. (CASNo.:90- mgKg Withreference 21):O.ANISIDINE performed by Gc/llls was Analysis 04{) 3 n.d. 3 n.d. 3 n.d. 18): O-TOLUIDINE(CAS No.: 95534) .,rr'41.;!!, [email protected]. 4,!a1ta {i trli Limit Test Report No.: CE/201214846ADaIe:2012102104Page,7 of 24 Il!t |||lu[llll CERAMTEC GMBH 15D.91207 LAUF,GERMANY CERAMICSLUITPOLDSTMSSE MULTIFUNCTIONAL Test ltem(s) Unit 22)rP-AMINOAZOBENzENE (CASNo.:60-09-3) (CASNo.:9523):2,4-XYLIDINE 68-1) m9Kg Method MDL R€ult Withreference to LFGB82.02-2. by GC/lllS. Analysis waspertormed to LFGB82.02-2. mg/Kg Withreference Analysis wasperfomedby GC/MS. to LFGB82.02-2. mg/Kg with reference Analysis wasperformed by GC/[iS. 3 No.1 n.d. 3 n.d. 3 n.d. mg/kg Withreference to USEPA5021 by method. Analysis wasperformed GC/MS. (CASNo.: mg/Kg Withrefefence to USEPA5021 Chlorof luorocarbon-12 Analysis wasperfomedby method. 75-71-A) GC/MS. 113(CASNo.: mg/Kg With referenceto US EPA5021 Chlorofluorocarbonby method. Analysis wasperformed 76-13-1) GC/t/lS. to USEPA5021 14 (CAS No.: mg/Kg Withreference Chlorofluorocalbon-'l wasperformed by method. Analy6is 76-14-21 GC/tS. to USEPA5021 luorocarbon-1 15 (CASNo.: mg/kg Withreference Chlorof by Analysis wasperformed method. 76-153) GC/tS. Grouplll mg/Kg With referenceto US EPA5021 luoroca6on-1 3 (CASNo.: Chlorof by Analysis wasperformed method. 75-72-9) GC/MS. (CASNo. mg/Kg With referenceto US EPA5021 Chlorofluoroca6on-111 by wasperformed method. Analysis 354-56-3) GC/MS, to us EPA5021 12(CASNo.: mg/Kg with reference Chlorofluorocarbon-1 by Analysis wasperformed method. 76-12-O) 'I n.d. 1 n-d- 1 n.d. 'I n.d. 'l n.d. 24): 2,6-XYLIDINE(CAS No.: 8762-7') CFC's(Chlorof,uorocarbons) GroupI 11 (CASNo.: Chlorofluorocarbon75.69-4) n.d. n.d. n.d. GC/MS, to USEPA5021 I (CASNo.: mg/Kg Withreference luoroca6on-21 Chlorof bY wasperformed Analysis method. 422-78-6) GC/MS. 1 n.o, Limit ll Test Report No.:CE/20'1214846ADale:2012j0A04 Page:8 of 24 CERAMTEC GMBH 15D.9'1207 LAUF,GERMANY CERAMICSLUITPOLDSTMSSE MULTIFUNCTIONAL Tost ltem(s) Unit Method to USEPA5021 12(CASNo.i mgikg Withreference Chlorofl uorocarbon-2 by method. Analysis waspertormed 3182-26-1) GCiMS. to USEPA502'1 luorocarbon-2l 3 (CASNo.: mg/Kg Withreference Chlorof wasperfomedby method. Analysis 2354-06-5) GC/MS. (CASNo.: mg/Kg With referenceto US EPA5021 luorocarbon-214 Chlorof wasperfomedby method. Analysis 29255-3'1-0) GC/MS, (CASNo.: mg/Kg With feferenceto US EPA502'l Chlorofluorocarbon-215 Analysis wasperformed by method. 425943-2) GC/MS. (CAS No.i mg/kg Withreference to USEPA5021 Chlorofluorocarbon-216 Analysis waspefo.medby method. ffil-97-2) GCitlts. (CASNo.: mEks Withreference to USEPA5021 luorocarbon-217 Chlorof method.Analysiswasperformedby 422-864\ GC/MS. (Chlorinate hydrocarbon) CHCs (CAs to USEPA5021 mg/Kg Withreference 1,1,1,2-Tetrachloroethane wasperfomedby method. Analysis No.r63G20€) GC/MS. '1,'1, to USEPA5021 (CASNo.l m!yKg Withrefefence 1-Trichloroethane wasperfonned by method. Analysi6 71-sffi) GC/MS. to USEPA5021 (CAS mg/Kg Wth reference 1,1,2,2-Tetrachloroethane bY Analysis wa6pertormed method. No.:7$34-5) GC/tMS. to uS EPA5021 (CASNo.: mgikg Withreference 1,1,2-Trichloroethane by waspertormed methodAnalysis 79-00-5) GC/MS. to USEPA502'1 (CASNo.:75- mgi'kg Withreference 1,1-Dichloroethane bY wasperformed method. Analysis 34-3) GC/|VS. '1 referenceto US EPA5021 mg/kg With (CAS No.: 75,1-Dichlooethene bY wasPerformed method. Analysis 3s4) GC/MS. MDL R€ult No.1 n.d. n.d. n.d. 1 n.d. 'I n.d. 1 n.d. 1 n.d. 1 n.o. n.d. n.d. n.d. 'I n.d. Limit scs Test Report No.: CE|201Z1484SADdet2O12l02lU Page:9 of 24 I| L |l|l[l[tilll GMBH CERAMTEC LAUF,GERMANY 15D.91207 CERAMICSLUITPOLDSTMSSE MULTIFUNCTIONAL Test ltem(s) '1,1-Dichloropropene (CASNo.: 1 Result No.t n.o. '1 n.o. 1 n.o. 1 n.o. 1 n.d. 1 n.o. MDL Method Unit to USEPA5021 m9Kg Withreference wasperformedbY method. Analysis 56+546) GC/MS. to USEPA5021 (CAsNo.: mgKg Withreference 1,2,3-Tichloropropane method.AnalysiswasperfomedbY 96-184) GC/MS. to USEPA5021 With reference (CASNo.: mg/Kg 1,2-Dichloroethane bY wasperformed method. Analysis 1O74e2l GC/MS. (CASNo.: mg/Kg with referenceto tJSEPA5021 1,2-Dichloropropane wasperfomedby method. Analy6is 78€7-5) GC/MS. (CASNo.: m!yKg With referenceto US EPA5021 1,3-Dichloropropane wasperfomedbY method. Analy6is 142-28.91 GC/MS. to IJSEPA5021 (CASNo.: mg/Kg Withreference 2,2-Dichloropropane method.Analysiswasperformedby 5S+20-71 GC/MS. referenceto US EPA5021 (CAS m(yKg With No.: Ca6ontetrachlodde waspedomedbY method. Analysis 56-23-s) GC/MS. (CASNo.:75-00-3) mg/Kg Withreference to USEPA502'1 Chloroethane bY wasperformed method. Analysis GC/MS. (CASNo.:6766-3) to USEPA5021 mg/kg Withreference Chloroform bY wasPerformed method. Analysis n,o. n.d'I n.d. mg/Kg With referenceto US EPA502! bY wEsPerformed Analysis method. GC/MS. to USEPA5021 mg/Kg Withreference bY wasPerformed Analysis method. GC/MS. 1 n.d. ,l n.d. to USEPA502'l (CAsNo.: mg/Kg Withreferenc€ cis-1,lDichloropropene bY wasPerfomed Analysis method. 1006141-5) GC/MS. 1 n.d. cc/Ms. (CASNo.;74-87Chloromethane 3) (CASNo.i cis-1,2-Dichloroethene 156-59-2) (Nevr3F 'ieL{'r}: r; I n:5n l:r 33i1 Limit Test Report No.:C92012/14846A Oale|2O12JO2|MPage: 10 of 24 t m CERAMTECGMBH CERAMICS LUITPOLDSTMSSE15 D-91207LAUF,GERMANY MULTIFUNCTIONAL Test ltem(s) Unit Method mg/Kg With referenceto US EPA5021 method.An€lysis\r€s performedbY GC/MS. (CAS No.:75- mg/kg With referenceto US EPA5021 Methylene Chloride by wasperformed method. Analysis 09-2) GC/|VS. (CASNo.:127- mg/kS With referenceto US EPA5021 Tetrachloroethene bY Analysis wasperformed method. 