ICPTest_451L_02 04 2013 pdf

ICP Test Report Certification Packet
Company name :
Littelfuse, Inc.
Product Series:
Nano2 Fuse - FA
Product #:
451xxxL Series
Issue Date:
February 4, 2013
It is hereby certified by Littelfuse, Inc. that there is neither RoHS (EU Directive 2002/95/EC,
2011/65/EU)-restricted substance nor such use, for materials to be used for unit parts, for
packing/packaging materials, and for additives and the like in the manufacturing processes.
In addition, it is hereby reported to you that the parts and sub-materials, the materials to be used
for unit parts, the packing/packaging materials, and the additives and the like in the manufacturing
processes, are all composed of the following components.
Issued by:
<Global EHS Engineer>
(1) Parts, sub-materials and unit parts
This document covers the Nano2 Fuse - FA RoHS-Compliant series products
manufactured by Littelfuse, Inc.
＜ Raw Materials Used
Please see Table 1
(2) The ICP data on all measurable substances
Please see appropriate pages as identifed in Table 1
Remarks：
Pb (lead) contained in the high temperature melting solder > 85% and is categorized as
exempt under section 7a of the RoHS Annex.
Form 585-047 Rev. A
1
2/21/06
Table 1: List of Raw Materials covered by this report
Total Parts
1
2
3
4
5
6
7
8
Raw Material Part Number
910-275
Frequenta C221 (909-434)
082xxx
082xxx
11-0803 (497xxx)
11-0894 (497xxx)
692321
425809
Raw Material Description
Cap
Body – Ceramic Tube
Element- 5% by weight Ag clad Cu
Element-2% by weight Ag clad Cu
Element - Ni42Fe58MCuMAg5%
Element-Ni36Fe64Mag7%
Solder
Ink-Black
2
Page(s)
3-8
9-37
38-42
43-47
48-52
53-58
59-64
65-73
Test Report
Applicant:
Number : TWNC00285774
Littelfuse Philippines Inc.
LIMA Technology Center, Lipa City,
Malvar, Batangas
Date
: Nov 19, 2012
Sample Description:
One (1) group of submitted samples said to be :
Part Description
: Cap
Part Number
: 910-275
Date Sample Received
: Nov 12, 2012
Date Test Started
: Nov 13, 2012
Test Conducted :
As requested by the applicant, for details please refer to attached pages.
Authorized By:
On Behalf Of Intertek Testing Services
Taiwan Limited
K. Y. Liang
Director
*THJ0285774*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410
Page 1 of 6
Number : TWNC00285774
Test Conducted
(Ⅰ) Test Result Summary :
Result (ppm)
(1)
(2)
Test Item
Heavy Metal
Cadmium (Cd) content
Lead (Pb) content
Mercury (Hg) content
Chromium VI (Cr6+) content (mg/kg with 50cm2)
ND
ND
ND
Negative
(< 0.02)
(#)
ND
ND
ND
Negative
(< 0.02)
(#)
Remarks: ppm = Parts per million based on weight of tested sample = mg/kg
ND = Not detected
<
= Less than
mg/kg with 50cm2 = milligram per kilogram with 50 square centimetre
Negative = A negative test result indicated positive observation
was not found at the time of Test.
#
= Due to the insufficient sample area, reduced total sample
surface of 25 cm2 was used and the dilution factor was
adjusted accordingly.
Tested Components
(1) Coppery metal base material
(2) Golden plating layer
Responsibility of Chemist : Irene Chiou / Kevin Liu
Date Sample Received
Test Period
: Nov 12, 2012
: Nov 13, 2012 to Nov 16, 2012
(Ⅱ) RoHS Limits:
Restricted Substances
Cadmium (Cd) Content
Lead (Pb) Content
Mercury (Hg) Content
Chromium VI (Cr6+) Content
Limits
0.01% (100ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
The above limits were quoted from Annex II of 2011/65/EU for homogeneous
material.
*THJ0285774*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410
Page 2 of 6
Number : TWNC00285774
Test Conducted
(Ⅲ) Test Method:
Test Item
Cadmium (Cd)
content
Lead (Pb) content
Mercury (Hg)
content
Chromium VI (Cr6+)
content
Test Method
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 7, by microwave
digestion until the tested samples are
totally dissolved and determined by
ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in annex B, by boiling water
extraction and determined by UV-Vis
Spectrophotometer.
Reporting Limit
2 ppm
2 ppm
2 ppm
0.02
mg/kg with 50cm2
Remark: Reporting limit = Quantitation limit of analyte in sample
*THJ0285774*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410
Page 3 of 6
Number : TWNC00285774
Test Conducted
(Ⅳ) Measurement Flowchart:
Test For Cd/Pb/Hg/Chromium (VI)
Reference Standard：IEC 62321 edition 1.0:2008
Sample preparation
Take sample and immerse into Aqua Regia, start to strip plating layer
Stop the stripping procedure upon color change completely
Take the Aqua solution as plating component and stripped body as substrate component
Cd/Pb/Hg
Substrate
Plating
For different
material, digest
the sample with
*1
appropriate acid
Cr
6+
By spot test
Confirm the tested
samples are
totally dissolved
Make up with
deionized water
Negative
*2
Get 50cm2 sample
By boiling water
extraction
Analyzed by ICP-OES
Make up with deionized water and add
diphenyl-carbazide solution
Analyzed by UV-VIS
*THJ0285774*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410
Page 4 of 6
Number : TWNC00285774
Test Conducted
Remarks:
*1: List Of Appropriate Acid：
Material
Polymers
Metals
Electronics
Acid Added For Digestion
HNO3,HCl,HF,H2O2,H3BO3
HNO3,HCl,HF
HNO3,HCl,H2O2,HBF4
*2: If the result of spot test is positive, Chromium VI would be determined as detected.
End of Report
This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a
recommendation for any particular course of action. Intertek does not accept a duty of care or any other responsibility to any person other than
the Client in respect of this report and only accepts liability to the Client insofar as is expressly contained in the terms and conditions
governing Intertek's provision of services to you. Intertek makes no warranties or representations either express or implied with respect to this
report save as provided for in those terms and conditions. We have aimed to conduct the Review on a diligent and careful basis and we do not
accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by statute or otherwise, except in
the event of our gross negligence or wilful misconduct.
*THJ0285774*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410
Page 5 of 6
Number : TWNC00285774
Test Conducted
Photo
*THJ0285774*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410
Page 6 of 6
Signature
FOTQUE
Please
Test Report
No.: CE/2013/13196Dale:2013101122P a g e : 1 o f 2 9
GMBH
CERAMTEC
5, 91207LAUF
MULTIFUNKTIONSKEMMIK,LUITPOLDSTRABE'1
GESCHAFTSBEREICH
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Thefollowingsample(3)was/weresubmittedand idontifiedby/onbehalfofthe clientas:
SampleDescription
Styldltem No.
Date
sampleReceiving
TestingPeriod
CERAIVIC
C221
FREOUENTA
2013t1t14
122
2013t1| 14 10 2013tO1
Test Result(s)
Pleasereferto nextpage(s).
Conclusion
thetestresultsof Cadmium'Lead'
samples,
Ba6edontheperfomedtestson submitted
PBDES
complywiththe limitsas setby
PBBS
and
Cr(Vl),
Hexavalent
Chromium
Mercury,
200295/EC
ll;
recasting
Annex
RoHSDirective
2011/65/Eu
(Nw4p
[Ner;]F
cryriits/rif'"i
'r' {li f {'}itgi!
Test Report
No.: CE/201t'13196 Date: 2013101122Page:2of 29
CERAMTECGMBH
15, 91207 LAUF
I\IULTIFUNKTIONSKERAMIK,LUITPOLDSTRABE
GESCHAFTSBEREICH
Test R€ultla)
PART I.]AME No.1
:
CREAMCERAMIC
Tst ltem(s)
Cadmium(Cd)
Lead(Pb)
(Hg)
Mercury
Cr(Vl)
Chromium
Hexavalent
(cAs
BBP(Benzylbutylphthalate)
No.:8568-7)
DEHP(Di-(2-ethylhexyl)
phthalate)
(CASNo.:1'1ru1-7)
DIDP (Di-isodecylphthalate)(CAS
No.:26761.40-0)
DINP(Di-isononylphthalate)(cAs
No.:28553-12-0)
DNOP(Di-n-oc'tylphthalate)(CAS
No.:117-84-0)
DBP (Dibutylphthalate)(CAS No.:
U-74-2)
Perfluorooctanesulfonates
(PFOS-Acid,
MetalSalt,Amide)
PFOA (CAS No.. 335€7-1)
Unit
Moihod
to IEC62321:2008and
mg/Kg Withreference
perfomedby ICP-AES.
to IEC62321;2008and
mg/Kg Withreference
pedormedby ICP-AES.
to IEC62321:2008and
mg/Kg Withreference
perfomedby lCPdES.
to IEC62321:2008and
mgik9 Vvitfrreierence
MDL
Result
No.'l
Limit
2
n.d.
100
2
n.d.
1000
2
n.o.
1000
2
n.d.
1000
pedormed
byUV-VIS.
to EN 14372.Analysis
Withrcference
wa6pertormedby GC/[is.
to EN 14372.Analysis
%
Withr€ference
wEsperfomedby GC/MS.
to EN 14372.Analysis
vvithreference
wEsperformedby GC/MS.
o/.
to EN 14372.Analysis
Withreference
wEsperfomedby GC/MS.
to EN 14372.Analysis
Withreference
perfomed
by GC/MS.
wEs
to EN 14372.Analysis
Withreference
%
wEsperfomedbYGC/MS.
mg/Kg Wi-threferenceto Us EPA3550C:
bY
waspedormed
2007.An€lysis
LC/MS.
mg/kg Withreferenceto US EPA3550C:
2007.AnalysiswasPerformedbY
LCiMS.
o/o
to USEPA3540C
(PCBS) mdKo Withreference
Biphenyls
Polychl''inated
bY
w?sPerfomed
Analysis
method.
