ANALYTICAL REPORT Job Number: 660-24356-1 Job Description: Raytheon For: ARCADIS U.S., Inc. 14055 Riveredge Drive Suite 400 Tampa, FL 33637 Attention: Mr. Gus Suarez _____________________________________________ Natalie Tafuni Project Manager I [email protected] 08/01/2008 Methods: FDEP, DOH Certification #: E84282, E81005 These test results meet all the requirements of NELAC unless specified in the case narrative. All questions regarding this test report should be directed to the TestAmerica Project Manager who signed this test report. The estimated uncertainty associated with these reported results is available upon request. The results contained in this test report relate only to these samples included herein. TestAmerica Laboratories, Inc. TestAmerica Tampa 6712 Benjamin Road, Suite 100, Tampa, FL 33634 Tel (813) 885-7427 Fax (813) 885-7049 www.testamericainc.com Page 1 of 42 Job Narrative 660-J24356-1 Comments No additional comments. Receipt All samples were received in good condition within temperature requirements. The samples were picked up at the Raytheon site by courier. The courier did not sign off as relinquishing the samples to the lab. Page 2 of 42 EXECUTIVE SUMMARY - Detections Client: ARCADIS U.S., Inc. Lab Sample ID Analyte 660-24356-6 Benzene Toluene Acetone m-Xylene & p-Xylene Job Number: 660-24356-1 Client Sample ID Result / Qualifier Reporting Limit Units Method ug/L ug/L ug/L ug/L 8260B 8260B 8260B 8260B CP-110(63'-65')_073008 1.2 2.6 34 1.1 I TestAmerica Tampa Page 3 of 42 1.0 1.0 20 2.0 METHOD SUMMARY Client: ARCADIS U.S., Inc. Description Job Number: 660-24356-1 Lab Location Method Preparation Method Volatile Organic Compounds by GC/MS Purge-and-Trap TAL TAM TAL TAM SW846 8260B SW846 5030B 1,4-Dioxane by SIM/Isotopic Dilution Purge-and-Trap TAL TAM TAL TAM SW846 8260C SIM/ID SW846 5030B Matrix Water Lab References: TAL TAM = TestAmerica Tampa Method References: SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates. TestAmerica Tampa Page 4 of 42 METHOD / ANALYST SUMMARY Client: ARCADIS U.S., Inc. Job Number: 660-24356-1 Method Analyst SW846 8260B SW846 8260B Carlson, Robyn Mathew, Pinky RC PM SW846 8260C SIM/ID SW846 8260C SIM/ID Carlson, Robyn Mathew, Pinky RC PM TestAmerica Tampa Page 5 of 42 Analyst ID SAMPLE SUMMARY Client: ARCADIS U.S., Inc. Job Number: 660-24356-1 Date/Time Sampled Date/Time Received Water 07/30/2008 0000 07/30/2008 1430 Water Water Water Water Water 07/30/2008 07/30/2008 07/30/2008 07/30/2008 07/30/2008 07/30/2008 07/30/2008 07/30/2008 07/30/2008 07/30/2008 Lab Sample ID Client Sample ID Client Matrix 660-24356-1 Trip Blank(7/30/08)_073008 CP-110(10'-12')_073008 CP-110(32'-34')_073008 CP-110(46'-48')_073008 CP-110(53'-55')_073008 CP-110(63'-65')_073008 660-24356-2 660-24356-3 660-24356-4 660-24356-5 660-24356-6 TestAmerica Tampa Page 6 of 42 0840 0909 0936 1005 1200 1430 1430 1430 1430 1430 SAMPLE RESULTS TestAmerica Tampa Page 7 of 42 Analytical Data Client: ARCADIS U.S., Inc. Job Number: 660-24356-1 Client Sample ID: Trip Blank(7/30/08)_073008 Lab Sample ID: Client Matrix: 660-24356-1 Water Date Sampled: Date Received: 07/30/2008 0000 07/30/2008 1430 8260B Volatile Organic Compounds by GC/MS Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260B 5030B 1.0 07/30/2008 2155 07/30/2008 2155 Analyte Benzene Bromobenzene 1,2-Dichlorobenzene Chlorobromomethane Dichlorobromomethane Bromoform Bromomethane n-Butylbenzene sec-Butylbenzene tert-Butylbenzene Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene Chlorodibromomethane 1,2-Dibromo-3-Chloropropane Ethylene Dibromide Dibromomethane 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans-1,3-Dichloropropene Ethylbenzene Hexachlorobutadiene Isopropylbenzene 4-Isopropyltoluene Methylene Chloride Naphthalene N-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane TestAmerica Tampa Analysis Batch: 660-65567 Result (ug/L) 0.50 0.58 0.44 0.58 0.35 0.58 2.5 0.67 0.63 0.84 0.42 0.63 2.5 0.90 1.0 0.65 0.52 0.34 2.5 0.50 0.41 0.64 0.52 2.5 0.52 0.57 0.45 0.65 0.44 0.52 0.39 0.36 0.31 0.14 0.14 0.44 0.40 0.19 0.69 4.0 2.5 0.59 0.98 0.63 Page 8 of 42 Instrument ID: BVMJ GC/MS Lab File ID: 3JG3019.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U MDL 0.50 0.58 0.44 0.58 0.35 0.58 2.5 0.67 0.63 0.84 0.42 0.63 2.5 0.90 1.0 0.65 0.52 0.34 2.5 0.50 0.41 0.64 0.52 2.5 0.52 0.57 0.45 0.65 0.44 0.52 0.39 0.36 0.31 0.14 0.14 0.44 0.40 0.19 0.69 4.0 2.5 0.59 0.98 0.63 PQL 1.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 4.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 5.0 5.0 1.0 2.0 1.0 Analytical Data Client: ARCADIS U.S., Inc. Job Number: 660-24356-1 Client Sample ID: Trip Blank(7/30/08)_073008 Lab Sample ID: Client Matrix: 660-24356-1 Water Date Sampled: Date Received: 07/30/2008 0000 07/30/2008 1430 8260B Volatile Organic Compounds by GC/MS Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260B 5030B 1.0 07/30/2008 2155 07/30/2008 2155 Analyte 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl chloride o-Xylene Acetone 2-Butanone (MEK) 4-Methyl-2-pentanone (MIBK) Carbon disulfide 2-Hexanone Methyl tert-butyl ether m-Xylene & p-Xylene Analysis Batch: 660-65567 Result (ug/L) 0.15 0.50 0.51 0.77 0.58 0.46 0.47 0.50 2.5 0.18 0.86 0.54 0.50 0.50 9.9 8.4 3.8 0.85 4.4 0.44 0.60 Surrogate Toluene-d8 (Surr) 4-Bromofluorobenzene Dibromofluoromethane %Rec 90 96 84 TestAmerica Tampa Page 9 of 42 Instrument ID: BVMJ GC/MS Lab File ID: 3JG3019.