ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: Nano2 Fuse - SB Product #: 454xxx Series Issue Date: May 31, 2013 It is hereby certified by Littelfuse, Inc. that there is neither RoHS (EU Directive 2002/95/EC, 2011/65/EU)-restricted substance nor such use, for materials to be used for unit parts, for packing/packaging materials, and for additives and the like in the manufacturing processes. In addition, it is hereby reported to you that the parts and sub-materials, the materials to be used for unit parts, the packing/packaging materials, and the additives and the like in the manufacturing processes, are all composed of the following components. Issued by: <Global EHS Specialist> (1) Parts, sub-materials and unit parts This document covers the Nano2 Fuse - SB RoHS-Compliant series products manufactured by Littelfuse, Inc. < Raw Materials Used Please see Table 1 (2) The ICP data on all measurable substances Please see appropriate pages as identifed in Table 1 Remarks: Pb (lead) contained in the high temperature melting solder > 85% and is categorized as exempt under section 7a of the RoHS Annex. Form 585-047 Rev. A 1 2/21/06 Table 1: List of Raw Materials covered by this report Total Parts 1 2 3 5 6 7 8 9 Raw Material Part Number 910-238 Frequenta C221 (909-434) 082xxx-001 692323 64811x 648106-001 648112-001 425809 Raw Material Description Cap (Silver Plated Brass) Body (Ceramic Tube) Element – Cu99.9MSn Solder Yarn 6481xx (GLZZXXX) Yarn Yarn Ink 2 Page(s) 3-7 8-36 37-40 41-46 47-53 54-61 62-69 70-83 Test Report Applicant: Littelfuse, Inc. LIMA Technology Center, Lipa City, Malvar, Batangas Number : TWNC00300506 Date : Mar 07, 2013 Sample Description: One (1) group of submitted samples said to be : Part Description : Cap Part Number : 910-238 Date Sample Received : Feb 26, 2013 Date Test Started : Feb 26, 2013 Test Conducted : As requested by the applicant, for details please refer to attached pages. Authorized by: On Behalf of Intertek Testing Services Taiwan Limited K. Y. Liang Director *THJ0300506* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C. 全國公證檢驗股份有限公司 11492 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 1 of 5 Number : TWNC00300506 Test Conducted (Ⅰ) Test Result Summary: Result Test Item Unit Test Method RL (1) (2) ND ND 2 22 ND 2 ND ND 2 Negative Negative 0.02 Heavy Metal Cadmium (Cd) content ppm Lead (Pb) content ppm Mercury (Hg) content ppm Chromium VI (Cr6+) content Remarks: mg/kg with 50 cm2 With reference to IEC 62321: 2008, by microwave digestion and determined by ICP-OES. With reference to IEC 62321: 2008, by microwave digestion and determined by ICP-OES. With reference to IEC 62321: 2008, by microwave digestion and determined by ICP-OES. With reference to IEC 62321: 2008, by boiling water extraction and determined by UV-Vis Spectrophotometer. ppm = parts per million based on weight of tested sample = mg/kg ND = Not detected RL = Reporting Limit, Quantitation limit of analyte in sample mg/kg with 50cm2 = milligram per kilogram with 50 square centimeter Negative = A negative test result indicated positive observation was not found at the time of Test. Tested Components (1)Silvery metal cap (2)Silvery plating layer Responsibility of Chemist: Date Sample Received Test Period Kevin Liu/ Irene Chiou : Feb 26, 2013 : Feb 26, 2013 to Mar 04, 2013 (Ⅱ) Limit: RoHS Limit Limits Restricted Substances Cadmium (Cd) content 0.01% (100ppm) Lead (Pb) content 0.1% (1000ppm) Mercury (Hg) content 0.1% (1000ppm) Chromium VI (Cr6+) content 0.1% (1000ppm) The above limits were quoted from Annex II of 2011/65/EU for homogeneous material. *THJ0300506* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C. 全國公證檢驗股份有限公司 11492 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 2 of 5 Number : TWNC00300506 Test Conducted (Ⅲ) Measurement Flowchart: Test For Cd/Pb/Hg/Chromium (VI) Reference Standard:IEC 62321 edition 1.0:2008 Sample preparation Take sample and immerse into Aqua Regia, start to strip plating layer Stop the stripping procedure upon color change completely Take the Aqua solution as plating component and stripped body as substrate component Cd/Pb/Hg Substrate Plating For different material, digest the sample with *1 appropriate acid Cr 6+ By spot test Confirm the tested samples are totally dissolved Make up with deionized water Negative *2 Get 50cm2 sample By boiling water extraction Analyzed by ICP-OES Make up with deionized water and add diphenyl-carbazide solution Analyzed by UV-VIS *THJ0300506* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C. 全國公證檢驗股份有限公司 11492 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 3 of 5 Number : TWNC00300506 Test Conducted Remarks: *1: List Of Appropriate Acid: Material Polymers Metals Electronics Acid Added For Digestion HNO3,HCl,HF,H2O2,H3BO3 HNO3,HCl,HF HNO3,HCl,H2O2,HBF4 *2: If the result of spot test is positive, Chromium VI would be determined as detected. End of Report This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a recommendation for any particular course of action. Intertek does not accept a duty of care or any other responsibility to any person other than the Client in respect of this report and only accepts liability to the Client insofar as is expressly contained in the terms and conditions governing Intertek's provision of services to you. Intertek makes no warranties or representations either express or implied with respect to this report save as provided for in those terms and conditions. We have aimed to conduct the Review on a diligent and careful basis and we do not accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by statute or otherwise, except in the event of our gross negligence or wilful misconduct. *THJ0300506* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C. 全國公證檢驗股份有限公司 11492 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 4 of 5 Number : TWNC00300506 Test Conducted Photo *THJ0300506* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C. 全國公證檢驗股份有限公司 11492 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 5 of 5 Signature ForQueqlion Please withSGS m 3/13196 Date: 2013/01122Page:1 of 29 Test Report GIVBH CERAIVTEC 15.91207LAUF MULTIFUNKTIOKERAMIK,LUITPOLDSTRABE GESCHAFTSBEREICH Thefoltowingsamplo(s)was/weresu ittedand identifiodby/onbehalfof the clientas: SampleDescription No. Style/ltem Date SampleReceiving Period Testing '14 |l||filrlllllrlru NTAC221 201 2013t 4 'to 2013101/22 €fer to nextpage(s). Te6t Result(s) thetestresultsof Cadmium'Leacl' samples, ontheperfomedtestson submitted complywiththe limitsas setby PBDES and r. i""i*i"nt cnrotirln Cr(Vl),PBBS 2002/95/EC recasting Annexll; directive2011/65/EU Conclusion {Nw g!|d ru|' lb.sd sGsTIW ltD, c|r.|ilcC trbo.ltory - T.lFa ;m tu;dLs L{ mdemnr@mnmd F d'd on s!!3 ale'aion ro.seryor comafutuy un.urhorzed Ht"":ff;t." llxrrii,il,l,Ti"'lHl * ?,::*::Lll8ffi iillii.?L#j",ii#il{.ifi ;;:J:;;d-;;';:n'ir;; ""o' "*1e- i-tiF*.*:;$i1;',rdff *i$=i:*"q*"i;"+.;r=rt t1 t't*jtT*i$i'L{i, r;$Jirur*s,:::u$'"1'mr"in"m["lfxHi";'n*"r*;ffiIJ*ls$:llii; NoI Test Report CERAMTECGMBH GESCFIAFTSBEREICH MULTIFUNKTIO 20'13/13196Dale 2013101122 Page2 of 29 lm[t||fll|tlull KERAMIK,LUITPOLDSTMBE'15, 91207 LAUF Test Rerultls) PARTl,lAMENo.l CERAIVIC Result Uni lrethod MDL Cadmium(Cd) mg/r 2 Lead(Pb) mg/l 2 n.d. 1000 (Hg) Mercury mg/| 2 n.d. 1000 Chromium Cr(Vl) Hexavalent mgA Withreference to IEC62321:2008and perfomedby ICP-AES. Withreference to IEC62321:2008and performed by |CP4ES. to IEC62321:2008and Withreference perfomedby ICP-AES. Withreference to IEC62321:2008and perfomedby UV-VIS. to EN 14372.Analysis Withreference wasperformedby GC/MS. Withreference to EN 14372.Analysis wEsperfomedby GC/MS. Withreference to EN14372.Analysis wasperfomedby GC/MS. to EN14372.Analysis Withreferenc€ wasperfomedby GC/MS. to EN 14372.Analysis Witfrreference performed by GC/MS. was to EN14372.Analysis with referenc€ wasperfomedby GC/MS. With referenceto tJSEPA3550C: bY waspedormed 2007.Analysis LC/MS. No.l n.d. 2 n.d. 1000 Test ltem(s) o/. (CAS BBP(Bonzylbutylphthalate) No.r85$8-7) DEHP(Di-(2-ethylheryl) phthalate) (CASNo.r'117-81-7) "/" phthalate) (CAS Yo DIDP(Di-isodecyl No.:26761-40-0) phthalate) (CAS % DINP(Di-isononyl No.:28553-12-0) DNOP(Di-n-octylphthalate)(CAS No-:117-84-0) (CASNo.: OBP(Dibuglphthalate) 84-74-2) mg/ s PerfIuorooctanesulfonates (PFOS-Acid, MetalSalt,Amide) m9 PFOA(CAS No: 33547l) to USePA3ssoOr Wr1fr-i66rence bY wasPer{ormed Analysis 2007. 0.003 n.d. 0.003 n.d. 0.01 n.d. 0.01 n.o. 0.003 n.d. 0.003 n-d. 10 n.d. 10 n.d- 0.5 n.o. LC/MS. to USEPA3540C (PCBS) mg]]Kg Withreference Biphenyls Polychlorinated bY wasPerformed Analysis method. (cAS No.:133s3S3) GC/MS. lnFsoheNsen4ktkresu|'s3h 9ffjli'J;"X, ,;'!i* ,i ;" #,";, l;6';j';; lr" qhtddsl0*o3 Como.n! My unalhd zed anadbn ]itr.,; Limit '100 No. Test Report 3t/13196Date:2013/01122 Page|3of 29 CERAI,,ITEC GMBH GESCHAFTSBEREICH MULTIFUNKTI Test ltem(e) ] Unil Polychlorinated Terphenyls (PCTS) tl] tI|||[|l TAMIK.LUITPOLDSTMBE 15.9'1207 LAUF Mothod MDL mg/k Withreferenceto US EPA3t40C 0.5 method. Analysis waspedormed by GC/MS. Polychlodnated Naphthalene mg/K With refefenc€io US EPA3540C 5 (PCNs) method. Analysis wasperformed by GC/|MS. Alkanes,C10-13,chloro(Sho 100 mgi/r( Withreference to USEPA3540C ChainChlorinatedParaffins)(CAS method.Analysiswasperformedby GC/MS. No.:8553tr 1-8) PVC An€lysis wasperformed by FTIRand FLAMETest. Formaldehyde(CAS No.: 5040{) mg/x Withreference to ISO17226-1(2008). 3 Analysis waspertormed by HPLC/DAD. mgil Withreference 0.5 Monomethyl dibromodiphenyl to USEPA8270D method. Analysis wasperformed by methane(DBBT) GC/MS. 0.5 mg/r With referenceto US EPA8270D Monomethyl dichlorodiphenyl Analysis wEsperformed by method. methane(Ugilec121) GC/MS. 0.5 mg/l With referenceto US EPA8270D tetrachlorodiphenyl Monomethyl performed by (Ugilec141) method. Analysis was methane GC/MS. Halogen 50 (F) (CAS No.i mg/l Halogen-Fluodne Result No.1 n.d. Limit n.o. n.d. Negative n.d. n.d. n.d. n.o. n.d. 14762-94-8) (Cl)(CASNo.: Halogen4hlorine -15-'t\ 22537 (Br)(CAsNo.: Halogen-Bromine 100€7-32-2) m9l (l) (CAS No.: Halogen-lodine 14 244-8) mg/ s mg/l . With referenceto BS EN 14582:2007 wasperfomedby lc. J Analysis organic-tincompounds Tdbutyl TinOBT) mg/ rriphenylTin(TphT) mg/ owi ! 