ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: Nano Product #: 456xxx Series – 40 Amp Issue Date: April 19, 2013 It is hereby certified by Littelfuse, Inc. that there is neither RoHS (EU Directive 2002/95/EC, 2011/65/EU)-restricted substance nor such use, for materials to be used for unit parts, for packing/packaging materials, and for additives and the like in the manufacturing processes. In addition, it is hereby reported to you that the parts and sub-materials, the materials to be used for unit parts, the packing/packaging materials, and the additives and the like in the manufacturing processes, are all composed of the following components. Issued by: <Global EHS Specialist> (1) Parts, sub-materials and unit parts This document covers the Nano RoHS-Compliant series products manufactured by Littelfuse, Inc. ＜ Raw Materials Used Please see Table 1 (2) The ICP data on all measurable substances Please see appropriate pages as identifed in Table 1 Remarks： Form 585-047 Rev. A 1 2/21/06 Table 1: List of Raw Materials covered by this report Total Parts 1 2 3 4 5 6 Raw Material Part Number 910-261 692540 079xxx 909-423 087266 425809 Raw Material Description Cap Solder Element Body Anaerobic Adhesive Ink 2 Page(s) 3-8 9-14 15-19 20-27 28-37 38-47 Test Report Applicant: Number : TWNC00290386 Littelfuse, S.A. de C.V. Blvd. Fausto Z. Martinez #1800 Col. Magisterio Seccion 38 C.P. 26070 Piedra Negras, Coahuila, Mexico Date : Dec 19, 2012 Sample Description: One (1) group of submitted samples said to be : Part Description : Cap Part Number : 910-261 Date Sample Received : Dec 11, 2012 Date Test Started : Dec 12, 2012 Test Conducted : As requested by the applicant, for details please refer to attached pages. Authorized by: On Behalf of Intertek Testing Services Taiwan Limited K. Y. Liang Director *THJ0290386* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C. 全國公證檢驗股份有限公司 11492 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410 Page 1 of 6 Number : TWNC00290386 Test Conducted (Ⅰ) Test Result Summary : Result (ppm) (1) (2) Test Item Heavy Metal Cadmium (Cd) content Lead (Pb) content Mercury (Hg) content Chromium VI (Cr6+) content (mg/kg with 50cm2) ND 25 ND Negative (< 0.02) ND ND ND Negative (< 0.02) Remarks: ppm = Parts per million based on weight of tested sample = mg/kg ND = Not detected < = Less than mg/kg with 50cm2 = milligram per kilogram with 50 square centimetre Negative = A negative test result indicated positive observation was not found at the time of Test. Tested Components (1) Coppery metal base material (2) Silvery plating layer Responsibility of Chemist : Irene Chiou / Kevin Liu Date Sample Received Test Period : Dec 11, 2012 : Dec 12, 2012 To Dec 14, 2012 (Ⅱ) RoHS Limits: Restricted Substances Cadmium (Cd) Content Lead (Pb) Content Mercury (Hg) Content Chromium VI (Cr6+) Content Limits 0.01% (100ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) The above limits were quoted from Annex II of 2011/65/EU for homogeneous material. *THJ0290386* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C. 全國公證檢驗股份有限公司 11492 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410 Page 2 of 6 Number : TWNC00290386 Test Conducted (Ⅲ) Test Method: Test Item Cadmium (Cd) content Lead (Pb) content Mercury (Hg) content Chromium VI (Cr6+) content Test Method With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in clause 7, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in annex B, by boiling water extraction and determined by UV-Vis Spectrophotometer. Reporting Limit 2 ppm 2 ppm 2 ppm 0.02 mg/kg with 50cm2 Remark: Reporting limit = Quantitation limit of analyte in sample *THJ0290386* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C. 全國公證檢驗股份有限公司 11492 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410 Page 3 of 6 Number : TWNC00290386 Test Conducted (Ⅳ) Measurement Flowchart: Test For Cd/Pb/Hg/Chromium (VI) Reference Standard：IEC 62321 edition 1.0:2008 Sample preparation Take sample and immerse into Aqua Regia, start to strip plating layer Stop the stripping procedure upon color change completely Take the Aqua solution as plating component and stripped body as substrate component Cd/Pb/Hg Substrate Plating For different material, digest the sample with *1 appropriate acid Cr 6+ By spot test Confirm the tested samples are totally dissolved Make up with deionized water Negative *2 Get 50cm2 sample By boiling water extraction Analyzed by ICP-OES Make up with deionized water and add diphenyl-carbazide solution Analyzed by UV-VIS *THJ0290386* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C. 