Test Report. No. SHAEC1202568639 A01 Date: 23 Mar 2012 . Page 1 of 14. JIANGSU CHANGJIANG ELECTRONICS TECHNOLOGY (SUQIAN) CO.,LTD . NO.5 PUTUO MOUNT RD.,SUCHENG DISTRICT, SUQIAN,JIANGSU CHINA . THIS REPORT IS TO SUPERSEDE TEST REPORT NO.SHAEC1202568619 DATE: 2012/03/08. The following sample(s) was/were submitted and identified on behalf of the clients as : Pinlead part TO-92 include(TO-92S/92L92MOD/94); Package part TO-92 include(TO-92S/92L92MOD/94) . SGS Job No. : SP12-005356 - SH . Composition :. Silvery Metal Part . Composition :. Black Plastic Part . Date of Sample Received : . 12 Mar 2012. Testing Period : . 12 Mar 2012 - 08 Mar 2012 . Test Requested : . Selected test(s) as requested by client. . Test Method : . Please refer to next page(s). . Test Results :. Please refer to next page(s). . Signed for and on behalf of SGS-CSTC Ltd. . Fan Jingjie, JJ. Approved Signatory . 0000656427 Test Report. No. SHAEC1202568639 A01 Date: 23 Mar 2012 . Page 2 of 14. Test Results :. Test Part Description : . Specimen No.. 1. SGS Sample ID. SHA12-025686.002 Description. Silvery metal. 2. SHA12-025686.033 Black noumenon(mix all*) . Remarks :. (1) 1 mg/kg = 1 ppm = 0.0001% . (2) MDL = Method Detection Limit . (3) ND = Not Detected ( < MDL ) . (4) "-" = Not Regulated . RoHS Directive 2011/65/EU. Test Method : . With reference to IEC 62321:2008 (1) Determination of Cadmium by ICP-OES. (2) Determination of Lead by ICP-OES. (3) Determination of Mercury by ICP-OES. (4) Determination of Hexavalent Chromium by Colorimetric Method using UV-Vis. (5) Determination of PBBs / PBDEs content by GC-MS. . Test Item(s). Limit. Unit. MDL. 033. Cadmium (Cd) . 100 mg/kg. 2 ND Lead (Pb). 1,000 mg/kg. 2 ND Mercury (Hg). 1,000 mg/kg. 2 ND Hexavalent Chromium (Cr(VI)) . 1,000 mg/kg. 2 ND Sum of PBBs . 1,000 mg/kg. - ND Monobromobiphenyl . - mg/kg. 5 ND Dibromobiphenyl . - mg/kg. 5 ND Tribromobiphenyl . - mg/kg. 5 ND Tetrabromobiphenyl . - mg/kg. 5 ND Pentabromobiphenyl . - mg/kg. 5 ND Hexabromobiphenyl . - mg/kg. 5 ND Heptabromobiphenyl . - mg/kg. 5 ND Octabromobiphenyl . - mg/kg. 5 ND Nonabromobiphenyl . - mg/kg. 5 ND - mg/kg. 5 ND 1,000 mg/kg. - ND Decabromobiphenyl . Sum of PBDEs . 0000656427 Test Report. No. SHAEC1202568639 A01 Date: 23 Mar 2012 . Limit. Unit. MDL. 033. Monobromodiphenyl ether . - mg/kg. 5 ND Dibromodiphenyl ether . - mg/kg. 5 ND Tribromodiphenyl ether . - mg/kg. 5 ND Tetrabromodiphenyl ether . - mg/kg. 5 ND Pentabromodiphenyl ether . - mg/kg. 5 ND Hexabromodiphenyl ether . - mg/kg. 5 ND Heptabromodiphenyl ether . - mg/kg. 5 ND Octabromodiphenyl ether . - mg/kg. 5 ND Nonabromodiphenyl ether . - mg/kg. 5 ND Decabromodiphenyl ether . - mg/kg. 5 ND Test Item(s). Page 3 of 14. Notes :. (1) The maximum permissible limit is quoted from directive 2011/65/EU, Annex II . RoHS Directive 2011/65/EU. Test Method : . With reference to IEC 62321:2008 (1) Determination of Cadmium by ICP-OES. (2) Determination of Lead by ICP-OES. (3) Determination of Mercury by ICP-OES. (4) Determination of Hexavalent Chromium by Spot test / Colorimetric Method using UV-Vis. (5) Determination of PBBs / PBDEs by GC-MS. . Test Item(s). Limit. Unit. MDL. 002. Cadmium (Cd) . 100 mg/kg. 2 ND Lead (Pb). 1,000 mg/kg. 2 6 Mercury (Hg). 