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U U U U U U U U U U U U U U U U U U U U U MDL 0.15 0.50 0.51 0.77 0.58 0.46 0.47 0.50 2.5 0.18 0.86 0.54 0.50 0.50 9.9 8.4 3.8 0.85 4.4 0.44 0.60 PQL 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 20 10 10 1.0 10 1.0 2.0 Acceptance Limits 77 - 122 74 - 126 70 - 130 Analytical Data Client: ARCADIS U.S., Inc. Job Number: 660-24356-1 Client Sample ID: CP-110(10'-12')_073008 Lab Sample ID: Client Matrix: 660-24356-2 Water Date Sampled: Date Received: 07/30/2008 0840 07/30/2008 1430 8260B Volatile Organic Compounds by GC/MS Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260B 5030B 1.0 07/31/2008 1111 07/31/2008 1111 Analyte Benzene Bromobenzene 1,2-Dichlorobenzene Chlorobromomethane Dichlorobromomethane Bromoform Bromomethane n-Butylbenzene sec-Butylbenzene tert-Butylbenzene Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene Chlorodibromomethane 1,2-Dibromo-3-Chloropropane Ethylene Dibromide Dibromomethane 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans-1,3-Dichloropropene Ethylbenzene Hexachlorobutadiene Isopropylbenzene 4-Isopropyltoluene Methylene Chloride Naphthalene N-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane TestAmerica Tampa Analysis Batch: 660-65594 Result (ug/L) 0.50 0.58 0.44 0.58 0.35 0.58 2.5 0.67 0.63 0.84 0.42 0.63 2.5 0.90 1.0 0.65 0.52 0.34 2.5 0.50 0.41 0.64 0.52 2.5 0.52 0.57 0.45 0.65 0.44 0.52 0.39 0.36 0.31 0.14 0.14 0.44 0.40 0.19 0.69 4.0 2.5 0.59 0.98 0.63 Page 10 of 42 Instrument ID: BVMJ GC/MS Lab File ID: 3JG3052.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U MDL 0.50 0.58 0.44 0.58 0.35 0.58 2.5 0.67 0.63 0.84 0.42 0.63 2.5 0.90 1.0 0.65 0.52 0.34 2.5 0.50 0.41 0.64 0.52 2.5 0.52 0.57 0.45 0.65 0.44 0.52 0.39 0.36 0.31 0.14 0.14 0.44 0.40 0.19 0.69 4.0 2.5 0.59 0.98 0.63 PQL 1.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 4.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 5.0 5.0 1.0 2.0 1.0 Analytical Data Client: ARCADIS U.S., Inc. Job Number: 660-24356-1 Client Sample ID: CP-110(10'-12')_073008 Lab Sample ID: Client Matrix: 660-24356-2 Water Date Sampled: Date Received: 07/30/2008 0840 07/30/2008 1430 8260B Volatile Organic Compounds by GC/MS Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260B 5030B 1.0 07/31/2008 1111 07/31/2008 1111 Analyte 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl chloride o-Xylene Acetone 2-Butanone (MEK) 4-Methyl-2-pentanone (MIBK) Carbon disulfide 2-Hexanone Methyl tert-butyl ether m-Xylene & p-Xylene Surrogate Toluene-d8 (Surr) 4-Bromofluorobenzene Dibromofluoromethane TestAmerica Tampa Analysis Batch: 660-65594 Result (ug/L) 0.15 0.50 0.51 0.77 0.58 0.46 0.47 0.50 2.5 0.18 0.86 0.54 0.50 0.50 9.9 8.4 3.8 0.85 4.4 0.44 0.60 %Rec 85 87 77 Page 11 of 42 Instrument ID: BVMJ GC/MS Lab File ID: 3JG3052.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U U U U U U U U U U U U U U U U U U U U U MDL 0.15 0.50 0.51 0.77 0.58 0.46 0.47 0.50 2.5 0.18 0.86 0.54 0.50 0.50 9.9 8.4 3.8 0.85 4.4 0.44 0.60 PQL 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 20 10 10 1.0 10 1.0 2.0 Acceptance Limits 77 - 122 74 - 126 70 - 130 Analytical Data Client: ARCADIS U.S., Inc. Job Number: 660-24356-1 Client Sample ID: CP-110(32'-34')_073008 Lab Sample ID: Client Matrix: 660-24356-3 Water Date Sampled: Date Received: 07/30/2008 0909 07/30/2008 1430 8260B Volatile Organic Compounds by GC/MS Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260B 5030B 1.0 07/31/2008 1133 07/31/2008 1133 Analyte Benzene Bromobenzene 1,2-Dichlorobenzene Chlorobromomethane Dichlorobromomethane Bromoform Bromomethane n-Butylbenzene sec-Butylbenzene tert-Butylbenzene Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene Chlorodibromomethane 1,2-Dibromo-3-Chloropropane Ethylene Dibromide Dibromomethane 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans-1,3-Dichloropropene Ethylbenzene Hexachlorobutadiene Isopropylbenzene 4-Isopropyltoluene Methylene Chloride Naphthalene N-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane TestAmerica Tampa Analysis Batch: 660-65594 Result (ug/L) 0.50 0.58 0.44 0.58 0.35 0.58 2.5 0.67 0.63 0.84 0.42 0.63 2.5 0.90 1.0 0.65 0.52 0.34 2.5 0.50 0.41 0.64 0.52 2.5 0.52 0.57 0.45 0.65 0.44 0.52 0.39 0.36 0.31 0.14 0.14 0.44 0.40 0.19 0.69 4.0 2.5 0.59 0.98 0.63 Page 12 of 42 Instrument ID: BVMJ GC/MS Lab File ID: 3JG3053.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U MDL 0.50 0.58 0.44 0.58 0.35 0.58 2.5 0.67 0.63 0.84 0.42 0.63 2.5 0.90 1.0 0.65 0.52 0.34 2.5 0.50 0.41 0.64 0.52 2.5 0.52 0.57 0.45 0.65 0.44 0.52 0.39 0.36 0.31 0.14 0.14 0.44 0.40 0.19 0.69 4.0 2.5 0.59 0.98 0.63 PQL 1.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 4.