ICPTest_977P pdf

ICP Test Report Certification Packet
Company name :
Littelfuse, Inc.
Product Series:
5x20 Fuse
Product #:
977 series
Issue Date:
Jun3 18, 2012
It is hereby certified by Littelfuse, Inc. that there is neither RoHS (2011/65/EU – recast of EU
Directive 2002/95/EC)-restricted substance nor such use, for materials to be used for unit parts,
for packing/packaging materials, and for additives and the like in the manufacturing processes.
In addition, it is hereby reported to you that the parts and sub-materials, the materials to be used
for unit parts, the packing/packaging materials, and the additives and the like in the manufacturing
processes, are all composed of the following components.
Issued by:
<Global EHS Engineer>
(1) Parts, sub-materials and unit parts
This document covers the 5x20 Fuse RoHS-Compliant series products manufactured by
Littelfuse, Inc.
＜ Raw Materials Used
Please see Table 1
(2) The ICP data on all measurable substances
Please see appropriate pages as identifed in Table 1
Remarks：
Form 585-047 Rev. A
1
2/21/06
Table 1: List of Raw Materials covered by this report
Total Parts Raw Material Part Number
1
909532
2
692529
3
692539-002
4
087355
5
C910510
6
C910541
7
311.7374.5000
8
648901
9
082xxx-001, 687xxx-001
10
004xxx
11
082xxx
12
030204, 934-077
13
030204, 934-077
Raw Material Description
Body
Solder
Solder
Glue
Cap
Cap
Filler
Yarn
Wire
Wire
Wire
Overcap - Cap Base & Plating
Overcap - Wire Base & Plating
2
Page(s)
3-26
27-31
32-36
37-48
49-52
49-52
53-61
62-70
71-80
81-90
91-100
101-104
101-104
Validi
ForQ
Please
Test Report
own
SGS
No. : CE/2012I14843ADare.2O12J02104Pagel.1o124
tll||Ill
CERAIVTEC
GIVBH
MULTIFUNCTIONAL
CERAI/IICSLUITPOLDSTMSSE
15 D.91207LAUF,GERMANY
ltltt]r
The following sample(s)was/u,€resubmiltsd and identifiedby/on behalfof the client as:
Sample Description
Stle/ltem No.
SampleReceivingDate
TestingPerjod
CERAMIC
c610
2012,01t30
2012J01| 30 TO 201Z 02t04
Te3tRe.ult(s)
: Pleasereferlo nextpage(s).
Conclu6ion
Lead,
: Bas€dontheperformed
testsonsubmitted
samples,
thetestresults
of Cadmium,
lvlercury,
Hexavalent
Cf(Vl),PBBS
andPBDES
comply
withthelimit6assetby
Ch.omium
RoHSDireclive
Annexll; recasting
200295/EC.
2011/65/EU
Sg|rad for||d
Cltorlcd Lborlbry-
T.Fd
comDafrAilB6;RE ,tRd-LXlAllHll lftlCt
!IAIA|
lq"1 )19{
"SFiAE
Th3dodm6dE6ebyfuconMy&bjedbi6Gengg|cddfooi3ds.s6pii6oveis43Eisb.on4wd
aadrsd tui i'no
t'lnld d6 kru6 doinoddroEi Adyhoderot hB tuhed
mt and
f sr rrE comp.nr'EE r.rspombrl'
"ih
comFry Atu sadoEs
. rodon torcsryor rslff€ton d rhe6ibd or sD
nd ofl.id.6 m.y e p,@dk
ih6 r ft or rtsiftmton
.*n, ;S-:HJ'Y
I iH::::gj;t.*t;:,$;;
'-;*,t^--
"
ro s. rd
r !6!a {Brts
***'*
Test Report
No.: CEJ2012/14843ADale| 201Z0ZM
Page: 2 o f 2 4
t]r||lrrfl||fllllt
CERAI\,ITEC
GMBH
MULTIFUNCTIOML
CERAITIICS
LUITPOLDSTMSSE
15 D.91207LAUF,GERIJANY
IeclBecc$GL
PARTNAMENo.l
Test ltem(s)
I
WHITECERAIVIC
lJnit
MDL
Method
R€ult
Limit
l{o.t
2
n,o,
100
2
178
1000
2
n.o.
1000
2
n.d.
1000
0.5
n.d.
mS/kS Withfeference
to USEPA3540C
0.5
n.d.
method.
Analysis
waspedormed
by
GC/MS.
mg/Kg Withreference
to uS EPA3540C
method.
Analysis
wasperformed
by
GC/|VS.
5
n.d.
0.01
n.d.
10
n.d.
Cadmium(Cd)
mS/kS With referenceto IEC 62321:2008 and
perfomed by ICP-AES.
Lead (Pb)
mg/Kg With referenceto IEC62321:2008 and
performedby ICP-AES.
lrercury(Hg)
mg&g Withreferenceto IEC62321:2008and
performedby ICP-AES.
Hexavalent
ChromiumCr(Vl)
mgikg Withreference
to IEC62321:2008and
pedormedby UV-VIS.
Polychlorinated
Biphenyls(PCBS) mgikg Withreference
to USEPA3g0C
(cAS No.:1336-3G3)
method.
Analysis
wasperformed
by
GC/rrs.
Polychlodnated
Terphenyls
(PCTs)
Polychlofi
natedNaphthalene
(PCNs)
oa
Alkanes,C1Gl3, chloro(Shoft
With referenc€to US EPA 3540C
ChainChlodnated
Paraffins)(CAS
method.Analysiswasperformed
by
No.:8553t0a-8)
GC/MS.
Pe|fluoroodanesulfonates
mgKs With referenceto US EPA 3540C:
(PFOS-Acid,
MetalSalt,Amide)
1996 methodfor PFOSContent.
Analysiswasperformed
by LC/MS.
PFOA(CASNo.:335{7-1)
m9Kg With referenceto US EPA 3540C:
1996methodfor PFOACont€nt.
Analysiswasperformed
by LC/MS(CASNo.:50{0-0) mg/kg With referenceto ISO 17226-11200$.
Formaldehyde
Analysiswas perfomed by HPLC/DAD.
Analysiswasperformed
by FTIRand
FLAMETest.
cmEm6, REest hElEielifidizliLbq.6fi-{s6-"
! . ? -" q r ' i
Er,]t&
fttrerdEE$dbyTconp'
I ohF d r.rr'r, 'n&nre'r
a{r]'d'do1's.!
e -.d w's'1 ary -016' d dBderuddad!e
tan*don ft6 a.B no ai h.r dod
comEry ary un&ibai srbEron bM
ori'iBrelon d b6 onbnr d.F
alnnr+nuunar-iI
q
10
3
n.d.
Negative
hr .
oodn.da Ti e oo@nofl @nd F sd
arapdciiv'rawd/firtd'rirr**Hmn:fiE
G
TestReport
Page:3 of 24
D e:2012102104
No.:CE/2012I14843A
Result
Test ltem(s)
Unit
Melhod
MDL
(CAS
BBP(Benzylbutylphthalate)
No-:85-68-7)
DEHP(Di-(2-€thylhexyl)
phthalate)
(CASNo.: 1'17-81-7)
DIDP(Di-isodecylphthalate)(CAS
No.:26761-40-0)
phthalate)
(CAS
DINP(Di-isononyl
No.:2855312-0)
phthalate)
(CAS
DNOP(Di-n-ociyl
No.:117"84-0)
(CASNo.:
DBP(Dibutylphthalate)
%
Withreference
to EN 14372.Analygs
was performedby GC/lVlS.
Withrofefenceto EN 14372.Analysis
wBspedormedby GC/lVlS.
With referenceto EN 14372.Analysis
wBspedormedby GC/IVS.
Withreference
to EN 14372.Analysis
rvasperformedby GC/MS.
Withreference
to EN 14372.Analysis
was perlomed by GC/MS.
0.003
n.d.
0.003
n.d.
0.01
n.d.
0.01
n.d.
0.003
n.d.
0.003
n.o.
0.5
n.d.
0.5
n.d.
0.5
n.d.
0.03
n-d.
0.03
n.d.
%
oa
y'Vith
Analysis
reference
to EN14372.
/vasperfomedby GC/MSl\Ionomethyl
dibromodiphenyl
mg/Kg Withreference
to USEPA8270D
methane(DBBT)
method.Analysiswasperformed
by
Go/tlls.
l\ronomethyl
mgikg Withrefefence
to USEPA8270D
dichlorodiphenyl
method.
Analysis
w€sperfomed
by
methane(Ugilec121)
GC/ttIS.
Monomethyl
tetrachlorodiphenyl mgikg Withrefefenceto USEPA8270D
(Ugilecl41)
methane
method.
Analysis
w6spefomedby
Go/tlls.
llll
|l]|||tllllll
CERAITTEC
GltlBH
MULTIFUNCTIONAL
LUITPOLDSTRASSE
15 D.91207LAUF,GERMANY
CERAI\/IICS
No.l
Limlt
u-74-2)
Organic-tincompounds
IributylTin (TBT)
IriphenylTin (TphT)
Halons
(CASNo.:353-59-3)
Halon-12'11
Halon-13o1
(CASNo.:75-63-8)
(CASNo.:124-73-2)
Halon-2402
mgikg Withrefefenceto DIN38407-13.
Analysiswas performed
by GC/FPD.
mgKs With reference
to DIN3840713.
AnalysiswEsperformed
by GC/FPD.
n.d.
mg/Kg with referenceto US EPA 5021
melhod.Analysiswas performedby
GC/MS.
mg/Kg With referenceto US EPA 5021
by
method-Analysiswas pertormed
Gc/tlls.
mg^g with refercnce
to us EPA5021
waspedormed
by
method.
Analysis
GC/tis.
redu€d..sdntur
comEfr [}ll B E$3! nE-L1l{91:!l:dzttfla
'mEn
a3 ndmsa
! 6_sd 4 bs
E
l Hd- lH4
-
l*lEii9 E
!.r dd*
<Bd4€
h.rr
i-*f,r
b r d or ib 'ftiwdo1
oits so {rhi
'dnffioi
tum ssEsm aii,ffi' nohbaiodcrm!
-ne b6rtuedori
comp.ny er mr6od&
a radoi
ta.ry o, tal6h6doi d rb 6ibd
or s
i "I f, I ft{.
d tE oodafl
n.d.
wLhdl rior k6
pomE! on d t6
;Bousd r.r 'do
a hrF. r Lbai /iurfi#JtE*$6nd4sct
TestReport
Pege: 4 d 24
Dale:2012102104
No.: CE/2012/14843A
rt|| tt]l
CERAIVTEC
GIVBH
LAUF,GERMANY
LUITPOLDSTRASSE
15D-91207
MULTIFUNCTIONAL
CERAI\/IICS
Test ltem(s)
Unit
Halog€n
(F) (CASNo.:
Halogen-Fluorine
14762-94-a)
(cl) (cAs No.:
Halosen-chlorine
22537-15-1)
(Br)(CASNo.:
Halogen-Bromine
10097-32-2)
(l) (CASNo.:
Halogen-lodine
14 24+81
MDL
Method
with ref€renc€
to BS EN 14582:2007Analysiswas performedby lC.
mS/kS Withreference
to BS EN 14582:2007.
Analysis
was performed
by lc.
mgKs With referenceto BS EN 14582:2007.
Analysiswaspedormedby lC.
mgKs r'Vithreference
to BS EN 14582:2007.
qnalysiswasperformed
by lC.
mg/kS
Result
No.l
50
50
n.d.
50
n,d.
50
n.o.
A3b€Bto3
AclinoliteICASNo.:77536-664)
Amosite(CASNo.:12172-73-5)
%
(CASNo.:77536-67Anthophyllite
5)
(CASNo.:12001-29-5)
Chry6otile
%
(CASNo.:12001-284)
Crocidolite
%
Tremolite{CASNo.:7753&686)
%
comD.frKJ AF.fl8n d H:8Rl{6,!
^i-ttlg(
t E-{R
Withreference
to EPA600/R-93/116
method.Analysiswas performedby
SM, PLMandXRD.
With referenceto EPA 600/R-93/116
method.Analysiswas performed
by
SM, PLMandXRD.
with refeence to EPA600/R-93/116
method.AnalysiswEsperformed
by
S[4,PL[4andXRD.
Negatave
Withreference
to EPA600/R'93/116
method.
Analysis
wasperformed
by
S[,],PL[,]andXRD.
Withreference
to EPA600/R-93/116
method.Analysis$raspedormedby
SM,PL[,]andXRD.
Negative
Withreference
to EPA600/R-93/116
method.AnalysiswEsperfomed by
SNl,PLNIandXRD.
Negative
l_" rE/r:
Negative
Negative
Negative
l"rJ n E{.
M€'rbqod.al'.€.b.d1qu
'miirnon or I rii ly. knnnfr€ron
end inld cds r$u6 dornd 6eF n Ad ho der or his dodmd
d.lftdi!'fti@lonf|rad#i
Fnldonbm.^esnoaida'
ndtr and od'G.tr3 ida, bs.6ieddi
a1 ruuroda-d a Fdoi,o$ry
.mFry
o.Elserol
d rhs @-6a o' I
effinr+Irror/rs|laa%|
tded
that into
' q!!g1ryr!:: ! li ll!'l5!:l?! NqrdF c! r'E{ / rirlrnsirL**FErn}t'n
l]l
Limlt
Test
Report
24
Pase:5of
No.: cE/2012/14843A
Date-2o1zo2to4
|ll
CEMMTEC GMBH
15 D.gl207LAUF,GERMANY
I\4ULTIFUNCTIONAL
CEMMICS LUITPOLDSTMSSE
Test liem(s)
Sumof PBBs
Monobromobiphenyl
Dibromobiphenyl
Tribromobiphenyl
Tetrabromobiphenyl
Pentabromobiphenyl
Hexabromobiphenyl
Heptabromobiphenyl
Oclabromobiphenyl
Nonabromobiphenyl
Decabromobiphenyl
Sum of PBDE3
Monobromodiphenyl
ether
Dibromodiphenyl
ether
Tribromodiphenyl
ether
Tetrabromodiphenylether
Pentabromodiphenyl
ether
Hexabromodiphenylether
Unit
MDL
lllethod
5
With referenceto IEC6232112008and
mg/Kg perfofined
by GC/MS.
5
5
5
5
5
5
5
5
|llt
R€sult
No.{
n.d.
n.d.
n.d.
n.d.
n.d.
n.d.
n.d.
n.d.
n.d.
n-d.
n.d.
5
5
5
5
5
5
n.d.
Heptabromodiphenyl
ether
5
n.o.
Octabromodiphenyl
ether
Nonabrcmodiphenyl
ether
5
5
Decabrcmodiphenyl
ether
5
n.d.
n.d.
n.d.
3
n.d.
AZO
to LFGB82.02-2.
1):4AIIINODIPHENYL(CASNo.l mg/kg Withreference
Analysiswasp€rfomedby GC/MS.
92-67-1)
m9/K9 With referenceto LFGB82.02-2.
2)i BENZIDINE(CAS No.: 92-87by GC/lvlS.
Analysiswasperformed
5)
3): +CHLORO-O-TOLUIDINE mg/Kg /Vith referenceto LFGB82.02-2.
Analysiswas performedby GC/MS.
(CASNo.:95692)
(CAS
4):2-MPHTHYLAIIINE
No.:91-59-8)
to LFGB82.02-2.
msftg with reference
Analysiswas perfo.medby GC/l/lS.
to LFGB82.02-2.
(CAS mg/kg with reference
5): O-AIVINOMOToLUENE
Analysis\ /as performedby GC/MS.
No.:97-5&3)
a;;;;hi
rtErca Di'-t+4r{.4-6HEc
(4d-r8..".:'-}
n,o,
n.d.
n.d.
n.d.
n.d.
3
3
n.d.
3
n.d.
3
n.d,
ro r)rl&"
inhel!lEI.'*i.d*d.dno'-*""d."**dcoturd;s
irii6iim-"j"in-inii*ij'iiilb''bnF.''.'[email protected]|fma.Doi!as1g{ws!sods4€i!g
]ii;;'6iifoidhnic!!aidiiirnidoili$@dmdMdn:ii;h;bl's];di{'md,i'ddmdi
ii
bs In !d c.a.n6rcr;i
i , i i , l i n d r,;"
,nii"e-- -r *"".i
;1;;
;-o
d, r*' "qtu ro d, odotu Ln6 h. t'nsdoi ooer.ma
baea d b 3'* * d ' r d;;:;;;';;;;l;
.o.oan, ay ..arho-a ,! s d-
-6{0''esb6d*w43@n|f!-!j'dgldg::ll
6cFaf,do.o!*rcdd6.dd
ni s [email protected] @nr b' €
doan"i4,"; ad a.o ot
llllll
Limit
1000
'1000
TestReport
No. ICE/2012114843ADaie:2O1Z0ZO4 Paoe:6 ot 24
tl]tI|tt
CERAIVTEC
GITIBH
MULTIFUNCTIOML
CERAIIIICSLUITPOLDSTMSSE
15 D-91207LAUF,GERIVANY
Testltem(s)
Unit
6)i 2'AMINO-4-NITROTOLUENEmgftg
(CASNo.:99-55.8)
7): P-CHLOROANILINE
(CASNo.: mdks
10647-8)
8): 2,4-DIAMINOANISOLE
(cAS
m9Kg
No.:615-05-4)
mg/Kg
9): 4,4L
DIAIIIINODIPHENYLMETHANE
(CASNo.:101-77-9)
10)r3,3'-DICHLOROBENZIDINEmg/kS
(CASNo.:91-9+1)
11): 3,3'-DIMETHOX/BENZIDINEmgikg
(CASNo.:11990-4)
12):3,3!DIMETHYLBENZIDINE mg/kg
(CASNo.:11993-7)
MDL
Method
With refercnceto LFGB82.02-2.
Analysiswas performed
by GC/MS.
With reference
to LFGB82.02-2.
Analysisw€sperfomedby GC/lVlS.
With reference
to LFGB82.02-2.
Analysiswasp€rformed
by GC/|\IS.
With reference
LFGB
to
82.02-2.
Analysiswas performedby GC/I\IS.
3
No.1
3
n.d.
3
n-d.
3
n.d.
Withreference
to LFGB82.02-2.
Analysiswasperformedby GC/MS.
