20126199344950316

Test Report.
No. SHAEC1207176309 A03
Date: 18 Jun 2012 .
Page 1 of 14.
JIANGSU CHANGJIANG ELECTRONICS TECHNOLOGY (SUQIAN) CO., LTD. .
NO.5 PUTUO MOUNT RD., SUCHENG DISTRICT,SUQIAN,JIANGSU CHINA
.
THIS REPORT IS TO SUPERSEDE TEST REPORT NO.SHAEC1207176307A02 DATE: 2012/06/06.
The following sample(s) was/were submitted and identified on behalf of the clients as : package part TO-247
(include TO-3P/251/252/220/220F/126/126C); pinlead part TO-247 (include
TO-3P/251/252/220/220F/126/126C)) .
SGS Job No. :
SP12-013405 - SH .
Composition :.
Black Plastic Part .
Composition :.
Silvery Metal Part .
Date of Sample Received : .
09 May 2012.
Testing Period : .
09 May 2012 - 13 May 2012 .
Test Requested : .
Selected test(s) as requested by client. .
Test Method : .
Please refer to next page(s). .
Test Results :.
Please refer to next page(s). .
Signed for and on behalf of
SGS-CSTC Ltd. .
Fan Jingjie, JJ.
Approved Signatory .
0000747644
Test Report.
No. SHAEC1207176309 A03
Date: 18 Jun 2012 .
Page 2 of 14.
Test Results :.
Test Part Description : .
Specimen No..
1.
SGS Sample ID.
SHA12-071763.001
Description.
Black body with silvery metal part(mix all*) .
2.
SHA12-071763.002
Silvery pin part .
Remarks :.
(1) 1 mg/kg = 1 ppm = 0.0001% .
(2) MDL = Method Detection Limit .
(3) ND = Not Detected ( < MDL ) .
(4) "-" = Not Regulated .
RoHS Directive 2011/65/EU.
Test Method : . With reference to IEC 62321:2008
(1) Determination of Cadmium by ICP-OES.
(2) Determination of Lead by ICP-OES.
(3) Determination of Mercury by ICP-OES.
(4) Determination of Hexavalent Chromium by Colorimetric Method using UV-Vis.
(5) Determination of PBBs / PBDEs content by GC-MS. .
Test Item(s).
Limit.
Unit.
MDL.
001.
Cadmium (Cd) .
100
mg/kg.
2
ND
Lead (Pb).
1000
mg/kg.
2
2981▲
Mercury (Hg).
1000
mg/kg.
2
ND
Hexavalent Chromium (Cr(VI)) .
1000
mg/kg.
2
ND
Sum of PBBs .
1000
mg/kg.
-
ND
Monobromobiphenyl .
-
mg/kg.
5
ND
Dibromobiphenyl .
-
mg/kg.
5
ND
Tribromobiphenyl .
-
mg/kg.
5
ND
Tetrabromobiphenyl .
-
mg/kg.
5
ND
Pentabromobiphenyl .
-
mg/kg.
5
ND
Hexabromobiphenyl .
-
mg/kg.
5
ND
Heptabromobiphenyl .
-
mg/kg.
5
ND
Octabromobiphenyl .
-
mg/kg.
5
ND
Nonabromobiphenyl .
-
mg/kg.
5
ND
-
mg/kg.
5
ND
1000
mg/kg.
-
ND
Decabromobiphenyl .
Sum of PBDEs .
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Test Report.
No. SHAEC1207176309 A03
Date: 18 Jun 2012 .
Limit.
Unit.
MDL.
001.
Monobromodiphenyl ether .
-
mg/kg.
5
ND
Dibromodiphenyl ether .
-
mg/kg.
5
ND
Tribromodiphenyl ether .
-
mg/kg.
5
ND
Tetrabromodiphenyl ether .
-
mg/kg.
5
ND
Pentabromodiphenyl ether .
-
mg/kg.
5
ND
Hexabromodiphenyl ether .
-
mg/kg.
5
ND
Heptabromodiphenyl ether .
-
mg/kg.
5
ND
Octabromodiphenyl ether .
-
mg/kg.
5
ND
Nonabromodiphenyl ether .
-
mg/kg.
5
ND
Decabromodiphenyl ether .
-
mg/kg.
5
ND
Test Item(s).