(CASNo.:133S36-3)
0.003
n.d.
0.003
n.o.
0.0!
n.o.
0.01
n.d.
0.003
n-o.
0.003
n.d.
10
n-d.
10
n.d.
0.5
n.d.
GC/MS.
$ffiw,fiffimt$uffidiffir.
N€wtrtsicirtdMn/ri : i
6 rr tl;! t i-r1331i
Test Report
No.: CE/2013/13'196Dale,2013101122P a g e : 3 o f 2 9
CERAMTEC
GMBH
15, 91207LAUF
MULTIFUNKTIONSKERAI'IK,LUITPOLDSTRABE
GESCHAFTSBEREICH
Test ltem(s)
Unlt
lrethod
TIDL
0.5
mg/Kg With referenceto US EPA3540C
method.Analysiswasperfodnedby
GC/MS,
5
mg/Kg With referenceto uS EPA3$0C
Polychlorinated
Naphthalene
method.Analysiswasperformedby
(PCN6)
GC/MS.
'100
mSikS Withreferenceto US EPA3g0C
Alkanes,
C10-13,chloro(Short
lr€s performed
by
methodAnalysis
ChainChlorinatedParaffins)(CAS
GC/IVS.
No.:85535-84-8)
Analysiswaspertormedby FTIRand
PVC
FLAMETesT,
to ISO17226-112008). 3
(CASNo.:50{0-0) mg/Kg Withreference
Formaldehyde
Anaiysiswasperformedby HPLC/DAD.
Terphenyl6
Polychlorinated
(PCTS)
Result
No.1
n.o,
n.d.
n.d.
Negative
n.o.
0.5
n.d.
0.5
n.d.
tetrachlorodiPhenYl mg/kg Withreferenceto Us EPA8270D
Monomethyl
wasPerfomedbY
Analysis
method.
methane(Ugilec14'1)
GC/MS.
Halogon
0.5
n.d.
(F) (CAS No.:
Halogen-Fluorine
'14762-94€)
mlyKg
50
n,d.
(Cl)(cAs No.:
Halogen-Chlorine
22537-15-1)
(Br)(CASNo.:
Halogen-Bromine
100€7-32-2'
mgKg
50
n.d.
With referenceto BS EN 14582:2007
mdkg Analysiswasperformedby lC.
50
n.d.
Halogenlodine(l) (CAS No.:
'143€'2444\
m!/Kg
50
n.d.
0.03
n.d.
n.o.
Monomethyl
dibromodipheny'
methane(DBBT)
Monomethyl
dichlorodiphenyl
methane(Ugilec12'l)
to USEPA8270D
mg/Kg Withreference
wasperfonned
by
method.
Analysis
GC/MS.
to USEPA8270D
mg/kg Withreference
Analysis
wEsperfomedbY
method.
GC/MS.
Organic-lincompound6
TdbutylTin(TBT)
(TphT)
TdphenylTin
mg/kg With referenceto DIN38407-13.
mg/Kg AnalysiswEsperfomedbYGC/FPD
r, w! cius Rd,N4 riird idsrdP'(
0.03
!"rirrrtGlqi
Limit
Test Report
No.: CEl2013/13196Dale:2013101122Page:4 of 29
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GMBH
CERAMTEC
15,91207LAUF
MULTIFUNKTIONSKERAIIIK,LUITPOLDSTMBE
GESCHAFTSBEREICH
Test ltem(6)
Unit
Asbe€toa
Adinolite(CASNo.:77536€6-4)
(CASNo.:12172-73-5)
Amosite
(CASNo.:77536€7Anthophyllite
o/.
(CASNo.:1200'l-29-5)
Chrysotile
Crocidolite(CASNo.: 12OOl2A4t
(CAsNo.r2536€8€)
Tremolite
AZO
%
o/o
oa
Mothod
MDL
Negative
Negative
Negative
To
Analysiswasperformedby GC/MS.
3):44HLORO-O-TOLUIDINE mg/Kg With referenceto LFGB82.02-2.
Analysiswasperformedby GC/l!lS.
(CASNo.:95$9-2)
to LFGB82.02-2.
(cAs
mg/kg Withreference
4):2-NAPHTHYIAMINE
performed
bYGC/MS.
was
Analysis
No.:91-594)
(CAS mgftg Withreferenceto LFGB82.02-2.
5):O-AMINOAZOTOLUENE
Analysis
wasperfomedby GC/MS.
No.r97-56-3)
to LFGB82.02-2.
mg/kg Withreference
6):2-AMINO-4-NITROTOLUENE
'rias
p€rformed
by GC/MS.
Analysis
(CASNo.:99-55-8)
(CASNo. mgKg With referenceto LFGB82.02-2.
7): PCHLOROANILINE
'10647-8)
bYGC/MS.
wasperformed
Analysis
(CAS mg/Kg With referenceto LFGB82.02-2+ 2,4-D|AMTNOANISOLE
Analy6iswas performedby GC/MS.
No-:615-054)
to LFGB82.02-2.
mg/Kg Withreference
9r:4,4'performed
bYGC/IIS.
was
Analysis
DIAMINODIPHENYLMETHANE
(CASNo.:101-77-9)
1O)..3,3!DtCHLOROBENZIDINEmlyKg With referenceto LFGB82.02-2.
wasperfomedbYGC/MS.
Analysis
(CASNo.;9'l-94-1)
mgikg uvitlrraferenceto LFGB82.02-2
1'1):3,3'-DIMETHOXYBENZIDINE
AnalysiswasperfomedbYGC/MS
(CASNo.:119-90-4)
12):3,3-DIMETHYLBENZIDINEmg/kg With referenceto LFGB82.02_2
AnalysiswasperformedbYGC/MS(CASNo.:119-93-7)
rxwu.hune-NewhiFrrndu5rirtu'
No.l
Negative
Negative
Negative
I6
With refercnceto EPA600/R-93'/1
method.Analy6iswasperformedby
(SlV),Dispe6ion
StereoMicroscope
Lightl\ricroscope
Staining
Poladzed
(DS-PLM)andX-€y Diffraction
(XRD).
Spectrometer
(CAS No.: mg/kg With referenceto LFGB82.02-2.
1): ,I-AMINODIPHENYL
Analysisw€sperformedby GC/MS.
9267-1)
to LFGB82.02-2.
(CASNo.:92-87- mlyKg Withreference
2): BENZIDINE
Re3ult
3
n.d-
3
n.d.
3
n.d.
3
n.d.
3
n.d.
n.o.
n.d.
3
n.d.
3
n.d.
3
n-o.
3
n.d.
3
n.d.
L,iii'rr"'nfirr\'t
Limit
TestReport
No.: CE/20f31 3196 Dale: 2013101122Page: 5 of 29
rrl[ttttllltl
CERAMTECGMBH
15, 91207 LAUF
MULTIFUNKTIONSKERAMIK,LUITPOLDSTRABE
GESCI-IAFTSBEREICH
To6tltem(s)
Unit
ethod
'13)r3,3'-DIMETHYL-4,4'to LFGB82.02-2.
mSikS with reference
,a/as
performed
by GC/MS.
Analysis
DIAI'INODIPHENYLMETFIANE
(CASNo.:838€84)
to LFGB82-02-2.
(2-METHOXY-mgKg Withreference
14):P-CRESIDINE
(CASNo.:
Analysis'r/asperformedby GC/MS.
s-METHYLANILINE)
12'+171-E'
(2to LFGB82.02-2.
mgKg Withreference
15):4,4'-METHYLENE-B|Sperformed
bYGC/MS.
was
(CAsNo.l
Analysis
CHLOROANILINE)
101-'t+4\
to LFGB82.02-2.
(CAS
mgKg Withreference
16) 4,4'-OXYDtANILINE
by GC/MS.
waspedormed
Analysis
No. 101€04)
'!7):4,4'-THIODANILINE(CAS
mg/Kg with refe€nceto LFGB82.02-2.
Analysiswaspertormedby GC/l!lS.
No.:13945-1)
to LFGB82.02-2.
(CASNo.:95- mg/Kg Withreference
18):O-TOLUIDINE
wasperfomedby GC/MS.
Analysi6
534)
to LFGB82.02-2.
19} 2,+TOLUYLENEDIAMINE mg/Kg with reference
prfomed
by GC/MS.
wEs
Analy6is
(CASNo.:95€G7)
to LFGB82.02-2.
20)r2,4,5-TRIMETHYLANILINEmg/kg Withreference
perfomed
bYGC/MS.
was
Analysis
(CASNo.:137-17-7)
to LFGB82.02-2.
(cASNo.:90- mgftg Withreference
-): o+NrsrDlNE
AnalysiswEsperfomedbYGC/MS04{)
to LFGB82.02-2.
mgKg Withreference
22F-AMINOAZOBENZENE
perfofmed
bYGC/MS.
was
An€lysis
(CASNo.:60{9-3)
(CASNo.:95- mgftg Withreferenceto LFGB82.02-2
23):2,4-xYLlD|NE
AnalysiswasperformedbYGC/MS
68-1)
to LFGB8202-2
(CASNo.:87- mgag Withreference
24):2,6-XYLIDINE
perfomed
bYGC/MS
wa6
Analysis
62-7)
CFC'3(Chlo|ofluorocaibons)
GroupI
luoroca6on-11 (CASNo.: mgKg With referenceto US EPA5021
Chlo,rof
bY
wasPerform€d
Analysis
method.