3
n.d.
With relerenceto LFGB82.02-2.
Analysis\ /as performedby GC/MS.
3
n,o,
3
n.o.
3
n.d.
3
n.d.
3
n.d.
mgftg Withrcfercnceto LFGB82.02-2.
Analysiswasperformed
by GC/MS-
3
n.d.
mgKg With reference
to LFGB82.02-2.
by Gc/lvls.
Analysiswas performed
3
n.d.
3
n.d.
3
n.d.
3
n.d.
3
n,d.
Withreference
to LFGB82.02-2.
Analy6iswasperfomedby GC/MS.
'|3):3,3-DlMETl-lYL-4,4'msfts With referenceto LFGB82.02-2.
DIAMINODIPHEI.IYLIIIETHANE
Analysiswaspertormed
by GC/lVlS.
(CASNo.:838-8&0)
(2]!IETHOXY- mg/Kg A/ithreference
14):P-CRESIDINE
to LFGB82.02-2.
(CASNo.:
5-METHYLANILINE)
Analysis
waspedomedbyGC/l\Is.
120-71-8)
(215):4,4'-[,IETHYLENE-BIS(CASNo.:
CHLOROANILINE)
101-14-4)
(CAS
16):4,4LOXYDIANILINE
No.:101-80-4)
(CAS
17):4,4'-THIODIANILINE
No.:13965-1)
(CASNo.:9$
18):O-TOLUIDINE
Result
mg&g With referenceto LFGB82.02-2.
||ttll!t
Limit
Analysiswas performedby GC/MS.
mg/Kg
5s)
Withreference
to LFGB82.02-2.
Analysiswasperfomedby GC/IVS.
19):2,4-TOLUYLENEDIAMINEmg/kg With .eferenceto LFGB82.02-2.
(CASNo.:95-80-7)
Analysiswas perfonnedby GC/MS.
20):2,4,5-TRIItIETHYLANILINE mg/Kg
(CASNo.:137-17-7)
(CAs No.:9G
mg/kg
2'l): O-ANISIDINE
04-0)
With referenceto LFGB82.02-2.
Analysiswasperfomedby GC/lVlS.
y]/ith.eferenceto LFGB82.02-2.
Analysiswas performedby GC/MS.
inALF,{rr!-i-Eeaa
tdd- iMt, lg6"+_I T lil:' u?
fi;6d,n;dB;;;'iti;@ind]li'ibd.o'i..fgeicsdnf.,*rn6qrbilode,'6|.d.o'Gqus
ed io,asdtr'ctud6.r.n!
*tidri,Tds.{cdmiomb-6d
;i;bn;]ni'i;;.ii'nd6'ilnijii'nd;fusd.mn60DDnAilhdde.dFEoodnaa''.oIsdF,''ft
-€conFnvt{ts@o13b"t'
-mdor
ary
hs m' d tr! 'nbii$ron 6k and*'rin h 'redlrsrtr
adb.cpdLddrcpl|1tr|
Jiii'i''neton a L* ontoni;ii,pp*Eme t 'h s [email protected] k mrdd sna or*dare mai bo prcedd
ii;i'inil;lii;dn;;a;G;;;1iiiriiry
];i1ira&eD6ri^;i
I
iiij;j;;:;;;t
'l;idD;;;t
i;;J;
d3rcE
!t ea tu
r$JrLfi*l[**l!6tfiflffi*tr
1.p.n6-bs
Test Report
No. : CE/2012/14843A Dele : 201210204 Page | 7 of 24
l]|||lll
CERAMTEC
GI/lBH
15 D.91207LAUF,GERMANY
I\4ULTIFUNCTIONAL
CERAMICSLUITPOLDSTRASSE
unit
T€st ltem(s)
22):P-A[,IINOAZOBENZENE
(CASNo.:60-09-3)
(CASNo.:9$
23):2,4-XYLIDINE
68-1)
(CASNo.:8724):2,6-XYLIDINE
62-n
CFC's(Chlorofluorocarbons)
Group I
luorccabonl 1 (CASNo.:
Chlorof
75-694)
(CASNo.:
Chlorofluorocarbon-12
7171-8)
3
ReBult
No.1
n.d.
3
n.d,
MDL
Method
msfts With referenceto LFGB82.02-2.
by GC/lVlS.
Analysis
was performed
to LFGB82-02-2.
mg/Kg /Vithreference
Analysiswas p€rformedby GC/MS.
mdks Withref€renceto LFGB82.02-2.
by GC/MS.
Analysiswas performed
ll
llll
Limlt
3
mg/kg With referenceto US EPA 5021
method.Analysiswas performedby
GC/MS,
to USEPA5021
mg/Kg Wth reference
n.d.
method.Analysiswasperformedby
Gc/rlls.
to uS EPA5021
13 (CASNo.: MEKg with reference
Chlorofluorocalbonl
wasperformed
by
method.
Analysis
76-13-1)
GCiMS.
n.d.
luoroca|bon-1
14 (CASNo.: mgikg With referenceto US EPA 502'1
Chlorof
method.AnalysiswaspedormedbY
76-14-2)
GC/MS.
to Us EPA5021
115 (CASNo.: mg/Kg Withreference
Chlorofluorocarbon-
'|
n.d.
1
n.d.
1
n.d.
1
n.d.
1
n.d.
bY
Analysis
wasPertormed
method.
6C/MS.
7&'ts-3)
Grouplll
3 (CASNo.:
Chlorof
luorocarbon-l
7U72-9)
mg/kg With .eferenceto US EPA 5021
method.Analysiswas performedbY
GC/MS.
(CAS
m9Kg
with referenceto us EPA 5021
I1
No.:
Chlorofluorocarbon-1
method.Analysisvrasperformedby
354-56-3)
GC/|\,IS.
to IJSEPA5021
Chlorofluoroca6on-112 (CAS No.: mgKg Withreference
mehod.Analysis\o?sperfomedbY
GC/tVlS.
7B-12-0)
Chlorofluorocarbon-2l1 (CAS No.
422-784)
n,o.
mg/kg Wilh feferenceto US EPA 5021
method.Analysiswas PerformedbY
GC/t\4S.
r5!E?;':r"
YisfPlT
?':;'il*'Tl"il]lli*:::]]:il :"*'"-**-'"-"-"
"f::Fri
;:li";iy*T
B#;rftETtisi4u
?ilrl",il
ffffi**;"lu*:ffir*"ieB,:.mr""*r*:[''*'inmv""r*irf#ilfi€sitr;:t$ijii"{s#xpa#
**.s's*-"'frvi i ' i i i n n n i i i l i i w t i t i " * r r - " * o" :"'*r,*cl '-" a L ' " r , * r . " - . i i ' ' i ' ; ; t ; d n . ! . € d s d r o | d t r b
i;6;;:!,;uft
d; r;,oi'"
t . . . u , g . . * " ' ' o ' r . r ' g . ; ; 6 ; ; d n ' " d * r g d * " ' b . 6r;;;"n;;id'ialia
a * -'.j;:;;;;;
s",r ri'tdo'
"
oird*
ra b p6eo*d 6 n'
4riiFiciv,r
TrtiJLinSl[&*6EE
st!fi
TestReport
No.: CE/201214843ADale:2o1Z0AU Page:8 or24
l:]
CERAMTEC
GIVBH
't5 D-91207LAUF,GERMANY
ItIULTIFUNCTIONAL
CERAlrlcS LUITPOLDSTMSSE
Test ltem(6)
(CASNo.:
luoroca6on-212
Chlorof
3182- -1)
Unit
MDL
ll/lethod
to uS EPA5021
mdks Withreference
lrn
Result
No.l
n,d,
tllllll
Limit
Analysis
wasperfomed
by
method.
GC/MS.
3 (CASNo.: mg/Kg With referenceto US EPA 5021
Chlorofluorocarbon-21
method-Analysiswas performedby
235,L0e5)
GC/ttIS.
(CASNo.: mgKg With referenceto uS EPA 5021
Chlorofl
uorocarbon-2'l4
method.Analysiswas performedby
292sr31-0)
GC/MS.
luorocarbon-2l
5 (CASNo.: mgikg With referenceto L,SEPA 502'l
Chlorof
method.AnalysiswaspedormedbY
425943-2)
GC/MS.
to uS EPA5021
Chlorof
luorocarbon-21
6 (CASNo.: mg/Kg Withreference
method.Analysiswasp€rformedby
661-97-2)
n.d.
n.d.
1
n.d.
mgKs With referenceto uS EPA 5021
method.Analysiswas perfomed by
GC/MS.
1
n.d.
With feferenceto uS EPA 5021
method.AnalysiswEsperformedby
GC/t\4S.
mdks With refeence to US EPA 5021
method.Analysiswas performedbY
GC/MS,
1
n.d.
1
n,o,
mg'ks with referenceto us EPA5021
1
n.d.
1
n.d.
GC/l\rs.
7 (CAS No.:
Chlorofluorocarbon-21
422-86-6)
CHCa(Chlorinalehydroca.bon)
(CAS
1,1,1,2-Tetrachloro€thane
No.r630-20-6)
(CASNo.:
1,1,1-Trichloro€thane
71-556)
(CAS
1,1,2,2-Tetrachloroethane
No.:79-3+5)
(CASNo.:
1,1,2-Trichlorcethane
7900-5)
mgKg
bY
waspedormed
method.
Analysis
GC/MS.
to USEPA5021
mg/kg Withreference
method.AnalysiswasperfomedbY
GC/MS.
to USEPA5021
Withreference
bY
wasPerformed
Analysis
method.
(CASNo.:751,1-Diclloroethane
mg/Kg
(CASNo.:751,1-Dichloroethene
GC/|VS.
mg/Kg With referenceto IJS EPA 5021
s+3)
3s)
n.d.
method.Analysiswas PerformedbY
GC/|VS.
""" *- *"*'*
?.gT+:ex;1:FdT6l.f
8"*affirli;sffr':!t'i?+riFs.t'li::E?'"iri:'13i:
ib::T::a:":1:
::,T"
.morr;dti
r*bFbGq€E
'#.?n"i*inni#noi*i*t*b]66d'.tcodm!b,Ei.:i;;'d;;;6iw4.;'.''n
il"i].i,i.ii"ni.ii'i.ini"ii'i&tona"ai"d@,$6dd"*b.1";.;;;;;b';mda'1'''e"9dFai'
*r q-'r"r
i"i =n: j;nryt
r"a"'#te-a
n tr' do' oM r
*'pd'dsod
-"''-.*d;'a"'"j'iJ
;:'laa *6 n'@s rui € d@dd 't traikd 'asr db' &
-.. ru;p"i":,il iirn'i;;;
","0
-'"'..'
r"' ""'g*"o
", ".
drr F cehwd/ijll
txirrc+Ffi f fi ki*
Test Report
Paqe:9of24
No. : CE/201214843A Date:2012,0i,M
rrrfirnl||
CERAIVTEC
GIlIBH
15 D-91207LAUF,GERMANY
MULTIFUNCTIONAL
CERAIVICSLUITPOLDSTMSSE
Testltem(s)
Unit
(CASNo.:
1,1-Dichloropropene
563-5&6)
'1,2,3-Tridlloropropane
(CASNo.:
9618-4)
(CASNo.:
1,2-Dichloroethane
1O7-06-2)
MOL
ilethod
Result
No.l
mg/kg Withreference
to USEPA5021
n.o.
Analysis
wasperformed
by
method.
GC/MS,
MEKq Wiihreference
to uS EPA5021
method.Analysiswasperfomedby
GC/MS.
n.d.
mg/Kg With referenceto US EPA 5021
n.d.
method.Analysis\ rasperfomed by
Gc/ltlS.
(CASNo.:
1,2-Dichloropropane
msr'(g With refefenceto US EPA 5021
method.Analysiswasperformed
by
78-87-5)
GC/MS.
(CASNo.:
l,SDichtoropropane
mg/Kg With referenceto US EPA 5021
method.Analysis\oasperformedby
142-28-3)
GC/MS.
(CASNo.:
2,2-Dichloropropane
mg,Kg Wth referenceto US EPA 5021
method.Analysjswas performedby
594-20-7)
GC/MS.
Carbontetrachlonde(CAS No.:
mg/kg With referenceto US EPA 5021
56-235)
method.Analysis$/asp€rformedby
GC/ltlS.
(CASNo-:75-00-3) mgikg With .eferenceto US EPA 5021
Chloroethane
method.AnalysiswEsperformed
by
GC/|VS.
(CASNo.:67-66-3)
Chloroform
m9K9 With referenceto US EPA 5021
method.Analysiswasperformed
by
GC/MS.
(CASNo-:74-87- m9KS With referenceto US EPA 5021
Chloromethane
3)
method,Analysiswas performeclby
GCiMS.
(CASNo.: mg/Kg Withreference
cis-1,2-Dichloroethene
to USEPA5021
n.d.
n.d-
n.d.
n.d.
n.d.
n.d,
n.d.
method.Analysiswasperformedby
GC/MS.
15G59-2)
(CASNo.: mg/Kg With referenceto US EPA 5021
cis-1,3-Dichloropropene
10061-01-5)
melhod.Analysiswes performedby
GC/t\4S.
n.d.
pdued&€pl'nfujmhodpndd
i-h'.on
cohpaa
^iy !i'6od;j
Bsddh?n
o b,6r 6i toaery tr hrsheb
d h6 trhr
*ydeddroo*readlq{std
o
or apts
qrdF
.M ta wd / ii:lld,|ilt**FmliEffitri
:]l
Limit
Test Report
No.:CU2O1Z14U3A Dale 201210i,04 Page: 10 of 24
t]|lrr
CERAI/ITEC
GIlIBH
LUITPOLDSTMSSE
15 D-91207LAUF,GERIJANY
MULTIFUNCTIONALCERAI\'ICS
Tost ltem(s)
(CASNo.:
Hexachlorobutadiene
8748-3)
unit
MDL
llethod
mgKg Withrefercnce
to uS EPA5021
by
method.Analysiswasperfo{med
GCiMS.
to Lls EPA5021
lMethylene
Chloride(CASNo.:7+ mg/kg Withreference
by
method.Analysiswaspertormed
0$.2)
GC/l\rs.
(CASNo.:127- mgKg Withrefercnce
to USEPA5021
Tetrachloroethene
method.Analysiswasperfomedby
184)
GC/MS.
msikg With referenceto L,S EPA 5021
ttang1,2-Dichloro6thene
{CAS
No.:15G60-5)
(CAS
trans-l,3-Dichloropropene
No.:10061-02-6)
(CASNo.:79Trichloroethylene
014)
method.Analysiswaspedormedby
GC/MS.
mg/Kg With referenceto US EPA 5021
method.Analysiswas performedbY
Go/tlls.
mgKg With rcferenceto IJS EPA 5021
method.Analysiswas perfomed bY
GC/rVlS.
Result
No.l
n.d.
|ll|rlr
Limit
n.d.
n.d.
n,d.
n.d,
1
n.d.
1
n.d.
1
n.d.
1
n.d.
1
n.o,
HCFcs
(llydrochlorofiuorocarbom)
HCFC-21(CASNo.:75-43-4)
HcFc-22(cAs No.: 7545{)
HCFG3l (CASNo.:593-7G4)
mg/Kg With referenceto IJS EPA 5021
method-Analysiswas performedbY
Gc/lrlS.
mg/Kg With rcferenceto uS EPA 5021
melhod.Analysiswas perfomed bY
Go/tlls.
to lJs EPA5021
mgKg with rcference
melhod.AnalysiswasperfomedbY
GC/l\,IS.
(cAs No.:35,4-14-3) msn(gWithrcfef€nc€to USEPA5021
HCFo12'1
bY
method.Analysiswasperformed
GC/tus.
(CAsNo.:3*21-2)
HCFG122
mgrs
to USEPA5021
Withreference
bY
wasPedomed
Analysis
method.
GC/MS.
n.d.
*-"f
stf,i"S"13::89';'.i:'rs,":g"r",F:'r'..i:iEr8ffintr8yq;HlErTftf
ill1:-:1"::--':,::"'""***'*'*
'i,?i;d,r.a !;dbyb6hE
y*b@bbk..
c-d *.d;
i lti;it
ds'bcorim!'0,e6ft
iA;;
:i,itn,iar'Jniii.innft-m"*oi"ao"-*"a"-to-.*"'i'nd;;'F,;-..-''*d*drd";;:;;;;;;i;;
d n ; ; : ; ; ; ; i ; ; : ; ; a ; F ' i i i . , . 6 d c | f l s ' M d m . , a " y € c d n s n Y ' ! d . l . : p o 1 6 b ' i t } -ir err'
@;.;3
. -"....
tr. 8a...0
i;sd m 'n o.€r,i
o n d t . @ +"-*n
{dr4
_a'6
a @ n l D m a . , T a l d b E t o ' i b w d ' 5"o,s*"
n ir
6-d b trpq"-ed
"h113fr.{;*'""".HT:iS X
"€er
I lLmfrtE*FffinfiRtfi
TestReport
No.: C9201214843A OaIe:201210204 Page:11of 24
llfir
CERAIVTEC
GIlIBH
15 D-91207LAUF,GERMANY
MULTIFUNCTIONAL
CERAIIIICSLUITPOLDSTMSSE
Te3t lt€m(s)
(CASNo.:30G83-2)
HCFG123
Unit
MDL
ilethod
Result
No.{
n.d.
to uS EPA5021
mgKg Withreference
method.Analysiswasperformedby
GC/tMS.
(CAS
to USEPA5021
HCFC-124
No.i2837-89-0) mg/kg Withreference
by
method.
Analysis
wasperformed
GC/MS.
n.d.
mgKg With referenceto US EPA 5021
method.Analysiswas perfomed by
GC/l\,1S.
(CASNo.:1649-0&n mg/kg With refe.enc€to US EPA 5021
HCFC-132b
by
method.Analysiswasperformed
GC/MS,
to USEPA5021
(CASNo.:75-88-7)
mg/Kg Withreference
HCFC-133a
n.d.
(CASNo.:1717-006) mg/Kg with referenceto US EPA 5021
HCFC-141b
method.Analysis\Nasperfomod bY
GC/MS.
mdts With referenceto US EPA 5021
HCFG142b(CASNo.:7568-3)
by
method.AnalysiswEsperfoamed
GC/MS.