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 5.0 5.0 1.0 2.0 1.0 Analytical Data Client: ARCADIS U.S., Inc. Job Number: 660-24356-1 Client Sample ID: CP-110(32'-34')_073008 Lab Sample ID: Client Matrix: 660-24356-3 Water Date Sampled: Date Received: 07/30/2008 0909 07/30/2008 1430 8260B Volatile Organic Compounds by GC/MS Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260B 5030B 1.0 07/31/2008 1133 07/31/2008 1133 Analyte 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl chloride o-Xylene Acetone 2-Butanone (MEK) 4-Methyl-2-pentanone (MIBK) Carbon disulfide 2-Hexanone Methyl tert-butyl ether m-Xylene & p-Xylene Surrogate Toluene-d8 (Surr) 4-Bromofluorobenzene Dibromofluoromethane TestAmerica Tampa Analysis Batch: 660-65594 Result (ug/L) 0.15 0.50 0.51 0.77 0.58 0.46 0.47 0.50 2.5 0.18 0.86 0.54 0.50 0.50 9.9 8.4 3.8 0.85 4.4 0.44 0.60 %Rec 99 110 91 Page 13 of 42 Instrument ID: BVMJ GC/MS Lab File ID: 3JG3053.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U U U U U U U U U U U U U U U U U U U U U MDL 0.15 0.50 0.51 0.77 0.58 0.46 0.47 0.50 2.5 0.18 0.86 0.54 0.50 0.50 9.9 8.4 3.8 0.85 4.4 0.44 0.60 PQL 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 20 10 10 1.0 10 1.0 2.0 Acceptance Limits 77 - 122 74 - 126 70 - 130 Analytical Data Client: ARCADIS U.S., Inc. Job Number: 660-24356-1 Client Sample ID: CP-110(46'-48')_073008 Lab Sample ID: Client Matrix: 660-24356-4 Water Date Sampled: Date Received: 07/30/2008 0936 07/30/2008 1430 8260B Volatile Organic Compounds by GC/MS Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260B 5030B 1.0 07/31/2008 1156 07/31/2008 1156 Analyte Benzene Bromobenzene 1,2-Dichlorobenzene Chlorobromomethane Dichlorobromomethane Bromoform Bromomethane n-Butylbenzene sec-Butylbenzene tert-Butylbenzene Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene Chlorodibromomethane 1,2-Dibromo-3-Chloropropane Ethylene Dibromide Dibromomethane 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans-1,3-Dichloropropene Ethylbenzene Hexachlorobutadiene Isopropylbenzene 4-Isopropyltoluene Methylene Chloride Naphthalene N-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane TestAmerica Tampa Analysis Batch: 660-65594 Result (ug/L) 0.50 0.58 0.44 0.58 0.35 0.58 2.5 0.67 0.63 0.84 0.42 0.63 2.5 0.90 1.0 0.65 0.52 0.34 2.5 0.50 0.41 0.64 0.52 2.5 0.52 0.57 0.45 0.65 0.44 0.52 0.39 0.36 0.31 0.14 0.14 0.44 0.40 0.19 0.69 4.0 2.5 0.59 0.98 0.63 Page 14 of 42 Instrument ID: BVMJ GC/MS Lab File ID: 3JG3054.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U MDL 0.50 0.58 0.44 0.58 0.35 0.58 2.5 0.67 0.63 0.84 0.42 0.63 2.5 0.90 1.0 0.65 0.52 0.34 2.5 0.50 0.41 0.64 0.52 2.5 0.52 0.57 0.45 0.65 0.44 0.52 0.39 0.36 0.31 0.14 0.14 0.44 0.40 0.19 0.69 4.0 2.5 0.59 0.98 0.63 PQL 1.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 4.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 5.0 5.0 1.0 2.0 1.0 Analytical Data Client: ARCADIS U.S., Inc. Job Number: 660-24356-1 Client Sample ID: CP-110(46'-48')_073008 Lab Sample ID: Client Matrix: 660-24356-4 Water Date Sampled: Date Received: 07/30/2008 0936 07/30/2008 1430 8260B Volatile Organic Compounds by GC/MS Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260B 5030B 1.0 07/31/2008 1156 07/31/2008 1156 Analyte 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl chloride o-Xylene Acetone 2-Butanone (MEK) 4-Methyl-2-pentanone (MIBK) Carbon disulfide 2-Hexanone Methyl tert-butyl ether m-Xylene & p-Xylene Surrogate Toluene-d8 (Surr) 4-Bromofluorobenzene Dibromofluoromethane TestAmerica Tampa Analysis Batch: 660-65594 Result (ug/L) 0.15 0.50 0.51 0.77 0.58 0.46 0.47 0.50 2.5 0.18 0.86 0.54 0.50 0.50 9.9 8.4 3.8 0.85 4.4 0.44 0.60 %Rec 98 103 90 Page 15 of 42 Instrument ID: BVMJ GC/MS Lab File ID: 3JG3054.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U U U U U U U U U U U U U U U U U U U U U MDL 0.15 0.50 0.51 0.77 0.58 0.46 0.47 0.50 2.5 0.18 0.86 0.54 0.50 0.50 9.9 8.4 3.8 0.85 4.4 0.44 0.60 PQL 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 20 10 10 1.0 10 1.0 2.0 Acceptance Limits 77 - 122 74 - 126 70 - 130 Analytical Data Client: ARCADIS U.S., Inc. Job Number: 660-24356-1 Client Sample ID: CP-110(53'-55')_073008 Lab Sample ID: Client Matrix: 660-24356-5 Water Date Sampled: Date Received: 07/30/2008 1005 07/30/2008 1430 8260B Volatile Organic Compounds by GC/MS Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260B 5030B 1.0 07/31/2008 1711 07/31/2008 1711 Analyte Benzene Bromobenzene 1,2-Dichlorobenzene Chlorobromomethane Dichlorobromomethane Bromoform Bromomethane n-Butylbenzene sec-Butylbenzene tert-Butylbenzene Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene Chlorodibromomethane 1,2-Dibromo-3-Chloropropane Ethylene Dibromide Dibromomethane 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans-1,3-Dichloropropene Ethylbenzene Hexachlorobutadiene Isopropylbenzene 4-Isopropyltoluene Methylene Chloride Naphthalene N-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane TestAmerica Tampa Analysis Batch: 660-65595 Result (ug/L) 0.50 0.58 0.44 0.58 0.35 0.58 2.5 0.67 0.63 0.84 0.42 0.63 2.5 0.90 1.0 0.65 0.52 0.34 2.5 0.50 0.41 0.64 0.52 2.5 0.52 0.57 0.45 0.65 0.44 0.52 0.39 0.36 0.31 0.14 0.14 0.44 0.40 0.19 0.69 4.0 2.5 0.59 0.98 0.63 Page 16 of 42 Instrument ID: BVMH GC/MS Lab File ID: 2HG3118.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U MDL 0.50 0.58 0.44 0.58 0.35 0.58 2.5 0.67 0.63 0.84 0.42 0.63 2.5 0.90 1.0 0.65 0.52 0.34 2.5 0.50 0.41 0.64 0.52 2.5 0.52 0.57 0.45 0.65 0.44 0.52 0.39 0.36 0.31 0.14 0.14 0.44 0.40 0.19 0.69 4.0 2.5 0.59 0.98 0.63 PQL 1.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 4.