756+4)
GC/MS.
mg/Kg With referenceto US EPA502'1
uorocabonl2 (CASNo.I
Chlorofl
method.AnalysiswasPerfomedbY
75-71-8)
GC/MS.
MDL
R€oult
No.l
3
n.d.
3
n.o.
3
n.d.
3
n.d.
3
n.d.
3
n.d.
3
n.d.
3
n.d.
3
n.d.
3
n.o.
3
n,o.
3
n.d.
I
n.d.
Limit
n.d.
ffi,ffiq*ffitrffit$gwl*ffi##f
Test Report
No.:CE/2013'/13196 Oale|2013101122 Page: 6 of 29
r]l[ttti[ltl.ll
GMBH
CERAMTEC
15' 91207LAUF
IVULTIFUNKTIONSKERAMIK,LUITPOLDSTRABE
GESCHAFTSBEREICH
Test ltem(s)
13 (CASNo.:
Chlorofluorocarbon-1
76-13-1)
Method
Unit
mg/Kg With referenceto Us EPA5021
method.AnalysiswEsPerfomedbY
GC/MS.
14(CASNo.: mg/kg With referenceto US EPA5021
Chloroftuorocarbon-1
meihod.AnalysiswEsPerfomedbY
76-14-2)
GC/MS.
15(CASNo.: mg/Kg With refefenceto US EPA5021
luoroca6on-1
Chlorof
method.AnalysiswasPerfom€dbY
76-15-3)
GC/MS.
Grouplll
3 (CASNo.:
Chk'rofiuorocarbon-1
75-7241
(CASNo l
Chtorofluorocarbon-1'11
354-s&3)
'12 (CASNo.:
Chlorofluorocarbon-1
76-12-O)
1 (CASNo :
Chlorofluoroca6on-21
422-74.6]
12 (CASNo.:
Chlorofluorocarbon-2
3182-m-1)
3 (cAs No
Chlorofluorocarbon-21
2354-06-5)
(CASNo.
Chlorofluorocadon-214
2925931-0)
(CASNo:
Chlorofluorocarbon-21s
425943-2)
to us EPA5021
mgftg vvithreference
bY
wasPerformed
Analysis
method.
GC/MS.
to us EPA5021
mg/kg with reference
bY
wE5perfomed
method.
Analysis
GC/MS.
MDL
'I
I'lo.l
n.d.
1
n.d-
1
n.d.
1
n.d.
1
n.d.
n.d.
mg/Kg With referenceto US EPA5021
method.AnalysiswasperfomedbY
GC/MS.
to uS EPA5021
m!/Kg Withreference
bY
wasPerformed
Analysis
method.
GC/MS,
to us EPA5021
mg/Kg vvithreference
Result
n.d.
1
n.d.
1
n-d.
1
n.d.
wasPedomedbY
Analysis
method.
cc/Ms.
m9K9 Wth referenceto US EPA5021
method.AnalysiswasPerformedbY
GC/MS.
mg/Kg With referenceto US EPA5021
method.Analysi6wasPedormedbY
GC/MS.
to USEPA502't
mg/kg Withreference
n.d.
bY
wasPerformed
Analysis
method.
GC/MS.
L .!.,iJd;i1li+n-qj
Limit
Test Report
No. : CE/2013/13 196
Date: 2013101122Page: 7 of 29
rtl| rIllr]llllllll
CEMMTEC GMBH
15' 91207 tAUF
MULTIFUNKTIONSKERAMIK,LUITPOLDSTRABE
GESCHAFTSBEREICH
Test ltom(s)
Mothod
Unit
(CASNo.: mg/Kg With referenc€to US EPA5021
luorocabon-2l6
Chlorof
method.AnalysiswasperfomedbY
661-97-2)
GC/MS.
(CASNo.: mgKg With referenceto tJSEPA5021
luoroca6on-217
Chlorcf
method.AnalysiswasPerfornedbY
42246-6\
GC/MS.
MDL
1
No.l
n.d.
1
n.d.
HCFC8
(Hyd rochlo.ofl uorocarbons)
(CASNo.:7543-4)
HCFC-21
(CASNo.:75454)
HCFC-22
R66ult
n.d.
mg/Kg With referenceto US EPA5021
bY
wasPerformed
Analysis
method.
GC/MS.
mg/Kg With referenceto US EPA5021
by
method.AnalysiswasperforYned
n.d.
cc/Ms.
l'lCFG31 (CASNo.: 5S3-7G4)
(CASNo.:354-14-3)
HCFC-121
(CASNo.:354-21-2)
HCFC-122
mgftg With reforenceto US EPA5021
method.Analysisw€sPerformedbY
GC/MS.
mg/Kg With referenceto US EPA5021
method.AnalysiswasPertormedbY
GC/MS.
to us EPA5021
mg/kg Witlrreference
1
n.o,
1
n.d.
1
n.d.
bY
wasPerfomecl
Analysis
method.
GC/MS.
n.d.
(cnsNo.:sos-eg-z) mg/K9 Wl[referenceto us EPn5o2t
Fierc-tzs
bY
wasPerformed
Analysis
method.
GC/MS.
(CASNo.:2837€9-0) mgKg With referenceto us EPA5021
FieFC-124
pertormed
by
$/as
Analysis
methodGC/MS.
to US EPA5021
trCf:i3T@SI6,,55r-tEi- mg/Kg With reference
wa6PerformedbY
Analysis
method.
GC/MS.
to USEPA5021
mg/Kg Wiihreference
-cFc-r32b(cAsNo.:164s-08-7)
bY
wasPerformed
Analysis
method.
GC/MS.
gffiffiffi
ri$r,iL1Hl];4'
1
n.d.
'I
n.d.
1
n.o.
Limit
TestReport
No.: CE2013/13196 Dale:2013J01122Page: 8 of 29
IlflI|rr][tlllll
CERAMTEC
GMBH
15, 91207LAUF
MULTIFUNKTIONSKERAMIK,LUITPOLDSTRABE
GESCHAFTSBEREICH
T€t lt.m(s)
(CASNo.:75-88-7)
HCFC-'133a
MDL
Method
Unit
mgKg With r€ferenceto US EPA5021
method.Analysiswaspedomed by
GC/MS.
HCFCl4lb (CASNo.:171740€) mlyKg With referenceto US EPA5021
method.AnalysiswasperformedbY
GC/MS.
mgKg with referenceto tjs EPA5021
HCFC-142b (CAS No.: 7ffi8-3)
method.AnalysiswasperformedbY
GC/MS.
HCFC221(CAsNo.r422-26-4) m9Kg wth referenceto Us EPA5021
method.AnalysiswasPerformedbY
GCA,rS.
(CASNo.:422-491)
mg/kg With refer€nceto US EPA5021
HCFC-222
by
wasperformed
Analysis
method.
GC/MS.
(CASNo.:422-526)
mg/Kg With referenceto US EPA5021
HCFC-223
method.AnalysiswasPerformedbY
GC/MS.
HCFG224(CASNo.i422-54-8) mgKg Wth referenceto US EPA5021
method.AnalysiswasPertormedbY
Result
No.l
1
n.d.
1
n.d.
1
n.d.
I
n.d.
1
n_o,
Llmit
n.d.
n.d.
cc/Ms.
(CASNo.:422-56-0) mg/kg With referenceto US EPA5021
HCFC-22sca
method.AnalysiswEsPerformedbY
GC/MS.
HCFG22scb(CASNo.:507-55-1) mg/Kg With referenceto US EPA5021
rnethod.Analysiswasperformedby
GC/MS.
mgKg Wth referenceto US EPA5021
(cAS No.:431-87€)
HCFC-226
method.Analysis$rasperformedby
GC/MS.
(CASNo.:421-94-3) msyKg With referenceto uS EPA5021
HCFC-231
bY
wasPerformed
Analysis
method.
GC/MS.
US EPA5021
EdFe'fidsxo-:?60-:3CE mg/Kg Vvithreferenceto was
method.Analysis
PerformedbY
GC/MS.
1
n.d-
I
n.o.
1
n.d.
n.d.
1
n.d.
ffii'*r-ffiffiffitrffig-#rffi
':irrr!r.rt1!r1riF'!a
I
r+e610?r,qrr 4s6o1rerr
ws+M
-,---
.-
Test Report
No.:CE2013/13196D are:2013101n2P a g e : 9 o f 2 9
tf]tt|al]
CERAMTEC
GMBH
15,91207LAUF
MULTIFUNKTIONSKERAMIK,LUITPOLDSTRABE
GESCHAFTSBEREICH
Test ltem(s)
Unit
f,lethod
(CASNo.:7'125-84-0) mgitg With roferenceto US EPA5021
HCFC-233
method.Analysisurasperformedby
GC/MS.
(CAS
With
referenceto US EPA5021
425-94-5)
mg/kg
HCFC-234
No.:
method.AnalysiswaspertormedbY
GC/rUS.
to USEPA5021
mgftg Withreference
HCFC-235(CASNo.:460-92-4)
v€s performed
bY
method.
Analysis
GC/MS.
(CASNo.:666-27-3) mgikg with refer€nce
to us EPA5021
HCFC-241
MDL
Result
No.1
n.d.
n.d.
'I
n.d.
I
n.d.
I
n.d.