HcFc-221(cASNo.:422-26-4) mg/kg With referenceto US EPA 502'l
bY
m€thod.Analysiswas performed
GC/t S.
(CASNo.r42249-1)
mg/Kg With referenceto US EPA 5021
HCFC-222
melhod-Analysiswas performedbY
n.d.
HCFG131(CASNo.r35$28-4)
n.d.
method.Analysiswasp6rformedby
GC/tS.
1
n.d.
'I
n,d,
I
n.d.
1
n.d.
1
n.d.
Gc/rlls.
(CASNo.r422-526)
HCFC-223
mgKg
With referenceto IJS EPA 5021
melhod.Analysis\ /as performedby
GC/|\,IS.
(CASNo.:422-54-8) mgKg Withfeference
to USEPA5021
HCFG224
bY
method.Analysiswasperformed
GC/tVlS.
to USEPA5021
(CASNo.:422-56-0) msftg Withreference
HCFG22sca
bY
wasperformed
Analysis
method.
GC/MS.
n.d.
iilit f&iFi#riE:ii:E8fdJrjie'€BlYs"'r,Fi:*r51':*dI'sEi':'or:nrF6::i-::1::l
l"*^'*-*-"*
asq.dregL6n.?!omsd..66e1ado!..adaI'!b€olELg'
;;;;;H.;.;t-d"*..ft!'.idhr"-.-dc*d'6-b#;i;6;,n'i's*4!or,sf.m
; i ; ; d ; n ; i * d - - | v * " * h 1 " " r . " e c . l .".n* .r -' a. i-i -] r- y* ei d. .; "c*o"a, i;''i;"!.do.6€dsdf gs od |E, vt dl b, i a d s o ' ft'"*r'nrrc'b'Fru
'"
*;"iihr;tui
r" or s,r *' *s
ldr
':;"@i':ri;in
- * ". -;:E;;;;
md ftnds
fuY b Pm
a rred. vr.dii
/ ttitirfiJ|x*mBndst6t
l
lllll
Limit
TeSt
RepOft
No.:cs201214843ADare:2o1zozo4Pasetl2ot24
tl
CERAIIITEC
GITIBH
MULTIFUNCTIONAL
CERAIVIICS
LUITPOLDSTMSSE
15 D-91207LAUF.GERITIANY
Test ltem(s)
Unit
MDL
Method
(CASNo.:507"55-1) mgKg Withreference
HCFC-22scb
to USEPA5021
method.Analysis\oasperfomedby
GC/t\4S.
-87-8)
(CAS
HCFC-226
No.:431
mg/kg Withreference
to USEPA5021
wasperformed
by
method.
Analysis
Go/tlls.
HCFG231(CASNo.:421-94-3)
m(/kg Withrefercnce
to uS EPA5021
method.Analysiswasperformed
by
GCiMS.
(CASNo.:460-89-9)
HCFC-232
mg/Kg Withreference
to USEPA5021
melhod.Analysiswasperformedby
GC/t\4S.
HCFG233(CASNo.:7125-84-0) m9ks Withrefercnceto US EPA5021
(CASNo.;666-27-3)
HCFC-241
by
method.Analysiswasperformed
GC/MS.
mg/Kg With referenceto US EPA 5021
method-Analysiswas performedby
GC/t S.
mgKg With rcferenceto US EPA 5021
method.Analysiswas performedby
GCA4S.
to USEPA502t
mg/kg Withreference
(CASNo.:460-63-9)
HCFC-242
mgKg
HCFC-234
{CASNo.:425-94-5)
HCFG235(CASNo.:46G92-4)
HCFS243(CASNo.:46G69-5)
Resull
t{o.'l
r mrrll|l
Limlt
n.d.
n.d.
n,d.
1
n.d-
1
n.d.
1
n.d.
1
n,d.
1
n,d,
1
n.d.
wasperformed
by
method,
Analysis
GC/MS.
With rsfefenceto US EPA 5021
method.Analysiswas perfomed bY
GC/MS.
mgfts With rcfefenceto US EPA 5021
method.Analysiswas performedbY
1
GC/tVrS.
HCFG244
(CASNo.:42141-0)
HCFC-251
msas Withreferenceto uS EPA5021
n.d.
by
Analysis
wasperformed
method.
GC/MS.
to USEPA5021
mg/kg Withreference
bY
method.Analysiswasper{ormed
GC/MS.
n.d.
":1::: - ll-:"'*-***""*
H#n#Hyqgg1:iffdf
+rsfi;T,.ffi8flq;i:"r."fi-tq"r'
jrj"er***:n*,f*njtru"rln*:."sltr,s:sr.".1x-rffrf*rrlgirsi"",Lrx$;"'trili:'#*tr"'r#ii**'".o*;
EUs o.rne t6c' 'ii; hod.'d rF .oor.a teied rar 'r'io
i"iu'.,i,i mnrii
oo iiddr
t i , i i i . ' . . g ' n r o - ."i'i#i-m^
* - ' - o . r i n ' h . ' n | E d c | 5 1 s , d d o T : ; i ' ; i . i ' " " J i " d . g p o * b ' . ' o -' ti s' oco| €d nn hi ' d6 '110- ', B
. d ' m o a m 4 m . 6 @ p rn a l
aad'ed
€maffqoo.e_'
r;;;;n';;ou_od
rs ns.
bilru;ad
36rdu 4d on ideB rut b p@ork
bs'ry d dr ier m d b.6nbdi;;F-;;at
cam;ry Ary-.dtu;.dEErm.
b he tuhd 'ns( d b' a*
ryrr+! crr ri wd / firlfisrlE+FmnERt*
TeSt
RepOft
Date.2o1zozo4
Pase:13or24
No.rcE/201214843A
|l] ||ttl[Ilrt]r
CEMMTEC GMBH
IVIULTIFUNCTIONAL
CERAMICSLUITPOLDSTMSSE
15 D-91207LAUF.GERMANY
Teetltem(s)
(CASNo.:819-0t!1)
HCFC-252
HCFC-253
{CASNo.:460-35-5)
Unit
Resull
MDL
Mothod
mgikg with refefenceto US EPA 5021
method.Analysiswaspedormedby
GC/MS.
mgKg Withreference
to USEPA5021
No.l
1
n.d.
1
n.d.
method.Analysiswasperfomedby
GC/MS.
(CASNo.:420-97-3)
HCFC-261
mg/kg Withreference
to USEPA5021
method.
Analysis
waspedormed
by
GC/|VS.
(CASNo.:421-02-03) m9Kg Withreference
HCFG262
to USEPA5021
method.Analysiswasperfotmedby
GCiMS.
(CASNo.:430-55-7)
HCFC-271
Limit
n.o.
n,d,
n.d.
mg/Kg With referenceto US EPA 5021
method.Analysiswas perfomed by
GC/MS.
= 1000ppm
1. mg/kg= ppm : 0.1wro,6
2. n.d.= NotDetected
3. MDL= llethod DetectionLimit
4."-"=NotRegulated
5- * = Qualitative
analysis(No Unit)
6. Negative= lJndeteclable/ Positive= Detectable
7. Asbestos: Negative= "< 1.0%", Positive= "> 1.0%"
PFOS Reterence Information : POPS- (EU) 757/20'10
productsor
above0.001%(10ppm),in s€mi-finished
or preparations
in conc€ntrations
OutlawingPFOSas substances
in textilesor othercoatedmatedalsabove1ug/m2
adiclesor partsat a levelabove0.1%(1000ppm),
'ntrBb3l€Fntt'01ylo.h.qd
cdmdi!kJr
El *qs { HlElllltflr'llH2Efi 61 " 4H& l Iti :)"lBd ldil l s _]ta'
_i;;n.1
mrud oi.^tr *dbds r @
Ed.d o d; cmFni aoF b tu crs6 coo'm; dlrc
A;;;i#';€!s;;;'atii"d
brd dntr+b &d@ b-!-' {d c"-ft-, h' ii;;;;
am.ro.ortu
i;;ft;d;
rbtilt'. hdanMata'iii"d i'iir;liai(n ''is ddlrei iDrein it; i'di* t h€ demi, 'isd{si ba iro
ftled'B'fumdmfxflo*o:1l€|fi.3dL.dlBl1ffgi!nyD.!mpa1yss€ceo'3'b|i,Gb
ft6 d*rsd e..d ba F
re
h6 Endon @ritu
migoo. rt""*go"|*'
ohb ro d{.r@
or $h edm$r ts m r[{ur sd
. i.dbi; hosry d h]!'idi
orih€ obi;i;iF,Ae
.mpanr tur d.dodd
crdido-lr'T€
o-6trs
abnb'306*roh'
ompaivi ird ie3d
4 hlts .lq,rawd / FirLrrirrd*Erdrifrffirs
Test Report
paoe: 14 of 24
No.: CE/201214843A Date:201i,02t}4
CERAMTEC
GMBH
MULTIFUNCTIONAL
CERAIJICSLUITPOLDSTMSSE
15 D-91207LAUF,GERIJANY
t]
tl| [ttttlrl
1 ) Thes€sampiesweredissolved
totallyby pre-conditioning
meihodaccording
to betowttowchart.
( Cf'lest methodexcluded)
yang
2) Nameoflhe personwho mademeasuremenl:
Climbgreat
3) Nameoflhe personin chargeof measurement
TroyChang
Samplelvleasurement
Aciddigestionby suitableacid
clepended
on differenlsample
mateial(as belowtable)
Microwave
digeslionwith
HNO/HCI/HF
Heatlo appropriate
temperalurelo exiract
Cool,tilterdigesiate
AlkaliFusion
HCllo dissolve
ICP-AES
SampleIVaterial
throughfilter
Add diphen9-carbazide
for
DigestionAcid
Steel,copper,aluminum,solder
Aquaregia,HNOr,HCl,HF,H,O,
Glass
HNO3/HF
measurethe absorbance
Gold,platinum,palladium,
ceramic
Aquarcgra
at 540nm by UV-VIS
Silver
HN03
Plastic
HrSO4,HrOr,HNO3,HCI
Others
Any acidlo totaldigestion
[email protected]
co.Dar t? / B l ;?!i .rlRA1l Rl6?ldlSt,&AlF? 4E- 1144- "i*EjAl
T lS.nlb!
I d brsd ro 'b c3?d cfdrol - d s.
usd b rmE 'i cond' m3 tu .tu
inturondrdrt idmnfieron,ndluddturrslsd.fn.dh.Dn.Adh
feyTh.comFrybe|'rs4odbity
cmFny tuy uiadoda
du6d.6€0tintur wr$dpdoffrlGnpomsdndb.
abdoii '@dryd h]3fidoi orrh€6L*r oraoFadtu. orlh s dodn.d c ui.['ur.nd on€nds n.i b6pGeMed b ib tu *id;ddb6rtu
*"un,,,i"&1,1ffii*,I
il{,tliiilgtiffI1?lil'"
T-
TestReport
No.: C9201214843A D3l.e:201210?,04Paoe:15 ol24
CERAIIITEC
GITIBH
MULTIFUNCTIOML
CEMI\4lCS LUITPOLDSTMSSE
15 II91207 LAUF.cERltlANY
t][Ilmfirllltl
Analyticalflow chan of Soxhletextracgon(LCIMS)procadure
a
r
Nameoflhe perconwhomademeasurementRomanWong
TroyChang
Nameof lhe perconin chafgeof measurement:
I Test lten3: PFOS/PFOA' Benzotriazole)
pretrcatmenuseparation
Sample
I
Data
comDafr
[r ]l-dFdE nH-LxlAlrrl:L:EtAa
and rq*ftntrmardidm*6
'c,':trr'6n.r.or19
" td;.
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i
A..bA
$68
6r6m3ed codhoGbrErtunc
ooomsds.t trw $'@n/ddnE
@!rn a.yrredd!dcmrdad!Hhi
l;-{rrdn <isdd
dir€'
[email protected],
.nd drsdon!
d edon! une
Lnd u.
b. hns.dori
[email protected]
eft.ro
ri
rh s3 ddmed
odn.r
-
ennor
endb b Ep.de
€p.d!E.
r tu
L ulM
wrd
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ha
sopt
sEp(
sopr n
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r.
w1M pnor
TeSt
No.:cEt2o12t14843A
24
Date.2o12to2to4
Pase:16of
RepOft
CERAMTEC
GMBH
I\4ULTIFUNCTIONAL
CERAI/IICSLUITPOLDSTMSSE
15 D-91207LAUF.GERMANY
Chlorinated Flamc retardant analytical flow chart
1) Nameoftheperson
whomademeasurcment:
BaryTseng
2) Nameoftheperson
in chaeeof measurenent:
TroyChang
I
r
Refercnce
method:
USEPA8270D,
USEPA3540
Teslltems:PCBS,
PCNS,
PCTS,
ltlkex,Ce MCCP
Data
C o m o a n h lq F e s r ' n E ; g F l { ? , s : i z t s , r E ! .
nbrond16rq'T*rnelonsrd
i
rn-I&
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pr€13)
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rfy
rh comFny6 de 4o$
'bi,v
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ll|l|t
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Test
No.: cE/201214843A
Date:2o1zo2!o4PasetlTof24
Report
|l][t
CERAMTEC
GMBH
ItIULTIFUNCTIONAL
CERAMICSLUITPOLDSTMSSE
l5 D'91207LAUF,GERMANY
Analysis flow chart for delerminalion of PVC in matorial
r
I
GinnyChen
Nameoflhe personwho mademeasuremenl:
Nameofthe personin charceof m€asurcmentr
TroyChang
Sampleanalyzedby FTIR
Chec* wave-numberof C-Clbonding
i n s s b { D F n ' $ e l o n ] y l o l h € & o p l @ d u d r e p t i f u | , d o d p i d " r i
'nEryrilTEl,&sj
,{HAl"i*l49l1li"E.:&flAE lEd- kl,l1, \.13 til
lq! llCS
rnhd€um$tlaig.dby1h6c0np.ry!ub]6dbbGsmBcodlon6ds
blddbr.-..nd cf d !0.Eb Er*n
-.*".;;i: il:|
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Test Report
No. : CE/2012l148434 Dai€.2O1ZOZO4 Paoe: 18 of 24
CERAIVTEC
GITIBH
MULTIFUNCTIONAL
CERAMICSLUITPOLDSTMSSE
15 D-91207LAUF,GERIVANY
trfllrI.
tllllll
Analyticalflowcha of Soxhlet€xlraction(GC/MS)procedure
I
r
Nameof lhe personwhomademeasurement
RomanWong
Nameoflhe personin chargeofmeasuremenlTroyChang
(TeEtltems:Phthalate' B€nzotriazole. HBCDD. NP . DBBT.
Oryanicphosphorus
compoundrs)
* ihdr Fiorwins p€m3sond h3
nrh.radGoodcrdontb{i.*nr€{e)l.sd.h6bn@od6nmLsrcpodu€d.€^6prrntur
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td&l:ldf-qEFdb
corraaBr. e e@ !BS4Fr*tdj^+-as
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ns4{4oT
on/rsd*0oor.i
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am codtms w
imibron d rdrt idmnneton l;d ':id doi i$u.s dsfind b.6 i Air io d.r ol rhi3doonenl adu$d hlr 'ft
u.lim.fi1!nEii€ntmd'ands.liin1i.imibo'c||€n|li9rudo6iai,rhconFnybd3r..ponEb''
-@didouMts
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cmFny Ary uruubodair abdon foasry or fsltr€ron or h' @i6d or ap
TestReport
No. : CE/201214843A Date:201i,02104 Page: 19of 24
CERAI/ITEC
GI/tBH
MULTIFUNCTIONAL
CERAIVICSLUITPOLDSTMSSE
15 D-91207LAUF,GERMANY
lll|t|::
l]t
Analyticalflow chart of Organic-Tincontent
I
I
Nameofthe personwhomademeasurement
GinnyChen
Nameoflhe perconin chaee of measurement:
T.oyChang
Concenbate/Dilute
Exkacted
solution
Analysiswas perfomedby GC/FPD
Dala
CmEi!hl
EJ8!
i E ,ERHtlr€ll2ll
l A r " IE"{t{|
i J.,b8l
"4h:n:
,ond oftdSe1uDnftdoER
drrdr.rerdco.ono$6rEr.m
oducdeeplifuldbodp'old
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iandid on E6
dnd
tudn An' h
rh rh6 dbideiadoi
onrvsnd * ihii h6 rh r d c iad3 insdons
iiry
hneo m rdm .rcEsm dl hq notu so dro.ron! und h. b.n*dod @
compary Ary unadhoruA rE,!r n bqary q bls i€ln
d hs trhr
or ap
n"**.,ffiiu';tl.':ji,;H.Jiil*iilI1n
$ff,991"**tr,i:1.""-,nu*'u***oon*.*
I
Test Report
No.: CE/201214e43ADale: 201210?,04Paoe:20 ot 24
CERAMTEC
GMBH
II,IULTIFUNCTIONAL
CERAMICSLUITPOLDSTMSSE
15 D.91207LAUF,GERMANY
Analyticalflow chart of halogencontent
1) Nameofthe personwho mademeasuremenl:
RitaChen
2) Nameofthe personin chafgeof measurement:
TroyChang
Sampleprelreatment
/ Sepataiion
Weighting
andputtingsamplein cell
OxygenBombCombustion
/ Absorpiion
Dilutbn10fixedvolume
Analysis
wasperformed
by lC
conFl[i]l teS3! -[HiL+liti]13
lliiAA. ldA f Ad .-FditE
rcddm. E s".d d u. cmEn
3d ro dftnrbrddLnfb
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i'ln*idm s6
ddd
badn. Anr fd
tErm.d6'miwmononkaowft
ihrmcrC
ads n$trotr3 iin
hiso
m irem &sE,ft
dl h.r iotu eo dr oar on! Lne h. hlnsdort
ecmda
comp'a Any!m6o,ze
dEErm'toEerydbsidbdhstrblorap
i " Eo\tqr'
ms odr6a
6nd
ba Eru
*-,nu"nuo*"*"oo"o
*"*'*ffilil]iio\'3;Il;k,ifig;|ff l"t*$$#gll"*.,lll:]"!k
TestReport
No.: CE|2O1Z14843A.Date: 2O1ZOZO4 Paae: 21 of 24
CEMMTEC GIMBH
MULTIFUNCTIONAL
CERAIJICSLUITPOLDSTMSSE
15 D-91207LAUF,GERIVANY
Analysis flow chart for determinationof Aabestos
1) Nameof the Dersonwho mademea6urcmenl:
VictorKao
2) Nameofthe personin chargeof measuremeni:
WendyWei
l6 )
I Refercncemothod:EPA600/R-93/l
Conlinuewh€nproblem€
a€ encounle€dwithPLlvl
and/orfor qualily assurancepurpo€€s
Inleriercncemahi\ removal
Asbeslos identificationby dispersion
stainingpobnzationlightmicroscopy
A€bestosidentiticationby X-€y
Notconraining
Asbesros/
cnFnyRJ BA&.8 {E: *lRl6flnld -AB Frt IEd-*l{4 \:ltffril
nidhi
d ri'driry. id.mn ieln
rE$don tm d.eno.i
cdmFry Ary u@rb4n
r.JfllSp
@dudrepliful.dodpidfr
'id j
h., nod
sbdon
blw
or raibf€ton
F hnEdon oodn.nri
d b. @ftdtr
@
Tdeoo@r
** f,iFi$l' I ;i*,?1.;r,];'i[il::t;.,]-**u;]'*.,
r ar'eb.,.lr
'**...*.
