ICPTest_448 pdf

ICP Test Report Certification Packet
Company name :
Littelfuse, Inc.
Product Series:
Nano2 Fuse - FA
Product #:
448xxx Series
Issue Date:
December 28, 2011
It is hereby certified by Littelfuse, Inc. that there is neither RoHS (EU Directive
2002/95/EC)-restricted substance nor such use, for materials to be used for unit parts, for
packing/packaging materials, and for additives and the like in the manufacturing processes.
In addition, it is hereby reported to you that the parts and sub-materials, the materials to be used
for unit parts, the packing/packaging materials, and the additives and the like in the manufacturing
processes, are all composed of the following components.
Issued by:
<Global EHS Engineer>
(1) Parts, sub-materials and unit parts
This document covers the Nano2 Fuse - FA RoHS-Compliant series products
manufactured by Littelfuse, Inc.
＜ Raw Materials Used
Please see Table 1
(2) The ICP data on all measurable substances
Please see appropriate pages as identifed in Table 1
Remarks：
Form 585-047 Rev. A
1
2/21/06
Table 1: List of Raw Materials covered by this report
Total Parts
1
2
3
4
5
6
7
8
9
Raw Material Part Number
910-275
Frequenta C221 (909-434)
082xxx
082xxx
11-0894 (497xxx)
11-0803 (497xxx)
4-1357 (497xxx)
082418-001
927-30x (927-303/ 927-304)
Raw Material Description
Cap
Ceramic tube - Body
Element (2% by weight AG Clad Cu)
Element (5% by weight AG Clad Cu)
Element (Ag Plated 36 Alloy)
Wire - Cu Clad Fe58 42Ni 5Ag By Weight
Element – Ni99.9
Element – Cu CDA 102 Sn Plated
Solder ( containing 1%-2% flux)
10
425809
Ink
2
Page(s)
3-7
8-30
31-35
36-40
41-47
48-54
55-61
62-66
67-71
72-77,
78-82
Number : TWNC00233554
Test Report
Applicant:
Littelfuse Philippines Inc.
LIMA Technology Center, Lipa City,
Malvar, Batangas
Date
: Nov 24, 2011
Sample Description:
One (1) group of submitted samples said to be :
Part Description
: Cap
Part Number
: 910-275
Date Sample Received
: Nov 21, 2011
Date Test Started
: Nov 23, 2011
Test Conducted :
As requested by the applicant, for details please refer to attached pages.
Authorized By:
On Behalf Of Intertek Testing Services
Taiwan Limited
K. Y. Liang
Director
This report shall not be reproduced
except in full, without the written
approval of the laboratory.
Page 1 of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00233554
Test Conducted
(Ⅰ) Test Result Summary :
Result (ppm)
(1)
(2)
Test Item
Heavy Metal
Cadmium (Cd) content
Lead (Pb) content
Mercury (Hg) content
Chromium VI (Cr6+) content (mg/kg with 50cm2)
ND
ND
ND
Negative
(< 0.02)
ND
ND
ND
Negative
(< 0.02)
Remarks: ppm = Parts per million based on weight of tested sample = mg/kg
ND = Not detected
<
= Less than
mg/kg with 50cm2 = milligram per kilogram with 50 square centimetre
Negative = A negative test result indicated positive observation
was not found at the time of Test.
Tested Components
(1) Brown Metal Base Material
(2) Golden Plating Layer
Responsibility of Chemist : Irene Chiou / Kevin Liu
Date Sample Received
Test Period
: Nov 21, 2011
: Nov 23, 2011 To Nov 24, 2011
(Ⅱ) RoHS Requirement:
Restricted Substances
Cadmium (Cd) Content
Lead (Pb) Content
Mercury (Hg) Content
Chromium VI (Cr6+) Content
Limits
0.01% (100ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for
homogeneous material.
Page 2 of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00233554
Test Conducted
(Ⅲ) Test Method:
Test Item
Cadmium (Cd)
content
Lead (Pb) content
Mercury (Hg)
content
Chromium VI (Cr6+)
content
Test Method
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 7, by microwave
digestion until the tested samples are
totally dissolved and determined by
ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in annex B, by boiling water
extraction and determined by UV-Vis
spectrophotometer.