全國公證檢驗股份有限公司 11492 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410 Page 4 of 6 Number : TWNC00290386 Test Conducted Remarks: *1: List Of Appropriate Acid： Material Polymers Metals Electronics Acid Added For Digestion HNO3,HCl,HF,H2O2,H3BO3 HNO3,HCl,HF HNO3,HCl,H2O2,HBF4 *2: If the result of spot test is positive, Chromium VI would be determined as detected. End of Report This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a recommendation for any particular course of action. Intertek does not accept a duty of care or any other responsibility to any person other than the Client in respect of this report and only accepts liability to the Client insofar as is expressly contained in the terms and conditions governing Intertek's provision of services to you. Intertek makes no warranties or representations either express or implied with respect to this report save as provided for in those terms and conditions. We have aimed to conduct the Review on a diligent and careful basis and we do not accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by statute or otherwise, except in the event of our gross negligence or wilful misconduct. *THJ0290386* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C. 全國公證檢驗股份有限公司 11492 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410 Page 5 of 6 Number : TWNC00290386 Test Conducted Photo *THJ0290386* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C. 全國公證檢驗股份有限公司 11492 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410 Page 6 of 6 Test Report Applicant: Number : TWNC00290652 Littelfuse Philippines Inc. LIMA Technology Center, Lipa City, Malvar, Batangas Date : Dec 20, 2012 Sample Description: One (1) group of submitted samples said to be : Part Description : Solder Part Number : 692540 Date Sample Received : Dec 13, 2012 Date Test Started : Dec 13, 2012 Test Conducted : As requested by the applicant, for details please refer to attached pages. Authorized by: On Behalf of Intertek Testing Services Taiwan Limited K. Y. Liang Director *THJ0290652* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C. 全國公證檢驗股份有限公司 11492 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410 Page 1 of 6 Number : TWNC00290652 Test Conducted (Ⅰ) Test Result Summary : Result (ppm) Silvery metal Test Item Heavy Metal Cadmium (Cd) content Lead (Pb) content Mercury (Hg) content Chromium VI (Cr6+) content (mg/kg with 50cm2) ND 283 ND Negative (< 0.02) Remarks: ppm = Parts per million based on weight of tested sample = mg/kg ND = Not detected < = Less than mg/kg with 50cm2 = milligram per kilogram with 50 square centimetre Negative = A negative test result indicated positive observation was not found at the time of Test. Responsibility of Chemist : Irene Chiou / Kevin Liu Date Sample Received Test Period : Dec 13, 2012 : Dec 13, 2012 To Dec 17, 2012 (Ⅱ) RoHS Limits: Restricted Substances Cadmium (Cd) Content Lead (Pb) Content Mercury (Hg) Content Chromium VI (Cr6+) Content Limits 0.01% (100ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) The above limits were quoted from Annex II of 2011/65/EU for homogeneous material. *THJ0290652* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C. 全國公證檢驗股份有限公司 11492 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410 Page 2 of 6 Number : TWNC00290652 Test Conducted (Ⅲ) Test Method: Test Item Cadmium (Cd) content Lead (Pb) content Mercury (Hg) content Chromium VI (Cr6+) content Test Method With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in clause 7, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in annex B, by boiling water extraction and determined by UV-Vis Spectrophotometer. Reporting Limit 2 ppm 2 ppm 2 ppm 0.02 mg/kg with 50cm2 Remark: Reporting limit = Quantitation limit of analyte in sample *THJ0290652* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C. 全國公證檢驗股份有限公司 11492 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410 Page 3 of 6 Number : TWNC00290652 Test Conducted (Ⅳ) Measurement Flowchart: Test For Cd/Pb/Hg/Chromium (VI) Reference Standard：IEC 62321 edition 1.0:2008 Sampling/grinding or cutting Cd/Pb/Hg Cr 6+ Polymers / Electronics Metal For different material, digest the sample with *1 appropriate acid By spot test Negative Confirm the tested samples are totally dissolved Make up with deionized water *2 Weigh sample and add alkaline solution Get 50cm2 sample Definite temp. extraction Boiling water extraction Cool and filter the extract Analyzed by ICP-OES Make up with deionized water and add diphenylcarbazide solution Analyzed by UV-VIS *THJ0290652* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C. 