ICPTest_453_12 26 2012 pdf

ICP Test Report Certification Packet
Company name :
Littelfuse, Inc.
Product Series:
Nano2 Fuse - FA
Product #:
453xxx Series
Issue Date:
December 26, 2012
It is hereby certified by Littelfuse, Inc. that there is neither RoHS (EU Directive 2002/95/EC,
2011/65/EU)-restricted substance nor such use, for materials to be used for unit parts, for
packing/packaging materials, and for additives and the like in the manufacturing processes.
In addition, it is hereby reported to you that the parts and sub-materials, the materials to be used
for unit parts, the packing/packaging materials, and the additives and the like in the manufacturing
processes, are all composed of the following components.
Issued by:
<Global EHS Engineer>
(1) Parts, sub-materials and unit parts
This document covers the Nano2 Fuse FA RoHS-Compliant series products manufactured
by Littelfuse, Inc.
＜ Raw Materials Used
Please see Table 1
(2) The ICP data on all measurable substances
Please see appropriate pages as identifed in Table 1
Remarks：
Pb (lead) contained in the high temperature melting solder > 85% and is categorized as
exempt under section 7a of the RoHS Annex.
1
Table 1: List of Raw Materials covered by this report
Total Parts
Raw Material Part Number
1
2
3
4
5
6
7
8
910-238
Frequenta C221 (909-434)
082xxx
082xxx
11-0894 (497xxx)
11-0803 (497xxx)
692321
425809
Form 585-047 Rev. A
Raw Material Description
Cap Base
Cap plating
Body (ceramic tube)
Wire - 2% by weight Ag Clad Cu
Wire - 5% By weight Ag Clad Cu
Wire - Ag Plated 36 Alloy
Wire - Cu Clad Fe58 42Ni 5Ag By Weight
Solder
Ink
2
Page(s)
3-10
11-34
35-39
40-44
45-50
51-56
57-62
63-71
2/21/06
nown
ForQueSti
PleaseCo
TestReport
ith sGS
No.: CH2O1Z14UEA Date: 2012J02104Page.l ol 24
CERAMTECGMBH
15 D-91207LAUF,GERMANY
MULTIFUNCTIONAL
CERAMICS LUITPOLDSTRASSE
r||
tUi||l]]$t
The followlng samplo{a)was/weresubmitted and identified by/on behalfofthe cllent as:
SampleDe6ciption
Styl€/ltem No.
SampleRecejvingDate
Testing Period
CERAMIC
FREQUENTA
C22'1
2012t01t30
2012J01|30 TO 201Z O2t04
T€6i Result(s)
: Pleasereferto nextpage(s).
Conclusion
Lead
thetestresultsof Cadmium,
samples,
: Basedontheperfomedtestsonsubmitted
limits
as
setby
PBDES
comply
with
the
Cr(Vl),
PBBS
and
Mercury,
Hexavalent
Chromium
2002/95/EC.
2011/65/EU
Annexll; recasting
RoHSDnective
gN|tad ftrltd
TestReport
Page:2of 24
D e,2012102104
No.:CE/201214846A
Llmt t
GMBH
CERAMTEC
LAUF.GERMANY
15D-91207
MULTIFUNCTIONAL
CERAMICSLUITPOLDSTMSSE
t]||!|r]
Test ReBult{s}
PARTllAMENo.1
:
CREAI, CERAMIC
mg/Kg With referenc€to IEC62321: 2008and
2
Result
No.t
n.o,
to IEC62321:2008and
mgKg Withreference
pedormed
by ICP-AES.
to IEC62321:2008and
(Hg)
mg/Kg Withreference
lllercury
oenotmeo
Dvtut -AEn,
mg/Kg Witheferenceto IEC62321:2008and
Cr(Vl)
Chromium
Hexavalent
per{ormedby UV-VIS.
(PCBS) m9Kg With referenceto US EPA3540c
Biphenyls
Polychlorinated
bY
Analysis
wasperlormed
method.
(CASNo.:133+363)
GC/MS.
to Us EPA3540c
mgKg Withreference
Terphenyls
Polychlorinated
bY
Analysis
wa6performed
method.
(PCTs)
2
n.d.
1000
2
n_o.
1000
2
n.d.
1000
Test ltem(s)
Cadmium(Cd)
Unit
Method
Lead(Pb)
MDL
n.d.
0.5
n.d.
5
n.d.
0.01
n.d.
10
n.d.
10
n.d.
3
n.d.
GC/[rS.
to USEPA3540C
mS/kS Withreference
wasperformed
by
method.
Analy6is
GC/tMS.
o/.
to USEPA3g0C
Withreference
Alkanes,C1G13,chloro(short
wasperformedbY
Analysi6
(CAS
method.
Paraffins)
ChainChlorinated
GC/MS.
No.:85535-44-8)
to Us EPA3540c:
m9Kg Withreference
Perfluorooctanesulfonates
1996methodfor PFOSContent.
(PFOS-Acid,
MetalSalt,Amide)
wasperfomedby LC/MS.
Analysis
to USEPA3540C:
mg/Kg Withreference
PFOA(CASNo.:335€7-1)
'1996methodfor PFOAContent.
bYLC/MS.
Analysis
wa6performed
Naphthalene
Polychlorinated
(PCNs)
ormaldehyde(CAS No.: 50-00-0) mg/kg With reference to ISO 17226-1(200A).
Analysiswas perfomed by HPLC/DAD
PVC
performed
bYFTIRand
Analysiswas
Test,
FLAME
Negative
Limit
100
TestReport
No.: CE/20'1214846ADale:201202104 Page 3 of 24
r ]lfltl|fl [tu||llll
CERAMTEC
GMBH
15D-91207
LAUF,GERMANY
CERAMICSLUITPOLDSTMSSE
I\4ULTIFUNCTIOML
Testltem(s)
Mothod
Unit
Analysis
to EN 14372.
Withreference
,nasperformedby GC/MS.
%
Witheferenceto EN 14372.Analysis
lva6per{ormedby GC/MS.
ok
to EN 14372.Analysis
Withreference
DIDP(Di-isodecylphthalate)(CAS
wasperformed
by GC/MS.
No.:26761-40-0)
o/o
Withreference
to EN14372.Analysis
DINP(Di-isononylphthalate)(CAS
per{ormed
was
by GC/irS.
No.r2855312-0)
to EN 14372.Analysis
phthalate)
%
With
reference
(cAS
(Di-n-octyl
DNOP
performed
by GC/MS.
was
11744-0)
No.:
to EN14372.Analysis
(CASNo.:
%
Withreference
DBP(Dibutylphthalate)
\ras performedby GC/MS.
u-74-2)
mg/Kg With referencetb US EPA8270D
dibromodiphenyl
Monomethyl
bY
Analysis
\rasperformed
method.
methane(DBBT)
GC/MS.
mg/Kg With referenceio US EPA8270D
dichlorodiphenyl
Monomethyl
by
Analysis
wasperformed
method.
methane(Ugilecl21)
(CAS
BBP(Benzylbdyl phthalate)
No.:8568-4
DEHP(Di-(2-ethylheryD
phthalate)
(cAs No.:117-81-7)
%
MDL
Result
No.1
0.003
n.d.
0.003
n.d.
0.01
0.01
n.d.
0.003
n.d.
0.003
n.d.
0.5
n.d.
0.5
n.d.
0.5
n.o.
0.03
n.d.
0.03
n.d.
I
n.d.
cc/Ms.
tetrachlorodiPhenYl mg/Kg With referenceto US EPA8270D
lronomethyl
wasperfomedbY
method.
Analysis
methane(Ugilec141)
GC/MS.
compounds
Organic.tln
TnbutylTin(TBT)
Tin (TphT)
Triphenyl
3.
mg/kg Wth referenceto DIN38407-1
perfomed
bY
GC/FPD.
was
Analysis
3.
mg/kg ul,/ithreferenceto DIN38407-1
by GC/FPDwasperformed
Analysis
Halons
to l-JSEPA5021
(CASNo.:353-59-3) m9Kg Withreference
Halon-1211
bY
Analysis
wasperformed
method.
GC/MS.
mg/Kg With referenceto US EPA5021
(CASNo.:7563-8)
Haion-1301
method.AnalysiswasPerformedbY
GC/MS.
to USEPA5021
(CASNo.:124-73-2) m9Kg Withreference
Halon-2402
bY
wasPedormed
Analysis
method.
GC/t!ts.
n-d.
n.d.
4r:'
r:2.J1.3!.101!ic
,1-3.3.9_19'l*:t
l?:L rrY :-s!,11
ur]r}il
Limit
scs
TestReport
No.I CE2012/14846AOalet2UA1ZU
Paget4of 24
|l]
CEMMTECGMBH
15D.91207LAUF,GERMANY
LUITPOLDSTMSSE
I,ULTIFUNCTIONAL
CERAIVICS
unit
T€6t ltem(s)
method
MDL
|lfl
Result
No.'l
Haloqen
mg/Kg Withreferenceto BS EN 1458212007.
(F) (CASNo.:
Halogen-Fluorine
14762-94-A)
(cl) (cAs No.:
Halogen-Chlorine
22537-15-11
(Br)(CASNo.:
Halogen-Bromine
10097-32-2)
by lC.
Analysis
wasperformed
.
mgKg With referenceto BS EN 1458212007
Analysis
wasperformed
by lC.
.
mg/Kg With referenceto BS EN 14582:2007
Analysis
wasperformed
by lC.
.
mg/Kg With referenceto BS EN 14582.2007
wasperformed
by lC.
Analysis
Halogenlodine(l) (CAS No.:
1436244-8)
Asbestos
(CASNo.:77536-66-4)
Actinolite
%
(CASNo.:12172-73-5)
Amosite
(CASNo.:n 53&67
Anthophyllite
(CASNo.r12001-29-5)
Chrysotile
%
Crocidolite(CASNo.: 12001-284\
o/o
(CASNo.:77536€8S)
Tremolite
%
com€n{ ,
t
ll
r+:
:,il
9:
Ltr
Withreference
to EPA600/R-93/116
wasperformed
by
method.
