MEASURING METHODS OF THERMOELECTRIC COOLERS NONSTATIONARY DYNAMICS IN Z-METERING 1 2 1 L.Yershova , I.Drabkin , V.Volodin , D.Kondratiev τ max = 1 Institute of Physics and High Technologies, Moscow, Russia Institute of Chemical Microelectronics Problems, Moscow, Russia Fax: +7-095-132-5870 1. Introduction Temporal characteristics of a thermoelectric cooler (TEC) are important performance parameters for any device involving TEC. In paper [1]a single thermoelectric pellet non-stationary processes in the so-called regular mode [2] were studied and the obtained formulae were generalized for one-stage TECs loaded by various heat to be pumped. In paper [3] there are derived expressions for the time constant of single-, two- and multi-stage TECs. This paper studies transient processes concerned in Figure-of-Merit measurements with the Z-meter. It compares experimental and theoretical [3] results and yields the evaluating approach for obtaining relaxation time values in real thermoelectric devices. 2. TEC Time Constant Theory Let us define the time constant as the period enough for the temperature difference between the initial and stationary states decreases e-proportionally. In paper [3] corresponding differential equations are solved and maximum time constants for the slowest exponential processes are found. The thermoelectric cooler (TEC) electrical current limit is as follows: j << αL , κ0 (2) where С1 is the heat capacity of cold side junctions, substrate and objects to be cooled; N is the module pellets number, s0 – a pellet cross-section. 2) One-stage TEC, its substrates in free heat exchange with the medium (free TEC): 1 2 LC1 , Lαj 1 + s0κ 0 N κ 0 (1а) where j – the current density, α – the Seebeck coefficient, κ0 – the average n/p pellets thermal conductivity, L – pellets height. Eq. (1) means the TEC current must be much lower than the maximum module current Imax, that is the current at which the TEC yields the highest temperature difference at zero heat load: I << I max , (1b) Designate the slowest expo-process as τmax. There are certain cases when this value is defined. 1) One-stage TEC, its hot side temperature constant and cold side adiabatically isolated: τ max = C1C 2 L , (C1 + C 2 )κ 0 Ns0 (3) where C1, C2, are the heat capacities of all the elements on the cold and hot substrates. Eq. (3) is the maximum time constant at j=0. When j≠0 the time constant is to be found via numerical solution of the corresponding characteristic equation. For the free module case this time is approximately twice lower than for the one with the thermally stabilized hot side, see (2). 3) Two-stage TEC, its hot side temperature constant and cold side adiabatically isolated. For this variant two exponential processes – slow and fast – manifest themselves. Their time constants are: τ max ≈ τ 1 max + τ 2 max , (4а) τ= Here τ 1 max and τ 2 max τ max 1τ max 2 (τ max 1 + τ max 2 ) (4b) are time constants of the one-stage TECs formed by each cascade. Therefore for an n-stage TEC time constant can be expressed as the sum of the each cascade times and all possible combinations like that in (4b): τ max ≈ τ 1 + τ 2 + ... + τ n , (5а) τ ij = τ max iτ max j (τ max i + τ max j ) ∀ i , j (5b) 3. Time Constant Measurement The Device DX3065 allows measuring the parameters of a TEC both in the air and while effective heat rejection from the TEC hot side is carried out, i.e. for the TEC mounted onto some heat sink. The function of the device is double. On the one hand, it enables testing the TEC Figure-of-Merit by the Harman method; on the other hand, it telemetrically tracks the kinetics of the TEC transfer to the stationary state, for it is this state the Harman method can be applied to. So, one device is not only Zmeter but also τ-meter. The accompanying software allows observing the kinetics data by measuring the temporal behaviour of Seebeck voltage Uα(t) and interpolating the data by the exponent: (6) U α (t ) = Ustα (1 − e −t / τ ) , where Ustα - the stationary Seebeck voltage, аnd τ - TEC time constant. Fig. 1. Z-meter exterior For checking if approximating the kinetics by a single exponent is correct additional study in the