全國公證檢驗股份有限公司 11492 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410 Page 4 of 6 Number : TWNC00290652 Test Conducted Remarks: *1: List of Appropriate Acid： Material Acid Added for Digestion Polymers HNO3,HCl,HF,H2O2,H3BO3 Metals HNO3,HCl,HF Electronics HNO3,HCl,H2O2,HBF4 *2: If the result of spot test is positive, Chromium VI would be determined as detected. End of Report This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a recommendation for any particular course of action. Intertek does not accept a duty of care or any other responsibility to any person other than the Client in respect of this report and only accepts liability to the Client insofar as is expressly contained in the terms and conditions governing Intertek's provision of services to you. Intertek makes no warranties or representations either express or implied with respect to this report save as provided for in those terms and conditions. We have aimed to conduct the Review on a diligent and careful basis and we do not accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by statute or otherwise, except in the event of our gross negligence or wilful misconduct. *THJ0290652* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C. 全國公證檢驗股份有限公司 11492 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410 Page 5 of 6 Number : TWNC00290652 Test Conducted Photo *THJ0290652* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C. 全國公證檢驗股份有限公司 11492 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410 Page 6 of 6 Test Report Applicant: Littelfuse Philippines Inc. LIMA Technology Center, Lipa City, Malvar, Batangas Number : TWNC00293764 Date : Jan 14, 2013 Sample Description: One (1) group of submitted samples said to be : Part Description : Element (Silver Strip Sn Plated) Part Number : 079026 Date Sample Received : Jan 07, 2013 Date Test Started : Jan 08, 2013 Test Conducted : As requested by the applicant, for details please refer to attached pages. Authorized by: On Behalf of Intertek Testing Services Taiwan Limited K. Y. Liang Director *THJ0293764* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C. 全國公證檢驗股份有限公司 11492 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410 Page 1 of 5 Number Test Conducted (Ⅰ) Test Result Summary: Test Item Unit : TWNC00293764 Test Method Result Silvery metal RL ND 2 34 2 ND 2 Negative 0.02 Heavy Metal Cadmium (Cd) content ppm Lead (Pb) content ppm Mercury (Hg) content ppm Chromium VI (Cr6+) content Remarks: mg/kg with 50 cm2 With reference to IEC 62321: 2008, by microwave digestion and determined by ICP-OES. With reference to IEC 62321: 2008, by microwave digestion and determined by ICP-OES. With reference to IEC 62321: 2008, by microwave digestion and determined by ICP-OES. With reference to IEC 62321: 2008, by boiling water extraction and determined by UV-Vis Spectrophotometer. ppm = parts per million based on weight of tested sample = mg/kg ND = Not detected RL = Reporting Limit, Quantitation limit of analyte in sample mg/kg with 50cm2 = milligram per kilogram with 50 square centimeter Negative = A negative test result indicated positive observation was not found at the time of Test. When the spot test showed a negative result, the boiling water extraction procedure shall be used to verify the result. Responsibility of Chemist: Kevin Liu/ Irene Chiou : Jan 07, 2013 : Jan 08, 2013 To Jan 11, 2013 Date Sample Received Test Period (Ⅱ) RoHS Limits: Restricted Substances Limits Cadmium (Cd) content Lead (Pb) content Mercury (Hg) content Chromium VI (Cr6+) content 0.01% (100ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) The above limits were quoted from Annex II of 2011/65/EU for homogeneous material. *THJ0293764* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C. 全國公證檢驗股份有限公司 11492 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410 Page 2 of 5 Number Test Conducted (Ⅲ) Measurement Flowchart: : TWNC00293764 Test For Cd/Pb/Hg/Chromium (VI) Reference Standard：IEC 62321 edition 1.0:2008 Sampling/grinding or cutting Cd/Pb/Hg Cr 6+ Polymers / Electronics Metal For different material, digest the sample with *1 appropriate acid By spot test Negative Confirm the tested samples are totally dissolved Make up with deionized water *2 Weigh sample and add alkaline solution Get 50cm2 sample Definite temp. extraction Boiling water extraction Cool and filter the extract Analyzed by ICP-OES Make up with deionized water and add diphenylcarbazide solution Analyzed by UV-VIS *THJ0293764* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C. 