Analysis
SM.PLII andXRD.
with reference
to EPA600/R-93/116
method.Analysiswasperformedby
SM,PLMandXRD.
Withreference
to EPA600/R-93/116
Analysis
wasperformed
by
method.
SI/| PLMand)(RD.
With referenceto EPA600/R-93/1
16
by
method.
Analysis
wasperformed
SM,PL[, andXRD.
Withreference
to EPA600/R-93/116
method.
Analysis
wasperfomedby
Sl,l,PLMandXRD.
With referenceto EPA600/R-93n16
method.
Analysis
wasperformed
by
SM.PLl andXRD.
{lj
i
:-:
rh s ddcumm s 'suad by ihe comoanvslhrd b 's cenedrCmdiotrsdr Sede pdtrd ovedeatava'she
i d'c'or '$$
de *seF
50
n.d.
50
n.d.
50
n.d.
50
n.d.
'I
Negative
I
Negative
'I
Negative
1
Negative
Negative
Negative
]|lt]t
Limit
TestReport
No.: CE/2012i
148464 Dale:201ZO2|M Page:5of24
n]
CEMMTECGMBH
15D-9'I207
LAUF,GERI,|ANY
LUITPOLDSTRASSE
MULTIFUNCTIONALCERAI/!ICS
Tost ltefi(s)
Method
Unit
Sumof PBB6
Monobromobiphenyl
Dibromobiphenyl
MDL
5
fdbromobiphenyl
Tetrabromobiphenyl
Pentabrcmobiphenyl
Hex€bromobiphenyl
Heptabromobiphenyl
Oclabromobiphenyl
Nonabromobiphenyl
Decabromobiphenyl
Sumof PBDE3
Monobromodiphenyl
ether
Dibromodiphenyl
ether
€ther
f ribromodiphenyl
Tetrabromodiphenyl
ether
ether
Pentabromodiphenyl
Hexabromodiphenyl
ether
Heptabromodiphenyl
ether
ether
Octabromodiphenyl
Nonabromodiphenyl
eth€r
Decabromodiphenyl
ether
Withreference
to IEC62321:2008and
m9Kg perfomed
by GC/MS.
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
Result
No.'l
n,o,
mg/Kg with referenceto LFGB82.02-2.
3): 4-CHLORO-O-TOLUIDINE
(CAS No.: 9569-2)
Analysiswas p€rfomed by GC/MS.
(CAS
4): 2-NAPHTHYLAMINE
mg/kg with reference
to LFGB82.02-2.
wasperformed
by GC/MS.
No.:9'l-59-8)
Analysis
5): O-A[4INOMOTOLUENE(CAS mg/Kg Withreference
to LFGB82.02-2.
Analysis
wasperformed
by GC/MS.
No.: 97-56-3)
, 1 / -
'
i - . -
j
_
r r
d I'jr sdidionbsFsdstidbsrsf.tuy
codp.ny 6y uiaurhodzei!5 b6r of. roee,y or birstct on or me onient o
hoderorth€ doamenrtadusedh
Limit
1000
n.d.
n.d.
n.d.
n.o.
n.dn.d.
n.d.
n.d.
n.o.
n.dn.d.
n.d.
n.d.
n.d.
n-d.
5
5
n.d.
n.d.
n.d.
n.o.
n.d.
n.d.
3
n.d.
3
n.d.
,zo
'1):4-AMINODIPHENYL
(CASNo.: mg/Kg Withreference
to LFGB82.02-2.
9247-1)
Analysis
w€sperformed
by GC/MS(CASNo.i92-87- mg/kg Withreference
2rlBENZIOINE
to LFGB82.02-2.
Analysis
wasperformed
by GC/IVS.
tlllfllllllll
n.o.
3
n.d.
3
n-d.
1000
Test
Report
Pase
: 6of24
o^e.2o12tozo4
No'cEt2o1z14u6A
ll
CERAMTEC
GMBH
LAUF,GERI'ANY
15D.91207
CERAMICSLUITPOLDSTRASSE
MULTIFUNCTTONAL
[alllllll[llllu!!
3
Result
No.l
n.d.
3
n.d.
3
n.d.
3
n.d.
'10): 3,3'-DICHLOROBENZIDINE mg/Kg With refefenceto LFGB82.02-2.
Analysiswas perfomed by GC/MS.
(CASNo.:91-94-1)
3
n.o.
to LFGB82.02-2.
mg/Kg Withreference
11):3,3'-DIMETHOXYBENZIDINE
by GC/MS.
wasperformed
Analysis
(CASNo.:119-90{)
to LFGB82.02-2.
12):3,3'-DIMETHYLBENZIDINEmsyKg Withreference
bYGC/MS.
Analysis
wa6performed
(CASNo.:119-93-7)
3
n.d.
3
n.d-
mg/Kg With referenceto LFGB82.02-2.
13): 3,3'-DlMETHYL4,4Analysiswas performedby GC/MS.
DIAMINODIPHENYLMETHANE
(CAS No.: 838€8-0)
3
n.d.
Test ltem(s)
Unit
MDL
Method
to LFGB82.02-2.
mg/Kg Withreference
6):2.AMlNO-4-NITROTOLUENE
by GC/l\rS.
Analysis
waspertormed
(CASNo.:99-s5-8)
to
LFGB
82.02-2.
(CAs
With
reference
No.: mg/Kg
7): P4HLORoANILINE
performed
by GC/MS.
Analysis
wBs
106-47-8)
to LFGB82.02-2.
(CAS mg/Kg with reference
8):2,+DIAIVINOANISOLE
wasperformed
by GC/MS.
Analysis
No.:615-054)
LFGB
82.02-2.
With
reference
to
m9Kg
9):4,4Analysiswas performedby GC/I\IS.
DIAIVINODIPHENYLMETHANE
(CASNo.:101-77-9)
(2-METHoXY- mg/Kg Withreference
to LFGB82.02-2.
14):P-CRESIDINE
by GC/MS.
(CASNo.:
Analysis
wasperformed
s-ITETHYLANILINE)
120-71-a)
'15)r4,4'-METHYLENE-B|Sto LFGB82.02-2.
(2mgKg Withreference
pertormed
was
bYGC/lrS.
Analysis
(CASNo.:
CHLOROANILINE)
101-144)
(CAS
to LFGB82.02-2.
mg/Kg Withreference
16):4,4-OXYDIANILINE
performed
bYGC/MS.
was
Analysis
101-80{)
No.:
'17):4,4'-THIODIANILINE
to LFGB82.02-2.
(CAS
mg/Kg with reference
by GC/MS.
wasperformed
Analysis
No.:139€5-1)
n.d.
3
n.o.
3
n.d.
3
n.d.
mg/kg With referenceto LFGB82.02-2.
Analysiswas performedbYGC/IVS.
3
n.d.
to LFGB82.02-2.
19):2,+TOLUYLENEDIAIVINE mg/Kg Withreference
bYGC/MS.
Analysis
$/asperformed
(CASNo.r95€G7)
to LFGB82.02-2.
20)r2,4,5.TRllVETHYLANlLlNEmgkg Withreference
Analysis$rasperformedbYGC/MS.
(CASNo.:137-17-7)
to LFGB82.02-2.
(CASNo.:90- mgKg Withreference
21):O.ANISIDINE
performed
by Gc/llls
was
Analysis
04{)
3
n.d.
3
n.d.
3
n.d.
18): O-TOLUIDINE(CAS No.: 95534)
.,rr'41.;!!,
[email protected].
4,!a1ta
{i trli
Limit
Test Report
No.: CE/201214846ADaIe:2012102104Page,7 of 24
Il!t |||lu[llll
CERAMTEC
GMBH
15D.91207
LAUF,GERMANY
CERAMICSLUITPOLDSTMSSE
MULTIFUNCTIONAL
Test ltem(s)
Unit
22)rP-AMINOAZOBENzENE
(CASNo.:60-09-3)
(CASNo.:9523):2,4-XYLIDINE
68-1)
m9Kg
Method
MDL
R€ult
Withreference
to LFGB82.02-2.
by GC/lllS.
Analysis
waspertormed
to LFGB82.02-2.
mg/Kg Withreference
Analysis
wasperfomedby GC/MS.
to LFGB82.02-2.
mg/Kg with reference
Analysis
wasperformed
by GC/[iS.
3
No.1
n.d.
3
n.d.
3
n.d.
mg/kg Withreference
to USEPA5021
by
method.
Analysis
wasperformed
GC/MS.
(CASNo.: mg/Kg Withrefefence
to USEPA5021
Chlorof
luorocarbon-12
Analysis
wasperfomedby
method.
75-71-A)
GC/MS.
113(CASNo.: mg/Kg With referenceto US EPA5021
Chlorofluorocarbonby
method.
Analysis
wasperformed
76-13-1)
GC/t/lS.
to USEPA5021
14 (CAS No.: mg/Kg Withreference
Chlorofluorocalbon-'l
wasperformed
by
method.
Analy6is
76-14-21
GC/tS.
to USEPA5021
luorocarbon-1
15 (CASNo.: mg/kg Withreference
Chlorof
by
Analysis
wasperformed
method.
76-153)
GC/tS.
Grouplll
mg/Kg With referenceto US EPA5021
luoroca6on-1
3 (CASNo.:
Chlorof
by
Analysis
wasperformed
method.
75-72-9)
GC/MS.
(CASNo. mg/Kg With referenceto US EPA5021
Chlorofluoroca6on-111
by
wasperformed
method.
Analysis
354-56-3)
GC/MS,
to us EPA5021
12(CASNo.: mg/Kg with reference
Chlorofluorocarbon-1
by
Analysis
wasperformed
method.