Page 3 of 14.
Notes :.
(1) The maximum permissible limit is quoted from directive 2011/65/EU, Annex II
(2) *The sample(s) was/were analyzed on behalf of the applicant as mixing sample in one testing. The
above result(s) was/were only given as the informality value and only for reference.
(3) ▲=According to the declaration from the client, Lead (Pb) in No.001 is exempted by EU RoHS
Directive 2011/65/EU based on: Lead in high melting temperature type solders (i.e. lead-based alloys
containing 85 % by weight or more lead). .
RoHS Directive 2011/65/EU.
Test Method : . With reference to IEC 62321:2008
(1) Determination of Cadmium by ICP-OES.
(2) Determination of Lead by ICP-OES.
(3) Determination of Mercury by ICP-OES.
(4) Determination of Hexavalent Chromium by Spot test / Colorimetric Method using UV-Vis.
(5) Determination of PBBs / PBDEs by GC-MS. .
Test Item(s).
Limit.
Unit.
MDL.
002.
Cadmium (Cd) .
100
mg/kg.
2
ND
Lead (Pb).
1000
mg/kg.
2
ND
Mercury (Hg).
1000
mg/kg.
2
ND
Hexavalent Chromium (Cr(VI)) .
-
-
♢
Negative
1000
mg/kg.
-
ND
Monobromobiphenyl .
-
mg/kg.
5
ND
Dibromobiphenyl .
-
mg/kg.
5
ND
Tribromobiphenyl .
-
mg/kg.
5
ND
Tetrabromobiphenyl .
-
mg/kg.
5
ND
Pentabromobiphenyl .
-
mg/kg.
5
ND
Hexabromobiphenyl .
-
mg/kg.
5
ND
Sum of PBBs .
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Test Report.
No. SHAEC1207176309 A03
Date: 18 Jun 2012 .
Limit.
Unit.
MDL.
002.
Heptabromobiphenyl .
-
mg/kg.
5
ND
Octabromobiphenyl .
-
mg/kg.
5
ND
Nonabromobiphenyl .
-
mg/kg.
5
ND
Test Item(s).
Decabromobiphenyl .
-
mg/kg.
5
ND
1000
mg/kg.
-
ND
Monobromodiphenyl ether .
-
mg/kg.
5
ND
Dibromodiphenyl ether .
-
mg/kg.
5
ND
Tribromodiphenyl ether .
-
mg/kg.
5
ND
Tetrabromodiphenyl ether .
-
mg/kg.
5
ND
Pentabromodiphenyl ether .
-
mg/kg.
5
ND
Hexabromodiphenyl ether .
-
mg/kg.
5
ND
Heptabromodiphenyl ether .
-
mg/kg.
5
ND
Octabromodiphenyl ether .
-
mg/kg.
5
ND
Nonabromodiphenyl ether .
-
mg/kg.
5
ND
Decabromodiphenyl ether .
-
mg/kg.
5
ND
Sum of PBDEs .
Page 4 of 14.
Notes :.
(1) The maximum permissible limit is quoted from directive 2011/65/EU, Annex II
(2) ◇Spot-test:
Negative = Absence of Cr(VI) coating, Positive = Presence of Cr(VI) coating;
(The tested sample should be further verified by boiling-water-extraction method if the spot test result
is Negative or cannot be confirmed.)
◇Boiling-water-extraction:
Negative = Absence of Cr(VI) coating
Positive = Presence of Cr(VI) coating; the detected concentration in boiling-water-extraction solution is
equal or greater than 0.02 mg/kg with 50 cm² sample surface area.
For corrosion protection coatings on metals: Information on storage conditions and production date of
the tested sample is unavailable and thus results of Cr(VI) represent status of the sample at the time
of testing. .
Phthalates.
Test Method : . With reference to EN14372: 2004, analysis was performed by GC-MS. .
Test Item(s).
Dibutyl Phthalate (DBP) .
Benzylbutyl Phthalate (BBP) .
Bis-(2-ethylhexyl) Phthalate (DEHP) .
Diisononyl Phthalate (DINP) .
Di-n-octyl Phthalate (DNOP) .
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Unit.
MDL.
001.
%.
%.
%.
%.
%.
0.003
0.003
0.003
0.010
0.003
ND
ND
ND
ND
ND
Test Report.