1,000 mg/kg. 2 ND Hexavalent Chromium (Cr(VI)) . - - ♢ Negative 1,000 mg/kg. - ND Monobromobiphenyl . - mg/kg. 5 ND Dibromobiphenyl . - mg/kg. 5 ND Tribromobiphenyl . - mg/kg. 5 ND Tetrabromobiphenyl . - mg/kg. 5 ND Pentabromobiphenyl . - mg/kg. 5 ND Hexabromobiphenyl . - mg/kg. 5 ND Heptabromobiphenyl . - mg/kg. 5 ND Octabromobiphenyl . - mg/kg. 5 ND Nonabromobiphenyl . - mg/kg. 5 ND Decabromobiphenyl . - mg/kg. 5 ND Sum of PBBs . 0000656427 Test Report. No. SHAEC1202568639 A01 Test Item(s). Limit. Unit. Sum of PBDEs . Date: 23 Mar 2012 . MDL. 002. 1,000 mg/kg. - ND Monobromodiphenyl ether . - mg/kg. 5 ND Dibromodiphenyl ether . - mg/kg. 5 ND Tribromodiphenyl ether . - mg/kg. 5 ND Tetrabromodiphenyl ether . - mg/kg. 5 ND Pentabromodiphenyl ether . - mg/kg. 5 ND Hexabromodiphenyl ether . - mg/kg. 5 ND Heptabromodiphenyl ether . - mg/kg. 5 ND Octabromodiphenyl ether . - mg/kg. 5 ND Nonabromodiphenyl ether . - mg/kg. 5 ND Decabromodiphenyl ether . - mg/kg. 5 ND Page 4 of 14. Notes :. (1) The maximum permissible limit is quoted from directive 2011/65/EU, Annex II (2) ◇Spot-test: Negative = Absence of CrVI coating, Positive = Presence of CrVI coating; (The tested sample should be further verified by boiling-water-extraction method if the spot test result is Negative or cannot be confirmed.) ◇Boiling-water-extraction: Negative = Absence of CrVI coating Positive = Presence of CrVI coating; the detected concentration in boiling-water-extraction solution is equal or greater than 0.02 mg/kg with 50 cm2 sample surface area. For corrosion protection coatings on metals: Information on storage conditions and production date of the tested sample is unavailable and thus results of Cr(VI) represent status of the sample at the time of testing.. Phthalates. Test Method : . With reference to EN14372: 2004, analysis was performed by GC-MS. . Test Item(s). Dibutyl Phthalate (DBP) . Benzylbutyl Phthalate (BBP) . Bis-(2-ethylhexyl) Phthalate (DEHP) . Diisononyl Phthalate (DINP) . Di-n-octyl Phthalate (DNOP) . Diisodecyl Phthalate (DIDP) . Di-n-hexyl Phthalate (DnHP) . Diisobutyl Phthalate (DIBP) . 0000656427 Unit. MDL. 033. %. %. %. %. %. %. %. %. 0.003 0.003 0.003 0.010 0.003 0.010 0.003 0.003 ND ND ND ND ND ND ND ND Test Report. No. SHAEC1202568639 A01 Date: 23 Mar 2012 . Page 5 of 14. Notes :. (1) DBP,BBP,DEHP Reference information: Entry 51 of Regulation (EC) No 552/2009 amending Annex XVII of REACH Regulation (EC) No 1907/2006 (previously restricted under Directive 2005/84/EC): i) Shall not be used as substances or in mixtures, in concentrations greater than 0,1 % by weight of the plasticised material, in toys and childcare articles. ii) Toys and childcare articles containing these phthalates in a concentration greater than 0.1 % by weight of the plasticised material shall not be placed on the market. Please refer to Regulation (EC) No 552/2009 to get more detail information DINP, DNOP, DIDP Reference information: Entry 52 of Regulation (EC) No 552/2009 amending Annex XVII of REACH Regulation (EC) No 1907/2006 (previously restricted under Directive 2005/84/EC). i) Shall not be used as substances or in mixtures, in concentrations greater than 0.1 % by weight of the plasticised material, in