76-12-O)
'I
n.d.
1
n-d-
1
n.d.
'I
n.d.
'l
n.d.
24): 2,6-XYLIDINE(CAS No.: 8762-7')
CFC's(Chlorof,uorocarbons)
GroupI
11 (CASNo.:
Chlorofluorocarbon75.69-4)
n.d.
n.d.
n.d.
GC/MS,
to USEPA5021
I (CASNo.: mg/Kg Withreference
luoroca6on-21
Chlorof
bY
wasperformed
Analysis
method.
422-78-6)
GC/MS.
1
n.o,
Limit
ll
Test Report
No.:CE/20'1214846ADale:2012j0A04 Page:8 of 24
CERAMTEC
GMBH
15D.9'1207
LAUF,GERMANY
CERAMICSLUITPOLDSTMSSE
MULTIFUNCTIONAL
Tost ltem(s)
Unit
Method
to USEPA5021
12(CASNo.i mgikg Withreference
Chlorofl
uorocarbon-2
by
method.
Analysis
waspertormed
3182-26-1)
GCiMS.
to USEPA502'1
luorocarbon-2l
3 (CASNo.: mg/Kg Withreference
Chlorof
wasperfomedby
method.
Analysis
2354-06-5)
GC/MS.
(CASNo.: mg/Kg With referenceto US EPA5021
luorocarbon-214
Chlorof
wasperfomedby
method.
Analysis
29255-3'1-0)
GC/MS,
(CASNo.: mg/Kg With feferenceto US EPA502'l
Chlorofluorocarbon-215
Analysis
wasperformed
by
method.
425943-2)
GC/MS.
(CAS No.i mg/kg Withreference
to USEPA5021
Chlorofluorocarbon-216
Analysis
waspefo.medby
method.
ffil-97-2)
GCitlts.
(CASNo.: mEks Withreference
to USEPA5021
luorocarbon-217
Chlorof
method.Analysiswasperformedby
422-864\
GC/MS.
(Chlorinate
hydrocarbon)
CHCs
(CAs
to USEPA5021
mg/Kg Withreference
1,1,1,2-Tetrachloroethane
wasperfomedby
method.
Analysis
No.r63G20€)
GC/MS.
'1,'1,
to USEPA5021
(CASNo.l
m!yKg Withrefefence
1-Trichloroethane
wasperfonned
by
method.
Analysi6
71-sffi)
GC/MS.
to USEPA5021
(CAS
mg/Kg Wth reference
1,1,2,2-Tetrachloroethane
bY
Analysis
wa6pertormed
method.
No.:7$34-5)
GC/tMS.
to uS EPA5021
(CASNo.:
mgikg Withreference
1,1,2-Trichloroethane
by
waspertormed
methodAnalysis
79-00-5)
GC/MS.
to USEPA502'1
(CASNo.:75- mgi'kg Withreference
1,1-Dichloroethane
bY
wasperformed
method.
Analysis
34-3)
GC/|VS.
'1
referenceto US EPA5021
mg/kg
With
(CAS
No.:
75,1-Dichlooethene
bY
wasPerformed
method.
Analysis
3s4)
GC/MS.
MDL
R€ult
No.1
n.d.
n.d.
n.d.
1
n.d.
'I
n.d.
1
n.d.
1
n.d.
1
n.o.
n.d.
n.d.
n.d.
'I
n.d.
Limit
scs
Test Report
No.: CE|201Z1484SADdet2O12l02lU Page:9 of 24
I| L |l|l[l[tilll
GMBH
CERAMTEC
LAUF,GERMANY
15D.91207
CERAMICSLUITPOLDSTMSSE
MULTIFUNCTIONAL
Test ltem(s)
'1,1-Dichloropropene
(CASNo.:
1
Result
No.t
n.o.
'1
n.o.
1
n.o.
1
n.o.
1
n.d.
1
n.o.
MDL
Method
Unit
to USEPA5021
m9Kg Withreference
wasperformedbY
method.
Analysis
56+546)
GC/MS.
to USEPA5021
(CAsNo.: mgKg Withreference
1,2,3-Tichloropropane
method.AnalysiswasperfomedbY
96-184)
GC/MS.
to USEPA5021
With
reference
(CASNo.:
mg/Kg
1,2-Dichloroethane
bY
wasperformed
method.
Analysis
1O74e2l
GC/MS.
(CASNo.:
mg/Kg with referenceto tJSEPA5021
1,2-Dichloropropane
wasperfomedby
method.
Analy6is
78€7-5)
GC/MS.
(CASNo.:
m!yKg With referenceto US EPA5021
1,3-Dichloropropane
wasperfomedbY
method.
Analy6is
142-28.91
GC/MS.
to IJSEPA5021
(CASNo.:
mg/Kg Withreference
2,2-Dichloropropane
method.Analysiswasperformedby
5S+20-71
GC/MS.
referenceto US EPA5021
(CAS
m(yKg
With
No.:
Ca6ontetrachlodde
waspedomedbY
method.
Analysis
56-23-s)
GC/MS.
(CASNo.:75-00-3) mg/Kg Withreference
to USEPA502'1
Chloroethane
bY
wasperformed
method.
Analysis
GC/MS.
(CASNo.:6766-3)
to USEPA5021
mg/kg Withreference
Chloroform
bY
wasPerformed
method.
Analysis
n,o.
n.d'I
n.d.
mg/Kg With referenceto US EPA502!
bY
wEsPerformed
Analysis
method.
GC/MS.
to USEPA5021
mg/Kg Withreference
bY
wasPerformed
Analysis
method.
GC/MS.
1
n.d.
,l
n.d.
to USEPA502'l
(CAsNo.: mg/Kg Withreferenc€
cis-1,lDichloropropene
bY
wasPerfomed
Analysis
method.
1006141-5)
GC/MS.
1
n.d.
cc/Ms.
(CASNo.;74-87Chloromethane
3)
(CASNo.i
cis-1,2-Dichloroethene
156-59-2)
(Nevr3F 'ieL{'r}:
r; I n:5n
l:r 33i1
Limit
Test Report
No.:C92012/14846A Oale|2O12JO2|MPage: 10 of 24
t m
CERAMTECGMBH
CERAMICS LUITPOLDSTMSSE15 D-91207LAUF,GERMANY
MULTIFUNCTIONAL
Test ltem(s)
Unit
Method
mg/Kg With referenceto US EPA5021
method.An€lysis\r€s performedbY
GC/MS.
(CAS
No.:75- mg/kg With referenceto US EPA5021
Methylene
Chloride
by
wasperformed
method.
Analysis
09-2)
GC/|VS.
(CASNo.:127- mg/kS With referenceto US EPA5021
Tetrachloroethene
bY
Analysis
wasperformed
method.
184)
GC/tVlS.
(CAS
mg/kg With referenceto US EPA5021
trane1,2-Dichloroethene
bY
Analysis
wasPerformed
method.
No.:15660-5)
GC/MS.
(CAS
mg/Kg With referenceto US EPA5021
trans-l,3-Dichloropropene
method.Analysis\ /asperfofmedby
No.:10061-024)
GC/MS.
(CASNo.:7$
mg/Kg with referenceto us EPA5021
Trichloroethylene
bY
Analysis
wasperformed
method.
01-6)
GC/MS.
HCFca
(Hydrochlorotluorccarbons)
mg/Kg Withreferenceto US EPA5021
HCFC-2l (CAS No.: 75-434)
wasperfomedbY
Analysis
method.
GC/MS.
m9Kg
With referenceto US EPA5021
(CAS
No.:
75-4S)
HCFC-22
bY
wasperformed
Analy6is
method.
GC/IVS,
mg/Kg Witll referenc€to US EPA502'!
(CASNo.:59!70'4)
HCFC-31
method.AnalysiswasPerformedbY
MDL
HCFC-121(CAS No.: 3gl4-3)
mg/Kg
With referenceto US EPA5021
wasperfomedbY
method.
Analysis
GC/MS.
to USEPAs021
(CASNo.:354-21-2) mg/Kg vVitlrreference
HcFc-122
bY
w€sPerfomed
Analysis
method.
GC/MS.
No.1
Limit
n.d.
(CASNo.:
Hexachlorobutadiene
87$8-3)
GC/lrs.
Result
[tlllll
I
n.d.
1
n.d.
1
n.d.
I
n.d.
1
n.d.
n.o.
1
n.d-
1
n.d.
'I
n.d.
n.d.
*" ^ - " - -- "'"
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r"is*r#rjnr"r.":"::;j.,;\lli:iTrr.5;,3::r.-"i'l#jili:n:*.ai."l;"*'ru;*#iair::'sih;*
Test Report
No.: CE/201214846A Date: 2012102104Page: 11 oI 24
ltfl ||[I|t l[]tr
CERAMTECGMBH
15 D-91207LAUF,GERMANY
CERAMICS LUITPOLDSTRASSE
MULTIFUNCTIONAL
Test ltem(s)
(CASNo.:306-83-2)
HCFC-123
Unit
lrethod
MDL
n.d.
mg/Kg Withreferenc€to US EPA502'1
method.
Analysis
wasperfomedby
GC/MS.
(CASNo.:2837-89-0) mg/Kg With referenceto US EPA502'1
HCFC-'124
wasperformed
by
method.
Analysis
GC/t S.
(CASNo.r359-28-4) mS/kg Withreference
to tJSEPA5021
HCFC-131
method.Analysiswasperformedby
GC/MS.
to USEPA5021
HCFCI32b(CASNo.:1649-08-7) mg/kg Withreference
wasperformed
by
method.
Analysis
GC/MS.
(cAs No.:75-88-7) mg/Kg With referenceto US EPA5021
HCFC-133a
method.Analysiswasperformedby
GC/MS.