184) GC/tVlS. (CAS mg/kg With referenceto US EPA5021 trane1,2-Dichloroethene bY Analysis wasPerformed method. No.:15660-5) GC/MS. (CAS mg/Kg With referenceto US EPA5021 trans-l,3-Dichloropropene method.Analysis\ /asperfofmedby No.:10061-024) GC/MS. (CASNo.:7$ mg/Kg with referenceto us EPA5021 Trichloroethylene bY Analysis wasperformed method. 01-6) GC/MS. HCFca (Hydrochlorotluorccarbons) mg/Kg Withreferenceto US EPA5021 HCFC-2l (CAS No.: 75-434) wasperfomedbY Analysis method. GC/MS. m9Kg With referenceto US EPA5021 (CAS No.: 75-4S) HCFC-22 bY wasperformed Analy6is method. GC/IVS, mg/Kg Witll referenc€to US EPA502'! (CASNo.:59!70'4) HCFC-31 method.AnalysiswasPerformedbY MDL HCFC-121(CAS No.: 3gl4-3) mg/Kg With referenceto US EPA5021 wasperfomedbY method. Analysis GC/MS. to USEPAs021 (CASNo.:354-21-2) mg/Kg vVitlrreference HcFc-122 bY w€sPerfomed Analysis method. GC/MS. No.1 Limit n.d. (CASNo.: Hexachlorobutadiene 87$8-3) GC/lrs. Result [tlllll I n.d. 1 n.d. 1 n.d. I n.d. 1 n.d. n.o. 1 n.d- 1 n.d. 'I n.d. n.d. *" ^ - " - -- "'" strFi#::i"lT "":;-;":xi.:;,","r# ;:::il:::$ ::iI::il ; ":l;ild ^ffi3"3ffx;#i*"is:;";;*:;"1;rr+;#"8:*ili;i"3-f$$ r;1ri:.1'ff1r16if"r"r;"idi:pi**#:g";,i";.-,,: r"is*r#rjnr"r.":"::;j.,;\lli:iTrr.5;,3::r.-"i'l#jili:n:*.ai."l;"*'ru;*#iair::'sih;* Test Report No.: CE/201214846A Date: 2012102104Page: 11 oI 24 ltfl ||[I|t l[]tr CERAMTECGMBH 15 D-91207LAUF,GERMANY CERAMICS LUITPOLDSTRASSE MULTIFUNCTIONAL Test ltem(s) (CASNo.:306-83-2) HCFC-123 Unit lrethod MDL n.d. mg/Kg Withreferenc€to US EPA502'1 method. Analysis wasperfomedby GC/MS. (CASNo.:2837-89-0) mg/Kg With referenceto US EPA502'1 HCFC-'124 wasperformed by method. Analysis GC/t S. (CASNo.r359-28-4) mS/kg Withreference to tJSEPA5021 HCFC-131 method.Analysiswasperformedby GC/MS. to USEPA5021 HCFCI32b(CASNo.:1649-08-7) mg/kg Withreference wasperformed by method. Analysis GC/MS. (cAs No.:75-88-7) mg/Kg With referenceto US EPA5021 HCFC-133a method.Analysiswasperformedby GC/MS. HCFC-141b {CASNo.:1717-00€) mg/Kg With referenceto US EPA5021 Analysis wasperformed by method. GC/trs. to USEPA5021 mg/Kg Withreference HCFCI42b(CASNo.:7568-3) by Analysis wasperformed methodGC/t S. (CASNo.:422-26-4) mgKg Withreference to USEPA5021 HCFC-221 wasperformed by method. Analy6is GC/t S. to USEPA5021 mg/Kg Withreference HCFC-222(CAS No.: 422.491) by Analysis w€spertormed method. GC/t!ts. to USEPA5021 mg/kg with reference HCFC-223 {CASNo.:422-526) by Analysis wasperformed method. GC/MS, (CASNo.:422-54-8) mg/Kg With referenceto US EPA5021 HCFC-224 method.AnalysiswasperformedbY GC/MS. to USEPA5021 (CASNo.:422-56-0)mg/kg Withreference HCFC-225C€ bY wasPertormed Analysis method. GC/lrs. Result No.1 n.d. 1 n.d. 1 n.o. 1 n.d. 1 n.d. I n.d. 1 n.d. n.d. n.d. n.d. ,] n.d. Llmit l scs Test Report No.: CE|2O1Z14846ADaIe:201ZO2|U Page: 12 ol 24 ||]u||||][llllllll CERAMTEC GMBH 15D-91207 LAUF,GERMANY CERAMICSLUITPOLDSTMSSE MULTIFUNCTIOML lest ltem(s) unit (CASNo.:507-55-1) mgilg HCFC-22scb Method MOL Result No,1 n.d. Withreference to USEPA5021 by Analysis waspedormed method. GC/trs. (CASNo.:43'1-87-8) HCFC-226 to USEPA5021 mg/Kg Withreference method. Analysi6 wasperfomedbY GC/MS. (CASNo.r42t-%-3) mg/Kg With referenceto US EPA5021 HCFC-231 by Analysis wasperformed method. GC/MS. (CASNo.:460-89-9) mg/Kg With referenc€to US EPA5021 HCFC-232 by method. Analysis wasperformed GC/MS. (CASNo.:7125-84-0) mg/Kg With refe.enceto US EPA5021 HCFC-233 by methodAnalysis wasperformed GC/[iS. (CASNo.:425-94-5) mg/Kg Withreference to USEPA5021 HCFC-234 by method. Analysis wa6pertormed GCi[rs. m9Kg With referenceto US EPA5021 HCFC-235 {CASNo.:460-9-4) Analysis wasperfomedby method. GC/MS. to USEPA5021 mgKg Withreference HCFC-241(CAS No.: 6€6-27-3) wasperfomedby method. Analy6is GC/MS. msyKg With referenceto US EPA5021 HCFC-242(CAS No.r4€0€3-9) method.Analysiswasperformedby GC/MS. (cAs With referenceto US EPA5021 m9Kg No.: 46059-5) HoFC-243 method.AnalysiswasPerformedbY I n.d- 1 n.d. 1 n.d. I n.d. 1 n.d. 1 n.d- 1 n,o. n.o_ n.d. GC/l\rs. mg/kg With referenceto Us EPA5021 HCFC-244 ',!asperformed by Analysis method. GC/MS. (CASNo.:42'l-41-0) mg/Kg Withreferenc€ to Us EPA5021 HCFC-25'1 bY wasPerformed Analysis method. GC/MS. I n.d. 1 n.d. Limit Test Report No.: CE12012,148464D ale .2O1Z0ZU Page 13 of 24 tl CEMMTECGMBH 15D-91207 LAUF,GERMANY MULTIFUNCTIONAL CERAMICSLUITPOLDSTRASSE Test ltem(6) HCFC-252{CAS No.: 819-001) Unit Method MDL [ |l[ [lll||llNt R.sult No.'l Limit n.d. mg/Kg Withreference to uS EPA5021 Analysis wasperformed by method. GC/MS. (CASNo.:,16G.35-5) mg/Kg With refefenceto us EPA5021 HCFC-253 method. Analysis wasperfomedby GC/MS. (CASNo.:420-97-3) mg/Kg Withreferenceto US EPA5021 HCFC-261 wasperformed by method. Analysis n.o. n.d. GC/l\rs. (CASNo.:421-02-03) mg/Kg Withreference to USEPA5021 HCFC-262 by method. Analysis wasperformed GC/MS. (CASNo.:430-55-7) mg/Kg With referenc€to US EPA5021 HCFC-271 method. Analysis wasperfomedby GC/MS. 1 n.d. 1 n.d. Note : '1. mg/kg= ppm i 0.1wf/o= 1000ppm 2. n.d. = Not Detected 3. MDL = MethodDeteclionLimit 4."