toys and childcare articles which can be placed in the mouth by children. ii) Such toys and childcare articles containing these phthalates in a concentration greater than 0.1 % by weight of the plasticised material shall not be placed on the market. Please refer to Regulation (EC) No 552/2009 to get more detail information . Polynuclear Aromatic Hydrocarbons (PAH). Test Method : . With reference to ZEK 01.2-08 of German ZLS and its amendments, analysis was performed by GC-MS.. Unit. MDL. 033. mg/kg. mg/kg. mg/kg. mg/kg. mg/kg. mg/kg. mg/kg. mg/kg. mg/kg. mg/kg. mg/kg. mg/kg. mg/kg. mg/kg. mg/kg. mg/kg. mg/kg. 0.2 0.2 0.2 0.2 0.2 0.2 0.2 0.2 0.2 0.2 0.2 0.2 0.2 0.2 0.2 0.2 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND Test Item(s). Sum of 16 PAH . Naphthalene(NAP) . Acenaphthylene(ANY) . Acenaphthene(ANA) . Fluorene(FLU) . Phenanthrene(PHE) . Anthracene(ANT) . Fluoranthene(FLT) . Pyrene(PYR) . Benzo(a)anthracene(BaA) . Chrysene(CHR) . Benzo(b)fluoranthene(BbF) . Benzo(k)fluoranthene(BkF) . Benzo(a)pyrene(BaP) . Indeno(1,2,3-c,d)pyrene(IPY) . Dibenzo(a,h)anthracene(DBA) . Benzo(g,h,i)perylene(BPE) . 0000656427 Test Report. No. SHAEC1202568639 A01 Date: 23 Mar 2012 . Page 6 of 14. ZEK 01.2-08: Restraining maximum values for products Parameter Category 1 Material indented to be put in the mouth or material for toys with normal skin contact for children aged < 36 months Category 2 Category 3 Materials which are not Materials which are not included in Category 1, with included in Category 1 or 2, predictable contact with the with predictable skin contact skin longer than 30 s. up to 30 s (short-term skin (long-term skin contact) contact). Benzo[a]pyrene (mg/kg) <MDL (<0.2)*** 1 20 Sum of 16 PAH(US EPA) (mg/kg)** <MDL (<0.2)*** 10 200 Remark : ** = Only PAH substances >0.2 mg/kg are taken into account while calculating the sum of PAH *** = In case that the maximum values exceed the limits of category 1, but are within the limits of category 2, one may confirm the suitability of the tested material which is indented to be put in the mouth by additional specific migration tests of PAH components based on DIN EN 1186ff and §64 LFGB 80.30-1. The conclusion of the migration test results must be made based on food law criteria. Tetrabromobisphenol A (TBBP-A). Test Method : . With reference to US EPA 3550C: 2007, analysis was performed by GC-MS. . Test Item(s). Unit. Tetrabromobisphenol A (TBBP-A) . mg/kg. MDL. 033. 10 ND Hexabromocyclododecane (HBCDD). Test Method : . With reference to US EPA 3550C: 2007, analysis was performed by GC-MS. . Unit. MDL. 033. mg/kg. 10 ND Test Item(s). Hexabromocyclododecane (HBCDD) . PFOS (Perfluorooctane Sulfonates) and PFOA (Perfluorooctanoic Acid). Test Method : . With reference to US EPA 3550C: 2007, analysis was performed by HPLC-MS. . 0000656427 Test Report. No. SHAEC1202568639 A01 Test Item(s). Perfluorooctane Sulfonates (PFOS) and related Acid,Metal Salt and Amide . Perfluorooctanoic Acid (PFOA) . Date: 23 Mar 2012 . Limit. Unit. 1,000. mg/kg. MDL. 10. ND. - mg/kg. 10. ND. Page 7 of 14. 