ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: Nano (Silver or Gold plated) Product #: 456xxx Series Issue Date: November 27, 2012 It is hereby certified by Littelfuse, Inc. that there is neither RoHS (EU Directive 2002/95/EC, and its recast 2011/ 65/EU)-restricted substance nor such use, for materials to be used for unit parts, for packing/packaging materials, and for additives and the like in the manufacturing processes. In addition, it is hereby reported to you that the parts and sub-materials, the materials to be used for unit parts, the packing/packaging materials, and the additives and the like in the manufacturing processes, are all composed of the following components. Issued by: <Global EHS Engineer> (1) Parts, sub-materials and unit parts This document covers the Nano RoHS-Compliant series products manufactured by Littelfuse, Inc. ＜ Raw Materials Used Please see Table 1 (2) The ICP data on all measurable substances Please see appropriate pages as identifed in Table 1 Remarks： Pb (lead) contained in the high temperature melting solder > 85% and is categorized as exempt under section 7a of the RoHS Annex. Form 585-047 Rev. A 1 2/21/06 Table 1: List of Raw Materials covered by this report Total Parts 1 2 3 4 5 6 7 8 Raw Material Part Number 909-422 910-259 (same as 910-238) 910-554 (same as 910-275) 087266 11-0010 (687xxx) 079xxx 692323 425809 Raw Material Description Body Cap – Silver plated Cap – Gold plated Anaerobic Adhesive Element-Pure Ag1000 Element Solder Ink 2 Page(s) 3-10 11-18 19-24 25-34 35-41 42-46 47-52 53-61 Test Report Applicant: Number : TWNC00285767 Littelfuse Philippines Inc. LIMA Technology Center, Lipa City, Malvar, Batangas Date : Nov 19, 2012 Sample Description: One (1) group of submitted samples said to be : Part Description : Body Part Number : 909-422 Date Sample Received : Nov 12, 2012 Date Test Started : Nov 13, 2012 Test Conducted : As requested by the applicant, for details please refer to attached pages. Authorized By: On Behalf Of Intertek Testing Services Taiwan Limited K. Y. Liang Director *THJ0285767* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410 Page 1 of 8 Number : TWNC00285767 Test Conducted (Ⅰ) Test Result Summary : Result (ppm) White Plastic Test Item Heavy Metal Cadmium (Cd) content Lead (Pb) content Mercury (Hg) content Chromium VI (Cr6+) content Polybrominated Biphenyls (PBBs) Monobrominated Biphenyls (MonoBB) Dibrominated Biphenyls (DiBB) Tribrominated Biphenyls (TriBB) Tetrabrominated Biphenyls (TetraBB) Pentabrominated Biphenyls (PentaBB) Hexabrominated Biphenyls (HexaBB) Heptabrominated Biphenyls (HeptaBB) Octabrominated Biphenyls (OctaBB) Nonabrominated Biphenyls (NonaBB) Decabrominated Biphenyl (DecaBB) Polybrominated Diphenyl Ethers (PBDEs) Monobrominated Diphenyl Ethers (MonoBDE) Dibrominated Diphenyl Ethers (DiBDE) Tribrominated Diphenyl Ethers (TriBDE) Tetrabrominated Diphenyl Ethers (TetraBDE) Pentabrominated Diphenyl Ethers (PentaBDE) Hexabrominated Diphenyl Ethers (HexaBDE) Heptabrominated Diphenyl Ethers (HeptaBDE) Octabrominated Diphenyl Ethers (OctaBDE) Nonabrominated Diphenyl Ethers (NonaBDE) Decabrominated Diphenyl Ether (DecaBDE) ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND *THJ0285767* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410 Page 2 of 8 Number : TWNC00285767 Test Conducted (Ⅰ) Test Result Summary : Result (ppm) White Plastic Test Item Halogen Content Fluorine (F) Chlorine (Cl) Bromine (Br) Iodine (I) ND ND ND ND Remarks: ppm = Parts per million based on weight of tested sample = mg/kg ND = Not detected Responsibility of Chemist : Irene Chiou / Kevin Liu / Cathy Chen Date Sample Received Test Period : Nov 12, 2012 : Nov 13, 2012 To Nov 15, 2012 (Ⅱ) RoHS Limits: Restricted Substances Cadmium (Cd) Content Lead (Pb) Content Mercury (Hg) Content Chromium VI (Cr6+) Content Polybrominated Biphenyls (PBBs) Polybrominated Diphenyl Ehters (PBDEs) Limits 0.01% (100ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) The above limits were quoted from Annex II of 2011/65/EU for homogeneous material. *THJ0285767* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410 Page 3 of 8 Number : TWNC00285767 Test Conducted (Ⅲ) Test Method: Test Item Cadmium (Cd) content Lead (Pb) content Mercury (Hg) content Chromium VI (Cr6+) content Polybrominated Biphenyls (PBBs) Polybrominated Diphenyl Ethers (PBDEs) Halogen Content Test Method With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in clause 7, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in annex C, by alkaline digestion and determined by UV-Vis spectrophotometer. With reference to IEC 62321 edition 1.0:2008 in annex A, by solvent extraction and determined by GC-MS and further HPLC-DAD confirmation when necessary. With reference to IEC 62321 edition 1.0:2008 in annex A, by solvent extraction and determined by GC-MS and further HPLC-DAD confirmation when necessary. With reference to EN 14582:2007 by calorimetric bomb with oxygen and determined by Ion Chromatograph. Reporting Limit 2 ppm 2 ppm 2 ppm 1 ppm 5 ppm 5 ppm 50 ppm Remark: Reporting limit = Quantitation limit of analyte in sample *THJ0285767* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410 Page 4 of 8 Number : TWNC00285767 Test Conducted (Ⅳ) Measurement Flowchart: Test for Cd/Pb/Hg/Chromium (VI)/PBBS/PBDES Contents Reference Standard: IEC 62321 edition 1.0:2008 Sample preparation For non-metal part For metal part Take sample and immerse into Aqua Regia, start to strip plating layer Stop the stripping procedure upon color change completely Take the Aqua solution as plating component and stripped body as substrate component PBBs/PBDEs Weigh sample and add organic solvent By Soxhlet extraction or Solvent extraction Concentrate the extract and make up with organic solvent Analyzed by GC-MSD Cr 6+ Substrate Cd/Pb/Hg Weigh sample and add alkaline solution For different material, digest the sample with *1 appropriate acid Plating Cr 6+ By spot test Definite temp. extraction Cool and filter the extract Confirm the tested samples are totally dissolved Negative *2 Get 50cm2 sample Make up with deionized water By boiling water extraction Analyzed by ICP-OES Make up with deionized water and add diphenyl-carbazide solution Analyzed by UV-VIS *THJ0285767* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410 Page 5 of 8 Number : TWNC00285767 Test Conducted (Ⅳ) Measurement Flowchart: Remarks: *1: List of Appropriate Acid： Material Polymers Metals Electronics Acid Added for Digestion HNO3,HCl,HF,H2O2,H3BO3 HNO3,HCl,HF HNO3,HCl,H2O2,HBF4 *2: If the result of spot test is positive, Chromium VI