ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: Nano2 Fuse - SB Product #: 452xxxL Series Issue Date: May 08, 2013 It is hereby certified by Littelfuse, Inc. that there is neither RoHS (EU Directive 2002/95/EC, 2011/65/EU)-restricted substance nor such use, for materials to be used for unit parts, for packing/packaging materials, and for additives and the like in the manufacturing processes. In addition, it is hereby reported to you that the parts and sub-materials, the materials to be used for unit parts, the packing/packaging materials, and the additives and the like in the manufacturing processes, are all composed of the following components. Issued by: <Global EHS Specialist> (1) Parts, sub-materials and unit parts This document covers the Nano2 Fuse - SB RoHS-Compliant series products manufactured by Littelfuse, Inc. < Raw Materials Used Please see Table 1 (2) The ICP data on all measurable substances Please see appropriate pages as identifed in Table 1 Remarks: Pb (lead) contained in the high temperature melting solder > 85% and is categorized as exempt under section 7a of the RoHS Annex. Form 585-047 Rev. A 1 2/21/06 Table 1: List of Raw Materials covered by this report Total Parts 1 2 3 4 5 6 7 8 Raw Material Part Number 910-275 Frequenta C221 (909-434) 11-0595 (082xxx-001) 692323 648118 648106-001 648112-001 425809 Raw Material Description Cap Body – Ceramic Tube Element – Cu99.9MSn(082xxx) Solder Yarn – GLZZXXX-6481XX Yarn Yarn Ink-Black 2 Page(s) 3-8 9-37 38-41 43-47 48-54 55-62 63-70 71-80 Test Report Applicant: Number : TWNC00285774 Littelfuse Philippines Inc. LIMA Technology Center, Lipa City, Malvar, Batangas Date : Nov 19, 2012 Sample Description: One (1) group of submitted samples said to be : Part Description : Cap Part Number : 910-275 Date Sample Received : Nov 12, 2012 Date Test Started : Nov 13, 2012 Test Conducted : As requested by the applicant, for details please refer to attached pages. Authorized By: On Behalf Of Intertek Testing Services Taiwan Limited K. Y. Liang Director *THJ0285774* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 1 of 6 Number : TWNC00285774 Test Conducted (Ⅰ) Test Result Summary : Result (ppm) (1) (2) Test Item Heavy Metal Cadmium (Cd) content Lead (Pb) content Mercury (Hg) content Chromium VI (Cr6+) content (mg/kg with 50cm2) ND ND ND Negative (< 0.02) (#) ND ND ND Negative (< 0.02) (#) Remarks: ppm = Parts per million based on weight of tested sample = mg/kg ND = Not detected < = Less than mg/kg with 50cm2 = milligram per kilogram with 50 square centimetre Negative = A negative test result indicated positive observation was not found at the time of Test. # = Due to the insufficient sample area, reduced total sample surface of 25 cm2 was used and the dilution factor was adjusted accordingly. Tested Components (1) Coppery metal base material (2) Golden plating layer Responsibility of Chemist : Irene Chiou / Kevin Liu Date Sample Received Test Period : Nov 12, 2012 : Nov 13, 2012 to Nov 16, 2012 (Ⅱ) RoHS Limits: Restricted Substances Cadmium (Cd) Content Lead (Pb) Content Mercury (Hg) Content Chromium VI (Cr6+) Content Limits 0.01% (100ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) The above limits were quoted from Annex II of 2011/65/EU for homogeneous material. *THJ0285774* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 2 of 6 Number : TWNC00285774 Test Conducted (Ⅲ) Test Method: Test Item Cadmium (Cd) content Lead (Pb) content Mercury (Hg) content Chromium VI (Cr6+) content Test Method With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in clause 7, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in annex B, by boiling water extraction and determined by UV-Vis Spectrophotometer. Reporting Limit 2 ppm 2 ppm 2 ppm 0.02 mg/kg with 50cm2 Remark: Reporting limit = Quantitation limit of analyte in sample *THJ0285774* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 3 of 6 Number : TWNC00285774 Test Conducted (Ⅳ) Measurement Flowchart: Test For Cd/Pb/Hg/Chromium (VI) Reference Standard:IEC 62321 edition 1.0:2008 Sample preparation Take sample and immerse into Aqua Regia, start to strip plating layer Stop the stripping procedure upon color change completely Take the Aqua solution as plating component and stripped body as substrate component Cd/Pb/Hg Substrate Plating For different material, digest the sample with *1 appropriate acid Cr 6+ By spot test Confirm the tested samples are totally dissolved Make up with deionized water Negative *2 Get 50cm2 sample By boiling water extraction Analyzed by ICP-OES Make up with deionized water and add diphenyl-carbazide solution Analyzed by UV-VIS *THJ0285774* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 4 of 6 Number : TWNC00285774 Test Conducted Remarks: *1: List Of Appropriate Acid: Material Polymers Metals Electronics Acid Added For Digestion HNO3,HCl,HF,H2O2,H3BO3 HNO3,HCl,HF HNO3,HCl,H2O2,HBF4 *2: If the result of spot test is positive, Chromium VI would be determined as detected. End of Report This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a recommendation for any particular course of action. Intertek does not accept a duty of care or any other responsibility to any person other than the Client in respect of this report and only accepts liability to the Client insofar as is expressly contained in the terms and conditions governing Intertek's provision of services to you. Intertek makes no warranties or representations either express or implied with respect to this report save as provided for in those terms and conditions. We have aimed to conduct the Review on a diligent and careful basis and we do not accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by statute or otherwise, except in the event of our gross negligence or wilful misconduct. *THJ0285774* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 5 of 6 Number : TWNC00285774 Test Conducted Photo *THJ0285774* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 6 of 6 Signature FOTQUE Please Test Report No.: CE/2013/13196Dale:2013101122P a g e : 1 o f 2 9 GMBH CERAMTEC 5, 91207LAUF MULTIFUNKTIONSKEMMIK,LUITPOLDSTRABE'1 GESCHAFTSBEREICH l!][!lllllIllllll Thefollowingsample(3)was/weresubmittedand idontifiedby/onbehalfofthe clientas: SampleDescription Styldltem No. Date sampleReceiving TestingPeriod CERAIVIC C221 FREOUENTA 2013t1t14 122 2013t1| 14 10 2013tO1 Test Result(s) Pleasereferto nextpage(s). Conclusion thetestresultsof Cadmium'Lead' samples, Ba6edontheperfomedtestson submitted PBDES complywiththe limitsas setby PBBS and Cr(Vl), Hexavalent Chromium Mercury, 200295/EC ll; recasting Annex RoHSDirective 2011/65/Eu (Nw4p [Ner;]F cryriits/rif'"i 'r' {li f {'}itgi! Test Report No.: CE/201t'13196 Date: 2013101122Page:2of 29 CERAMTECGMBH 15, 91207 LAUF I\IULTIFUNKTIONSKERAMIK,LUITPOLDSTRABE GESCHAFTSBEREICH Test R€ultla) PART I.]AME No.1 : CREAMCERAMIC Tst ltem(s) Cadmium(Cd) Lead(Pb) (Hg) Mercury Cr(Vl) Chromium Hexavalent (cAs BBP(Benzylbutylphthalate) No.:8568-7) DEHP(Di-(2-ethylhexyl) phthalate) (CASNo.:1'1ru1-7) DIDP (Di-isodecylphthalate)(CAS No.:26761.40-0) DINP(Di-isononylphthalate)(cAs No.:28553-12-0) DNOP(Di-n-oc'tylphthalate)(CAS No.:117-84-0) DBP (Dibutylphthalate)(CAS No.: U-74-2) Perfluorooctanesulfonates (PFOS-Acid, MetalSalt,Amide) PFOA (CAS No.. 335€7-1) Unit Moihod to IEC62321:2008and mg/Kg Withreference perfomedby ICP-AES. to IEC62321;2008and mg/Kg Withreference pedormedby ICP-AES. to IEC62321:2008and mg/Kg Withreference perfomedby lCPdES. to IEC62321:2008and mgik9 Vvitfrreierence MDL Result No.'l Limit 2 n.d. 100 2 n.d. 1000 2 n.o. 1000 2 n.d. 1000 pedormed byUV-VIS. to EN 14372.Analysis Withrcference wa6pertormedby GC/[is. to EN 14372.Analysis % Withr€ference wEsperfomedby GC/MS. to EN 14372.Analysis vvithreference wEsperformedby GC/MS. o/. to EN 14372.Analysis Withreference wEsperfomedby GC/MS. to EN 14372.Analysis Withreference perfomed by GC/MS. wEs to EN 14372.Analysis Withreference % wEsperfomedbYGC/MS. mg/Kg Wi-threferenceto Us EPA3550C: bY waspedormed 2007.An€lysis LC/MS. mg/kg Withreferenceto US EPA3550C: 2007.AnalysiswasPerformedbY LCiMS. o/o to USEPA3540C (PCBS) mdKo Withreference Biphenyls Polychl''inated bY w?sPerfomed Analysis method. (CASNo.:133S36-3) 0.003 n.d. 0.003 n.o. 0.0! n.o. 0.01 n.d. 0.003 n-o. 0.003 n.d. 10 n-d. 10 n.d. 0.5 n.d. GC/MS. $ffiw,fiffimt$uffidiffir. N€wtrtsicirtdMn/ri : i 6 rr tl;! t i-r1331i Test Report No.: CE/2013/13'196Dale,2013101122P a g e : 3 o f 2 9 CERAMTEC GMBH 15, 91207LAUF MULTIFUNKTIONSKERAI'IK,LUITPOLDSTRABE GESCHAFTSBEREICH Test ltem(s) Unlt lrethod TIDL 0.5 mg/Kg With referenceto US EPA3540C method.Analysiswasperfodnedby GC/MS, 5 mg/Kg With referenceto uS EPA3$0C Polychlorinated Naphthalene method.Analysiswasperformedby (PCN6) GC/MS. '100 mSikS Withreferenceto US EPA3g0C Alkanes, C10-13,chloro(Short lr€s performed by methodAnalysis ChainChlorinatedParaffins)(CAS GC/IVS. No.:85535-84-8) Analysiswaspertormedby FTIRand PVC FLAMETesT, to ISO17226-112008). 3 (CASNo.:50{0-0) mg/Kg Withreference Formaldehyde Anaiysiswasperformedby HPLC/DAD. Terphenyl6 Polychlorinated (PCTS) Result No.1 n.o, n.d. n.d. Negative n.o. 0.5 n.d. 0.5 n.d. tetrachlorodiPhenYl mg/kg Withreferenceto Us EPA8270D Monomethyl wasPerfomedbY Analysis method. methane(Ugilec14'1) GC/MS. Halogon 0.5 n.d. (F) (CAS No.: Halogen-Fluorine '14762-94€) mlyKg 50 n,d. (Cl)(cAs No.: Halogen-Chlorine 22537-15-1) (Br)(CASNo.: Halogen-Bromine 100€7-32-2' mgKg 50 n.d. With referenceto BS EN 14582:2007 mdkg Analysiswasperformedby lC. 50 n.d. Halogenlodine(l) (CAS No.: '143€'2444\ m!