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 5.0 5.0 1.0 2.0 1.0 Analytical Data Client: ARCADIS U.S., Inc. Job Number: 660-24356-1 Client Sample ID: CP-110(53'-55')_073008 Lab Sample ID: Client Matrix: 660-24356-5 Water Date Sampled: Date Received: 07/30/2008 1005 07/30/2008 1430 8260B Volatile Organic Compounds by GC/MS Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260B 5030B 1.0 07/31/2008 1711 07/31/2008 1711 Analyte 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl chloride o-Xylene Acetone 2-Butanone (MEK) 4-Methyl-2-pentanone (MIBK) Carbon disulfide 2-Hexanone Methyl tert-butyl ether m-Xylene & p-Xylene Surrogate Toluene-d8 (Surr) 4-Bromofluorobenzene Dibromofluoromethane TestAmerica Tampa Analysis Batch: 660-65595 Result (ug/L) 0.15 0.50 0.51 0.77 0.58 0.46 0.47 0.50 2.5 0.18 0.86 0.54 0.50 0.50 9.9 8.4 3.8 0.85 4.4 0.44 0.60 %Rec 100 98 104 Page 17 of 42 Instrument ID: BVMH GC/MS Lab File ID: 2HG3118.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U U U U U U U U U U U U U U U U U U U U U MDL 0.15 0.50 0.51 0.77 0.58 0.46 0.47 0.50 2.5 0.18 0.86 0.54 0.50 0.50 9.9 8.4 3.8 0.85 4.4 0.44 0.60 PQL 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 20 10 10 1.0 10 1.0 2.0 Acceptance Limits 77 - 122 74 - 126 70 - 130 Analytical Data Client: ARCADIS U.S., Inc. Job Number: 660-24356-1 Client Sample ID: CP-110(63'-65')_073008 Lab Sample ID: Client Matrix: 660-24356-6 Water Date Sampled: Date Received: 07/30/2008 1200 07/30/2008 1430 8260B Volatile Organic Compounds by GC/MS Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260B 5030B 1.0 07/30/2008 2217 07/30/2008 2217 Analyte Benzene Bromobenzene 1,2-Dichlorobenzene Chlorobromomethane Dichlorobromomethane Bromoform Bromomethane n-Butylbenzene sec-Butylbenzene tert-Butylbenzene Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene Chlorodibromomethane 1,2-Dibromo-3-Chloropropane Ethylene Dibromide Dibromomethane 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans-1,3-Dichloropropene Ethylbenzene Hexachlorobutadiene Isopropylbenzene 4-Isopropyltoluene Methylene Chloride Naphthalene N-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane TestAmerica Tampa Analysis Batch: 660-65567 Result (ug/L) 1.2 0.58 0.44 0.58 0.35 0.58 2.5 0.67 0.63 0.84 0.42 0.63 2.5 0.90 1.0 0.65 0.52 0.34 2.5 0.50 0.41 0.64 0.52 2.5 0.52 0.57 0.45 0.65 0.44 0.52 0.39 0.36 0.31 0.14 0.14 0.44 0.40 0.19 0.69 4.0 2.5 0.59 0.98 0.63 Page 18 of 42 Instrument ID: BVMJ GC/MS Lab File ID: 3JG3020.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U MDL 0.50 0.58 0.44 0.58 0.35 0.58 2.5 0.67 0.63 0.84 0.42 0.63 2.5 0.90 1.0 0.65 0.52 0.34 2.5 0.50 0.41 0.64 0.52 2.5 0.52 0.57 0.45 0.65 0.44 0.52 0.39 0.36 0.31 0.14 0.14 0.44 0.40 0.19 0.69 4.0 2.5 0.59 0.98 0.63 PQL 1.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 4.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 5.0 5.0 1.0 2.0 1.0 Analytical Data Client: ARCADIS U.S., Inc. Job Number: 660-24356-1 Client Sample ID: CP-110(63'-65')_073008 Lab Sample ID: Client Matrix: 660-24356-6 Water Date Sampled: Date Received: 07/30/2008 1200 07/30/2008 1430 8260B Volatile Organic Compounds by GC/MS Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260B 5030B 1.0 07/30/2008 2217 07/30/2008 2217 Analyte 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl chloride o-Xylene Acetone 2-Butanone (MEK) 4-Methyl-2-pentanone (MIBK) Carbon disulfide 2-Hexanone Methyl tert-butyl ether m-Xylene & p-Xylene Surrogate Toluene-d8 (Surr) 4-Bromofluorobenzene Dibromofluoromethane TestAmerica Tampa Analysis Batch: 660-65567 Result (ug/L) 0.15 0.50 2.6 0.77 0.58 0.46 0.47 0.50 2.5 0.18 0.86 0.54 0.50 0.50 34 8.4 3.8 0.85 4.4 0.44 1.1 %Rec 99 106 92 Page 19 of 42 Instrument ID: BVMJ GC/MS Lab File ID: 3JG3020.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U U U U U U U U U U U U U U U U U U I MDL 0.15 0.50 0.51 0.77 0.58 0.46 0.47 0.50 2.5 0.18 0.86 0.54 0.50 0.50 9.9 8.4 3.8 0.85 4.4 0.44 0.60 PQL 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 20 10 10 1.0 10 1.0 2.0 Acceptance Limits 77 - 122 74 - 126 70 - 130 Analytical Data Client: ARCADIS U.S., Inc. Job Number: 660-24356-1 Client Sample ID: Trip Blank(7/30/08)_073008 Lab Sample ID: Client Matrix: 660-24356-1 Water Date Sampled: Date Received: 07/30/2008 0000 07/30/2008 1430 8260C SIM/ID 1,4-Dioxane by SIM/Isotopic Dilution Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260C SIM/ID 5030B 1.0 07/30/2008 2155 07/30/2008 2155 Analyte 1,4-Dioxane TestAmerica Tampa Analysis Batch: 660-65568 Result (ug/L) 0.54 Page 20 of 42 Instrument ID: BVMJ GC/MS Lab File ID: 3JG3019.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U MDL 0.54 PQL 1.0 Analytical Data Client: ARCADIS U.S., Inc. Job Number: 660-24356-1 Client Sample ID: CP-110(10'-12')_073008 Lab Sample ID: Client Matrix: 660-24356-2 Water Date Sampled: Date Received: 07/30/2008 0840 07/30/2008 1430 8260C SIM/ID 1,4-Dioxane by SIM/Isotopic Dilution Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260C SIM/ID 5030B 1.0 07/30/2008 1756 07/30/2008 1756 Analyte 1,4-Dioxane TestAmerica Tampa Analysis Batch: 660-65504 Result (ug/L) 0.54 Page 21 of 42 Instrument ID: BVMH GC/MS Lab File ID: 1HG3029.