would be determined as detected. *THJ0285767* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410 Page 6 of 8 Number : TWNC00285767 Test Conducted (Ⅳ) Measurement Flowchart: Test for Halogen Content Reference Standard：EN 14582 Sampling/grinding or cutting Add absorbent in a combustion flask & place weighed sample in equipment Fill oxygen into calorimetric bomb Ignite then leave the bomb at room temperature Transfer the absorbent into a volumetric flask Make up with deionized water Analyzed by ion chromatography End of Report This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a recommendation for any particular course of action. Intertek does not accept a duty of care or any other responsibility to any person other than the Client in respect of this report and only accepts liability to the Client insofar as is expressly contained in the terms and conditions governing Intertek's provision of services to you. Intertek makes no warranties or representations either express or implied with respect to this report save as provided for in those terms and conditions. We have aimed to conduct the Review on a diligent and careful basis and we do not accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by statute or otherwise, except in the event of our gross negligence or wilful misconduct. *THJ0285767* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410 Page 7 of 8 Number : TWNC00285767 Test Conducted Photo *THJ0285767* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410 Page 8 of 8 scs Test Report No.:LB12-01094C March5, 2012 Page1 of 4 LTTTELFUSE PHtLS.,tNC. LimaTech Center,SEZ, Lipa,Malvar,Batangas The followingsample(s)was/veere submittedand identifiedbylonbehaltol the clientas: ProductName Cap 910-259/ Base SGSSamplgNumber LB12-01094.004 RecelvedDate FebrJary21,2012 Test PerlormingDate F€bruary 21,20121o March5,2012 T6sl Perlormed SGS Philippines subcontracted the testingot sampte(s) setecl€dby applicantwithfollowingresults Test Requested Selectedtest(s)as requested by client. Test llethod Pleaserelerto nextpage(s). Ted n6sult(5) Pleaserefer1onextpage(s). C,oncluslon Basedon the perfomedtestson submittedsample(s), the resultsof Lead,Cadmium,Hexavalent chromiumand l\,,lercury complywith lhe RoHSDnective2002/95/EC and iis subsequeniamendments. This reportwillbekepl on filefor six monthsfromthe dateol issue. Signedfor and on behaltol INC. SGSPHILIPPINES, I'EDEN L. PENEYHA LaboraloryOperalions Manager ''Thl! docum i. r*ru.d by th. co o.ny rbt.cr ro r|3 6s.6r cddirro. ot s.rur6 pndod oqlEl, fl.ihbb oh 6qu6d 4 ac6*lbl. .l jAttolr@!-d!gtE$&!b q, Alidtllon b dren lo lh.limil.lion ol lirbihy, hd.nnit€rion and iurl.dtclld ls.u6.Ll|md lh€Eh. Any hordoror lhrs [email protected] b advr$d lh.l [email protected] hrs r.rr€.1. lh. comps9. llndino! .r rh. rim ol n5 inr6m 16 on,y .nd $$rn rh. llnrt ol clr.nr'3 lmrMrron., r, dy. Ih. comFny s $1. repoFiblllry i! ro irs clk anrl $is rlocun.d do. nor .rcnr.l. p.nb. ro . lnn$crbn r6m 4rcrdhg .rr rrsrf rrgrtu .nd obrrg.t nt!. This d*[email protected] ..nnor b. Eproduc€d .EDt In turr,Tlnoul prrd rrnl.n .D9.mr ot rh. conp.ny, any unrurhdi2.d ,ledrid, l6rgeryor r.w. o$.frr$ !r.r€d rh. 63ulr. llwn l. rhle rhb ddmnr l. unl.wlul .nd ofi.nd.6 n.v b. .Mur.d ro rh. tull.3r 6rem or !i. unre.t b31 Ep..r dr onryro rho3flpr.(3) l.!r.d *d ech *mpl€l.) .E Br.in.d td 50rlrys dly-- SGS Test Report No.:LB12'01094C Page2 ol4 March5.2012 : LB11-01094.004 SampleNumber metal of silvercolored PhyslcalDas€ription : Basematerial Item/ BatchNumb€r : fl/A RoHSDlreclive2002/95/EC Tesl ltem(s) unit (Cd) Cadmium mg/Kg Lead(Pb) MEKg (Hg) Mercury mg/Kg C(Vl) Hexavalent Chromium Itothod IEC62321:2008application of modifieddigestionby surlaceetchingand perfomedby ICP-AES. withreference to lEc 62321: 2008andperfomedby Boiling waterextraction Method.# iIDL n6sult 2 2 ND '|19 2 ND Negative Nole : 1 mg/kg= ppm ; 0.1wt%= lOOOppm 2. ND = Not Detected 3. MDL = lllethodDet€ctionLimit 4. " = Oualitative analysis(NoUnit) 5. # = a. Posilivemeansthe presenceol CrVlon the testedareas b. Negativemeansthe.absenceof CrVlon the testedareas solulionis equalorgrealerthan0 02 mg/kg in boiling-water'extraction The detecGdconcentration with 50 cm2lesleda€as. 6. Analyseswere subcontractedto SGS Taiwan,Ltd 'c.sibl6 '1 l. L.$.d by lh. c.np.ny.uq.cr b ib G.w.r condhiont or s{vid F.hl€rr oErlal' daiLbl' M '€qFr oro6'unstt "Thr. dddd tl lor.l€.lbnic lom.l dodmnl.! .ubier io rmr and cddllle! tor Elecrrdnic rd ;dmdhim;nd, |w.;iffi .ddmtt.hll.ntbn i3 dlM io ih. lidrd|6 d li.birilir, lnd.mnilicarbh tnd jrtudlctlon blA rt'lln€d rhs"n' ffi;ffi. t. stv6d thd intoma on 6nl.tned heM r.lt.cl' rh. comtfy . rhdinss n $. n. ol 1l! Int Mxro onry G;Etdor ot thti d*um i"iii'njlrL.ii.Ir"iiciii'ii:i"ai""rroninmv.r*conprny'sotggpon.|bi|ityB6n.c|Btand r-. .I i,r ririhrs.id obirs.rld. undr ih6rdn.icn4 deumhrs. rhF [email protected]'odu... ni,rrii r, i, i.*.ir"; d!Do"6n€or ".Et.hg *imi rpdd.rd rh.-conp.nv.Art unlthorrrd.ri.6rr6, tor!€tvor r'l.nE onorrl.@nl. ii"iii r" r"ri *l|i,ip'rnav b. Drc*xur.droih.lurlod ert.''t ol rhortw utir$' orh'nrs 3r'tedrh' E Uh"hdn h rhis ir'ii[""*i,i r. "nd'i.6 "nrlirut"o i.d.d andsicn *mpl43) ae ra.lmd lot 60day3dlv " to thr *nde{.) iict dn dor ory sGs TestReport No.:LB12-01094C March 5,2012 Page 3 of 4 ATALYSISFLOWCHARTOFHEAVYMETALS Pb, cd, Hg Negalive A d d i n q1 , 5 lor diph€nylcalbazide Adding1.5the prssenceo, Cl6+. "[email protected]'sbi€dtoit.G*n|cohdtr|dro|s.d'cepdnbd.y.l|.a|''.||.b|.onftqed4*e.llb|..| 'r bm.mo $d. ior a.dbdc ;;"i oiiii'i"G nrr; i" r"-" "nd cdin'om ror Ererbnic D*!-mnt' ;lXi:,tr:tr;:;#T##ir;;.]';r;i#K-:|'"dd"'r;:iqiirFi:l-a.,b"F-1'i^ljll:i:d-:i"11':,::,.11t'1*Ll'""i *"".'"-"-'*ffiJi #gtffi+ffi1ffffi1Y,i#il.;',r;&!.-i4iq,ss-4i"idl**lS:1r..,*.,';':"':ll*'S'*iJJtrf,llifll; orv ii" cip-v" ma"ril $' tmeorn' inte*nrron ; iiriial ;r; ;'po*ibi rv E t6 iddffr 'hi'r tni! do@mnrda' nororod e cr".rt r"a*rr."' ,r -v. rr'. c"."iiis -- -;-.J"ii"rh"a-o *-'" - ""iiin;;U;;;;;r;;;-rcbnsdrhdrndhE.idobitJq+tq:4":1i::*:l*o-*:J;jy;;:':""T1tr*"1"#i:::*":T or ar"at'"' r"'s"'v torirrc'ton orrrF6nud d 'r?6'Ene ' h!.nv i@or In lulr, withdr pdd wlbn rP?rd.l ol lhe"-" m 4 u"i"*"t a*o& dn'd tt'' Bur! 3hnn rnrhi3 ."vjna - p,.-*,'" iiir'i r'iiin rhEd@umnrE unr*rur ancd"o. "'t"4.'t rs 60d+ onrv" *' r'rai^'d iqJirixrca :i,ctrmmpr.{st iij5;;;ift;.;ii;ih;; Anv bldd ol lhh docurenl i..c i"j i-r,;nilr'r'"iiirJii SGS Test Report No.:LB12-010S4C March5, 2012 Page4 of 4 SamplePhoto (As Becaived): LB12-01094.004 , -l , .; ol Report... ...End ftiijffili.l-ifi,r$','fi'l ffi ffi********#*'ni'fr ,"r"r"g"'""''.'o""*""iGi6ii,"a.'i*mda..a.