/Kg 50 n.d. 0.03 n.d. n.o. Monomethyl dibromodipheny' methane(DBBT) Monomethyl dichlorodiphenyl methane(Ugilec12'l) to USEPA8270D mg/Kg Withreference wasperfonned by method. Analysis GC/MS. to USEPA8270D mg/kg Withreference Analysis wEsperfomedbY method. GC/MS. Organic-lincompound6 TdbutylTin(TBT) (TphT) TdphenylTin mg/kg With referenceto DIN38407-13. mg/Kg AnalysiswEsperfomedbYGC/FPD r, w! cius Rd,N4 riird idsrdP'( 0.03 !"rirrrtGlqi Limit Test Report No.: CEl2013/13196Dale:2013101122Page:4 of 29 r] [tlt][ttllll GMBH CERAMTEC 15,91207LAUF MULTIFUNKTIONSKERAIIIK,LUITPOLDSTMBE GESCHAFTSBEREICH Test ltem(6) Unit Asbe€toa Adinolite(CASNo.:77536€6-4) (CASNo.:12172-73-5) Amosite (CASNo.:77536€7Anthophyllite o/. (CASNo.:1200'l-29-5) Chrysotile Crocidolite(CASNo.: 12OOl2A4t (CAsNo.r2536€8€) Tremolite AZO % o/o oa Mothod MDL Negative Negative Negative To Analysiswasperformedby GC/MS. 3):44HLORO-O-TOLUIDINE mg/Kg With referenceto LFGB82.02-2. Analysiswasperformedby GC/l!lS. (CASNo.:95$9-2) to LFGB82.02-2. (cAs mg/kg Withreference 4):2-NAPHTHYIAMINE performed bYGC/MS. was Analysis No.:91-594) (CAS mgftg Withreferenceto LFGB82.02-2. 5):O-AMINOAZOTOLUENE Analysis wasperfomedby GC/MS. No.r97-56-3) to LFGB82.02-2. mg/kg Withreference 6):2-AMINO-4-NITROTOLUENE 'rias p€rformed by GC/MS. Analysis (CASNo.:99-55-8) (CASNo. mgKg With referenceto LFGB82.02-2. 7): PCHLOROANILINE '10647-8) bYGC/MS. wasperformed Analysis (CAS mg/Kg With referenceto LFGB82.02-2+ 2,4-D|AMTNOANISOLE Analy6iswas performedby GC/MS. No-:615-054) to LFGB82.02-2. mg/Kg Withreference 9r:4,4'performed bYGC/IIS. was Analysis DIAMINODIPHENYLMETHANE (CASNo.:101-77-9) 1O)..3,3!DtCHLOROBENZIDINEmlyKg With referenceto LFGB82.02-2. wasperfomedbYGC/MS. Analysis (CASNo.;9'l-94-1) mgikg uvitlrraferenceto LFGB82.02-2 1'1):3,3'-DIMETHOXYBENZIDINE AnalysiswasperfomedbYGC/MS (CASNo.:119-90-4) 12):3,3-DIMETHYLBENZIDINEmg/kg With referenceto LFGB82.02_2 AnalysiswasperformedbYGC/MS(CASNo.:119-93-7) rxwu.hune-NewhiFrrndu5rirtu' No.l Negative Negative Negative I6 With refercnceto EPA600/R-93'/1 method.Analy6iswasperformedby (SlV),Dispe6ion StereoMicroscope Lightl\ricroscope Staining Poladzed (DS-PLM)andX-€y Diffraction (XRD). Spectrometer (CAS No.: mg/kg With referenceto LFGB82.02-2. 1): ,I-AMINODIPHENYL Analysisw€sperformedby GC/MS. 9267-1) to LFGB82.02-2. (CASNo.:92-87- mlyKg Withreference 2): BENZIDINE Re3ult 3 n.d- 3 n.d. 3 n.d. 3 n.d. 3 n.d. n.o. n.d. 3 n.d. 3 n.d. 3 n-o. 3 n.d. 3 n.d. L,iii'rr"'nfirr\'t Limit TestReport No.: CE/20f31 3196 Dale: 2013101122Page: 5 of 29 rrl[ttttllltl CERAMTECGMBH 15, 91207 LAUF MULTIFUNKTIONSKERAMIK,LUITPOLDSTRABE GESCI-IAFTSBEREICH To6tltem(s) Unit ethod '13)r3,3'-DIMETHYL-4,4'to LFGB82.02-2. mSikS with reference ,a/as performed by GC/MS. Analysis DIAI'INODIPHENYLMETFIANE (CASNo.:838€84) to LFGB82-02-2. (2-METHOXY-mgKg Withreference 14):P-CRESIDINE (CASNo.: Analysis'r/asperformedby GC/MS. s-METHYLANILINE) 12'+171-E' (2to LFGB82.02-2. mgKg Withreference 15):4,4'-METHYLENE-B|Sperformed bYGC/MS. was (CAsNo.l Analysis CHLOROANILINE) 101-'t+4\ to LFGB82.02-2. (CAS mgKg Withreference 16) 4,4'-OXYDtANILINE by GC/MS. waspedormed Analysis No. 101€04) '!7):4,4'-THIODANILINE(CAS mg/Kg with refe€nceto LFGB82.02-2. Analysiswaspertormedby GC/l!lS. No.:13945-1) to LFGB82.02-2. (CASNo.:95- mg/Kg Withreference 18):O-TOLUIDINE wasperfomedby GC/MS. Analysi6 534) to LFGB82.02-2. 19} 2,+TOLUYLENEDIAMINE mg/Kg with reference prfomed by GC/MS. wEs Analy6is (CASNo.:95€G7) to LFGB82.02-2. 20)r2,4,5-TRIMETHYLANILINEmg/kg Withreference perfomed bYGC/MS. was Analysis (CASNo.:137-17-7) to LFGB82.02-2. (cASNo.:90- mgftg Withreference -): o+NrsrDlNE AnalysiswEsperfomedbYGC/MS04{) to LFGB82.02-2. mgKg Withreference 22F-AMINOAZOBENZENE perfofmed bYGC/MS. was An€lysis (CASNo.:60{9-3) (CASNo.:95- mgftg Withreferenceto LFGB82.02-2 23):2,4-xYLlD|NE AnalysiswasperformedbYGC/MS 68-1) to LFGB8202-2 (CASNo.:87- mgag Withreference 24):2,6-XYLIDINE perfomed bYGC/MS wa6 Analysis 62-7) CFC'3(Chlo|ofluorocaibons) GroupI luoroca6on-11 (CASNo.: mgKg With referenceto US EPA5021 Chlo,rof bY wasPerform€d Analysis method. 756+4) GC/MS. mg/Kg With referenceto US EPA502'1 uorocabonl2 (CASNo.I Chlorofl method.AnalysiswasPerfomedbY 75-71-8) GC/MS. MDL R€oult No.l 3 n.d. 3 n.o. 3 n.d. 3 n.d. 3 n.d. 3 n.d. 3 n.d. 3 n.d. 3 n.d. 3 n.o. 3 n,o. 3 n.d. I n.d. Limit n.d. ffi,ffiq*ffitrffit$gwl*ffi##f Test Report No.:CE/2013'/13196 Oale|2013101122 Page: 6 of 29 r]l[ttti[ltl.ll GMBH CERAMTEC 15' 91207LAUF IVULTIFUNKTIONSKERAMIK,LUITPOLDSTRABE GESCHAFTSBEREICH Test ltem(s) 13 (CASNo.: Chlorofluorocarbon-1 76-13-1) Method Unit mg/Kg With referenceto Us EPA5021 method.AnalysiswEsPerfomedbY GC/MS. 14(CASNo.: mg/kg With referenceto US EPA5021 Chloroftuorocarbon-1 meihod.AnalysiswEsPerfomedbY 76-14-2) GC/MS. 15(CASNo.: mg/Kg With refefenceto US EPA5021 luoroca6on-1 Chlorof method.AnalysiswasPerfom€dbY 76-15-3) GC/MS. Grouplll 3 (CASNo.: Chk'rofiuorocarbon-1 75-7241 (CASNo l Chtorofluorocarbon-1'11 354-s&3) '12 (CASNo.: Chlorofluorocarbon-1 76-12-O) 1 (CASNo : Chlorofluoroca6on-21 422-74.6] 12 (CASNo.: Chlorofluorocarbon-2 3182-m-1) 3 (cAs No Chlorofluorocarbon-21 2354-06-5) (CASNo. Chlorofluorocadon-214 2925931-0) (CASNo: Chlorofluorocarbon-21s 425943-2) to us EPA5021 mgftg vvithreference bY wasPerformed Analysis method. GC/MS. to us EPA5021 mg/kg with reference bY wE5perfomed method. Analysis GC/MS. MDL 'I I'lo.l n.d. 1 n.d- 1 n.d. 1 n.d. 1 n.d. n.d. mg/Kg With referenceto US EPA5021 method.AnalysiswasperfomedbY GC/MS. to uS EPA5021 m!/Kg Withreference bY wasPerformed Analysis method. GC/MS, to us EPA5021 mg/Kg vvithreference Result n.d. 1 n.d. 1 n-d. 1 n.d. wasPedomedbY Analysis method. cc/Ms. m9K9 Wth referenceto US EPA5021 method.AnalysiswasPerformedbY GC/MS. mg/Kg With referenceto US EPA5021 method.Analysi6wasPedormedbY GC/MS. to USEPA502't mg/kg Withreference n.d. bY wasPerformed Analysis method. GC/MS. L .!.,iJd;i1li+n-qj Limit Test Report No. : CE/2013/13 196 Date: 2013101122Page: 7 of 29 rtl| rIllr]llllllll CEMMTEC GMBH 15' 91207 tAUF MULTIFUNKTIONSKERAMIK,LUITPOLDSTRABE GESCHAFTSBEREICH Test ltom(s) Mothod Unit (CASNo.: mg/Kg With referenc€to US EPA5021 luorocabon-2l6 Chlorof method.AnalysiswasperfomedbY 661-97-2) GC/MS. (CASNo.: mgKg With referenceto tJSEPA5021 luoroca6on-217 Chlorcf method.AnalysiswasPerfornedbY 42246-6\ GC/MS. MDL 1 No.l n.d. 1 n.d. HCFC8 (Hyd rochlo.ofl uorocarbons) (CASNo.:7543-4) HCFC-21 (CASNo.:75454) HCFC-22 R66ult n.d. mg/Kg With referenceto US EPA5021 bY wasPerformed Analysis method. GC/MS. mg/Kg With referenceto US EPA5021 by method.AnalysiswasperforYned n.d. cc/Ms. l'lCFG31 (CASNo.: 5S3-7G4) (CASNo.:354-14-3) HCFC-121 (CASNo.:354-21-2) HCFC-122 mgftg With reforenceto US EPA5021 method.Analysisw€sPerformedbY GC/MS. mg/Kg With referenceto US EPA5021 method.AnalysiswasPertormedbY GC/MS. to us EPA5021 mg/kg Witlrreference 1 n.o, 1 n.d. 1 n.d. bY wasPerfomecl Analysis method. GC/MS. n.d. (cnsNo.:sos-eg-z) mg/K9 Wl[referenceto us EPn5o2t Fierc-tzs bY wasPerformed Analysis method. GC/MS. (CASNo.:2837€9-0) mgKg With referenceto us EPA5021 FieFC-124 pertormed by $/as Analysis methodGC/MS. to US EPA5021 trCf:i3T@SI6,,55r-tEi- mg/Kg With reference wa6PerformedbY Analysis method. GC/MS. to USEPA5021 mg/Kg Wiihreference -cFc-r32b(cAsNo.:164s-08-7) bY wasPerformed Analysis method. GC/MS. gffiffiffi ri$r,iL1Hl];4' 1 n.d. 'I n.d. 1 n.o. Limit TestReport No.: CE2013/13196 Dale:2013J01122Page: 8 of 29 IlflI|rr][tlllll CERAMTEC GMBH 15, 91207LAUF MULTIFUNKTIONSKERAMIK,LUITPOLDSTRABE GESCHAFTSBEREICH T€t lt.m(s) (CASNo.:75-88-7) HCFC-'133a MDL Method Unit mgKg With r€ferenceto US EPA5021 method.Analysiswaspedomed by GC/MS. HCFCl4lb (CASNo.:171740€) mlyKg With referenceto US EPA5021 method.AnalysiswasperformedbY GC/MS. mgKg with referenceto tjs EPA5021 HCFC-142b (CAS No.: 7ffi8-3) method.AnalysiswasperformedbY GC/MS. HCFC221(CAsNo.r422-26-4) m9Kg wth referenceto Us EPA5021 method.AnalysiswasPerformedbY GCA,rS. (CASNo.:422-491) mg/kg With refer€nceto US EPA5021 HCFC-222 by wasperformed Analysis method. GC/MS. (CASNo.:422-526) mg/Kg With referenceto US EPA5021 HCFC-223 method.AnalysiswasPerformedbY GC/MS. HCFG224(CASNo.i422-54-8) mgKg Wth referenceto US EPA5021 method.AnalysiswasPertormedbY Result No.l 1 n.d. 1 n.d. 1 n.d. I n.d. 1 n_o, Llmit n.d. n.d. cc/Ms. (CASNo.:422-56-0) mg/kg With referenceto US EPA5021 HCFC-22sca method.AnalysiswEsPerformedbY GC/MS. HCFG22scb(CASNo.:507-55-1) mg/Kg With referenceto US EPA5021 rnethod.Analysiswasperformedby GC/MS. mgKg Wth referenceto US EPA5021 (cAS No.:431-87€) HCFC-226 method.Analysis$rasperformedby GC/MS. (CASNo.:421-94-3) msyKg With referenceto uS EPA5021 HCFC-231 bY wasPerformed Analysis method. GC/MS. US EPA5021 EdFe'fidsxo-:?60-:3CE mg/Kg Vvithreferenceto was method.Analysis PerformedbY GC/MS. 1 n.d- I n.o. 1 n.d. n.d. 1 n.d. ffii'*r-ffiffiffitrffig-#rffi ':irrr!r.rt1!r1riF'!a I r+e610?r,qrr 4s6o1rerr ws+M -,--- .- Test Report No.:CE2013/13196D are:2013101n2P a g e : 9 o f 2 9 tf]tt|al] CERAMTEC GMBH 15,91207LAUF MULTIFUNKTIONSKERAMIK,LUITPOLDSTRABE GESCHAFTSBEREICH Test ltem(s) Unit f,lethod (CASNo.:7'125-84-0) mgitg With roferenceto US EPA5021 HCFC-233 method.Analysisurasperformedby GC/MS. (CAS With referenceto US EPA5021 425-94-5) mg/kg HCFC-234 No.: method.AnalysiswaspertormedbY GC/rUS. to USEPA5021 mgftg Withreference HCFC-235(CASNo.:460-92-4) v€s performed bY method. Analysis GC/MS. (CASNo.:666-27-3) mgikg with refer€nce to us EPA5021 HCFC-241 MDL Result No.1 n.d. n.d. 