-"=NotRegulated 5. " = Qualitativeanalysis(No Unit) / Positive= Detectable 6. Negative= Undetectable 7. Asbestos: Negative= "< 1.0%", Positive='> 1.0%" PFOSRefe.enceInformatlon: POPS- (EU)7572010 products or in semi-finished above0.001%('1oppm), in concedtrations or preparations Outlawing PFOSas substances above1Fg/m'z in textilesor othercoatedmaterials articlesor partsat a levelabove0.1%(lOOOppm), Test Report No.I CEi2012/14846ADate| 2012102104Page'.14d 24 l|| CERAI,iITEC GIVBH 15 D.91207LAUF,GERMANY CERAMICS LUITPOLDSTRASSE MULTIFUNCTIONAL |!l||lflttl||rtl '1) Thes€samplesweredissolvedtotallyby pre-conditioning methodaccordingto belowflow chart ( Cr"' test method excluded) 2) Nameof the personwho mademeasurementClimbgre€tYang 3) Nameof the personin charg€of measulemenlTroyChang SampleMeasurement by suitable acid Aciddigestion on difierent s€mple dep€nded mateial(asbelowtable) digestion with Microwave HNq/HCUHF amountof Addappropriate reagent digestion Heatto appropriate temperatureto extract Cool,filterdige6tate AlkaliFusion HCltodissolve throughfilter ICP-AES DigestionAcid SampleMaterial S'teel,coppet aluminum,solder Aqua regia,HNO3,HCl,HF,HrO, HNO3/HF Glass palladium, ceramic Aquaregia Gold,platinum, Silver HN03 Plastic HrOr,HNO3,HCI H2SO4, Others Anyacidto totaldigestion measurethe absorbance at 540nmby UV-VIS Test Report No. CE/2012J14846A Dale:2012tO21O4 Page : 15 of 24 tt||]t CERAMTECGMBH CERAMICS LUITPOLDSTMSSE15 D.91207LAUF' GERIVANY IJULTIFUNCTIONAL |l0Lllllllllull Analyticalflow chartof soxhletextractlon(LC/MS)procedure I I RomanWong Nameofthepersonwhomademeasulement: TroyChang peBon of measurement: in charge Nameof the ' Benzotriazolo ( Testltems:PFOSTPFOA ) SamplepretreatmenuseParation I Data *ffirffiN,f*,tr ffiffiffiffiN'g'gffirft rrh'rr)1]irf j-l I L,*!qq9lE?r1r,11 i'99!ol!:,-:147_ !!rY:4r.lY -- ,- ;;;";;; TestReport No.: CE201214846A Oale: 2012102104Page: 16 oI 24 CERAMTEC GMBH LAUF,GERMANY 15D-91207 LUITPoLDSTRASSE CERAIVICS I,,IULTIFUNCTIoNAL rtr||[ttllllllu:rl| Chlorinated Flame retardant analytical flow chart '1) Nameof thepersonwhomademeasufement: BarfyTseng Troychang 2) Nameof thepersonin chargeof mea6ufement: I r method: USEPA8270D,US EPA3540 RefeGnce PCTS, Mirex,CP,MCCP Testltems:PCBS.PCNS, -- *-" "'" * "' :"1"*;;;d 'ifi;i{i-"i:. iljlJii."; ;ffi ;' ; T;*; {#i:;':T,:":iH :irk;,t"'iriF,;"Fd#lfl:'h,lit*q+tdr.tr:i#q.#$Etlt'*i{*d .cL"i""ro.o"*,0a,..'"s1,rod"earcl -?r.,r"'tx,1T;&%r'; ..1 -; .* "*. "d"' " ";: "";1;:lT,i,:"Tfi."..""":Tlti:;;;;;;;1,j TestReport D ale:2012102M Page: 17 of 24 No.:CE/201214846A CERAMTEC GMBH 15D.91207 LAUF,GERIUANY CERAIJICSLUITPOLDSTRASSE MULTIFUNCTIONAL of PVCin material Analyslsflow chartfor determination I I GinnyChen Nameof thep€rsonwhomademeasurement TroyChang Nameofthepe6onin chargeof measurementr Samplepretreatment by FTIR Sample analyzed Checkwave-number of C-Clbonding Data i'i:;;;i;;l".'--&'hiet.m]!.i''-odjo'.c."€|'ro.mso Lred ,nd o edrctu romardoc,mnts *tir'16hr\atLc0no$b i;";;;"n;,i,h;,.;;i;,;,, i n e i ; ; ; ] , i . . i ; i ! m i m 6 ? f d " . ; ' } ' . ' o m p a n " 9 " ' . . p d . o ' com Fnr Av unaurhmtd a[e6td. roeery o. raibicrion or rlre @meii o I- !0,--r:::: t?rl ..- rlr 1er.!1 ! !9!tq,!!!11:11 l_',s,6 nrrIlllulltlt]t TestReport No.: CE/2012l148464Dale :2012,0210/' Page: 18 ol 24 CEMMTEC GMBH MULTIFUNCTIONALCERAMICS LUITPOLDSTRASSE'15 D-91207LAUF.GERIMANY procedure Analyticalflow chartof Soxhlet extraction(GC/MS) r r Nameofthepersonwhomademeasurement RomanWong TroyChang Nameof thepersonin chargeofmeasufement ' HBCOD. NP. DBBT' (Test ltems:Phthalate' Benzotriazole Organicphosphoruscompounds) -n. r -e:01y o'!:! P!!r,,'€dff c o m o . n v :; ! l('' i;;;;;*'"**ds.c;.W1;:.,i;n'.."Pkicotrcn.d dnorc'e€drcn!fomaldoUmen-'-dFi'-.saroco1dio.'|o'|'s l'i.i,ij''i'inin']ni"imiJi.;^ldi'jaa;-;:o'Tq't?.e'fddao.fi'oo,'-€'';sd.s'1 0eLru or.s nti*nior 01!do n comDrryMyL.a {-o1ena F,toi b o"ro' *iao o 1"6tre1ro |:l|rtrumm: I! scs I Test Report No.'.CE|201Z14UGA Dale:2012102104Paqe: 19of 24 CERAMTEC GMBH 15D-91207 LAUF,GERMANY IVULTIFUNCTIONAL CERAMICSLUITPOLDSTMSSE Analyticalflow chartof O.ganic-Tin content I I Nameofthe pe6onwhomademeasurement: GinnyChen person Nameof the in chafgeof measurement: TroyChang anosG) ele.d IhLsle$ rcPod€nnd ii, do.rnid i ts&4 d h€ LomDrr $od ro sc{"?'condio'ro and,olele@nr|o.go.a*ksbi'.c'b|eT3.tco'o1oTh'-'"' "{ m r ya' o d od "c6| '-. te' "\ dued' o. *1d.. ;*n. \yyrT' e o@ n'ao'fd' i eoi tmi o; no oi 6r 'ianoe" T . *" |_?. .. -d- -. ah .ndli!, ,d-' B € o' o| t-l p a 1m, 9e e oniento abBron bosry of rairer@ronorbe cmoaiv Mv mau'honzdd t - r l |ltfl[]trtrll TestReport No.: CE201214846A Dale| 201U0210/' Paae:20of24 CERAMTECGMBH MULTIFUNCTIONAL CERAMICS LUITPOLDSTRASSE 15 D.91207LAUF,GERMANY tr!l[]|l[ t]||t Analytical flow chart of halogen content 'l) Nameofihe D€rsonwho mademeasurementRitiaChen 2) Nameof the personin chargeof measurementTroyChang / Separation Sampiepretrealrnent Weighting andputtingsamplein cell / Absorption OxygenBombCombustion Dilution to fixedvolume Analysis wasperformed by lC 4".*^,in"?ij**',=*" n ui"i".oi, *d& i" ; i",ior.s i s3D? /.{ o*+r .." Ld. o "*"" o'FR md ddedon' rfuoaamnb. ,Jbi'ecr'd"ararcononns i;;;;a ; ;de;;ia d;n:d ,ii d'd€n €&€. d.ria n.rc o &v r o. or r ' onman taoJ rd tra " he he of it i^r€i*di6 onrvands'hin th€limilsdf clanls isLuclom f;iv Theco@ar s $e rsponsb rirvI ro is c enrtnd $i5 d@mem dcs ior dmqaE pai€s r0 a { t d r o 1 o !' 4 r € 1 a o o ' d voa. i P q ' i E d o a m r ; re' .iooJ -,i ;;;r;ni6tr;F€i,o,"q TestReport No.rCE/2012I14846AOale| 201202/c4' Paae:21o124 i||] ttll CERAMTEC GMBH 15D.91207 LAUF,GERI'ANY MULTIFUNCTIONAL CERAMICSLUITPOLDSTMSSE l rrl Analysisflow chartfor determinationof Asbestos '1) Nameof thepersonwhomademeasurement VictorKao WendyWei 2) Nameof thepersonin chargeof measurement method:EPA600/R-93/11 6| I Reference Asbestos identifcation bydispersion polarizalion staining lightmicroscopy Asbestos/ Containing LdessdsN* 'a,e b. rc$c ahoMLi!f sLes.r rpenE eren,/.?fi:sj_sr.,:J:fi":,i1.tir[tr'* Asbestos identificalion byx-|ay Asbestos/ Notconlaining *"** *". itrH]'...',*,;-";";":,''"''*f."