semi-logarithmic scale is possible: Ustα − U ( t ) , f ( t ) = ln Ustα (7) 4. One-stage TEC: Experiment and Theory Here there are experimental and theoretical [3] data for one-stage TECs both in the free substrates option and with the hot sides thermally stabilized. Denote I for the electric current, τexp, τtheory for the measured and calculated time constants, D for dimensionless root-mean-square declination, normalized to the stationary Seebeck voltage. In the calculations hereafter the following parameters are used: thermoelectric material heat capacity 0.13 J/g, density 7.5 g/сm3, the corresponding ceramics values are 0,8 J/g and 3,5 g/сm3, for the solders – 0,17 J/g and 9,3 g/сm3, the ceramics is 0.5mm thick. Table 1. TECs measured parameters TEC Type Substrate sizes, mm2 s 0, mm2 L, mm N Imax, A Cold Hot 1MT03-004-13 2,0х1,0 2,3х2,3 0,09 1,3 8 0,3 1MC04-032-15 6,4х6,4 6,4х8,0 0,16 1,5 64 0,5 1MC06-030-05 8,2х8,2 8,2х8,2 0,36 0,5 60 3,2 1MC06-060-05 10,0х12,0 12,0х12,0 0,36 0,5 120 3,2 1MC06-018-15 6,0х6,0 6,0х8,0 0,36 1,55 36 1,1 1MC06-024-15 8,0х8,0 8,0х8,0 0,36 1,55 48 1,1 1MT04-059-16 8,0х7,0 8,0х7,0 0,16 1,6 118 0,45 Experiment and theory were taken at two current values 5mА and 25 mА. Table 1 shows that these currents satisfy the requirement (1b). Table 2. Measured and calculated one-stage free-substrated TECs time constants TEC Type I, mА D τtheory, s τexp, s 1MT03-004-13 5 1.92 2.43 0.0018 25 2.87 2.55 0.0007 1MC04-032-15* 5 2.56 3.20 0.0003 25 3.53 3.14 0.0001 1MC06-030-05* 5 0.82 0.75 0.0012 25 0.82 0.71 0.0003 1MC06-060-05 5 0.80 0.68 0.0009 25 0.80 0.65 0.0002 1MC06-018-15* 5 2.56 2.23 0.0007 25 2.57 2.26 0.0002 1MC06-024-15 5 2.56 2.44 0.0005 25 2.95 2.47 0.0002 1MT04-059-16 5 2.91 2.47 0.0002 25 2.91 2.50 0.0001 The sign «*» in Table 2 marks TECs, tested also on the heat sink – see Table 3. Table 3 Measured and calculated time constants of the one-stage TECs mounted on the heat sink TEC Type I, mА D τtheory, s τexp, s 1MC04-032-15* 5 6.59 6.10 0.0057 25 6.43 5.77 0.0098 1MC06-030-05* 5 1.65 1.28 0.0036 25 1.64 1.45 0.0062 1MC06-018-15* 5 4.77 3.96 0.0049 25 4.71 3.96 0.0071 Table 3 proves that calculated time constants are mainly 10 – 20 % higher than the tested ones. This may be explained by the heat exchange with the environment being allowed for not accurately enough. These processes are apt to diminish time constant. It is also seen that time constants for the free module are nearly twice lower than those for the modules on the heat sinks. Typical telemetric data are given in Fig. 2. 0 120 80 Ln(U), Thot=const -1 U in air -2 60 lnU U, mV 100 40 -3 Ln(U) in air -4 U, Thot=const 20 -5 0 0 5 10 t, s 15 20 -6 0 2 4 6 8 10 12 14 t, s Fig. 2. Measured Seebeck voltage values for the TEC 1МС04-032-15 at 25mА The data in the logarithmic scale depend on time linearly. Corresponding time constants found from the linear approximation yield 3s and 5.5s, which is agreeable with the results of Tables 2, 3. It is clear that one-stage TEC kinetics is covered by single characteristic time. 5. Two- and Three-stage TECs: Experiment and Theory The calculations for the multi-stage TECs were only taken at 5 mА and only for the thermally stabilized hot sides. Measurements were carried out at 5 mА both for this very case and for the free modules. The parameters of the tested two-stage TECs are in Table 4. Table 4. The two-stage TECs parameters Substrate sizes, mm2 s0, TEC Type N1 2 l, mm Сold Medium Hot mm 2MC06-10-10 3,2х3,2 4,0х4,0 4,0х4,0 0,36 1,05 6 2MC04-039-15 4,9х4,9 6,5х6,5 6,5х6,5 0,16 1,55 36 N2 14 42 Imax, A 1,3 0,3 Here are the calculations results. Table 5. Calculated time constants of the two-stage TECs mounted on the heat sink TEC Type τ1, s τ2, s τ1+τ2, s τ1τ2/(τ1+τ2), s 2MC06-10-10 5.04 3.53 8.57 2.07 2MC04-039-15 6.83 9.80 16.63 4.02 We see that the temporal relaxation for two-cascade modules reveal a fast and slow components. So a single exponent approximation is only admitted as a sort of estimation. To what extent is it acceptable? In Table 7 the experimental results are given. Table 7. Experimental time constants for the two-stage TEC Mounted Module Free Module TEC Type D D τexp, с τexp, с 