--o c t -u"it'" p,r* *,'n"..pFi"-r orrr* co'p'nv G'" Jnrut*i:ao rtte'ntonro's*v fiJi'- rli iri,;i;;i ott''fri* 't'r€d th' E3urtrshdn r' rhr' iiiriili iir-"i'r'"ini i* - p-*'*"iJi# one."".."v i: unr.wrur.nd ,hF d.cumnr " d'va dry iili *ri' -rv r. rn" *.ptel') b3r.d .hd .uch*mpq.' * t'r'i*d rot60 "ii,-'i SG Test Heport No.:1812-01094A March5, 2012 Page1 ot 4 INC. LITTELFUSEPHII..S., LimaTech Center,SEz, Lipa,Malvar,Batangas bylonbehalfof theclientas: andidentilied The followingsample(s)was/were submitled ProductName Cap910'259/ Plaling SGSSampleNumbel L812,01094.002 RecelvedDate Fehtuary21, 2012 Test PerformingDate 21, 2012to lllarch5, 2012 February T€st Perfurmed by selected lheteslingol sample(s) subconlracted SGSPhilippines results wilhfollowing applicant Te€t Requested byclient. teg(s)asrequested Selecled Test Method Pleaserelerto nextPage(s) Tqrt R.eult(s) Pleaserefer10nextpage(s). conclugion theresultsof sample(s)' testsonsubmitted Basedontheperlormed complywlth andl\rercury Hexavalent chromium Lead,Cadmium, amendments anditssubsequent 2oo2l95/Eo theRoHSDkective This repodwill be kept on filelor six monthsfromthe dale of issue' Signedlor and on behalfol INC. SGSPHILIPPINES, i,EDEN L. PENEYRA LaboratoryOperationsManager 'ffi 'ffi W**********;ff "lt#ffi rhr! docu@nrdnnot b' dPrcdued ao-'dr' .'lro. ro . ln@ctron i,omerc.r,'"g ar $"n .gn'" .- o"lis.iioniijiai'iit"i'*iarn oi rh' @nr' or'ppe Bnroi I'r'rrurion r'!sv d 'rb'r'n -uni*" A'-v un.uthd'ed p"$.b.6Fnv. *r*n.pp;o,.ror lillii,iiririiir,iii,r ott'ryr!' sraGrrrh' E urBlhdn Inrhi! ii- i"l,iir r. -o onein* .o te o.*,neo 6in" tuttertinor a m l* "^r.h"r io tt -.pre{.l blt.d and3irch'.mpre{t .ro Etain'dro' 60dtveonrv ili .-,ia i"t"i .itv " sGs TestReport No.:1812-01094A PaOe2 ol 4 Llarch5, 2012 : LB11-01094.002 SampleNumber PhygicalDescriplion : Platinglayerot siMercolored metal Itom/ BalchNumbor RoHS Dlrectlve 2002/95/EC Test ltem(s) (tu) Cadmium Lead(Pb) (Hg) Mercury Unlt Method MDL Rg€ult mgKg m9Kg mg/kg IEC62321:2006application ol modifieddigestionby surfaceetchingand performedby ICP-AES. 2 2 ND 18 NO HexavalentChromiumC(Vl) wilh reference to lEc 62321: 2008andperformedby Boiling waterextraction Method.# Negalive Nole : 1 . mdks=ppm; 0.1M%=1000ppm 2. ND= NotDetected Limit 3. MDL= MethodDetection (NoUnit) analysis 4. " = Qualitative meansthepresence ot CrVlonthetestedareas 5. # = a. Positive b. Negativemoansthe absenceof CrVlonlhe testedareas is equalorgreaterthan 0.02mg/kg Thedetected concentration in boiling-waterexlraction solulion with50 cm,testedarcas. to SGSTaiwan,Ltd 6. Analys€sweresubcontracled "Th|.do.uEnt'.isU.dbylh6conp..|y{bt.dto|l.Gffi|c.nditi43.|sa|rn.hHdn6'' .nd .;dhbnr.nin sbFcl lo T.ds and coildl m tor EloclDnlc Docutrsllt .r swr.-Mn.d. .nd, tor .l.crDni. lod.l doon.n€t d.fimd rh'orn. An.dbn rs dwn ro rE hhn rq or rr.bnhyi Ind.nn'r'cdris $d lo,r.drctron r.!s d=ffiffiEelmdrnn. lindinc. .t ft. rlm. oi it inrorF.rlm onlv |! .dvi!.d rh.r i dnrnbn conl.h.d h.Ed re{ 13 rh€ compdf! Atrv h.ld.rcr rr'r. ddmnr d.cumln d4. nol .&.e.r. ..1. E$ondbiritv i. ro lB dldl and lhii Instdcll@ il anv. Th. c.nptrv. $; thl. rh. linir. ol cll.d. [email protected].. Thlt d@umnl @hnol b. Eptodu.€d tdn osrcl.lno .ll $.k noms .nd ouigrlion. unrL. th. lrn{ctd r.nb. ro . t aEdm or rlt 6lion. rolg v d l.llni@uon or rh. 6tunr d .r0€.6n6 aslr h tul. wirhod Fir fhbn .DDroEl ol lh€ comlt'ry. any u..ulhdP.d lr.red rh. E.ulr! lhoan In rhr' or rh. rtu. unr6's orh.fris ro I'. tur6d.rrdr rhi. ircumi Leonk*rur .nd onqiJ€.. na h. lE;urod r.3r dpon rd.f onry io rh. umpl4.) l6red lnd 3uch smpk{!) aE eitin.d L. 50 d.vr dlv " SGS Test Report No.:LB12-01094A Page3 of 4 March5,2012 OF HEAVYMETALS ANALYSISFLOWCHART l,leasursmenl Sample Pb, cd, Hg Posilive Negative Heating ro90-95'C TotatDigestion A d d i n g1 , 5 - ol Cr6+. thepresence -rhrsdocuNmr. r$u.d byrn coi'e.ny{q.d16|ts6d.6rcmdnid.ds.niepn.d.w!"1:g*'^"ll,:ljf_*,L#llil -.ff;".?Hi;;i.;;;ilifr.i:iG.ffi1','iril-rl{;ro*-"1.;-?,tr"L':y1:.i*:n"l'i*",,lt,.lm,Lmg[,i: i1* -' -- - -"-* r'or*. as*-y or ffir,or*. f i"1o"u1-, "01*ifiir..iit ---;;' pgifi31:*a?.i1"-?TJ?l'i;g:T"'"" th'' d@un'nr do nor ;sEibinry B d idc|dt and,1;1":l1;":L'f.ff#i*:1"',:g "on'Er' ;; h.lMlion* ..ni n d wwirhin i l h i n luF l F hlrdr. d a o l .t c | |clLr{. .t{'.h.lM l i o n * f D y ' |rnDv . @ mrh. p o ncom yl oblgn ,rsnu_" -ircxi-i E|3ha dn rm, $dr trghl!.nd rcr"r"o in"t*joo" ae"*,r.rt! ".0., :rr*'rron' t".s.'v * t"rn"*I;i .i*rr-. "r; or .d.r .t i;'#;;":; rh rh€comr..v. Anvun.urhonad !F ri-rn ut'"i,i pa-Drd.r r" u mt'u "ltun iiirii inr."r .i.n! or $e r*.-unre$ or'*i* iiJr md ie ilei"iJiiiil hi;ru|rnr .nd otidlr.E rhl. d@umnr bi. ddfl |lnlstul .nd lLiii !i-a i$ ;;;;ii.i;i;iift;;iii,:r-ii.r.al"r .i,.t *.pcr'r *. Erah'dt" 60d'v"onrv !aTAt?lT:f-:fj:,:: orrh' @'r'nr o.pp'dfr' ol 3r'rcd$' t'sh' shdn in rhr' SGS Test Report No.:LB12-01094A March5,2012 Pege 4 ol 4 SamolePhoto (As Receiv€dl: LB12-01094.002 , ..1 ...Endof Report... _Thi.documnrl.Lltu.dbyrh.conrF.yebl.cltoir'c6.6lcddrtro:ols.Blc.pnni.dderl..J,{.ll.br.onrqdd'*dbl€al .r ih ;nd. ror €t.cr'o.ic remt [email protected]. sbFd to rons ond c6ndn'oN ror Er4'6hrc DaltrFr. .nd d;di'dn swsaod.m' ffifi.-..de,mdltl'DAl.d|oh|ldRsnbrhe[frildIdo|||.bi|ity'indefrn|l|c.llon.ndjUrisd onry rn, h-adc-;Alh-b d-;umnr te.dvl*d |hlr intorndion cont.ln.d h.6on rd|4rs tho comp.nv's thdh$ .l lh. fine oi llt ld.mnlion tot. @tohslhllllv i5 lo ilr cllenr .nd rhb dod@nr d63 nol 'roMale il dy. The c.mp-v. d; firhh $e rrmh. ol clionfs lEtruc{d3, rbm.eE,.in0 . lhsir ndhl..nd obislt'bn3 uid€r irF tEn*iclio. docum-l3, Thi3 documnr o.nor b. EpEdued @nr6 ro a r,rEctid or or rh6 6@nr or .pp..Bne ot th. comp€ny. ary un.urh4rz€d .lt r.rion, lorgdy q l.l.iicari.n ;ed h tu[. withdt sior wnM .!!bEt irri i*,*ii r' -a oll.iricr nd borrca;u|ad b $. tulr.lr .nFi orrh€l$. unr€.sorhwis. .rded $' E!uh' 'hdn r' rhis ";r"fu"r rothespl6(!) I6redlnd 3uche.mpL{s).E Et h6dtd 60d.y3onlv." ro.r EpodELr only Test Report Applicant: Number : TWNC00285774 Littelfuse Philippines Inc. LIMA Technology Center, Lipa City, Malvar, Batangas Date : Nov 19, 2012 Sample Description: One (1) group of submitted samples said to be : Part Description : Cap Part Number : 910-275 / 910-554 Date Sample Received : Nov 12, 2012 Date Test Started : Nov 13, 2012 Test Conducted : As requested by the applicant, for details please refer to attached pages. Authorized By: On Behalf Of Intertek Testing Services Taiwan Limited K. Y. Liang Director *THJ0285774* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410 Page 1 of 6 Number : TWNC00285774 Test Conducted (Ⅰ) Test Result Summary : Result (ppm) (1) (2) Test Item Heavy Metal Cadmium (Cd) content Lead (Pb) content Mercury (Hg) content Chromium VI (Cr6+) content (mg/kg with 50cm2) ND ND ND Negative (< 0.02) (#) ND ND ND Negative (< 0.02) (#) Remarks: ppm = Parts per million based on weight of tested sample = mg/kg ND = Not detected < = Less than mg/kg with 50cm2 = milligram per kilogram with 50 square centimetre Negative = A negative test result indicated positive observation was not found at the time of Test. # = Due to the insufficient sample area, reduced total sample surface of 25 cm2 was used and the dilution factor was adjusted accordingly. Tested Components (1) Coppery metal base material (2) Golden plating layer Responsibility of Chemist : Irene Chiou / Kevin Liu Date Sample Received Test Period : Nov 12, 2012 : Nov 13, 2012 to Nov 16, 2012 (Ⅱ) RoHS Limits: Restricted Substances Cadmium (Cd) Content Lead (Pb) Content Mercury (Hg) Content Chromium VI (Cr6+) Content Limits 0.01% (100ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) The above limits were quoted from Annex II of 2011/65/EU for homogeneous material. *THJ0285774* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410 Page 2 of 6 Number : TWNC00285774 Test Conducted (Ⅲ) Test Method: Test Item Cadmium (Cd) content Lead (Pb) content Mercury (Hg) content Chromium VI (Cr6+) content Test Method With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in clause 7, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in annex B, by boiling water extraction and determined by UV-Vis Spectrophotometer. Reporting Limit 2 ppm 2 ppm 2 ppm 0.02 mg/kg with 50cm2 Remark: Reporting limit = Quantitation limit of analyte in sample *THJ0285774* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410 Page 3 of 6 Number : TWNC00285774 Test Conducted (Ⅳ) Measurement Flowchart: Test For Cd/Pb/Hg/Chromium (VI) Reference Standard：IEC 62321 edition 1.0:2008 Sample preparation Take sample and immerse into Aqua Regia, start to strip plating layer Stop the stripping procedure upon color change completely Take the Aqua solution as plating component and stripped body as substrate component Cd/Pb/Hg Substrate For different material, digest the sample with *1 appropriate acid Cr 6+ By spot test Confirm the tested samples are totally dissolved Make up with deionized water Plating Negative *2 Get 50cm2 sample By boiling water extraction Analyzed by ICP-OES Make up with deionized water and add diphenyl-carbazide solution Analyzed by UV-VIS *THJ0285774* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410 Page 4 of 6 Number : TWNC00285774 Test Conducted Remarks: *1: List Of Appropriate Acid： Material Polymers Metals Electronics Acid Added For Digestion HNO3,HCl,HF,H2O2,H3BO3 HNO3,HCl,HF HNO3,HCl,H2O2,HBF4 *2: If the result of spot test is positive, Chromium VI would be determined as detected. End of Report This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a recommendation for any particular course of action. Intertek does not accept a duty of care or any other responsibility to any person other than the Client in respect of this report and only accepts liability to the Client insofar as is expressly contained in the terms and conditions governing Intertek's provision of services to you. Intertek makes no warranties or representations either express or implied with respect to this report save as provided for in those terms and conditions. We have aimed to conduct the Review on a diligent and careful basis and we do not accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by statute or otherwise, except in the event of our gross negligence or wilful misconduct. *THJ0285774* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410 Page 5 of 6 Number : TWNC00285774 Test Conducted Photo *THJ0285774* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410 Page 6 of 6 Test Report Applicant: Number : TWNC00285781 Littelfuse Philippines Inc. LIMA Technology Center, Lipa City, Malvar, Batangas Date : Nov 19, 2012 Sample Description: One (1) group of submitted samples said to be : Part Description : Anaerobic Adhesive Part Number : 087266 Date Sample Received : Nov 12, 2012 Date Test Started : Nov 13, 2012 Test Conducted : As requested by the applicant, for details please refer to attached pages. Authorized By: On Behalf Of Intertek Testing Services Taiwan Limited K. Y. Liang Director *THJ0285781* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410 Page 1 of 10 Number : TWNC00285781 Test Conducted (Ⅰ) Test Result Summary : Result (ppm) Green Liquid Test Item Heavy Metal Cadmium (Cd) content Lead (Pb) content Mercury (Hg) content Chromium VI (Cr6+) content Polybrominated Biphenyls (PBBs) Monobrominated Biphenyls (MonoBB) Dibrominated Biphenyls (DiBB) Tribrominated Biphenyls (TriBB) Tetrabrominated Biphenyls (TetraBB) Pentabrominated Biphenyls (PentaBB) Hexabrominated Biphenyls (HexaBB) Heptabrominated Biphenyls (HeptaBB) Octabrominated Biphenyls (OctaBB) Nonabrominated Biphenyls (NonaBB) Decabrominated Biphenyl (DecaBB) Polybrominated Diphenyl Ethers (PBDEs) Monobrominated Diphenyl Ethers (MonoBDE) Dibrominated Diphenyl Ethers (DiBDE) Tribrominated Diphenyl Ethers (TriBDE) Tetrabrominated Diphenyl Ethers (TetraBDE) Pentabrominated Diphenyl Ethers (PentaBDE) Hexabrominated Diphenyl Ethers (HexaBDE) Heptabrominated Diphenyl Ethers (HeptaBDE) Octabrominated Diphenyl Ethers (OctaBDE) Nonabrominated Diphenyl Ethers (NonaBDE) Decabrominated Diphenyl Ether (DecaBDE) ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND *THJ0285781* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410 Page 2 of 10 Number : TWNC00285781 Test Conducted (Ⅰ) Test Result Summary : Result (ppm) Green Liquid Test Item Halogen Content Fluorine (F) Chlorine (Cl) Bromine (Br) Iodine (I) Phthalates Di(2-ethylhexyl) Phthalate (DEHP) Dibutyl Phthalate (DBP) Benzyl Butyl Phthalate (BBP) Others Hexabromocyclododecane (HBCDD) ND ND ND ND ND 77 ND ND Remarks: ppm = Parts per million based on wet weight of tested sample = mg/kg ND = Not detected Responsibility of Chemist : Irene Chiou / Kevin Liu / Cathy Chen Date Sample Received Test Period : Nov 12, 2012 : Nov 13, 2012 To Nov 15, 2012 (Ⅱ) RoHS Limits: Restricted Substances Cadmium (Cd) Content Lead (Pb) Content Mercury (Hg) Content Chromium VI (Cr6+) Content Polybrominated Biphenyls (PBBs) Polybrominated Diphenyl Ehters (PBDEs) Limits 0.01% (100ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) The above limits were quoted from Annex II of 2011/65/EU for homogeneous material. *THJ0285781* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410 Page 3 of 10 Number : TWNC00285781 