'I n.d. I n.d. I n.d. 1 n.d. bY wasPedormed method. Analysis GC/MS. (CASNo.:42141-0) HCFC-251 mgikg With referenceto US EPA502'1 method.AnalysiswasperformedbY GC/MS. mg/kg With referenc€to US EPA502't Analysis wasperfomedbY method. GC/MS. mgKg With referenceto US EPA5021 bY wasPerformed Analy6is method. GC/l,lS. to USEPA5021 mg/kg Vviltrreference (CASNo.:819-00-1) HCFC-252 mg,iKg With referenceto tJSEPA5021 (CASNo.:460€3-9) HCFC-242 (CASNo.:460-69-5) HCFC-243 HCFC-244 (CASNo.:460-35-5) HCFC-253 HCFC-261(CASNo.:42G97-3) N-;Ain {s)trCFdt6-tGAs ffi n.d. n,o. bY wasPerformed Analysis method. GC/MS. bY wasPerformed Analysis method. GC/MS. mg/Kg With referenceto uS EPA5021 bY wasPerlormed Analysis methodGC/MS. m9Kg With referenceto US EPA5021 bY wasPerformed Analysis method. GC/MS. referenceto US EPA5021 With m9Kg bY method.Analy6iswasPerfoamed GC/MS. ix4itir.lt |tiri 1 n.d. 1 n.d. ,l n.d. n.d. llllll Limlt TestReport No.: CE2013'13196 Oanet 2913101122Paoe: 10of 29 CERAMTEC GMBH GESCHAFTSBEREICH MULTIFUNKNONSKERAMIK.LUITPOLDSTRABE 15.91207LAUF Testltem(s) (CASNo.:43G55-7) HCFC-271 Unit Method I'DL mgKg With referenceto US EPA5021 method. Analysis wEsperfomedby GC/MS. Halona (CASNo.:353*59-3) mSikg Wathreferenceto Us EPA502'1 Halon-1211 (CASNo.:75$!8) Halon-1301 mgftg method.Analysiswasperformedby (CAS Halon-2402 No.: 124-73-2) mg/Kg GC/MS. 1 [] [ta]l[ttll|t Rosult No.1 n.d. I 1 1 n.d. mg/Kg With referenceto LJSEPA5021 method. Analysis wasperfomedby GC/MS. rngL/Kg Withreference to USEPA5021 method.Analysiswaspertormedby GC/MS. mg/Kg With referenceto US EPA5021 m€thod. Analysis wasperformed by GC/tUS. mg/kg Withreference to USEPA5021 method.Analysiswasperformedby GCiMS. mg,iKg Wth referenceto US EPA5021 method.Analysiswaspertormedby GC/MS. mg/Kg With referenceto US EPA5021 method.Analysiswa8performedby GC/MS. to uS EPA5021 mg/Kg Withreference 1 n.d. (CASNo.: 1,2,3-Trichloopropane 96-184) (CASNo.: 1,2-Dichloroethane 107,cF2]- n.o. n.o. CHCS(Chlodnate hyd.ocarbon) (CAS 1,1,1,2-Tetrachloroethane No.:630-20€) '1,1 (CASNo.: ,1-Tdchloroethane 71+56) (CAS 1,1,2,2-Tet€chloroethane No.:7$34-5) '1 1 (CASNo.l , ,2-Trichloroethane 79-00-5) (CASNo.:7$ 1,1-Dichloroethane 34-3) (CASNo.:7$ 1,'1-Dichloroethene 3s4) (CASNo.: 1,1-Dichloropropene 563-586) n.d. n.d. n.d. n.d. 1 n.d. 1 n.d. msyKg With ref€renceto US EPA5021 method.Analysiswaspertormedby 1 n.d. mg/kg With refe.enceto Us EPA502'1 bY wasperformed method. Analysis GC/|V]S. I n-d. wasperfomed by method. Analy6is GC/MS. cciMs. N4laipd.tvr.iwm/ii r ' 6 i Hil ilErit!: Limit TeSt pase:ii of2s No.:cE/2013/r3196 Date:2o13t01t22 RepOft GERAI,IITEC GMBH GESCHAFTSBEREICH MULTIFUNKTIONSKERAMIK.LUITPOLDSTRABE 15.91207LAUF Test ltem(s) Unit Method 1 Result No.t n.o. 1 n.d. 1 n.d- I n.d. I n.d- MDL 1,2-Dichloropropane (CASNo.: 78€7-5) mg/Kg With referenceto US EPA5021 method.Analysiswasperlormedby GC/MS. (CASNo.: 1,3-Dichloropropane mgikS Withreference to LJSEPA5021 't42-2E-9) method.Analysiswa6perfomedby GC/MS. 2,2-Dichloropropane (CASNo.: mg/Kg With referenceto LJSEPA5021 594-20-7) method.Analysisw€sperformedby GC/[rS. L;arbontetrachloide(cAs No.: mg/Kg With referencato US EPA502'1 methodAnalysis wasperfomedby GC/t\rs. (CASNo.:75-0G3) mg/Kg With ref€renceto US EPA5021 Chloroethane method. Analysis wasperfomedby GC/[rS. Chlorcfom(CASNo.:67€6-3) mg/Kg With referenceto uS EPA5021 m€thod.Analysiswasperformedby GC/MS. (CASNo.:7,f€7- m9Kg Withreference Chloromethane to USEPA5021 3) method.Analysi6wasperformedby GC/MS. (CAS cis-1,2-Dichloroethene No.: mg/kg With referenceto US EPA5021 15e59-2) method. Analysis wasperformed by GC/MS. cis-1,3-Dichloropropene (CASNo.; mg/Kg With referenceto US EPA5021 '10061-01-5) method.AnalysiswEsperformedby GC/MS. (CASNo.: Hexachlorobutadiene mg/kg With referenceto US EPA5021 876&3) method. Analysis wasperformed by GC/[rS. Methylene Chlodde(CASNo.:7$ mg/Kg Withreference to uS EPA5021 method.Analysiswasperformedby 09-2) GC/MS. (CASNo.:127- m9Kg Wth reference Tetrachloroethene to USEPA5021 method. Analysis waspeafomed by 184) GC/MS. !]l||||r]tllttltl '| n.d. 1 n.d. 'I n.d. 1 n.d. 'I n-o. n.o, n.d. amoeG)Gsd rhs6repodHm ' ' , I I l l rn ! dGnmsnr 'r 3tu{ bYtr. como ano io' dcrcn'c romar dbumd { 'aadv sd h rd6r oi ot rhbr|e ,idem rddn md tndidon 'sss d6f d.d rh.rc n any horderd hB tumd ihelruoibin1ei!edonon|yandrlth|n$e|im1solc|ienIsfunsifaryfiecoqany!d€B5pon!bi|[ysbisc|ientandlhsdoamsnld hngfuniomsreGinoa|''heL1 co@4 &y JnaLtrd'.o rreElon oaea o' rie 5€ oror se @-.n d .. .-.. 5.r:Ill:"ri, " | ! s.c, ;.. ":2:air; i.r)i33n Limit Test Report No.:CE/2013i/13'196 Date 2O13tO1n2 paae: 12of 29 CERAMTECGMBH GESCHAFTSBEREICH MULTIFUNKTIONSKERAMIK,LUITPOLDSTRABE 15,91207LAUF Testltem(s) Unit Method t€ns-1,2-Dichloroe'thene (CAS No.:15640-5) mdks With referenceto l-JSEPA5021 tran8.l,3-Dichloropropene (CAS No.:10061-02€) mg/Kg With referenceto US EPA5021 method. Analysis wasperfomedby GC/MS. mgKg Withreference to USEPA5021 mothod.Analysiswasperformedby GC/MS. mSI(S mgftg mgftg mg/Kg mg/Kg ttl[tttl[It r,DL R€6ult l{o,1 1 n.d. 1 n.d. 1 n.d- melhod.AnalysiswEsperformedby |l Limit GC/r\,ts. Trichloroethylene (CASNo.:7901€) Sum ot PBBS Monobromobiphenyl Dibromobiphenyl Tribromobiphenyl Tetrabromobiphenyl Pentabromobiphenyl Hexabromobiphenyl Heptabromobiphenyl Octabromobiphenyl Nonabromobiphenyl Decabromobiphenyl Sum of PBDES Monobromodiphenyl ether Dibromodiphenyl 9ther Tribromodiphenyl ether Tetrabaomodiphenyl ether ethea Pentabromodiphenyl Hexabromodiphenyl ether ether Heptabromodiphenyl ether Octabromodiphenyl ether Nonabromodiphenyl ether Decabromodjphenyl n.d. 5 5 mg/Kg mg/Kg n.o, n.o, n.d. n.d. n.d. n.d- mo/Kg mgikg mg/Kg mg/Kg Withreference to IEC62321:2008and mgikg perfomedby GC/MS. m9/Kg mg/Kg m9Kg mg/Kg mg/Kg mg/kg 5 5 5 5 5 5 5 5 n.d. n.o. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.d. n.o. mg/Kg m9Kg mg/Kg 5 5 n.d. n.d. n.d. mgig 5 n.d. @n'nrh'sbstr€eonrcrerorrb$es.mpoG)lesredrhlst6trcpodermt '',:-: :4F; \ : c;; : . i ; ; ; . * . b : # b ' h c m " s € ' € ! r . e d o d 1 a a l ' a € n a b | e o L l aD;d 6 rems ad c.t bm h' El i,ii"a oi-.*t .ili'. rin?icii-; ;;;';;;,,brNd.mn,idDo1a.d..ln$od'sd.'d"'"adtr6d:;;;";';;M de r e s m s b r ' i v ' ; !, + d' ,ei 'so&m+€dirvh' d iiii'n o s'r.iw.,o"-.y*o* 6 * c t d t . * ! 9 q a | | f " " d o n m m 1 t s ' i ' 9 d o e _ . r ' * 1 d ;;;;;;";;;"lD;|d;b;*:'dseryonai"nd*'rh'6;;ii;;pd;;*thnd@*i"*ra'turoidonends*maiben-'-"hdbI 1000 <b 5chrrdr5<ei--g , .1) dl.1ildt4rt, 1000 Test Report No.: CE2013,/13196 Date: 2013t01t22Page: 13of 29 CERAMTEC GMBH GESCHAFTSBEREICH MULTIFUNKTIONSKERAIVIK,LUITPOLDSTMBE'1 5, 91207LAUF ll tI]tIltttll Note: 1. mg/kg= ppm;0.lwt%= 1000ppm 2. n.d.= NotDetected 3. MDL= MethodDeteclion Limit 4. " - " = NotRegulated 5. '* = Qualitative analysis(Nounit) = 6. Negative Undeteclable/ Positive= Detectable qualitative 7. Testingrangeof asbesto€ analysi6 isfromlessthan0.'10lo to 100%.Thejudgmentcriterion: asbestos fibe6 beingfoundis shownas "Positive'; asbeslos fibersnotbeingfoundis shownas "Negative',. PFOSRofercnceInformation: POP3- (EU)7572010 Outlawing PFOSas sub€tances (1oppm), products or pr€parations in concentrations above0.001o,4 in semi-finished or adiclesor partsat a levelabo,/e0.1%(1000ppm), in textilesor othercoatedmaterials above1Ug/m,. M r t ! bi €pqrdA onrvo hi *_dq3l!.r{ -hr d reml u'nor o i.'trh'','",,;.d';"-.;";'',.''"!].""o..":j.;;;;."'s.**-'*"*''"""***" @cd "lne dd codtoonre 61-s do umdtd ' b E Mo1{ oo;-c r d ;; A;;;;; ffi; A;;;n.;6d "'w:ge -'m* -d rddr*m o^"*,ru" 'd.*,r-*" *ori, ddm .qia 6.e ma;;aiiinii. ra} F"'o pa.vr3oFF F ub' Brdt* i*fi;;i;;d;;i'.*rv-d.iilFeiarocr€ds i E ; 9 ' * " t s . - e e @ 5 . o J h " ' . d . i d n - . l i ' i 5 d d m | l f i;:;G;::.;ri;tr;;dar.*m"[email protected];;;i;i;ip;;re;th,'doerd6mrd'.rao|e"-'ru,o"G*ddo ':id;;;;iN -i'r du d i'ffi:;irg* 9"::.;tr;,.";T;%"j I i iIfta'i4;1t1r H r r ' ' € i r , r l ; ; * i i ; z t ; t iewr.dhdut-rtu*Nryr.rd.lqrriwln/ii 1 . a a 6 o ? ) 2 e , ;, $ i w , , - _ . _ . _ * _ _ _ Test Report No.: CE/201313196 Dale: 2013101122Paoe: 14ol 29 rflfltt|lItttlll CERAMTEC GMBH GESCFIAFTSBEREICH MULTIFUNKTIONSKERAI'IK,LUITPOLDSTRABE 15, 91207LAUF 1) Thesesamples weredissolved totallyby pre-conditioning methodaccording to beloa/flowchart. ( Cf' test methode)duded) 2) Nameof the peEonwhomademeasurement: Climbg|eat Yang Nameof the personin chargeofmeasuremer : TroyChang of measuremer cf. SampleMeasulement Addappropriate amount of digestion reagent Acid digestionby suitableacid deoended on different samDl€ material (a6 below table) Heatto appopriate temperatureto extract '1) AlkaliFusion Cool, filter digestiate throughfilter 2) HCltodissolve SamDlel\Iaterial Add diphenyl-carbazide for colordevelopment Acid Diqestion Aqua reqi€.HNO3.HCl,HF,H,O, 6older Sleel,coppetaluminum, HNO3/HF Glass palladium, Gold.platinum, cgramic Aqua reqia Silver Plastic Others measurethe absorbance at 540 nmby UV-VIS HNOg H,SO1,H,O,, HNO3,HCI Addedappropriatereagentto total digestion digestion eagentandheatto 90-95C m€terial, addalkaline ilotg" : (1)Fornon-metallic pure waterand heatto boiling (2) Forrnetallicmatedal,add J;;"-:#;ilffi1;l ::f.t;ll:::;Llr:::::":":::::ru;il krJi],:T":lT ;.l"ffi;H ;"T:: il,j il, tiliJ,i,"i iii,iir,n-,arg rJtien r61-s do cmdrd s 'o:F do rads' &r hdd' o d'dr'**o i' d'd m *^&heFaM ';i:{-d;;|;ii' 'd'r'1-*" i*ii'i"i,ii;iiJ;;;.*rvma*dnl*|_{'",c|"d!"M;;'i;;i"":.Ftv'-n*.