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U MDL 0.54 PQL 1.0 Analytical Data Client: ARCADIS U.S., Inc. Job Number: 660-24356-1 Client Sample ID: CP-110(32'-34')_073008 Lab Sample ID: Client Matrix: 660-24356-3 Water Date Sampled: Date Received: 07/30/2008 0909 07/30/2008 1430 8260C SIM/ID 1,4-Dioxane by SIM/Isotopic Dilution Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260C SIM/ID 5030B 1.0 07/30/2008 1816 07/30/2008 1816 Analyte 1,4-Dioxane TestAmerica Tampa Analysis Batch: 660-65504 Result (ug/L) 0.54 Page 22 of 42 Instrument ID: BVMH GC/MS Lab File ID: 1HG3030.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U MDL 0.54 PQL 1.0 Analytical Data Client: ARCADIS U.S., Inc. Job Number: 660-24356-1 Client Sample ID: CP-110(46'-48')_073008 Lab Sample ID: Client Matrix: 660-24356-4 Water Date Sampled: Date Received: 07/30/2008 0936 07/30/2008 1430 8260C SIM/ID 1,4-Dioxane by SIM/Isotopic Dilution Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260C SIM/ID 5030B 1.0 07/30/2008 1836 07/30/2008 1836 Analyte 1,4-Dioxane TestAmerica Tampa Analysis Batch: 660-65504 Result (ug/L) 0.54 Page 23 of 42 Instrument ID: BVMH GC/MS Lab File ID: 1HG3031.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U MDL 0.54 PQL 1.0 Analytical Data Client: ARCADIS U.S., Inc. Job Number: 660-24356-1 Client Sample ID: CP-110(53'-55')_073008 Lab Sample ID: Client Matrix: 660-24356-5 Water Date Sampled: Date Received: 07/30/2008 1005 07/30/2008 1430 8260C SIM/ID 1,4-Dioxane by SIM/Isotopic Dilution Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260C SIM/ID 5030B 1.0 07/31/2008 1711 07/31/2008 1711 Analyte 1,4-Dioxane TestAmerica Tampa Analysis Batch: 660-65596 Result (ug/L) 0.54 Page 24 of 42 Instrument ID: BVMH GC/MS Lab File ID: 2HG3118.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U MDL 0.54 PQL 1.0 Analytical Data Client: ARCADIS U.S., Inc. Job Number: 660-24356-1 Client Sample ID: CP-110(63'-65')_073008 Lab Sample ID: Client Matrix: 660-24356-6 Water Date Sampled: Date Received: 07/30/2008 1200 07/30/2008 1430 8260C SIM/ID 1,4-Dioxane by SIM/Isotopic Dilution Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260C SIM/ID 5030B 1.0 07/30/2008 2217 07/30/2008 2217 Analyte 1,4-Dioxane TestAmerica Tampa Analysis Batch: 660-65568 Result (ug/L) 0.54 Page 25 of 42 Instrument ID: BVMJ GC/MS Lab File ID: 3JG3020.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U MDL 0.54 PQL 1.0 DATA REPORTING QUALIFIERS Client: ARCADIS U.S., Inc. Lab Section Job Number: 660-24356-1 Qualifier Description U Indicates that the compound was analyzed for but not detected. I The reported value is between the laboratory method detection limit and the laboratory practical quantitation limit. GC/MS VOA TestAmerica Tampa Page 26 of 42 QUALITY CONTROL RESULTS TestAmerica Tampa Page 27 of 42 Quality Control Results Client: ARCADIS U.S., Inc. Job Number: 660-24356-1 Surrogate Recovery Report 8260B Volatile Organic Compounds by GC/MS Client Matrix: Water TOL %Rec BFB %Rec DBFM %Rec 90 96 84 85 87 77 99 110 91 98 103 90 100 98 104 99 106 92 MB 660-65567/3 94 101 90 MB 660-65594/3 98 102 91 MB 660-65595/3 100 97 105 LCS 660-65567/1 99 107 95 LCS 660-65594/1 92 96 86 LCS 660-65595/1 98 98 104 LCSD 660-65567/2 93 102 89 LCSD 660-65594/2 94 98 87 LCSD 660-65595/2 98 98 102 Lab Sample ID Client Sample ID 660-24356-1 Trip Blank(7/30/08)_07300 8 CP-110(10'-12')_0730 08 CP-110(32'-34')_0730 08 CP-110(46'-48')_0730 08 CP-110(53'-55')_0730 08 CP-110(63'-65')_0730 08 660-24356-2 660-24356-3 660-24356-4 660-24356-5 660-24356-6 Surrogate TOL = Toluene-d8 (Surr) BFB = 4-Bromofluorobenzene DBFM = Dibromofluoromethane Acceptance Limits 77-122 74-126 70-130 TestAmerica Tampa Page 28 of 42 Quality Control Results Client: ARCADIS U.S., Inc. Job Number: 660-24356-1 Method Blank - Batch: 660-65567 Lab Sample ID: Client Matrix: Dilution: Date Analyzed: Date Prepared: MB 660-65567/3 Water 1.0 07/30/2008 2132 07/30/2008 2132 Method: 8260B Preparation: 5030B Analysis Batch: 660-65567 Prep Batch: N/A Units: ug/L Instrument ID: BVMJ GC/MS Lab File ID: 3JG3018.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Analyte Result Qual MDL PQL Benzene Bromobenzene 1,2-Dichlorobenzene Chlorobromomethane Dichlorobromomethane Bromoform Bromomethane n-Butylbenzene sec-Butylbenzene tert-Butylbenzene Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene Chlorodibromomethane 1,2-Dibromo-3-Chloropropane Ethylene Dibromide Dibromomethane 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans-1,3-Dichloropropene Ethylbenzene Hexachlorobutadiene Isopropylbenzene 4-Isopropyltoluene Methylene Chloride Naphthalene 0.50 0.58 0.44 0.58 0.35 0.58 2.5 0.67 0.63 0.84 0.42 0.63 2.5 0.90 1.0 0.65 0.52 0.34 2.5 0.50 0.41 0.64 0.52 2.5 0.52 0.57 0.45 0.65 0.44 0.52 0.39 0.36 0.31 0.14 0.14 0.44 0.40 0.19 0.69 4.0 2.5 U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U 0.50 0.58 0.44 0.58 0.35 0.58 2.5 0.67 0.63 0.84 0.42 0.63 2.5 0.90 1.0 0.65 0.52 0.34 2.5 0.50 0.41 0.64 0.52 2.5 0.52 0.57 0.45 0.65 0.44 0.52 0.39 0.36 0.31 0.14 0.14 0.44 0.40 0.19 0.69 4.0 2.5 1.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 4.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 5.0 5.0 Calculations are performed before rounding to avoid round-off errors in calculated results. TestAmerica Tampa Page 29 of 42 Quality Control Results Client: ARCADIS U.S., Inc. Job Number: 660-24356-1 Method Blank - Batch: 660-65567 Lab Sample ID: Client Matrix: Dilution: Date Analyzed: Date Prepared: MB 660-65567/3 Water 1.0 07/30/2008 2132 07/30/2008 2132 Method: 8260B Preparation: 5030B Analysis Batch: 660-65567 Prep Batch: N/A Units: ug/L Instrument ID: BVMJ GC/MS Lab File ID: 3JG3018.