1
n.d.
bY
wasPedormed
method.
Analysis
GC/MS.
(CASNo.:42141-0)
HCFC-251
mgikg With referenceto US EPA502'1
method.AnalysiswasperformedbY
GC/MS.
mg/kg With referenc€to US EPA502't
Analysis
wasperfomedbY
method.
GC/MS.
mgKg With referenceto US EPA5021
bY
wasPerformed
Analy6is
method.
GC/l,lS.
to USEPA5021
mg/kg Vviltrreference
(CASNo.:819-00-1)
HCFC-252
mg,iKg With referenceto tJSEPA5021
(CASNo.:460€3-9)
HCFC-242
(CASNo.:460-69-5)
HCFC-243
HCFC-244
(CASNo.:460-35-5)
HCFC-253
HCFC-261(CASNo.:42G97-3)
N-;Ain {s)trCFdt6-tGAs
ffi
n.d.
n,o.
bY
wasPerformed
Analysis
method.
GC/MS.
bY
wasPerformed
Analysis
method.
GC/MS.
mg/Kg With referenceto uS EPA5021
bY
wasPerlormed
Analysis
methodGC/MS.
m9Kg With referenceto US EPA5021
bY
wasPerformed
Analysis
method.
GC/MS.
referenceto US EPA5021
With
m9Kg
bY
method.Analy6iswasPerfoamed
GC/MS.
ix4itir.lt
|tiri
1
n.d.
1
n.d.
,l
n.d.
n.d.
llllll
Limlt
TestReport
No.: CE2013'13196 Oanet 2913101122Paoe: 10of 29
CERAMTEC
GMBH
GESCHAFTSBEREICH
MULTIFUNKNONSKERAMIK.LUITPOLDSTRABE
15.91207LAUF
Testltem(s)
(CASNo.:43G55-7)
HCFC-271
Unit
Method
I'DL
mgKg With referenceto US EPA5021
method.
Analysis
wEsperfomedby
GC/MS.
Halona
(CASNo.:353*59-3) mSikg Wathreferenceto Us EPA502'1
Halon-1211
(CASNo.:75$!8)
Halon-1301
mgftg method.Analysiswasperformedby
(CAS
Halon-2402
No.: 124-73-2) mg/Kg GC/MS.
1
[] [ta]l[ttll|t
Rosult
No.1
n.d.
I
1
1
n.d.
mg/Kg With referenceto LJSEPA5021
method.
Analysis
wasperfomedby
GC/MS.
rngL/Kg Withreference
to USEPA5021
method.Analysiswaspertormedby
GC/MS.
mg/Kg With referenceto US EPA5021
m€thod.
Analysis
wasperformed
by
GC/tUS.
mg/kg Withreference
to USEPA5021
method.Analysiswasperformedby
GCiMS.
mg,iKg Wth referenceto US EPA5021
method.Analysiswaspertormedby
GC/MS.
mg/Kg With referenceto US EPA5021
method.Analysiswa8performedby
GC/MS.
to uS EPA5021
mg/Kg Withreference
1
n.d.
(CASNo.:
1,2,3-Trichloopropane
96-184)
(CASNo.:
1,2-Dichloroethane
107,cF2]-
n.o.
n.o.
CHCS(Chlodnate hyd.ocarbon)
(CAS
1,1,1,2-Tetrachloroethane
No.:630-20€)
'1,1
(CASNo.:
,1-Tdchloroethane
71+56)
(CAS
1,1,2,2-Tet€chloroethane
No.:7$34-5)
'1 1
(CASNo.l
, ,2-Trichloroethane
79-00-5)
(CASNo.:7$
1,1-Dichloroethane
34-3)
(CASNo.:7$
1,'1-Dichloroethene
3s4)
(CASNo.:
1,1-Dichloropropene
563-586)
n.d.
n.d.
n.d.
n.d.
1
n.d.
1
n.d.
msyKg With ref€renceto US EPA5021
method.Analysiswaspertormedby
1
n.d.
mg/kg With refe.enceto Us EPA502'1
bY
wasperformed
method.
Analysis
GC/|V]S.
I
n-d.
wasperfomed
by
method.
Analy6is
GC/MS.
cciMs.
N4laipd.tvr.iwm/ii
r ' 6 i Hil ilErit!:
Limit
TeSt
pase:ii of2s
No.:cE/2013/r3196
Date:2o13t01t22
RepOft
GERAI,IITEC
GMBH
GESCHAFTSBEREICH
MULTIFUNKTIONSKERAMIK.LUITPOLDSTRABE
15.91207LAUF
Test ltem(s)
Unit
Method
1
Result
No.t
n.o.
1
n.d.
1
n.d-
I
n.d.
I
n.d-
MDL
1,2-Dichloropropane
(CASNo.:
78€7-5)
mg/Kg With referenceto US EPA5021
method.Analysiswasperlormedby
GC/MS.
(CASNo.:
1,3-Dichloropropane
mgikS Withreference
to LJSEPA5021
't42-2E-9)
method.Analysiswa6perfomedby
GC/MS.
2,2-Dichloropropane
(CASNo.:
mg/Kg With referenceto LJSEPA5021
594-20-7)
method.Analysisw€sperformedby
GC/[rS.
L;arbontetrachloide(cAs No.:
mg/Kg With referencato US EPA502'1
methodAnalysis
wasperfomedby
GC/t\rs.
(CASNo.:75-0G3) mg/Kg With ref€renceto US EPA5021
Chloroethane
method.
Analysis
wasperfomedby
GC/[rS.
Chlorcfom(CASNo.:67€6-3)
mg/Kg With referenceto uS EPA5021
m€thod.Analysiswasperformedby
GC/MS.
(CASNo.:7,f€7- m9Kg Withreference
Chloromethane
to USEPA5021
3)
method.Analysi6wasperformedby
GC/MS.
(CAS
cis-1,2-Dichloroethene No.: mg/kg With referenceto US EPA5021
15e59-2)
method.
Analysis
wasperformed
by
GC/MS.
cis-1,3-Dichloropropene
(CASNo.; mg/Kg With referenceto US EPA5021
'10061-01-5)
method.AnalysiswEsperformedby
GC/MS.
(CASNo.:
Hexachlorobutadiene
mg/kg With referenceto US EPA5021
876&3)
method.
Analysis
wasperformed
by
GC/[rS.
Methylene
Chlodde(CASNo.:7$ mg/Kg Withreference
to uS EPA5021
method.Analysiswasperformedby
09-2)
GC/MS.
(CASNo.:127- m9Kg Wth reference
Tetrachloroethene
to USEPA5021
method.
Analysis
waspeafomed
by
184)
GC/MS.
!]l||||r]tllttltl
'|
n.d.
1
n.d.
'I
n.d.
1
n.d.
'I
n-o.
n.o,
n.d.
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I
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ano io' dcrcn'c romar dbumd
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ihelruoibin1ei!edonon|yandrlth|n$e|im1solc|ienIsfunsifaryfiecoqany!d€B5pon!bi|[ysbisc|ientandlhsdoamsnld
hngfuniomsreGinoa|''heL1
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"
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Limit
Test Report
No.:CE/2013i/13'196
Date 2O13tO1n2 paae: 12of 29
CERAMTECGMBH
GESCHAFTSBEREICH
MULTIFUNKTIONSKERAMIK,LUITPOLDSTRABE
15,91207LAUF
Testltem(s)
Unit
Method
t€ns-1,2-Dichloroe'thene
(CAS
No.:15640-5)
mdks With referenceto l-JSEPA5021
tran8.l,3-Dichloropropene
(CAS
No.:10061-02€)
mg/Kg With referenceto US EPA5021
method.
Analysis
wasperfomedby
GC/MS.
mgKg Withreference
to USEPA5021
mothod.Analysiswasperformedby
GC/MS.
mSI(S
mgftg
mgftg
mg/Kg
mg/Kg
ttl[tttl[It
r,DL
R€6ult
l{o,1
1
n.d.
1
n.d.
1
n.d-
melhod.AnalysiswEsperformedby
|l
Limit
GC/r\,ts.
Trichloroethylene
(CASNo.:7901€)
Sum ot PBBS
Monobromobiphenyl
Dibromobiphenyl
Tribromobiphenyl
Tetrabromobiphenyl
Pentabromobiphenyl
Hexabromobiphenyl
Heptabromobiphenyl
Octabromobiphenyl
Nonabromobiphenyl
Decabromobiphenyl
Sum of PBDES
Monobromodiphenyl
ether
Dibromodiphenyl
9ther
Tribromodiphenyl
ether
Tetrabaomodiphenyl
ether
ethea
Pentabromodiphenyl
Hexabromodiphenyl
ether
ether
Heptabromodiphenyl
ether
Octabromodiphenyl
ether
Nonabromodiphenyl
ether
Decabromodjphenyl
n.d.
5
5
mg/Kg
mg/Kg
n.o,
n.o,
n.d.
n.d.
n.d.
n.d-
mo/Kg
mgikg
mg/Kg
mg/Kg Withreference
to IEC62321:2008and
mgikg perfomedby GC/MS.
m9/Kg
mg/Kg
m9Kg
mg/Kg
mg/Kg
mg/kg
5
5
5
5
5
5
5
5
n.d.
n.o.
n.d.
n.d.
n.d.
n.d.
n.d.
n.d.
n.d.
n.d.
n.o.
mg/Kg
m9Kg
mg/Kg
5
5
n.d.
n.d.
n.d.
mgig
5
n.d.