Test Conducted (Ⅲ) Test Method: Test Item Reporting Limit Test Method With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the Cadmium (Cd) content 2 ppm tested samples are totally dissolved and determined by ICPOES. With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the Lead (Pb) content 2 ppm tested samples are totally dissolved and determined by ICPOES. With reference to IEC 62321 edition 1.0:2008 in clause 7, by microwave Mercury (Hg) content digestion until the tested samples 2 ppm are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition Chromium VI (Cr6+) 1.0:2008 in annex C, by alkaline 1 ppm digestion and determined by UV-Vis content spectrophotometer. With reference to IEC 62321 edition 1.0:2008 in annex A, by solvent Polybrominated extraction and determined by GC-MS 5 ppm Biphenyls (PBBs) and further HPLC-DAD confirmation when necessary. With reference to IEC 62321 edition 1.0:2008 in annex A, by solvent Polybrominated Diphenyl Ethers extraction and determined by GC-MS 5 ppm (PBDEs) and further HPLC-DAD confirmation when necessary. With reference to EN 14582:2007 by 50 ppm Halogen Content calorimetric bomb with oxygen and determined by Ion Chromatograph. With reference to EN 14372: 2004, by Phthalates solvent extraction and determined by 50 ppm GC-MS. With reference to USEPA 3540C, by Hexabromocyclododecane 10 ppm solvent extraction and determined by (HBCDD) GC-MS. Remark: Reporting limit = Quantitation limit of analyte in sample *THJ0285781* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410 Page 4 of 10 Number : TWNC00285781 Test Conducted (Ⅳ) Measurement Flowchart: Test for Cd/Pb/Hg/Chromium (VI)/PBBS/PBDES Contents Reference Standard: IEC 62321 edition 1.0:2008 Sample preparation For non-metal part For metal part Take sample and immerse into Aqua Regia, start to strip plating layer Stop the stripping procedure upon color change completely Take the Aqua solution as plating component and stripped body as substrate component PBBs/PBDEs Weigh sample and add organic solvent By Soxhlet extraction or Solvent extraction Concentrate the extract and make up with organic solvent Analyzed by GC-MSD Cr 6+ Substrate Cd/Pb/Hg Weigh sample and add alkaline solution For different material, digest the sample with *1 appropriate acid Plating Cr 6+ By spot test Definite temp. extraction Cool and filter the extract Confirm the tested samples are totally dissolved Negative *2 Get 50cm2 sample Make up with deionized water By boiling water extraction Analyzed by ICP-OES Make up with deionized water and add diphenyl-carbazide solution Analyzed by UV-VIS *THJ0285781* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410 Page 5 of 10 Number : TWNC00285781 Test Conducted (Ⅳ) Measurement Flowchart: Remarks: *1: List of Appropriate Acid： Material Polymers Metals Electronics Acid Added for Digestion HNO3,HCl,HF,H2O2,H3BO3 HNO3,HCl,HF HNO3,HCl,H2O2,HBF4 *2: If the result of spot test is positive, Chromium VI would be determined as detected. *THJ0285781* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410 Page 6 of 10 Number : TWNC00285781 Test Conducted (Ⅳ) Measurement Flowchart: Test for Halogen Content Reference Standard：EN 14582 Sampling/grinding or cutting Add absorbent in a combustion flask & place weighed sample in equipment Fill oxygen into calorimetric bomb Ignite then leave the bomb at room temperature Transfer the absorbent into a volumetric flask Make up with deionized water Analyzed by ion chromatography *THJ0285781* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410 Page 7 of 10 Number : TWNC00285781 Test Conducted (Ⅳ) Measurement Flowchart: Test For Phthalates Contents Reference Method: EN 14372: 2004 Sampling/grinding or cutting Weigh sample and add organic solvent By solvent extraction Concentrate the extract and make up with organic solvent Analyzed by GC-MSD *THJ0285781* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410 Page 8 of 10 Number : TWNC00285781 Test Conducted (Ⅳ) Measurement Flowchart: Test For Hexabromocyclododecane (HBCDD) Reference Standard：USEPA 3540C Sampling/grinding or cutting Weigh sample and add organic solvent By soxhlet extraction Concentrate the extract and make up with organic solvent Analyzed by GC-MSD End of Report This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a recommendation for any particular course of action. Intertek does not accept a duty of care or any other responsibility to any person other than the Client in respect of this report and only accepts liability to the Client insofar as is expressly contained in the terms and conditions governing Intertek's provision of services to you. Intertek makes no warranties or representations either express or implied with respect to this report save as provided for in those terms and conditions. We have aimed to conduct the Review on a diligent and careful basis and we do not accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by statute or otherwise, except in the event of our gross negligence or wilful misconduct. *THJ0285781* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410 Page 9 of 10 Number : TWNC00285781 Test Conducted Photo *THJ0285781* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410 Page 10 of 10 nown Validit ForOuesti PleaseCo TestReport No.: CE20'11184940 ithsGS Pager'1of 7 Dale:2011h21o1 Ll|| lllllllll AG POLYFIL ZUG/ SWITZERLAND 2OA,CH$3OO OBERALLMENDSTRASSE ll Thefollowingsample(s)was/werosubmittedand identifiedby/onbehalfof the clientas: SampleDescfiption No. Buyer/Order Date SampleReceiving Period Testing Test Reault(s) A91000 11-0010 2011t11t25 201III1125rO 201Il12to1 Pleasereferto nextpage(s). Ch..r{.{ lrbq.a..Y -Tdld praG)radd hs@@d€nndb c * * - , , iiifji'iiiii;":;ovm'c";p,'iyi,bFatec*""rc*dioreas;"*Fi.l***"d*.abb-"q li,;i#,-.i.i'*1'lt.j'.*Jb,"iti-.""ac*a*o,ea"o*':*"*e"-.'"*..l d"isdrt'"' rtmdff.mndhe@nciedssecnp5ir'srnd.qsdse ,il-.liiJ.ii.lru,".aa,*;**isr ;;;;ft";'".'*;.;";'*'.'enoo."en'jo"-.*.ore-j-*a.e""., ,r '*.;.Dkie,;or.6rs 1rn.r +!1iiE ti 1M 10r2o tD I i e6 iorrrs tt dw{<om MeD&' or$e scsGldp l\6' 5A) TestReport No.: CE/2011/84940 Paga:2ol7 Date| 2011112J01 r POLYFILAG ZUG/ SWITZERLAND OBERALLMENDSTMSSE2OA,CH€3OO rIlt flttlt TestR6ult(s) SILVERCOLOREDIVETALWIRE PARTNAIVENo.1 Tostltem(s) Unit (Cd) Cadmium MDL ethod mgKg Lead (Pb) Mercury(Hg) Cr(Vl) Hexavalent Chromium to IEC62321r2008and Withreference mg/Kg perfomedby ICP-AES. mS/kS 2 2 Withr€fefence to IEC62321:2008and perfomedby Boilingwaterext€ction Method.