**";;.""i., aiidr.o1;ra-'-r"ra'd.-*s",dFd;re..".c-'|"';;L'e:.ni''km.1GdM{'€fugre i.i''i.^ds''Nm@mnEjnmo,ima,a.""**oron.ji-,ni;;di.iid."ai-'*dtr, liri1tu*4dffi##i#s*il{ir**lidiF#"r""*glfrrff h*$fiff#,#ifff,,##i$;*$$;jtj' (NevraF.it''r?lanrr ./ :t::il ri1r3|! Test Report No. : CE/2012l14846A Dare| 201i,02J04 Page'.22 ol 24 r CERAMTECGMBH [JULTIFUNCTIONAL CERAMICS LUITPOLDSTMSSE15 D-91207LAUF,GERMANY fitr| [lulllll Analyticalflow chart I I RomanWong Nameof thepe€onwhomademeasurement TroyChang Nameof thepeEonin chargeof measurement: TBBP-A-b|S I I Testltems:PBB/PBDE, - '> -----' Optionalscreen process prccess-""' Confirnation process Firsltesling r r r r r r r r r r ...r ...t Scteenanalysis Sampleextfactionmethod solution concenhate/Dilute Extracted Filter v @ V lssueReport slei€ee1*'m':ioji€ru::";:"::l:ffi:".":::*j;::;::-j;1":;:";::::':; 3i:;:."*-*"""d'" "'-*"?:r'! rh6 do.nm6r s 'sued w rtu co@ iffi"ry#'j."',";{:f;r-"rft!T""#fu1*;"','i;,;"',f"*:'"!;;,:iiF"Ct-lmr:.**nr'-""f,:""e.""rir*:;:,T" ;;;;''';F;;i"'-i'.d*ih:1@'.Aotc'"as|shdors'i;!||..o-p"ts,|erc$dn"b|| ;;;;;1;;ec4oaho16"toog:b..'@..Fn'i.do.do-;rd-i^mm"{Jo a;*;.;; tu; -*h*.id, bd*: lrr'n ii r': rsrf SGq Test Report No.: cE/2012/14846ADare| 201210204 Paae:23of24 CERAMTECGMBH IVULTIFUNCTIONAL CERAMICS LUITPOLDSTMSSE15 D-91207LAUF,GERMANY Analyticalflow chartofvolatileorganlccompounds(VOCS) I I : ChunWu Nameoflhe personwhomademeasurement : ShinjyhChen Nameoflhe personin chargeofmeasurement ( Refercnce : method USEPA5021) Samplepretreatment Takesampleandputit into glasswarc. headspace amp€(s)B€d ih' dodnisr B*e d h6 (omo s'riFir o "T.drLo d n d b r e e d o n ' "( b m d o o e - c f L dqJero'rud\0Pr*\0slo'n 01o1.'ore.. i'*t*r" hird;;irabiie.d; d..;;;'6ndab-|'"d^'fi|eF'so.c|e1''<'dos.i,'.Lo Drft \r. rh s tes repon'aino 'J'1o',.nakaro'roTpryo rir. 6o1o hroFnro t |||t'|l|[l[]] t TestReport No.rCE/2012'14846ADale:201zo2lM Page:24ot 24 CERAMTEC GMBH LAUF,GERIVANY 15D-91207 MULTIFUNCTIONAL CERAIIICSLUITPOLDSTMSSE ' Thetestedsample/ paft is matkedby an arow if ifs shownon the photo.' 14846 " Endof Report "' ' nBednm' ;,sJsd n h6 c6m€ sdFo;-" a n o b ' e r e d ' o 1 .b r a ' o d d r e r 6 . . r eL T o r b . F r f d o , - sJ oLonoio. : o1y.,d { c o m D d r re y L r a J T ? € 1 a F € t o r . r o o " r y d d i r sa o : or-. T na,saloidoo-e,i o r,.elro .i, ddhr eF1pd.sb.\\.o6.i .oLm"i, r. o o" "podL@d l[ tmfl||rrllrlr Test Report Applicant: Number : TWNC00249177 Littelfuse Philippines Inc. LIMA Technology Center, Lipa City, Malvar, Batangas Date : Mar 26, 2012 Sample Description: One (1) group of submitted samples said to be : Part Description : Silver Clad Cu Wire with 5% Ag Part Number : 082xxx(082375) Date Sample Received : Mar 22, 2012 Date Test Started : Mar 22, 2012 Test Conducted : As requested by the applicant, for details please refer to attached pages. Authorized By: On Behalf Of Intertek Testing Services Taiwan Limited K. Y. Liang Director This report shall not be reproduced except in full, without the written approval of the laboratory. Page 1 of 5 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401 Number : TWNC00249177 Test Conducted (Ⅰ) Test Result Summary : Test Item Heavy Metal Cadmium (Cd) content Lead (Pb) content Mercury (Hg) content Chromium VI (Cr6+) content (mg/kg with 50cm2) Remarks: ppm = ND = < = mg/kg Result (ppm) Silvery Wire ND ND ND Negative (< 0.02) Parts per million based on weight of tested sample = mg/kg Not detected Less than with 50cm2 = milligram per kilogram with 50 square centimetre Responsibility of Chemist : Irene Chiou / Kevin Liu / Cathy Chen Date Sample Received Test Period : Mar 22, 2012 : Mar 22, 2012 To Mar 26, 2012 (Ⅱ) RoHS Requirement: Restricted Substances Cadmium (Cd) Content Lead (Pb) Content Mercury (Hg) Content Chromium VI (Cr6+) Content Limits 0.01% (100ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for homogeneous material. Page 2 of 5 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401 Number : TWNC00249177 Test Conducted (Ⅲ) Test Method: Test Item Cadmium (Cd) content Lead (Pb) content Mercury (Hg) content Chromium VI (Cr6+) content Test Method With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in clause 7, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in annex B, by boiling water extraction and determined by UV-Vis Spectrophotometer. Reporting Limit 2 ppm 2 ppm 2 ppm 0.02 mg/kg with 50cm2 Remark: Reporting limit = Quantitation limit of analyte in sample Page 3 of 5 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401 Number : TWNC00249177 Test Conducted (Ⅳ) Measurement Flowchart: Test For Cd/Pb/Hg/Chromium (VI) Reference Standard:IEC 62321 edition 1.0:2008 Sampling/grinding or cutting Cd/Pb/Hg Cr Polymers / Electronics Metal For different material, digest the sample with *1 appropriate acid By spot test Negative Confirm the tested samples are totally dissolved Make up with deionized water 6+ *2 Weigh sample and add alkaline solution Get 50cm2 sample Definite temp. extraction Boiling water extraction Cool and filter the extract Analyzed by ICP-OES Make up with deionized water and add diphenylcarbazide solution Remarks: *1: List Of Appropriate Acid: Material Polymers Metals Electronics Analyzed by UV-VIS Acid Added For Digestion HNO3,HCl,HF,H2O2,H3BO3 HNO3,HCl,HF HNO3,HCl,H2O2,HBF4 *2: If the result of spot test is positive, Chromium VI would be determined as detected. End of Report Page 4 of 5 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401 Number : TWNC00249177 Test Conducted Photo Page 5 of 5 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401 Test Report Applicant: Number : TWNC00285771 Littelfuse Philippines Inc. LIMA Technology Center, Lipa City, Malvar, Batangas Date : Nov 16, 2012 Sample Description: One (1) group of submitted samples said to be : Part Description : Solder (Pb is ≥ 90%) Part Number : 692321 Date Sample Received : Nov 12, 2012 Date Test Started : Nov 13, 2012 Test Conducted : As requested by the applicant, for details please refer to attached pages. Authorized By: On Behalf Of Intertek Testing Services Taiwan Limited K. Y. Liang Director *THJ0285771* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 1 of 6 Number : TWNC00285771 Test Conducted (Ⅰ) Test Result Summary : Result (ppm) Silvery metal Test Item Heavy Metal Cadmium (Cd) content Lead (Pb) content Mercury (Hg) content Chromium VI (Cr6+) content (mg/kg with 50cm2) ND 934557 ND Negative (< 0.02) Remarks: ppm = Parts per million based on weight of tested sample = mg/kg ND = Not detected < = Less than mg/kg with 50cm2 = milligram per kilogram with 50 square centimetre Negative = A negative test result indicated positive observation was not found at the time of Test. Responsibility of Chemist : Irene Chiou / Kevin Liu Date Sample Received Test Period : Nov 12, 2012 : Nov 13, 2012 to Nov 16, 2012 (Ⅱ) RoHS Limits: Restricted Substances Cadmium (Cd) Content Lead (Pb) Content Mercury (Hg) Content Chromium VI (Cr6+) Content Limits 0.01% (100ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) The above limits were quoted from Annex II of 2011/65/EU for homogeneous material. *THJ0285771* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 2 of 6 Number : TWNC00285771 Test Conducted (Ⅲ) Test Method: Test Item Cadmium (Cd) content Lead (Pb) content Mercury (Hg) content Chromium VI (Cr6+) content Test Method With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in clause 7, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in annex B, by boiling water extraction and determined by UV-Vis Spectrophotometer. Reporting Limit 2 ppm 2 ppm 2 ppm 0.02 mg/kg with 50cm2 Remark: Reporting limit = Quantitation limit of analyte in sample *THJ0285771* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 3 of 6 Number : TWNC00285771 Test Conducted (Ⅳ) Measurement Flowchart: Test For Cd/Pb/Hg/Chromium (VI) Reference Standard:IEC 62321 edition 1.0:2008 Sampling/grinding or cutting Cd/Pb/Hg Cr 6+ Polymers / Electronics Metal For different material, digest the sample with *1 appropriate acid By spot test Negative Confirm the tested samples are totally dissolved Make up with deionized water *2 Weigh sample and add alkaline solution Get 50cm2 sample Definite temp. extraction Boiling water extraction Cool and filter the extract Analyzed by ICP-OES Make up with deionized water and add diphenylcarbazide solution Analyzed by UV-VIS *THJ0285771* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 4 of 6 Number : TWNC00285771 Test Conducted Remarks: *1: List of Appropriate Acid: Acid Added for Digestion Material Polymers HNO3,HCl,HF,H2O2,H3BO3 Metals HNO3,HCl,HF Electronics HNO3,HCl,H2O2,HBF4 *2: If the result of spot test is positive, Chromium VI would be determined as detected. End of Report This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a recommendation for any particular course of action. Intertek does not accept a duty of care or any other responsibility to any person other than the Client in respect of this report and only accepts liability to the Client insofar as is expressly contained in the terms and conditions governing Intertek's provision of services to you. Intertek makes no warranties or representations either express or implied with respect to this report save as provided for in those terms and conditions. We have aimed to conduct the Review on a diligent and careful basis and we do not accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by statute or otherwise, except in the event of our gross negligence or wilful misconduct. *THJ0285771* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 5 of 6 Number : TWNC00285771 Test Conducted Photo *THJ0285771* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 6 of 6 Test Report Applicant: Number : TWNC00285781 Littelfuse Philippines Inc. LIMA Technology Center, Lipa City, Malvar, Batangas Date : Nov 19, 2012 Sample Description: One (1) group of submitted samples said to be : Part Description : Anaerobic Adhesive Part Number : 087266 Date Sample Received : Nov 12, 2012 Date Test Started : Nov 13, 2012 Test Conducted : As requested by the applicant, for details please refer to attached pages. Authorized By: On Behalf Of Intertek Testing Services Taiwan Limited K. Y. Liang Director *THJ0285781* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 1 of 10 Number : TWNC00285781 Test Conducted (Ⅰ) Test Result Summary : Result (ppm) Green Liquid Test Item Heavy Metal Cadmium (Cd) content Lead (Pb) content Mercury (Hg) content Chromium VI (Cr6+) content Polybrominated Biphenyls (PBBs) Monobrominated Biphenyls (MonoBB) Dibrominated Biphenyls (DiBB) Tribrominated Biphenyls (TriBB) Tetrabrominated Biphenyls (TetraBB) Pentabrominated Biphenyls (PentaBB) Hexabrominated Biphenyls (HexaBB) Heptabrominated Biphenyls (HeptaBB) Octabrominated Biphenyls (OctaBB) Nonabrominated Biphenyls (NonaBB) Decabrominated Biphenyl (DecaBB) Polybrominated Diphenyl Ethers (PBDEs) Monobrominated Diphenyl Ethers (MonoBDE) Dibrominated Diphenyl Ethers (DiBDE) Tribrominated Diphenyl Ethers (TriBDE) Tetrabrominated Diphenyl Ethers (TetraBDE) Pentabrominated Diphenyl Ethers (PentaBDE) Hexabrominated Diphenyl Ethers (HexaBDE) Heptabrominated Diphenyl Ethers (HeptaBDE) Octabrominated