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Analyte Result Qual MDL PQL N-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl chloride o-Xylene Acetone 2-Butanone (MEK) 4-Methyl-2-pentanone (MIBK) Carbon disulfide 2-Hexanone Methyl tert-butyl ether m-Xylene & p-Xylene 0.59 0.98 0.63 0.15 0.50 0.51 0.77 0.58 0.46 0.47 0.50 2.5 0.18 0.86 0.54 0.50 0.50 9.9 8.4 3.8 0.85 4.4 0.44 0.60 U U U U U U U U U U U U U U U U U U U U U U U U 0.59 0.98 0.63 0.15 0.50 0.51 0.77 0.58 0.46 0.47 0.50 2.5 0.18 0.86 0.54 0.50 0.50 9.9 8.4 3.8 0.85 4.4 0.44 0.60 1.0 2.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 20 10 10 1.0 10 1.0 2.0 Surrogate Toluene-d8 (Surr) 4-Bromofluorobenzene Dibromofluoromethane % Rec Acceptance Limits 94 101 90 77 - 122 74 - 126 70 - 130 Calculations are performed before rounding to avoid round-off errors in calculated results. TestAmerica Tampa Page 30 of 42 Quality Control Results Client: ARCADIS U.S., Inc. Job Number: 660-24356-1 Lab Control Spike/ Lab Control Spike Duplicate Recovery Report - Batch: 660-65567 Method: 8260B Preparation: 5030B LCS Lab Sample ID: LCS 660-65567/1 Client Matrix: Water Dilution: 1.0 07/30/2008 2025 Date Analyzed: 07/30/2008 2025 Date Prepared: Analysis Batch: 660-65567 Prep Batch: N/A Units: ug/L Instrument ID: BVMJ GC/MS Lab File ID: 3JG3015.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL LCSD Lab Sample ID: LCSD 660-65567/2 Client Matrix: Water Dilution: 1.0 07/30/2008 2047 Date Analyzed: 07/30/2008 2047 Date Prepared: Analysis Batch: 660-65567 Prep Batch: N/A Units: ug/L Instrument ID: BVMJ GC/MS Lab File ID: 3JG3016.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Analyte LCS Benzene Chlorobenzene 1,1-Dichloroethene Toluene Trichloroethene 87 88 93 87 87 % Rec. LCSD 94 93 98 91 92 Limit RPD RPD Limit 62 - 135 72 - 127 46 - 147 68 - 131 56 - 143 7 5 5 5 6 37 22 30 33 35 Calculations are performed before rounding to avoid round-off errors in calculated results. TestAmerica Tampa Page 31 of 42 LCS Qual LCSD Qual Quality Control Results Client: ARCADIS U.S., Inc. Job Number: 660-24356-1 Method Blank - Batch: 660-65594 Lab Sample ID: Client Matrix: Dilution: Date Analyzed: Date Prepared: MB 660-65594/3 Water 1.0 07/31/2008 0759 07/31/2008 0759 Method: 8260B Preparation: 5030B Analysis Batch: 660-65594 Prep Batch: N/A Units: ug/L Instrument ID: BVMJ GC/MS Lab File ID: 3JG3046.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Analyte Result Qual MDL PQL Benzene Bromobenzene 1,2-Dichlorobenzene Chlorobromomethane Dichlorobromomethane Bromoform Bromomethane n-Butylbenzene sec-Butylbenzene tert-Butylbenzene Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene Chlorodibromomethane 1,2-Dibromo-3-Chloropropane Ethylene Dibromide Dibromomethane 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans-1,3-Dichloropropene Ethylbenzene Hexachlorobutadiene Isopropylbenzene 4-Isopropyltoluene Methylene Chloride Naphthalene 0.50 0.58 0.44 0.58 0.35 0.58 2.5 0.67 0.63 0.84 0.42 0.63 2.5 0.90 1.0 0.65 0.52 0.34 2.5 0.50 0.41 0.64 0.52 2.5 0.52 0.57 0.45 0.65 0.44 0.52 0.39 0.36 0.31 0.14 0.14 0.44 0.40 0.19 0.69 4.0 2.5 U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U 0.50 0.58 0.44 0.58 0.35 0.58 2.5 0.67 0.63 0.84 0.42 0.63 2.5 0.90 1.0 0.65 0.52 0.34 2.5 0.50 0.41 0.64 0.52 2.5 0.52 0.57 0.45 0.65 0.44 0.52 0.39 0.36 0.31 0.14 0.14 0.44 0.40 0.19 0.69 4.0 2.5 1.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 4.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 5.0 5.0 Calculations are performed before rounding to avoid round-off errors in calculated results. TestAmerica Tampa Page 32 of 42 Quality Control Results Client: ARCADIS U.S., Inc. Job Number: 660-24356-1 Method Blank - Batch: 660-65594 Lab Sample ID: Client Matrix: Dilution: Date Analyzed: Date Prepared: MB 660-65594/3 Water 1.0 07/31/2008 0759 07/31/2008 0759 Method: 8260B Preparation: 5030B Analysis Batch: 660-65594 Prep Batch: N/A Units: ug/L Instrument ID: BVMJ GC/MS Lab File ID: 3JG3046.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Analyte Result Qual MDL PQL N-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl chloride o-Xylene Acetone 2-Butanone (MEK) 4-Methyl-2-pentanone (MIBK) Carbon disulfide 2-Hexanone Methyl tert-butyl ether m-Xylene & p-Xylene 0.59 0.98 0.63 0.15 0.50 0.51 0.77 0.58 0.46 0.47 0.50 2.5 0.18 0.86 0.54 0.50 0.50 9.9 8.4 3.8 0.85 4.4 0.44 0.60 U U U U U U U U U U U U U U U U U U U U U U U U 0.59 0.98 0.63 0.15 0.50 0.51 0.77 0.58 0.46 0.47 0.50 2.5 0.18 0.86 0.54 0.50 0.50 9.9 8.4 3.8 0.85 4.4 0.44 0.60 1.0 2.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 20 10 10 1.0 10 1.0 2.0 Surrogate Toluene-d8 (Surr) 4-Bromofluorobenzene Dibromofluoromethane % Rec Acceptance Limits 98 102 91 77 - 122 74 - 126 70 - 130 Calculations are performed before rounding to avoid round-off errors in calculated results. TestAmerica Tampa Page 33 of 42 Quality Control Results Client: ARCADIS U.S., Inc. Job Number: 660-24356-1 Lab Control Spike/ Lab Control Spike Duplicate Recovery Report - Batch: 660-65594 Method: 8260B Preparation: 5030B LCS Lab Sample ID: LCS 660-65594/1 Client Matrix: Water Dilution: 1.0 07/31/2008 0715 Date Analyzed: 07/31/2008 0715 Date Prepared: Analysis Batch: 660-65594 Prep Batch: N/A Units: ug/L Instrument ID: BVMJ GC/MS Lab File ID: 3JG3044.