Test Report
No.: CEi2012l14843A Date: 2O1Z0ZM
Paoe: 22 ol 24
CERAITITEC
GMBH
IJULTIFUNCTIONAL
CERAMICSLUITPOLDSTMSSE
15 I}91207LAUF,GERITIANY
Analyticalflowchart
I
I
Nameof lhe personwho mademeasurcmentRomanWong
Nameof lhe personin chargeofmeasurement
TroyChang
TBBP-A-bb)
I Tesl llem3:PBB/PBDE,
pfoceEs---.
Firsllestingproc€ss-----+ Optionalscrcen
proces€-.>
Confirmation
Screenanalysis
'Li-;iirn-rrn;i;;;i.ii
.i;ii.
Sampleextraclion
method
Concentrale/DiluteExtractedsolulion
Filter
Analysisby GC/lt/S
lssueRepod
c o F o . r a JF H & ! i - { & d E
- l l q U d l nI E E A { . i € b f l 4 d r " - s a , q .
-d6rnh6dolend
irturondrdi
t
sa.ftdn<ifuMonf|ya'od
bjd b rffir
ad codi
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m3 tu E 6dm
b a ' d d i s . f 3 ' r d e . ' 0 . ? 9 d o n p d L e d 4 e p l i l f u |
.r
t]ttllll||Iltt]l
Test Report
No.: CE|2O1Z14A$A Dale:2012102104Paoe:23 of 24
CERAMTEC
GI\,iBH
MULTIFUNCTIONAL
CERAI\/IICS
LUITPOLDSTMSSE
15 D,91207LAUF.GERMANY
Analyticalflow cha(otvolatils oryaniccompounds(VOCS)
I
I
Nameof lhe personwhomademeasuremenl
: ChunWu
Nameof the personin chargeofmeasurement
: ShinjyhChen
I Referencemelhod : US EPA 5021)
Samplepretrealmenl
Takesampleandputil into
glassware.
headspace
o r p a n y u Jt l r ; t 8 r ' { F 1 t : R @ 9 l d l t 4
&-AE
lEl,-{lil
":-"q
. rE&"
nlfltm
lm0trmt
Test Report
No.: CEI2O1Z14U3A, Date 201210?,A4 Page 24 ot 24
CEMMTEC G[/lBH
MULTIFUNCTIONAL
CERAIVICSLUITPOLDSTMSSE
15 D-91207LAUF,GERMANY
r:|| tt]||ln|rr|l
* The tested sample / paft i6 marl(ed by an anow if if,s shown on the photo. .
L4843
** End of Report "
cmF.th/
- t s f u 9 1 3 i gtq$qS
. d b y s o .llmel
ffF
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llt li"
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-_*-***-_*^_1
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T€6tRgport
No. SHAEC1116009840
Date:14Oct2011
Page 1 of 5
I\4ATERIAL
CO.,LTD
ASIAGENEMLSOLDERING
& BRAZING
ZHEJIANG
PROVINCE.CHINA
CITY,ZHEJIANG
XIHUINDUSTRIAL
PARK,SANDUN,HANGZHOU
SoLDER
was/were
submitted
andidentified
onbehalfof theclientsas : LEAD-FREE
Thefollowing
6ample(s)
WIRE
- SH
SP11-030781
SGSJobNo.:
ModelNo.:
Composition:
:
Dateof SampleReceived
TestingPeriod:
Test Requested:
Testl\rethod:
T€stResults:
YTW206
Sno.3Ago.7ouoe
09Oct201'1
09Od 2011- 13Oct20'11
Seiectedtest(s)as requestedby client.
Pleasereferto nextpage(s).
Pleasereferto nen page(s).
Basedon the performedtestson submitteds€mples,the resultsof Lead,
l/lercury,
(PBB),
Cadmium,
Hexavalent
chromium,
Polybrominated
biphenyls
Polybrominated
diphenyl
etheE(PBDE)
complywiththelimitsas setby RoHS
Direclive
2011/65/EU
Annexll; recasting
2002/95/EC.
Conclusion:
Signedforandon behalfof
SG$CSTCLtd.
7Qv
Fan Jingjie,JJ
Approved Signatory
l'Arhlh,.olbhdx,,f4tnCratrt
t! .tl.*trAltl€3oTlft
tt
z(Mc
2!@o
ra[(6r?r)01@@ lElE6-?l)G€SE
8L{a-z}G1/t@14 rIj(!F.?r)6aat63
rna{.6
.q.d'ire.!.@
Mbfit.r ot rh. SOSgrllD (SGSSA)
SGS
TestReport
No.SHAECl 116009840
Date:14 Oct2011
Page2 of 5
TestResults:
TestPartDescriotion:
sp€ctmenNo.
I
SGSSamdelD
D€6cridion
SHA11160098.035Silverymotalwire
Remarks
:
(1)1 mgikg=1 PPm:00001%
(2) MDL= lrethod DeteclionLimit
(3)ND= NotDeteded( < irDL )
(4) 1" = NotRegulated
RoHSDir€dir€ 2011/65/El,J
TestMelhod: Withreferenceto IEC62321:2008
(1)Determination
ofCadmium
by ICP-OES.
(2)Determination
of Le€dby ICP-OES.
(3) Dotermination
of Mercuryby ICP-OES.
(4)Detemination
l\rethod
usingUV-Vis.
of Hexavalent
Chromium
by Spottest/ Colorimekic
(5)Detemination
of PBBS/ PBDES
by GC-lvlS.
p35
tioi!
Udt
MDt
10O ms/ks
2
N
D
Test ltem(s)
Cadmium(Cd)
Lead(Pb)
Mercury(H9)
HexavalentChromium(Cr(Vl))
Sumof PBBS
Monobromobiphenyl
Dibrcmobiphenyl
Tnbromobiphenyl
Tetrabrornobiphenyl
Pentabromobiphenyl
Hexabromobiphenyl
Heptabromobiphenyl
Octabromobiphenyl
Nonabromobiphenyl
Decabromobiphenyl
Sumof PBDES
Monob.omodiphenyl
eiher
' ad!rrr
!6do bnr
cM9.'r.r{.db
d.d|nd,e{d
nr osdrc.ir,!M.
b rh.
1,000
1,000
mg/kg
mgr'kg
1,000
-
mg/kg
ms/Kg
mg/Kg
mg/Kg
mg/Kg
mgKs
mgKg
mg/Kg
mg/Kg
-
mdks
mgrc
1,000
_
mg/kg
mgKg
o.srri..
rhd
d.n t,.6rd.
dd ltr (bn,t
L .d{r{d
(rw. 'lh.Coolsrt
6r. dhi.rb
i{N|lll.!to!.ntl
h.f{odo,
bnc.tr0
.6uerhhEd|m
.rnr tul
, rq!.yri..ridrs
dun .hsr.dr&inedbi.'cirb'h.rnr.(.)tnrd.
f tatrtGYt$dldrer4$.dJttrr
tI -.tl.;EEltltas|!+l
2
2
O
.
4
1
N
D
Negalive
N
D
5
5
5
5
5
5
5
5
5
5
-
N
N
N
N
N
N
N
N
N
N
N
D
D
D
D
D
D
D
D
D
D
D
5
N
D
{.q!d
4 dr*h.r
hrbrrwr.s.6fl,rrn
6d*i.d h.n* dd
t.c4.it
!.rliioo.dr
rr r.6tbCr{d.nnt&.uMrnnrd.ffibF
FpD&-d.rdpt|nMr,*dE6rrr*di'irr9d,orrn
2@39
ll.2@3
IE EIF?)01@63 lElEP6-AJ6{$t0
HL{e-20611e5e1n:{6-AFra0@3
d
6d!,q!!
drbrtuEe
aomo.rr.
fr o.ll.m
..Sd1-Ee96
Mdb6. or*|e aOs Or.!p (gqg s,{)
TestReport
No.SHAECl116009840
ud!
tini!
I€U19nISI
mS/kg
mg/kg
mdkS
mg/kg
mg/kg
mS/kS
mSftS
mg/kg
mg/kg
ether
Dibromodiphenyl
ether
Tribromodiphenyl
elher
Tetrabromodiphenyl
ether
Pentabromodiphenyl
Hexabrornodiphenyl
ether
elher
Heptabromodiphenyl
ether
Oclabromodiphenyl
ether
Nonabromodiphenyl
ether
Decabromodiphenyl
Date:14Oc12011
MDt
5
5
5
5
5
5
5
5
5
Page3 of 5
a5
ND
ND
ND
ND
ND
ND
ND
ND
ND
Notes:
permissible
(l) Themaximum
Annexll
limitis quotedfromdi€ctive201'1/65/EU,
(2) o spot{est:
Negative= Absenceof CrVlcoating,Positive= Presenceof CrVlcoating;
methodif the spottest resultis
Thetestedsampleshouldbefurtherverifiedby boiling-w€teFextraction
Negativeor cannotbe confimed.
o Boiling-wateFextraction:
Negative= Absenceof CrVlcoating;Positive= Prcsenceof CrVlcoating
in boiling-water-extraclion
solutionis equalor greaterthan0 02 mg/kgwith50
Thedetectedconc€ntration
cfi" samolesurfa@area,
on sto€ge conditionsand prcductiondateof the
Forcorosion protectioncoatingson metals:Information
andthusresultsof Cr(Vl)representstatusof the sampleat the timeof
lestedsampleis unavailable
testing
k .I.r
rl! dffi
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ly fu coitsry $!l.d
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TestReoort
Page4 of 5
No.SHAEC1116009840 Daler14Oct2011
ATTACHMENTS
RoHSTestingFlowChari
Xu
Wangy'Allen
Xiao/Gary
1)Nameof thepersonwhomadetesting:JanShi/Yoyo
Xu/ElimLin
2) Nameof thepersonin chargeof testing:JeffZhang/George
methodaccofding
to belowflowchart.
totallyby pre-conditioning
3)Theses€mples\Neredissolved
(Cr6+andPBBS/PBDEStest
methodexcluded)
SampleMeasu€ment
PBBs/PBDE8
Pb/Cd/Hg
1) AlkaliFusion/
DryAshing
2) Acidto dissolve
FiltratonandpH
adjustment
Adding1,5diphenylcalbazide
for color
development
lnrd@nd
b hd
by rbor''tsry &qdb
d.din'.r4d
rl (l|.orcor'attd..l3.d€
br.mq{
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v 6..rbk
x4rr|k
rndd dEd.tt .rhbb
ffi .r]oidr'n...ddii6:
Effii;Eiiita!-iEa-fl..tu
Adding
1,S
diphenylcarbazide
for color
development
A redcolor
indicates
the
presence
of cf.
nece66ary,
1[a!!a4nr4!!44_@_E!4Ld.
d
!!a]r
mli-nffi
F6-666i
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.te.-d'netF@
(8OSS)
MolnDor
olrh.sGSGorrP
SGS
Te6tReport
No.SHAEC1116009840
Page5 of 5
Date:14Oct2011
Samplephoto:
sHAl1-160098.035
reportonly
SGSauthgnticate
th€photoonoriginal
"' End of Report *'
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TestR€port
No.SHAEC1116009839
Date:14 Ocl2011
Page1of 5
ZHEJIANGASIA GENERALSOLDERING& BRAZINGMATERIALCO,,LTD
XIHU INDUSTRIALPARK,SANDUN,HANGZHOU
CITY,ZHEJIANG
PROVINCE,CHINA
Thefollowing
sample(s)
was^/vere
submitted
andidentified
on behalfof thecrients
as : LEAD-FREE
soLDER
WIRE
SGSJobNo.:
ModelNo.:
Composition:
Dateof SampleReceived
:
TestingPedod:
Test Requested:
- SH
sP11-030781
YTW102(692539-002)
Sn2.ocuRE
09 Oct2011
09Oct2011- 13Oct2011
Selectedtest(s)as requestedby client.
Test Method:
Pleasereferto nextpage(s).
Test Results;
Pleasereferto nextpage(s).
Basedontheperformed
testson submitted
samples,
theresultsof Lead,
Mercury,
Cadmium,
Hexavalent
chromium,
Polybrominated
(pBB),
biphenyls
Polybrominated
diphenylethers
(PBDE)complywith
thetimitsas setby RoHS
Directive
20'11/65/EU
Annexll; recasting
2002/95/EC.
Condusion
:
Signedforandon behalfof
SGS-CSTC
Ltd.
7Qv
Fan Jingjie,JJ
Approved
Signatory
rd adlrN
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M6nboror$€ 69S Oroop(SGSa )
TestReport
No.SHAECl116009839
Date:14 Oc12011
Page2 of 5
TestResults:
Test PartDescdotion:
SpodrnonNo.
SGSSamptotD
DosoriBlon
I
SHA11_160098.034Si|very
metalwhe
Rem€rks:
(1)1 mg/kg= 1 PPm=0.0001%
= MethodDetection
(2) IVIDL
Limit
=
(3) ND NotDetected
( < MDL)
(4)"-" = NotRegulated
RoHSDl€dive 2011r'65/EU
TestMethod: Withreference
to IEC62321:2008
(1)Determination
of Cadmium
by ICP-OES.
(2)Determination
of Leadby ICP-OES.
(3)Determination
of Mercury
by lCP-OES.
(4)Determination
of Hexavalent
Chromilmby Spottest/ Colodmetric
MethodusingUV-Vis.
(5)Deterfiination
of PBBS/ PBDES
by GC-IrS.
Test ltem{s)
Cadmium(Cd)
Lead(Pb)
Mercury(Hg)
Hexavalent
Chromium(Cr(Vl))
Sumol PBBS
Monobromobiphenyl
Dibromobiphenyl
Tribromobiphenyl
Tetrabrcmobiphonyl
Pentabromobiphenyl
Hexabromobiphenyl
Heptabromobiphenyl
Odabromobiphenyl
Nonabromobiphenyl
Decabromobiphenyl
thi!
ud!
10O
1,000
mg/kg
mgikg
1,0_00mslks
1,000
-
mg/kg
mg/Kg
mg/Kg
mdks
mwKs
mgKg
mg/Kg
ms,Ks
mg/kg
_
mgKg
mgiKg
1,000 ms/ks
-
l\ronobromodiphenyl
ether
mg/Kg
MD!
034
2
2
2
O
-
N
D
165
N
D
Negative
N
D
5
5
5
5
5
5
5
5
5
5
,
N
N
N
N
N
N
N
N
N
N
N
D
D
D
D
D
D
D
D
D
D
D
5
N
D
, bYrb cdtsnr $$.r b rr sd{
tu
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H!(S-Z)6 q04
Hjl6-AF.a)Br
w.6,t!.@
. qFd'aroF.o
Momhcrorihe 8CSOroup(sGA8l)
TestReport
No.SHAEC1116009839
Test ltem{s)
Dibromodiphenyl
ether
Tribromodiphenyl
ether
Tetrabromodiphenyl
ether
Pentabromodiphenyl
ether
Hexabromodiphenyl
elher
Heptabromodiphenyl
ether
Oc€bromodiph€nyl
ether
Nonabromodiphenyl
ether
Decabromodiphenyl
ether
Date:14 Oct 2011
ud!
tiEil
ng/Kg
mg/Kg
mgKg
mgKg
mg/Kg
mg/Kg
mg/(g
mg/kg
mg/kg
MDt
034
5
5
5
5
5
5
5
5
5
ND
ND
ND
ND
ND
ND
ND
ND
ND
Page 3 of 5
Notes:
(1)Themaximum
permissible
limitis quotedfromdirective
2011/65/EU,
Annexll
(2)o spot-test:
= AbsenceofCrVlcoating,
= presence
Negative
Positive
of CrVtcoating;
Thetestedsampleshouldbefurtherverifiedby boiting-waterextraction
methodifthe spottestresultis
Negative
or cannotbeconfirmed.
. Boiling-water-extraction:
= Abs€nceof CrVlcoating;Positive
= Presenc€
Negative
of CrVlcoating
Thedetected
concenhation
in boiling-water-extraction
solutionis equalor greaterthan0.02mg/kgwith5C
cmzsamolesurfacearea.
protection
Forcorrosion
coatings
on metals:Information
onstorageconditions
andproduction
dateofthe
testedsampleis un€vaibble
andthusresultsof Cr(Vl)represent
stratus
of thesampteat thetimeof
testing
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TestReport
No.SHAEC1116009839
Date:14 Oct 2011
Page4 of 5
ATTACHMENTS
RoHSTestingFtowChart
'1)Nameof the pe6onwhomade
testing:
JanShi/yoyo
Wangy'Allen
Xiao/Gary
Xu
2) Nameof the personin chargeof testing:
JeffZhanglceorge
Xu/EtimLin
3) Thesesamples
weredissolved
totallyby preconditioning
methodaccordlng
to belowflowcnan.
(Cr6+andPBBS/PBDEStest
methodexctuded)
SamplePreparation
SampleMeasurement
Pb/Cd/Hg
PBBs/PBDES
Heatingto 90-9511
for extraclion
1)AlkaliFusion/
DryAshing
2) Acidto dissolve
Filtrationand pH
adjustment
Adding1,5diphenylcarbazide
forcolor
development
rh!@d
b b.!d br rh. Od4.ny uqd b r| Or.ra C.d{!.