# Rs6ult l.lo.l n.d. n.d. n.o, Negative n.o. Sumof PBB3 Monobromobiphenyl Dibromobiphenyl Tribromobiphenyl 5 5 5 Tetrabromobiphenyl Pentabromobiphenyl Hexabromobiphenyl Hoptabro.nobiphenyl Octabromobiphenyl Nonabromobiphenyl Decabromobiphenyl Sumof PBDES ether Monobromodiphenyl ether Dibromodiphenyl ether Tribromodiphenyl Tetrabromodiphenyl ether 5 2008and Withreference to IEC6232'1r mg/Kg perfomed by GC/MS. 5 5 5 5 5 5 n.d- n.d. n_o, n.d. n.d. n.d. n.d. n.d. n-o. n.d. n.d. n.o. n.d. n.d. 5 5 5 Pentabromodiphenyl ether ether Hexabromodiphenyl ether Heptabrornodiphenyl ether Octabromodiphenyl 5 5 ether Nonabromodiphenyl n.d. n.d. n.d. n.d. n.d. n.d. n.d. ether Decabromodiphenyl sGrrsdd rhs rd @d €n@lb € ni" i*i-.a;";;;ovdc"'mry ioi"ar r c*.a c"ar*" a s r-ogoi-ttauj'o*'$;bi'.'"dc"dl-'l.,Ed-"*-.*ua*"g"..'t. l*i.'ii]*r-"rl*i;a."**ieiam"ryho6dat"a*,..n"a&i*dlsl"b,'d;^ffi"&hi* p.i.bivsioBoam5d66@m *,".* -,'r*"u"i."ac ,ro*repua**ptot..w m*-. o"-^eno "w-'ia ll r,: +i,!4i'r 3)7e| + & taa2a )t1 w \t r 336to2t22ee 4"an Test Report No.: CEl201'1/84940 Page:3 of 7 Dale: 2O11112J01 rl POLYFILAG OBERALLMENDSTMSSE2OA,CH€3OOZUG / SWITZERLAND T€t lt.m(s) Halogen (F) Halogen-Fluorine (CASNo.:14762-9+8) (Cl) Halogen-Chlorin€ (CASNo.:22537-15-1) (Br) Halogen-Bromine (CASNo.:10097-32-2) (l) Halogen-lodine (CASNo.:14362.44-8) Unit mg/Kg Method With referenceto BS EN ASAZ2007. wasperfomedby lC. Analysis [IDL [|||llt[l]t Result No.1 50 n.o, 50 n.d. 50 n-d. 50 n.d. Note : 1. mg/kg= ppm i 0.1M%= 1000ppm 2. n.d. = Not Det€cted Limit 3. MDL= MethodDeteclion 4."-"=NotRegulated analysis(NoUnit) 5. " = Qualitative 6. # = a. Positivemeansthe presenceof ClVl on the testedareas b. Negativemeansthe absenceof OVI on the testedareas solutionis equalor grcatefthan0.02mg/kgwith 50 cm'z The de'tectedconcent€tionin boiling-watea-extraction testedareas. a**. , i"il'ln '^lhsl6tts@1delm'Lo1bgamplel'igddft3l6drcpd€molbercp i'' !i"a uyt;c".pry -bdb k c.€€rc-di *'; n'ii iilj'i'ii*i* "ae;;a-,**; 'r i,.," o c,""* *' *r,.* , ; . , d L . M"'"^ d.rffi.nda, ostra fu"[email protected]'"digdbTm"'dcmd€B6E|M"o"-..a'**.e'..l"*'" h-.^'' EEidondne@ ss tud;i€dad ed sad'edrhd ;or*_p-'*.@". '' ,ror Test Report No.: CE/2011/84940 Page:4 ol7 Dale.201111i,01 ||t] tlt POLYFILAG OBERALLMENDSTRASSE 2OA,CH63OOZUG / SWTZERLAND trlll methodaccording to belowflowchart. 1) Thesesamples weredissolved totallyby pretonditioning ( Cr- test methodexcluded) Yang Climbgreat 2) Nameofthe personwhom€demeasurernent: TroyChang 3) Nameof thepersonin chargeof measu.ement: Cutting/ Preparation acid Aciddigestion by suitable dependedon difierentsample material{a8belowtable) Addappropiateamountof digestion reagent Heatto appropriate t€rnperatureto exttact 1) AlkaliFusion 2) HCltodi6solve ICP.AES Add diphenyl-carbazidef or colordevelopment Dige*ionAcid S€mpleMaterial solder Steel,copper,aluminum, Aqua €gia, HNO3,HCl,HF,HrO, Gla6s HNO3/HF measurethe absotbance Gold,platinum,palladium,ceramic Aqua fegia at 5,10nm by W-VIS Silver HNOg Plastic HrSO4, HrOr,HNq, HCI Others Anyacidtototaldigestion ipsGlb{d rh s rd reD.d €nid b cmtsry alrrjllr!I. iri.if::l.r{iji;;i-\Jl*, i*"f.inF*}ri1'r:\, +j'an fn:/tE+' l."*.i,'.nggauymc"'pny3u$].dbAGm66|coidlonso's b i*.. ..d cddiom ro, Eefu rc t"-a aoajmero. j**;";or; "e-" ,"M"if,*ld."d]@nd"" ory .r *u, rt'" i. e otc iear e tu;,ob"dd ods.6e,tuh tr4!.1 lt rFrl|ri 14610r)re TestReport No.: CE/2011/84940 Dale.2011hZO1 [fir POLYFILAG ZUG/ SWITZERLAND 2OA,CH€3OO OBERALLMENDSTRASSE PBBIPBDE analyticalFLow CHART Wong 1) l.lade of the personwhonEderBasurerEnl Rornan 2) l{anE of the personin chargeof nEasurenEntTroyChang Fi6t te6tingprocess------' Optional screenprocess---. proce6s - .> Confinmtion Screenanalysis i..........1.......... Sanplee)draction/ So*rlet d€thod ConcentratdDilute Extractedsoftlion v Filter Analysisby GC/MS csF nirhsl6itspdBlsrdvroibsamprqtbd€d i;:Jret4i..!ril'j!.;!1{t,; jiilni:rEi,l-,1llri+ttr^1\i=fl:'' fr s6nrcFd6nde r!11t4' riii i"ii'Ja i. 'i'i.a u.,r. c"'eny &brd ,os c6€6 cmdib* orsn o ims -a c*4"* t". et* r.LiL" r-J ir"",j'"ai "or.i ,"is",r,*isponsbrt sb ccie^randrhsd@ "ae*aa"" "*i *r-a*mnrci,.:s*cr"nt "sr ei."oe"^o"lg"*"*o,u"t"**.'"d;.d.ri,do@.*l-ndbe.s$o!ucedeic€p1.fu[wihod r.a"t o' |aLsi€6" d 'h" @i1ad d .,rll,,4iirrl;'r.:. i6".,-,r Page:5 of 7 +Jr r+i'r'!i+M10r'$'r r+s |l lt]||]t TestReport No.:CE/2011/84940 Date:.2011h21j POLYFIL AG OBERALLMENDSTRASSE 2OA,CH-6300 ZUG/ SWITZERLAND Analyticalflow chartof halogencontent '1) tlarneof theperson whorEde rEasurerpnt:RitaChen 2) lLarE of the personin chaee of fiEa6urefl€nt:TroyChang Sanpleprekeatrent/ Separatbn Weigtrting andputting sarple in cell OrygenBombCombustion / Ab6orption Dilution to fixedvolufl€ AnalysiswasperfonyEdby lC comtsiy3r;tlri."i4 ,r 4i+;:rlait;.ri!r,!iir.a! ft s 6ummr s Gsu6d bys6 coipa -i-it++if.l.1\. Jrrr+.. ^:i.- lul!11. p.fubly6lo8cl3n|ad|his@m rbrldceidob oar63 undr rh3ra ,:iit(:: +gt rr/di1i+er@rae Pagei 6 of 7 lm[r[ ttlltl|] TestReport No.: CE/2011/84940 Page:7 ol7 Date:2011h2J01 f][Ilrt]tlltttt! POLYFIL AG 2OA,CH-6300 ZUG/ SWITZERLAND OBERALLMENDSTMSSE ' Thetestedsample/ part ls markedby an anow if its shownon tho photo.' '* Endof Report " n $6 ron repondd on y b rhe smdaG)rad* Th. b! @on enid b.qod f!l:$rrl!' cmp.ny+I:rllirql.nrirf;tllrSii;;ilrliirEii 1-lli5*11t{llr -i;:4 Th€d&.d..dby1h"c.'Fny&q.db6Gs66lcmdioBdssruceFnl€de€d6al.*a|abem6q tu €ktrd bmd &imstu strl hi.ohbadd od m6 uid., u,. r. r-d,,;r +!r l{!liiirlas6 Dtre Test Report Applicant: Number : TWNC00237228 Littelfuse Philippines Inc. LIMA Technology Center, Lipa City, Malvar, Batangas Date : Jan 05, 2012 Sample Description: One (1) group of submitted samples said to be : Part Description : Element (Silver Strip Sn Plated) Part Number : 079026 Date Sample Received : Dec 15, 2011 Date Test Started : Jan 03, 2012 Test Conducted : As requested by the applicant, for details please refer to attached pages. Authorized By: On Behalf Of Intertek Testing Services Taiwan Limited K. Y. Liang Director This report shall not be reproduced except in full, without the written approval of the laboratory. Page 1 of 5 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401 Number : TWNC00237228 Test Conducted (Ⅰ) Test Result Summary : Test Item Heavy Metal Cadmium (Cd) content Lead (Pb) content Mercury (Hg) content Chromium VI (Cr6+) content (mg/kg with 50cm2) Result (ppm) Silvery Metal ND ND ND Negative (< 0.02) Remarks: ppm = Parts per million based on weight of tested sample = mg/kg ND = Not detected < = Less than mg/kg with 50cm2 = milligram per kilogram with 50 square centimetre Negative = A negative test result indicated positive observation was not found at the time of Test. Responsibility of Chemist : Irene Chiou / Kevin Liu Date Sample Received Test