033. Notes :. Max. limit specified by commission regulation (EU) No. 757/2010 (previously restricted under entry 53 of Regulation (EC) No 552/2009 amending Annex XVII of REACH Regulation (EC) No 1907/2006) . Remark: *The sample(s) was/were analyzed on behalf of the applicant as mixing sample in one testing. The above result(s) was/were only given as the informality value and only for reference. . 0000656427 Test Report. No. SHAEC1202568639 A01 Date: 23 Mar 2012 . Page 8 of 14. ATTACHMENTS RoHS Testing Flow Chart 1) Name of the person who made testing: Jan Shi/Yoyo Wang/Allen Xiao/Gary Xu 2) Name of the person in charge of testing: Jeff Zhang/George Xu/ Elim Lin 3) These samples were dissolved totally by pre-conditioning method according to below flow chart. (Cr6+ and PBBs/PBDEs test method excluded) Sample Preparation Sample Measurement Pb/Cd/Hg Acid digestion with microwave/ hotplate Sample solvent extraction Filtration Concentration/ Dilution of extraction solution Solution + Cr6 PBBs/PBDEs Nonmetallic material Adding digestion reagent Residue Positive Spot test Negative Filtration 1) Alkali Fusion / Dry Ashing 2) Acid to dissolve Metallic material GC/MS Heating to 90~95℃ for extraction Filtration and pH adjustment DATA ICP-OES Adding 1,5diphenylcarbazide for color development DATA UV-Vis DATA 0000656427 Boiling water extraction Adding 1,5diphenylcarbazide for color development A red color indicates the 6+ presence of Cr . If necessary, confirm with UV-Vis. DATA Test Report. No. SHAEC1202568639 A01 Date: 23 Mar 2012 . Phthalates Testing Flow Chart 1) Name of the person who made testing: Elyn Yao 2) Name of the person in charge of testing: Rachel Zhang Sample cutting/preparation Sample measurement Solvent extraction Concentration/Dilution Filtration GC-MS DATA 0000656427 Page 9 of 14. Test Report. No. SHAEC1202568639 A01 Date: 23 Mar 2012 . HBCDD Testing Flow Chart 1) Name of the person who made testing: Gary Xu 2) Name of the person in charge of testing: Elim Lin Sample cutting/preparation Sample measurement Solvent extraction Concentration/Dilution Filtration GC-MS DATA 0000656427 Page 10 of 14. Test Report. No. SHAEC1202568639 A01 Date: 23 Mar 2012 . PFOS/PFOA Testing Flow Chart 1) Name of the person who made testing: Judy Li 2) Name of the person in charge of testing: Linda Li Sample cutting/preparation Sample measurement Solvent extraction Concentration/Dilution Filtration LC-MS DATA 0000656427 Page 11 of 14. Test Report. No. SHAEC1202568639 A01 Date: 23 Mar 2012 . PAHs Testing Flow Chart 1) Name of the person who made testing: Jessie Huang 2) Name of the person in charge of testing: Elim Lin Sample cutting/preparation Sample measurement Solvent extraction Concentration/Dilution Filtration GC-MS DATA 0000656427 Page 12 of 14. Test Report. No. SHAEC1202568639 A01 Date: 23 Mar 2012 . TBBP-A Testing Flow Chart 1) Name of the person who made testing: Gary Xu 2) Name of the person in charge of testing: Elim Lin Sample cutting/preparation Sample measurement Solvent extraction Derivatization Liquid-liquid extraction Concentration/Dilution Filtration GC-MS DATA 0000656427 Page 13 of 14. Test Report. No. SHAEC1202568639 A01 Date: 23 Mar 2012 . Sample photo: . SHAEC1202568639 A01 SHA12-025686.002 . SHAEC1202568639 A01 SHA12-025686.033 . SGS authenticate the photo on original report only . *** End of Report *** . 0000656427 Page 14 of 14.