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Test Report
No.: CE2013,/13196
Date: 2013t01t22Page: 13of 29
CERAMTEC
GMBH
GESCHAFTSBEREICH
MULTIFUNKTIONSKERAIVIK,LUITPOLDSTMBE'1
5, 91207LAUF
ll
tI]tIltttll
Note:
1. mg/kg= ppm;0.lwt%= 1000ppm
2. n.d.= NotDetected
3. MDL= MethodDeteclion
Limit
4. " - " = NotRegulated
5. '* = Qualitative
analysis(Nounit)
=
6. Negative Undeteclable/ Positive= Detectable
qualitative
7. Testingrangeof asbesto€
analysi6
isfromlessthan0.'10lo
to 100%.Thejudgmentcriterion:
asbestos
fibe6
beingfoundis shownas "Positive';
asbeslos
fibersnotbeingfoundis shownas "Negative',.
PFOSRofercnceInformation: POP3- (EU)7572010
Outlawing
PFOSas sub€tances
(1oppm),
products
or pr€parations
in concentrations
above0.001o,4
in semi-finished
or
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in textilesor othercoatedmaterials
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Test Report
No.: CE/201313196 Dale: 2013101122Paoe: 14ol 29
rflfltt|lItttlll
CERAMTEC
GMBH
GESCFIAFTSBEREICH
MULTIFUNKTIONSKERAI'IK,LUITPOLDSTRABE
15, 91207LAUF
1) Thesesamples
weredissolved
totallyby pre-conditioning
methodaccording
to beloa/flowchart.
( Cf' test methode)duded)
2) Nameof the peEonwhomademeasurement:
Climbg|eat
Yang
Nameof the personin chargeofmeasuremer
: TroyChang
of measuremer
cf.
SampleMeasulement
Addappropriate
amount
of digestion
reagent
Acid digestionby suitableacid
deoended on different samDl€
material (a6 below table)
Heatto appopriate
temperatureto extract
'1) AlkaliFusion
Cool, filter digestiate
throughfilter
2) HCltodissolve
SamDlel\Iaterial
Add diphenyl-carbazide
for colordevelopment
Acid
Diqestion
Aqua reqi€.HNO3.HCl,HF,H,O,
6older
Sleel,coppetaluminum,
HNO3/HF
Glass
palladium,
Gold.platinum,
cgramic Aqua reqia
Silver
Plastic
Others
measurethe absorbance
at 540 nmby UV-VIS
HNOg
H,SO1,H,O,, HNO3,HCI
Addedappropriatereagentto total
digestion
digestion
eagentandheatto 90-95C
m€terial,
addalkaline
ilotg" : (1)Fornon-metallic
pure
waterand heatto boiling
(2) Forrnetallicmatedal,add
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No.: CE/2013/13196Dale: 2013101122Page: 15of 29
1!l ||lt][tttllt
CERAI\,ITEC
GMBH
GESCHAFTSBEREICH
MULTIFUNKTIONSKERAMIK.LUITPOLDSTRABE
15. 91207LAUF
PFOA/PFOSanalyticalflow cha ot lJltrasonicoxtraction (LC/MS)prccedure
I Nameof thepe6onwhomademeasurement:
RomanWong
I Nameof lhe perconin chargeof measurement:
TroyChang
Sampleextractionby Ultrasonicextraction
(Reference
method:USEPA3550C)
Concentrate/Dilute
Ext€cled solution
*"'*
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No.: CE/2013/13'196Dale: 2013101122Pagei 16 of 29
CEMMTECGMBH
GESCHAFTSBEREICH
[,,lULTIFUNKTIONSKERAMIK,LUITPOLDSTRABE
15, 91207LAUF
FgTsanalyticalf lowchaft
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No.: CE/2013/13196DaIe: 20131O1n2 P a g e r ' 1 7 o f 2 9
CERAMTEC
GMBH
GESCHAFTSBEREICH
MULTIFUNKTIONSKERAI'IK,LUITPOLDSTMBE
15, 91207LAUF
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Nameofthepersonwhomademeasurcment:
RomanWong
Nameofthe personin charged measurement
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No.: CEl201313196 Dele:2013101122Page: 18 of 29
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CERAMTECGMBH
MULTIFUNKTIONSKERAMIK.LUITPOLDSTMBE
GESCHAFTSBEREICH
15, 91207 LAUF
PCB9analyticalflow chart
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No.:CE/201?'/13196
Dale: 2013101122Pagei 1I of 29
CEMMTECGIVBH
GESCHAFTSBEREICH
MULTIFUNfiIONSKERAMIK.LUITPOLDSTRABE
15,91207LAUF
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No.I CE2013/'13196Date| 2013101122Page| 20 ol 29
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GMBH
[/|ULTIFUNKTIONSKERAMIK.LUITPOLDSTMBE
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No.: CEl201313196 Date: 201?,101122
Paoe: 21ol 29
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CERAMTEC
GMBH
GESCHAFTSBEREICH
MULTIFUNKTIONSKERAMIK.LUITPOLDSTMBE
15.91207LAUF
Analyticalflow cha of Organic-Tin
content
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Nameofthepersonwhomademeasurem€nt:
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CERAMTECGMBH
15, 91207 LAUF
MULTIFUNKTIONSKERAMIK,LUITPOLDSTRABE
GESCI.I,AFTSBEREICH
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No.: CE201313196 Dale:2013101122Page:23of 29
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5, 9'1207LAUF
MULTIFUNKTIONSKERAMIK,LUITPOLDSTRABE'I
GESCHAFTSBEREICH
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RomanWong
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No.: CE20'1313196 Date: 2013101
122 Page: 24 ol 29
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CERAMTEC
GMBH
GESCHAFTSBEREICH
IVULTIFUNKTIONSKERAMIK.LUITPOLDSTRABE
15. 91207LAUF
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Nameof the personwhomademeasurement:
ScottKu
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No.:CEl2013i/13196Dale.2013tO1122Page:25 ol 29
CERAMTECGMBH
15. 91207LAUF
GESCI-I,AFTSBEREICH
[/|ULTIFUNKTIONSKERAMIK,LUITPOLDSTRABE
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of C-Clbonding
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Test Report
No.: CE12013/13196
DaIe| 201310122 Page 26ot29
CERAMTEC
GMBH
GESCI-IAFTSBEREICH
MULTIFUNKTIONSKERAI/|IK,LUITPOLDSTMBE'15,
91207LAUF
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No.: CE/2013/13196Dale| 2013101122Paoe:27cf29
CERAMTEC
GMBH
GESCHAFTSBEREICH
MULTIFUNKTIONSKERAMIK,LUITPOLDSTRABE
15, 9'1207
LAUF
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No.: CE/201313196 Dale:2013101n2 Pag€: 28 of 29
CERAMTEC
GMBH
GESCHAFTSBEREICH
IUULTIFUNKTIONSKERAMIK,LUITPOLDSTMBE
I5, 91207LAUF
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: ShinjyhChen
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No.:CE2013/13196D aie.2013101122Page: 29 of 29
CEMMTECGMBH
GESC|-|,AFTSBEREICH
MULTIFUNKTIONSKERAMIK.LUITPOLDSTRABE
15.91207LAUF
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Test Report
Applicant:
Number : TWNC00249177
Littelfuse Philippines Inc.
LIMA Technology Center, Lipa City,
Malvar, Batangas
Date
: Mar 26, 2012
Sample Description:
One (1) group of submitted samples said to be :
Part Description
: Silver Clad Cu Wire with 5% Ag
Part Number
: 082xxx(082375)
Date Sample Received
: Mar 22, 2012
Date Test Started
: Mar 22, 2012
Test Conducted :
As requested by the applicant, for details please refer to attached pages.
Authorized By:
On Behalf Of Intertek Testing Services
Taiwan Limited
K. Y. Liang
Director
This report shall not be reproduced
except in full, without the written
approval of the laboratory.
Page 1 of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00249177
Test Conducted
(Ⅰ) Test Result Summary :
Test Item
Heavy Metal
Cadmium (Cd) content
Lead (Pb) content
Mercury (Hg) content
Chromium VI (Cr6+) content (mg/kg with 50cm2)
Remarks: ppm =
ND =
<
=
mg/kg
Result (ppm)
Silvery Wire
ND
ND
ND
Negative (< 0.02)
Parts per million based on weight of tested sample = mg/kg
Not detected
Less than
with 50cm2 = milligram per kilogram with 50 square centimetre
Responsibility of Chemist : Irene Chiou / Kevin Liu / Cathy Chen
Date Sample Received
Test Period
: Mar 22, 2012
: Mar 22, 2012 To Mar 26, 2012
(Ⅱ) RoHS Requirement:
Restricted Substances
Cadmium (Cd) Content
Lead (Pb) Content
Mercury (Hg) Content
Chromium VI (Cr6+) Content
Limits
0.01% (100ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for
homogeneous material.
Page 2 of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00249177
Test Conducted
(Ⅲ) Test Method:
Test Item
Cadmium (Cd)
content
Lead (Pb) content
Mercury (Hg)
content
Chromium VI (Cr6+)
content
Test Method
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 7, by microwave
digestion until the tested samples are
totally dissolved and determined by
ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in annex B, by boiling water
extraction and determined by UV-Vis
Spectrophotometer.