全國公證檢驗股份有限公司 11492 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410 Page 3 of 5 Test Conducted Remarks: *1: List of Appropriate Acid： Material Acid Added for Digestion Polymers HNO3,HCl,HF,H2O2,H3BO3 Metals HNO3,HCl,HF Electronics HNO3,HCl,H2O2,HBF4 Number : TWNC00293764 *2: If the result of spot test is positive, Chromium VI would be determined as detected. End of Report This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a recommendation for any particular course of action. Intertek does not accept a duty of care or any other responsibility to any person other than the Client in respect of this report and only accepts liability to the Client insofar as is expressly contained in the terms and conditions governing Intertek's provision of services to you. Intertek makes no warranties or representations either express or implied with respect to this report save as provided for in those terms and conditions. We have aimed to conduct the Review on a diligent and careful basis and we do not accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by statute or otherwise, except in the event of our gross negligence or wilful misconduct. *THJ0293764* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C. 全國公證檢驗股份有限公司 11492 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410 Page 4 of 5 Number Test Conducted : TWNC00293764 Photo *THJ0293764* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C. 全國公證檢驗股份有限公司 11492 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410 Page 5 of 5 Test Report Applicant: Number : TWNC00285768 Littelfuse Philippines Inc. LIMA Technology Center, Lipa City, Malvar, Batangas Date : Nov 16, 2012 Sample Description: One (1) group of submitted samples said to be : Part Description : Body Part Number : 909-423 Date Sample Received : Nov 12, 2012 Date Test Started : Nov 13, 2012 Test Conducted : As requested by the applicant, for details please refer to attached pages. Authorized By: On Behalf Of Intertek Testing Services Taiwan Limited K. Y. Liang Director *THJ0285768* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410 Page 1 of 8 Number : TWNC00285768 Test Conducted (Ⅰ) Test Result Summary : Result (ppm) Gray Plastic Test Item Heavy Metal Cadmium (Cd) content Lead (Pb) content Mercury (Hg) content Chromium VI (Cr6+) content Polybrominated Biphenyls (PBBs) Monobrominated Biphenyls (MonoBB) Dibrominated Biphenyls (DiBB) Tribrominated Biphenyls (TriBB) Tetrabrominated Biphenyls (TetraBB) Pentabrominated Biphenyls (PentaBB) Hexabrominated Biphenyls (HexaBB) Heptabrominated Biphenyls (HeptaBB) Octabrominated Biphenyls (OctaBB) Nonabrominated Biphenyls (NonaBB) Decabrominated Biphenyl (DecaBB) Polybrominated Diphenyl Ethers (PBDEs) Monobrominated Diphenyl Ethers (MonoBDE) Dibrominated Diphenyl Ethers (DiBDE) Tribrominated Diphenyl Ethers (TriBDE) Tetrabrominated Diphenyl Ethers (TetraBDE) Pentabrominated Diphenyl Ethers (PentaBDE) Hexabrominated Diphenyl Ethers (HexaBDE) Heptabrominated Diphenyl Ethers (HeptaBDE) Octabrominated Diphenyl Ethers (OctaBDE) Nonabrominated Diphenyl Ethers (NonaBDE) Decabrominated Diphenyl Ether (DecaBDE) ND 60 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND *THJ0285768* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410 Page 2 of 8 Number : TWNC00285768 Test Conducted (Ⅰ) Test Result Summary : Result (ppm) Gray Plastic Test Item Halogen Content Fluorine (F) Chlorine (Cl) Bromine (Br) Iodine (I) ND ND ND ND Remarks: ppm = Parts per million based on weight of tested sample = mg/kg ND = Not detected Responsibility of Chemist : Irene Chiou / Kevin Liu / Cathy Chen Date Sample Received Test Period : Nov 12, 2012 : Nov 13, 2012 To Nov 15, 2012 (Ⅱ) RoHS Limits: Restricted Substances Cadmium (Cd) Content Lead (Pb) Content Mercury (Hg) Content Chromium VI (Cr6+) Content Polybrominated Biphenyls (PBBs) Polybrominated Diphenyl Ehters (PBDEs) Limits 0.01% (100ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) The above limits were quoted from Annex II of 2011/65/EU for homogeneous material. *THJ0285768* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410 Page 3 of 8 Number : TWNC00285768 Test Conducted (Ⅲ) Test Method: Test Item Cadmium (Cd) content Lead (Pb) content Mercury (Hg) content Chromium VI (Cr6+) content Polybrominated Biphenyls (PBBs) Polybrominated Diphenyl Ethers (PBDEs) Halogen Content Test Method With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in clause 7, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in annex C, by alkaline digestion and determined by UV-Vis spectrophotometer. With reference to IEC 62321 edition 1.0:2008 in annex A, by solvent extraction and determined by GC-MS and further HPLC-DAD confirmation when necessary. With reference to IEC 62321 edition 1.0:2008 in annex A, by solvent extraction and determined by GC-MS and further HPLC-DAD confirmation when necessary. With reference to EN 14582:2007 by calorimetric bomb with oxygen and determined by Ion Chromatograph. Reporting Limit 2 ppm 2 ppm 2 ppm 1 ppm 5 ppm 5 ppm 50 ppm Remark: Reporting limit = Quantitation limit of analyte in sample *THJ0285768* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410 Page 4 of 8 Number : TWNC00285768 Test Conducted (Ⅳ) Measurement Flowchart: Test for Cd/Pb/Hg/Chromium (VI)/PBBS/PBDES Contents Reference Standard: IEC 62321 edition 1.0:2008 Sample preparation