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ll.m!€i ot rh66Gs Grolp lSGssA)
TestReport
No.SHAECIl16009839
Date:14 Oct2011
Page 5 of 5
Samplephoto:
sHAl 1-160098.034
SGSauthenticate
the photoon originalreporlonly
'** Endof Report'"
'-6.hk
ht'rH
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drybr[
rmpr.{.) hdi
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Mc,nturoltlo SOSOrcu9IAGS&1)
TestReport
No.TSNEC1200272601
Date:09Apr2012
Page 1 of I
BEIJINGHYSTICNEW MATERIALSCO,,LTD.
5 SHUANGYUAN
ROAD,BADACHUHIGH.TECH
ZONE,BEIJING,
100041,
cHtNA
Thefollowing
sample(s)
was^^/ere
submitted
andidentified
onbehalfof thectientsas : EpOXyADHESTVE
- TJ
SGSJobNo.:
TP12-004950
l\rodelNo.:
Dateof SampleReceived:
EP6O8
3l Mat2012
31Mat2012- 09 Apt2012
Selecledtest(s)as requestedby client.
TestingPeriod:
TestRequested:
TestMethod:
Pleasereferto nextpage(s).
Pleasereferto nextpage(s).
TestResults:
Basedontheperfomedtesb onsubmitted
samples,
theresutts
of Lead,
Mercury,
Cadmium,
Hexavalent
chromium,
Polybrominated
(PBB),
biphenyts
Polybrominated
diphenyl
ethers(PBDE)
complywiththelimitsas setby RoHS
Directive
2011/65/EU
Annexll; recasting
2002/95/EC.
Conclusion
i
Signedforandon behalfof
scs-csTcLtd.
O\
N6'(
AimyWang
ApprovedSignatory
rh!do.!n'lt6!.d5ylh.con!.iy
'id !' .drdoi r.i,.; dsr..d 't.,.h
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r
I iis
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;iir..d
h!'F''fl
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I l|t2ri5e95?52
rloA,Ti.njn china3ol4s7 r 13t2?66233000
srf Avenue
scsMans'6i.N6.41Th.
r 136-?a2546?52 e s!.c\ia@6!3@
es6s*l
Srl 300457r 136266233000
4 E .*tlisftfi{*€6tt*S4l
M e m b e rrohl.S G S G o l p { S GSSA I
Te€tReport
No.TSNEC1200272601
Date: 09 Apr 20 12
Page2 ol8
TestResults:
TestPartDescription:
Sp€d.n€nNo.
SGSSsmplelD
D€6criplion
1
TSN12-002726.001ivory-white
paste
Remarks:
(1)1mg/kg=1 ppm= 0.0001%
(2)IIDL = MethodDetection
Limit
(3)ND= NotDeteded( < MDL)
(4)"-' = 1o1q"nu,","o
RoHSDirodive201t/66/EU
TestMethod: Withreference
to |EC62321:2008
(1)Determination
ofCadmium
by tCP-OES.
(2)Determination
of Leadby ICP-OES.
(3)Detemination
of l,rercury
by ICP-OES.
(4)Determination
of Hexavalent
Chrcmium
byColo metricMethodusingUV-Vis
(5)Detemination
of PBBS/ PBDES
contentby GC-MS.
Test ltem(s)
Cadmium(Cd)
Lead(Pb)
lllercury (Hg)
(Cr(Vl))
Hexavalent
Chromium
Sumof PBBS
Ivlonobromobiphenyl
Dibromobiphenyl
Tribromobiphenyl
Tetrabromobiphenyl
Pentabromobiphenyl
Hexabromobiphenyl
Heptabromobiphenyl
Oclabromobiphenyl
Nonabromobiphenyl
Decabromobiphenyl
Sumof PBDES
Monobromodiphenyl
ether
;trvdGhFo&de,sr,E^rh.;d.i@br.^
tr' bt6$n;tonl!N{h'i
rh rnir
i'ci't6rr.nE
i DaDbh" -d d e
h,q!aoit"
tinit
Ud!
100
1000
1000
1000
1000
'
-
mg/kg
mS/kS
mS/KS
mS/kS
mdks
mg/Kg
mg/Kg
mg/Kg
mg-fts
mgKg
mgKS
ms/Ks
mg/kg
mgKg
m9x9
ms/ks
mg/Kg
1000
-
{1d".'db.
MDt
0p1
2
2
2
2
-
N
N
N
N
N
5
5
5
5
5
5
5
5
5
5
N
N
N
N
N
N
N
N
N
N
5
O
D
D
D
D
D
D
D
D
D
D
D
D
D
D
ND
N
D
t r rd r . 6i1rir h 6do.vnld d.d
rc'rdn dr s.iod.d'
f,nqc'i!9s@r
| 0G42529s29
2aBA80CC
sGs MadsioiNc.41.Tho slh AvenueTEoA,llanin,chiM 1l}a57 I 136
s sss.f'[email protected]
s F . *lriE*fitrtte8lit641Cscs*l
ffll: 300457I {3f2r66?8806l1e2?26&12
Membero,rbeSGSGroup(SGSSA)
TestReport
No.TSNEC1200272601
Tost ltem(s)
Dibromodiphenyl
elher
Tdbromodiphenyl
elher
Telrab.omodiphenylether
Pentabromodiphenyl
elh€r
Hexabromodiphenyl
ether
Heptabromodiphenyl
ether
Octabromodiphenyl
ether
Nonabromodiphenyl
ether
Decabromodiphenyl
elher
trd!
Date:09Apr2012
udt
MDt
@1
ms/Kg
mg/Kg
mS/kS
ms/Ks
mg/kg
mg/Kg
m9KS
mgKs
mgKs
5
5
5
5
5
5
5
5
5
ND
ND
ND
ND
ND
ND
ND
ND
ND
Page3 of 8
Notes:
(1)Themaximum
permissibte
limitis quotedfromdirective
2011/65/EU.
Annexlt.
Horebrpmocrrdododecane
THBCDD)
Testlvlethod
: Withreference
to IEC62321:2008,
anatysis
wasp€rfomedby GC-N4S.
T€stltem(s)
Hexabromocyclododecane
(HBCDD)
Ulit
MDI
pp1
mgKg
10
ND
Notes:
(1)Reference
Information:
Diredive2011/6S/EU
recasting
RoHSdirective
200?J9S/EC:
Hexabromocydododec€ne
(HBCDD)
is considered
as a priority
forriskevaluation
andsubstance
restriclion.
Phthalatss
Testl\Iethod: Withreference
to EN14372:2004,
anatysis
wasperformed
by co-tvts.
Test ltem(s)
DibutylPhthalate
(DBP)
B€nzylbutylPhthalate(BBP)
(DEHP)
Bis (2-elhylhexyD
Phthalale
Notes :
!d!
MDt
%(w4,,/) 0.003
%(ww) 0.003
%(Ww) 0.003
0p1
ND
ND
ND
(1)Reference
Infomation:
Directive
2011/65/EU
recasting
RoHSdirective
200295/EC:
phthaiate
Bis(2-ethylhexyl)
(DEHP),
Butylbenzytphthatate
(BBP)andoibutytphthatate
(DBp)are
considered
as a pdority
forriskevaluation
andsubslance
restiction.
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M , m b eor l r h eS G S G , o r pt S G SS A I
TestReport
No.TSNEC1200272601
Date:09Apr2012
Page 4 of I
Resultshownis of the total weight of wet sample
y rubt.cr 'o {. o.i.'.r coid [oi. ors.
rdrtrr @Mr,idrJ.d
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SGSTest ReDort
No.TSNEC1200272601
Date:09 Apr 2012
Page 5 of 8
ATTACHMENTS
cd/Pb/Hg/Cf'lPBB5&PBOES Flow Chart
Aer0nWang/Jason
Li/AngellYao
1 )Nameoflhe personwho madetesling:
percon
in chargeoftesting:
CindyYin/RelZhu
2) Nameofthe
tolallyby pre-condilioning
melhodaccording
to
3) Thssesampleswsrs dissolved
belowllowchari.(C16*
andPBBS/PBDES
testmelhodexcluded)
Preparation
Sample
lVeasuremenl
Sample
PEB'PEDE5
Fb/Cd/Hg
Sample
solvent
Aciddigestion
wilh
micrcwave/holplale
reagent
Addingdigestion
Heatingio 9tF95'C for
extraction
Concentralion/
Dilution
ofextraction
s0iuIt0n
Solution
ResiduB
Filtralion
andpH
adjustmenl
I
1)AkaliFusion
DryAshing
2) Acid to
dissolve
ill;l,ffi;i;lii'#:;'
i i
i;
;ii;
Adding1,5'
fo!
diphenylcarbazide
coloidevelopment
i;;;;i'-,iiiliir
ii'iiii;'";l;;n
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TestReport
No.TSNEC1200272601
Date:09 Apr 2012
Page6 ofB
ATTACHMENTS
HECDD Tosting Flow Chaft
'l) Nameofthe perconwho made
testing:MarineSun
2) Namsoflhe personin chargeoftestingr
RexZhu
Sample
cutting/preparation
Sample
measurement
Solvenlexhaction
ConcBntraliodDilution
h'iii
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TestReport
No.TSNEC1200272601
Date:09Apr2012
Page7 of I
ATTACHMENTS
Phthalde Testng Floli, chaft
1) Namsoflhe pelsonwho madelestingiMaina Sun
2) Nameofthe personin chargeoftesling:RsxZhu
Solvenlexhaclion
ution
Concentralion/Dil
Fihralion
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SGs6roup{SGs5A)
TestReport
No.TSNEC1200272601
Date:09 Apr2012
Page 8 of 8
Samplephoto:
TSN12-002726.001
the photoon originalrepoionly
SGS authenticate
'*. End of Report'-
l#;tr$#,Ii.1i;;iffi
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Mehboror$€ scs GbuP (SGSSA)
TestReport
No.TSNEC1200272602
Date:09Apr2012
Page1 of 4
BEIJINGHYSTICNEWIVATERIALS
CO,,LTD,
ROAD,BADACHUHIGH.TECHZONE,BEIJING.
5 SHUANGYUAN
100041,
cHtNA
The followingsample(6)wasirere submittedand identifiedon behalfofthe clientsas : EPOXYADHESIVE
- TJ
TP12-004950
SGSJobNo.:
lvodelNo.:
Dateof SampleReceived
TestingPedod:
EP6O8
31 Mat2012
31 Mat 2012- 0g Apt2012
Test Requested:
Selecledtest(s)as requestedby client.
Testlvlethod:
Pleasereferto nextpage(s).
Pleasereferto nextpage(s).
TestResults:
Signedfor and on behalfof
scs-csTcLtd.
o*) N-(
AimyWang
ApprovedSignatory
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TestRemrt
No.TSNEC1200272602
Date:09 Apr20'l2
Page2 of 4
TestResults:
TestPartDescdption:
Spodm€i No.
1
SGSSamplelD
D€6cription
TSN12-002726.002ivorv-whiteDaste
Remarks:
0 )1 m g / k g = 1 p p m = 0 . 0 0 0 1 %
(2)[,lDL = lllethod DetectionLimit
(3)ND = Not Detected( < IVIDL)
(4) '!" = Not Regulated
Halogen
(lC).
performed
by lonChromatograph
TestMethod: Withreferenceto EN 14582:2007,analysiswas
Testltem(s)
(F)
Fluorine
Chlorine(Cl)
(Br)
Bromine
(l)
lodine
u!j!
mg/(9
mgKs
mg/Kg
mg/kg
MDt
O@
50
50
50
50
57
7557
ND
NO
Result shown is of the total weight of wet sample
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TestReport
Dater09Apr2012
No.TSNEC1200272602
Page 3 of 4
ATTACHMENTS
HalogenTestingFlow Chad
Angell
Yao
whomadetesling:
1)Nameofthepercon
Rsx
Zhu
psrson
in
charge
oflesling:
ofthe
2) Name
Samplecutting/preparation
measuremsnl
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in oxygenbomb
Combuslion
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by ion
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TestReport
Date:09 Apr 2012
No.TSNEC1200272602
Page4 of 4
Samplephoto:
TSNl2-002726.002
SGS authenticatethe photo on odginal report only
'*" End of Report""'
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lhosGs Goup(sGSSAI
Momb€rot
nov'
TESTREPORT
NO.jA002E11121307'1R02
page1of4
DaG:Dec.t5,2Oi1
Custom6iSuzhouFuHongEteclronic
IndustialCo.,
L6.
AddT€sg:
NO.89WEIDUROAD,WANGTINGTOWN.
XIANGCHENG
oIsTRIcT.sUzHoU.CHINA
Reporton tie subnitiedsamptes.idto be
Samplename:Coppershell
Modsl:/
Materlal:/
D€cripiion:/
Buyer:/
Supplier:/
SamPlercceiwd date:Elec.'13,2011
T€dng poriod:FromDec.13,2011
lo Dec.15,2o.l1
T€lino Reou6ted
As sp€cified
by client,to deteminethe L€ad,Cadmium,
Mercury
& Hexavat€nt
Chromilmcontentantheslbmifiedsamptein
accordancewilh Dircctive200295/EC(RoHS).
Te.Unomethod:
T€slingliem
Lead(Pb)
IEC62321:2008,
sectionI
IEC62321:20t,3,
s€clion9
cadmium(cd)
llercury(Hg)
(Crl'1)
Chromrum
IEC62321:2008,
section7
IEC62321:2008,
AnnexB
Measuring
instrument MQL
rcP-oEs
2mg/kg
tcPoEs
lcPoEs
2 mg/kg
2 mg/kg
0 o2mgkg'
leg
-' 0.02mg/kgreGrclo theMQLof sampte
extraction
tiquid.
99!9!cis!i
-When
tesledas specined
thesubmi(ed
sample
compli€d
wilhthercquirements
of commission
Decision
of 18Aug2005
amendingDirective2002/95/ECnotiliedundefdocument2005/618/EC.
---FOR
Pro,ect
Leader
(Engine€r)
FURTHERDETAILS,PLEASEREFERTOTHEFOLLOWNGPAGE(ST**'
/{bjA-L
J4
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lnsoected
bv
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BRANCIi
SHENZHEnlAOVTESTINC TECHNO!OGY CO..L.TD,KUI\ISIIAI\I
Holline
8 6 . 5 1 2 . 5 5 1800 0 0
nov.
TESTREPORT
NO,:A002E11121307-1
R02
Weighthesampleinto
Add the digestionsotutionithe
vesselis healeduntilthe sampl€
hasb€€ndissolved
F*_-lTo
Tesledby ICP-OES
Content(MelalsubstEle)
Add the digeslionsolutjon,ctose
The sampleis digesredin the
the micfowaveves:€|.
mrcrowave
oveniollowinga sp€citic
program.
decomposilion
+
Coolingthe vessel,fltet washedand
filled to the ma* with distilled wat€r.
To Detenn
exavalenl
Chromium
(bojtingContent
(Metatsubstrate)
wateFextraction):
Heat50 mL of Dl walerin the
samplein the beaker.
beakerto boilingior 10 min
F;;1.To Delemine
Remove
thesample,
andcool
thebeakerto roomlemperature,
anddothecolorleadion
Tesllh€s€mplesolution
andthe0.02
mg/kgstandardsolutionby UV-VIS.
andl\Iercury
Content(Plaling)
andlilled
___+l coorins.rirteiwashed
l_-_----|lresteo oy l+fl_*l
t ot h em a * w i tD
ht w a t e r .
l r n " r , u r n " nI , l " * '
I
I
SHENZHsN AOV TG6TINGICCHITOI"OGYCO.,L'O.KUNAHAN BRANCH
a
I
Hotline
86-512-551
80 0 0
nov'
TESTREPORT
NO.i4002E11121307-rR02
oste:oec15,2011
5. ToO€temineHexavalent
Chromium
Contentincolorlessand cotorcdcnromaEcoatingon metats(Plaljng)
,':"j":::i
v^02
lf the tesl rcsultis posilive,
the sampleis considercdto
havehexavalenl
chromilm
Place
1-5
Compare
the
Eoiling- wateF ext€ctjon
prccedurcshall be usedto
andlhe 0.02mg/(q
standa.d
solution
lfthereis int€rference
or it is hardto decidewhether
thesampl€havetie h€xavatent
chromium
5 2 Eoilingwat6Fextraction
Tako the (50+5) cm'?
Heat50 mlof Dlwaier in the
samplein the beaker.
beakerlo boilingfor 10 min
Removetie sample,and cool
lhe beaksrto roomtempeEture,
and do the colorreaolion
Testthesamplesolution
andthe0.02
mg/kgstandard
solution
by UV,VIS.
T€t Re6ult3:
Unit
Limil
Substrate
Plating'
N.O.
N.O.
N.D.
Negalive
Lead(Pb)
(cd)
Cadmium
mg/Kg
(Hg)
lvercury
mgn(]s
1000
100
1000
chromium(Crl'I)
mg/Kg
1000
mg/Kg
Result
RoHS
N.D,
N.D.
N.D.
Negative
S!IENZHENAOV'CSTING IECIINOIOGY CO..ITD,KUNSHAN gNANCH
Hotline
a6-512-551
80 0 0
novTESTREPORT
NO 4002E11121307.rR02
'The new RoHSdirective2011/65/EU,on Jul. 21 2011 comeintolorce
,
on Jan.03, 2013 the fomat imptementation.
Direclive
2002,95/ECshallbe rcpeatedsimuttaneousty.
-specimens,whichrequestedto determineLead,cadmiumand l,rercury
conteni,havebeendissorvedcomprererv
-N.D.=notdetected(<tltoL)
-MOL=ntethodOuantitation
Limit
-Negative=Absenceof Cr (VIir
PositivFPresenceofCr (\ll)i
Unc€rlain=can not verifywhetlerthe samptehaveHexavatent
Chromiumby spoltest.
(The test€d sample should be fufthet verifiedby boiling-waler-€nraction
method if the spot test resutt |s uncertainor
negalive.)
-'The tesl is basedon lhe followingassumption:Thesampteptatingis a singtetayefand
each paft is uniform.The tesr resutt
maybecannotslandbr lhe physicaltruthofsampteptating.