-*"'' _rsod*t -* aojo--.,i j";';o:i;i";;;r h,i'd;;;;iit'i'i,ift ce o-:"iiii-"d;;;;;r -"'"re cil#ii;c;i r -,,i'*r " f6-dnd.kldroB ma oie F" N' e n 4.nro -c F "*tukd NryriiF,.irt'w:i/i l: j a r ':]i ir'rri trtitti TestReport No.: CE/2013/13196Dale: 2013101122Page: 15of 29 1!l ||lt][tttllt CERAI\,ITEC GMBH GESCHAFTSBEREICH MULTIFUNKTIONSKERAMIK.LUITPOLDSTRABE 15. 91207LAUF PFOA/PFOSanalyticalflow cha ot lJltrasonicoxtraction (LC/MS)prccedure I Nameof thepe6onwhomademeasurement: RomanWong I Nameof lhe perconin chargeof measurement: TroyChang Sampleextractionby Ultrasonicextraction (Reference method:USEPA3550C) Concentrate/Dilute Ext€cled solution *"'* 6.:1.o$'i"T'*'-","1:?"f"*1"**"11 3;x;H'Tlr*ydtu :::::i:":"::::" < q M e o ' F d o € d "1:ll. a j ' a v a:::::: abeol ,iili iil"di'ii f';.1i,i-;;"'n" Itr - '016ob ,rs andcoadbhro El or"ngo-*'..**',Jn'';bqo,F6&La4'jd'Adh .'"'. h"'€ ' . ' - , " ;i ;-;;d;'i**"s ;,ia;t'.;a;.;s"s-'-$rib!vF'o atooqaq"ns " .unoe "!b 6 n s rc-ftr "-s"ry. "'*- " ". -i;tn; ioi,'l"ii bc's andtFr"'+ndF 'sff"r' rad oro'o€5 -at b' p.se' rcoroi .!:-(4rdtilti TestReport No.: CE/2013/13'196Dale: 2013101122Pagei 16 of 29 CEMMTECGMBH GESCHAFTSBEREICH [,,lULTIFUNKTIONSKERAMIK,LUITPOLDSTRABE 15, 91207LAUF FgTsanalyticalf lowchaft I I Nameof the p6r6onwhomademeasurementBarryTseng Nameof the personin chargeof measurementi TroyChang Data s _pi'L3l!'+d 1!tt 'por411 if;ruj.",,'*"*.'l";.;,'-'".;J."*"#.;;;"".s"+*".'o"*ai'"l"*-."' oi'iid;rt.n'ct-loio.-"'J4.c6|dtaldcondirs|oE. ri;; idan o na mc. -e, i.d"$d tr *Lh 6tnd,*;,n :-,hbi d:d,,".demni€bn mo ":nddd t; -'B d c."1! 'nqddor. i;,rv l.cmo.nvesats-solhobcrdndlFdrJtnde h ;; oid;dtutu;"tA;nii L."]!.;jjiii#.iii'i''''il'i'r*;-ii'iiji.i,.jioj**'i,itJmni'infdooT+Trsdd-ql-md'!.TPrc!t'.d.G0'|h| ran. oneid.G mavb€ prcleclied ro i too.,r n ral!'rEdq o' th€ 6@ii;i ailiGril;c.i o-,'th;;o;G'do: |ll|lflltItIltllll TestReport No.: CE/2013/13196DaIe: 20131O1n2 P a g e r ' 1 7 o f 2 9 CERAMTEC GMBH GESCHAFTSBEREICH MULTIFUNKTIONSKERAI'IK,LUITPOLDSTMBE 15, 91207LAUF PBB/PBDE analyticalFLOWCHART a I Nameofthepersonwhomademeasurcment: RomanWong Nameofthe personin charged measurement TroyChang Firsttestingprocess-----) prccess.... Optional screen prccess - .> Confimation i I c^.-^ Scre€n.^.r^r analysis r....... |: t t !...1.,... . .... . . r Sampleextraction/ Soxhletmethod ConcentrateJDilute Extracted solution Filter Analysis by GCr/lllS lssueReport tl fillll[t ]l TestReport No.: CEl201313196 Dele:2013101122Page: 18 of 29 trt|[ttt][lttltl CERAMTECGMBH MULTIFUNKTIONSKERAMIK.LUITPOLDSTMBE GESCHAFTSBEREICH 15, 91207 LAUF PCB9analyticalflow chart r I BarryTseng Nameofthe personwhomademeasurement Nameof thepersonin chargeof measurement TroyChang Data Nsrjd.ryriiw?i/r' r .!i'i : lf fii3rff Test Report No.:CE/201?'/13196 Dale: 2013101122Pagei 1I of 29 CEMMTECGIVBH GESCHAFTSBEREICH MULTIFUNfiIONSKERAMIK.LUITPOLDSTRABE 15,91207LAUF tr][tt] |ltt!tl ChlorlnatedPa6ffins anaMical flow chart r r Nameofthe pe6onwhomademeasurement: BarryTseng Nameof thepe6onin ch€rgeof measurementi TroyChang by GC/MS Analysis wEsperformed -. '*":"r' ,ry -q." o^u-.. l i ' l i f i ; ; ; 6 ; ; 1 ; ; i ' ' . , d F a 6 ' s * d @ n d i d ! o i : . d ; i ( - _ r s'*r.R+;**i{*,1;:i:-;; a.Msg.ded q mder,leDn m"u ddd *f. *fred i.:;i6;i.r '60i, ,1i,,;ffi;gx ;g::s r;'f ty"?p,t -ii i i:'J J;;"i b' tp'*' d ' 'eco"' ' os -" * s*r." '-" '.*"*:;1i;h.,;;;s,' ft'oa1t "'6'i^iii a 'dakn ana **-e1 "ii!;ilioii !b r me or is 'nGt.'mon onrr and w t;:t";H[.":1.;T."j Nd rriFi.i, tiiwe, ir'1 .ii iiirrtjiltr {re6rcl2rr7e f 's610?)2ett Test Report No.I CE2013/'13196Date| 2013101122Page| 20 ol 29 l CERAMTEC GMBH [/|ULTIFUNKTIONSKERAMIK.LUITPOLDSTMBE 15. 91207LAUF GESCHAFTSBEREICH |||Itl[[ttt]l Analysis flow chart for deteJminationof Asbestos I I Nameof the personwhomademeasu€ment:Vic{orKao WendyWei Nameof thepe6onin chaqeof measurement: method:EPA600/R-93/116l I Reforence Sampiing with Continuewhenproblsnsarc encountered DS-PLNIand/orfor qualityassurancepurposes lnt€rfe€ncematfix removal Asb€stosidenirficetionby dispersionstaining (DS-PLM) polarizedlightmicroscope ContainingAsbestosr/Positve Asbestosidentfic€tionby x-ray dififactionspedrcrnder(XRD) Not containingAsbesiovNegalrve r!Newhpei.{tftrsii;:r:ri ;i d L "i r i f i r $ TestReport No.: CEl201313196 Date: 201?,101122 Paoe: 21ol 29 [[i[tltl[ttlttl CERAMTEC GMBH GESCHAFTSBEREICH MULTIFUNKTIONSKERAMIK.LUITPOLDSTMBE 15.91207LAUF Analyticalflow cha of Organic-Tin content I I Nameofthepersonwhomademeasurem€nt: GinnyChen Nameof the personin ohargeof measuremenlTroyChang Data o!.r r +'s Fs '€Pon Ft :i""d-"i ri ini "i " o- / ro t€ ! **d a h" c.-"aa uqe.r b a c4e6' cd.bm.r' dm'iic*-. rv -hi1 te aboic.rsm{rua;;;'ii,';'nc".*"'"-"-'**b11 |"tiTha1dod'g€!9n'unoqltni'in-**-.'|i'doe-e..ndbe'edm.LFo *-"1;;:;#;;;;;n'3;*in-r T""';$?;lgXi";[ 's ''trrmoo"€roe' a b€ Fin/i 'i n'i1rCtr'{i TestReport No.: CE/20f 913196 Dale: 2O13|O1D2Page'.22d 29 CERAMTECGMBH 15, 91207 LAUF MULTIFUNKTIONSKERAMIK,LUITPOLDSTRABE GESCI.I,AFTSBEREICH ult[tat][t|rl[ PCNSanalyticalflow chaft I I B€rryTseng Nameofthe pe6onwhomademeasurement TroyChang Nameof thepersonin chaeeof measurement Data ( Nfl raiF .Iv rlivii / r 'lr:i r'El1rjt*ilil TestReport No.: CE201313196 Dale:2013101122Page:23of 29 |r] rIltl][ttttll CERAMTECGMBH 5, 9'1207LAUF MULTIFUNKTIONSKERAMIK,LUITPOLDSTRABE'I GESCHAFTSBEREICH Analyticalflow chat of phthalalacontent I I RomanWong Nameof the personvrhomademeasurement: TroyChang Nameof the personin chargeof measurement: iifFd;:: :';Hi::;i#;;;ffi;:;;,il#d;={;;;*; ;fi li:;tlt:, :":T ffi l.::;;;:ij *..nru'."-o,:"sa* 'ee"e',are[r'L'i;i+?"tm,ii;'.gli"*"1":,C,f";;2,"**5;TffieirT"*f,:il?',:il:l',[%"j ii"ii,ri", o ao.,Y' ''il'inii,.i.".roma'oa..e"r1d.db|er.mdco*bFfo'EF r..rmporEdffrfonrvars{nrsc!m6dIe'f1'1{!done_14ry,-:-:':ii"i1"'xi-""Y:'i"'"1.?":;;:;;;;;i;;;"r;,;:"itm,mi"e.do. mds tu' 6t oololrilne a rr'{t ir e"-'a h;;b" ' ,. *'iliili"iiiiii* "' i n"n .r. n;i r;l:{trrri TestReport No.: CE20'1313196 Date: 2013101 122 Page: 24 ol 29 []l[tu][trlr]r CERAMTEC GMBH GESCHAFTSBEREICH IVULTIFUNKTIONSKERAMIK.LUITPOLDSTRABE 15. 91207LAUF Fo.maldehyde analyticalflow chart I I Nameof the personwhomademeasurement: ScottKu Nameof the personin chargeof measurementTroyChang I Test Method : US EPA8315A' ISO 17226-1) Sampleextr€ction Derivedby DNPHConcentrat€/Dilute Extracted 60lution Data Naraiod.l1y,r.iwmrri1 .i ":r."lrr rllliliri Test Report No.:CEl2013i/13196Dale.2013tO1122Page:25 ol 29 CERAMTECGMBH 15. 91207LAUF GESCI-I,AFTSBEREICH [/|ULTIFUNKTIONSKERAMIK,LUITPOLDSTRABE lfl |lr]tIltttll Analysisflow chartfor determination of PVc in material ! I Nameof thepersonv,/t1o mademeasurement: GinnyChen TroyChang Nameof thepersonin chargeof measurementr Samplepre-trealment Sampleanalyzedby FTIR of C-Clbonding Checkwave-number Data N4tiitsi.tvrriwm/iil::r '' rr i l'r iirfi4tll Test Report No.: CE12013/13196 DaIe| 201310122 Page 26ot29 CERAMTEC GMBH GESCI-IAFTSBEREICH MULTIFUNKTIONSKERAI/|IK,LUITPOLDSTMBE'15, 91207LAUF t[| ttt lllttll DBBTanalyticalfow cha I I Nameof the personwhomademeasurement: RomanWong Nam€ofthepersonin chargeof me€suremenl: TroyChang Data M.+'eFn ? p o n r e ' . ! 0 1 to r ' s a m o a L r ' ' e > c dr 1 s ' € d b p o ' r - { !i;'.:J,H"i'.'',;,".;'l";.:;..+".^*"].i".i-".]*".*--i:'"."..l']','",''"".',"qJsdo'lM$o:-a|M'3!'(od 'iili#.]"i"i,'iinii'i.i'"i-.*saoF"br*'*dco1db..dF|ear6.cooemenla'm4soa. imlioi,liilirll ;rl;ai;;'r;i;;;ii rins o. '*ps oe'46dueo' *! trd{ ort1trdoemdn''iadv !6do rlei..oeleio'.-ry""wlfe'm'bdcs"En'ad;n. i'doe-6nrald onodmo$ ' o t6dsclo.hslt.qaif. g. ,;| ' on * - ii;iiii"*-ijiieii'i -, dd: wg"4 ' ra'rdo o d;;,;;;;d; i;;;; "" s r' comomv)rind'r$ a s o o'snde''-'i b" orctur'd6 | I r.i i i {rir lrlit\t TestReport No.: CE/2013/13196Dale| 2013101122Paoe:27cf29 CERAMTEC GMBH GESCHAFTSBEREICH MULTIFUNKTIONSKERAMIK,LUITPOLDSTRABE 15, 9'1207 LAUF tr] tIltl][ttIl Analytical flow chart of halogen content 1) NameoftheDerson whomademeasurement: RitaChen 2) Nameoftheperson incharge ofmeasur€ment: TroyChang Samplepretreat nent/ Separation Weighting andputtingsamplein cell OrygenBombCombustion / Absorption Dilution to fxed volume Analy6is wasperfomedby lC o.:@so'^ar-.*'s!ftunr'ie-a1o s*i ^ c.*"ic.."*"' -;,"" iKlHS;,. *,J";;;"". "."0 "*"'"a "-uot..-Fqr{ ;;fi;e#;;;;a:;id;;n"'*oFgbh-"*dco]db'6i.iel',.Di''mmuaM6gs@ivfa " ou"..-"***.*,"jn-,i,i,;o|dqo,'16doemn''i.oJ.odd d'-'po"'bnv i;.t'.;a;.;;";' r. .b d - e', he rmed b d€s d ont d sh. Fia ri'o*-Jr4-db'-oolud'*p ".-;;, r iiinir,ili*,i,.;iii unos ,T i!1u sr oo,s:qons b!.fto?Hd.. '.-,,i;:;1i,"*"."*or s"** t o^ " rls6or)ner^ r+s6or2ert o'drd!'n TestReport No.: CE/201313196 Dale:2013101n2 Pag€: 28 of 29 CERAMTEC GMBH GESCHAFTSBEREICH IUULTIFUNKTIONSKERAMIK,LUITPOLDSTMBE I5, 91207LAUF |r] [tt:][tttl|r Analyticalflowchartot volatileorganiccompounds(VOCS) I I Nameof the personwhomademeasurement: ChunWu Nameofthe personin chaeeof measufement : ShinjyhChen (Reference method: US EPA5@11 S€mplepreheaknent Takesampleandputit into headspaceglas6wBre, Bakelhe samplein theoven AnalysiswEsperfomed by GC/MS prs\E|!er{ hn ' E@1 omo' oe r F ' hi EFI .r' oir, o t !! t " -".;."+-* -.; tbid b ik censracondi fts dd,mnr s '.s!ed bvft comoanv "-*i, "*,*"oreo*" ;;;:i;;i|ifudi,dmm6'lutisd6..ftaldcondtrc:lo'cdo .-es ov hdda o h€ oo!'^P- '-e{ss r a*"eo mam ,r -m mo r,i.so'"ri"i*i,'i i;ii'aliii";** -re cr@N' me ?s6 sd' -rv a.a* hh T r-N d ur.d! h{ran. d t ' i* tiiri d rii' -*r- i.':r'":ei,le;i'.Eg; 'T.".'"Hsl'":1H*i#'#..'#j:?'J'hiJT*;."I: C*$ry;.";3,r":;"mlti;t;','4;111v$."1e"'y-grgg"s:?";:$ ,ii +;ir - r {#rli TestReport No.:CE2013/13196D aie.2013101122Page: 29 of 29 CEMMTECGMBH GESC|-|,AFTSBEREICH MULTIFUNKTIONSKERAMIK.LUITPOLDSTRABE 15.91207LAUF Ilfllttt] tttfll ' The teated sample/ part b mark€dby an arow if it'5 shown on the photo. * 13196 " EndofRepo('" c.q':..:u;"''',b;;";;.c;;".b';j.