Diphenyl Ethers (OctaBDE) Nonabrominated Diphenyl Ethers (NonaBDE) Decabrominated Diphenyl Ether (DecaBDE) ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND *THJ0285781* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 2 of 10 Number : TWNC00285781 Test Conducted (Ⅰ) Test Result Summary : Result (ppm) Green Liquid Test Item Halogen Content Fluorine (F) Chlorine (Cl) Bromine (Br) Iodine (I) Phthalates Di(2-ethylhexyl) Phthalate (DEHP) Dibutyl Phthalate (DBP) Benzyl Butyl Phthalate (BBP) Others Hexabromocyclododecane (HBCDD) ND ND ND ND ND 77 ND ND Remarks: ppm = Parts per million based on wet weight of tested sample = mg/kg ND = Not detected Responsibility of Chemist : Irene Chiou / Kevin Liu / Cathy Chen Date Sample Received Test Period : Nov 12, 2012 : Nov 13, 2012 To Nov 15, 2012 (Ⅱ) RoHS Limits: Restricted Substances Cadmium (Cd) Content Lead (Pb) Content Mercury (Hg) Content Chromium VI (Cr6+) Content Polybrominated Biphenyls (PBBs) Polybrominated Diphenyl Ehters (PBDEs) Limits 0.01% (100ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) The above limits were quoted from Annex II of 2011/65/EU for homogeneous material. *THJ0285781* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 3 of 10 Number : TWNC00285781 Test Conducted (Ⅲ) Test Method: Test Item Reporting Limit Test Method With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the Cadmium (Cd) content 2 ppm tested samples are totally dissolved and determined by ICPOES. With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the Lead (Pb) content 2 ppm tested samples are totally dissolved and determined by ICPOES. With reference to IEC 62321 edition 1.0:2008 in clause 7, by microwave Mercury (Hg) content digestion until the tested samples 2 ppm are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition Chromium VI (Cr6+) 1.0:2008 in annex C, by alkaline 1 ppm digestion and determined by UV-Vis content spectrophotometer. With reference to IEC 62321 edition 1.0:2008 in annex A, by solvent Polybrominated extraction and determined by GC-MS 5 ppm Biphenyls (PBBs) and further HPLC-DAD confirmation when necessary. With reference to IEC 62321 edition 1.0:2008 in annex A, by solvent Polybrominated Diphenyl Ethers extraction and determined by GC-MS 5 ppm (PBDEs) and further HPLC-DAD confirmation when necessary. With reference to EN 14582:2007 by 50 ppm Halogen Content calorimetric bomb with oxygen and determined by Ion Chromatograph. With reference to EN 14372: 2004, by Phthalates solvent extraction and determined by 50 ppm GC-MS. With reference to USEPA 3540C, by Hexabromocyclododecane 10 ppm solvent extraction and determined by (HBCDD) GC-MS. Remark: Reporting limit = Quantitation limit of analyte in sample *THJ0285781* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 4 of 10 Number : TWNC00285781 Test Conducted (Ⅳ) Measurement Flowchart: Test for Cd/Pb/Hg/Chromium (VI)/PBBS/PBDES Contents Reference Standard: IEC 62321 edition 1.0:2008 Sample preparation For non-metal part For metal part Take sample and immerse into Aqua Regia, start to strip plating layer Stop the stripping procedure upon color change completely Take the Aqua solution as plating component and stripped body as substrate component PBBs/PBDEs Weigh sample and add organic solvent By Soxhlet extraction or Solvent extraction Concentrate the extract and make up with organic solvent Analyzed by GC-MSD Cr 6+ Substrate Cd/Pb/Hg Weigh sample and add alkaline solution For different material, digest the sample with *1 appropriate acid Plating Cr 6+ By spot test Definite temp. extraction Cool and filter the extract Confirm the tested samples are totally dissolved Negative *2 Get 50cm2 sample Make up with deionized water By boiling water extraction Analyzed by ICP-OES Make up with deionized water and add diphenyl-carbazide solution Analyzed by UV-VIS *THJ0285781* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 5 of 10 Number : TWNC00285781 Test Conducted (Ⅳ) Measurement Flowchart: Remarks: *1: List of Appropriate Acid: Material Polymers Metals Electronics Acid Added for Digestion HNO3,HCl,HF,H2O2,H3BO3 HNO3,HCl,HF HNO3,HCl,H2O2,HBF4 *2: If the result of spot test is positive, Chromium VI would be determined as detected. *THJ0285781* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 6 of 10 Number : TWNC00285781 Test Conducted (Ⅳ) Measurement Flowchart: Test for Halogen Content Reference Standard:EN 14582 Sampling/grinding or cutting Add absorbent in a combustion flask & place weighed sample in equipment Fill oxygen into calorimetric bomb Ignite then leave the bomb at room temperature Transfer the absorbent into a volumetric flask Make up with deionized water Analyzed by ion chromatography *THJ0285781* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 7 of 10 Number : TWNC00285781 Test Conducted (Ⅳ) Measurement Flowchart: Test For Phthalates Contents Reference Method: EN 14372: 2004 Sampling/grinding or cutting Weigh sample and add organic solvent By solvent extraction Concentrate the extract and make up with organic solvent Analyzed by GC-MSD *THJ0285781* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 8 of 10 Number : TWNC00285781 Test Conducted (Ⅳ) Measurement Flowchart: Test For Hexabromocyclododecane (HBCDD) Reference Standard:USEPA 3540C Sampling/grinding or cutting Weigh sample and add organic solvent By soxhlet extraction Concentrate the extract and make up with organic solvent Analyzed by GC-MSD End of Report This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a recommendation for any particular course of action. Intertek does not