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL LCSD Lab Sample ID: LCSD 660-65594/2 Client Matrix: Water Dilution: 1.0 07/31/2008 0737 Date Analyzed: 07/31/2008 0737 Date Prepared: Analysis Batch: 660-65594 Prep Batch: N/A Units: ug/L Instrument ID: BVMJ GC/MS Lab File ID: 3JG3045.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Analyte LCS % Rec. LCSD Benzene Chlorobenzene 1,1-Dichloroethene Toluene Trichloroethene 91 91 100 90 88 87 90 99 88 87 Limit RPD RPD Limit 62 - 135 72 - 127 46 - 147 68 - 131 56 - 143 4 1 1 2 2 37 22 30 33 35 Calculations are performed before rounding to avoid round-off errors in calculated results. TestAmerica Tampa Page 34 of 42 LCS Qual LCSD Qual Quality Control Results Client: ARCADIS U.S., Inc. Job Number: 660-24356-1 Method Blank - Batch: 660-65595 Lab Sample ID: Client Matrix: Dilution: Date Analyzed: Date Prepared: MB 660-65595/3 Water 1.0 07/31/2008 1651 07/31/2008 1651 Method: 8260B Preparation: 5030B Analysis Batch: 660-65595 Prep Batch: N/A Units: ug/L Instrument ID: BVMH GC/MS Lab File ID: 2HG3117.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Analyte Result Qual MDL PQL Benzene Bromobenzene 1,2-Dichlorobenzene Chlorobromomethane Dichlorobromomethane Bromoform Bromomethane n-Butylbenzene sec-Butylbenzene tert-Butylbenzene Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene Chlorodibromomethane 1,2-Dibromo-3-Chloropropane Ethylene Dibromide Dibromomethane 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans-1,3-Dichloropropene Ethylbenzene Hexachlorobutadiene Isopropylbenzene 4-Isopropyltoluene Methylene Chloride Naphthalene 0.50 0.58 0.44 0.58 0.35 0.58 2.5 0.67 0.63 0.84 0.42 0.63 2.5 0.90 1.0 0.65 0.52 0.34 2.5 0.50 0.41 0.64 0.52 2.5 0.52 0.57 0.45 0.65 0.44 0.52 0.39 0.36 0.31 0.14 0.14 0.44 0.40 0.19 0.69 4.0 2.5 U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U 0.50 0.58 0.44 0.58 0.35 0.58 2.5 0.67 0.63 0.84 0.42 0.63 2.5 0.90 1.0 0.65 0.52 0.34 2.5 0.50 0.41 0.64 0.52 2.5 0.52 0.57 0.45 0.65 0.44 0.52 0.39 0.36 0.31 0.14 0.14 0.44 0.40 0.19 0.69 4.0 2.5 1.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 4.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 5.0 5.0 Calculations are performed before rounding to avoid round-off errors in calculated results. TestAmerica Tampa Page 35 of 42 Quality Control Results Client: ARCADIS U.S., Inc. Job Number: 660-24356-1 Method Blank - Batch: 660-65595 Lab Sample ID: Client Matrix: Dilution: Date Analyzed: Date Prepared: MB 660-65595/3 Water 1.0 07/31/2008 1651 07/31/2008 1651 Method: 8260B Preparation: 5030B Analysis Batch: 660-65595 Prep Batch: N/A Units: ug/L Instrument ID: BVMH GC/MS Lab File ID: 2HG3117.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Analyte Result Qual MDL PQL N-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl chloride o-Xylene Acetone 2-Butanone (MEK) 4-Methyl-2-pentanone (MIBK) Carbon disulfide 2-Hexanone Methyl tert-butyl ether m-Xylene & p-Xylene 0.59 0.98 0.63 0.15 0.50 0.51 0.77 0.58 0.46 0.47 0.50 2.5 0.18 0.86 0.54 0.50 0.50 9.9 8.4 3.8 0.85 4.4 0.44 0.60 U U U U U U U U U U U U U U U U U U U U U U U U 0.59 0.98 0.63 0.15 0.50 0.51 0.77 0.58 0.46 0.47 0.50 2.5 0.18 0.86 0.54 0.50 0.50 9.9 8.4 3.8 0.85 4.4 0.44 0.60 1.0 2.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 20 10 10 1.0 10 1.0 2.0 Surrogate Toluene-d8 (Surr) 4-Bromofluorobenzene Dibromofluoromethane % Rec Acceptance Limits 100 97 105 77 - 122 74 - 126 70 - 130 Calculations are performed before rounding to avoid round-off errors in calculated results. TestAmerica Tampa Page 36 of 42 Quality Control Results Client: ARCADIS U.S., Inc. Job Number: 660-24356-1 Lab Control Spike/ Lab Control Spike Duplicate Recovery Report - Batch: 660-65595 Method: 8260B Preparation: 5030B LCS Lab Sample ID: LCS 660-65595/1 Client Matrix: Water Dilution: 1.0 07/31/2008 1611 Date Analyzed: 07/31/2008 1611 Date Prepared: Analysis Batch: 660-65595 Prep Batch: N/A Units: ug/L Instrument ID: BVMH GC/MS Lab File ID: 2HG3115.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL LCSD Lab Sample ID: LCSD 660-65595/2 Client Matrix: Water Dilution: 1.0 07/31/2008 1631 Date Analyzed: 07/31/2008 1631 Date Prepared: Analysis Batch: 660-65595 Prep Batch: N/A Units: ug/L Instrument ID: BVMH GC/MS Lab File ID: 2HG3116.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Analyte LCS % Rec. LCSD Benzene Chlorobenzene 1,1-Dichloroethene Toluene Trichloroethene 103 100 93 99 109 93 93 85 90 91 Limit RPD RPD Limit 62 - 135 72 - 127 46 - 147 68 - 131 56 - 143 9 7 9 10 18 37 22 30 33 35 Calculations are performed before rounding to avoid round-off errors in calculated results. TestAmerica Tampa Page 37 of 42 LCS Qual LCSD Qual Quality Control Results Client: ARCADIS U.S., Inc. Job Number: 660-24356-1 Method Blank - Batch: 660-65504 Lab Sample ID: Client Matrix: Dilution: Date Analyzed: Date Prepared: MB 660-65504/1 Water 1.0 07/30/2008 1212 07/30/2008 1212 Method: 8260C SIM/ID Preparation: 5030B Analysis Batch: 660-65504 Prep Batch: N/A Units: ug/L Instrument ID: BVMH GC/MS Lab File ID: 1HG3012.