For non-metal part For metal part Take sample and immerse into Aqua Regia, start to strip plating layer Stop the stripping procedure upon color change completely Take the Aqua solution as plating component and stripped body as substrate component PBBs/PBDEs Weigh sample and add organic solvent By Soxhlet extraction or Solvent extraction Concentrate the extract and make up with organic solvent Analyzed by GC-MSD Cr 6+ Substrate Cd/Pb/Hg Weigh sample and add alkaline solution For different material, digest the sample with *1 appropriate acid Plating Cr 6+ By spot test Definite temp. extraction Cool and filter the extract Confirm the tested samples are totally dissolved Negative *2 Get 50cm2 sample Make up with deionized water By boiling water extraction Analyzed by ICP-OES Make up with deionized water and add diphenyl-carbazide solution Analyzed by UV-VIS *THJ0285768* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410 Page 5 of 8 Number : TWNC00285768 Test Conducted (Ⅳ) Measurement Flowchart: Remarks: *1: List of Appropriate Acid： Material Polymers Metals Electronics Acid Added for Digestion HNO3,HCl,HF,H2O2,H3BO3 HNO3,HCl,HF HNO3,HCl,H2O2,HBF4 *2: If the result of spot test is positive, Chromium VI would be determined as detected. *THJ0285768* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410 Page 6 of 8 Number : TWNC00285768 Test Conducted (Ⅳ) Measurement Flowchart: Test for Halogen Content Reference Standard：EN 14582 Sampling/grinding or cutting Add absorbent in a combustion flask & place weighed sample in equipment Fill oxygen into calorimetric bomb Ignite then leave the bomb at room temperature Transfer the absorbent into a volumetric flask Make up with deionized water Analyzed by ion chromatography End of Report This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a recommendation for any particular course of action. Intertek does not accept a duty of care or any other responsibility to any person other than the Client in respect of this report and only accepts liability to the Client insofar as is expressly contained in the terms and conditions governing Intertek's provision of services to you. Intertek makes no warranties or representations either express or implied with respect to this report save as provided for in those terms and conditions. We have aimed to conduct the Review on a diligent and careful basis and we do not accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by statute or otherwise, except in the event of our gross negligence or wilful misconduct. *THJ0285768* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410 Page 7 of 8 Number : TWNC00285768 Test Conducted Photo *THJ0285768* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410 Page 8 of 8 Test Report Applicant: Number : TWNC00285781 Littelfuse Philippines Inc. LIMA Technology Center, Lipa City, Malvar, Batangas Date : Nov 19, 2012 Sample Description: One (1) group of submitted samples said to be : Part Description : Anaerobic Adhesive Part Number : 087266 Date Sample Received : Nov 12, 2012 Date Test Started : Nov 13, 2012 Test Conducted : As requested by the applicant, for details please refer to attached pages. Authorized By: On Behalf Of Intertek Testing Services Taiwan Limited K. Y. Liang Director *THJ0285781* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410 Page 1 of 10 Number : TWNC00285781 Test Conducted (Ⅰ) Test Result Summary : Result (ppm) Green Liquid Test Item Heavy Metal Cadmium (Cd) content Lead (Pb) content Mercury (Hg) content Chromium VI (Cr6+) content Polybrominated Biphenyls (PBBs) Monobrominated Biphenyls (MonoBB) Dibrominated Biphenyls (DiBB) Tribrominated Biphenyls (TriBB) Tetrabrominated Biphenyls (TetraBB) Pentabrominated Biphenyls (PentaBB) Hexabrominated Biphenyls (HexaBB) Heptabrominated Biphenyls (HeptaBB) Octabrominated Biphenyls (OctaBB) Nonabrominated Biphenyls (NonaBB) Decabrominated Biphenyl (DecaBB) Polybrominated Diphenyl Ethers (PBDEs) Monobrominated Diphenyl Ethers (MonoBDE) Dibrominated Diphenyl Ethers (DiBDE) Tribrominated Diphenyl Ethers (TriBDE) Tetrabrominated Diphenyl Ethers (TetraBDE) Pentabrominated Diphenyl Ethers (PentaBDE) Hexabrominated Diphenyl Ethers (HexaBDE) Heptabrominated Diphenyl Ethers (HeptaBDE) Octabrominated Diphenyl Ethers (OctaBDE) Nonabrominated Diphenyl Ethers (NonaBDE) Decabrominated Diphenyl Ether (DecaBDE) ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND *THJ0285781* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410 Page 2 of 10 Number : TWNC00285781 Test Conducted (Ⅰ) Test Result Summary : Result (ppm) Green Liquid Test Item Halogen Content Fluorine (F) Chlorine (Cl) Bromine (Br) Iodine (I) Phthalates Di(2-ethylhexyl) Phthalate (DEHP) Dibutyl Phthalate (DBP) Benzyl Butyl Phthalate (BBP) Others