'hLs13$rep9d d rhe tftd anys!0taEEG.!. bred b remsamLq $u$ der lidl!n4don M.mnrfatoi 6 dmnl'on ont rid w gh63ndoblg,llonsun' ltl,/ithreferenceto DIN38407-13. bYGC/FPD wasperformed Analysis 'r + i, rl 50 n.d. 50 n.d. 50 n-o. 0.03 0.03 n.d. n.o. I ]r,--r ltlv;'":'nrr.";m'.:'i.":f.l:'-tr;;'":*vi.'j rtr*ss"i;;r::ffitrtrllijlslrm"r" '* b 1"."dmn a'rc, F Ee1dJ?oecvo' ;; i*YSiJ""i": Ii1"?'S";i'":;l ";;"i-*"d"I 'reor2q,, rle6lon:$" vw$!:r_ No: c Test Report CERAMTECGMBH IVULTIFUNKT GESCHAFTSBEREICH Test ltem(s) 13/13196 Date:2013/01122Page| 4of 29 ttff[t||l MDL Mothod Unil Asbestos (CASNo.:77536-66-4) Yo Aclinolite (CAS Amosite No.: 12172-73-5\ (CASNo.:77536S7- o/o Anthophyllite 5) (CASNo.:12001-29-5) % Chrysotile (CASNo.:12001-28-4) % Crocidolite o/o (CAS Tremolite No.:77536€8€) EO Withreference to EPA600/R-93/116 method. Analysis waspedormed by (SM),Dispersion StereoMicroscope PolaizedLightllicroscope Staining (DS-PLM)andX-rayDiffraotion (XRD). Spectometer (CAS No.: mg/f 1): 4-AMINODIPHENYL 92-87-1) With referenceto LFGB82.02-2. Analysiswas performedby GC/MS. (CASNo.:92-872):BENZIDINE @m^fGtoi R6€ult No.'l Negative Negative Negalive Negative Negative Negative with reference to LFGB82.02-2. Analysis wasperformed by GC/MS. to LFGB82.02-2. 3);4-CHLORO-O-ToLUIDINE mg/| with reference wa6performed by GC/MS. (CASNo.:95€9-2) Analysi6 reference to LFGB 82.02-2. (CAS mg4 With 4):2-NAPHTHYLAMINE performed Analysis u/as by Gc/Ms. No.:9159{) to LFGB82.02-2. (cAS mg/l Withrefefence 5):O-AMINOAZOTOLUENE by GC/MS. Analysis wasperformed No.:97-56-3) to LFGB82.02-2. mg/r with reference 6):2-AMINO-4-NITROTOLUENE wasperformed by GC/MSAnatysis (cAs No.r99-55-8) to LFGB 82.02-2. (CASNo.: mg/l l Withreference 7): P-CHLOROANILINE '106-47-8) Analysis wasperfomedby GC/MS. to LFGB82.02-2. (cAS m9ng with reference 8)r2,+DIAMINOANISOLE performed was by GC/MS. Analysis No.r615{5-4) to LFGB82.02-2. m9 g Withreference 9)i 4,4L by GC/lllS. wasperformed Analy6is DIAMINODIPHENYLMETHANE (CASNo.:101-77-9) '10):3,3-OICHLOROBENZIDINEmg/ s Withreference to LFGB82.02-2. perfomed by GC/MS. was Analysis (CASNo.:91-9+1) to LFGB82.02-2. mg/s with rcference 11): 3,3'-DIMETHOXYBENZIDINE performed bYGC/MS. was Analysis (CASNo.:119-904) to LFGB82.02-2. 12):3,3'-DIMETHYLBENZIDINEmg/ s Withreference performed bYGC/MS. was Analysis (CASNo.:119-93-7) comoaN,rl ,i, ! rh s d@ftnr 's islusd bv ft comqant sqd Iltt]ll RAMIK.LUITPOLDSTRABE 15,91207LAUF mg/l o E !e!' sndllnsnLoi 3sue5o€ qhGandobrsargnsu I i+e10r,et7e r{e6ion24tt vRjq'Iw 3 n.d. 3 n.d. 3 n.d. 3 n.d. 3 n.d. 3 n.d. 3 n.d. 3 n.d. 3 n.d- 3 n.d. 3 n.d. 3 n.d. Limit No Test RePort CERAMTECGMBH MULTIFUNKT GESCHAFTSBEREICH Testltem(s) 3i/13196Date: 2013i/01122 Page:5 ol29 lr][tttl Unil 13):3,3'-DIMETHYL-4,4'me/( DIAIIINODIPHENYLMETHANE (CASNo : 838€8{) '14):P-CRESIDINE (2-METHOXY-mg/k (CASNo.: s-METHYLANILINE) 120-71-8) (215):4,4'-METFIYLENE-B|Smg/N (CASNo.: CHLOROANILINE) 't01-144) (CAs mgiX 16)i4,4'-OXYDANILINE No.:101€04) (CAS mg/N 17) 4,4'-THiODtANtLtNE No. 13965-1) (CASNo.:95- mlyr 18):O-TOLUIDINE s3-4) 19):2,4-TOLUYLENEDIAMINE mg/r (CASNo.:95-80-7) 20):2,4,s-TRIMETHYLANILINEmgn (CASNo.:13717-7) (CASNo.:90- m(yr 21):O-ANISIDINE 04{) 22):P-AMINOMOBENZENE (CASNo.:60-09-3) (CASNo.:9523):2,4-XYLIDINE 68-1) 24):2.6-X/LlDlNE(CASNo.:8762-7) CFC's{Chlorofluoiocarbons) Method Result No.l n.d. Withreference to LFGB82.02-2. Analysiswasperformedby GC/lVlS. 3 .n . d . Withreference to LFGB82.02-2. Analysis wEsperformed by GC/MS. 3 n.d. Withreference to LFGB82.02-2. Analysis u€s performed by GC/lllS. 3 n.d. Wiih referenc€to LFGB82.02-2. Analysi6was performedby GC/MS. 3 n.o. 3 n.d. 3 n.o. 3 n.d. 3 n.d. 3 n.d. 3 n.d. 3 n.d. 1 n.d. I n.d. GroupI With referenceto US EPA502'1 bY wasperformed method. Analysis 1 (CASNo.: Chlo.ofluorocarbon-'1 75€94) mg,/ (CAsNo.: ehbrofluorocarbon-12 75-714) to l-JSEPA5021 mg/s Withreference rhetm. or 6 deiwntononvandd MDL Withreference to LFGB82.02-2. Analysis wasperformed by GC/MS. Withreference to LFGB82.02-2. Analysis waspedormed by GC/l\rS. Withreference to LFGB82.02-2. Analysis waspe.fomedby GC/MS. Withreference to LFGB82.02-2. Analysis wasperfomedby GC/MS. to LFGB82.02-2. Withreference by GC/l\rS. Analysis waspedormed to LFGB82.02-2. mg/r Withreferenc€ wasperfomedby GC/MS. Analysis to LFGB82.02-2. mg/l ) Withreference by GC/MS. Analysis wa6performed to LFGB 82.02-2. with reference mg/ s by GC/MS. wasperformed Analysi6 [rs. GCi o9nm5|e9rcpdrt I i l comoan{rrr ,'ebrd ro 6 c.!( bv bs c omp'nv rhs ddneni '' Blued ohts.nd obBaL4^3ur t!] IAIVIK.LUITPOLDSTMBE'15. 9'1207 LAUF bY wasPerformed Analysis method. GC/tVS. Limit l Test Report No CERAMTECGMBH MULTIFUNKT GESCHAFTSBEREICH Test ltern(s) t]|||tr] mg/N luorocarbon-1 15 (CASNo.: mgA Chlorof 76-15-3) Method With referenc€to US EPA5021 wasperformed by method. Analysis GC/MS. to Us EPA5021 Withreference by Analysis \rasperformed method. GC/MS. With referenceto US EPA5021 wasperformed by method. Analysis GC/[rS. MDL Re-Bult No.1 1 n.o, 1 n.d. I n.d. 1 n.d. 1 n.d. lll Group 3 (CASNo.: Chlorof luorocarbon-1 75-724l, lttlt|l] 15, 9'I207LAUF RAMIK,LUITPOLDSTRABE lJnil 113(CASNo.: mg/x Chlorofluorocadon7613r ) luorocadcon-'1 14(CASNo.: Chlorof 76-14:2) 13/13196 Date: 2013/01122 Page: 6 of 29 mgn With feferenceto US EPA5021 by Analysis wasperformed methodGC/t!ts. to USEPA5021 11(CASNo.: mgn Withreference Chlorofluorocarbon-1 bY wasperfoamed method. Analysis 354-5e3) GC/l\rs. (cAs No.: mg/l ) with refe.enceto us EPA5021 Chlorofluorocarbon-'l'12 bY Analysis wasperformed method. 76-12-0) GC/MS. 1 (CASNo.: mg/ s nrith referenc€to US EPA5021 Chlorofluorocarbon-21 bY wEsperformed method. Analysis 422-78-6) GC/MS. to USEPA5021 (CAS No.: mg/ s Withreference Chlorofluorocarbon-212 bY Analysis wasPertormed method. 3142-26-1) GC/tVS. 3 (CASNo.: mg/ s With referenceto US EPA5021 luorocarbon-21 Chlorof bY wasperformed method. Analysis 2354-06-5) n.d. n.d. 1 n.d- 1 n.d. cc/Ms. (CASNo. luorocarbon-214 Chlorof 29255-31-0) to USEPA5021 m9/ .s Wttr reference bY wasPerformed Analysis method. GC/MS. 1 n.d. 5 (CASNo: luoroca6on-21 Chlorcf 42s943-2) m9 to USEPA5021 Withreference bY wasPertormed Analysis method. GC/tVS. 1 n.d. un,s$oseRE ra'd ihares!fshori 'n'hEb'repPd rt suqelt ro is ert rh'[email protected] bv rhecomparry ,e rme ot[s 'nreiredoi onrYandm Comorn,hy unrllTnzed one€lon |,.e0:p3,rp''e610,r2e" Limit Test Report 013/13196 Date:2013101122Page:7 ot 29 No. CERAMTECGMBH GESCHAFTSBEREICH IVULTIFUN :l T€€t ltem(s) Unit Chlorofluoroca.bon-216 (CAS No.: 661-57-2] mg/K Chlorofluorocarbon-2'17 (CAS No.: 422-86-8) m(yK Method MDL With referenceto US EPA5021 method. Analysis wasper{ormed by GC/MS. Withreference to USEPA5021 method. Analysis wEsperformed by GC/MS. R€5ult No.1 n.d- n.d. HCFCs (Hydrochlorofluorocalbons) (CASNo.:7543-4) HCFC-21 mg/k With referenceto US EPA5021 method. Analysis wa6performed by GC/MS. HCFC-22 {CASNo.:7545€) mg/k With referenceto US EPA5021 method. Analysis wasperformed by GC/MS. (CASNo.:593-704) HCFC-31 mg/K With referenceto US EPA5021 methodAnalysis \ €s pedormed by GCiMS. (CASNo.:354-14-3) mg/K With referenceto US EPA5021 HCFC-121 method. Analysis wasperfomedby GC/r\4S. HCFCI22(CASNo.:354-21-2) mgik Withreference to USEPA5021 method. Analysis wasper{ormed by GC/MS, HCFC-123(CAS No.: 306-83-2) mg/K Withrefefence to uS EPA5021 method. Analysis wasperformed by GC/MS. HCFCI24(CASNo.:2837-89-0) mg/k With referenceto US EPA5021 wasperformed by method. Analysis GC/tds. (CASNo.:359-28{) mg/( Withreference to USEPA5021 HCFC-131 by method. Analysis wasperformed GC/[rS. (CAS to USEPA502'1 No.:1d49-08-7) mg/r Withreference HCFC-132b wa6performed by method. Analysi6 GC/MS. c o m a N . ,r l r , r l L il r r ( , l r i rhs doci,mnrs 'ssrsdbt he conoanysubi*r b iu censr ,b r me or tr! 'meiurton oni and { Co@d d iuidid on ss6tr al'€'don Anvunadhorized t tlt|ltrrrr ERAMIK,LUITPOLDSTMBE 15, 91207LAUF condftotu or S.TF 01 id h. (mo.n'. rtrdon' iinr h hn,rondoareft ord"r' t,o" sa edtJ don{ n.d. n.d. n.d. n.o. n.d. n.o. n.d. 1 n.d. 1 n.d. Limit TestReport CERAMTEC GMBH GESCHAFTSBEREICH MULTIFUNfiIO 913'196 Date:2013i01122Page 8c'29 ,lS,91207LAUF KERAMIK,LUITPOLDSTMBE t|| tIIl||rIlrtfll Test ltem(s) (CASNo.:75-88-7) HCFC-133a reference to USEPA5021 method.Analysiswas perfomed by GC/[,ilS. HCFC-I41b(CASNo.:1717-00€) Withreference to USEPA502'1 method. Analysis wasperformed by GC/[rtS. HCFC-142b(CAS No.: 75-68-3) With refefenceto US EPA 5021 method.Analysiswas performedby GC/r!ts. FC-221(CASNo.: 422-264) FC-222(CASNo.:422-49-1) With referenc€to US EPA5021 methodAnalysis waspedormed by GC/MS. Withreference to USEPA5021 method. Analysis M€spedormed by GC/trs. FC-223(CASNo.:422-52-6) (CASNo.i422-54-8) HCFC-224 (CASNo.:422-56-0) HCFC-225ca Withreference to USEPA5021 method. Analysis w€sperfomedby GC/|VS. reference to LJSEPA5021 method. Analysi6 wasperfomedby GC/MS. referenceto US EPA5021 method. Analysis waspedormed by GC/t\rs. (CASNo.:507-55-1) HCFC-22scb (CASNo.:431-87-8) HCFC-226 (CASNo.:421-94-3) HCFC-231 Withreference to IJSEPA502'1 method. Analysis wasperformed by GC/MS. With referenceto uS EPA5021 method. Analysis wasperformed by GC/MS. with refe€nceto us EPA5021 ethod.Analysiswas performedby HCFC-232(CAS No.:460-89-9) to us EPA5021 ith reference wasperformed by method. Analysis GC/tVS. I I i c o m o a n { i r !l } i r l : n i l i ft s duftnr B Bsded hy rhs company&bid b ls cenea ubied b rems 3.d con( l ns rorE doih LEnetun tom .^ercrno alrhern t l l ' ! : Do;uneft arwW r,floru1o1 te".o' irrm, it' F c o m m n ' ss e _"r.