Photograph
ofSample
Coppershell
ARANCTI
SHENZHEN
AOVT€STINGTECHNOLOGYCO.,IID,XUNSHAN
e!:-"Jllls,.*
Intertek Testing Services Ltd., Shanghai
TFH Division
Block B, Jinling Business Square,No.801 Yi Shan Road,
Shanghai, China, 200233
Tel: +86 21 6120 6565
Fax: +86 21 6127 9740
www.intertek.com
www.intertek.com.cn
China Toll-Free: 800 999 1338
TEST REPORT
APPLICANT: LITTELFUSE,INC.
800 E. NORTHWEST HWY
ATTN: A. CESISTA/ K. BACILA
NUMBER: SHAH00296134
DATE: DEC 20, 2011
SAMPLE DESCRIPTION:
One(1) submitted sample said to be Sand.
Part Description
: Sand.
Part Number
: 311.7374.5000.
Date Sample Received
: Dec.14, 2011.
Date Test Started
: Dec.14, 2011.
***********************************************************************
TESTS CONDUCTED:
AS REQUESTED BY THE APPLICANT, FOR DETAILS REFER TO ATTACHED PAGE(S)
**********************************************************************
TO BE CONTINUED
PREPARED AND CHECKED BY:
FOR INTERTEK TESTING SERVICES
LTD., SHANGHAI
AUTHORIZED BY:
FOR INTERTEK TESTING SERVICES
LTD., SHANGHAI
MYRA LV
CHEMICAL LAB SENIOR MANAGER
STEPHEN TSANG
GENERAL MANAGER
PAGE 1 OF 9
Intertek Testing Services Ltd., Shanghai
TFH Division
Block B, Jinling Business Square,No.801 Yi Shan Road,
Shanghai, China, 200233
Tel: +86 21 6120 6565
Fax: +86 21 6127 9740
www.intertek.com
www.intertek.com.cn
China Toll-Free: 800 999 1338
TEST REPORT
NUMBER: SHAH00296134
TESTS CONDUCTED
1
(I) Test Result Summary :
Testing Item
Halogen Content
Fluorine (F)
Chlorine (Cl)
Bromine (Br)
Iodine (I)
Result (ppm)
ND
230
ND
ND
Remarks: ppm = Parts per million based on weight of tested sample =
mg/kg
ND = Not detected
Responsibility Of Chemist
(II) Test Method:
Testing Item
Halogen Content
: Ken He
Testing Method
With reference to EN 14582:2007 by
combustion flask with oxygen and
determined by ion chromatography
Reporting Limit
50 ppm
Remark: Reporting limit = Quantitation limit of analyte in sample
**********************************************************************
TO BE CONTINUED
PAGE 2 OF 9
Intertek Testing Services Ltd., Shanghai
TFH Division
Block B, Jinling Business Square,No.801 Yi Shan Road,
Shanghai, China, 200233
Tel: +86 21 6120 6565
Fax: +86 21 6127 9740
www.intertek.com
www.intertek.com.cn
China Toll-Free: 800 999 1338
TEST REPORT
NUMBER: SHAH00296134
TESTS CONDUCTED
(III) Measurement Flowchart:
Test For Halogen Content
Reference Standard： EN 14582
sampling/grinding or
cutting
add absorbent in a
combustion flask &
place weighed sample in
equipment
fill the combustion
flask with oxygen
ignite then leave the
flask at room
temperature
transfer the absorbent
into a volumetric flask
make up with deionized
water
analyzed by ion
chromatography
**********************************************************************
TO BE CONTINUED
PAGE 3 OF 9
Intertek Testing Services Ltd., Shanghai
TFH Division
Block B, Jinling Business Square,No.801 Yi Shan Road,
Shanghai, China, 200233
Tel: +86 21 6120 6565
Fax: +86 21 6127 9740
www.intertek.com
www.intertek.com.cn
China Toll-Free: 800 999 1338
TEST REPORT
NUMBER: SHAH00296134
TESTS CONDUCTED
2
(I) Test Result Summary :
Result (ppm)
Testing Item
Heavy Metal
Cadmium (Cd) content
ND
Lead (Pb) content
ND
Mercury (Hg) content
ND
Chromium VI (Cr6+) content
ND
Polybrominated Biphenyls (PBBs)
Monobrominated Biphenyls (MonoBB)
ND
Dibrominated Biphenyls (DiBB)
ND
Tribrominated Biphenyls (TriBB)
ND
Tetrabrominated Biphenyls (TetraBB)
ND
Pentabrominated Biphenyls (PentaBB)
ND
Hexabrominated Biphenyls (HexaBB)
ND
Heptabrominated Biphenyls (HeptaBB)
ND
Octabrominated Biphenyls (OctaBB)
ND
Nonabrominated Biphenyls (NonaBB)
ND
Decabrominated Biphenyl (DecaBB)
ND
Polybrominated Diphenyl Ethers (PBDEs)
Monobrominated Diphenyl Ethers (MonoBDE)
ND
Dibrominated Diphenyl Ethers (DiBDE)
ND
Tribrominated Diphenyl Ethers (TriBDE)
ND
Tetrabrominated Diphenyl Ethers (TetraBDE)
ND
Pentabrominated Diphenyl Ethers (PentaBDE)
ND
Hexabrominated Diphenyl Ethers (HexaBDE)
ND
Heptabrominated Diphenyl Ethers (HeptaBDE)
ND
Octabrominated Diphenyl Ethers (OctaBDE)
ND
Nonabrominated Diphenyl Ethers (NonaBDE)
ND
Decabrominated Diphenyl Ether (DecaBDE)
ND
**********************************************************************
TO BE CONTINUED
PAGE 4 OF 9
Intertek Testing Services Ltd., Shanghai
TFH Division
Block B, Jinling Business Square,No.801 Yi Shan Road,
Shanghai, China, 200233
Tel: +86 21 6120 6565
Fax: +86 21 6127 9740
www.intertek.com
www.intertek.com.cn
China Toll-Free: 800 999 1338
TEST REPORT
NUMBER: SHAH00296134
TESTS CONDUCTED
Remarks: ppm = Parts per million = mg/kg
ND = Not detected
Responsibility Of Chemist : Dent Fang / Ken He
(II) RoHS Requirement:
Restricted Substances
Cadmium (Cd) Content
Lead (Pb) Content
Mercury (Hg) Content
Chromium VI (Cr6+) Content
Polybrominated Biphenyls (PBBs)
Polybrominated Diphenyl Ehters (PBDEs)
Limits
0.01% (100ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
The above limits were quoted from 2002/95/EC and amendment
2005/618/EC for homogeneous material.
**********************************************************************
TO BE CONTINUED
PAGE 5 OF 9
Intertek Testing Services Ltd., Shanghai
TFH Division
Block B, Jinling Business Square,No.801 Yi Shan Road,
Shanghai, China, 200233
Tel: +86 21 6120 6565
Fax: +86 21 6127 9740
www.intertek.com
www.intertek.com.cn
China Toll-Free: 800 999 1338
TEST REPORT
NUMBER: SHAH00296134
TESTS CONDUCTED
(III) Test Method:
Testing Item
Testing Method
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
Cadmium (Cd)
microwave digestion until the
content
tested samples are totally
dissolved and determined by ICPOES.
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the
Lead (Pb) content
tested samples are totally
dissolved and determined by ICPOES.
With reference to IEC 62321 edition
1.0:2008 in clause 7, by microwave
Mercury (Hg)
digestion until the tested samples
content
are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
Chromium VI (Cr6+) 1.0:2008 in annex C, by alkaline
content
digestion and determined by UV-Vis
spectrophotometer.
With reference to IEC 62321 edition
1.0:2008 in annex A, by solvent
Polybrominated
extraction and determined by GC-MSD
Biphenyls (PBBs)
and further HPLC confirmation when
necessary.
With reference to IEC 62321 edition
Polybrominated
1.0:2008 in annex A, by solvent
Diphenyl Ethers
extraction and determined by GC-MSD
(PBDEs)
and further HPLC confirmation when
necessary.
Reporting
Limit
2 ppm
2 ppm
2 ppm
1 ppm
5 ppm
5 ppm
Remark: Reporting limit = Quantitation limit of analyte in sample
DATE SAMPLE RECEIVED : DEC.14, 2011
TESTING PERIOD : DEC.14, 2011 TO DEC.19, 2011
**********************************************************************
TO BE CONTINUED
PAGE 6 OF 9
Intertek Testing Services Ltd., Shanghai
TFH Division
Block B, Jinling Business Square,No.801 Yi Shan Road,
Shanghai, China, 200233
Tel: +86 21 6120 6565
Fax: +86 21 6127 9740
www.intertek.com
www.intertek.com.cn
China Toll-Free: 800 999 1338
TEST REPORT
NUMBER: SHAH00296134
TESTS CONDUCTED
(IV) Measurement Flowchart:
Test For Cd/Pb/Hg/Chromium (VI)/PBBs/PBDEs Contents
Reference Standard: IEC 62321 edition 1.0:2008
sampling/grinding or cutting
Cr6+
Cd/Pb/Hg
metal
weigh sample and
for different
material, digest
the sample with
confirm the tested
samples are totally
dissolved
spot test
negative*2
No
polymers /
electronics
weigh sample
and add
alkaline
solution
get 50cm2
samples
definite
temp.
boiling water
extraction
cool and
filter the
extract
PBBs/PBDEs
weigh sample
and add
organic
soxhlet
extraction or
solvent
extraction
make up with
deionized water
analyzed by ICP-OES
make up with deionized
water and add diphenylcarbazide solution
concentrate
the extract
and make up
with organic
analyzed by GCMSD
analyzed by UV-VIS
**********************************************************************
TO BE CONTINUED
PAGE 7 OF 9
Intertek Testing Services Ltd., Shanghai
TFH Division
Block B, Jinling Business Square,No.801 Yi Shan Road,
Shanghai, China, 200233
Tel: +86 21 6120 6565
Fax: +86 21 6127 9740
www.intertek.com
www.intertek.com.cn
China Toll-Free: 800 999 1338
TEST REPORT
NUMBER: SHAH00296134
TESTS CONDUCTED
REMARKS:
*1: List of appropriate acid：
Material
Acid added for digestion
Polymers
HNO3,HCl,HF,H2O2,H3BO3
Metals
HNO3,HCl,HF
Electronics
HNO3,HCl,H2O2,HBF4
*2: If the result of spot test is positive, Chromium VI would be
determined as detected.
**********************************************************************
TO BE CONTINUED
PAGE 8 OF 9
Intertek Testing Services Ltd., Shanghai
TFH Division
Block B, Jinling Business Square,No.801 Yi Shan Road,
Shanghai, China, 200233
Tel: +86 21 6120 6565
Fax: +86 21 6127 9740
www.intertek.com
www.intertek.com.cn
China Toll-Free: 800 999 1338
TEST REPORT
NUMBER: SHAH00296134
TESTS CONDUCTED
**********************************************************************
END OF REPORT
PAGE 9 OF 9
Intertek Testing Services Ltd., Shanghai
TFH Division
Block B, Jinling Business Square,No.801 Yi Shan Road,
Shanghai, China, 200233
Tel: +86 21 6120 6565
Fax: +86 21 6127 9740
www.intertek.com
www.intertek.com.cn
China Toll-Free: 800 999 1338
TEST REPORT
APPLICANT: LITTELFUSE,INC.
800 E. NORTHWEST HWY
ATTN: A. CESISTA/ K. BACILA
NUMBER: SHAH00299962
DATE: JAN 18, 2012
SAMPLE DESCRIPTION:
One(1) submitted sample said to be White yarn.
Part Description
: YARN.
Part Number
: 648901.
Date Sample Received
: Jan.11, 2012.
Date Test Started
: Jan.11, 2012.
***********************************************************************
TESTS CONDUCTED:
AS REQUESTED BY THE APPLICANT, FOR DETAILS REFER TO ATTACHED PAGE(S)
**********************************************************************
TO BE CONTINUED
PREPARED AND CHECKED BY:
FOR INTERTEK TESTING SERVICES
LTD., SHANGHAI
AUTHORIZED BY:
FOR INTERTEK TESTING SERVICES
LTD., SHANGHAI
MYRA LV
CHEMICAL LAB SENIOR MANAGER
STEPHEN TSANG
GENERAL MANAGER
PAGE 1 OF 9
Intertek Testing Services Ltd., Shanghai
TFH Division
Block B, Jinling Business Square,No.801 Yi Shan Road,
Shanghai, China, 200233
Tel: +86 21 6120 6565
Fax: +86 21 6127 9740
www.intertek.com
www.intertek.com.cn
China Toll-Free: 800 999 1338
TEST REPORT
NUMBER: SHAH00299962
TESTS CONDUCTED
1
(I) Test Result Summary :
Testing Item
Halogen Content
Fluorine (F)
Chlorine (Cl)
Bromine (Br)
Iodine (I)
Result (ppm)
820
ND
ND
ND
Remarks: ppm = Parts per million based on weight of tested sample =
mg/kg
ND = Not detected
Responsibility Of Chemist
(II) Test Method:
Testing Item
Halogen Content
: Ken He
Testing Method
With reference to EN 14582:2007 by
combustion flask with oxygen and
determined by ion chromatography
Reporting Limit
50 ppm
Remark: Reporting limit = Quantitation limit of analyte in sample
**********************************************************************
TO BE CONTINUED
PAGE 2 OF 9
Intertek Testing Services Ltd., Shanghai
TFH Division
Block B, Jinling Business Square,No.801 Yi Shan Road,
Shanghai, China, 200233
Tel: +86 21 6120 6565
Fax: +86 21 6127 9740
www.intertek.com
www.intertek.com.cn
China Toll-Free: 800 999 1338
TEST REPORT
NUMBER: SHAH00299962
TESTS CONDUCTED
(III) Measurement Flowchart:
Test For Halogen Content
Reference Standard： EN 14582
sampling/grinding or
cutting
add absorbent in a
combustion flask &
place weighed sample in
equipment
fill the combustion
flask with oxygen
ignite then leave the
flask at room
temperature
transfer the absorbent
into a volumetric flask
make up with deionized
water
analyzed by ion
chromatography
**********************************************************************
TO BE CONTINUED
PAGE 3 OF 9
Intertek Testing Services Ltd., Shanghai
TFH Division
Block B, Jinling Business Square,No.801 Yi Shan Road,
Shanghai, China, 200233
Tel: +86 21 6120 6565
Fax: +86 21 6127 9740
www.intertek.com
www.intertek.com.cn
China Toll-Free: 800 999 1338
TEST REPORT
NUMBER: SHAH00299962
TESTS CONDUCTED
2
(I) Test Result Summary :
Result (ppm)
Testing Item
Heavy Metal
Cadmium (Cd) content
ND
Lead (Pb) content
ND
Mercury (Hg) content
ND
Chromium VI (Cr6+) content
ND
Polybrominated Biphenyls (PBBs)
Monobrominated Biphenyls (MonoBB)
ND
Dibrominated Biphenyls (DiBB)
ND
Tribrominated Biphenyls (TriBB)
ND
Tetrabrominated Biphenyls (TetraBB)
ND
Pentabrominated Biphenyls (PentaBB)
ND
Hexabrominated Biphenyls (HexaBB)
ND
Heptabrominated Biphenyls (HeptaBB)
ND
Octabrominated Biphenyls (OctaBB)
ND
Nonabrominated Biphenyls (NonaBB)
ND
Decabrominated Biphenyl (DecaBB)
ND
Polybrominated Diphenyl Ethers (PBDEs)
Monobrominated Diphenyl Ethers (MonoBDE)
ND
Dibrominated Diphenyl Ethers (DiBDE)
ND
Tribrominated Diphenyl Ethers (TriBDE)
ND
Tetrabrominated Diphenyl Ethers (TetraBDE)
ND
Pentabrominated Diphenyl Ethers (PentaBDE)
ND
Hexabrominated Diphenyl Ethers (HexaBDE)
ND
Heptabrominated Diphenyl Ethers (HeptaBDE)
ND
Octabrominated Diphenyl Ethers (OctaBDE)
ND
Nonabrominated Diphenyl Ethers (NonaBDE)
ND
Decabrominated Diphenyl Ether (DecaBDE)
ND
**********************************************************************
TO BE CONTINUED
PAGE 4 OF 9
Intertek Testing Services Ltd., Shanghai
TFH Division
Block B, Jinling Business Square,No.801 Yi Shan Road,
Shanghai, China, 200233
Tel: +86 21 6120 6565
Fax: +86 21 6127 9740
www.intertek.com
www.intertek.com.cn
China Toll-Free: 800 999 1338
TEST REPORT
NUMBER: SHAH00299962
TESTS CONDUCTED
Remarks: ppm = Parts per million = mg/kg
ND = Not detected
Responsibility Of Chemist : Dent Fang / Ken He
(II) RoHS Requirement:
Restricted Substances
Cadmium (Cd) Content
Lead (Pb) Content
Mercury (Hg) Content
Chromium VI (Cr6+) Content
Polybrominated Biphenyls (PBBs)
Polybrominated Diphenyl Ehters (PBDEs)
Limits
0.01% (100ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
The above limits were quoted from 2002/95/EC and amendment
2005/618/EC for homogeneous material.
**********************************************************************
TO BE CONTINUED
PAGE 5 OF 9
Intertek Testing Services Ltd., Shanghai
TFH Division
Block B, Jinling Business Square,No.801 Yi Shan Road,
Shanghai, China, 200233
Tel: +86 21 6120 6565
Fax: +86 21 6127 9740
www.intertek.com
www.intertek.com.cn
China Toll-Free: 800 999 1338
TEST REPORT
NUMBER: SHAH00299962
TESTS CONDUCTED
(III) Test Method:
Testing Item
Testing Method
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
Cadmium (Cd)
microwave digestion until the
content
tested samples are totally
dissolved and determined by ICPOES.
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the
Lead (Pb) content
tested samples are totally
dissolved and determined by ICPOES.
With reference to IEC 62321 edition
1.0:2008 in clause 7, by microwave
Mercury (Hg)
digestion until the tested samples
content
are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
Chromium VI (Cr6+) 1.0:2008 in annex C, by alkaline
content
digestion and determined by UV-Vis
spectrophotometer.
With reference to IEC 62321 edition
1.0:2008 in annex A, by solvent
Polybrominated
extraction and determined by GC-MSD
Biphenyls (PBBs)
and further HPLC confirmation when
necessary.