\'.!"r",i];#.o*"*mn*"r.'",:.ao'". i'i.".ni.irurcnro-arao-*.rgbledb-em3AtcoJo.6\.o'E€d o'.g.*'*'.'*,*.'lii-li;'"edr'd'*"';.d,"*. tr {':'*"r$rrl"i 'r.i'S;:ii;rri"i;'*r"ffi #,s+";,"'r';'*";Hjrr"us:lrri ,ffii*lir*:*iia'r; ["*ffifl"ff "'-Tf;5.1;l"t:i"Tijir' "."'.*.''.''''''";;:i'n;iig.oma!"dgF<pmrb| L+s6e)r,err r1sDt0,)2! l?ll q1 Test Report Applicant: Number: LITTELFUSE,INC. 800 E. NORTHWEST HWY A.DIVIETRO/D.UNTIEDT Attn: Date: SHAH00361401 JAN 16, 2013 Sample Description: One (1) submitted sample said to be Grey Wire. Item Name : Wire Tin Plated Cu. Part No. : Element. ************************************************************************************************************************************************************ Tests Conducted: As requested by the applicant, for details refer to attached page(s). ************************************************************************************************************************************************************ To be continued Authorized by: For intertek testing services Ltd., Shanghai Jacob Lin General Manager Page 1 Of 4 Intertek Testing Services Ltd., Shanghai Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233 上海天祥質量技術服務有限公司 上海市宜山路 801 號金陵商務廣場 B 座 200233 Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740 www.intertek.com www.intertek.com.cn Test Report SHAH00361401 Number: Tests Conducted (Ⅰ) Test Result Summary: Result (ppm) (1) Testing Item Heavy Metal Cadmium (Cd) content Lead (Pb) content Mercury (Hg) content 6+ 2 Chromium VI (Cr ) content (mg/kg With 50cm ) ND ND ND Negative (< 0.02) Testing Item Result (ppm) (2) Heavy Metal Cadmium (Cd) content / Plating Lead (Pb) content / Plating Mercury (Hg) content / Plating 6+ 2 Chromium VI (Cr ) content (mg/kg With 50cm ) / Plating ND 60 ND Negative (< 0.02) Remarks: ppm = parts per million = mg/kg ND = not detected 2 @ = Due to the insufficient sample area, reduced total sample surface of 10 cm was used and the dilution factor was adjusted accordingly. 2 mg/kg with 50cm = milligram per kilogram with 50 square centimetre Tested components: (1)Substrate. (2)Plating. Responsibility of Chemist: Dent Fang / Ken He (Ⅱ) RoHS Requirement: Restricted substances Cadmium (Cd) Content Lead (Pb) Content Mercury (Hg) Content 6+ Chromium VI (Cr ) Content Polybrominated Biphenyls (PBBs) Polybrominated Diphenyl Ethers (PBDEs) Limits 0.01% (100ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) The above limits were quoted from RoHS Directive 2011/65/EU for homogeneous material. (Ⅲ) Test Method: Testing item Cadmium (Cd) content Lead (Pb) content Mercury (Hg) content 6+ Chromium VI (Cr ) content Testing method With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in clause 7, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in Annex B, by boiling water extraction and determined by UV-VIS Spectrophotometer. Reporting limit 2 ppm 2 ppm 2 ppm 0.02 2 mg/kg with 50cm Remark:Reporting limit = Quantitation limit of analyze in sample Date Sample Received:Jan.9, 2013 Testing Period:Jan.9, 2013 to Jan.14, 2013 ************************************************************************************************************************************************************ To be continued Page 2 Of 4 Intertek Testing Services Ltd., Shanghai Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233 上海天祥質量技術服務有限公司 上海市宜山路 801 號金陵商務廣場 B 座 200233 Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740 www.intertek.com www.intertek.com.cn Test Report Number: SHAH00361401 Tests Conducted (Ⅳ) MEASUREMENT FLOWCHART: Test for Cd/ Pb/ Hg/Cr (VI)/ PBBs/PBDEs contents Reference standard: IEC 62321 edition 1.0:2008 Sampling/grinding or cutting Cr Cd/Pb/Hg Metal Weigh sample and for different material, digest the sample with *1 appropriate acid No Get 50cm samples Yes Weigh sample and add organic solvent *2 Soxhlet extraction or Solvent extraction Cool and filter the extract Make up with deionized water and add Diphenylcarbazide solution Analyzed by ICP-OES PBBs/PBDEs Definite temp. Extraction 2 Boiling water extraction Make up with deionized water Polymers / electronics Weigh sample and add alkaline solution Spot test Negative Confirm the tested samples are totally dissolved 6+ Concentrate the extract and make up with organic solvent Analyzed by GC-MSD Analyzed by UV-VIS REMARKS: *1: LIST OF APPROPRIATE ACID: MATERIAL Polymers Metals Electronics ACID ADDED FOR DIGESTION HNO3,HCl,HF,H2O2,H3BO3 HNO3,HCL,HF HNO3,HCL,H2O2,HBF4 *2: IF THE RESULT OF SPOT TEST IS POSITIVE, CHROMIUM (VI) WOULD BE DETERMINED AS DETECTED. ************************************************************************************************************************************************************ To be continued Page 3 Of 4 Intertek Testing Services Ltd., Shanghai Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233 上海天祥質量技術服務有限公司 上海市宜山路 801 號金陵商務廣場 B 座 200233 Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740 www.intertek.com www.intertek.com.cn Test Report Number: SHAH00361401 Tests Conducted *********************************************************************************************************************************************************** End of report This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a recommendation for any particular course of action. Intertek does not accept a duty of care or any other responsibility to any person other than the Client in respect of this report and only accepts liability to the Client insofar as is expressly contained in the terms and conditions governing Intertek's provision of services to you. Intertek makes no warranties or representations either express or implied with respect to this report save as provided for in those terms and conditions. We have aimed to conduct the Review on a diligent and careful basis and we do not accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by statute or otherwise, except in the event of our gross negligence or wilful misconduct. Page 4 Of 4 Intertek Testing Services Ltd., Shanghai Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233 上海天祥質量技術服務有限公司 上海市宜山路 801 號金陵商務廣場 B 座 200233 Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740 www.intertek.com www.intertek.com.cn Test Report Applicant: Number : TWNC00285770 Littelfuse Philippines Inc. LIMA Technology Center, Lipa City, Malvar, Batangas Date : Nov 19, 2012 Sample Description: One (1) group of submitted samples said to be : Part Description : Solder (Pb is ≥ 90%) Part Number : 692323 Date Sample Received : Nov 12, 2012 Date Test Started : Nov 13, 2012 Test Conducted : As requested by the applicant, for details please refer to attached pages. Authorized By: On Behalf Of Intertek Testing Services Taiwan Limited K. Y. Liang Director *THJ0285770* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 1 of 6 Number : TWNC00285770 Test Conducted (Ⅰ) Test Result Summary : Result (ppm) Silvery Metal Test Item Heavy Metal Cadmium (Cd) content Lead (Pb) content Mercury (Hg) content Chromium VI (Cr6+) content (mg/kg with 50cm2) ND 910679 ND Negative (< 0.02) Remarks: ppm = Parts per million based on weight of tested sample = mg/kg ND = Not detected < = Less than mg/kg with 50cm2 = milligram per kilogram with 50 square centimetre Negative = A negative test result indicated positive observation was not found at the time of Test. Responsibility of Chemist : Irene Chiou / Kevin Liu Date Sample Received Test Period : Nov 12, 2012 : Nov 13, 2012 To Nov 15, 2012 (Ⅱ) RoHS Limits: Restricted Substances Cadmium (Cd) Content Lead (Pb) Content Mercury (Hg) Content Chromium VI (Cr6+) Content Limits 0.01% (100ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) The above limits were quoted from Annex II of 2011/65/EU for homogeneous material. *THJ0285770* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 2 of 6 Number : TWNC00285770 Test Conducted (Ⅲ) Test Method: Test Item Cadmium (Cd) content Lead (Pb) content Mercury (Hg) content Chromium VI (Cr6+) content Test Method With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in clause 7, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in annex B, by boiling water extraction and determined by UV-Vis Spectrophotometer. Reporting Limit 2 ppm 2 ppm 2 ppm 0.02 mg/kg with 50cm2 Remark: Reporting limit = Quantitation limit of analyte in sample *THJ0285770* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 3 of 6 Number : TWNC00285770 Test Conducted (Ⅳ) Measurement Flowchart: Test For Cd/Pb/Hg/Chromium (VI) Reference Standard:IEC 62321 edition 1.0:2008 Sampling/grinding or cutting Cd/Pb/Hg Cr 6+ Polymers / Electronics Metal For different material, digest the sample with *1 appropriate acid By spot test Negative Confirm the tested samples are totally dissolved Make up with deionized water *2 Weigh sample and add alkaline solution Get 50cm2 sample Definite temp. extraction Boiling water extraction Cool and filter the extract Analyzed by ICP-OES Make up with deionized water and add diphenylcarbazide solution Analyzed by UV-VIS *THJ0285770* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 4 of 6 Number : TWNC00285770 Test Conducted (Ⅳ) Measurement Flowchart: Remarks: *1: List of Appropriate Acid: Acid Added for Digestion Material Polymers HNO3,HCl,HF,H2O2,H3BO3 Metals HNO3,HCl,HF Electronics HNO3,HCl,H2O2,HBF4 *2: If the result of spot test is positive, Chromium VI would be determined as detected. End of Report