HCFC-141b
{CASNo.:1717-00€) mg/Kg With referenceto US EPA5021
Analysis
wasperformed
by
method.
GC/trs.
to USEPA5021
mg/Kg Withreference
HCFCI42b(CASNo.:7568-3)
by
Analysis
wasperformed
methodGC/t S.
(CASNo.:422-26-4) mgKg Withreference
to USEPA5021
HCFC-221
wasperformed
by
method.
Analy6is
GC/t S.
to USEPA5021
mg/Kg Withreference
HCFC-222(CAS No.: 422.491)
by
Analysis
w€spertormed
method.
GC/t!ts.
to USEPA5021
mg/kg with reference
HCFC-223
{CASNo.:422-526)
by
Analysis
wasperformed
method.
GC/MS,
(CASNo.:422-54-8) mg/Kg With referenceto US EPA5021
HCFC-224
method.AnalysiswasperformedbY
GC/MS.
to USEPA5021
(CASNo.:422-56-0)mg/kg Withreference
HCFC-225C€
bY
wasPertormed
Analysis
method.
GC/lrs.
Result
No.1
n.d.
1
n.d.
1
n.o.
1
n.d.
1
n.d.
I
n.d.
1
n.d.
n.d.
n.d.
n.d.
,]
n.d.
Llmit
l
scs
Test Report
No.: CE|2O1Z14846ADaIe:201ZO2|U Page: 12 ol 24
||]u||||][llllllll
CERAMTEC
GMBH
15D-91207
LAUF,GERMANY
CERAMICSLUITPOLDSTMSSE
MULTIFUNCTIOML
lest ltem(s)
unit
(CASNo.:507-55-1) mgilg
HCFC-22scb
Method
MOL
Result
No,1
n.d.
Withreference
to USEPA5021
by
Analysis
waspedormed
method.
GC/trs.
(CASNo.:43'1-87-8)
HCFC-226
to USEPA5021
mg/Kg Withreference
method.
Analysi6
wasperfomedbY
GC/MS.
(CASNo.r42t-%-3)
mg/Kg With referenceto US EPA5021
HCFC-231
by
Analysis
wasperformed
method.
GC/MS.
(CASNo.:460-89-9) mg/Kg With referenc€to US EPA5021
HCFC-232
by
method.
Analysis
wasperformed
GC/MS.
(CASNo.:7125-84-0) mg/Kg With refe.enceto US EPA5021
HCFC-233
by
methodAnalysis
wasperformed
GC/[iS.
(CASNo.:425-94-5) mg/Kg Withreference
to USEPA5021
HCFC-234
by
method.
Analysis
wa6pertormed
GCi[rs.
m9Kg With referenceto US EPA5021
HCFC-235
{CASNo.:460-9-4)
Analysis
wasperfomedby
method.
GC/MS.
to USEPA5021
mgKg Withreference
HCFC-241(CAS No.: 6€6-27-3)
wasperfomedby
method.
Analy6is
GC/MS.
msyKg With referenceto US EPA5021
HCFC-242(CAS No.r4€0€3-9)
method.Analysiswasperformedby
GC/MS.
(cAs
With referenceto US EPA5021
m9Kg
No.:
46059-5)
HoFC-243
method.AnalysiswasPerformedbY
I
n.d-
1
n.d.
1
n.d.
I
n.d.
1
n.d.
1
n.d-
1
n,o.
n.o_
n.d.
GC/l\rs.
mg/kg With referenceto Us EPA5021
HCFC-244
',!asperformed
by
Analysis
method.
GC/MS.
(CASNo.:42'l-41-0) mg/Kg Withreferenc€
to Us EPA5021
HCFC-25'1
bY
wasPerformed
Analysis
method.
GC/MS.
I
n.d.
1
n.d.
Limit
Test Report
No.: CE12012,148464D ale .2O1Z0ZU
Page 13 of 24
tl
CEMMTECGMBH
15D-91207
LAUF,GERMANY
MULTIFUNCTIONAL
CERAMICSLUITPOLDSTRASSE
Test ltem(6)
HCFC-252{CAS No.: 819-001)
Unit
Method
MDL
[ |l[ [lll||llNt
R.sult
No.'l
Limit
n.d.
mg/Kg Withreference
to uS EPA5021
Analysis
wasperformed
by
method.
GC/MS.
(CASNo.:,16G.35-5) mg/Kg With refefenceto us EPA5021
HCFC-253
method.
Analysis
wasperfomedby
GC/MS.
(CASNo.:420-97-3) mg/Kg Withreferenceto US EPA5021
HCFC-261
wasperformed
by
method.
Analysis
n.o.
n.d.
GC/l\rs.
(CASNo.:421-02-03) mg/Kg Withreference
to USEPA5021
HCFC-262
by
method.
Analysis
wasperformed
GC/MS.
(CASNo.:430-55-7) mg/Kg With referenc€to US EPA5021
HCFC-271
method.
Analysis
wasperfomedby
GC/MS.
1
n.d.
1
n.d.
Note :
'1.
mg/kg= ppm i 0.1wf/o= 1000ppm
2. n.d. = Not Detected
3. MDL = MethodDeteclionLimit
4."-"=NotRegulated
5. " = Qualitativeanalysis(No Unit)
/ Positive= Detectable
6. Negative= Undetectable
7. Asbestos: Negative= "< 1.0%", Positive='> 1.0%"
PFOSRefe.enceInformatlon: POPS- (EU)7572010
products
or
in semi-finished
above0.001%('1oppm),
in concedtrations
or preparations
Outlawing
PFOSas substances
above1Fg/m'z
in textilesor othercoatedmaterials
articlesor partsat a levelabove0.1%(lOOOppm),
Test Report
No.I CEi2012/14846ADate| 2012102104Page'.14d 24
l||
CERAI,iITEC
GIVBH
15 D.91207LAUF,GERMANY
CERAMICS LUITPOLDSTRASSE
MULTIFUNCTIONAL
|!l||lflttl||rtl
'1) Thes€samplesweredissolvedtotallyby pre-conditioning
methodaccordingto belowflow chart
( Cr"' test method excluded)
2) Nameof the personwho mademeasurementClimbgre€tYang
3) Nameof the personin charg€of measulemenlTroyChang
SampleMeasurement
by suitable
acid
Aciddigestion
on difierent
s€mple
dep€nded
mateial(asbelowtable)
digestion
with
Microwave
HNq/HCUHF
amountof
Addappropriate
reagent
digestion
Heatto appropriate
temperatureto extract
Cool,filterdige6tate
AlkaliFusion
HCltodissolve
throughfilter
ICP-AES
DigestionAcid
SampleMaterial
S'teel,coppet aluminum,solder
Aqua regia,HNO3,HCl,HF,HrO,
HNO3/HF
Glass
palladium,
ceramic Aquaregia
Gold,platinum,
Silver
HN03
Plastic
HrOr,HNO3,HCI
H2SO4,
Others
Anyacidto totaldigestion
measurethe absorbance
at 540nmby UV-VIS
Test Report
No. CE/2012J14846A Dale:2012tO21O4 Page : 15 of 24
tt||]t
CERAMTECGMBH
CERAMICS LUITPOLDSTMSSE15 D.91207LAUF' GERIVANY
IJULTIFUNCTIONAL
|l0Lllllllllull
Analyticalflow chartof soxhletextractlon(LC/MS)procedure
I
I
RomanWong
Nameofthepersonwhomademeasulement:
TroyChang
peBon
of
measurement:
in
charge
Nameof the
' Benzotriazolo
( Testltems:PFOSTPFOA
)
SamplepretreatmenuseParation
I
Data
*ffirffiN,f*,tr
ffiffiffiffiN'g'gffirft
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TestReport
No.: CE201214846A Oale: 2012102104Page: 16 oI 24
CERAMTEC
GMBH
LAUF,GERMANY
15D-91207
LUITPoLDSTRASSE
CERAIVICS
I,,IULTIFUNCTIoNAL
rtr||[ttllllllu:rl|
Chlorinated Flame retardant analytical flow chart
'1) Nameof thepersonwhomademeasufement:
BarfyTseng
Troychang
2) Nameof thepersonin chargeof mea6ufement:
I
r
method:
USEPA8270D,US EPA3540
RefeGnce
PCTS,
Mirex,CP,MCCP
Testltems:PCBS.PCNS,
-- *-" "'"
*
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'ifi;i{i-"i:.
iljlJii.";
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TestReport
D ale:2012102M Page: 17 of 24
No.:CE/201214846A
CERAMTEC
GMBH
15D.91207
LAUF,GERIUANY
CERAIJICSLUITPOLDSTRASSE
MULTIFUNCTIONAL
of PVCin material
Analyslsflow chartfor determination
I
I
GinnyChen
Nameof thep€rsonwhomademeasurement
TroyChang
Nameofthepe6onin chargeof measurementr
Samplepretreatment
by FTIR
Sample
analyzed
Checkwave-number
of C-Clbonding
Data
i'i:;;;i;;l".'--&'hiet.m]!.i''-odjo'.c."€|'ro.mso
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,nd o edrctu romardoc,mnts *tir'16hr\atLc0no$b
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com Fnr Av unaurhmtd a[e6td.
roeery o. raibicrion or rlre @meii o
I-
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t?rl ..- rlr 1er.!1
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nrrIlllulltlt]t
TestReport
No.: CE/2012l148464Dale :2012,0210/' Page: 18 ol 24
CEMMTEC GMBH
MULTIFUNCTIONALCERAMICS
LUITPOLDSTRASSE'15
D-91207LAUF.GERIMANY
procedure
Analyticalflow chartof Soxhlet extraction(GC/MS)
r
r
Nameofthepersonwhomademeasurement
RomanWong
TroyChang
Nameof thepersonin chargeofmeasufement
' HBCOD. NP. DBBT'
(Test ltems:Phthalate' Benzotriazole
Organicphosphoruscompounds)
-n. r
-e:01y o'!:!