Reporting Limit
2 ppm
2 ppm
2 ppm
0.02
mg/kg with 50cm2
Remark: Reporting limit = Quantitation limit of analyte in sample
Page 3 of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00249177
Test Conducted
(Ⅳ) Measurement Flowchart:
Test For Cd/Pb/Hg/Chromium (VI)
Reference Standard：IEC 62321 edition 1.0:2008
Sampling/grinding or cutting
Cd/Pb/Hg
Cr
Polymers /
Electronics
Metal
For different
material, digest
the sample with
*1
appropriate acid
By spot test
Negative
Confirm the tested
samples are
totally dissolved
Make up with
deionized water
6+
*2
Weigh sample
and add
alkaline
solution
Get 50cm2 sample
Definite temp.
extraction
Boiling water
extraction
Cool and filter
the extract
Analyzed by ICP-OES
Make up with deionized
water and add diphenylcarbazide solution
Remarks:
*1: List Of Appropriate Acid：
Material
Polymers
Metals
Electronics
Analyzed by UV-VIS
Acid Added For Digestion
HNO3,HCl,HF,H2O2,H3BO3
HNO3,HCl,HF
HNO3,HCl,H2O2,HBF4
*2: If the result of spot test is positive, Chromium VI would be determined as detected.
End of Report
Page 4 of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00249177
Test Conducted
Photo
Page 5 of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Test Report
Applicant:
Number : TWNC00249178
Littelfuse Philippines Inc.
LIMA Technology Center, Lipa City,
Malvar, Batangas
Date
: Mar 26, 2012
Sample Description:
One (1) group of submitted samples said to be :
Part Description
: Silver Clad Cu Wire with 2% Ag
Part Number
: 082xxx(082684)
Date Sample Received
: Mar 22, 2012
Date Test Started
: Mar 22, 2012
Test Conducted :
As requested by the applicant, for details please refer to attached pages.
Authorized By:
On Behalf Of Intertek Testing Services
Taiwan Limited
K. Y. Liang
Director
This report shall not be reproduced
except in full, without the written
approval of the laboratory.
Page 1 of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00249178
Test Conducted
(Ⅰ) Test Result Summary :
Test Item
Heavy Metal
Cadmium (Cd) content
Lead (Pb) content
Mercury (Hg) content
Chromium VI (Cr6+) content (mg/kg with 50cm2)
Remarks: ppm =
ND =
<
=
mg/kg
Result (ppm)
Silvery Wire
ND
ND
ND
Negative (< 0.02)
Parts per million based on weight of tested sample = mg/kg
Not detected
Less than
with 50cm2 = milligram per kilogram with 50 square centimetre
Responsibility of Chemist : Irene Chiou / Kevin Liu / Cathy Chen
Date Sample Received
Test Period
: Mar 22, 2012
: Mar 22, 2012 To Mar 26, 2012
(Ⅱ) RoHS Requirement:
Restricted Substances
Cadmium (Cd) Content
Lead (Pb) Content
Mercury (Hg) Content
Chromium VI (Cr6+) Content
Limits
0.01% (100ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for
homogeneous material.
Page 2 of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00249178
Test Conducted
(Ⅲ) Test Method:
Test Item
Cadmium (Cd)
content
Lead (Pb) content
Mercury (Hg)
content
Chromium VI (Cr6+)
content
Test Method
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 7, by microwave
digestion until the tested samples are
totally dissolved and determined by
ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in annex B, by boiling water
extraction and determined by UV-Vis
Spectrophotometer.
Reporting Limit
2 ppm
2 ppm
2 ppm
0.02
mg/kg with 50cm2
Remark: Reporting limit = Quantitation limit of analyte in sample
Page 3 of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00249178
Test Conducted
(Ⅳ) Measurement Flowchart:
Test For Cd/Pb/Hg/Chromium (VI)
Reference Standard：IEC 62321 edition 1.0:2008
Sampling/grinding or cutting
Cd/Pb/Hg
Cr
Polymers /
Electronics
Metal
For different
material, digest
the sample with
*1
appropriate acid
By spot test
Negative
Confirm the tested
samples are
totally dissolved
Make up with
deionized water
6+
*2
Weigh sample
and add
alkaline
solution
Get 50cm2 sample
Definite temp.
extraction
Boiling water
extraction
Cool and filter
the extract
Analyzed by ICP-OES
Make up with deionized
water and add diphenylcarbazide solution
Remarks:
*1: List Of Appropriate Acid：
Material
Polymers
Metals
Electronics
Analyzed by UV-VIS
Acid Added For Digestion
HNO3,HCl,HF,H2O2,H3BO3
HNO3,HCl,HF
HNO3,HCl,H2O2,HBF4
*2: If the result of spot test is positive, Chromium VI would be determined as detected.
End of Report
Page 4 of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00249178
Test Conducted
Photo
Page 5 of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Test Report
Applicant:
Littelfuse Philippines Inc.
LIMA Technology Center, Lipa City,
Malvar, Batangas
Number
: TWNC00294417
Date
: Jan 17, 2013
Sample Description:
One (1) group of submitted samples said to be :
Part Description
: Ni42Fe58MCuAg5% Element
Part Number
: 497226 (497xxx)
Date Sample Received
: Jan 11, 2013
Date Test Started
: Jan 11, 2013
Test Conducted :
As requested by the applicant, for details please refer to attached pages.
Authorized by:
On Behalf of Intertek Testing Services
Taiwan Limited
K. Y. Liang
Director
*THJ0294417*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C.
全國公證檢驗股份有限公司
11492 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410
Page 1 of 5
Number
: TWNC00294417
Test Conducted
(Ⅰ) Test Result Summary:
Test Item
Unit
Test Method
Result
Silvery
metal wire
RL
ND
2
ND
2
ND
2
Negative
0.02
Heavy Metal
Cadmium (Cd) content
ppm
Lead (Pb) content
ppm
Mercury (Hg) content
ppm
Chromium VI (Cr6+) content
Remarks:
mg/kg
with
50 cm2
With reference to IEC
62321: 2008, by
microwave digestion and
determined by ICP-OES.
With reference to IEC
62321: 2008, by
microwave digestion and
determined by ICP-OES.
With reference to IEC
62321: 2008, by
microwave digestion and
determined by ICP-OES.
With reference to IEC
62321: 2008, by boiling
water extraction and
determined by UV-Vis
Spectrophotometer.
ppm = parts per million based on weight of tested sample = mg/kg
ND
= Not detected
RL
= Reporting Limit, Quantitation limit of analyte in sample
mg/kg with 50cm2 = milligram per kilogram with 50 square centimeter
Negative = A negative test result indicated positive observation was not
found at the time of Test. When the spot test showed a negative
result, the boiling water extraction procedure shall be used to
verify the result.
Responsibility of Chemist:
Date Sample Received
Test Period
Kevin Liu/ Irene Chiou
: Jan 11, 2013
: Jan 11, 2013 To Jan 15, 2013
(Ⅱ) RoHS Limits:
Restricted Substances
Limits
Cadmium (Cd) content
Lead (Pb) content
Mercury (Hg) content
Chromium VI (Cr6+) content
0.01% (100ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
The above limits were quoted from Annex II of 2011/65/EU for homogeneous material.
*THJ0294417*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C.
全國公證檢驗股份有限公司
11492 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410
Page 2 of 5
Number
: TWNC00294417
Test Conducted
(Ⅳ) Measurement Flowchart:
Test For Cd/Pb/Hg/Chromium (VI)
Reference Standard：IEC 62321 edition 1.0:2008
Sampling/grinding or cutting
Cd/Pb/Hg
Cr
6+
Polymers /
Electronics
Metal
For different
material, digest
the sample with
*1
appropriate acid
By spot test
Negative
Confirm the tested
samples are
totally dissolved
Make up with
deionized water
*2
Weigh sample
and add
alkaline
solution
Get 50cm2 sample
Definite temp.
extraction
Boiling water
extraction
Cool and filter
the extract
Analyzed by ICP-OES
Make up with deionized
water and add diphenylcarbazide solution
Analyzed by UV-VIS
*THJ0294417*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C.
全國公證檢驗股份有限公司
11492 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410
Page 3 of 5
Number
: TWNC00294417
Test Conducted
Remarks:
*1: List of Appropriate Acid：
Material
Acid Added for Digestion
Polymers
HNO3,HCl,HF,H2O2,H3BO3
Metals
HNO3,HCl,HF
Electronics
HNO3,HCl,H2O2,HBF4
*2: If the result of spot test is positive, Chromium VI would be determined as
detected.
End of Report
This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a
recommendation for any particular course of action. Intertek does not accept a duty of care or any other responsibility to any person other than
the Client in respect of this report and only accepts liability to the Client insofar as is expressly contained in the terms and conditions
governing Intertek's provision of services to you. Intertek makes no warranties or representations either express or implied with respect to this
report save as provided for in those terms and conditions. We have aimed to conduct the Review on a diligent and careful basis and we do not
accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by statute or otherwise, except in
the event of our gross negligence or wilful misconduct.
*THJ0294417*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C.
全國公證檢驗股份有限公司
11492 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410
Page 4 of 5
Number
: TWNC00294417
Test Conducted
Photo
*THJ0294417*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C.
全國公證檢驗股份有限公司
11492 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410
Page 5 of 5
Intertek Consumer Goods GmbH · Würzburger Straße 152 · 90766 Fürth ·
Polyfil AG
Gina Gregorio
Oberallmendstrasse 20A
6300 Zug / Switzerland
Fürth, 2012-12-19
Test report No. FUHL1236935
Testing of a material sample according to the RoHS directive 2011/65/EC
Sample description: Ni36Fe64MAg wire; part no. 962464; batch 497255Rev.B
Arrival in lab: 2012-012-04; Period of XRF analysis incl. sample preparation and photo documentation: 2012-12-07 – 2012-12-10
Head of Inorganic Lab: Claudia List
Copying this test report is permitted only in agreement with the contracted lab. The test results refer only to the tested item.