This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a recommendation for any particular course of action. Intertek does not accept a duty of care or any other responsibility to any person other than the Client in respect of this report and only accepts liability to the Client insofar as is expressly contained in the terms and conditions governing Intertek's provision of services to you. Intertek makes no warranties or representations either express or implied with respect to this report save as provided for in those terms and conditions. We have aimed to conduct the Review on a diligent and careful basis and we do not accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by statute or otherwise, except in the event of our gross negligence or wilful misconduct. *THJ0285770* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 5 of 6 Number : TWNC00285770 Test Conducted Photo *THJ0285770* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 6 of 6 Test Report Applicant: Number : TWNC00286464 Littelfuse Philippines Inc. LIMA Technology Center, Lipa City, Malvar, Batangas Date : Nov 22, 2012 Sample Description: One (1) group of submitted samples said to be : Part Description : Yarn Part Number : 648118_648119_648120 (6481xxx_GLZZxxx) Date Sample Received : Nov 15, 2012 Date Test Started : Nov 16, 2012 Test Conducted : As requested by the applicant, for details please refer to attached pages. Authorized By: On Behalf Of Intertek Testing Services Taiwan Limited K. Y. Liang Director *THJ0286464* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 1 of 7 Number : TWNC00286464 Test Conducted (Ⅰ) Test Result Summary : Result (ppm) White Yarn Test Item Heavy Metal Cadmium (Cd) content Lead (Pb) content Mercury (Hg) content Chromium VI (Cr6+) content Polybrominated Biphenyls (PBBs) Monobrominated Biphenyls (MonoBB) Dibrominated Biphenyls (DiBB) Tribrominated Biphenyls (TriBB) Tetrabrominated Biphenyls (TetraBB) Pentabrominated Biphenyls (PentaBB) Hexabrominated Biphenyls (HexaBB) Heptabrominated Biphenyls (HeptaBB) Octabrominated Biphenyls (OctaBB) Nonabrominated Biphenyls (NonaBB) Decabrominated Biphenyl (DecaBB) Polybrominated Diphenyl Ethers (PBDEs) Monobrominated Diphenyl Ethers (MonoBDE) Dibrominated Diphenyl Ethers (DiBDE) Tribrominated Diphenyl Ethers (TriBDE) Tetrabrominated Diphenyl Ethers (TetraBDE) Pentabrominated Diphenyl Ethers (PentaBDE) Hexabrominated Diphenyl Ethers (HexaBDE) Heptabrominated Diphenyl Ethers (HeptaBDE) Octabrominated Diphenyl Ethers (OctaBDE) Nonabrominated Diphenyl Ethers (NonaBDE) Decabrominated Diphenyl Ether (DecaBDE) Halogen Content Fluorine (F) Chlorine (Cl) Bromine (Br) Iodine (I) ND 14 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND Remarks: ppm = Parts per million based on weight of tested sample = mg/kg ND = Not detected Responsibility of Chemist : Irene Chiou / Kevin Liu / Cathy Chen Date Sample Received Test Period : Nov 15, 2012 : Nov 16, 2012 To Nov 21, 2012 *THJ0286464* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 2 of 7 Number : TWNC00286464 Test Conducted (Ⅱ) RoHS Limits: Restricted Substances Cadmium (Cd) Content Lead (Pb) Content Mercury (Hg) Content Chromium VI (Cr6+) Content Polybrominated Biphenyls (PBBs) Polybrominated Diphenyl Ehters (PBDEs) Limits 0.01% (100ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) The above limits were quoted from Annex II of 2011/65/EU for homogeneous material. (Ⅲ) Test Method: Test Item Cadmium (Cd) content Lead (Pb) content Mercury (Hg) content Chromium VI (Cr6+) content Test Method With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in clause 7, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in annex C, by alkaline digestion and determined by UV-Vis spectrophotometer. Reporting Limit *THJ0286464* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 2 ppm 2 ppm 2 ppm 1 ppm Page 3 of 7 Number : TWNC00286464 Test Conducted (Ⅲ) Test Method: Test Item Polybrominated Biphenyls (PBBs) Polybrominated Diphenyl Ethers (PBDEs) Halogen Content Test Method With reference to IEC 62321 edition 1.0:2008 in annex A, by solvent extraction and determined by GC-MS and further HPLC-DAD confirmation when necessary. With reference to IEC 62321 edition 1.0:2008 in annex A, by solvent extraction and determined by GC-MS and further HPLC-DAD confirmation when necessary. With reference to EN 14582:2007 by calorimetric bomb with oxygen and determined by Ion Chromatograph. Reporting Limit 5 ppm 5 ppm 50 ppm Remark: Reporting limit = Quantitation limit of analyte in sample *THJ0286464* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 4 of 7 Number : TWNC00286464 Test Conducted (Ⅳ) Measurement Flowchart: Test for Cd/Pb/Hg/Chromium (VI)/PBBS/PBDES Contents Reference Standard: IEC 62321 edition 1.0:2008 Sample preparation For non-metal part For metal part Take sample and immerse into Aqua Regia, start to strip plating layer Stop the stripping procedure upon color change completely Take the Aqua solution as plating component and stripped body as substrate component PBBs/PBDEs Weigh sample and add organic solvent By Soxhlet extraction or Solvent extraction Concentrate the extract and make up with organic solvent Cr 6+ Substrate Cd/Pb/Hg Weigh sample and add alkaline solution For different material, digest the sample with *1 appropriate acid Plating Cr 6+ By spot test Definite temp. extraction Cool and filter the extract Confirm the tested samples are totally dissolved Negative Get 50cm2 sample Make up with deionized water By boiling water extraction Analyzed by ICP-OES Analyzed by GC-MSD Remarks: *1: List of Appropriate Acid: Material Polymers Metals Electronics *2 Make up with deionized water and add diphenyl-carbazide solution Analyzed by UV-VIS Acid Added for Digestion HNO3,HCl,HF,H2O2,H3BO3 HNO3,HCl,HF HNO3,HCl,H2O2,HBF4 *2: If the result of spot test is positive, Chromium VI would be determined as detected. *THJ0286464* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 5 of 7 Number : TWNC00286464 Test Conducted (Ⅳ) Measurement Flowchart: Test for Halogen Content Reference Standard:EN 14582 Sampling/grinding or cutting Add absorbent in a combustion flask & place weighed sample in equipment Fill oxygen into calorimetric bomb Ignite then leave the bomb at room temperature Transfer the absorbent into a volumetric flask Make up with deionized water Analyzed by ion chromatography End of Report This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a recommendation for any particular course of action. Intertek does not accept a duty of care or any other responsibility to any person other than the Client in respect of this report and only accepts liability to the Client insofar as is expressly contained in the terms and conditions governing Intertek's provision of services to you. Intertek makes no warranties or representations either express or implied with respect to this report save as provided for in those terms and conditions. We have aimed to conduct the Review on a diligent and careful basis and we do not accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by statute or otherwise, except in the event of our gross negligence or wilful misconduct. *THJ0286464* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 6 of 7 Number : TWNC00286464 Test Conducted Photo *THJ0286464* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 7 of 7 Test Report Applicant: Number : TWNC00285760 Littelfuse Philippines Inc. LIMA Technology Center, Lipa City, Malvar, Batangas Date : Nov 19, 2012 Sample Description: One (1) group of submitted samples said to be : Part Description : Yarn Part Number : 648106-001 Date Sample Received : Nov 12, 2012 Date Test Started : Nov 13, 2012 Test Conducted : As requested by the applicant, for details please refer to attached pages. Authorized By: On Behalf Of Intertek Testing Services Taiwan Limited K. Y. Liang Director *THJ0285760* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 1 of 8 Number : TWNC00285760 Test Conducted (Ⅰ) Test Result Summary : Result (ppm) White Yarn Test Item Heavy Metal Cadmium (Cd) content Lead (Pb) content Mercury (Hg) content Chromium VI (Cr6+) content Polybrominated Biphenyls (PBBs) Monobrominated Biphenyls (MonoBB) Dibrominated Biphenyls (DiBB) Tribrominated Biphenyls (TriBB) Tetrabrominated Biphenyls (TetraBB) Pentabrominated Biphenyls (PentaBB) Hexabrominated Biphenyls (HexaBB) Heptabrominated Biphenyls (HeptaBB) Octabrominated Biphenyls (OctaBB) Nonabrominated Biphenyls (NonaBB) Decabrominated Biphenyl (DecaBB) Polybrominated Diphenyl Ethers (PBDEs) Monobrominated Diphenyl Ethers (MonoBDE) Dibrominated Diphenyl Ethers (DiBDE) Tribrominated Diphenyl Ethers (TriBDE) Tetrabrominated Diphenyl Ethers (TetraBDE) Pentabrominated Diphenyl Ethers (PentaBDE) Hexabrominated Diphenyl Ethers (HexaBDE) Heptabrominated Diphenyl Ethers (HeptaBDE) Octabrominated Diphenyl Ethers (OctaBDE) Nonabrominated Diphenyl Ethers (NonaBDE) Decabrominated Diphenyl Ether (DecaBDE) ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND *THJ0285760* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 2 of 8 Number : TWNC00285760 Test Conducted (Ⅰ) Test Result Summary : Result (ppm) White Yarn Test Item Halogen Content Fluorine (F) Chlorine (Cl) Bromine (Br) Iodine (I) ND ND ND ND Remarks: ppm = Parts per million based on weight of tested sample = mg/kg ND = Not detected Responsibility of Chemist : Irene Chiou / Kevin Liu / Cathy Chen Date Sample Received Test Period : Nov 12, 2012 : Nov 13, 2012 To Nov 15, 2012 (Ⅱ) RoHS Limits: Restricted Substances Cadmium (Cd) Content Lead (Pb) Content Mercury (Hg) Content Chromium VI (Cr6+) Content Polybrominated Biphenyls (PBBs) Polybrominated Diphenyl Ehters (PBDEs) Limits 0.01% (100ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) The above limits were quoted from Annex II of 2011/65/EU for homogeneous material. *THJ0285760* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 3 of 8 Number : TWNC00285760 Test Conducted (Ⅲ) Test Method: Test Item Cadmium (Cd) content Lead (Pb) content Mercury (Hg) content Chromium VI (Cr6+) content Polybrominated Biphenyls (PBBs) Polybrominated Diphenyl Ethers (PBDEs) Halogen Content Test Method With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in clause 7, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in annex C, by alkaline digestion and determined by UV-Vis spectrophotometer. With reference to IEC 62321 edition 1.0:2008 in annex A, by solvent extraction and determined by GC-MS and further HPLC-DAD confirmation when necessary. With reference to IEC 62321 edition 1.0:2008 in annex A, by solvent extraction and determined by GC-MS and further HPLC-DAD confirmation when necessary. With reference to EN 14582:2007 by calorimetric bomb with oxygen and determined by Ion Chromatograph. Reporting Limit 2 ppm 2 ppm 2 ppm 1 ppm 5 ppm 5 ppm 50 ppm Remark: Reporting limit = Quantitation limit of analyte in sample *THJ0285760* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 4 of 8 Number : TWNC00285760 Test Conducted (Ⅳ) Measurement Flowchart: Test for Cd/Pb/Hg/Chromium (VI)/PBBS/PBDES Contents Reference Standard: IEC 62321 edition 1.0:2008 Sample preparation For non-metal part For metal part Take sample and immerse into Aqua Regia, start to strip plating layer Stop the stripping procedure upon color change completely Take the Aqua solution as plating component and stripped body as substrate component PBBs/PBDEs Weigh sample and add organic solvent By Soxhlet extraction or Solvent extraction Concentrate the extract and make up with organic solvent Analyzed by GC-MSD Cr 6+ Substrate Cd/Pb/Hg Weigh sample and add alkaline solution For different material, digest the sample with *1 appropriate acid Plating Cr 6+ By spot test Definite temp. extraction Cool and filter the extract Confirm the tested samples are totally dissolved Negative *2 Get 50cm2 sample Make up with deionized water By boiling water extraction Analyzed by ICP-OES Make up with deionized water and add diphenyl-carbazide solution Analyzed by UV-VIS *THJ0285760* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 5 of 8 Number : TWNC00285760 Test Conducted (Ⅳ) Measurement Flowchart: Remarks: *1: List of Appropriate Acid: Material Polymers Metals Electronics Acid Added for Digestion HNO3,HCl,HF,H2O2,H3BO3 HNO3,HCl,HF HNO3,HCl,H2O2,HBF4 *2: If the result of spot test is positive, Chromium VI would be determined as detected. *THJ0285760* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 6 of 8 Number : TWNC00285760 Test Conducted (Ⅳ) Measurement Flowchart: Test for Halogen Content Reference Standard:EN 14582 Sampling/grinding or cutting Add absorbent in a combustion flask & place weighed sample in equipment Fill oxygen into calorimetric bomb Ignite then leave the bomb at room temperature Transfer the absorbent into a volumetric flask Make up with deionized water Analyzed by ion chromatography End of Report This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a recommendation for any particular course of action. Intertek does not accept a duty of care or any other responsibility to any person other than the Client in respect of this report and only accepts liability to the Client insofar as is expressly contained in the terms and conditions governing Intertek's provision of services to you. Intertek makes no warranties or representations either express or implied with respect to this report save as provided for in those terms and conditions. We have aimed to conduct the Review on a diligent and careful basis and we do not accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by statute or otherwise, except in the event of our gross negligence or wilful misconduct. *THJ0285760* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 7 of 8 Number : TWNC00285760 Test Conducted Photo *THJ0285760* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 8 of 8 Test Report Applicant: Number : TWNC00285761 Littelfuse Philippines Inc. LIMA Technology Center, Lipa City, Malvar, Batangas Date : Nov 19, 2012 Sample Description: One (1) group of submitted samples said to be : Part Description : Yarn Part Number : 648112-001 Date Sample Received : Nov 12, 2012 Date Test Started : Nov 13, 2012 Test Conducted : As requested by the applicant, for details please refer to attached pages. Authorized By: On Behalf Of Intertek Testing Services Taiwan Limited K. Y. Liang Director *THJ0285761* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 1 of 8 Number : TWNC00285761 Test Conducted (Ⅰ) Test Result Summary : Result (ppm) Submitted Samples Test Item Heavy Metal Cadmium (Cd) content Lead (Pb) content Mercury (Hg) content Chromium VI (Cr6+) content Polybrominated Biphenyls (PBBs) Monobrominated Biphenyls (MonoBB) Dibrominated Biphenyls (DiBB) Tribrominated Biphenyls (TriBB) Tetrabrominated Biphenyls (TetraBB) Pentabrominated Biphenyls (PentaBB) Hexabrominated Biphenyls (HexaBB) Heptabrominated Biphenyls (HeptaBB) Octabrominated Biphenyls (OctaBB) Nonabrominated Biphenyls (NonaBB) Decabrominated Biphenyl (DecaBB) Polybrominated Diphenyl Ethers (PBDEs) Monobrominated Diphenyl Ethers (MonoBDE) Dibrominated Diphenyl Ethers (DiBDE) Tribrominated Diphenyl Ethers (TriBDE) Tetrabrominated Diphenyl Ethers (TetraBDE) Pentabrominated Diphenyl Ethers (PentaBDE) Hexabrominated Diphenyl Ethers (HexaBDE) Heptabrominated Diphenyl Ethers (HeptaBDE) Octabrominated Diphenyl Ethers (OctaBDE) Nonabrominated Diphenyl Ethers (NonaBDE) Decabrominated Diphenyl Ether (DecaBDE) ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND *THJ0285761* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 2 of 8 Number : TWNC00285761 Test Conducted (Ⅰ) Test Result Summary : Result (ppm) Submitted Samples Test Item Halogen Content Fluorine (F) Chlorine (Cl) Bromine (Br) Iodine (I) ND ND ND ND Remarks: ppm = Parts per million based on weight of tested sample = mg/kg ND = Not detected Responsibility of Chemist : Irene Chiou / Kevin Liu / Cathy Chen Date Sample Received Test Period : Nov 12, 2012 : Nov 13, 2012 To Nov 15, 2012 (Ⅱ) RoHS Limits: Restricted Substances Cadmium (Cd) Content Lead (Pb) Content Mercury (Hg) Content Chromium VI (Cr6+) Content Polybrominated Biphenyls (PBBs) Polybrominated Diphenyl Ehters (PBDEs) Limits 0.01% (100ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) The above limits were quoted from Annex II of 2011/65/EU for homogeneous material. *THJ0285761* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 3 of 8 Number : TWNC00285761 Test Conducted (Ⅲ) Test Method: Test Item Cadmium (Cd) content Lead (Pb) content Mercury (Hg) content Chromium VI (Cr6+) content Polybrominated Biphenyls (PBBs) Polybrominated Diphenyl Ethers (PBDEs) Halogen Content Test Method With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in clause 7, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in annex C, by alkaline digestion and determined by UV-Vis spectrophotometer. With reference to IEC 62321 edition 1.0:2008 in annex A, by solvent extraction and determined by GC-MS and further HPLC-DAD confirmation when necessary. With reference to IEC 62321 edition 1.0:2008 in annex A, by solvent extraction and determined by GC-MS and further HPLC-DAD confirmation when necessary. With reference to EN 14582:2007 by calorimetric bomb with oxygen and determined by Ion Chromatograph. Reporting Limit 2 ppm 2 ppm 2 ppm 1 ppm 5 ppm 5 ppm 50 ppm Remark: Reporting limit = Quantitation limit of analyte in sample *THJ0285761* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 4 of 8 Number : TWNC00285761 Test Conducted (Ⅳ) Measurement Flowchart: Test for Cd/Pb/Hg/Chromium (VI)/PBBS/PBDES Contents Reference Standard: IEC 62321 edition 1.0:2008 Sample preparation For non-metal part For metal part Take sample and immerse into Aqua Regia, start to strip plating layer Stop the stripping procedure upon color change completely Take the Aqua solution as plating component and stripped body as substrate component PBBs/PBDEs Weigh sample and add organic solvent By Soxhlet extraction or Solvent extraction Concentrate the extract and make up with organic solvent Analyzed by GC-MSD Cr 6+ Substrate Cd/Pb/Hg Weigh sample and add alkaline solution For different material, digest the sample with *1 appropriate acid Plating Cr 6+ By spot test Definite temp. extraction Cool and filter the extract Confirm the tested samples are totally dissolved Negative *2 Get 50cm2 sample Make up with deionized water By boiling water extraction Analyzed by ICP-OES Make up with deionized water and add diphenyl-carbazide solution Analyzed by UV-VIS *THJ0285761* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 5 of 8 Number : TWNC00285761 Test Conducted (Ⅳ) Measurement Flowchart: Remarks: *1: List of Appropriate Acid: Material Polymers Metals Electronics Acid Added for Digestion HNO3,HCl,HF,H2O2,H3BO3 HNO3,HCl,HF HNO3,HCl,H2O2,HBF4 *2: If the result of spot test is positive, Chromium VI would be determined as detected. *THJ0285761* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 6 of 8 Number : TWNC00285761 Test Conducted (Ⅳ) Measurement Flowchart: Test for Halogen Content Reference