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!
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comDrryMyL.a {-o1ena F,toi
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|:l|rtrumm: I!
scs
I
Test Report
No.'.CE|201Z14UGA Dale:2012102104Paqe: 19of 24
CERAMTEC
GMBH
15D-91207
LAUF,GERMANY
IVULTIFUNCTIONAL
CERAMICSLUITPOLDSTMSSE
Analyticalflow chartof O.ganic-Tin
content
I
I
Nameofthe pe6onwhomademeasurement:
GinnyChen
person
Nameof the
in chafgeof measurement:
TroyChang
anosG) ele.d IhLsle$ rcPod€nnd
ii, do.rnid i ts&4 d h€ LomDrr $od ro sc{"?'condio'ro
and,olele@nr|o.go.a*ksbi'.c'b|eT3.tco'o1oTh'-'"'
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r ya' o
d od "c6| '-. te' "\ dued' o. *1d.. ;*n. \yyrT' e
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oniento
abBron bosry of rairer@ronorbe
cmoaiv Mv mau'honzdd
t -
r
l |ltfl[]trtrll
TestReport
No.: CE201214846A Dale| 201U0210/' Paae:20of24
CERAMTECGMBH
MULTIFUNCTIONAL
CERAMICS LUITPOLDSTRASSE
15 D.91207LAUF,GERMANY
tr!l[]|l[
t]||t
Analytical flow chart of halogen content
'l) Nameofihe D€rsonwho mademeasurementRitiaChen
2) Nameof the personin chargeof measurementTroyChang
/ Separation
Sampiepretrealrnent
Weighting
andputtingsamplein cell
/ Absorption
OxygenBombCombustion
Dilution
to fixedvolume
Analysis
wasperformed
by lC
4".*^,in"?ij**',=*"
n ui"i".oi, *d& i" ;
i",ior.s i s3D? /.{
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"*""
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TestReport
No.rCE/2012I14846AOale| 201202/c4' Paae:21o124
i||] ttll
CERAMTEC
GMBH
15D.91207
LAUF,GERI'ANY
MULTIFUNCTIONAL
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l rrl
Analysisflow chartfor determinationof Asbestos
'1) Nameof thepersonwhomademeasurement
VictorKao
WendyWei
2) Nameof thepersonin chargeof measurement
method:EPA600/R-93/11
6|
I Reference
Asbestos
identifcation
bydispersion
polarizalion
staining
lightmicroscopy
Asbestos/
Containing
LdessdsN* 'a,e b. rc$c ahoMLi!f sLes.r
rpenE eren,/.?fi:sj_sr.,:J:fi":,i1.tir[tr'*
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identificalion
byx-|ay
Asbestos/
Notconlaining
*"**
*".
itrH]'...',*,;-";";":,''"''*f."**";;.""i.,
aiidr.o1;ra-'-r"ra'd.-*s",dFd;re..".c-'|"';;L'e:.ni''km.1GdM{'€fugre
i.i''i.^ds''Nm@mnEjnmo,ima,a.""**oron.ji-,ni;;di.iid."ai-'*dtr,
liri1tu*4dffi##i#s*il{ir**lidiF#"r""*glfrrff
h*$fiff#,#ifff,,##i$;*$$;jtj'
(NevraF.it''r?lanrr
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:t::il
ri1r3|!
Test Report
No. : CE/2012l14846A Dare| 201i,02J04 Page'.22 ol 24
r
CERAMTECGMBH
[JULTIFUNCTIONAL
CERAMICS LUITPOLDSTMSSE15 D-91207LAUF,GERMANY
fitr| [lulllll
Analyticalflow chart
I
I
RomanWong
Nameof thepe€onwhomademeasurement
TroyChang
Nameof thepeEonin chargeof measurement:
TBBP-A-b|S
I
I Testltems:PBB/PBDE,
- '>
-----' Optionalscreen
process
prccess-""' Confirnation
process
Firsltesling
r r r r r r r r r r ...r ...t
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solution
concenhate/Dilute
Extracted
Filter
v
@
V
lssueReport
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a;*;.;;
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Test Report
No.: cE/2012/14846ADare| 201210204 Paae:23of24
CERAMTECGMBH
IVULTIFUNCTIONAL
CERAMICS LUITPOLDSTMSSE15 D-91207LAUF,GERMANY
Analyticalflow chartofvolatileorganlccompounds(VOCS)
I
I
: ChunWu
Nameoflhe personwhomademeasurement
: ShinjyhChen
Nameoflhe personin chargeofmeasurement
( Refercnce
:
method USEPA5021)
Samplepretreatment
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TestReport
No.rCE/2012'14846ADale:201zo2lM Page:24ot 24
CERAMTEC
GMBH
LAUF,GERIVANY
15D-91207
MULTIFUNCTIONAL
CERAIIICSLUITPOLDSTMSSE
' Thetestedsample/ paft is matkedby an arow if ifs shownon the photo.'
14846
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Test Report
Applicant:
Number : TWNC00249178
Littelfuse Philippines Inc.
LIMA Technology Center, Lipa City,
Malvar, Batangas
Date
: Mar 26, 2012
Sample Description:
One (1) group of submitted samples said to be :
Part Description
: Silver Clad Cu Wire with 2% Ag
Part Number
: 082xxx(082684)
Date Sample Received
: Mar 22, 2012
Date Test Started
: Mar 22, 2012
Test Conducted :
As requested by the applicant, for details please refer to attached pages.
Authorized By:
On Behalf Of Intertek Testing Services
Taiwan Limited
K. Y. Liang
Director
This report shall not be reproduced
except in full, without the written
approval of the laboratory.
Page 1 of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00249178
Test Conducted
(Ⅰ) Test Result Summary :
Test Item
Heavy Metal
Cadmium (Cd) content
Lead (Pb) content
Mercury (Hg) content
Chromium VI (Cr6+) content (mg/kg with 50cm2)
Remarks: ppm =
ND =
<
=
mg/kg
Result (ppm)
Silvery Wire
ND
ND
ND
Negative (< 0.02)
Parts per million based on weight of tested sample = mg/kg
Not detected
Less than
with 50cm2 = milligram per kilogram with 50 square centimetre
Responsibility of Chemist : Irene Chiou / Kevin Liu / Cathy Chen
Date Sample Received
Test Period
: Mar 22, 2012
: Mar 22, 2012 To Mar 26, 2012
(Ⅱ) RoHS Requirement:
Restricted Substances
Cadmium (Cd) Content
Lead (Pb) Content
Mercury (Hg) Content
Chromium VI (Cr6+) Content
Limits
0.01% (100ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for
homogeneous material.
Page 2 of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00249178
Test Conducted
(Ⅲ) Test Method:
Test Item
Cadmium (Cd)
content
Lead (Pb) content
Mercury (Hg)
content
Chromium VI (Cr6+)
content
Test Method
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 7, by microwave
digestion until the tested samples are
totally dissolved and determined by
ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in annex B, by boiling water
extraction and determined by UV-Vis
Spectrophotometer.
Reporting Limit
2 ppm
2 ppm
2 ppm
0.02
mg/kg with 50cm2
Remark: Reporting limit = Quantitation limit of analyte in sample
Page 3 of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00249178
Test Conducted
(Ⅳ) Measurement Flowchart:
Test For Cd/Pb/Hg/Chromium (VI)
Reference Standard：IEC 62321 edition 1.0:2008
Sampling/grinding or cutting
Cd/Pb/Hg
Cr
Polymers /
Electronics
Metal
For different
material, digest
the sample with
*1
appropriate acid
By spot test
Negative
Confirm the tested
samples are
totally dissolved
Make up with
deionized water
6+
*2
Weigh sample
and add
alkaline
solution
Get 50cm2 sample
Definite temp.
extraction
Boiling water
extraction
Cool and filter
the extract
Analyzed by ICP-OES
Make up with deionized
water and add diphenylcarbazide solution
Remarks:
*1: List Of Appropriate Acid：
Material
Polymers
Metals
Electronics
Analyzed by UV-VIS
Acid Added For Digestion
HNO3,HCl,HF,H2O2,H3BO3
HNO3,HCl,HF
HNO3,HCl,H2O2,HBF4
*2: If the result of spot test is positive, Chromium VI would be determined as detected.
End of Report
Page 4 of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00249178
Test Conducted
Photo
Page 5 of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Test Report
Applicant:
Number : TWNC00249177
Littelfuse Philippines Inc.
LIMA Technology Center, Lipa City,
Malvar, Batangas
Date
: Mar 26, 2012
Sample Description:
One (1) group of submitted samples said to be :
Part Description
: Silver Clad Cu Wire with 5% Ag
Part Number
: 082xxx(082375)
Date Sample Received
: Mar 22, 2012
Date Test Started
: Mar 22, 2012
Test Conducted :
As requested by the applicant, for details please refer to attached pages.
Authorized By:
On Behalf Of Intertek Testing Services
Taiwan Limited
K. Y. Liang
Director
This report shall not be reproduced
except in full, without the written
approval of the laboratory.
Page 1 of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00249177
Test Conducted
(Ⅰ) Test Result Summary :
Test Item
Heavy Metal
Cadmium (Cd) content
Lead (Pb) content
Mercury (Hg) content
Chromium VI (Cr6+) content (mg/kg with 50cm2)
Remarks: ppm =
ND =
<
=
mg/kg
Result (ppm)
Silvery Wire
ND
ND
ND
Negative (< 0.02)
Parts per million based on weight of tested sample = mg/kg
Not detected
Less than
with 50cm2 = milligram per kilogram with 50 square centimetre
Responsibility of Chemist : Irene Chiou / Kevin Liu / Cathy Chen
Date Sample Received
Test Period
: Mar 22, 2012
: Mar 22, 2012 To Mar 26, 2012
(Ⅱ) RoHS Requirement:
Restricted Substances
Cadmium (Cd) Content
Lead (Pb) Content
Mercury (Hg) Content
Chromium VI (Cr6+) Content
Limits
0.01% (100ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for
homogeneous material.