With reference to IEC 62321 edition
Polybrominated
1.0:2008 in annex A, by solvent
Diphenyl Ethers
extraction and determined by GC-MSD
(PBDEs)
and further HPLC confirmation when
necessary.
Reporting
Limit
2 ppm
2 ppm
2 ppm
1 ppm
5 ppm
5 ppm
Remark: Reporting limit = Quantitation limit of analyte in sample
DATE SAMPLE RECEIVED : JAN.11, 2012
TESTING PERIOD : JAN.11, 2012 TO JAN.13, 2012
**********************************************************************
TO BE CONTINUED
PAGE 6 OF 9
Intertek Testing Services Ltd., Shanghai
TFH Division
Block B, Jinling Business Square,No.801 Yi Shan Road,
Shanghai, China, 200233
Tel: +86 21 6120 6565
Fax: +86 21 6127 9740
www.intertek.com
www.intertek.com.cn
China Toll-Free: 800 999 1338
TEST REPORT
NUMBER: SHAH00299962
TESTS CONDUCTED
(IV) Measurement Flowchart:
Test For Cd/Pb/Hg/Chromium (VI)/PBBs/PBDEs Contents
Reference Standard: IEC 62321 edition 1.0:2008
sampling/grinding or cutting
Cr6+
Cd/Pb/Hg
metal
weigh sample and
for different
material, digest
the sample with
confirm the tested
samples are totally
dissolved
spot test
negative*2
No
polymers /
electronics
weigh sample
and add
alkaline
solution
get 50cm2
samples
definite
temp.
boiling water
extraction
cool and
filter the
extract
PBBs/PBDEs
weigh sample
and add
organic
soxhlet
extraction or
solvent
extraction
make up with
deionized water
analyzed by ICP-OES
make up with deionized
water and add diphenylcarbazide solution
concentrate
the extract
and make up
with organic
analyzed by GCMSD
analyzed by UV-VIS
**********************************************************************
TO BE CONTINUED
PAGE 7 OF 9
Intertek Testing Services Ltd., Shanghai
TFH Division
Block B, Jinling Business Square,No.801 Yi Shan Road,
Shanghai, China, 200233
Tel: +86 21 6120 6565
Fax: +86 21 6127 9740
www.intertek.com
www.intertek.com.cn
China Toll-Free: 800 999 1338
TEST REPORT
NUMBER: SHAH00299962
TESTS CONDUCTED
REMARKS:
*1: List of appropriate acid：
Material
Acid added for digestion
Polymers
Metals
Electronics
HNO3,HCl,HF,H2O2,H3BO3
HNO3,HCl,HF
HNO3,HCl,H2O2,HBF4
*2: If the result of spot test is positive, Chromium VI would be determined as
detected.
**********************************************************************
TO BE CONTINUED
PAGE 8 OF 9
Intertek Testing Services Ltd., Shanghai
TFH Division
Block B, Jinling Business Square,No.801 Yi Shan Road,
Shanghai, China, 200233
Tel: +86 21 6120 6565
Fax: +86 21 6127 9740
www.intertek.com
www.intertek.com.cn
China Toll-Free: 800 999 1338
TEST REPORT
NUMBER: SHAH00299962
TESTS CONDUCTED
**********************************************************************
END OF REPORT
PAGE 9 OF 9
Validi
Please
,Ffff,*r+
i B 4 q ( N o ). : C E / 2 0 1 2 l 1 0 8 3 6
Test Report
Efi(Date):2012l0r/11 q l t ( P a s e ) : 1 o f 1 0
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87, D-98669 \aEILSDOnr, CrnUrry
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87, D.98669 VEILSDORF,GEL\LAIY
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( R e s u lt )
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2
reference to IEC 62321: 2008 and
perlorned by ICP-AIS.
,5
+*rDt 6232L'2oo8ttA, ,r(&,6F
r
A{*AA44I{*&A:.1.
r e f e r € n c € t o I E C 6 2 3 2 r : 2 0 0 8"i,n
and
/ Lead ( Pb)
perforf,ed by ICP-nnS.
4+Is. 6232rt2008rii. /,*Bl4
/ {i ih
+€tF+*4i{r*'ft*xl.
*. / vercury (Es)
2
reference to IEc 62321: 2008 and
pe.forn€d by ICP-A!S.
++tgc 6232r.2oo9fit, r/)k,Y"4
7i'llr& / nexavalentchroniun cr(vI)
4.i*lt;Fl. / rith ref€rence to IEc
62321: ?008and perfor0€d by
BoiI inE water extraction Merhod,#
An+R&*
sulfonat€s
4+us EPA35.10C,1996ti4, 'Xr{
/ Perrluoroocta.e
h.t 44f, ;*A,if :rlAfl.*R tt&+E.
( P F O S - A ci d , M e r a l S a l t
/ Iilh referen.e 16 us EPA 3540C:
1 9 9 6 n e t h o d f o r P F o SC o n t e n t .
Analysis sas perforned by LCINS,
ift+d.(14)
/ PFoA(cAsNo.: 33s-6?-
4+US EPA35a0c:l996tii,
,)(t{
4fr.+c(J*)n&
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1)
/ s i t h r e f e r e n c e t o U S E P A3 5 . { 0 c
1 9 9 6n e t h o d f o r P F O AC o n t e n t .
Analysis vas perforned by tClMS.
c o m o a n+vj l 1 / n r l , r r , f ' | , 1 , i : 1 f i l r ,
r.I ltri{::
ny ssbled io b GeneG cond[dns d se
on|yandw$|.lhelmcolc6i|sns
bi€d rh s €d €Podennd e
PrsG)
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Test Report
lE*r(No-) : CE/2012/108s6
ES(Dare) : 2012101/11 F&(pase)
ELSCHUKOIELEKTROGCHUTZLOVPoNU,ITINtsAU
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8?, D-98669 VEIISDoRF,CERMANry
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/ M o r o b r o n o bpih e n y l
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/ T ri b r o n o b
rphcnyl
/ Tetrabronobiphenyl
/ P € n t a b ! o m o bDi h e n Iv
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:i*d86d
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qAdSEt
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/ P e n t a b r o n o d i D n e r v€l t h € r
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5
5
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5
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to IEC 62321. 2008a,d p€.lorhed
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t ttfltlltrfr
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5
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6*
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(F) (cAs
(fi") / Haloser-chlorine (cl) (c'{s
6*
!o.: 22537-15-1)
(;i) / Halos€.-Bronine(Br) (cAs
&l
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(4t) / Halogen-lodin€(l)
6*
50
r,lrt+,gff
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ag/(t
50
/ I[ith .efe.ence io Bs EN
&r)fi.
1 4 5 8 |22 0 0 ? .A n a l y s i s{ a s
(cAs
50
No.: 14362-44-8)
c o m D a n; "v, r 1 r i | l , f _ a { l , r . r r , , Jnt i j l r : r ] . 2 j i
ii!.fli,
r . 1rr rrlJLl.
r i r : ' I l l l ) . : l : , i l t . , i + s 6 i o n r * r 7 e r + s 6 o r ) r e e r rv t u { r @ h
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frq(No-) : cE/201?/10836 g i ! ( D a i e ) : 2 0 r 2 l o r l r l F * . ( P a r e ) ; 4 o f l o
EISCHIJXOI'{
ELEKTROSCHUTZKO\{PONEI\'TENBAU
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8?, D-98669 VEIT,SDoRF,GERMANry
lllIrIlrl||||u[tl|l
fiii(Note):
1. nglkg = ppni 0.lwt% = 100oppn
z. n.d. = Nor D"t.cr.d (*.ifA)
3 . M D L= M e t t r o dD € r e c t i o n L i n i r ( t t i l F x l E f B l & )
' : Nor Resulated (**ei'.ii.)
,t.
.
.
=
5.
Qualitaiive analysis (No u.ir) €,I4r)tt(*+dn)
6, # =
a. Posjlive
(Posi t i
b,
"e*. +;r{ 3t E &,1i,rl t{ ,r.ll r8)
Negative
(Nesa
ti
Eeais the Fresence of CrVI on rhe tested areas
neans the
absence of
C.VI
on rhe
iesied
areas
"€e + iri:;l E ii. i1A trlt{ '\fiJ} )
The d€tected concentration in boiling-water-ext.action solutibn is equal or sreate. th:n 0.02 bglkg with
50 cm, tested areas. / lii)*i{,i,8=0.02
malks sith 50 cm, (tested areas)
7. *l s 0t,nl?i,t.
A+ + if ^*,i,E 6tFl:lt' *r+ f ftliEe;il*,3*
+rri.a4f&r!
+-titr 616s.
(The satuples sas/{€re anaiyzed on b e h a l f o f l h e a f p l i c a n t a s n i x i n s s a m p l €i n o n e t e s t i n g . T h € a b o v e
r e s u l i s w a s / w e r eo n l y g i v e n a s t h e i n f o r n a l i l y v a l u € . )
PrOs++itfi.(Refer."ce Inforiatior)
(Directive 2006/122lEc)
. lE+ 2006/122/FL
(1) :**r( 6irE,ai4-Ld..n,s :ar+*lrf d.Ec.Er\rl**r*a++{.i'i+o. 00s%.
(Maynot be placed on ihe oarket or used as a srbstanceor constituent of preparations in a €onc€ntratioi
€qu,l io or !igher lhan 0.005 % by nass.)
(2,t hY4q&*fr*rii+d.sd.fi"%4.*#r{+r 1kr5e+rExfirt4ApFosltti€,*+6-La&.rElt€_LitSPFlsg&
i.lA+,Ad.ri^0.1%,d,1&& A,t+!-&6,*,9,t'*Isos.arts't f + Al+Ad.d,Arus/".
(May.ot be placed on th€ narke! in seni finished products or a.ticles, or paris rh€reof, if the
concentration of PIOS is equal to or hiab€r than 0.1 % by nass calculated *ith r€ference to the nass of
s t r u c t u . a l l y o . n i c r o s t r u c t u r a 1 Ly d i s t i n c t p a r r s r h a t c o n t a i n P F 0 6 o r , f o ! t € x t i l e s o r o t h e . c o a t e d
naterials,
i f t b e a m o u n t o t P F O Si s e q u a l t o o r h i s h c r t h a n l U s / n : o f i h € c o a i e d n a t e r i a l . )
c o m o a n4v , r / t r , , t - i ' : , 1 " : i : ! n l r r i
, I
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r r _ i ir ? r r 1 , , r
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t A , 4 ( N " . ) c, E / 2 0 L 2 / t A A 3 6
E&(Date):20I2l0r/11
FjR(P:se):5ofro
tl|
ELSCIIUKON
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CMERBESTi.ASSE
8?, D-98669 WII,SDORF, GER\{A\Y
t e o N o .)
*.S4ft(styre/l
( c - 1 ) 1 0 1 . 0 1 7 7 .o ( c - 2 ) 1 0 1 _0 1 8 3 . 0 ( c - 3 ) 1 0 1 . 0 1 ? 2 .0 ( c - 4 )r 0 r . 0 r 8 r . 0
( c - 5 ) 1 0 1 . 0 1 3 2 -. ( c - 6 ) 1 0 1 . 0 1 3 1 . 0(c-?) 101.01?1.0
( c - 8 ) 1 0 1 . 0 1 3 s -. ( c - 9 ) r 0 1 . 0 1 5 7 .0 ( c - 1 0 ) 1 0 1 . 0 1 3 6 -. (c-11) 101-- 064. ( c - r 2 ) 1 0 1 . 0 1 6 6 -. ( c - 1 3 ) 1 0 1 . 0 1 s 8 -. ( c - 1 4 ) 1 0 1 . 0 1 6 1 -. ( c - 1 5 ) 1 0 1 . 0 1 5 5O
.
( c - 1 6 ) 1 0 1 . 0 1 2 8 0. -
cdpaiy:
copper tin alloy wire CuSn6
copper cLad{ire - Elcon 30
coppcr cLad steel wire - Elcon F
copper clad iron-nick€l-alloy si.e
Elcon D
silve. copper alloy wire
AgC!50
silver copper alLoy wi.e Agcugo
.opper vire
Cu99.9%
silver copper alloy wire Ag72Cu28
copper-zinc-alloy
wire C u 8 0Z n 2 0
.il'er copnerallo/ ri-F A g 4 5 C L 5 5( A g a L 5 5 )
-
copper plared, brass plared sp.ing-steel wire silver copperalloy sire
A 8 c u 7 0( E l c u 7 0 )
silv€r coppe. alloy vire
ANu80 (Elcu8o)
oxyaenfr€€ copper vire
OF Cu
copper-,in.-alloy
vi.e
C!70 Zn30 (Vs 70)
tungsten Furiry uire
lV
1 1lt r-ll i,,r i;.llilr'i 1!.I11 1ir..l:
DyabPdlob6ela|cofuldi3bis
i4riii;,x{1i.r!,),r16.^En
tN ntlnl
:r.,.,,rift,y.
-:,r r:r:*!t..:i1+s60,r,,errt
FST, Cu -%
scs
,n{-d,*E+
Test Report
!tr6(No.) : cE/2012l108s6 E S ( D a t e ) : 2 0 1 2 l 0 1 / 1 1 q r & . ( P a s e ) : 6 o f 1 0
||l| [ttn]t
DI-SCHLTI(OI\4
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87. D 98669 VEII^SDoRF,CEL\IAI\ry
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!o belowiow chan. ( cP bst methodexcluded)
2) jd :l\',,.I : t} 4.L / N6meorthe personwhomademeasuremsntr
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3) ,Ilit I t ^ . t[4* / Nam€of the personin chaqe of measuRent Trry Chans
tri{ ' {I*i*.s /Cutins.Pl€ aBlion
idnt*stl
/ Sample
Measu€menl
f.f,1. Fl*e $tl f ,6,x,af 6lriG lifi lt (:{'T,i.
ti) /Acid digstion by suilableaciddepeded on
direren!ssmde maiedal(as belowlable)
4i CJ{ Ct/l.f!&trr&,tfi rL /
Micro'i/avedigeslion wilh HNOy'HCUHF
,!ll4,6f [A4tiifrit,+
*. / Healto apprcpdate
lftA|+
a|!g+€d4+41#t*&
Material
{,%+tJ / SamPle
q€el. coo!€i. aluminun. soltler
/ HCllo di$ol',€
irlLAitllt
/ oiqeslion
Acd
.t,t, diaa,taa, &,*.at,,tl"t /
/add
'tX,l/.-q t +,k).ltr't
jrii{srg{a 540nm6t4
{.d, !ln+, 4&, Ec / H,so.,Ho,, HNo!Hcl
,! \1t1T.{4:
i
,"^*ailxa
&@ Esia. HNO3,HCl,Hl H,o,
/ HNOyI-IF
{ft,1Rli
Gdld datirum Mlladium erami.
c o m e a nlyi l , 1 / l l r i r ! - t i ' i , r r , . ' i , ! i ! . i
filier digestatelhough liller
/ rcP-AES
rrii ).?rl;r
ont 3id w u'n rh6h{s or c iads nshldLoisiany rhaConFntssoe6s
?,:|6tl
/ Any acrd to total dig€€tion
p 6(s)resredrh s led epod eiid
i n 4n Lritlrl.
*
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|l!r
rfla#+
Test Report
ftt6(No.) : cE/2012l10836 E S ( D u t " ) , 2 o l 2 l 0 1 / 1 1 F * . ( p a s e ) : z o r r 0
ET,SCIIUKOMELEK'|RGSCHUTZKOMPONENTENMU
GMBq
GEWERBESTTSSE 87. D-98669 \,'EII-SDOXF. GERV,q\Y
t*t*/
t i**tl,*+&fiaf
tl|
/ PBB/PBDE
FLOWCHART
anaryticat
. ,|l:{,,i.F I 44ry / Nameoltheperson$ho mademeasurement
RomanWong
. t'l*i F 1,,- : 'f,+q / Nameof lhep€rconin cnaeeof measufement
T'oyChang
t\,ilil{rr
/ FiFltsiing prccess----------.f
...----.
prcc€ss
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/ tSriif
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byGc/lvfs/ RleE&f.'*&.+&
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fi,6(r".),
CE/2012/1aa36 E r q ( D a r e: ,2 0 1 2 / 0 r / r r F i H . t p a B :e8) o r t 0
EISCIIUKOM
ELEKTROGCHUTZI{OIIPONENTENB,{U
GMBH
GEtrERBESTRASSE
8?. D-98669 WII.SDORF. CXRMANry
f f'+fit€f,
t
I
trffLntI| Ilrtfll
/ Analyticalflou,chartof halogencontent
,!13t,\F : ttg* / Nameofthepersonwhomademeesurement:
RitaChen
tr!3t,€ l,\ : 'Fr$4 / Nameof thepersonin chargeof measu€ment:
TroyChang
*a & frFr}+trI
Analysiswasperformedby lC
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Test Report
€i6(No. ) : CE/20t2lr0836
AS(Date):2012l01/ll
FlR(Pase)ieofto
rtl |lll
ET-SCHUI{OM
ELEI{TROSCHUTZ(OMPONENTENMU
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GEWE&BESTMSSE
87. D 98669 VEILSDORF.GE&\!AIY
*{+F}frfi4cf
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Analyticalflow chartof So)drletextraction(LC/MS)procedure
r
I
ic|l:{ -F: Ai4# / Nameof theperconwhomademeasurement
RomanWong
tll*,Atl.:
tiBF / Nameof thepersonin chargeof measurement:Trcy
Chang
( ls'{ E: AE+H,*.t/An+*(s)' *it:4i{E6&
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Itfr i Data
c o m p a n y . r 1. , l 1 l L r i : , r l , 1 1 i: | r r l .
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Test Report
: CE/2012l10836
Es(Date) , 2012l01/11F{(page)
ET-SCHUI<OI.T
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t RH fst*fi*+
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E *(Dare)
: 2ai.2/a1/1z
Validit
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ELSCHI'{Oi' ELEKTROSChUTZ(OVPONEMENBAU
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trTi{*&efi*8P
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as) :
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11"9"4fi(sryl€/I temNo.)
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To PAGE
5)
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2012/t1
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itIS(N6. ) : cE/2012l10834
qs(DaLe): uol2lot/tl
n*(pa8e) : 2 oI r0
ELSCIIU(OTI
ELEKMOSCiIUTZKO}TIONENTBNMU
GMBH
GESSRBESTRASSE
87, D 98669 \'EIISMRF, CERN,{IY
idLg*(Test
llfllflNl[lttutl
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.eference ro IEC 62321: 2008 aid
perforned by ICP-A'S.