*rdbe?D'ooL(ed rF hn,artridoem.ns li e do! . i . , ; r r r t 1 . , 1l3 r TestReport No. CERAMTEC GMBH GESCFI,AFTSBEREICH IMULTIFUN Testltem(s) (CASNo.:7125€4{) HCFC-233 13/13196Date:2013l01n2 Page9 of29 t[| ||Illml RAMIK,LUITPOLDSTRABE 15,91207 LAUF Unit It ethod HCFC-244 mg/K Withreference to USEPA5021 method. Analysis wasperfomedby GC/tVlS. m9K Withreference to USEPA5021 method. Analysis wEsperformed by GC/MS. mg/K Withreference to USEPA5021 method. Analysis wasperfomedby GC/MS. mg/K With referenceto US EPA5021 method. Analysis wasperformed by GC/MS. mg/K With referenc€to US EPA502'1 method. Analysis wasperformed by GC/tVS. m(yK Withreference to USEPA5021 method. Anaiysis wasperformed by GC/MS. mg/K with reference to us EPA5021 (CASNo.r42141-0) HCFC-251 mg/( (CASNo.:819-00-1) HCFC-252 mg/N (CASNo.:425-94-5) HCFC-234 (CASNo.:460-92-4) HCFC-235 HCFC-241 {CASNo.:666-27-3) (CASNo.:460-63-9) HCFC-242 HCFC-243{CAS No.: 4606$5) MDL Result No.t n.o, Limit n.d. n.d. n.d. n.d. n.d. method. Analysis wasperformed by GC/tds. (CASNo.:,160-35-5) mlyf HCFC-253 (CASNo.:42G97-3) HCFC-261 m9r HCFC-262ICAS No.: 421-02-03) mg/r 1. c o m D a t u i . I, Jl i, l!-ir'rrL rh's docinsd 's $ued by rtu cmeafr subieo ro ts Gn-q Withreference to USEPA5021 method. Analysis waspedormed by GC/MS. With referenceto US EPA5021 by method. Analysis wa6performed GC/MS. With referenceto uS EPA502'1 method. Analysis wasperformed by GC/MS. With referenceto US EPA5021 by method. Analysis wasperformed GC/MS. With referenceto US EPA5021 by Analysis waspedormed method. GC/MS, r' 1 n.d. 1 n.d. 1 n.d. 1 n.d. 1 n.d. nl r l l lonsb'.borcflcfudmenbals i 6.;i ti,io&' dMs@am1 .druopm 4,,,-" rhe ime d b deiwdidn onryard * shs andobrisa9ns un. ; | n n ; o r c ' i o d m f u - n . e d m " i ' € - o . € F p o d ' " o " c p | d "dP# b441o a Test Report No. CERAMTECGMBH GESCHAFTSBEREICH IVULTIFUN Testltem(s) (CASNo.:430-55-7) HCFC-271 13/13196 Date:2013/01122Page 10 of 29 t|| ||t] .15.91207LAUF RAMIK.LUITPOLDSTMBE Unil Method MDL msyK With referenceto US EPA5021 method. Analysjs w€sperfomedby GC/MS. Result No.l n.d. Halona Halon-1211 {CASNo.:353-59-3) (CASNo.:7553-8) Halon-1301 (CASNo.:124-73-2) Halon-2402 CHCS(Chlorinatehvdrocarbon) (CAS 1,1,1,2-Te'trachloroethane No.:63G20$) mg/K (CASNo.: 1,1,1-Trichloroethane 71-55€) mg/K (CAS 1,1,2,2-Tetrachloroethane No.:79-34-5) m(y( (CAS No.: 1,1,2-Tichloroethane 7940-5) mg/N (CASNo.:7$ 1.1-Dichloroethane 34-3) mgr '1,1-Dichloroethene (CAS No.: 7$ 354) (CASNo.: 1,1-Dichloropropene 5635&6) (CASNo.: 1,2,3-Trichloropropane 96-184) (cASNo.: 1,2-Dichloroethane 107-06-2) mg/K GC/frs. n.o, mg/K Withreference to USEPA5021 method. Analysis wasperformed by GC/MS. With referenc€to US EPA5021 method. Analysis waspedormed by GC/tVS. Withreference to USEPA5021 Analysis wasperformed by method. GC/MS, n.d. With reference to US EPA 5021 method.Analysiswas perfomed by GC/MS. With referenceto US EPA5021 wasperformed by method. Analysis GC/MS. to USEPA5021 mlyr Withreference by Analysis wasperformed method. GC/MS. to USEPA5021 mg/l Withreference by Analysis wasperformed method. GC/tMS. mgn) With referenceto US EPA5021 bY waspedormed Analysis method. GC/MS. to Us EPA5021 mg/ s Withreference bY wasPerformed Analysis method. LrnesdheMs *bd riere5dnssfMrn h sle' dePdrcr rh , d@manr 6 6!ued by d'e companvebr& b s aele romar do.umirs ! and.for e &hft ComFnv hY dnalriotredaileraion n.d. n.d. With referenceto US EPA5021 mg/K method. Analysis wasperformed by GC/MS. n.d. 1 n.d. 1 n.d. 1 n.d. 1 n,o. 1 n.d. n.d. n.d. ||ttl!l] Limit TestReport No. 013/13196Date:2013101/22Page.11ol29 [ltl t tnm|l]l CERAI,TTEC G[,iBH GESCHAFTSBEREICH MULTIFU Test ltem(s) (CASNo-: 1,2-Dichloropropane 78€7-5) '1,$Dichloropropane (CASNo.: A2-24-9') ERAMIK.LUITPOLDSTRABE 15.91207LAUF Uni Method mga mg4 (CASNo.: 2,2-Dichloropropane 594-20-7) mg/l (CASNo.: Carbontetrachloride 56-23-s) m9r (CAS No.: 7M0-3) Chloroethane mg/r WithGference to IJSEPA5021 method. Analysi6 wasperfomedby GC/MS. With referenceto US EPA5021 method. Analysis wasperformed by GC/tlts. Withrefefence 1oUSEPA5021 method. Analysis wasperformed by GC/tVS. Withreference to IJSEPA502'1 method. Analysis wasperfomedby GC/MS. With referenceto Us EPA5021 method. Analysis M€sperformed by I'DL Result 1 No.l n.d. I n.d. 1 n.o. 1 n.d. 'I n.d. 1 n.d. 'I n.o. Limit GC/t\rs. (CASNo.:67€6-3) Chloroform m!yr Withreference to USEPA5021 method. Analysis wasperformed by GC/MS. (CASNo.r74-87- mg/r Withreference to USEPA5021 Chloromethane wasperfomedby method. Analysis 3) GC/MS, (cAs No.: mg/l J With referenceto US EPA5021 cis.l,2-Dichlofoethene Analysis wEsperfomedby method. 156-59-2) GC/MS. (CASNo.: mg/ I With referenceto US EPA5021 cis-1,3-Dichloropropene Analysis wasperfomedby method. 10061-01-5) GC/MS. mg/ s With referenc€to US EPA5021 (CASNo.: Hexachlorobutadiene bY wasperformed method. Analysis 87€8-3) n.d. n.d. n-d. GC/MS. to USEPA5021 mg/ g Withreference bY wasperformed Analysis method. GC/tutS. to USEPA5021 (CAS mg/ No.: 127letrachloroethene s Withreference bY wasperformed method. Analysis 184) GC/|V]S. MethyleneChlodde(CAS No.: 75 09-2) comanvnli I Ll lL I Ths dornmnr s 'esuedby rh companysubid b coent $. tme or {s 'nraten' on onlv and w shs andoDroarlds!f Anydna!ho';ed aiieraton ComDanv 1 n.d. 1 n.d. Ie"!]ri..,.i'lpl"l:,!":i:l:{:.ifi , .".d;.-+"* -i- "-d;; :6 m"o es.d ""F-.oa #E;;?:.:!tTi.?;:J"1i".+ ;l,i.i::";:ifl%".j i:?;i':; i:mr *i:a'*;il;'';*;i:u*,1't;';': :li "i";":% r$1""1 lil:r'"fjlrri#:: J.:J l;fJ*;;i:l;,:::,i. ";;;;"":::.r.'i.:lil*:',;3'#;;;"qj€'"': TestReport No.: 'f3/13196Date:2013/01 n2 c CERAIVTEC GMBH GESCHAFTSBEREICH I,TULTIFUN Testltem(s) Page:12ot29 ll| |l[I|l tttt||] RAMIK.LUITPOLDSTMBE 15.9'I207LAUF Unil tulethod MDL (CAS trans-1,2-Dichloroethene No.r156€0-5) mg/K Withreference to USEPA5021 \.'/as performed method. Analysis by (CAS trans-1,3-Dichloropropene No.:10061-02€) mg/K Trichloroethylene (CASNo.:79016) mg/K With referenceto US EPA5021 methodAnalysis wasperformed by GC/MS. With referenc€to US EPA5021 method. Analysis wasperformed by Result No.1 n.d. Limit GC/l\rs. n.d. n.d. GC/t\rs. Sumof PBEI5 Monobromobiphenyl Dibromobiphenyl mg/K mg/x 5 mgk n.d. n.d. n.d. n.d. n.d. n.d- Tribromobiphenyl Tetrabromobiphenyl Pentabromobiphenyl mgr( m!/x mgI( 5 Hexabromobiphenyl mg/t( mg/x mg/x 5 5 5 n.d. Heptabromobiphenyl Octabromobiphenyl Nonabromobiphenyl Dec€bromobiphenyl Sum of PBDE9 Monobromodiphenyl ether Dibromodiphenyl ether Tribromodiphenyl ether Tetrabromodiphenyl ether Pentabromodiphenyl ether Hexabromodiphenyl ether Heptabromodiphenyl ether Octabromodiphenyl other ether Nonabromodiphenyl ether Decabromodjphenyl 5 n.o. coft,nrtrlf fts dclmnr 5 5 mg/N mg/N mg/x Withreference to IEC62321:2008and performed by GC/MS. mg/r 5 5 5 mg/l mg/N mg/l mgn mg/| mgn mg/r osnlh9|ejrcpdrc' r l; l -ll \ 1 1,i sBsued bv 'he aomoanv subid d is Genq - 1 -md.ions or >eM- o,itu e{e. ;.dDrrdoB i;n, TheLomoa\< {" Pd td' m -/o n.d. n.d. n.dn.d. n.o, n.d. 5 5 n.d. 5 5 5 mg4 n.d. n.d. 5 mlyl 1000 n.d. n.d. n.d. n.d. n.d. 1000 Test Report E/2013i/'1 3'196 CERAMTEC GMBH GESCFI,AFTSBEREICH MULTIFUNKT Date: 2013101122Paoe: 13 of 29 |r][ttl][||ta|ll '15,9'1207 IK,LUITPOLDSTMBE LAUF Note : 'l- mgrkg= ppm; 0.1M%= 1o00ppm 2. n.d. = Not Detec{ed 3. MDL= MethodDetection Limit = 4. " " NotRegulated (NoUnit) analysis 5- *' = Qualitative = / Positive Detectable 6. Negative Undetectable qual 7. Testingrangeof asbestos analysis is fiom lessthan0.1%to '1000/6. Thejudgment critedon: asbestos fibe6 beingfound is shownas "Positive'; fibersnolbeingfoundis 6hownas "Negalive". PFOSReferenceInformation: POPS- ( 757t20.to parationsin concentrations products (1oppm), OutlawingPFOSas suo$ancesor above0.0010/6 in semi-finished or in textilesor othercoatedmaterials abovelpg/m'. articles or pads at a levelabove0.1 1000ppm), rhisdodme 6 sued bYthe compary subled ro b G lbled b r4ms md diunidon's<des :iI. l.t ,i!!t. t . i t. r- r" u " s " , e p ' ep.dedowddar -d"-;.,jdDho|'eod'o'Jor''0A'dss c6d,irisorse 6{ errennld o oroio 5r"r'eDo-r oi'rmqh d dih;;"r "-,s' {^e:91: q'ilj19-r-: I ,::;:'";,:3+:":",r:*":k*'tl.g;.':t*'",;t"t";;;".1ti;l"i:T,$I inituclrons I any rh. compants s e "1;is?r1""',119%ii b pon\b,it !,o ;;' l;::i;.t;.o;;:;; r:i''..*oo"-".-n'i.doa-f.e1D'F'"ot!d@e rc.r'd{r\do .-.doP\ ol TestReport 13/13't96Date| 2013101122Page: 14of 29 CERAMTEC GMBH 15.91207IAUF GESCHAFTSBEREICH IVULTIFUNKTIOKERAMIK.LUITPOLDSTMBE totallyby pre-conditioning methodaccording to belowflort/chart. Thesesamplesu/€re 1) I|| tII|[||lttlll ( Cre test method uded) Yang 2l Nameof the person mademeasurement: Climbgreat person charge of measurement Troy Chang Name the 3) of SampleMeasurement Addappropdate amount reagent of digestion Acid digestionby suitable depended on different sam (asbelowtable) material Heatto appropriate temperatureto etfact 1) AlkaliFusion 2) HCltodissolve Cool,filterdigestate through filter AdddiphenyFcarbazide for colordevelopment solder steel,copper,aluminum, measure theabsorbance at 540 nm by UV-VIS H,SO4,HrOr,HNO3,HCI Addedappropriatereagentto total digestion add alkalinedigestionreagentand heatto 90-95 C. ( 1)For nonfi licmaterial, (2) For metall material,add purewaterand heatto boiling. como.iY,rlf r,' I ; l bled b rem' !d rhe tm ot s meiwilononvaidw c! sh6 aid obrioatlonsd lY i illl'f."li i"Ii.i5,iiTl''il LTiAru".#i[ffi31**"":f*fl"".:5?1tl"t!"#f*s]trffii"J:!?1'wir##]i'xli.il" Bli':r**l*r*:.,*.":*lr*E::x#Jr$ffJiiir"tf'ff?i,i,ilfl,tffi*:x:"'s'"?*"":l1l1T *i$##:#f:is#iiHi#$"?Ji.}qfi"r**d$$$:T #f";*tft No: Test Report CERAI'TEC GlllBH GESCHAFTSBEREICH MULTIFUNKTIO PFOA/PFOS I r Nameoft Nameoft Page:15of 29 3/13196 Date:2013/01122 t|| |l[] RAMIK.LUITPOLDSTRABE 15,91207LAUF procedur€ flow chartof Ultrasonicextraction(LCymS) person whomademeasurementr Roman Wong person incharge of measurement TrcyChang ole extraction bv ljltrasonic extr€ction method:USEPA3550C) {Reference Concentrate/Dilute Extracted solution Analysiswas performedby LC/IIS ' , ' ] ' ! . . 