Page 2 of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00249177
Test Conducted
(Ⅲ) Test Method:
Test Item
Cadmium (Cd)
content
Lead (Pb) content
Mercury (Hg)
content
Chromium VI (Cr6+)
content
Test Method
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 7, by microwave
digestion until the tested samples are
totally dissolved and determined by
ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in annex B, by boiling water
extraction and determined by UV-Vis
Spectrophotometer.
Reporting Limit
2 ppm
2 ppm
2 ppm
0.02
mg/kg with 50cm2
Remark: Reporting limit = Quantitation limit of analyte in sample
Page 3 of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00249177
Test Conducted
(Ⅳ) Measurement Flowchart:
Test For Cd/Pb/Hg/Chromium (VI)
Reference Standard：IEC 62321 edition 1.0:2008
Sampling/grinding or cutting
Cd/Pb/Hg
Cr
Polymers /
Electronics
Metal
For different
material, digest
the sample with
*1
appropriate acid
By spot test
Negative
Confirm the tested
samples are
totally dissolved
Make up with
deionized water
6+
*2
Weigh sample
and add
alkaline
solution
Get 50cm2 sample
Definite temp.
extraction
Boiling water
extraction
Cool and filter
the extract
Analyzed by ICP-OES
Make up with deionized
water and add diphenylcarbazide solution
Remarks:
*1: List Of Appropriate Acid：
Material
Polymers
Metals
Electronics
Analyzed by UV-VIS
Acid Added For Digestion
HNO3,HCl,HF,H2O2,H3BO3
HNO3,HCl,HF
HNO3,HCl,H2O2,HBF4
*2: If the result of spot test is positive, Chromium VI would be determined as detected.
End of Report
Page 4 of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00249177
Test Conducted
Photo
Page 5 of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Intertek Consumer Goods GmbH · Würzburger Straße 152 · 90766 Fürth ·
Polyfil AG
Gina Gregorio
Oberallmendstrasse 20A
6300 Zug / Switzerland
Fürth, 2012-12-19
Test report No. FUHL1236935
Testing of a material sample according to the RoHS directive 2011/65/EC
Sample description: Ni36Fe64MAg wire; part no. 962464; batch 497255Rev.B
Arrival in lab: 2012-012-04; Period of XRF analysis incl. sample preparation and photo documentation: 2012-12-07 – 2012-12-10
Head of Inorganic Lab: Claudia List
Copying this test report is permitted only in agreement with the contracted lab. The test results refer only to the tested item.
This report consists of 6 page(s).
The test methods signed with * are not listed in the attachment of the accreditation certificate.
Conclusion based on tested item
Status
Test order
testing according to the RoHS directive 2011/65/EC
°
conform°
Please see overview of test results
- Test results see next pages -
Intertek Consumer Goods GmbH
Würzburger Straße 152
90766 Fürth, Germany
Tel.: +49 911 74075 0
Fax: +49 911 74075 30
[email protected]
Sitz Fürth
Amtsgericht Fürth, HRB 5756
USt-IdNr. DE169317871
Geschäftsführer
Kay Grönhardt
Rainer Mast
Durch die DAkkS nach DIN EN ISO/IEC
17025 akkreditiertes Prüflaboratorium
Die Akkreditierung gilt für die in der
Urkunde aufgeführten Prüfverfahren.
Page 2 of 6 page(s) of our test report No. FUHL1236935 dated 2012-12-19
Sample description: Ni36Fe64MAg wire; part no. 962464; batch 497255Rev.B
nM = non Metal
M = Metal
cM = composite Material
List of component parts:
Sample No. Part No.
236935
1
Intertek Consumer Goods GmbH
Würzburger Straße 152
90766 Fürth, Germany
Material Description
M
Ni36Fe64MAg wire; part no. 962464; batch 497255Rev.B
Tel.: +49 911 74075 0
Fax: +49 911 74075 30
[email protected]
Sitz Fürth
Amtsgericht Fürth, HRB 5756
Ust-IdNr. DE169317871
Geschäftsführer
Kay Grönhardt
Rainer Mast
Page 3 of 6 page(s) of our test report No. FUHL1236935 dated 2012-12-19
Sample description: Ni36Fe64MAg wire; part no. 962464; batch 497255Rev.B
Comment
LOD = Limit of Detection
BL
OL
X
σ
=
=
=
=
Below Limit
Over Limit
Inconclusive, further test necessary
Standard deviation
CS
= Composite sample
Remark:
Results were obtained by EDXRF for primary screening. Additional chemical testing using ICP (for Cd, Pb),
AAS (for Hg), IC-UC/VIS (for CrVI) and GC/MS (for PBBs/PBDEs) are recommended, if the concentration
exceeds the below warning value according to IEC 62321.
Element
Cd
Pb
Hg
Br
Cr
Unit
mg / kg
mg / kg
mg / kg
mg / kg
mg / kg
non - metal
BL ≤ (70-3σ) < X < (130+3σ) ≤ OL
BL ≤ (700-3σ) < X < (1300+3σ) ≤ OL
BL ≤ (700-3σ) < X < (1300+3σ) ≤ OL
BL ≤ (300-3σ) < X
BL ≤ (700-3σ) < X
Element
Cd
Pb
Hg
Br
Cr
Unit
mg / kg
mg / kg
mg / kg
mg / kg
mg / kg
composite material
LOD < X < (150+3σ) ≤ OL
BL ≤ (500-3σ) < X < (1500+3σ) ≤ OL
BL ≤ (500-3σ) < X < (1500+3σ) ≤ OL
BL ≤ (250-3σ) < X
BL ≤ (500-3σ) < X
Intertek Consumer Goods GmbH
Würzburger Straße 152
90766 Fürth, Germany
Tel.: +49 911 74075 0
Fax: +49 911 74075 30
[email protected]
metal
BL ≤ (70-3σ) < X < (130+3σ) ≤ OL
BL ≤ (700-3σ) < X < (1300+3σ) ≤ OL
BL ≤ (700-3σ) < X < (1300+3σ) ≤ OL
-BL ≤ (700-3σ) < X
Sitz Fürth
Amtsgericht Fürth, HRB 5756
Ust-IdNr. DE169317871
Geschäftsführer
Kay Grönhardt
Rainer Mast
Page 4 of 6 page(s) of our test report No. FUHL1236935 dated 2012-12-19
Sample description: Ni36Fe64MAg wire; part no. 962464; batch 497255Rev.B
1. XRF screening
Method:
Sample No.
236935
XRF according to IEC 62321:2008*
Part No.
1
Pb
Hg
Cd
Crtotal
Br
Status
BL
BL
BL
BL
--
conform
Comment:
Elements
Lead (Pb)
Mercury (Hg)
Cadmium (Cd)
Chromium VI (Cr VI)
Polybrominated Biphenyle (PBBs)
Polybrominated Diphenyl ether (PBDEs)
RoHS-limit value
1000 mg/kg
1000 mg/kg
100 mg/kg
1000 mg/kg
1000 mg/kg
1000 mg/kg
- Flow charts see next page(s) -
Intertek Consumer Goods GmbH
Würzburger Straße 152
90766 Fürth, Germany
Tel.: +49 911 74075 0
Fax: +49 911 74075 30
[email protected]
Sitz Fürth
Amtsgericht Fürth, HRB 5756
Ust-IdNr. DE169317871
Geschäftsführer
Kay Grönhardt
Rainer Mast
Test procedure
Page 5 of 6 page(s)
YES
non-destructive
sample
preparation
sample
uniform ?
screening
procedure
by XRF
YES
NO
samples
mechanical
sample
preparation
screening
by XRF ?
metallic
materials,
pass
meets
limits ?
YES
NO
YES
fail
further
testing ?
NO
NO
mechanical
sample
preparation
polymer
materials,
entity based
conforming
sample
chemical test
procedure (verification)
various methods
(please see verification test
procedure below)
entity based
non conforming
sample
pass
YES
electronics
(PCB / component)
entity based
conforming
sample
meets
limits ?
fail
NO
Intertek Consumer Goods GmbH
Würzburger Straße 152
90766 Fürth, Germany
Tel.: +49 911 74075 0
Fax: +49 911 74075 30
[email protected]
Sitz Fürth
Amtsgericht Fürth, HRB 5756
Ust-IdNr. DE169317871
Geschäftsführer
Kay Grönhardt
Rainer Mast
entity based
non conforming
sample
Verification test procedure
Page 6 of 6 page(s)
Sample Preparation
Sample Measurement
Acid digestion with
microwave / hotplate
Sample solvent
extraction
Filtration
Concentration/
Dilution of extraction
solution
Solution
Cr6+
PBBs/PBDEs
Pb/Cd/Hg
Residue
Filtration
Total digestion
GC/MS
DATA
Non-metallic
material
Alkaline extraction
Adding extraction
solution
Metallic
material
Positive
Negative
Boiling water
extraction
Alkaline extraction
Heating to 90~95°C
for extraction
Adding 1,5diphenylcarbazide
for color development
Filtration and pH
adjustment
ICP-OES/AAS
A red color indicates
the presence of Cr6+
If necessary, confirm
with UV-VIS or
IC-UV/VIS
Adding 1,5diphenylcarbazide
for color development
DATA
DATA
UV-VIS or
IC-UV/VIS
DATA
Intertek Consumer Goods GmbH
Würzburger Straße 152
90766 Fürth, Germany
Tel.: +49 911 74075 0
Fax: +49 911 74075 30
[email protected]
Sitz Fürth
Amtsgericht Fürth, HRB 5756
Ust-IdNr. DE169317871
Spot test
Geschäftsführer
Kay Grönhardt
Rainer Mast
Intertek Consumer Goods GmbH · Würzburger Straße 152 · 90766 Fürth ·
Polyfil AG
Gina Gregorio
Oberallmendstrasse 20A
6300 Zug / Switzerland
Fürth, 2012-12-19
Test report No. FUHL1236937
Testing of a material sample according to the RoHS directive 2011/65/EC
Sample description: Ni42Fe58MCuMAg wire; part no. HL26351
Arrival in lab: 2012-012-04; Period of XRF analysis incl. sample preparation and photo documentation: 2012-12-07 – 2012-12-10
Head of Inorganic Lab: Claudia List
Copying this test report is permitted only in agreement with the contracted lab. The test results refer only to the tested item.