This report consists of 6 page(s).
The test methods signed with * are not listed in the attachment of the accreditation certificate.
Conclusion based on tested item
Status
Test order
testing according to the RoHS directive 2011/65/EC
°
conform°
Please see overview of test results
- Test results see next pages -
Intertek Consumer Goods GmbH
Würzburger Straße 152
90766 Fürth, Germany
Tel.: +49 911 74075 0
Fax: +49 911 74075 30
[email protected]
Sitz Fürth
Amtsgericht Fürth, HRB 5756
USt-IdNr. DE169317871
Geschäftsführer
Kay Grönhardt
Rainer Mast
Durch die DAkkS nach DIN EN ISO/IEC
17025 akkreditiertes Prüflaboratorium
Die Akkreditierung gilt für die in der
Urkunde aufgeführten Prüfverfahren.
Page 2 of 6 page(s) of our test report No. FUHL1236935 dated 2012-12-19
Sample description: Ni36Fe64MAg wire; part no. 962464; batch 497255Rev.B
nM = non Metal
M = Metal
cM = composite Material
List of component parts:
Sample No. Part No.
236935
1
Intertek Consumer Goods GmbH
Würzburger Straße 152
90766 Fürth, Germany
Material Description
M
Ni36Fe64MAg wire; part no. 962464; batch 497255Rev.B
Tel.: +49 911 74075 0
Fax: +49 911 74075 30
[email protected]
Sitz Fürth
Amtsgericht Fürth, HRB 5756
Ust-IdNr. DE169317871
Geschäftsführer
Kay Grönhardt
Rainer Mast
Page 3 of 6 page(s) of our test report No. FUHL1236935 dated 2012-12-19
Sample description: Ni36Fe64MAg wire; part no. 962464; batch 497255Rev.B
Comment
LOD = Limit of Detection
BL
OL
X
σ
=
=
=
=
Below Limit
Over Limit
Inconclusive, further test necessary
Standard deviation
CS
= Composite sample
Remark:
Results were obtained by EDXRF for primary screening. Additional chemical testing using ICP (for Cd, Pb),
AAS (for Hg), IC-UC/VIS (for CrVI) and GC/MS (for PBBs/PBDEs) are recommended, if the concentration
exceeds the below warning value according to IEC 62321.
Element
Cd
Pb
Hg
Br
Cr
Unit
mg / kg
mg / kg
mg / kg
mg / kg
mg / kg
non - metal
BL ≤ (70-3σ) < X < (130+3σ) ≤ OL
BL ≤ (700-3σ) < X < (1300+3σ) ≤ OL
BL ≤ (700-3σ) < X < (1300+3σ) ≤ OL
BL ≤ (300-3σ) < X
BL ≤ (700-3σ) < X
Element
Cd
Pb
Hg
Br
Cr
Unit
mg / kg
mg / kg
mg / kg
mg / kg
mg / kg
composite material
LOD < X < (150+3σ) ≤ OL
BL ≤ (500-3σ) < X < (1500+3σ) ≤ OL
BL ≤ (500-3σ) < X < (1500+3σ) ≤ OL
BL ≤ (250-3σ) < X
BL ≤ (500-3σ) < X
Intertek Consumer Goods GmbH
Würzburger Straße 152
90766 Fürth, Germany
Tel.: +49 911 74075 0
Fax: +49 911 74075 30
[email protected]
metal
BL ≤ (70-3σ) < X < (130+3σ) ≤ OL
BL ≤ (700-3σ) < X < (1300+3σ) ≤ OL
BL ≤ (700-3σ) < X < (1300+3σ) ≤ OL
-BL ≤ (700-3σ) < X
Sitz Fürth
Amtsgericht Fürth, HRB 5756
Ust-IdNr. DE169317871
Geschäftsführer
Kay Grönhardt
Rainer Mast
Page 4 of 6 page(s) of our test report No. FUHL1236935 dated 2012-12-19
Sample description: Ni36Fe64MAg wire; part no. 962464; batch 497255Rev.B
1. XRF screening
Method:
Sample No.
236935
XRF according to IEC 62321:2008*
Part No.
1
Pb
Hg
Cd
Crtotal
Br
Status
BL
BL
BL
BL
--
conform
Comment:
Elements
Lead (Pb)
Mercury (Hg)
Cadmium (Cd)
Chromium VI (Cr VI)
Polybrominated Biphenyle (PBBs)
Polybrominated Diphenyl ether (PBDEs)
RoHS-limit value
1000 mg/kg
1000 mg/kg
100 mg/kg
1000 mg/kg
1000 mg/kg
1000 mg/kg
- Flow charts see next page(s) -
Intertek Consumer Goods GmbH
Würzburger Straße 152
90766 Fürth, Germany
Tel.: +49 911 74075 0
Fax: +49 911 74075 30
[email protected]
Sitz Fürth
Amtsgericht Fürth, HRB 5756
Ust-IdNr. DE169317871
Geschäftsführer
Kay Grönhardt
Rainer Mast
Test procedure
Page 5 of 6 page(s)
YES
non-destructive
sample
preparation
sample
uniform ?
screening
procedure
by XRF
YES
NO
samples
mechanical
sample
preparation
screening
by XRF ?
metallic
materials,
pass
meets
limits ?
YES
NO
YES
fail
further
testing ?
NO
NO
mechanical
sample
preparation
polymer
materials,
entity based
conforming
sample
chemical test
procedure (verification)
various methods
(please see verification test
procedure below)
entity based
non conforming
sample
pass
YES
electronics
(PCB / component)
entity based
conforming
sample
meets
limits ?
fail
NO
Intertek Consumer Goods GmbH
Würzburger Straße 152
90766 Fürth, Germany
Tel.: +49 911 74075 0
Fax: +49 911 74075 30
[email protected]
Sitz Fürth
Amtsgericht Fürth, HRB 5756
Ust-IdNr. DE169317871
Geschäftsführer
Kay Grönhardt
Rainer Mast
entity based
non conforming
sample
Verification test procedure
Page 6 of 6 page(s)
Sample Preparation
Sample Measurement
Acid digestion with
microwave / hotplate
Sample solvent
extraction
Filtration
Concentration/
Dilution of extraction
solution
Solution
Cr6+
PBBs/PBDEs
Pb/Cd/Hg
Residue
Filtration
Total digestion
GC/MS
DATA
Non-metallic
material
Alkaline extraction
Adding extraction
solution
Metallic
material
Positive
Negative
Boiling water
extraction
Alkaline extraction
Heating to 90~95°C
for extraction
Adding 1,5diphenylcarbazide
for color development
Filtration and pH
adjustment
ICP-OES/AAS
A red color indicates
the presence of Cr6+
If necessary, confirm
with UV-VIS or
IC-UV/VIS
Adding 1,5diphenylcarbazide
for color development
DATA
DATA
UV-VIS or
IC-UV/VIS
DATA
Intertek Consumer Goods GmbH
Würzburger Straße 152
90766 Fürth, Germany
Tel.: +49 911 74075 0
Fax: +49 911 74075 30
[email protected]
Sitz Fürth
Amtsgericht Fürth, HRB 5756
Ust-IdNr. DE169317871
Spot test
Geschäftsführer
Kay Grönhardt
Rainer Mast
Test Report
Applicant:
Number : TWNC00285771
Littelfuse Philippines Inc.
LIMA Technology Center, Lipa City,
Malvar, Batangas
Date
: Nov 16, 2012
Sample Description:
One (1) group of submitted samples said to be :
Part Description
: Solder (Pb is ≥ 90%)
Part Number
: 692321
Date Sample Received
: Nov 12, 2012
Date Test Started
: Nov 13, 2012
Test Conducted :
As requested by the applicant, for details please refer to attached pages.
Authorized By:
On Behalf Of Intertek Testing Services
Taiwan Limited
K. Y. Liang
Director
*THJ0285771*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410
Page 1 of 6
Number : TWNC00285771
Test Conducted
(Ⅰ) Test Result Summary :
Result (ppm)
Silvery metal
Test Item
Heavy Metal
Cadmium (Cd) content
Lead (Pb) content
Mercury (Hg) content
Chromium VI (Cr6+) content (mg/kg with 50cm2)
ND
934557
ND
Negative (< 0.02)
Remarks: ppm = Parts per million based on weight of tested sample = mg/kg
ND = Not detected
<
= Less than
mg/kg with 50cm2 = milligram per kilogram with 50 square centimetre
Negative = A negative test result indicated positive observation
was not found at the time of Test.
Responsibility of Chemist : Irene Chiou / Kevin Liu
Date Sample Received
Test Period
: Nov 12, 2012
: Nov 13, 2012 to Nov 16, 2012
(Ⅱ) RoHS Limits:
Restricted Substances
Cadmium (Cd) Content
Lead (Pb) Content
Mercury (Hg) Content
Chromium VI (Cr6+) Content
Limits
0.01% (100ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
The above limits were quoted from Annex II of 2011/65/EU for homogeneous
material.
*THJ0285771*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410
Page 2 of 6
Number : TWNC00285771
Test Conducted
(Ⅲ) Test Method:
Test Item
Cadmium (Cd)
content
Lead (Pb) content
Mercury (Hg)
content
Chromium VI (Cr6+)
content
Test Method
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 7, by microwave
digestion until the tested samples are
totally dissolved and determined by
ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in annex B, by boiling water
extraction and determined by UV-Vis
Spectrophotometer.