Period : Dec 15, 2011 : Jan 03, 2012 To Jan 05, 2012 (Ⅱ) RoHS Requirement: Restricted Substances Cadmium (Cd) Content Lead (Pb) Content Mercury (Hg) Content Chromium VI (Cr6+) Content Limits 0.01% (100ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for homogeneous material. Page 2 of 5 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401 Number : TWNC00237228 Test Conducted (Ⅲ) Test Method: Test Item Cadmium (Cd) content Lead (Pb) content Mercury (Hg) content Chromium VI (Cr6+) content Test Method With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in clause 7, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in annex B, by boiling water extraction and determined by UV-Vis spectrophotometer. Reporting Limit 2 ppm 2 ppm 2 ppm 0.02 mg/kg with 50cm2 Remark: Reporting limit = Quantitation limit of analyte in sample Page 3 of 5 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401 Number : TWNC00237228 Test Conducted (Ⅳ) Measurement Flowchart: Test for Cd/Pb/Hg/Chromium (VI) Reference Standard：IEC 62321 edition 1.0:2008 Sample preparation Take sample and immerse into Aqua Regia, start to strip plating layer Stop the stripping procedure upon color change completely Take the Aqua solution as plating component and stripped body as substrate component Cd/Pb/Hg Cr Polymers / electronics Metal For different material, digest the sample with *1 appropriate acid By spot test Negative Confirm the tested samples are totally dissolved Make up with deionized water Analyzed by ICP-OES 6+ *2 Weigh sample and add alkaline solution Get 50cm2 sample Definite temp. extraction By boiling water extraction Cool and filter the extract Make up with deionized water and add diphenyl-carbazide solution Analyzed by UV-VIS Remarks: *1: List of Appropriate Acid： Acid Added for Digestion Material Polymers HNO3,HCl,HF,H2O2,H3BO3 Metals HNO3,HCl,HF Electronics HNO3,HCl,H2O2,HBF4 *2: If the result of spot test is positive, Chromium VI would be determined as detected. End of Report Page 4 of 5 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401 Number : TWNC00237228 Test Conducted Photo Page 5 of 5 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401 Test Report Applicant: Number : TWNC00285770 Littelfuse Philippines Inc. LIMA Technology Center, Lipa City, Malvar, Batangas Date : Nov 19, 2012 Sample Description: One (1) group of submitted samples said to be : Part Description : Solder (Pb is ≥ 90%) Part Number : 692323 Date Sample Received : Nov 12, 2012 Date Test Started : Nov 13, 2012 Test Conducted : As requested by the applicant, for details please refer to attached pages. Authorized By: On Behalf Of Intertek Testing Services Taiwan Limited K. Y. Liang Director *THJ0285770* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410 Page 1 of 6 Number : TWNC00285770 Test Conducted (Ⅰ) Test Result Summary : Result (ppm) Silvery Metal Test Item Heavy Metal Cadmium (Cd) content Lead (Pb) content Mercury (Hg) content Chromium VI (Cr6+) content (mg/kg with 50cm2) ND 910679 ND Negative (< 0.02) Remarks: ppm = Parts per million based on weight of tested sample = mg/kg ND = Not detected < = Less than mg/kg with 50cm2 = milligram per kilogram with 50 square centimetre Negative = A negative test result indicated positive observation was not found at the time of Test. Responsibility of Chemist : Irene Chiou / Kevin Liu Date Sample Received Test Period : Nov 12, 2012 : Nov 13, 2012 To Nov 15, 2012 (Ⅱ) RoHS Limits: Restricted Substances Cadmium (Cd) Content Lead (Pb) Content Mercury (Hg) Content Chromium VI (Cr6+) Content Limits 0.01% (100ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) The above limits were quoted from Annex II of 2011/65/EU for homogeneous material. *THJ0285770* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410 Page 2 of 6 Number : TWNC00285770 Test Conducted (Ⅲ) Test Method: Test Item Cadmium (Cd) content Lead (Pb) content Mercury (Hg) content Chromium VI (Cr6+) content Test Method With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in clause 7, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in annex B, by boiling water extraction and determined by UV-Vis Spectrophotometer. Reporting Limit 2 ppm 2 ppm 2 ppm 0.02 mg/kg with 50cm2 Remark: Reporting limit = Quantitation limit of analyte in sample *THJ0285770* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410 Page 3 of 6 Number : TWNC00285770 Test Conducted (Ⅳ) Measurement Flowchart: Test For Cd/Pb/Hg/Chromium (VI) Reference Standard：IEC 62321 edition 1.0:2008 Sampling/grinding or cutting Cd/Pb/Hg Cr 6+ Polymers / Electronics Metal For different material, digest the sample with *1 appropriate acid By spot test Negative Confirm the tested samples are totally dissolved Make up with deionized water *2 Weigh sample and add alkaline solution Get 50cm2 sample Definite temp. extraction Boiling water extraction Cool and filter the extract Analyzed by ICP-OES Make up with deionized water and add diphenylcarbazide solution Analyzed by UV-VIS *THJ0285770* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410 Page 4 of 6 Number : TWNC00285770 Test Conducted (Ⅳ) Measurement Flowchart: Remarks: *1: List of Appropriate Acid： Acid Added for Digestion Material Polymers HNO3,HCl,HF,H2O2,H3BO3 Metals HNO3,HCl,HF Electronics HNO3,HCl,H2O2,HBF4 *2: If the result of spot test is positive, Chromium VI would be determined as detected. End of Report This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a recommendation for any particular course of action. Intertek does not accept a duty of care or any other responsibility to any person other than the Client in respect of this report and only accepts liability to the Client insofar as is expressly contained in the terms and conditions governing Intertek's provision of services to you. Intertek makes no warranties or representations either express or implied with respect to this report save as provided for in those terms and conditions. We have aimed to conduct the Review on a diligent and careful basis and we do not accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by statute or otherwise, except in the event of our gross negligence or wilful misconduct. *THJ0285770* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410 Page 5 of 6 Number : TWNC00285770 Test Conducted Photo *THJ0285770* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410 Page 6 of 6 Test Report Applicant: Number : TWNC00253636 Littelfuse Philippines Inc. LIMA Technology Center, Lipa City, Malvar, Batangas Date : Apr 24, 2012 Sample Description: One (1) group of submitted samples said to be : Part Description : Black Ink Part