1 ' r r " bled'o r.m6 ad co Memni(aionsidilnddon isue5 dei ;'ii;;:;; ;;;.i;N he !m or E ireiuironoivand 0 !rt shc rnd obriqargm h;ld7t 6 a d;""*d ;fr rhe tltttll Test Report 0f3/13196 Dale:2013t01t22Page 16ot29 CERAMTECGI/|BH GESCHAFTSBEREICH MULTIFUNKTIO ll| |l [ttttll RAMIK,LUITPOLDSTRABE 15. 91207LAUF PCTSanalylical flow chart ofthepersonwhomademeasurement: BarryTseng ofthepersonin chargeof measurement: TfoyChang Sampleprekealrnent Sampleextraction by organicsolveni Concenhate/Dilute theextracled solution AnalysiswEsperformedby GC/MS rr / , c o m a N . rr ! I rh s d@ftir : issEd byrhecompant>uqeqb s Geir d iu' sd'd o^ 5q6 shEmd drs*lm( (omoany arreBlon tuYunauhtrzed de q1rllff.:r'r(e tie! pemLsson pnorwdten oirhe eeot i iuI witrour eprcdu@d Jliif..s)repon€motbe gtr;""#.:ri.,i#?;:,liT; S i;:.1'Xgir' :l-.",":"'.::,3'i;f::1.? 1";;;";g;:1;." :?;.?g'";;il[';'j ::i,:: :jT: $ri"ei:;5:l- : k*r:t',."r.Trtrl'% ff ,"::;:#" ;; Test Report 01A1Y CERAI\4TEC GlilBH GESCHAFTSBEREICH MULTIFU I I Firsttestingprocess Optionalscreenp Confirmationproce6s Oate.2013l01l22 Page:17ol 29 :I||||I[] RAMIK,LUITPOLDSTRABE 15,91207LAUF PBB/PBDE analyticalFLOWCHART of thepersonwhomademeasurement: RomanWong person ofthe in chargeof measurement: TfoyChang -_r- fs"'pe---_-] s""tr"p,"G#t-------r-----Screenanalysis """"""'f """""" Sampleextraction/ Soxhletmethod Concentrate/Dilute Extractedsolution Analysisby GC/MS lssueReport ft6 docnmd sFEued byrhe(o@any ubjed oBG' -.*riiad*dsd fi";da.i;hhi,i d iunid on kussd6h ;'i;;' Dh{on, |i , 1PLomo4 3 se -1' ' do* rf rF hn*donooa LdnEadrnhoms^€dtnq alrher n ftmdor6d,nd r ', r, r f i N rl ttt]t TestReport 3/13196 Date: 2013/01122Page 18o129 CERAMTEC GMBH GESCHAFTSBEREICH IVULTIFUN r ttl [tt] RAMIK,LUITPOLDSTRABE 15,91207LAUF PCBSanalyticalflow chart I N r N e of the perconwhomademeasurement BarryTseng e ofthe personin chafgeof measurement: TroyChang Samplepretreatment Sampleextractionby organicso'vent Concentrate/Dilute the extrac{ed6olution AnalysiswEs pedormedby GC/MS : i.. +r -.1 T!'i!'!r!:! r"l-';:iif*, "1":;1"."; i""i'r3"i'.t;t." "":{i;3.""T'lli';* 3.1.v{f;il..i ,ii!'i, i.lla",i a"-.n j l'i i ;-.p l .nnoi be *o,m "d" ep r, ' s10 'o "t"r app'oilr or 0 P l Test Report CERAIVTECGMBH GESCHAFTSBEREICH [,ilULTIFU 013'/13196Date: 2013t01t22 page: i9 of 29 IK,LUITPOLDSTMBE 15,91207LAUF otinat€d PaEffins analyticalflow chart e ofthe personwhomademeasurement BarrvTseno e ofthe personInchargeof measurement: troy Cnaig Samplepretreatment Sampleedractionby organicsolvent Concentrate/Dilute theextracled solution Analysis wasperfomedby cCYI\rS :"|.tl::ii,t.{itl":ij,.ii:i li ;dhed hd 'domrion conrainadh rcspoisb]iyblobcislandlhsd llfl||[l [t ]rl TestReport 13/13'196 Date:2013/01t22 page| 20 of 29 CERAIVTEC GIVBH GESCHAFTSBEREICH IVULTIFUN RAMIK.LUITPOLDSTMBE 15, 91207LAUF tl||||l|||l tlow chartfor determination of Asb6tos e of the personwhomademeasurefientVictorKao e ofthe personin chargeof measuremer : WendvWd I I Refercn6e EPA500/R-S3/fi61 Transportalion andStoEge Prcparalion of pimaryanalyticat sample Examrnation by stereorn icrcscope(SM) Asb€stosidentification by disp€rsronstarning polaizedightmicrcscope (DS-PLM) problsnsarcencountefed Continuewhen with DS-PLM purposes ancl/or forqlatityassumnc€ Inted€rence matix removal Asbestos rdentfic€tion Asb€stos idenlification by xiay dilhaction spectrometer(XRD) Not coniaining AsbestovNegalive - . t condllioisofSedeonnldovedeaf. d iuiddof rssuesdd {adoB rirl - 'e(ompr,'Torgs. e Lomprl' € s€ a6ponsbity' ro s cFr' 3t I tl!Il]u TestReport 013/'13'196Date:2013101122Page:21 oI 29 CEMMTECGMBH GESCHAFTSBEREICH MULTIFUNKTIO tl]]||l[tx IK.LUITPOLDSTMBE 15.91207LAUF alyticalflow chadof Organic-Tin content I I Ne of thepersonwhomademeasurement: GinnyChen ofthepersonin chargeof measurement: TroyChang Samplepretreatment Sampleextractionby organlcsolvent Derived by Sodium tetraethylborate Concentrate/Dilute Extracted solution Analysis wasperformed by GC/FPD lose smp 4s) de! rh s le:rrcedi i _,i , r.ii Irijnr,l t l|ll Test Report 3/13196 Date:2013/01n2 Page 22 of 29 CERAMTEC GMBH GESCHAFTSBEREICH MULTIFUN IK,LUITPOLDSTMBE 15,91207LAUF PCNSanalyticalflow chart e of the personwhomademeasurement: BarryT6eng e of thepersonin chargeof measurement: TroyChang Samplepretreatrnent Sampleextraction by organicsolvent Concentrate/Dilute the extractedsolution Analysis was performed by GC,/ltlS 'l,. .r 'lfl' rh'snod,msdE3s6d rhecomp lr I e('&.i:! rTf,.sl! :1i|fi:rslT I anr rhe comoants :de 'esp( lllllllll][l|lt Test Report 013i/13196Date: 2013101122Page: 23 o129 CERAIVTECGMBH GESCHAFTSBEREICH MULTIFUNKTIO RAMIK,LUITPOLDSTRABE,l 5, 91207LAUF Itl|ifll|tltflrr]l Analyticalflow chartof phthalatecontent ofthe per6on whomademeasurement: RomanWong ofthe personin chargeof measurement: TroyChang Samplepreleatmenuseparation Sampleextraction by soxhletmethod ConcentratdDilute Extracted solution Analysis w€sperfomedby GCYIIIS ..i",,.;, *-- *" i.;,;;;Jl[". ;; ff,T?i?,*i ,,.""".,i,1;. .lle add ro,eledronLdomddbomnE. s """:; i o ' , r ; i e"d ; : . D o", . - r 5 a"*n;"1 s" atudoB { iinr lneComodl lmh^9don'ocmedb|i"oo'-""*."o'o".p.o""*. r L ,+e or.rsrD 're so oL_€ d_onFrd$_aco Test Report NO '13i/13196 Date: 2013/01122 Page: 24 of 29 ||]rIltl]fll|||||l CERAMTEC GMBH 15.91207LAUF IVlULTIFUNKTI o KERAMIK,LUITPOLDSTMBE GESCHAFTSBEREICH Formaldehyde analyticalf,owchart I I ScottKu am ofthe pe6onwhomademeasurementi Chang Na am of the personin chargeof mea6urementTroyCl T€6tMethod: US EPA8315A' lso 17226-1 ) Samplepretreatrnent Sampleextraction Extracted )edvedby DNPHConcentratey'Oilute solution by HPLC/DAD Analysis wasperformed Data r < sdbv rh'snodnmedu h€cmP he rme or ts LmeMdio ont and s r I rr 'i,.^.roBd sesrorn-oor'" tu '.-, r* ;;;i;; A "'0" i , n o f _t ,.o! or 'm p , 1 , . d d run* dd u5u9so€ ; d ' h ; . " ,dnruoon, ';' r E h€ hnbaonooom" I b 1q doo m"o - nralo' e.aiidbe'orolrs'r"o o r"r . BiF prc*aEdb h.r'r*,e.mr dhe a{ TestReport E2013/13'196Dale:2O13101n2Page:25ot 29 CERAI,ITEC G[,|BH GESCHAFTSBEREICH MULTIFUN Ana Lt l||ll[tttlll IK,LUITPOLDSTRABE 15,91207LAUF s flow chartfor determination of PVCin material ofthepersonwhomademeasu€ment: GinnyChen ofthepersonin chargeof mea6urement: T.oyChang Samplepre{reatnent Sempleanalyzedby FTIR Checkwave-number of C-Clbondrng ;t*llt".;'": l-ji 'T"':' .xre;i''1;; f"lj,ii tr x'":""""j,q:."""1i: "1.:r+::.*.:; k N4r'ts.rrlivdi i Test Report 13/13196Date:2013/01122 Page:26of 29 CERAMTEC GMBH GESCHAFTSBEREICH ['ULTIF r l[tt|[[tt]l SKERAIVIK.LUITPOLDSTMBE'15, 9,I207LAUF DBBTanalyticalflor,Y chart ofthepersonwhomademea6urement: RomanWong of thepersonin ch€rgeof measurement: TroyChang SamplepretreatmenUseparation Sampleextfaction by soxhletmethod ConcentratdDilute Extracted solution Analysiswas performedby GC/lllS *car n i.lii:.f:llrepodGddberemodtred ijq"lvreili*ryr"l")$'f ' k t me of [5 inleiledon onrv.nd s diuii'dod $ues e 0h s and ob selns ur ";$ fl;":"l";-."#?;1':'"* lr::"*.i;;'sr" :1"e1 ,,t*t**t;;." "':i:,:'.'ffi'""x r,"lli;".g :H: ;,i:Lllfli ;:L';1";'.1 iH.;:l;ff% igii'1,liirl;'";f;:l;..;";i#l:s-ry*""-Tiff#: f l"{:i :;::#j,r#S::,*l ;.1"'":r;E;. T:;:,jJJ r$,."+"T;"-lr,jf Test Report No. E/201313196 Oalet201AO1n2 Page: 27 ol 29 CERAMTEC GMBH GESCHAFTSBEREICH MULTIFUNKT : || t][]|l tl IK,LUITPOLDSTMBE 15,9,1207 LAUF alytical flow chart of halogen content 1) 2) ofthe personwhomademeasurement: RitaChen ofthe personin chargeof measuremedt TroyChang Samplepretreatment / Separation Weighting andputtingsamplein cell OrygenBombCombustion / Absorption Dilution to fixedvolume Analysis w€sperfomedby lC "rHi'::'f';!#."":.4:;i:":'-#1"""r'"-'it,:'."L-3!i.;"iil'ii ffi-",;li'*:,:ng;;* -r,i"lo;qi --1 .di,-."",,j"o,saa-"',-1. - u, - r- iii:i i;;,;:,;", i;;:i;.1;;;,;: *her.n$donoo.Jmedh ;;i;.i;;b,'v, F'doo "nratb' !r:i-1- b o"'a!dJ@d "rdor !r flFoi -{9::i:'lIls:^., 01or 4 ue aDorva o re TestReport 1Y13196 Date:2013/01122 Page 28of 29 CERAMTEC GMBH GESCHAFTSBEREICH MULTIFUNKTIO RAMIK,LUITPOLDSTMBE I5. 9'1207 LAUF Analytical chartofvolatileo.ganiccompounds(VOCS) Name rneperson whomademeasurement : ChunWu Name me peason in chargeof measurement : ShiniyhChen I Referencemethod: USEPA5021l I I Takesampleandputit into headspaceglas6wBre. Bakethe samplein the oven Analysiswasperformedby GC/MS 'rr : l meci by hoe. ot s s eumnt it druclons lr .ry. The comp.iy s sre respotribi ty s : taisadDn d@umens lihdftumlGonoi b eDd€ed ecpr n iu. |It|[ttt][l|| l Test Report No 313196 Date:20f3/01n2 Page:29ot 29 CERAMTEC GMBH GESCI-IAFTSBEREICH MULTIFUNKI tl| tI|| ||ttll! IK,LUITPOLDSTMBE 15,91207LAUF ' TheGstedsamplq/ partb markedby an arow if it'5shownon the photo.. l2oL313196 *' End of Report " e"t.b lh"ijTt'1'tj.:,f ,ri,: d iuid'd.n rssus &i hnsrDn tEm e/ebsLnoalrher n rra,n dd rhe companv\ ind, dgs ar bv hdde, hdder or docungd. tt.dvised h, o: rhis nE 00.,-6 i ; r n , n ec m o a n " . . o . - - r " o trmeemmri ri,oc.q,-moib" ep,m,"d" ep. rr Test Report Applicant: Number: LITTELFUSE,INC. 800 E. NORTHWEST HWY A.DIVIETRO/D.UNTIEDT Attn: Date: SHAH00361401 JAN 16, 2013 Sample Description: One (1) submitted sample said to be Grey Wire. Item Name : Wire Tin Plated Cu. Part No. : Element. ************************************************************************************************************************************************************ Tests Conducted: As requested by the applicant, for details refer to attached page(s). ************************************************************************************************************************************************************ To be continued Authorized by: For intertek testing services Ltd., Shanghai Jacob Lin General Manager Page 1 Of 4 Intertek Testing Services Ltd., Shanghai Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233 上海天祥質量技術服務有限公司 上海市宜山路 801 號金陵商務廣場 B 座 200233 Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740 www.intertek.com www.intertek.com.cn Test Report SHAH00361401 Number: Tests Conducted (Ⅰ) Test Result Summary: Result (ppm) (1) Testing Item Heavy Metal Cadmium (Cd) content Lead (Pb) content Mercury (Hg) content 6+ 2 Chromium VI (Cr ) content (mg/kg With 50cm ) ND ND ND Negative (< 0.02) Testing Item Result (ppm) (2) Heavy Metal Cadmium (Cd) content / Plating Lead (Pb) content / Plating Mercury (Hg) content / Plating 6+ 2 Chromium VI (Cr ) content (mg/kg With 50cm ) / Plating ND 60 ND Negative (< 0.02) Remarks: ppm = parts per million = mg/kg ND = not detected 2 @ = Due to the insufficient sample area, reduced total sample surface of 10 cm was used and the dilution factor was adjusted accordingly. 