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++rFE 62321,,
A€*,.f +*+lrt r*A*,!i. / wirh
68
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by ICP-AXS.
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by ICP AXS.
perforn€d
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/ iri rh ief erence to tEc
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6 2 3 2 1 , 2 0 0 Aa n d p e r f o r n e d b y
B oi t i n s ' a i € r € x t r a c t i o n l t e t h o d . #
An+B,*&
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s u l f o n a t e s ( P F O S - A C i dv, e t a l s a l r ,
4+us EPA3510c,1996rii, ,(ri
l0
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/ Sit! reference io US EPA 3540C:
1 9 9 6 n e t h o d l o r P F O SC o ! r e n r ,
Analysis vas pe.fo.ned by tClMS.
an+6(r4)
/ PFoA(cAsNo.: 335-6?-
4+us EPA3b1oc,r996til,
,x,t
t0
€,?{ f, rt&l*,fl }n+d.(r*) 6t
1)
/ r / i t h r e f e f e n c e i o u s E P A3 5 1 0 c
1 9 9 6n c t h o d f o r P F o Ac o n t e n t .
Analysis {as peiforned 6y rc/MS.
ri
comranY
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lrr'lr'i
i ,.'irl;l nii
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*4(No. ) : cE/2012l10834
a&(Date) : 20r2/or/r2
F*.(par€) : 3 of ro
E-scllUKOIl ELE(TROSCHUTZI(oIPONENTEN&{U
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87, D 98669 VEITSDoRF, GERII,AI\'Y
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ro IEC 62321.2008 and p€rforned
by CC/MS-
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ether
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l er
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(;*) / Halogen-Brosi.e(8.) (cAs
6*
{o.: r0097-32-2)
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50
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50
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&i*1.
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50
50
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.r
r . , l r . , r i
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fi|fi,+r+
TestReport
*€(No. ) : cE/2012l10834
AA\Date) : 20r2/0r/r2
Fg.(pase) : a of 10
E-sCIruIOU ELB<TROSCHUTZKOIIPOIIENTINB,{U
GMBH
GESERBESTRASSE
87, D-98669 VEItsDoRF, GIRMANry
tI|||l||lt][trt|l!
f,li(Note):
r . n s l k 8: P p n ;0 . l n t %: 1 0 0 0 P P n
2 . n . d . = N o r D e t e c r e (d, f t . A * )
3. MDL= MerhodDere.rionLioit (t*.l*tFltsfE.ti)
4. '-' : Noi Res'1.r.d (**n*.i4.)
5 . . . : Q u a l i r a t i v ea n a l y s i s( N oU n i t ) . t , E r > r 4 G R + A )
6. #:
a . P o s i r i v e m e a n s r b e p r e s € n c eo f C r V I o n t h e t e s r e d a r e 2 s
(posi r i vei.6n,l:d, E&jA ;Flr|l ,r.ll J} )
b. Nesative means th€ abs€nce of C.VI on tle
( Negar i veA + jr,l:i, E }{ ^.fi '4lr,j ,rllj*
tesred areas
)
T l e d € t e c t e dc o d c e n t . a t i o ni n 6 . i r i n s _ q a r e r - e x t r a c i i o sn o l u r i o n i s e q u a Lo r g r e a t e . t h a r o , o 2 o g l k g w i t h
s0 csr tesred ar"a", / it8ii;AA=o.02
na/ks uiih 50 cm?(tested areas)
7- *tsiitrl:{€I,'A
f ;6^*,tEAtslit
' lE*f tli&A)rl:t}: *.ir1ti.4 f tEfl+-+iJ{ t.l+&.
(Tn€ sanples vas/sere analyzed on b€nalf of rhe applicanl
resulls sas/-€re only giv€n as rh€ info.naliry value.)
as nixing
sanple i.
one resring.
Tle above
8. ttr)*E+4c.f\2orzlor
/ rrir'tt *gcE/20t2/tos3l&+.
( T h i s r e p o r t s ! p e r s e d e s t h e p r e v i o r s d d . u D e n tb e a r i n g r h e r e s r r e p o r t n u m b e rC E / 2 0 1 2 l 1 0 8 3v4h i . h v a s
i s s u € do n 2 0 1 2 l 0 1 / 1 1 . )
Plost+
fin (R.f.'.nce
InJoraa!ion) | )A+ 2006/r22/M (Dltecrirc
2oo6/t22/w,
(r) Ji&( 4;rfl +t4_Ld.&n r{.++**rlfd.aeflrt+€g;ia+,a*.rJi+o. oo5%.
(May not be placed on rhe oarket or used as a substaace or constituent
equal to or higher than 0.005 % hy hass.)
of Dreparaiions in a conc€n!ra!ion
(2r r hy4rr &*fi 8!at+d.s{.ff tr"d.4b4; 1Rri+t+}3EH*.4{ pFoss49€-.r*fi}a&hii€}g4pFos6i
j'*.P!osAA}.{tf f 5g+,i4,*.ji'ifrug/.r.
,tA++t A,Ao.t%, fi,rt,{'sd.*{tt$*rtr,
(Nay not be Placed on rh€ narket in seEi-finished products or arricles, or parts rh€reof, if the
conc€n1.ation of PFOSis equal to of hiChe. than 0.1 % by nass calculared virh r€ference to the nass oI
s t r u c t u r a l l y o . m i c r o s t r u c t u r a l l y d i s t i d c i p a ! t s t h a t c o n t a i n P F O So r , f o r t € x t i l e s o r o t l e r c o a t e d
naterials,
if
the a'iount of PIOS is equal to or Iigher
cmoanyr:fr111r! Lll i.,ri,j.,lnlr.i i: i.tri
li,,!,Ll\
i.r
than 1Ug/n? of the coated nareriaL.)
4.r ir,rtr,,!.
fil-d,+E+
it6(No.)
Test Report
: cEl2012lI0834
Aq(Date)
, 2012/01/12
ELSCI1UKOM
ELEKTROSCHU']'ZKONPONENTENBAU
CMBH
GEIERBESTRASSE
8?, D-98669 \'EILSDORF, CETMI\Y
tlB4lt
: 5 of t0
F]R(p,s")
t||uI|
(siyle/ I !€n No.)
(A-1) 101 - - 2?1.0 - - - -tinned copperwi.e-Cu, Sn %
(A-2) 101 - - 283. 0 - - - -tinned.opper clad wire-El.on 30, Sn - - %
- - -tinned copper clad wirc-Elcon F, Sn - -%
(A-3) 101 272.0_
_
(A-4) 101
281. 0 - - - -tinned copper clad wi.e-ElconD, sn - - %
(A-5) 101(A-6) 101 (A-?) l0l _
(A-8) I0l -
- 221,.0 - - - 24-. O - - - 257,0
- - 232. 0
-
(A-9) 101 - -234.0(A-10) 10r- - 255. (A-11) 101- - 229. (A_12) 101- - 235. (A-13) r01 - 23r. (A-14)r01
cmpaiy;,.
r,
llr'r:
-rinned
-tinned
-rinned
- - -ti.n€d
- -
-tinned
- - - -tinned
- - - -tinned
- - - -tinned
236.----
i
-tinned
: ,l.lj,lilr+
copper nickel alloy ui.e-CuNi{4, Sn - -%
s i l v e r p i a t e d c o p p € rF i r e - c ! ,
As--%, sn -- %
brass vire-Ct802n20, Sn - - %
silver copper aitoy vir€-Ascu50, Sn
%
s i l v e r c o p p e r a L L o yw i r € - A s c u g o , s n - - % ( E l c u g o , s i
coppe. zinc aLloy pire-Cu702n30, Sn - - %
c o p p € r n i c k e l a L L o yr i r e - C ! N i 1 2 , S n - - ,
%)
s i l v € r . o p p e r a L L o yv i r e - A g 7 2 c u 2 8 , s n - - ,
- %
wire-A81000, sn
sitver
- t i n n e d s i t v e r c o p p e ra l l o y
r.ril
-
l+!r,]].
"ire
P]BG)bsbd rh 3 bi cPod €nnd e
r 4, L|\i.
poigb't}6lobcl€daodhsdgm
A s 4 5 c u 5 5s. n -
- % ( A g c u s 5S, n )
]||lr]|lt
,Ff'd,*E+
Test Report
itS(No. ) : cE/2Or2l10834 a*(Date) : 2ar2/a1/L2 F*(P.8.)
EI-SCHLXOM
ELEKTROSCHUTZ.(OVPOMNTENBAU
CVBII
GEFMBESTMSSE87, D-98669 VEIT^SDORF,
GEL\!AIry
|r []t
. ( ilt jtjrt i{t* ff + ) / Thes€sampt€€
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we€
dissolvEdlolalt by pHonditioning methodaccoftting10betM no/r ch€rt. ( CP testm€thodexcluded)
4 ir, d^ I : lr.Ett / Nameof the pe6onwio ftade m€surement ctimbs€aryans
3) )rlll fi I ^ : tl,l|^ / Nameorthe p€Bonin chaBeol measu€mentTroyChans
. Peporation
/ Cutting
t{.'1.*{*.9
dq$slil
/ sampleMe*uemenr
fti{ r E*.s n{ { 6,} !! f,.0 *i3li,I &(r,T*.
rf +) / rdd dtg€slion
bysuitaueaciddep€nded
d
(asbetowtabte)
diffe€ntsamplsmateriat
d &/I &/i. s.*at&tit ib /
Micwve digestian
wnhHNoJHct/HF
j!ti l{ it +
,, t*4iitE&
+. / Heatro appropnab
1) &8fi;4 /AlkaliFudon
2) i*t8t+ / HCllodissoh€
rgrt'rst*,*+*4.Jt,rlfl
*.sltrf
/ ICP-AES
/ sampleMatedal
S1eel.coooer.aluminum.solder
/ Cool,
AftlirQ*{'s
nllel digeclaleomugh liher
/ oiqestion
Add
tXib*&&t
.at! sr!, !at, i.f.*, !*.+ /
Aquareqia,
HNOrBCl,HF,H,O,
e\*eilf,e
/Add
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4&,1Rt
/*tlX-a A,kk1+t't
tl*eatta 54onmAt4
Gold.Dlatinum,
Dalladium.
c6'dmic
.t&, ttr.+, drn, 4.t / HzsorH:o, HNo:,HCI
rF\4+t;r&7?aa4
4atedb16Geie€rcodroisot
| Anyacidlo lotal dbestion
s
3polgb'ty6lo'9c'd'ddh6e!
ab6dban@ al 540 nm by
UV.VIS
fllr
,t{'d,+E+
Test Report
it4(No. ) : CE/2012lr0834 A * ( D a r e )
. 2072/07/t2
F*(P.g.)
ET.SCHU(OM
ELH(TRG5CHU1'ZKOMA)NEMENBAU
GI{BH
GEAERBESTI.ASSE
87, D.98669 VEILSDORF.GERVAIY
t*i+/
tmrum tlltmr
/ PBB/PBDE
analytlcal
FLOwCHART
t*i&g,.&*,€ll
r ;il$r'.t : 4iir# / Nameoflh€peEonwhomademeasurcment:
RomanWong
r FIE\A l/\ : 'E-** / Nameof thepersonin chaEeof measurement
TroyChang
---------+
?r^,rli{fll / Firsttestingproc€€s
1ti*la$*€,+ / oplional
sc€[email protected].
SrS{1,l / ConfnnalionDrcGs - . - .)
Sc.eenanalys's/ir$
"+4
I
I
Sampleext€c1ionSa;+*.-/
Soxhleimethod*1.++t*
Concenvate/Dilute
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sfrR;i*ffif
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Analysis
by GCAIS/ *,IAEf|ii'*it+4
c o m e a !n: v
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of prepararrons
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ure
c o n c e n t . a t i o n o f P F O Si s e q u a t r o o r h i g h e . t h a n 0 . 1 % b y n a s s c a l c ! l a t e d s i t h r e f e r e n c e t o t l e n a s s o f
s t . u c t u r a l i y o . f r i c . o s t r u c r u r a l l y d i s r i n . r p a r r s t ! a i c o n t a i n P F o . so r , f o . r e x r i t e s o r o t h e . c o a r e d
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TESTREPORT
NO.:4002E11121307-2R02
page1of4
Oa!aiDec15,2o11
Customer:SuzhouFuHongElectrcnic
IndustfialCo,
Ltd.
Addrgs8:NO.89WElDUROAD,WANGTING
TOWN,
XTANGCHENG
D|STR|CT,
SUZHOU,
CHTNA
Reporton th6 3ubmittedssmplesaidio be
Samplename:Fusoscoppershell
llodol: /
Material:/
D$cription:/
Buyea:/
supplier:/
Sa|nplerecelveddate:Dec.13,2011
Tcatlngp€riod:FrcmDec.13,2011
to Dec.15,2011
T€tino Reau6ted
As specined
by client,to delermine
theL€ad,Cadmium,
Mercrry& Hexavatent
Chrcmium
contentin thesubmitted
samptein
accordancewilh Direclive2002/95/EC(RoHS).
Tcstindmethod:
Testing llem
[,leasudng
inslrument
MQL
Lead (Pb)
EC 62321:2008,seclion9
ICP-OES
2mglkg
cadmium(Cd)
(Hg)
Mercury
EC62321:2008,sectionI
ICP€ES
2 mg/kg
EC62321r
2008,section7
rcP-oEs
2 mg/kg
(Crl'I)
Chrom'um
EC62321:2008,
AnnexI
0.02mg,a(g'
lsg
-'0.02mg/kgreturs
10lheMQLofsample
extEction
tiquid.
99!s!.c!i9!j
-ffien tesiedas specifred
thesubmitted
sample
complied
withtherequircments
of commission
Decision
of 18Aug2005
amending
Directive
2002l95/EC
nolified
lnderdocument
2005/618/EC
ILS, PLEASEREFERTOTHE FOLLOWINGPAGE(S)'**'
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S}'EI{ZN€N AOV TGSTINGT€CHNOlOGY CO.,L'D.KUNSHAN EiANCH
Hotllne
86-512-551
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6
TESTREPORT
NO.:4002E11121307-2R02
Add the digestionsolution;the
vesselis heatedLrntillhe sampl€
AddHrO,unlilthesampl€is clear
F;;1.-F;;,",..;-1.-
Cooling
thevessel,fllleriwashedand
filledto themarkwithdistilled
water.
{Melalsubslrat€)
Add lhe digestionsolution,clos€
The sampleis digestedin the
the macrowavevess€|.
micrcwave oven following a specific
program.
decomposilion
Coolingthe vessel,filter washedand
filled to the mark with distilled water.
Remove
thesample,
andcool
lhe beakerlo rcomtempefalure,
anddo1ie colorreaction
Heal50 mL ofDlwaterin lhe
beakertoboilingfor 10 min
Testthesamplesolution
andlhe 0.02
mg/kgstandard
solution
by UV-VIS.
To Detemine
(Praring)
andl\rercury
Content:
coor,ns.
nrr",
*""n"0 r"o
_____-l
""0 |
I
tothemark
withDtwater
I
,l o*o
-ill_.;*--;-l
I r*r.r*t
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STIENZH€NAOV TESIING T€CIII{OLOGYCO.,lIO,KUII9HAN BFANCH
Hdpi/j,w.o{,6n
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Hotline
8 6 - 5 1 2 " s 5 18 0o O 0
nov.
TESTREPORT
NO.:
4002E11121
307-2R02
Date:Dec.15,2011
Page3 ol4
5. ToDetemineHexavalent
Chromium
Contentln
colorless
andcolored
ctlromate
coalingon metals: (Plating)
'' ',.'1
re$eoovr I r
s.t sw-resi (M&
lflhe lest resullis positive,
the sampleis considered
1o
havehexavalenlchromium
Boiling- waieF extraction
procedure
shallbe usedto
and the 0.02 mg/kg
lfthe€ isrnterference
orI rshardto decide*terhel
lhesamplehavethehexavalent
chrcmium
5 2 BoilingwEter-en€ction
Takethe (5015)cm'z
samplein thebeaker.
Heat50 mlof Olwaterin the
beaker
lo boilingfor 10min
Remove
he sample,
andcool
lhe beaker
1oroomtemperature,
anddo thecolorreaction
Testthe samplesolutionand the 0.02
mg/kgstandardsolutionby UV-VIS.
Srmple d93cription:
Coppershellsubslrate
Leadwle Platrng
Unil
24
CoppershellPlaling
RoHS
Limit
2-3
24"
Lead(Pb)
mg/Kg
1000
N.D.
2.5
40.0
N.D.
Cadmium
{Cd)
mg/kg
100
N,D.
N.D.
N.D.
N.D.
(Hs)
Msrorry
(Crvl)
Chromium
mg/kg
1000
N.D,
N.D,
N.D.
N.D.
mg/Kg
1000
Negative Negative Negalive
Negative
SH!NZHEN AOV TESTINGTCCTNOIqGY CO.,L}D,KUNSHAN BFANCH
n
Hotline
86'512^551
80 0 0
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TESTREPORT
NO.rA002E11121307-2R02
Dat€iOec15,2011
-The new RoHSdi.ective2011/65/EU,
on Jul 21, 2011comeinto force,on Jan.03, 2013the fomat imotementation.
Dircctive
2002l95/ECshallbe reoealedsimultaneouslv.
Sp€cim€ns,wnicnrequestedto determineLead,Cadmiumand l4ercuryConlent,havebeendissotvedcomptetety.
-mg/kg=ppm
-N.D.=notdetected(<tVoL)
-MQL=l'rethodOuaniilationLimit
-Negalive=Abs€nce of Cr (VI);
Posilive=Prcs€nce
of Cr (VI)i
Uncedain=c€n noi ve fy whetherthe samplehaveHexavat€nt
Chrcmium by spoliesl.
(The tested s€mple should be furlher venfed by boiling-waterextradion
method if the spol test result is uncertainor
-'The test is basedon the followingassumption:Thesampteptatingis a singtetayerandeach pad is unifom. The test resutt
maybecannolslandior rhe physicartruthof sampleplating.
Photog.aphofSample
"'End of Repod"'
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n
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