Number : 425809 Date Sample Received : Apr 19, 2012 Date Test Started : Apr 19, 2012 Test Conducted : As requested by the applicant, for details please refer to attached pages. Authorized By: On Behalf Of Intertek Testing Services Taiwan Limited K. Y. Liang Director This report shall not be reproduced except in full, without the written approval of the laboratory. Page 1 of 9 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401 Number : TWNC00253636 Test Conducted (Ⅰ) Test Result Summary : Test Item Heavy Metal Cadmium (Cd) content Lead (Pb) content Mercury (Hg) content Chromium VI (Cr6+) content Polybrominated Biphenyls (PBBs) Monobrominated Biphenyls (MonoBB) Dibrominated Biphenyls (DiBB) Tribrominated Biphenyls (TriBB) Tetrabrominated Biphenyls (TetraBB) Pentabrominated Biphenyls (PentaBB) Hexabrominated Biphenyls (HexaBB) Heptabrominated Biphenyls (HeptaBB) Octabrominated Biphenyls (OctaBB) Nonabrominated Biphenyls (NonaBB) Decabrominated Biphenyl (DecaBB) Polybrominated Diphenyl Ethers (PBDEs) Monobrominated Diphenyl Ethers (MonoBDE) Dibrominated Diphenyl Ethers (DiBDE) Tribrominated Diphenyl Ethers (TriBDE) Tetrabrominated Diphenyl Ethers (TetraBDE) Pentabrominated Diphenyl Ethers (PentaBDE) Hexabrominated Diphenyl Ethers (HexaBDE) Heptabrominated Diphenyl Ethers (HeptaBDE) Octabrominated Diphenyl Ethers (OctaBDE) Nonabrominated Diphenyl Ethers (NonaBDE) Decabrominated Diphenyl Ether (DecaBDE) Result (ppm) Black Paste ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND Page 2 of 9 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401 Number : TWNC00253636 Test Conducted (Ⅰ) Test Result Summary : Test Item Result (ppm) Black Paste Halogen Content Fluorine (F) Chlorine (Cl) Bromine (Br) Iodine (I) Phthalates Di(2-ethylhexyl) Phthalate (DEHP) Dibutyl Phthalate (DBP) Benzyl Butyl Phthalate (BBP) Others Hexabromocyclododecane (HBCDD) ND 610 ND ND ND ND ND ND Remarks: ppm = Parts per million based on wet weight of tested sample = mg/kg ND = Not detected Responsibility of Chemist : Irene Chiou / Kevin Liu / Cathy Chen Date Sample Received Test Period : Apr 19, 2012 : Apr 19, 2012 To Apr 24, 2012 (Ⅱ) RoHS Requirement: Restricted Substances Cadmium (Cd) Content Lead (Pb) Content Mercury (Hg) Content Chromium VI (Cr6+) Content Polybrominated Biphenyls (PBBs) Polybrominated Diphenyl Ehters (PBDEs) Limits 0.01% (100ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for homogeneous material. Page 3 of 9 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401 Number : TWNC00253636 Test Conducted (Ⅲ) Test Method: Test Item Test Method With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by Cadmium (Cd) content microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by Lead (Pb) content microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in clause 7, by microwave Mercury (Hg) content digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition Chromium VI (Cr6+) 1.0:2008 in annex C, by alkaline content digestion and determined by UV-Vis spectrophotometer. With reference to IEC 62321 edition 1.0:2008 in annex A, by solvent Polybrominated extraction and determined by GC-MS Biphenyls (PBBs) and further HPLC-DAD confirmation when necessary. With reference to IEC 62321 edition Polybrominated 1.0:2008 in annex A, by solvent Diphenyl Ethers extraction and determined by GC-MS (PBDEs) and further HPLC-DAD confirmation when necessary. With reference to EN 14582:2007 by Halogen Content calorimetric bomb with oxygen and determined by Ion Chromatograph. With reference to EN 14372: 2004, by Phthalates solvent extraction and determined by GC-MS. With reference to USEPA 3540C, by Hexabromocyclododecane solvent extraction and determined by (HBCDD) GC-MSD. Reporting Limit 2 ppm 2 ppm 2 ppm 1 ppm 5 ppm 5 ppm 50 ppm 10 ppm 10 ppm Remark: Reporting limit = Quantitation limit of analyte in sample Page 4 of 9 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401 Number : TWNC00253636 Test Conducted (Ⅳ) Measurement Flowchart: Test for Cd/Pb/Hg/Chromium (VI)/PBBS/PBDES Contents Reference Standard: IEC 62321 edition 1.0:2008 Sample preparation For non-metal part For metal part Take sample and immerse into Aqua Regia, start to strip plating layer Stop the stripping procedure upon color change completely Take the Aqua solution as plating component and stripped body as substrate component Cd/Pb/Hg Cr Weigh sample and add organic solvent By spot test Negative Confirm the tested samples are totally dissolved Make up with deionized water PBBs/PBDEs Polymers / electronics Metal For different material, digest the sample with *1 appropriate acid 6+ Get 50cm2 sample By boiling water extraction *2 Weigh sample and add alkaline solution By Soxhlet extraction or Solvent extraction Definite temp. extraction Cool and filter the extract Analyzed by ICP-OES Concentrate the extract and make up with organic solvent Analyzed by GC-MSD Make up with deionized water and add diphenylcarbazide solution Analyzed by UV-VIS Remarks: *1: List of Appropriate Acid： Acid Added for Digestion Material Polymers HNO3,HCl,HF,H2O2,H3BO3 Metals HNO3,HCl,HF Electronics HNO3,HCl,H2O2,HBF4 *2: If the result of spot test is positive, Chromium VI would be determined as detected. Page 5 of 9 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401 Number : TWNC00253636 Test Conducted (Ⅳ) Measurement Flowchart: Test for Halogen Content Reference Standard：EN 14582 Sampling/grinding or cutting Add absorbent in a combustion flask & place weighed sample in equipment Fill oxygen into calorimetric bomb Ignite then leave the bomb at room temperature Transfer the absorbent into a volumetric flask Make up with deionized water Analyzed by ion chromatography Page 6 of 9 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401 Number : TWNC00253636 Test Conducted (Ⅳ) Measurement Flowchart: Test For Phthalates Contents Reference Method: EN 14372: 2004 Sampling/grinding or cutting Weigh sample and add organic solvent By solvent extraction Concentrate the extract and make up with organic solvent Analyzed by GC-MSD Page 7 of 9 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401 Number : TWNC00253636 Test Conducted (Ⅳ) Measurement Flowchart: Test For Hexabromocyclododecane (HBCDD) Reference Standard：USEPA 3540C Sampling/grinding or cutting Weigh sample and add organic solvent By soxhlet extraction Concentrate the extract and make up with organic solvent Analyzed by GC-MSD End of Report Page 8 of 9 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401 Number : TWNC00253636 Test Conducted Photo Page 9 of 9 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401