Hexabromocyclododecane (HBCDD) ND ND ND ND ND 77 ND ND Remarks: ppm = Parts per million based on wet weight of tested sample = mg/kg ND = Not detected Responsibility of Chemist : Irene Chiou / Kevin Liu / Cathy Chen Date Sample Received Test Period : Nov 12, 2012 : Nov 13, 2012 To Nov 15, 2012 (Ⅱ) RoHS Limits: Restricted Substances Cadmium (Cd) Content Lead (Pb) Content Mercury (Hg) Content Chromium VI (Cr6+) Content Polybrominated Biphenyls (PBBs) Polybrominated Diphenyl Ehters (PBDEs) Limits 0.01% (100ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) The above limits were quoted from Annex II of 2011/65/EU for homogeneous material. *THJ0285781* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410 Page 3 of 10 Number : TWNC00285781 Test Conducted (Ⅲ) Test Method: Test Item Reporting Limit Test Method With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the Cadmium (Cd) content 2 ppm tested samples are totally dissolved and determined by ICPOES. With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the Lead (Pb) content 2 ppm tested samples are totally dissolved and determined by ICPOES. With reference to IEC 62321 edition 1.0:2008 in clause 7, by microwave Mercury (Hg) content digestion until the tested samples 2 ppm are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition Chromium VI (Cr6+) 1.0:2008 in annex C, by alkaline 1 ppm digestion and determined by UV-Vis content spectrophotometer. With reference to IEC 62321 edition 1.0:2008 in annex A, by solvent Polybrominated extraction and determined by GC-MS 5 ppm Biphenyls (PBBs) and further HPLC-DAD confirmation when necessary. With reference to IEC 62321 edition 1.0:2008 in annex A, by solvent Polybrominated Diphenyl Ethers extraction and determined by GC-MS 5 ppm (PBDEs) and further HPLC-DAD confirmation when necessary. With reference to EN 14582:2007 by 50 ppm Halogen Content calorimetric bomb with oxygen and determined by Ion Chromatograph. With reference to EN 14372: 2004, by Phthalates solvent extraction and determined by 50 ppm GC-MS. With reference to USEPA 3540C, by Hexabromocyclododecane 10 ppm solvent extraction and determined by (HBCDD) GC-MS. Remark: Reporting limit = Quantitation limit of analyte in sample *THJ0285781* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410 Page 4 of 10 Number : TWNC00285781 Test Conducted (Ⅳ) Measurement Flowchart: Test for Cd/Pb/Hg/Chromium (VI)/PBBS/PBDES Contents Reference Standard: IEC 62321 edition 1.0:2008 Sample preparation For non-metal part For metal part Take sample and immerse into Aqua Regia, start to strip plating layer Stop the stripping procedure upon color change completely Take the Aqua solution as plating component and stripped body as substrate component PBBs/PBDEs Weigh sample and add organic solvent By Soxhlet extraction or Solvent extraction Concentrate the extract and make up with organic solvent Analyzed by GC-MSD Cr 6+ Substrate Cd/Pb/Hg Weigh sample and add alkaline solution For different material, digest the sample with *1 appropriate acid Plating Cr 6+ By spot test Definite temp. extraction Cool and filter the extract Confirm the tested samples are totally dissolved Negative *2 Get 50cm2 sample Make up with deionized water By boiling water extraction Analyzed by ICP-OES Make up with deionized water and add diphenyl-carbazide solution Analyzed by UV-VIS *THJ0285781* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410 Page 5 of 10 Number : TWNC00285781 Test Conducted (Ⅳ) Measurement Flowchart: Remarks: *1: List of Appropriate Acid： Material Polymers Metals Electronics Acid Added for Digestion HNO3,HCl,HF,H2O2,H3BO3 HNO3,HCl,HF HNO3,HCl,H2O2,HBF4 *2: If the result of spot test is positive, Chromium VI would be determined as detected. *THJ0285781* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410 Page 6 of 10 Number : TWNC00285781 Test Conducted (Ⅳ) Measurement Flowchart: Test for Halogen Content Reference Standard：EN 14582 Sampling/grinding or cutting Add absorbent in a combustion flask & place weighed sample in equipment Fill oxygen into calorimetric bomb Ignite then leave the bomb at room temperature Transfer the absorbent into a volumetric flask Make up with deionized water Analyzed by ion chromatography *THJ0285781* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410 Page 7 of 10 Number : TWNC00285781 Test Conducted (Ⅳ) Measurement Flowchart: Test For Phthalates Contents Reference Method: EN 14372: 2004 Sampling/grinding or cutting Weigh sample and add organic solvent By solvent extraction Concentrate the extract and make up with organic solvent Analyzed by GC-MSD *THJ0285781* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410 Page 8 of 10 Number : TWNC00285781 Test Conducted (Ⅳ) Measurement Flowchart: Test For Hexabromocyclododecane (HBCDD) Reference Standard：USEPA 3540C Sampling/grinding or cutting Weigh sample and add organic solvent By soxhlet extraction Concentrate the extract and make up with organic solvent Analyzed by GC-MSD End of Report This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a recommendation for any particular course of action. Intertek does not accept a duty of care or any other responsibility to any person other than the Client in respect of this report and only accepts liability to the Client insofar as is expressly contained in the terms and conditions governing Intertek's provision of services to you. Intertek makes no warranties or representations either express or implied with respect to this report save as provided for in those terms and conditions. We have aimed to conduct the Review on a diligent and careful basis and we do not accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by statute or otherwise, except in the event of our gross negligence or wilful misconduct. *THJ0285781* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410 Page 9 of 10 Number : TWNC00285781 Test Conducted Photo *THJ0285781* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410 Page 10 of 10 Test Report Applicant: Littelfuse Philippines Inc. LIMA Technology Center, Lipa City, Malvar, Batangas Number : TWNC00306991 Date : Apr 16, 2013 Sample Description: One (1) group of submitted samples said to be : Part Description : Black Ink Part Number : 425809 Date Sample Received : Apr 10, 2013 Date Test Started : Apr 11, 2013 Test Conducted : As requested by the applicant, for details please refer to attached pages. Authorized by: On Behalf of Intertek Testing Services Taiwan Limited K. Y. Liang Director *THJ0306991* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C. 全國公證檢驗股份有限公司 11492 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410 Page 1 of 10 Number : TWNC00306991 Test Conducted (Ⅰ) Test Result Summary: Result Test Item Unit Test Method Black paste RL Heavy Metal ND 2 ND 2 ND 2 ND 1 ppm ND 5 ppm ND 5 ppm ND 5 ND 5 ND 5 ND 5 ND 5 ppm ND 5 ppm ND 5 ppm ND 5 Cadmium (Cd) Content ppm Lead (Pb) Content ppm Mercury (Hg) Content ppm Chromium VI (Cr6+) Content ppm Polybrominated Biphenyls (PBBs) Monobrominated Biphenyls (MonoBB) Dibrominated Biphenyls (DiBB) Tribrominated Biphenyls (TriBB) Tetrabrominated Biphenyls (TetraBB) Pentabrominated Biphenyls (PentaBB) Hexabrominated Biphenyls (HexaBB) Heptabrominated Biphenyls (HeptaBB) Octabrominated Biphenyls (OctaBB) Nonabrominated Biphenyls (NonaBB) Decabrominated Biphenyl (DecaBB) With reference to IEC 62321: 2008, by microwave digestion and determined by ICP-OES. With reference to IEC 62321: 2008, by microwave digestion and determined by ICP-OES. With reference to IEC 62321: 2008, by microwave digestion and determined by ICP-OES. With reference to IEC 62321: 2008, by alkaline digestion and determined by UV-Vis Spectrophotometer. ppm ppm ppm ppm With reference to IEC 62321: 2008, by solvent extraction and determined by GC-MS and further HPLC-DAD confirmation when necessary. *THJ0306991* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C. 全國公證檢驗股份有限公司 11492 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410 Page 2 of 10 Number : TWNC00306991 Test Conducted Result Test Item Unit Polybrominated Diphenyl Ethers (PBDEs) Monobrominated Diphenyl Ethers ppm (MonoBDE) Dibrominated Diphenyl Ethers ppm (DiBDE) Tribrominated Diphenyl Ethers ppm (TriBDE) Tetrabrominated Diphenyl ppm Ethers (TetraBDE) Pentabrominated Diphenyl ppm Ethers (PentaBDE) Hexabrominated Diphenyl Ethers ppm (HexaBDE) Heptabrominated Diphenyl ppm Ethers (HeptaBDE) Octabrominated Diphenyl Ethers ppm (OctaBDE) Nonabrominated Diphenyl Ethers ppm (NonaBDE) Decabrominated Diphenyl Ether ppm (DecaBDE) Phthalates Di(2-ethylhexyl) Phthalate ppm (DEHP) Dibutyl Phthalate (DBP) ppm Benzyl Butyl Phthalate (BBP) ppm Halogen Content Fluorine (F) ppm Chlorine (Cl) ppm Bromine (Br) ppm Iodine (I) ppm Others Hexabromo cyclododecane (HBCDD) ppm Test Method Black paste With reference to IEC 62321: 2008, by solvent extraction and determined by GC-MS and further HPLC-DAD confirmation when necessary. RL ND 5 ND 5 ND 5 ND 5 ND 5 ND 5 ND 5 ND 5 ND 5 ND 5 With reference to EN 14372: 2004, by solvent extraction and determined by GC-MS. ND 50 ND ND 50 50 With reference to EN 14582:2007 by calorimetric bomb with oxygen and determined by Ion Chromatograph. ND ND ND ND 50 50 50 50 With reference to USEPA 3540C, by solvent extraction and determined by GC-MS. ND 10 *THJ0306991* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C. 