2 mg/kg with 50cm = milligram per kilogram with 50 square centimetre Tested components: (1)Substrate. (2)Plating. Responsibility of Chemist: Dent Fang / Ken He (Ⅱ) RoHS Requirement: Restricted substances Cadmium (Cd) Content Lead (Pb) Content Mercury (Hg) Content 6+ Chromium VI (Cr ) Content Polybrominated Biphenyls (PBBs) Polybrominated Diphenyl Ethers (PBDEs) Limits 0.01% (100ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) The above limits were quoted from RoHS Directive 2011/65/EU for homogeneous material. (Ⅲ) Test Method: Testing item Cadmium (Cd) content Lead (Pb) content Mercury (Hg) content 6+ Chromium VI (Cr ) content Testing method With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in clause 7, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in Annex B, by boiling water extraction and determined by UV-VIS Spectrophotometer. Reporting limit 2 ppm 2 ppm 2 ppm 0.02 2 mg/kg with 50cm Remark:Reporting limit = Quantitation limit of analyze in sample Date Sample Received:Jan.9, 2013 Testing Period:Jan.9, 2013 to Jan.14, 2013 ************************************************************************************************************************************************************ To be continued Page 2 Of 4 Intertek Testing Services Ltd., Shanghai Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233 上海天祥質量技術服務有限公司 上海市宜山路 801 號金陵商務廣場 B 座 200233 Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740 www.intertek.com www.intertek.com.cn Test Report Number: SHAH00361401 Tests Conducted (Ⅳ) MEASUREMENT FLOWCHART: Test for Cd/ Pb/ Hg/Cr (VI)/ PBBs/PBDEs contents Reference standard: IEC 62321 edition 1.0:2008 Sampling/grinding or cutting Cr Cd/Pb/Hg Metal Weigh sample and for different material, digest the sample with *1 appropriate acid No Get 50cm samples Yes Weigh sample and add organic solvent *2 Soxhlet extraction or Solvent extraction Cool and filter the extract Make up with deionized water and add Diphenylcarbazide solution Analyzed by ICP-OES PBBs/PBDEs Definite temp. Extraction 2 Boiling water extraction Make up with deionized water Polymers / electronics Weigh sample and add alkaline solution Spot test Negative Confirm the tested samples are totally dissolved 6+ Concentrate the extract and make up with organic solvent Analyzed by GC-MSD Analyzed by UV-VIS REMARKS: *1: LIST OF APPROPRIATE ACID: MATERIAL Polymers Metals Electronics ACID ADDED FOR DIGESTION HNO3,HCl,HF,H2O2,H3BO3 HNO3,HCL,HF HNO3,HCL,H2O2,HBF4 *2: IF THE RESULT OF SPOT TEST IS POSITIVE, CHROMIUM (VI) WOULD BE DETERMINED AS DETECTED. ************************************************************************************************************************************************************ To be continued Page 3 Of 4 Intertek Testing Services Ltd., Shanghai Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233 上海天祥質量技術服務有限公司 上海市宜山路 801 號金陵商務廣場 B 座 200233 Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740 www.intertek.com www.intertek.com.cn Test Report Number: SHAH00361401 Tests Conducted *********************************************************************************************************************************************************** End of report This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a recommendation for any particular course of action. Intertek does not accept a duty of care or any other responsibility to any person other than the Client in respect of this report and only accepts liability to the Client insofar as is expressly contained in the terms and conditions governing Intertek's provision of services to you. Intertek makes no warranties or representations either express or implied with respect to this report save as provided for in those terms and conditions. We have aimed to conduct the Review on a diligent and careful basis and we do not accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by statute or otherwise, except in the event of our gross negligence or wilful misconduct. Page 4 Of 4 Intertek Testing Services Ltd., Shanghai Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233 上海天祥質量技術服務有限公司 上海市宜山路 801 號金陵商務廣場 B 座 200233 Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740 www.intertek.com www.intertek.com.cn Test Report Applicant: Number : TWNC00285770 Littelfuse Philippines Inc. LIMA Technology Center, Lipa City, Malvar, Batangas Date : Nov 19, 2012 Sample Description: One (1) group of submitted samples said to be : Part Description : Solder (Pb is ≥ 90%) Part Number : 692323 Date Sample Received : Nov 12, 2012 Date Test Started : Nov 13, 2012 Test Conducted : As requested by the applicant, for details please refer to attached pages. Authorized By: On Behalf Of Intertek Testing Services Taiwan Limited K. Y. Liang Director *THJ0285770* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 1 of 6 Number : TWNC00285770 Test Conducted (Ⅰ) Test Result Summary : Result (ppm) Silvery Metal Test Item Heavy Metal Cadmium (Cd) content Lead (Pb) content Mercury (Hg) content Chromium VI (Cr6+) content (mg/kg with 50cm2) ND 910679 ND Negative (< 0.02) Remarks: ppm = Parts per million based on weight of tested sample = mg/kg ND = Not detected < = Less than mg/kg with 50cm2 = milligram per kilogram with 50 square centimetre Negative = A negative test result indicated positive observation was not found at the time of Test. Responsibility of Chemist : Irene Chiou / Kevin Liu Date Sample Received Test Period : Nov 12, 2012 : Nov 13, 2012 To Nov 15, 2012 (Ⅱ) RoHS Limits: Restricted Substances Cadmium (Cd) Content Lead (Pb) Content Mercury (Hg) Content Chromium VI (Cr6+) Content Limits 0.01% (100ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) The above limits were quoted from Annex II of 2011/65/EU for homogeneous material. *THJ0285770* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 2 of 6 Number : TWNC00285770 Test Conducted (Ⅲ) Test Method: Test Item Cadmium (Cd) content Lead (Pb) content Mercury (Hg) content Chromium VI (Cr6+) content Test Method With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in clause 7, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in annex B, by boiling water extraction and determined by UV-Vis Spectrophotometer. Reporting Limit 2 ppm 2 ppm 2 ppm 0.02 mg/kg with 50cm2 Remark: Reporting limit = Quantitation limit of analyte in sample *THJ0285770* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 3 of 6 Number : TWNC00285770 Test Conducted (Ⅳ) Measurement Flowchart: Test For Cd/Pb/Hg/Chromium (VI) Reference Standard:IEC 62321 edition 1.0:2008 Sampling/grinding or cutting Cd/Pb/Hg Cr 6+ Polymers / Electronics Metal For different material, digest the sample with *1 appropriate acid By spot test Negative Confirm the tested samples are totally dissolved Make up with deionized water *2 Weigh sample and add alkaline solution Get 50cm2 sample Definite temp. extraction Boiling water extraction Cool and filter the extract Analyzed by ICP-OES Make up with deionized water and add diphenylcarbazide solution Analyzed by UV-VIS *THJ0285770* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 4 of 6 Number : TWNC00285770 Test Conducted (Ⅳ) Measurement Flowchart: Remarks: *1: List of Appropriate Acid: Acid Added for Digestion Material Polymers HNO3,HCl,HF,H2O2,H3BO3 Metals HNO3,HCl,HF Electronics HNO3,HCl,H2O2,HBF4 *2: If the result of spot test is positive, Chromium VI would be determined as detected. End of Report This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a recommendation for any particular course of action. Intertek does not accept a duty of care or any other responsibility to any person other than the Client in respect of this report and only accepts liability to the Client insofar as is expressly contained in the terms and conditions governing Intertek's provision of services to you. Intertek makes no warranties or representations either express or implied with respect to this report save as provided for in those terms and conditions. We have aimed to conduct the Review on a diligent and careful basis and we do not accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by statute or otherwise, except in the event of our gross negligence or wilful misconduct. *THJ0285770* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 5 of 6 Number : TWNC00285770 Test Conducted Photo *THJ0285770* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 6 of 6 Test Report Applicant: Number : TWNC00286464 Littelfuse Philippines Inc. LIMA Technology Center, Lipa City, Malvar, Batangas Date : Nov 22, 2012 Sample Description: One (1) group of submitted samples said to be : Part Description : Yarn Part Number : 648118_648119_648120 (6481xxx_GLZZxxx) Date Sample Received : Nov 15, 2012 Date Test Started : Nov 16, 2012 Test Conducted : As requested by the applicant, for details please refer to attached pages. Authorized By: On Behalf Of Intertek Testing Services Taiwan Limited K. Y. Liang Director *THJ0286464* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 1 of 7 Number : TWNC00286464 Test Conducted (Ⅰ) Test Result Summary : Result (ppm) White Yarn Test Item Heavy Metal Cadmium (Cd) content Lead (Pb) content Mercury (Hg) content Chromium VI (Cr6+) content Polybrominated Biphenyls (PBBs) Monobrominated