Reporting Limit
2 ppm
2 ppm
2 ppm
0.02
mg/kg with 50cm2
Remark: Reporting limit = Quantitation limit of analyte in sample
*THJ0285771*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410
Page 3 of 6
Number : TWNC00285771
Test Conducted
(Ⅳ) Measurement Flowchart:
Test For Cd/Pb/Hg/Chromium (VI)
Reference Standard：IEC 62321 edition 1.0:2008
Sampling/grinding or cutting
Cd/Pb/Hg
Cr
6+
Polymers /
Electronics
Metal
For different
material, digest
the sample with
*1
appropriate acid
By spot test
Negative
Confirm the tested
samples are
totally dissolved
Make up with
deionized water
*2
Weigh sample
and add
alkaline
solution
Get 50cm2 sample
Definite temp.
extraction
Boiling water
extraction
Cool and filter
the extract
Analyzed by ICP-OES
Make up with deionized
water and add diphenylcarbazide solution
Analyzed by UV-VIS
*THJ0285771*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410
Page 4 of 6
Number : TWNC00285771
Test Conducted
Remarks:
*1: List of Appropriate Acid：
Acid Added for Digestion
Material
Polymers
HNO3,HCl,HF,H2O2,H3BO3
Metals
HNO3,HCl,HF
Electronics
HNO3,HCl,H2O2,HBF4
*2: If the result of spot test is positive, Chromium VI would be determined
as detected.
End of Report
This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a
recommendation for any particular course of action. Intertek does not accept a duty of care or any other responsibility to any person other than
the Client in respect of this report and only accepts liability to the Client insofar as is expressly contained in the terms and conditions
governing Intertek's provision of services to you. Intertek makes no warranties or representations either express or implied with respect to this
report save as provided for in those terms and conditions. We have aimed to conduct the Review on a diligent and careful basis and we do not
accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by statute or otherwise, except in
the event of our gross negligence or wilful misconduct.
*THJ0285771*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410
Page 5 of 6
Number : TWNC00285771
Test Conducted
Photo
*THJ0285771*
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410
Page 6 of 6
Test Report
Applicant:
Number : TWNC00253636
Littelfuse Philippines Inc.
LIMA Technology Center, Lipa City,
Malvar, Batangas
Date
: Apr 24, 2012
Sample Description:
One (1) group of submitted samples said to be :
Part Description
: Black Ink
Part Number
: 425809
Date Sample Received
: Apr 19, 2012
Date Test Started
: Apr 19, 2012
Test Conducted :
As requested by the applicant, for details please refer to attached pages.
Authorized By:
On Behalf Of Intertek Testing Services
Taiwan Limited
K. Y. Liang
Director
This report shall not be reproduced
except in full, without the written
approval of the laboratory.
Page 1 of 9
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00253636
Test Conducted
(Ⅰ) Test Result Summary :
Test Item
Heavy Metal
Cadmium (Cd) content
Lead (Pb) content
Mercury (Hg) content
Chromium VI (Cr6+) content
Polybrominated Biphenyls (PBBs)
Monobrominated Biphenyls (MonoBB)
Dibrominated Biphenyls (DiBB)
Tribrominated Biphenyls (TriBB)
Tetrabrominated Biphenyls (TetraBB)
Pentabrominated Biphenyls (PentaBB)
Hexabrominated Biphenyls (HexaBB)
Heptabrominated Biphenyls (HeptaBB)
Octabrominated Biphenyls (OctaBB)
Nonabrominated Biphenyls (NonaBB)
Decabrominated Biphenyl (DecaBB)
Polybrominated Diphenyl Ethers (PBDEs)
Monobrominated Diphenyl Ethers (MonoBDE)
Dibrominated Diphenyl Ethers (DiBDE)
Tribrominated Diphenyl Ethers (TriBDE)
Tetrabrominated Diphenyl Ethers (TetraBDE)
Pentabrominated Diphenyl Ethers (PentaBDE)
Hexabrominated Diphenyl Ethers (HexaBDE)
Heptabrominated Diphenyl Ethers (HeptaBDE)
Octabrominated Diphenyl Ethers (OctaBDE)
Nonabrominated Diphenyl Ethers (NonaBDE)
Decabrominated Diphenyl Ether (DecaBDE)
Result (ppm)
Black Paste
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Page 2 of 9
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00253636
Test Conducted
(Ⅰ) Test Result Summary :
Test Item
Result (ppm)
Black Paste
Halogen Content
Fluorine (F)
Chlorine (Cl)
Bromine (Br)
Iodine (I)
Phthalates
Di(2-ethylhexyl) Phthalate (DEHP)
Dibutyl Phthalate (DBP)
Benzyl Butyl Phthalate (BBP)
Others
Hexabromocyclododecane (HBCDD)
ND
610
ND
ND
ND
ND
ND
ND
Remarks: ppm = Parts per million based on wet weight of tested sample =
mg/kg
ND = Not detected
Responsibility of Chemist : Irene Chiou / Kevin Liu / Cathy Chen
Date Sample Received
Test Period
: Apr 19, 2012
: Apr 19, 2012 To Apr 24, 2012
(Ⅱ) RoHS Requirement:
Restricted Substances
Cadmium (Cd) Content
Lead (Pb) Content
Mercury (Hg) Content
Chromium VI (Cr6+) Content
Polybrominated Biphenyls (PBBs)
Polybrominated Diphenyl Ehters (PBDEs)
Limits
0.01% (100ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for
homogeneous material.
Page 3 of 9
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00253636
Test Conducted
(Ⅲ) Test Method:
Test Item
Test Method
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
Cadmium (Cd) content
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
Lead (Pb) content
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 7, by microwave
Mercury (Hg) content
digestion until the tested samples
are totally dissolved and determined
by ICP-OES.
With reference to IEC 62321 edition
Chromium VI (Cr6+)
1.0:2008 in annex C, by alkaline
content
digestion and determined by UV-Vis
spectrophotometer.
With reference to IEC 62321 edition
1.0:2008 in annex A, by solvent
Polybrominated
extraction and determined by GC-MS
Biphenyls (PBBs)
and further HPLC-DAD confirmation
when necessary.
With reference to IEC 62321 edition
Polybrominated
1.0:2008 in annex A, by solvent
Diphenyl Ethers
extraction and determined by GC-MS
(PBDEs)
and further HPLC-DAD confirmation
when necessary.
With reference to EN 14582:2007 by
Halogen Content
calorimetric bomb with oxygen and
determined by Ion Chromatograph.
With reference to EN 14372: 2004, by
Phthalates
solvent extraction and determined by
GC-MS.
With reference to USEPA 3540C, by
Hexabromocyclododecane
solvent extraction and determined by
(HBCDD)
GC-MSD.
Reporting Limit
2 ppm
2 ppm
2 ppm
1 ppm
5 ppm
5 ppm
50 ppm
10 ppm
10 ppm
Remark: Reporting limit = Quantitation limit of analyte in sample
Page 4 of 9
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00253636
Test Conducted
(Ⅳ) Measurement Flowchart:
Test for Cd/Pb/Hg/Chromium (VI)/PBBS/PBDES Contents
Reference Standard: IEC 62321 edition 1.0:2008
Sample preparation
For non-metal part
For metal part
Take sample and immerse into Aqua Regia, start to strip plating layer
Stop the stripping procedure upon color change completely
Take the Aqua solution as plating component and stripped body as substrate component
Cd/Pb/Hg
Cr
Weigh sample and
add organic solvent
By spot test
Negative
Confirm the tested
samples are
totally dissolved
Make up with
deionized water
PBBs/PBDEs
Polymers /
electronics
Metal
For different
material, digest
the sample with
*1
appropriate acid
6+
Get 50cm2 sample
By boiling water
extraction
*2
Weigh sample
and add
alkaline
solution
By Soxhlet
extraction or
Solvent extraction
Definite temp.
extraction
Cool and filter
the extract
Analyzed by ICP-OES
Concentrate the
extract and make up
with organic
solvent
Analyzed by GC-MSD
Make up with deionized
water and add diphenylcarbazide solution
Analyzed by UV-VIS
Remarks:
*1: List of Appropriate Acid：
Acid Added for Digestion
Material
Polymers
HNO3,HCl,HF,H2O2,H3BO3
Metals
HNO3,HCl,HF
Electronics
HNO3,HCl,H2O2,HBF4
*2: If the result of spot test is positive, Chromium VI would be determined as detected.
Page 5 of 9
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00253636
Test Conducted
(Ⅳ) Measurement Flowchart:
Test for Halogen Content
Reference Standard：EN 14582
Sampling/grinding or
cutting
Add absorbent in a
combustion flask &
place weighed sample in
equipment
Fill oxygen into
calorimetric bomb
Ignite then leave the
bomb at room
temperature
Transfer the absorbent
into a volumetric flask
Make up with deionized
water
Analyzed by ion
chromatography
Page 6 of 9
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00253636
Test Conducted
(Ⅳ) Measurement Flowchart:
Test For Phthalates Contents
Reference Method: EN 14372: 2004
Sampling/grinding or
cutting
Weigh sample and add
organic solvent
By solvent extraction
Concentrate the extract
and make up with
organic solvent
Analyzed by GC-MSD
Page 7 of 9
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00253636
Test Conducted
(Ⅳ) Measurement Flowchart:
Test For Hexabromocyclododecane (HBCDD)
Reference Standard：USEPA 3540C
Sampling/grinding or cutting
Weigh sample and add organic
solvent
By soxhlet extraction
Concentrate the extract and
make up with organic solvent
Analyzed by GC-MSD
End of Report
Page 8 of 9
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00253636
Test Conducted
Photo
Page 9 of 9
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401