Standard:EN 14582 Sampling/grinding or cutting Add absorbent in a combustion flask & place weighed sample in equipment Fill oxygen into calorimetric bomb Ignite then leave the bomb at room temperature Transfer the absorbent into a volumetric flask Make up with deionized water Analyzed by ion chromatography End of Report This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a recommendation for any particular course of action. Intertek does not accept a duty of care or any other responsibility to any person other than the Client in respect of this report and only accepts liability to the Client insofar as is expressly contained in the terms and conditions governing Intertek's provision of services to you. Intertek makes no warranties or representations either express or implied with respect to this report save as provided for in those terms and conditions. We have aimed to conduct the Review on a diligent and careful basis and we do not accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by statute or otherwise, except in the event of our gross negligence or wilful misconduct. *THJ0285761* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 7 of 8 Number : TWNC00285761 Test Conducted Photo *THJ0285761* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 8 of 8 Test Report Applicant: Littelfuse Philippines Inc. LIMA Technology Center, Lipa City, Malvar, Batangas Number : TWNC00306991 Date : Apr 16, 2013 Sample Description: One (1) group of submitted samples said to be : Part Description : Black Ink Part Number : 425809 Date Sample Received : Apr 10, 2013 Date Test Started : Apr 11, 2013 Test Conducted : As requested by the applicant, for details please refer to attached pages. Authorized by: On Behalf of Intertek Testing Services Taiwan Limited K. Y. Liang Director *THJ0306991* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C. 全國公證檢驗股份有限公司 11492 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 1 of 10 Number : TWNC00306991 Test Conducted (Ⅰ) Test Result Summary: Result Test Item Unit Test Method RL Black paste Heavy Metal ND 2 ND 2 ND 2 ND 1 ppm ND 5 ppm ND 5 ppm ND 5 ND 5 ND 5 ND 5 ND 5 ppm ND 5 ppm ND 5 ppm ND 5 Cadmium (Cd) Content ppm Lead (Pb) Content ppm Mercury (Hg) Content ppm Chromium VI (Cr6+) Content ppm Polybrominated Biphenyls (PBBs) Monobrominated Biphenyls (MonoBB) Dibrominated Biphenyls (DiBB) Tribrominated Biphenyls (TriBB) Tetrabrominated Biphenyls (TetraBB) Pentabrominated Biphenyls (PentaBB) Hexabrominated Biphenyls (HexaBB) Heptabrominated Biphenyls (HeptaBB) Octabrominated Biphenyls (OctaBB) Nonabrominated Biphenyls (NonaBB) Decabrominated Biphenyl (DecaBB) With reference to IEC 62321: 2008, by microwave digestion and determined by ICP-OES. With reference to IEC 62321: 2008, by microwave digestion and determined by ICP-OES. With reference to IEC 62321: 2008, by microwave digestion and determined by ICP-OES. With reference to IEC 62321: 2008, by alkaline digestion and determined by UV-Vis Spectrophotometer. ppm ppm ppm ppm With reference to IEC 62321: 2008, by solvent extraction and determined by GC-MS and further HPLC-DAD confirmation when necessary. *THJ0306991* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C. 全國公證檢驗股份有限公司 11492 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 2 of 10 Number : TWNC00306991 Test Conducted Result Test Item Unit Test Method RL Black paste Polybrominated Diphenyl Ethers (PBDEs) Monobrominated Diphenyl Ethers ppm (MonoBDE) Dibrominated Diphenyl Ethers ppm (DiBDE) Tribrominated Diphenyl Ethers ppm (TriBDE) Tetrabrominated Diphenyl ppm Ethers (TetraBDE) Pentabrominated Diphenyl ppm Ethers (PentaBDE) Hexabrominated Diphenyl Ethers ppm (HexaBDE) Heptabrominated Diphenyl ppm Ethers (HeptaBDE) Octabrominated Diphenyl Ethers ppm (OctaBDE) Nonabrominated Diphenyl Ethers ppm (NonaBDE) Decabrominated Diphenyl Ether ppm (DecaBDE) Phthalates Di(2-ethylhexyl) Phthalate ppm (DEHP) Dibutyl Phthalate (DBP) ppm Benzyl Butyl Phthalate (BBP) ppm Halogen Content Fluorine (F) ppm Chlorine (Cl) ppm Bromine (Br) ppm Iodine (I) ppm Others Hexabromo cyclododecane (HBCDD) ppm With reference to IEC 62321: 2008, by solvent extraction and determined by GC-MS and further HPLC-DAD confirmation when necessary. ND 5 ND 5 ND 5 ND 5 ND 5 ND 5 ND 5 ND 5 ND 5 ND 5 With reference to EN 14372: 2004, by solvent extraction and determined by GC-MS. ND 50 ND ND 50 50 With reference to EN 14582:2007 by calorimetric bomb with oxygen and determined by Ion Chromatograph. ND ND ND ND 50 50 50 50 With reference to USEPA 3540C, by solvent extraction and determined by GC-MS. ND 10 *THJ0306991* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C. 全國公證檢驗股份有限公司 11492 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 3 of 10 Number : TWNC00306991 Test Conducted Remarks: ppm ND RL = parts per million based on wet weight of tested sample = mg/kg = Not detected = Reporting Limit, Quantitation limit of analyte in sample Responsibility of Chemist: Date Sample Received Test Period Kevin Liu/ Irene Chiou/ Vico Lin : Apr 10, 2013 : Apr 11, 2013 to Apr 15, 2013 (Ⅱ) Limit: RoHS Limit Restricted Substances Cadmium (Cd) content Lead (Pb) content Mercury (Hg) content Chromium VI (Cr6+) content Polybrominated Biphenyls (PBBs) Polybrominated Diphenyl Ehters (PBDEs) Limits 0.01% (100ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) The above limits were quoted from Annex II of 2011/65/EU for homogeneous material. *THJ0306991* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C. 全國公證檢驗股份有限公司 11492 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 4 of 10 Number : TWNC00306991 Test Conducted (Ⅲ) Measurement Flowchart: Test for Cd/Pb/Hg/Chromium (VI)/PBBS/PBDES Contents Reference Standard: IEC 62321 edition 1.0:2008 Sample preparation For non-metal part For metal part Take sample and immerse into Aqua Regia, start to strip plating layer Stop the stripping procedure upon color change completely Take the Aqua solution as plating component and stripped body as substrate component PBBs/PBDEs Weigh sample and add organic solvent By Soxhlet extraction or Solvent extraction Concentrate the extract and make up with organic solvent Analyzed by GC-MSD Cr 6+ Substrate Cd/Pb/Hg Weigh sample and add alkaline solution For different material, digest the sample with *1 appropriate acid Plating Cr 6+ By spot test Definite temp. extraction Cool and filter the extract Confirm the tested samples are totally dissolved Negative *2 Get 50cm2 sample Make up with deionized water By boiling water extraction Analyzed by ICP-OES Make up with deionized water and add diphenyl-carbazide solution Analyzed by UV-VIS *THJ0306991* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C. 全國公證檢驗股份有限公司 11492 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 5 of 10 Number : TWNC00306991 Test Conducted Remarks: *1: List of Appropriate Acid: Material Polymers Metals Electronics Acid Added for Digestion HNO3,HCl,HF,H2O2,H3BO3 HNO3,HCl,HF HNO3,HCl,H2O2,HBF4 *2: If the result of spot test is positive, Chromium VI would be determined as detected. *THJ0306991* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C. 全國公證檢驗股份有限公司 11492 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 6 of 10 Number : TWNC00306991 Test Conducted Test for Halogen Content Reference Standard:EN 14582 Sampling/grinding or cutting Add absorbent in a combustion flask & place weighed sample in equipment Fill oxygen into calorimetric bomb Ignite then leave the bomb at room temperature Transfer the absorbent into a volumetric flask Make up with deionized water Analyzed by ion chromatography *THJ0306991* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C. 全國公證檢驗股份有限公司 11492 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 7 of 10 Number : TWNC00306991 Test Conducted Test For Phthalates Contents Reference Method: EN 14372: 2004 Sampling/grinding or cutting Weigh sample and add organic solvent By solvent extraction Concentrate the extract and make up with organic solvent Analyzed by GC-MSD *THJ0306991* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C. 全國公證檢驗股份有限公司 11492 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 8 of 10 Number : TWNC00306991 Test Conducted Test For Hexabromocyclododecane (HBCDD) Reference Standard:USEPA 3540C Sampling/grinding or cutting Weigh sample and add organic solvent By soxhlet extraction Concentrate the extract and make up with organic solvent Analyzed by GC-MSD End of Report This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a recommendation for any particular course of action. Intertek does not accept a duty of care or any other responsibility to any person other than the Client in respect of this report and only accepts liability to the Client insofar as is expressly contained in the terms and conditions governing Intertek's provision of services to you. Intertek makes no warranties or representations either express or implied with respect to this report save as provided for in those terms and conditions. We have aimed to conduct the Review on a diligent and careful basis and we do not accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by statute or otherwise, except in the event of our gross negligence or wilful misconduct. *THJ0306991* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C. 全國公證檢驗股份有限公司 11492 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 9 of 10 Number : TWNC00306991 Test Conducted Photo *THJ0306991* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C. 全國公證檢驗股份有限公司 11492 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 10 of 10