全國公證檢驗股份有限公司 11492 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410 Page 3 of 10 Number : TWNC00306991 Test Conducted Remarks: ppm ND RL = parts per million based on wet weight of tested sample = mg/kg = Not detected = Reporting Limit, Quantitation limit of analyte in sample Responsibility of Chemist: Date Sample Received Test Period Kevin Liu/ Irene Chiou/ Vico Lin : Apr 10, 2013 : Apr 11, 2013 to Apr 15, 2013 (Ⅱ) Limit: RoHS Limit Restricted Substances Cadmium (Cd) content Lead (Pb) content Mercury (Hg) content Chromium VI (Cr6+) content Polybrominated Biphenyls (PBBs) Polybrominated Diphenyl Ehters (PBDEs) Limits 0.01% (100ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) The above limits were quoted from Annex II of 2011/65/EU for homogeneous material. *THJ0306991* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C. 全國公證檢驗股份有限公司 11492 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410 Page 4 of 10 Number : TWNC00306991 Test Conducted (Ⅲ) Measurement Flowchart: Test for Cd/Pb/Hg/Chromium (VI)/PBBS/PBDES Contents Reference Standard: IEC 62321 edition 1.0:2008 Sample preparation For non-metal part For metal part Take sample and immerse into Aqua Regia, start to strip plating layer Stop the stripping procedure upon color change completely Take the Aqua solution as plating component and stripped body as substrate component PBBs/PBDEs Weigh sample and add organic solvent By Soxhlet extraction or Solvent extraction Concentrate the extract and make up with organic solvent Analyzed by GC-MSD Cr 6+ Substrate Cd/Pb/Hg Weigh sample and add alkaline solution For different material, digest the sample with *1 appropriate acid Plating Cr 6+ By spot test Definite temp. extraction Cool and filter the extract Confirm the tested samples are totally dissolved Negative *2 Get 50cm2 sample Make up with deionized water By boiling water extraction Analyzed by ICP-OES Make up with deionized water and add diphenyl-carbazide solution Analyzed by UV-VIS *THJ0306991* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C. 全國公證檢驗股份有限公司 11492 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410 Page 5 of 10 Number : TWNC00306991 Test Conducted Remarks: *1: List of Appropriate Acid： Material Polymers Metals Electronics Acid Added for Digestion HNO3,HCl,HF,H2O2,H3BO3 HNO3,HCl,HF HNO3,HCl,H2O2,HBF4 *2: If the result of spot test is positive, Chromium VI would be determined as detected. *THJ0306991* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C. 全國公證檢驗股份有限公司 11492 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410 Page 6 of 10 Number : TWNC00306991 Test Conducted Test for Halogen Content Reference Standard：EN 14582 Sampling/grinding or cutting Add absorbent in a combustion flask & place weighed sample in equipment Fill oxygen into calorimetric bomb Ignite then leave the bomb at room temperature Transfer the absorbent into a volumetric flask Make up with deionized water Analyzed by ion chromatography *THJ0306991* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C. 全國公證檢驗股份有限公司 11492 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410 Page 7 of 10 Number : TWNC00306991 Test Conducted Test For Phthalates Contents Reference Method: EN 14372: 2004 Sampling/grinding or cutting Weigh sample and add organic solvent By solvent extraction Concentrate the extract and make up with organic solvent Analyzed by GC-MSD *THJ0306991* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C. 全國公證檢驗股份有限公司 11492 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410 Page 8 of 10 Number : TWNC00306991 Test Conducted Test For Hexabromocyclododecane (HBCDD) Reference Standard：USEPA 3540C Sampling/grinding or cutting Weigh sample and add organic solvent By soxhlet extraction Concentrate the extract and make up with organic solvent Analyzed by GC-MSD End of Report This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a recommendation for any particular course of action. Intertek does not accept a duty of care or any other responsibility to any person other than the Client in respect of this report and only accepts liability to the Client insofar as is expressly contained in the terms and conditions governing Intertek's provision of services to you. Intertek makes no warranties or representations either express or implied with respect to this report save as provided for in those terms and conditions. We have aimed to conduct the Review on a diligent and careful basis and we do not accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by statute or otherwise, except in the event of our gross negligence or wilful misconduct. *THJ0306991* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C. 全國公證檢驗股份有限公司 11492 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410 Page 9 of 10 Number : TWNC00306991 Test Conducted Photo *THJ0306991* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C. 全國公證檢驗股份有限公司 11492 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410 Page 10 of 10