accept a duty of care or any other responsibility to any person other than the Client in respect of this report and only accepts liability to the Client insofar as is expressly contained in the terms and conditions governing Intertek's provision of services to you. Intertek makes no warranties or representations either express or implied with respect to this report save as provided for in those terms and conditions. We have aimed to conduct the Review on a diligent and careful basis and we do not accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by statute or otherwise, except in the event of our gross negligence or wilful misconduct. *THJ0285781* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 9 of 10 Number : TWNC00285781 Test Conducted Photo *THJ0285781* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 10 of 10 Test Report Applicant: Number : TWNC00253636 Littelfuse Philippines Inc. LIMA Technology Center, Lipa City, Malvar, Batangas Date : Apr 24, 2012 Sample Description: One (1) group of submitted samples said to be : Part Description : Black Ink Part Number : 425809 Date Sample Received : Apr 19, 2012 Date Test Started : Apr 19, 2012 Test Conducted : As requested by the applicant, for details please refer to attached pages. Authorized By: On Behalf Of Intertek Testing Services Taiwan Limited K. Y. Liang Director This report shall not be reproduced except in full, without the written approval of the laboratory. Page 1 of 9 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401 Number : TWNC00253636 Test Conducted (Ⅰ) Test Result Summary : Test Item Heavy Metal Cadmium (Cd) content Lead (Pb) content Mercury (Hg) content Chromium VI (Cr6+) content Polybrominated Biphenyls (PBBs) Monobrominated Biphenyls (MonoBB) Dibrominated Biphenyls (DiBB) Tribrominated Biphenyls (TriBB) Tetrabrominated Biphenyls (TetraBB) Pentabrominated Biphenyls (PentaBB) Hexabrominated Biphenyls (HexaBB) Heptabrominated Biphenyls (HeptaBB) Octabrominated Biphenyls (OctaBB) Nonabrominated Biphenyls (NonaBB) Decabrominated Biphenyl (DecaBB) Polybrominated Diphenyl Ethers (PBDEs) Monobrominated Diphenyl Ethers (MonoBDE) Dibrominated Diphenyl Ethers (DiBDE) Tribrominated Diphenyl Ethers (TriBDE) Tetrabrominated Diphenyl Ethers (TetraBDE) Pentabrominated Diphenyl Ethers (PentaBDE) Hexabrominated Diphenyl Ethers (HexaBDE) Heptabrominated Diphenyl Ethers (HeptaBDE) Octabrominated Diphenyl Ethers (OctaBDE) Nonabrominated Diphenyl Ethers (NonaBDE) Decabrominated Diphenyl Ether (DecaBDE) Result (ppm) Black Paste ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND Page 2 of 9 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401 Number : TWNC00253636 Test Conducted (Ⅰ) Test Result Summary : Test Item Result (ppm) Black Paste Halogen Content Fluorine (F) Chlorine (Cl) Bromine (Br) Iodine (I) Phthalates Di(2-ethylhexyl) Phthalate (DEHP) Dibutyl Phthalate (DBP) Benzyl Butyl Phthalate (BBP) Others Hexabromocyclododecane (HBCDD) ND 610 ND ND ND ND ND ND Remarks: ppm = Parts per million based on wet weight of tested sample = mg/kg ND = Not detected Responsibility of Chemist : Irene Chiou / Kevin Liu / Cathy Chen Date Sample Received Test Period : Apr 19, 2012 : Apr 19, 2012 To Apr 24, 2012 (Ⅱ) RoHS Requirement: Restricted Substances Cadmium (Cd) Content Lead (Pb) Content Mercury (Hg) Content Chromium VI (Cr6+) Content Polybrominated Biphenyls (PBBs) Polybrominated Diphenyl Ehters (PBDEs) Limits 0.01% (100ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for homogeneous material. Page 3 of 9 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401 Number : TWNC00253636 Test Conducted (Ⅲ) Test Method: Test Item Test Method With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by Cadmium (Cd) content microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by Lead (Pb) content microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in clause 7, by microwave Mercury (Hg) content digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition Chromium VI (Cr6+) 1.0:2008 in annex C, by alkaline content digestion and determined by UV-Vis spectrophotometer. With reference to IEC 62321 edition 1.0:2008 in annex A, by solvent Polybrominated extraction and determined by GC-MS Biphenyls (PBBs) and further HPLC-DAD confirmation when necessary. With reference to IEC 62321 edition Polybrominated 1.0:2008 in annex A, by solvent Diphenyl Ethers extraction and determined by GC-MS (PBDEs) and further HPLC-DAD confirmation when necessary. With reference to EN 14582:2007 by Halogen Content calorimetric bomb with oxygen and determined by Ion Chromatograph. With reference to EN 14372: 2004, by Phthalates solvent extraction and determined by GC-MS. With reference to USEPA 3540C, by Hexabromocyclododecane solvent extraction and determined by (HBCDD) GC-MSD. Reporting Limit 2 ppm 2 ppm 2 ppm 1 ppm 5 ppm 5 ppm 50 ppm 10 ppm 10 ppm Remark: Reporting limit = Quantitation limit of analyte in sample Page 4 of 9 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401 Number : TWNC00253636 Test Conducted (Ⅳ) Measurement Flowchart: Test for Cd/Pb/Hg/Chromium (VI)/PBBS/PBDES Contents Reference Standard: IEC 62321 edition 1.0:2008 Sample preparation For non-metal part For metal part Take sample and immerse into Aqua Regia, start to strip plating layer Stop the stripping procedure upon color change completely Take the Aqua solution as plating component and stripped body as substrate component Cd/Pb/Hg Cr Confirm the tested samples are totally dissolved Make up with deionized water PBBs/PBDEs Polymers / electronics Metal For different material, digest