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Analyte Result Qual MDL PQL 1,4-Dioxane 0.54 U 0.54 1.0 Lab Control Spike/ Lab Control Spike Duplicate Recovery Report - Batch: 660-65504 Method: 8260C SIM/ID Preparation: 5030B LCS Lab Sample ID: LCS 660-65504/2 Client Matrix: Water Dilution: 1.0 07/30/2008 1111 Date Analyzed: 07/30/2008 1111 Date Prepared: Analysis Batch: 660-65504 Prep Batch: N/A Units: ug/L Instrument ID: BVMH GC/MS Lab File ID: 1HG3009.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL LCSD Lab Sample ID: LCSD 660-65504/3 Client Matrix: Water Dilution: 1.0 07/30/2008 1131 Date Analyzed: 07/30/2008 1131 Date Prepared: Analysis Batch: 660-65504 Prep Batch: N/A Units: ug/L Instrument ID: BVMH GC/MS Lab File ID: 1HG3010.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Analyte LCS 1,4-Dioxane 108 % Rec. LCSD 105 Limit RPD RPD Limit 50 - 150 4 50 Calculations are performed before rounding to avoid round-off errors in calculated results. TestAmerica Tampa Page 38 of 42 LCS Qual LCSD Qual Quality Control Results Client: ARCADIS U.S., Inc. Job Number: 660-24356-1 Method Blank - Batch: 660-65568 Lab Sample ID: Client Matrix: Dilution: Date Analyzed: Date Prepared: MB 660-65568/3 Water 1.0 07/30/2008 2132 07/30/2008 2132 Method: 8260C SIM/ID Preparation: 5030B Analysis Batch: 660-65568 Prep Batch: N/A Units: ug/L Instrument ID: BVMJ GC/MS Lab File ID: 3JG3018.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Analyte Result Qual MDL PQL 1,4-Dioxane 0.54 U 0.54 1.0 Lab Control Spike/ Lab Control Spike Duplicate Recovery Report - Batch: 660-65568 Method: 8260C SIM/ID Preparation: 5030B LCS Lab Sample ID: LCS 660-65568/1 Client Matrix: Water Dilution: 1.0 07/30/2008 2025 Date Analyzed: 07/30/2008 2025 Date Prepared: Analysis Batch: 660-65568 Prep Batch: N/A Units: ug/L Instrument ID: BVMJ GC/MS Lab File ID: 3JG3015.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL LCSD Lab Sample ID: LCSD 660-65568/2 Client Matrix: Water Dilution: 1.0 07/30/2008 2047 Date Analyzed: 07/30/2008 2047 Date Prepared: Analysis Batch: 660-65568 Prep Batch: N/A Units: ug/L Instrument ID: BVMJ GC/MS Lab File ID: 3JG3016.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Analyte LCS % Rec. LCSD 1,4-Dioxane 107 89 Limit RPD RPD Limit 50 - 150 18 50 Calculations are performed before rounding to avoid round-off errors in calculated results. TestAmerica Tampa Page 39 of 42 LCS Qual LCSD Qual Quality Control Results Client: ARCADIS U.S., Inc. Job Number: 660-24356-1 Method Blank - Batch: 660-65596 Lab Sample ID: Client Matrix: Dilution: Date Analyzed: Date Prepared: MB 660-65596/3 Water 1.0 07/31/2008 1651 07/31/2008 1651 Method: 8260C SIM/ID Preparation: 5030B Analysis Batch: 660-65596 Prep Batch: N/A Units: ug/L Instrument ID: BVMH GC/MS Lab File ID: 2HG3117.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Analyte Result Qual MDL PQL 1,4-Dioxane 0.54 U 0.54 1.0 Lab Control Spike/ Lab Control Spike Duplicate Recovery Report - Batch: 660-65596 Method: 8260C SIM/ID Preparation: 5030B LCS Lab Sample ID: LCS 660-65596/1 Client Matrix: Water Dilution: 1.0 07/31/2008 1611 Date Analyzed: 07/31/2008 1611 Date Prepared: Analysis Batch: 660-65596 Prep Batch: N/A Units: ug/L Instrument ID: BVMH GC/MS Lab File ID: 2HG3115.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL LCSD Lab Sample ID: LCSD 660-65596/2 Client Matrix: Water Dilution: 1.0 07/31/2008 1631 Date Analyzed: 07/31/2008 1631 Date Prepared: Analysis Batch: 660-65596 Prep Batch: N/A Units: ug/L Instrument ID: BVMH GC/MS Lab File ID: 2HG3116.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Analyte LCS 1,4-Dioxane 112 % Rec. LCSD 112 Limit RPD RPD Limit 50 - 150 0 50 Calculations are performed before rounding to avoid round-off errors in calculated results. TestAmerica Tampa Page 40 of 42 LCS Qual LCSD Qual Page 41 of 42 Login Sample Receipt Check List Client: ARCADIS U.S., Inc. Job Number: 660-24356-1 Login Number: 24356 Creator: Atkins, Amy List Number: 1 List Source: TestAmerica Tampa Question T / F/ NA Radioactivity either was not measured or, if measured, is at or below background The cooler's custody seal, if present, is intact. N/A The cooler or samples do not appear to have been compromised or tampered with. Samples were received on ice. Cooler Temperature is acceptable. True Cooler Temperature is recorded. COC is present. COC is filled out in ink and legible. COC is filled out with all pertinent information. There are no discrepancies between the sample IDs on the containers and the COC. Samples are received within Holding Time. Sample containers have legible labels. Containers are not broken or leaking. True True True True True Sample collection date/times are provided. Appropriate sample containers are used. Sample bottles are completely filled. There is sufficient vol. for all requested analyses, incl. any requested MS/MSDs VOA sample vials do not have headspace or bubble is <6mm (1/4") in diameter. If necessary, staff have been informed of any short hold time or quick TAT needs Multiphasic samples are not present. Samples do not require splitting or compositing. True True True True TestAmerica Tampa Comment N/A True True True True True True True True True Page 42 of 42 4 Degrees. CU-04