This report consists of 6 page(s).
The test methods signed with * are not listed in the attachment of the accreditation certificate.
Conclusion based on tested item
Status
Test order
testing according to the RoHS directive 2011/65/EC
°
conform°
Please see overview of test results
- Test results see next pages -
Intertek Consumer Goods GmbH
Würzburger Straße 152
90766 Fürth, Germany
Tel.: +49 911 74075 0
Fax: +49 911 74075 30
[email protected]
Sitz Fürth
Amtsgericht Fürth, HRB 5756
USt-IdNr. DE169317871
Geschäftsführer
Kay Grönhardt
Rainer Mast
Durch die DAkkS nach DIN EN ISO/IEC
17025 akkreditiertes Prüflaboratorium
Die Akkreditierung gilt für die in der
Urkunde aufgeführten Prüfverfahren.
Page 2 of 6 page(s) of our test report No. FUHL1236937 dated 2012-12-19
Sample description: Ni42Fe58MCuMAg wire; part no. HL26351
nM = non Metal
M = Metal
cM = composite Material
List of component parts:
Sample No. Part No.
236937
1
Intertek Consumer Goods GmbH
Würzburger Straße 152
90766 Fürth, Germany
Material Description
M
Ni42Fe58MCuMAg wire; part no. HL26351
Tel.: +49 911 74075 0
Fax: +49 911 74075 30
[email protected]
Sitz Fürth
Amtsgericht Fürth, HRB 5756
Ust-IdNr. DE169317871
Geschäftsführer
Kay Grönhardt
Rainer Mast
Page 3 of 6 page(s) of our test report No. FUHL1236937 dated 2012-12-19
Sample description: Ni42Fe58MCuMAg wire; part no. HL26351
Comment
LOD = Limit of Detection
BL
OL
X
σ
=
=
=
=
Below Limit
Over Limit
Inconclusive, further test necessary
Standard deviation
CS
= Composite sample
Remark:
Results were obtained by EDXRF for primary screening. Additional chemical testing using ICP (for Cd, Pb),
AAS (for Hg), IC-UC/VIS (for CrVI) and GC/MS (for PBBs/PBDEs) are recommended, if the concentration
exceeds the below warning value according to IEC 62321.
Element
Cd
Pb
Hg
Br
Cr
Unit
mg / kg
mg / kg
mg / kg
mg / kg
mg / kg
non - metal
BL ≤ (70-3σ) < X < (130+3σ) ≤ OL
BL ≤ (700-3σ) < X < (1300+3σ) ≤ OL
BL ≤ (700-3σ) < X < (1300+3σ) ≤ OL
BL ≤ (300-3σ) < X
BL ≤ (700-3σ) < X
Element
Cd
Pb
Hg
Br
Cr
Unit
mg / kg
mg / kg
mg / kg
mg / kg
mg / kg
composite material
LOD < X < (150+3σ) ≤ OL
BL ≤ (500-3σ) < X < (1500+3σ) ≤ OL
BL ≤ (500-3σ) < X < (1500+3σ) ≤ OL
BL ≤ (250-3σ) < X
BL ≤ (500-3σ) < X
Intertek Consumer Goods GmbH
Würzburger Straße 152
90766 Fürth, Germany
Tel.: +49 911 74075 0
Fax: +49 911 74075 30
[email protected]
metal
BL ≤ (70-3σ) < X < (130+3σ) ≤ OL
BL ≤ (700-3σ) < X < (1300+3σ) ≤ OL
BL ≤ (700-3σ) < X < (1300+3σ) ≤ OL
-BL ≤ (700-3σ) < X
Sitz Fürth
Amtsgericht Fürth, HRB 5756
Ust-IdNr. DE169317871
Geschäftsführer
Kay Grönhardt
Rainer Mast
Page 4 of 6 page(s) of our test report No. FUHL1236937 dated 2012-12-19
Sample description: Ni42Fe58MCuMAg wire; part no. HL26351
1. XRF screening
Method:
Sample No.
236937
XRF according to IEC 62321:2008*
Part No.
1
Pb
Hg
Cd
Crtotal
Br
Status
BL
BL
BL
BL
--
conform
Comment:
Elements
Lead (Pb)
Mercury (Hg)
Cadmium (Cd)
Chromium VI (Cr VI)
Polybrominated Biphenyle (PBBs)
Polybrominated Diphenyl ether (PBDEs)
RoHS-limit value
1000 mg/kg
1000 mg/kg
100 mg/kg
1000 mg/kg
1000 mg/kg
1000 mg/kg
- Flow charts see next page(s) -
Intertek Consumer Goods GmbH
Würzburger Straße 152
90766 Fürth, Germany
Tel.: +49 911 74075 0
Fax: +49 911 74075 30
[email protected]
Sitz Fürth
Amtsgericht Fürth, HRB 5756
Ust-IdNr. DE169317871
Geschäftsführer
Kay Grönhardt
Rainer Mast
Test procedure
Page 5 of 6 page(s)
YES
non-destructive
sample
preparation
sample
uniform ?
screening
procedure
by XRF
YES
NO
samples
mechanical
sample
preparation
screening
by XRF ?
metallic
materials,
pass
meets
limits ?
YES
NO
YES
fail
further
testing ?
NO
NO
mechanical
sample
preparation
polymer
materials,
entity based
conforming
sample
chemical test
procedure (verification)
various methods
(please see verification test
procedure below)
entity based
non conforming
sample
pass
YES
electronics
(PCB / component)
entity based
conforming
sample
meets
limits ?
fail
NO
Intertek Consumer Goods GmbH
Würzburger Straße 152
90766 Fürth, Germany
Tel.: +49 911 74075 0
Fax: +49 911 74075 30
[email protected]
Sitz Fürth
Amtsgericht Fürth, HRB 5756
Ust-IdNr. DE169317871
Geschäftsführer
Kay Grönhardt
Rainer Mast
entity based
non conforming
sample
Verification test procedure
Page 6 of 6 page(s)
Sample Preparation
Sample Measurement
Acid digestion with
microwave / hotplate
Sample solvent
extraction
Filtration
Concentration/
Dilution of extraction
solution
Solution
Cr6+
PBBs/PBDEs
Pb/Cd/Hg
Residue
Filtration
Total digestion
GC/MS
DATA
Non-metallic
material
Alkaline extraction
Adding extraction
solution
Metallic
material
Positive
Negative
Boiling water
extraction
Alkaline extraction
Heating to 90~95°C
for extraction
Adding 1,5diphenylcarbazide
for color development
Filtration and pH
adjustment
ICP-OES/AAS
A red color indicates
the presence of Cr6+
If necessary, confirm
with UV-VIS or
IC-UV/VIS
Adding 1,5diphenylcarbazide
for color development
DATA
DATA
UV-VIS or
IC-UV/VIS
DATA
Intertek Consumer Goods GmbH
Würzburger Straße 152
90766 Fürth, Germany
Tel.: +49 911 74075 0
Fax: +49 911 74075 30
[email protected]
Sitz Fürth
Amtsgericht Fürth, HRB 5756
Ust-IdNr. DE169317871
Spot test
Geschäftsführer
Kay Grönhardt
Rainer Mast
Test Report
Applicant:
Number : TWNC00285771
Littelfuse Philippines Inc.
LIMA Technology Center, Lipa City,
Malvar, Batangas
Date
: Nov 16, 2012
Sample Description:
One (1) group of submitted samples said to be :
Part Description
: Solder (Pb is ≥ 90%)
Part Number
: 692321
Date Sample Received
: Nov 12, 2012
Date Test Started
: Nov 13, 2012
Test Conducted :
As requested by the applicant, for details please refer to attached pages.
Authorized By:
On Behalf Of Intertek Testing Services
Taiwan Limited
K. Y. Liang
Director
*THJ0285771*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410
Page 1 of 6
Number : TWNC00285771
Test Conducted
(Ⅰ) Test Result Summary :
Result (ppm)
Silvery metal
Test Item
Heavy Metal
Cadmium (Cd) content
Lead (Pb) content
Mercury (Hg) content
Chromium VI (Cr6+) content (mg/kg with 50cm2)
ND
934557
ND
Negative (< 0.02)
Remarks: ppm = Parts per million based on weight of tested sample = mg/kg
ND = Not detected
<
= Less than
mg/kg with 50cm2 = milligram per kilogram with 50 square centimetre
Negative = A negative test result indicated positive observation
was not found at the time of Test.
Responsibility of Chemist : Irene Chiou / Kevin Liu
Date Sample Received
Test Period
: Nov 12, 2012
: Nov 13, 2012 to Nov 16, 2012
(Ⅱ) RoHS Limits:
Restricted Substances
Cadmium (Cd) Content
Lead (Pb) Content
Mercury (Hg) Content
Chromium VI (Cr6+) Content
Limits
0.01% (100ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
The above limits were quoted from Annex II of 2011/65/EU for homogeneous
material.
*THJ0285771*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410
Page 2 of 6
Number : TWNC00285771
Test Conducted
(Ⅲ) Test Method:
Test Item
Cadmium (Cd)
content
Lead (Pb) content
Mercury (Hg)
content
Chromium VI (Cr6+)
content
Test Method
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 7, by microwave
digestion until the tested samples are
totally dissolved and determined by
ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in annex B, by boiling water
extraction and determined by UV-Vis
Spectrophotometer.