Biphenyls (MonoBB) Dibrominated Biphenyls (DiBB) Tribrominated Biphenyls (TriBB) Tetrabrominated Biphenyls (TetraBB) Pentabrominated Biphenyls (PentaBB) Hexabrominated Biphenyls (HexaBB) Heptabrominated Biphenyls (HeptaBB) Octabrominated Biphenyls (OctaBB) Nonabrominated Biphenyls (NonaBB) Decabrominated Biphenyl (DecaBB) Polybrominated Diphenyl Ethers (PBDEs) Monobrominated Diphenyl Ethers (MonoBDE) Dibrominated Diphenyl Ethers (DiBDE) Tribrominated Diphenyl Ethers (TriBDE) Tetrabrominated Diphenyl Ethers (TetraBDE) Pentabrominated Diphenyl Ethers (PentaBDE) Hexabrominated Diphenyl Ethers (HexaBDE) Heptabrominated Diphenyl Ethers (HeptaBDE) Octabrominated Diphenyl Ethers (OctaBDE) Nonabrominated Diphenyl Ethers (NonaBDE) Decabrominated Diphenyl Ether (DecaBDE) Halogen Content Fluorine (F) Chlorine (Cl) Bromine (Br) Iodine (I) ND 14 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND Remarks: ppm = Parts per million based on weight of tested sample = mg/kg ND = Not detected Responsibility of Chemist : Irene Chiou / Kevin Liu / Cathy Chen Date Sample Received Test Period : Nov 15, 2012 : Nov 16, 2012 To Nov 21, 2012 *THJ0286464* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 2 of 7 Number : TWNC00286464 Test Conducted (Ⅱ) RoHS Limits: Restricted Substances Cadmium (Cd) Content Lead (Pb) Content Mercury (Hg) Content Chromium VI (Cr6+) Content Polybrominated Biphenyls (PBBs) Polybrominated Diphenyl Ehters (PBDEs) Limits 0.01% (100ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) The above limits were quoted from Annex II of 2011/65/EU for homogeneous material. (Ⅲ) Test Method: Test Item Cadmium (Cd) content Lead (Pb) content Mercury (Hg) content Chromium VI (Cr6+) content Test Method With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in clause 7, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in annex C, by alkaline digestion and determined by UV-Vis spectrophotometer. Reporting Limit *THJ0286464* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 2 ppm 2 ppm 2 ppm 1 ppm Page 3 of 7 Number : TWNC00286464 Test Conducted (Ⅲ) Test Method: Test Item Polybrominated Biphenyls (PBBs) Polybrominated Diphenyl Ethers (PBDEs) Halogen Content Test Method With reference to IEC 62321 edition 1.0:2008 in annex A, by solvent extraction and determined by GC-MS and further HPLC-DAD confirmation when necessary. With reference to IEC 62321 edition 1.0:2008 in annex A, by solvent extraction and determined by GC-MS and further HPLC-DAD confirmation when necessary. With reference to EN 14582:2007 by calorimetric bomb with oxygen and determined by Ion Chromatograph. Reporting Limit 5 ppm 5 ppm 50 ppm Remark: Reporting limit = Quantitation limit of analyte in sample *THJ0286464* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 4 of 7 Number : TWNC00286464 Test Conducted (Ⅳ) Measurement Flowchart: Test for Cd/Pb/Hg/Chromium (VI)/PBBS/PBDES Contents Reference Standard: IEC 62321 edition 1.0:2008 Sample preparation For non-metal part For metal part Take sample and immerse into Aqua Regia, start to strip plating layer Stop the stripping procedure upon color change completely Take the Aqua solution as plating component and stripped body as substrate component PBBs/PBDEs Weigh sample and add organic solvent By Soxhlet extraction or Solvent extraction Concentrate the extract and make up with organic solvent Cr 6+ Substrate Cd/Pb/Hg Weigh sample and add alkaline solution For different material, digest the sample with *1 appropriate acid Plating Cr 6+ By spot test Definite temp. extraction Cool and filter the extract Confirm the tested samples are totally dissolved Negative *2 Get 50cm2 sample Make up with deionized water By boiling water extraction Analyzed by ICP-OES Analyzed by GC-MSD Make up with deionized water and add diphenyl-carbazide solution Remarks: *1: List of Appropriate Acid: Material Polymers Metals Electronics Analyzed by UV-VIS Acid Added for Digestion HNO3,HCl,HF,H2O2,H3BO3 HNO3,HCl,HF HNO3,HCl,H2O2,HBF4 *2: If the result of spot test is positive, Chromium VI would be determined as detected. *THJ0286464* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 5 of 7 Number : TWNC00286464 Test Conducted (Ⅳ) Measurement Flowchart: Test for Halogen Content Reference Standard:EN 14582 Sampling/grinding or cutting Add absorbent in a combustion flask & place weighed sample in equipment Fill oxygen into calorimetric bomb Ignite then leave the bomb at room temperature Transfer the absorbent into a volumetric flask Make up with deionized water Analyzed by ion chromatography End of Report This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a recommendation for any particular course of action. Intertek does not accept a duty of care or any other responsibility to any person other than the Client in respect of this report and only accepts liability to the Client insofar as is expressly contained in the terms and conditions governing Intertek's provision of services to you. Intertek makes no warranties or representations either express or implied with respect to this report save as provided for in those terms and conditions. We have aimed to conduct the Review on a diligent and careful basis and we do not accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by statute or otherwise, except in the event of our gross negligence or wilful misconduct. *THJ0286464* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 6 of 7 Number : TWNC00286464 Test Conducted Photo *THJ0286464* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 7 of 7 Test Report Applicant: Number : TWNC00285760 Littelfuse Philippines Inc. LIMA Technology Center, Lipa City, Malvar, Batangas Date : Nov 19, 2012 Sample Description: One (1) group of submitted samples said to be : Part Description : Yarn Part Number : 648106-001 Date Sample Received : Nov 12, 2012 Date Test Started : Nov 13, 2012 Test Conducted : As requested by the applicant, for details please refer to attached pages. Authorized By: On Behalf Of Intertek Testing Services Taiwan Limited K. Y. Liang Director *THJ0285760* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 1 of 8 Number : TWNC00285760 Test Conducted (Ⅰ) Test Result Summary : Result (ppm) White Yarn Test Item Heavy Metal Cadmium (Cd) content Lead (Pb) content Mercury (Hg) content Chromium VI (Cr6+) content Polybrominated Biphenyls (PBBs) Monobrominated Biphenyls (MonoBB) Dibrominated Biphenyls (DiBB) Tribrominated Biphenyls (TriBB) Tetrabrominated Biphenyls (TetraBB) Pentabrominated Biphenyls (PentaBB) Hexabrominated Biphenyls (HexaBB) Heptabrominated Biphenyls (HeptaBB) Octabrominated Biphenyls (OctaBB) Nonabrominated Biphenyls (NonaBB) Decabrominated Biphenyl (DecaBB) Polybrominated Diphenyl Ethers (PBDEs) Monobrominated Diphenyl Ethers (MonoBDE) Dibrominated Diphenyl Ethers (DiBDE) Tribrominated Diphenyl Ethers (TriBDE) Tetrabrominated Diphenyl Ethers (TetraBDE) Pentabrominated Diphenyl Ethers (PentaBDE) Hexabrominated Diphenyl Ethers (HexaBDE) Heptabrominated Diphenyl Ethers (HeptaBDE) Octabrominated Diphenyl Ethers (OctaBDE) Nonabrominated Diphenyl Ethers (NonaBDE) Decabrominated Diphenyl Ether (DecaBDE) ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND *THJ0285760* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 2 of 8 Number : TWNC00285760 Test Conducted (Ⅰ) Test Result Summary : Result (ppm) White Yarn Test Item Halogen Content Fluorine (F) Chlorine (Cl) Bromine (Br) Iodine (I) ND ND ND ND Remarks: ppm = Parts per million based on weight of tested sample = mg/kg ND = Not detected Responsibility of Chemist : Irene Chiou / Kevin Liu / Cathy Chen Date Sample Received Test Period : Nov 12, 2012 : Nov 13, 2012 To Nov 15, 2012 (Ⅱ) RoHS Limits: Restricted Substances Cadmium (Cd) Content Lead (Pb) Content Mercury (Hg) Content Chromium VI (Cr6+) Content Polybrominated Biphenyls (PBBs) Polybrominated Diphenyl Ehters (PBDEs) Limits 0.01% (100ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) The above limits were quoted from Annex II of 2011/65/EU for homogeneous material. *THJ0285760* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 3 of 8 Number : TWNC00285760 Test Conducted (Ⅲ) Test Method: Test Item Cadmium (Cd) content Lead (Pb) content Mercury (Hg) content Chromium VI (Cr6+) content Polybrominated Biphenyls (PBBs) Polybrominated Diphenyl Ethers (PBDEs) Halogen Content Test Method With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in clause 7, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in annex C, by alkaline digestion and determined by UV-Vis spectrophotometer. With reference to IEC 62321 edition 1.0:2008 in annex A, by solvent extraction and determined by GC-MS and further HPLC-DAD confirmation when necessary. With reference to IEC 62321 edition 1.0:2008 in annex A, by solvent extraction and determined by GC-MS and further HPLC-DAD confirmation when necessary. With reference to EN 14582:2007 by calorimetric bomb with oxygen and determined by Ion Chromatograph. Reporting Limit 2 ppm 2 ppm 2 ppm 1 ppm 5 ppm 5 ppm 50 ppm Remark: Reporting limit = Quantitation limit of analyte in sample *THJ0285760* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 4 of 8 Number : TWNC00285760 Test Conducted (Ⅳ) Measurement Flowchart: Test for Cd/Pb/Hg/Chromium (VI)/PBBS/PBDES Contents Reference Standard: IEC 62321 edition 1.0:2008 Sample preparation For non-metal part For metal part Take sample and immerse into Aqua Regia, start to strip plating layer Stop the stripping procedure upon color change completely Take the Aqua solution as plating component and stripped body as substrate component PBBs/PBDEs Weigh sample and add organic solvent By Soxhlet extraction or Solvent extraction Concentrate the extract and make up with organic solvent Analyzed by GC-MSD Cr 6+ Substrate Cd/Pb/Hg Weigh sample and add alkaline solution For different material, digest the sample with *1 appropriate acid Plating Cr 6+ By spot test