the sample with *1 appropriate acid 6+ Weigh sample and add organic solvent By spot test Negative Get 50cm2 sample By boiling water extraction *2 Weigh sample and add alkaline solution By Soxhlet extraction or Solvent extraction Definite temp. extraction Cool and filter the extract Analyzed by ICP-OES Concentrate the extract and make up with organic solvent Analyzed by GC-MSD Make up with deionized water and add diphenylcarbazide solution Analyzed by UV-VIS Remarks: *1: List of Appropriate Acid: Acid Added for Digestion Material Polymers HNO3,HCl,HF,H2O2,H3BO3 Metals HNO3,HCl,HF Electronics HNO3,HCl,H2O2,HBF4 *2: If the result of spot test is positive, Chromium VI would be determined as detected. Page 5 of 9 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401 Number : TWNC00253636 Test Conducted (Ⅳ) Measurement Flowchart: Test for Halogen Content Reference Standard:EN 14582 Sampling/grinding or cutting Add absorbent in a combustion flask & place weighed sample in equipment Fill oxygen into calorimetric bomb Ignite then leave the bomb at room temperature Transfer the absorbent into a volumetric flask Make up with deionized water Analyzed by ion chromatography Page 6 of 9 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401 Number : TWNC00253636 Test Conducted (Ⅳ) Measurement Flowchart: Test For Phthalates Contents Reference Method: EN 14372: 2004 Sampling/grinding or cutting Weigh sample and add organic solvent By solvent extraction Concentrate the extract and make up with organic solvent Analyzed by GC-MSD Page 7 of 9 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401 Number : TWNC00253636 Test Conducted (Ⅳ) Measurement Flowchart: Test For Hexabromocyclododecane (HBCDD) Reference Standard:USEPA 3540C Sampling/grinding or cutting Weigh sample and add organic solvent By soxhlet extraction Concentrate the extract and make up with organic solvent Analyzed by GC-MSD End of Report Page 8 of 9 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401 Number : TWNC00253636 Test Conducted Photo Page 9 of 9 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401 Test Report Applicant: Number : TWNC00243603 Littelfuse, Philippines Inc. LIMA Technology Center, Lipa City, Malvar, Batangas Date : Feb 16, 2012 Sample Description: One (1) group of submitted samples said to be : Part Description : Tin Bar Part Number : NA Date Sample Received : Feb 13, 2012 Date Test Started : Feb 13, 2012 Test Conducted : As requested by the applicant, for details please refer to attached pages. Authorized By: On Behalf Of Intertek Testing Services Taiwan Limited K. Y. Liang Director This report shall not be reproduced except in full, without the written approval of the laboratory. Page 1 of 5 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401 Number : TWNC00243603 Test Conducted (Ⅰ) Test Result Summary : Test Item Heavy Metal Cadmium (Cd) content Lead (Pb) content Mercury (Hg) content Chromium VI (Cr6+) content (mg/kg with 50cm2) Result (ppm) Silvery Metal ND 267 ND Negative (< 0.02) Remarks: ppm = Parts per million based on weight of tested sample = mg/kg ND = Not detected < = Less than mg/kg with 50cm2 = milligram per kilogram with 50 square centimetre Negative = A negative test result indicated positive observation was not found at the time of Test. Responsibility of Chemist : Irene Chiou / Kevin Liu Date Sample Received Test Period : Feb 13, 2012 : Feb 13, 2012 To Feb 16, 2012 (Ⅱ) RoHS Requirement: Restricted Substances Cadmium (Cd) Content Lead (Pb) Content Mercury (Hg) Content Chromium VI (Cr6+) Content Limits 0.01% (100ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for homogeneous material. Page 2 of 5 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401 Number : TWNC00243603 Test Conducted (Ⅲ) Test Method: Test Item Test Method With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by Cadmium (Cd) microwave digestion until the tested content samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by Lead (Pb) content microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in clause 7, by microwave Mercury (Hg) digestion until the tested samples are content totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition 6+ Chromium VI (Cr ) 1.0:2008 in annex B, by boiling water content(mg/kg with extraction and determined by UV-Vis 50cm2) Spectrophotometer. Reporting Limit 2 ppm 2 ppm 2 ppm 0.02 mg/kg with 50cm2 Remark: Reporting limit = Quantitation limit of analyte in sample Page 3 of 5 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401 Number : TWNC00243603 Test Conducted (Ⅳ) Measurement Flowchart: Test For Cd/Pb/Hg/Chromium (VI) Reference Standard:IEC 62321 edition 1.0:2008 Sampling/grinding or cutting Cd/Pb/Hg Cr Polymers / Electronics Metal For different material, digest the sample with *1 appropriate acid By spot test Negative Confirm the tested samples are totally dissolved Make up with deionized water 6+ *2 Weigh sample and add alkaline solution Get 50cm2 sample Definite temp. extraction Boiling water extraction Cool and filter the extract Analyzed by ICP-OES Make up with deionized water and add diphenylcarbazide solution Remarks: *1: List Of Appropriate Acid: Material Polymers Metals Electronics Analyzed by UV-VIS Acid Added For Digestion HNO3,HCl,HF,H2O2,H3BO3 HNO3,HCl,HF HNO3,HCl,H2O2,HBF4 *2: If the result of spot test is positive, Chromium VI would be determined as detected. End of Report Page 4 of 5 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401 Number : TWNC00243603 Test Conducted Photo Page 5 of 5 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401