No. SHAEC1207176309 A03
Test Item(s).
Diisodecyl Phthalate (DIDP) .
Di-n-hexyl Phthalate (DnHP) .
Diisobutyl Phthalate (DIBP) .
Date: 18 Jun 2012 .
Unit.
MDL.
001.
%.
%.
%.
0.010
0.003
0.003
ND
ND
ND
Page 5 of 14.
Notes :.
(1) DBP,BBP,DEHP Reference information: Entry 51 of Regulation (EC) No 552/2009 amending Annex
XVII of REACH Regulation (EC) No 1907/2006 (previously restricted under Directive 2005/84/EC):
i) Shall not be used as substances or in mixtures, in concentrations greater than 0,1 % by weight of
the plasticised material, in toys and childcare articles. ii) Toys and childcare articles containing these phthalates in a concentration greater than 0.1 % by
weight of the plasticised material shall not be placed on the market.
Please refer to Regulation (EC) No 552/2009 to get more detail information
DINP, DNOP, DIDP Reference information: Entry 52 of Regulation (EC) No 552/2009 amending
Annex XVII of REACH Regulation (EC) No 1907/2006 (previously restricted under Directive
2005/84/EC). i) Shall not be used as substances or in mixtures, in concentrations greater than 0.1 % by weight of
the plasticised material, in toys and childcare articles which can be placed in the mouth by
children.
ii) Such toys and childcare articles containing these phthalates in a concentration greater than 0.1 %
by weight of the plasticised material shall not be placed on the market.
Please refer to Regulation (EC) No 552/2009 to get more detail information .
Polynuclear Aromatic Hydrocarbons (PAH).
Test Method : . With reference to ZEK 01.2-08 of German ZLS and its amendments, analysis was performed by
GC-MS..
Test Item(s).
Unit.
MDL.
001.
Total 18 PAHs .
mg/kg.
-
ND
Naphthalene(NAP) .
mg/kg.
0.2
ND
Acenaphthylene(ANY) .
mg/kg.
0.2
ND
Acenaphthene(ANA) .
mg/kg.
0.2
ND
Fluorene(FLU) .
mg/kg.
0.2
ND
Phenanthrene(PHE) .
mg/kg.
0.2
ND
Anthracene(ANT) .
mg/kg.
0.2
ND
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Test Report.
No. SHAEC1207176309 A03
Date: 18 Jun 2012 .
Unit.
MDL.
001.
Fluoranthene(FLT) .
mg/kg.
0.2
ND
Pyrene(PYR) .
mg/kg.
0.2
ND
Benzo(a)anthracene(BaA) .
mg/kg.
0.2
ND
Chrysene(CHR) .
mg/kg.
0.2
ND
Benzo(b)fluoranthene(BbF)
Benzo(j)fluoranthene(BjF) .
Benzo(k)fluoranthene(BkF) .
mg/kg.
0.4
ND
mg/kg.
0.2
ND
Benzo(a)pyrene(BaP) .
mg/kg.
0.2
ND
Indeno(1,2,3-c,d)pyrene(IPY) .
mg/kg.
0.2
ND
Dibenzo(a,h)anthracene(DBA) .
mg/kg.
0.2
ND
Benzo(g,h,i)perylene(BPE) .
mg/kg.
0.2
ND
Benzo(e)pyrene(BeP) .
mg/kg.
0.2
ND
Test Item(s).
Tetrabromobisphenol A (TBBP-A).
Test Method : . With reference to US EPA 3550C: 2007, analysis was performed by GC-MS. .
Test Item(s).
Unit.
Tetrabromobisphenol A (TBBP-A) .
mg/kg.
MDL.
001.
10
ND
Hexabromocyclododecane (HBCDD).
Test Method : . With reference to US EPA 3550C: 2007, analysis was performed by GC-MS. .
Unit.
MDL.
001.
mg/kg.
10
ND
Test Item(s).
Hexabromocyclododecane (HBCDD) .
PFOS (Perfluorooctane Sulfonates) and PFOA (Perfluorooctanoic Acid).
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Test Report.
No. SHAEC1207176309 A03
Date: 18 Jun 2012 .
Page 7 of 14.
Test Method : . With reference to US EPA 3550C: 2007, analysis was performed by HPLC-MS. .
Test Item(s).