Definite temp. extraction Cool and filter the extract Confirm the tested samples are totally dissolved Negative *2 Get 50cm2 sample Make up with deionized water By boiling water extraction Analyzed by ICP-OES Make up with deionized water and add diphenyl-carbazide solution Analyzed by UV-VIS *THJ0285760* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 5 of 8 Number : TWNC00285760 Test Conducted (Ⅳ) Measurement Flowchart: Remarks: *1: List of Appropriate Acid: Material Polymers Metals Electronics Acid Added for Digestion HNO3,HCl,HF,H2O2,H3BO3 HNO3,HCl,HF HNO3,HCl,H2O2,HBF4 *2: If the result of spot test is positive, Chromium VI would be determined as detected. *THJ0285760* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 6 of 8 Number : TWNC00285760 Test Conducted (Ⅳ) Measurement Flowchart: Test for Halogen Content Reference Standard:EN 14582 Sampling/grinding or cutting Add absorbent in a combustion flask & place weighed sample in equipment Fill oxygen into calorimetric bomb Ignite then leave the bomb at room temperature Transfer the absorbent into a volumetric flask Make up with deionized water Analyzed by ion chromatography End of Report This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a recommendation for any particular course of action. Intertek does not accept a duty of care or any other responsibility to any person other than the Client in respect of this report and only accepts liability to the Client insofar as is expressly contained in the terms and conditions governing Intertek's provision of services to you. Intertek makes no warranties or representations either express or implied with respect to this report save as provided for in those terms and conditions. We have aimed to conduct the Review on a diligent and careful basis and we do not accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by statute or otherwise, except in the event of our gross negligence or wilful misconduct. *THJ0285760* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 7 of 8 Number : TWNC00285760 Test Conducted Photo *THJ0285760* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 8 of 8 Test Report Applicant: Number : TWNC00285761 Littelfuse Philippines Inc. LIMA Technology Center, Lipa City, Malvar, Batangas Date : Nov 19, 2012 Sample Description: One (1) group of submitted samples said to be : Part Description : Yarn Part Number : 648112-001 Date Sample Received : Nov 12, 2012 Date Test Started : Nov 13, 2012 Test Conducted : As requested by the applicant, for details please refer to attached pages. Authorized By: On Behalf Of Intertek Testing Services Taiwan Limited K. Y. Liang Director *THJ0285761* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 1 of 8 Number : TWNC00285761 Test Conducted (Ⅰ) Test Result Summary : Result (ppm) Submitted Samples Test Item Heavy Metal Cadmium (Cd) content Lead (Pb) content Mercury (Hg) content Chromium VI (Cr6+) content Polybrominated Biphenyls (PBBs) Monobrominated Biphenyls (MonoBB) Dibrominated Biphenyls (DiBB) Tribrominated Biphenyls (TriBB) Tetrabrominated Biphenyls (TetraBB) Pentabrominated Biphenyls (PentaBB) Hexabrominated Biphenyls (HexaBB) Heptabrominated Biphenyls (HeptaBB) Octabrominated Biphenyls (OctaBB) Nonabrominated Biphenyls (NonaBB) Decabrominated Biphenyl (DecaBB) Polybrominated Diphenyl Ethers (PBDEs) Monobrominated Diphenyl Ethers (MonoBDE) Dibrominated Diphenyl Ethers (DiBDE) Tribrominated Diphenyl Ethers (TriBDE) Tetrabrominated Diphenyl Ethers (TetraBDE) Pentabrominated Diphenyl Ethers (PentaBDE) Hexabrominated Diphenyl Ethers (HexaBDE) Heptabrominated Diphenyl Ethers (HeptaBDE) Octabrominated Diphenyl Ethers (OctaBDE) Nonabrominated Diphenyl Ethers (NonaBDE) Decabrominated Diphenyl Ether (DecaBDE) ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND *THJ0285761* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 2 of 8 Number : TWNC00285761 Test Conducted (Ⅰ) Test Result Summary : Result (ppm) Submitted Samples Test Item Halogen Content Fluorine (F) Chlorine (Cl) Bromine (Br) Iodine (I) ND ND ND ND Remarks: ppm = Parts per million based on weight of tested sample = mg/kg ND = Not detected Responsibility of Chemist : Irene Chiou / Kevin Liu / Cathy Chen Date Sample Received Test Period : Nov 12, 2012 : Nov 13, 2012 To Nov 15, 2012 (Ⅱ) RoHS Limits: Restricted Substances Cadmium (Cd) Content Lead (Pb) Content Mercury (Hg) Content Chromium VI (Cr6+) Content Polybrominated Biphenyls (PBBs) Polybrominated Diphenyl Ehters (PBDEs) Limits 0.01% (100ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) The above limits were quoted from Annex II of 2011/65/EU for homogeneous material. *THJ0285761* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 3 of 8 Number : TWNC00285761 Test Conducted (Ⅲ) Test Method: Test Item Cadmium (Cd) content Lead (Pb) content Mercury (Hg) content Chromium VI (Cr6+) content Polybrominated Biphenyls (PBBs) Polybrominated Diphenyl Ethers (PBDEs) Halogen Content Test Method With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in clause 7, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in annex C, by alkaline digestion and determined by UV-Vis spectrophotometer. With reference to IEC 62321 edition 1.0:2008 in annex A, by solvent extraction and determined by GC-MS and further HPLC-DAD confirmation when necessary. With reference to IEC 62321 edition 1.0:2008 in annex A, by solvent extraction and determined by GC-MS and further HPLC-DAD confirmation when necessary. With reference to EN 14582:2007 by calorimetric bomb with oxygen and determined by Ion Chromatograph. Reporting Limit 2 ppm 2 ppm 2 ppm 1 ppm 5 ppm 5 ppm 50 ppm Remark: Reporting limit = Quantitation limit of analyte in sample *THJ0285761* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 4 of 8 Number : TWNC00285761 Test Conducted (Ⅳ) Measurement Flowchart: Test for Cd/Pb/Hg/Chromium (VI)/PBBS/PBDES Contents Reference Standard: IEC 62321 edition 1.0:2008 Sample preparation For non-metal part For metal part Take sample and immerse into Aqua Regia, start to strip plating layer Stop the stripping procedure upon color change completely Take the Aqua solution as plating component and stripped body as substrate component PBBs/PBDEs Weigh sample and add organic solvent By Soxhlet extraction or Solvent extraction Concentrate the extract and make up with organic solvent Analyzed by GC-MSD Cr 6+ Substrate Cd/Pb/Hg Weigh sample and add alkaline solution For different material, digest the sample with *1 appropriate acid Plating Cr 6+ By spot test Definite temp. extraction Cool and filter the extract Confirm the tested samples are totally dissolved Negative *2 Get 50cm2 sample Make up with deionized water By boiling water extraction Analyzed by ICP-OES Make up with deionized water and add diphenyl-carbazide solution Analyzed by UV-VIS *THJ0285761* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 5 of 8 Number : TWNC00285761 Test Conducted (Ⅳ) Measurement Flowchart: Remarks: *1: List of Appropriate Acid: Material Polymers Metals Electronics Acid Added for Digestion HNO3,HCl,HF,H2O2,H3BO3 HNO3,HCl,HF HNO3,HCl,H2O2,HBF4 *2: If the result of spot test is positive, Chromium VI would be determined as detected. *THJ0285761* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 6 of 8 Number : TWNC00285761 Test Conducted (Ⅳ) Measurement Flowchart: Test for Halogen Content Reference Standard:EN 14582 Sampling/grinding or cutting Add absorbent in a combustion flask & place weighed sample in equipment Fill oxygen into calorimetric bomb Ignite then leave the bomb at room temperature Transfer the absorbent into a volumetric flask Make up with deionized water Analyzed by ion chromatography End of Report This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a recommendation for any particular course of action. Intertek does not accept a duty of care or any other responsibility to any person other than the Client in respect of this report and only accepts liability to the Client insofar as is expressly contained in the terms and conditions governing Intertek's provision of services to you. Intertek makes no warranties or representations either express or implied with respect to this report save as provided for in those terms and conditions. We have aimed to conduct the Review on a diligent and careful basis and we do not accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by statute or otherwise, except in the event of our gross negligence or wilful misconduct. *THJ0285761* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 7 of 8 Number : TWNC00285761 Test Conducted Photo *THJ0285761* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 8 of 8 Test Report Applicant: Littelfuse Philippines Inc. LIMA Technology Center, Lipa City, Malvar, Batangas Number : TWNC00306991 Date : Apr 16, 2013 Sample Description: One (1) group of submitted samples said to be : Part Description : Black Ink Part Number : 425809 Date Sample Received : Apr 10, 2013 Date Test Started : Apr 11, 2013 Test Conducted : As requested by the applicant, for details please refer to attached pages. Authorized by: On Behalf of Intertek Testing Services Taiwan Limited K. Y. Liang Director *THJ0306991* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C. 全國公證檢驗股份有限公司 11492 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 1 of 10 Number : TWNC00306991 Test Conducted (Ⅰ) Test Result Summary: Result Test Item Unit Test Method Black paste RL Heavy Metal ND 2 ND 2 ND 2 ND 1 ppm ND 5 ppm ND 5 ppm ND 5 ND 5 ND 5 ND 5 ND 5 ppm ND 5 ppm ND 5 ppm ND 5 Cadmium (Cd) Content ppm Lead (Pb) Content ppm Mercury (Hg) Content ppm Chromium VI (Cr6+) Content ppm Polybrominated Biphenyls (PBBs) Monobrominated Biphenyls (MonoBB) Dibrominated Biphenyls (DiBB) Tribrominated Biphenyls (TriBB) Tetrabrominated Biphenyls (TetraBB) Pentabrominated Biphenyls (PentaBB) Hexabrominated Biphenyls (HexaBB) Heptabrominated Biphenyls (HeptaBB) Octabrominated Biphenyls (OctaBB) Nonabrominated Biphenyls (NonaBB) Decabrominated Biphenyl (DecaBB) With reference to IEC 62321: 2008, by microwave digestion and determined by ICP-OES. With reference to IEC 62321: 2008, by microwave digestion and determined by ICP-OES. With reference to IEC 62321: 2008, by microwave digestion and determined by ICP-OES. With reference to IEC 62321: 2008, by alkaline digestion and determined by UV-Vis Spectrophotometer. ppm ppm ppm ppm With reference to IEC 62321: 2008, by solvent extraction and determined by GC-MS and further HPLC-DAD confirmation when necessary. *THJ0306991* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C. 