2MC06-10-10 3.1 0.0012 5.02 0.0011 2MC04-039-15 9.3 0.0007 12.5 0.0001 Consider time behaviour of 2МС04-039-15. Fig. 3 depicts the Seebeck voltage dynamics for two heat exchange variants. Table 9. Calculated time constants of the three-stage TECs mounted on the heat sink TEC Type τ1, s τ2, s τ3, s τ1+τ2+τ3, s 3MC06-024-13 6.11 5.32 4.73 16.16 3MC07-098-115 9.54 5.32 3.08 17.94 Ln(U), Thot=const -t/12.5 Ln(U) in air 0 5 10 15 20 25 30 35 40 t, s In the three-cascade case except the slow evolution described by the summed time constant there are three faster transitory processes referring to (5b). The averaged experimental data on a single exponent regression are offered in Table 10. Fig. 3. 2МС04-039-15 dynamics for two heat exchange variants It is seen that for the mounted option the logarithm has a linear character. Fig. 4 discovers the same TEC dynamics in the free option. TEC type 3MC06-024-13 3MC07-098-115 lnU air 0,0 -1,0 -t/15-0.34 -2,0 -t/6.8 -3,0 -4,0 0 5 10 15 20 t, s 25 30 35 40 Both TECs are very sensitive to the environmental change on the hot side. The reason may be a high cascading coefficient for both these modules (see the similar case for 2MC06-10-10, Table7). Below there are time behaviour pictures for the TEC 3MC06-024-13. In Fig. 5 one sees the dynamics for two heat exchange variants. Fig. 4. Logarithmic time behaviour for 2МС04-039-15 in the free heat exchange option at 5mA Table 8. Substrate sizes, mm2 Imax, s0, TEC type 2 l, mm N1 N2 N3 A Сold Medium Hot mm 4,0х4,0, 3MC06-024-13 2.5х2.5 6.1х6.1 0.36 1.3 6 14 32 1.05 6.1х6.1 3MC07-09810х10, 8х8 12х12 0.49 1.15 36 42 132 1.45 115 12х12 0,0 7 U in air 6 4 U, Thot=const 3 Ln(U), Thot=const -0,5 5 U, mV Time constants defined in the semi-logarithmic scale are τ =15s и τ=6.8 s, which is quite close to the calculated results of Table 5. The study for the three-stage TECs is simular. The parameters of the threestage TECs and the theory results can be found in Tables 8 and 9. Table 10. Measured results for the three-stage TECs Free Module Mounted Module D D τexp, s τexp, s 5.9 0.0009 11.2 0.0005 4.1 0.0006 8.7 0.0003 lnU lnU 0,0 -0,5 -1,0 -1,5 -2,0 -2,5 -3,0 -3,5 -4,0 -1,0 -1,5 Ln(U) in air 2 -2,0 1 0 -2,5 0 10 20 30 t, s 40 50 60 0 4 8 t, s 12 16 Fig. 5. Measured Seebeck voltage dynamics for the TEC 3МС06-024-13 at 5 mА The logic found out on the two-stage option remains fair. It is illustrated by Fig. 6. 0,0 -0,5 -0,2 -0,4 lnU air -1,0 -t/10.7-0.5 -1,5 -2,0 -t/3.8 -2,5 -t/7.7-0.5 -3,0 0 2 4 6 8 10 12 14 16 t, s lnU Thot=const 0,0 -0,6 -0,8 -t/11.2-0.02 -1,0 -1,2 -1,4 -1,6 0 2 4 6 8 10 12 14 16 t, s Fig. 6. Logarithmic time behaviour for 3МС06-024-13 for the free heat exchange and mounted options at 5mA. Fig. 5 convinces one of the fast component presence in the free module testing. This can be captured by the kink of the curve in the semi-logarithmic scale. The three-cascade case reveals at least three linear curve parts corresponding to different time constants. Comparison of the theory and experiment shows that the tested values are some 30 % lower than the calculated ones, which is no wonder if taking into account the one-stage preceding disagreement. Conclusion With the help of the Z-meter DX3065 it is possible to study the process of TECs transfer to the stationary state both in the free heat exchange option (standard Z-meter configuration) and in real performance conditions for modules mounted on the headers, heat sinks, in devices, etc. Comparison of the theory and experiment shows that the tested values are 10 – 30 % lower than the theoretically predicted figures. However the theory correctly catches the basic relaxation characteristics of TECs as dependent on their real operational-environmental conditions. Time constants evaluated by Z-meter allow more accurately describing non-stationary kinetics in real thermoelectric devices. 1. E.I.Astakhova, V.P.Babin, U.I.Ravich. Calculation and Measurement of the Cooling Thermoelement in the Regular Mode. Eng.Phys.J., 62, 1992, 284. 2. G.M. Kondratiev. Regular Thermal Mode. Moscow, GITTL, 1954, 408. 3. I.A. Drabkin. Transient Processes in Thermoelectric Cooling Modules and Devices. (Ibid)