Perfluorooctane Sulfonates (PFOS) and related
Acid,Metal Salt and Amide .
Perfluorooctanoic Acid (PFOA) .
Limit.
1000.
Unit.
mg/kg.
MDL.
10.
001.
ND.
-
mg/kg.
10.
ND.
Notes :.
Max. limit specified by commission regulation (EU) No. 757/2010 (previously restricted under entry 53 of
Regulation (EC) No 552/2009 amending Annex XVII of REACH Regulation (EC) No 1907/2006) .
0000747644
Test Report.
No. SHAEC1207176309 A03
Date: 18 Jun 2012 .
Page 8 of 14.
ATTACHMENTS
RoHS Testing Flow Chart
1) Name of the person who made testing: Jan Shi/Yoyo Wang/Allen Xiao/Gary Xu
2) Name of the person in charge of testing: Jeff Zhang/George Xu/ Linda Li
3) These samples were dissolved totally by pre-conditioning method according to below flow chart.
(Cr6+ and PBBs/PBDEs test method excluded)
Sample Preparation
Sample Measurement
Pb/Cd/Hg
Acid digestion with
microwave/ hotplate
Sample solvent
extraction
Filtration
Concentration/
Dilution of extraction
solution
Solution
+
Cr6
PBBs/PBDEs
Nonmetallic
material
Adding digestion
reagent
Residue
Positive
Spot test
Negative
Filtration
1) Alkali Fusion /
Dry Ashing
2) Acid to dissolve
Metallic
material
GC/MS
Heating to 90~95℃
for extraction
Filtration and pH
adjustment
DATA
ICP-OES
Adding 1,5diphenylcarbazide
for color
development
DATA
UV-Vis
DATA
0000747644
Boiling water
extraction
Adding 1,5diphenylcarbazide
for color
development
A red color
indicates the
6+
presence of Cr . If
necessary,
confirm with
UV-Vis.
DATA
Test Report.
No. SHAEC1207176309 A03
Date: 18 Jun 2012 .
PFOS/PFOA Testing Flow Chart
1) Name of the person who made testing: Judy Li
2) Name of the person in charge of testing: Linda Li
Sample cutting/preparation
Sample measurement
Solvent extraction
Concentration/Dilution
Filtration
LC-MS
DATA
0000747644
Page 9 of 14.
Test Report.
No. SHAEC1207176309 A03
Date: 18 Jun 2012 .
Phthalates Testing Flow Chart
1) Name of the person who made testing: Elyn Yao
2) Name of the person in charge of testing: Rachel Zhang
Sample cutting/preparation
Sample measurement
Solvent extraction
Concentration/Dilution
Filtration
GC-MS
DATA
0000747644
Page 10 of 14.
Test Report.
No. SHAEC1207176309 A03
Date: 18 Jun 2012 .
HBCDD Testing Flow Chart
1) Name of the person who made testing: Gary Xu
2) Name of the person in charge of testing: Linda Li
Sample cutting/preparation
Sample measurement
Solvent extraction
Concentration/Dilution
Filtration
GC-MS
DATA
0000747644
Page 11 of 14.
Test Report.
No. SHAEC1207176309 A03
Date: 18 Jun 2012 .
PAHs Testing Flow Chart
1) Name of the person who made testing: Lisa Duan
2) Name of the person in charge of testing: Jessie Huang
Sample cutting/preparation
Sample measurement
Solvent extraction
Concentration/Dilution
Filtration
GC-MS
DATA
0000747644
Page 12 of 14.
Test Report.
No. SHAEC1207176309 A03
Date: 18 Jun 2012 .
TBBP-A Testing Flow Chart
1) Name of the person who made testing: Gary Xu
2) Name of the person in charge of testing: Linda Li
Sample cutting/preparation
Sample measurement
Solvent extraction
Derivatization
Liquid-liquid extraction
Concentration/Dilution
Filtration
GC-MS
DATA
0000747644
Page 13 of 14.
Test Report.
No. SHAEC1207176309 A03
Date: 18 Jun 2012 .
Sample photo: .
SHAEC1207176309 A03
SHA12-071763.001 .
SHAEC1207176309 A03
SHA12-071763.002 .
SGS authenticate the photo on original report only .
*** End of Report *** .
0000747644
Page 14 of 14.