全國公證檢驗股份有限公司 11492 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 2 of 10 Number : TWNC00306991 Test Conducted Result Test Item Unit Polybrominated Diphenyl Ethers (PBDEs) Monobrominated Diphenyl Ethers ppm (MonoBDE) Dibrominated Diphenyl Ethers ppm (DiBDE) Tribrominated Diphenyl Ethers ppm (TriBDE) Tetrabrominated Diphenyl ppm Ethers (TetraBDE) Pentabrominated Diphenyl ppm Ethers (PentaBDE) Hexabrominated Diphenyl Ethers ppm (HexaBDE) Heptabrominated Diphenyl ppm Ethers (HeptaBDE) Octabrominated Diphenyl Ethers ppm (OctaBDE) Nonabrominated Diphenyl Ethers ppm (NonaBDE) Decabrominated Diphenyl Ether ppm (DecaBDE) Phthalates Di(2-ethylhexyl) Phthalate ppm (DEHP) Dibutyl Phthalate (DBP) ppm Benzyl Butyl Phthalate (BBP) ppm Halogen Content Fluorine (F) ppm Chlorine (Cl) ppm Bromine (Br) ppm Iodine (I) ppm Others Hexabromo cyclododecane (HBCDD) ppm Test Method Black paste With reference to IEC 62321: 2008, by solvent extraction and determined by GC-MS and further HPLC-DAD confirmation when necessary. RL ND 5 ND 5 ND 5 ND 5 ND 5 ND 5 ND 5 ND 5 ND 5 ND 5 With reference to EN 14372: 2004, by solvent extraction and determined by GC-MS. ND 50 ND ND 50 50 With reference to EN 14582:2007 by calorimetric bomb with oxygen and determined by Ion Chromatograph. ND ND ND ND 50 50 50 50 With reference to USEPA 3540C, by solvent extraction and determined by GC-MS. ND 10 *THJ0306991* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C. 全國公證檢驗股份有限公司 11492 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 3 of 10 Number : TWNC00306991 Test Conducted Remarks: ppm ND RL = parts per million based on wet weight of tested sample = mg/kg = Not detected = Reporting Limit, Quantitation limit of analyte in sample Responsibility of Chemist: Date Sample Received Test Period Kevin Liu/ Irene Chiou/ Vico Lin : Apr 10, 2013 : Apr 11, 2013 to Apr 15, 2013 (Ⅱ) Limit: RoHS Limit Restricted Substances Cadmium (Cd) content Lead (Pb) content Mercury (Hg) content Chromium VI (Cr6+) content Polybrominated Biphenyls (PBBs) Polybrominated Diphenyl Ehters (PBDEs) Limits 0.01% (100ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) The above limits were quoted from Annex II of 2011/65/EU for homogeneous material. *THJ0306991* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C. 全國公證檢驗股份有限公司 11492 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 4 of 10 Number : TWNC00306991 Test Conducted (Ⅲ) Measurement Flowchart: Test for Cd/Pb/Hg/Chromium (VI)/PBBS/PBDES Contents Reference Standard: IEC 62321 edition 1.0:2008 Sample preparation For non-metal part For metal part Take sample and immerse into Aqua Regia, start to strip plating layer Stop the stripping procedure upon color change completely Take the Aqua solution as plating component and stripped body as substrate component PBBs/PBDEs Weigh sample and add organic solvent By Soxhlet extraction or Solvent extraction Concentrate the extract and make up with organic solvent Analyzed by GC-MSD Cr 6+ Substrate Cd/Pb/Hg Weigh sample and add alkaline solution For different material, digest the sample with *1 appropriate acid Plating Cr 6+ By spot test Definite temp. extraction Cool and filter the extract Confirm the tested samples are totally dissolved Negative *2 Get 50cm2 sample Make up with deionized water By boiling water extraction Analyzed by ICP-OES Make up with deionized water and add diphenyl-carbazide solution Analyzed by UV-VIS *THJ0306991* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C. 全國公證檢驗股份有限公司 11492 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 5 of 10 Number : TWNC00306991 Test Conducted Remarks: *1: List of Appropriate Acid: Material Polymers Metals Electronics Acid Added for Digestion HNO3,HCl,HF,H2O2,H3BO3 HNO3,HCl,HF HNO3,HCl,H2O2,HBF4 *2: If the result of spot test is positive, Chromium VI would be determined as detected. *THJ0306991* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C. 全國公證檢驗股份有限公司 11492 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 6 of 10 Number : TWNC00306991 Test Conducted Test for Halogen Content Reference Standard:EN 14582 Sampling/grinding or cutting Add absorbent in a combustion flask & place weighed sample in equipment Fill oxygen into calorimetric bomb Ignite then leave the bomb at room temperature Transfer the absorbent into a volumetric flask Make up with deionized water Analyzed by ion chromatography *THJ0306991* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C. 全國公證檢驗股份有限公司 11492 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 7 of 10 Number : TWNC00306991 Test Conducted Test For Phthalates Contents Reference Method: EN 14372: 2004 Sampling/grinding or cutting Weigh sample and add organic solvent By solvent extraction Concentrate the extract and make up with organic solvent Analyzed by GC-MSD *THJ0306991* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C. 全國公證檢驗股份有限公司 11492 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 8 of 10 Number : TWNC00306991 Test Conducted Test For Hexabromocyclododecane (HBCDD) Reference Standard:USEPA 3540C Sampling/grinding or cutting Weigh sample and add organic solvent By soxhlet extraction Concentrate the extract and make up with organic solvent Analyzed by GC-MSD End of Report This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a recommendation for any particular course of action. Intertek does not accept a duty of care or any other responsibility to any person other than the Client in respect of this report and only accepts liability to the Client insofar as is expressly contained in the terms and conditions governing Intertek's provision of services to you. Intertek makes no warranties or representations either express or implied with respect to this report save as provided for in those terms and conditions. We have aimed to conduct the Review on a diligent and careful basis and we do not accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by statute or otherwise, except in the event of our gross negligence or wilful misconduct. *THJ0306991* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C. 全國公證檢驗股份有限公司 11492 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 9 of 10 Number : TWNC00306991 Test Conducted Photo *THJ0306991* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C. 全國公證檢驗股份有限公司 11492 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 10 of 10 Test Report Applicant: Number : TWNC00292460 Littelfuse Philippines Inc. LIMA Technology Center, Lipa City, Malvar, Batangas Date : Jan 07, 2013 Sample Description: One (1) group of submitted samples said to be : Part Description : Ink Part Number : 425809 Date Sample Received : Dec 27, 2012 Date Test Started : Dec 27, 2012 Test Conducted : As requested by the applicant, for details please refer to attached pages. Authorized by: On Behalf of Intertek Testing Services Taiwan Limited K. Y. Liang Director *THJ0292460* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C. 全國公證檢驗股份有限公司 11492 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 1 of 4 Number : TWNC00292460 Test Conducted (Ⅰ) Test Result Summary : Result (ppm) Black ink ND Test Item Antimony (Sb) Content Remarks: ppm = Parts per million based on wet weight of tested sample = mg/kg ND = Not detected Responsibility of Chemist : Irene Chiou / Kevin Liu Date Sample Received Test Period (Ⅱ) Test Method: Test Item Antimony (Sb) Content : Dec 27, 2012 : Dec 27, 2012 To Jan 03, 2013 Test Method With reference to USEPA 3052, by microwave digestion until the tested samples are totally dissolved and determined by ICPOES. Reporting Limit 2 ppm Remark: Reporting limit = Quantitation limit of analyte in sample *THJ0292460* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C. 全國公證檢驗股份有限公司 11492 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 2 of 4 Number : TWNC00292460 Test Conducted (Ⅲ) Measurement Flowchart: Test For Heavy Metal (Sb) Contents Reference Standard:USEPA 3052 Sampling/grinding or cutting Weigh sample and digest in microwave digestion oven with suitable acid Confirm the tested samples are totally dissolved Transfer the digested solution and make up with deionized water Analyzed by ICP-OES End of Report This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a recommendation for any particular course of action. Intertek does not accept a duty of care or any other responsibility to any person other than the Client in respect of this report and only accepts liability to the Client insofar as is expressly contained in the terms and conditions governing Intertek's provision of services to you. Intertek makes no warranties or representations either express or implied with respect to this report save as provided for in those terms and conditions. We have aimed to conduct the Review on a diligent and careful basis and we do not accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by statute or otherwise, except in the event of our gross negligence or wilful misconduct. *THJ0292460* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C. 全國公證檢驗股份有限公司 11492 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 3 of 4 Number : TWNC00292460 Test Conducted Photo *THJ0292460* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C. 全國公證檢驗股份有限公司 11492 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 4 of 4