Reporting Limit
2 ppm
2 ppm
2 ppm
0.02
mg/kg with 50cm2
Remark: Reporting limit = Quantitation limit of analyte in sample
*THJ0285771*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410
Page 3 of 6
Number : TWNC00285771
Test Conducted
(Ⅳ) Measurement Flowchart:
Test For Cd/Pb/Hg/Chromium (VI)
Reference Standard：IEC 62321 edition 1.0:2008
Sampling/grinding or cutting
Cd/Pb/Hg
Cr
6+
Polymers /
Electronics
Metal
For different
material, digest
the sample with
*1
appropriate acid
By spot test
Negative
Confirm the tested
samples are
totally dissolved
Make up with
deionized water
*2
Weigh sample
and add
alkaline
solution
Get 50cm2 sample
Definite temp.
extraction
Boiling water
extraction
Cool and filter
the extract
Analyzed by ICP-OES
Make up with deionized
water and add diphenylcarbazide solution
Analyzed by UV-VIS
*THJ0285771*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410
Page 4 of 6
Number : TWNC00285771
Test Conducted
Remarks:
*1: List of Appropriate Acid：
Acid Added for Digestion
Material
Polymers
HNO3,HCl,HF,H2O2,H3BO3
Metals
HNO3,HCl,HF
Electronics
HNO3,HCl,H2O2,HBF4
*2: If the result of spot test is positive, Chromium VI would be determined
as detected.
End of Report
This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a
recommendation for any particular course of action. Intertek does not accept a duty of care or any other responsibility to any person other than
the Client in respect of this report and only accepts liability to the Client insofar as is expressly contained in the terms and conditions
governing Intertek's provision of services to you. Intertek makes no warranties or representations either express or implied with respect to this
report save as provided for in those terms and conditions. We have aimed to conduct the Review on a diligent and careful basis and we do not
accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by statute or otherwise, except in
the event of our gross negligence or wilful misconduct.
*THJ0285771*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410
Page 5 of 6
Number : TWNC00285771
Test Conducted
Photo
*THJ0285771*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410
Page 6 of 6
Test Report
Applicant:
Number : TWNC00253636
Littelfuse Philippines Inc.
LIMA Technology Center, Lipa City,
Malvar, Batangas
Date
: Apr 24, 2012
Sample Description:
One (1) group of submitted samples said to be :
Part Description
: Black Ink
Part Number
: 425809
Date Sample Received
: Apr 19, 2012
Date Test Started
: Apr 19, 2012
Test Conducted :
As requested by the applicant, for details please refer to attached pages.
Authorized By:
On Behalf Of Intertek Testing Services
Taiwan Limited
K. Y. Liang
Director
This report shall not be reproduced
except in full, without the written
approval of the laboratory.
Page 1 of 9
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00253636
Test Conducted
(Ⅰ) Test Result Summary :
Test Item
Heavy Metal
Cadmium (Cd) content
Lead (Pb) content
Mercury (Hg) content
Chromium VI (Cr6+) content
Polybrominated Biphenyls (PBBs)
Monobrominated Biphenyls (MonoBB)
Dibrominated Biphenyls (DiBB)
Tribrominated Biphenyls (TriBB)
Tetrabrominated Biphenyls (TetraBB)
Pentabrominated Biphenyls (PentaBB)
Hexabrominated Biphenyls (HexaBB)
Heptabrominated Biphenyls (HeptaBB)
Octabrominated Biphenyls (OctaBB)
Nonabrominated Biphenyls (NonaBB)
Decabrominated Biphenyl (DecaBB)
Polybrominated Diphenyl Ethers (PBDEs)
Monobrominated Diphenyl Ethers (MonoBDE)
Dibrominated Diphenyl Ethers (DiBDE)
Tribrominated Diphenyl Ethers (TriBDE)
Tetrabrominated Diphenyl Ethers (TetraBDE)
Pentabrominated Diphenyl Ethers (PentaBDE)
Hexabrominated Diphenyl Ethers (HexaBDE)
Heptabrominated Diphenyl Ethers (HeptaBDE)
Octabrominated Diphenyl Ethers (OctaBDE)
Nonabrominated Diphenyl Ethers (NonaBDE)
Decabrominated Diphenyl Ether (DecaBDE)
Result (ppm)
Black Paste
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Page 2 of 9
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00253636
Test Conducted
(Ⅰ) Test Result Summary :
Test Item
Result (ppm)
Black Paste
Halogen Content
Fluorine (F)
Chlorine (Cl)
Bromine (Br)
Iodine (I)
Phthalates
Di(2-ethylhexyl) Phthalate (DEHP)
Dibutyl Phthalate (DBP)
Benzyl Butyl Phthalate (BBP)
Others
Hexabromocyclododecane (HBCDD)
ND
610
ND
ND
ND
ND
ND
ND
Remarks: ppm = Parts per million based on wet weight of tested sample =
mg/kg
ND = Not detected
Responsibility of Chemist : Irene Chiou / Kevin Liu / Cathy Chen
Date Sample Received
Test Period
: Apr 19, 2012
: Apr 19, 2012 To Apr 24, 2012
(Ⅱ) RoHS Requirement:
Restricted Substances
Cadmium (Cd) Content
Lead (Pb) Content
Mercury (Hg) Content
Chromium VI (Cr6+) Content
Polybrominated Biphenyls (PBBs)
Polybrominated Diphenyl Ehters (PBDEs)
Limits
0.01% (100ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for
homogeneous material.
Page 3 of 9
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00253636
Test Conducted
(Ⅲ) Test Method:
Test Item
Test Method
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
Cadmium (Cd) content
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
Lead (Pb) content
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 7, by microwave
Mercury (Hg) content
digestion until the tested samples
are totally dissolved and determined
by ICP-OES.
With reference to IEC 62321 edition
Chromium VI (Cr6+)
1.0:2008 in annex C, by alkaline
content
digestion and determined by UV-Vis
spectrophotometer.
With reference to IEC 62321 edition
1.0:2008 in annex A, by solvent
Polybrominated
extraction and determined by GC-MS
Biphenyls (PBBs)
and further HPLC-DAD confirmation
when necessary.
With reference to IEC 62321 edition
Polybrominated
1.0:2008 in annex A, by solvent
Diphenyl Ethers
extraction and determined by GC-MS
(PBDEs)
and further HPLC-DAD confirmation
when necessary.
With reference to EN 14582:2007 by
Halogen Content
calorimetric bomb with oxygen and
determined by Ion Chromatograph.
With reference to EN 14372: 2004, by
Phthalates
solvent extraction and determined by
GC-MS.
With reference to USEPA 3540C, by
Hexabromocyclododecane
solvent extraction and determined by
(HBCDD)
GC-MSD.
Reporting Limit
2 ppm
2 ppm
2 ppm
1 ppm
5 ppm
5 ppm
50 ppm
10 ppm
10 ppm
Remark: Reporting limit = Quantitation limit of analyte in sample
Page 4 of 9
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00253636
Test Conducted
(Ⅳ) Measurement Flowchart:
Test for Cd/Pb/Hg/Chromium (VI)/PBBS/PBDES Contents
Reference Standard: IEC 62321 edition 1.0:2008
Sample preparation
For non-metal part
For metal part
Take sample and immerse into Aqua Regia, start to strip plating layer
Stop the stripping procedure upon color change completely
Take the Aqua solution as plating component and stripped body as substrate component
Cd/Pb/Hg
Cr
Weigh sample and
add organic solvent
By spot test
Negative
Confirm the tested
samples are
totally dissolved
Make up with
deionized water
PBBs/PBDEs
Polymers /
electronics
Metal
For different
material, digest
the sample with
*1
appropriate acid
6+
Get 50cm2 sample
By boiling water
extraction
*2
Weigh sample
and add
alkaline
solution
By Soxhlet
extraction or
Solvent extraction
Definite temp.
extraction
Cool and filter
the extract
Analyzed by ICP-OES
Concentrate the
extract and make up
with organic
solvent
Analyzed by GC-MSD
Make up with deionized
water and add diphenylcarbazide solution
Analyzed by UV-VIS
Remarks:
*1: List of Appropriate Acid：
Acid Added for Digestion
Material
Polymers
HNO3,HCl,HF,H2O2,H3BO3
Metals
HNO3,HCl,HF
Electronics
HNO3,HCl,H2O2,HBF4
*2: If the result of spot test is positive, Chromium VI would be determined as detected.
Page 5 of 9
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00253636
Test Conducted
(Ⅳ) Measurement Flowchart:
Test for Halogen Content
Reference Standard：EN 14582
Sampling/grinding or
cutting
Add absorbent in a
combustion flask &
place weighed sample in
equipment
Fill oxygen into
calorimetric bomb
Ignite then leave the
bomb at room
temperature
Transfer the absorbent
into a volumetric flask
Make up with deionized
water
Analyzed by ion
chromatography
Page 6 of 9
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00253636
Test Conducted
(Ⅳ) Measurement Flowchart:
Test For Phthalates Contents
Reference Method: EN 14372: 2004
Sampling/grinding or
cutting
Weigh sample and add
organic solvent
By solvent extraction
Concentrate the extract
and make up with
organic solvent
Analyzed by GC-MSD
Page 7 of 9
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00253636
Test Conducted
(Ⅳ) Measurement Flowchart:
Test For Hexabromocyclododecane (HBCDD)
Reference Standard：USEPA 3540C
Sampling/grinding or cutting
Weigh sample and add organic
solvent
By soxhlet extraction
Concentrate the extract and
make up with organic solvent
Analyzed by GC-MSD
End of Report
Page 8 of 9
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00253636
Test Conducted
Photo
Page 9 of 9
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401