Reporting Limit
2 ppm
2 ppm
2 ppm
0.02
mg/kg with 50cm2
Remark: Reporting limit = Quantitation limit of analyte in sample
Page 3 of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00233554
Test Conducted
(Ⅳ) Measurement Flowchart:
Test for Cd/Pb/Hg/Chromium (VI)
Reference Standard：IEC 62321 edition 1.0:2008
Sample preparation
Take sample and immerse into Aqua Regia, start to strip plating layer
Stop the stripping procedure upon color change completely
Take the Aqua solution as plating component and stripped body as substrate component
Cd/Pb/Hg
Cr
Polymers /
electronics
Metal
For different
material, digest
the sample with
*1
appropriate acid
By spot test
Negative
Confirm the tested
samples are
totally dissolved
Make up with
deionized water
6+
*2
Weigh sample
and add
alkaline
solution
Get 50cm2 sample
Definite temp.
extraction
By boiling water
extraction
Cool and filter
the extract
Analyzed by ICP-OES
Make up with deionized water and add
diphenyl-carbazide solution
Remarks:
*1: List of Appropriate Acid：
Material
Polymers
Metals
Electronics
Analyzed by UV-VIS
Acid Added for Digestion
HNO3,HCl,HF,H2O2,H3BO3
HNO3,HCl,HF
HNO3,HCl,H2O2,HBF4
*2: If the result of spot test is positive, Chromium VI would be determined as detected.
End of Report
Page 4 of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00233554
Test Conducted
Photo
Page 5 of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
nown
ForQues-li
PleaseCo
TestRePort
ithscs
No.. CE2U121775 Dale: 2011102,22 Pagetlof23
t
CERAMTECGMBH
||ll ll]lll[|lll
by/onbehalfoftheclientas:
Thefollowingsample(s)was/weresubmittedand idenlified
TUBE
CERAMIC
C221
FREQUENTA
201110?,14
2011tOZ14 10 2011l12l22
SampleOescdption
Style/ltem No.
SampleReceivingDate
Testing Period
Te6t Resul(s)
Pleasereferto nextPage(6).
Conclusion
the test €sults of Cadmi{n'..
Bas€duponthe performodte6tsby submittedramples'
pees
withthelimitsor
"l!ji, ffiil,
ri;;ntirrioniium crfvrt'
complv
andPBDES
amendmems
and its subs€quent
RoHSDirective2OO2|95/EC
Sfmd fald
Chat*J
LerrtorY
- f!|Pd
'j:;;T-**" -:'"' ": -;-"- ;:.
-:_-^^"-"""_""
";;;r,f {
"""-"..
. """",; ".;;" ".";'-"*"".-";,:':'-iy-::-:.^=.":::"::x*:;,1$ffi'l#
1T,:1.'"'"
*f*;",
,.-.
i
.
;'"X?J":';;::"Jf":":TJ"."i"'j.':'T;-"i;{;;';.+:ll,-r}"'":*x-:X";*:g*"1:".T1","
:r:ff:.;::r*H:';lre*:!'":!{:"j:ji::,;:rr.i*;t*:;:;.,.;.;:::T;..
:;.;.:;:;;':-':::':{",
'."";iJ;et
t.;$":J.:";T I'trr:xr;irii,&?l:':i#!::"r*:*!:i:i;:;i*;1lr-'-?x-":;,rJ'"r;'.t';:;:.r":;'
;-T:";;r'
j ] ] . , i j ] ] . * . . . " ' * , ! L F l . ' L | d 4 ] ; r i - L j i i :
TestReport
No.I CEJ2o11l21Tl5Dale.2011102122Page|2ol23
[nt]tt
CERAMTECGMBH
[ll|l]r
Teai Re€ult{s)
NO,1
PART|,|AI,,!E
Test ltem (s):
BEIGECERAMIC
Unit
method
2008and
to IEC6232'1:
m(yKg Withreference
performed
by ICP{ES.
to IEC62321:2008and
mgKg Witfrreference
Lead (Pb)
perfonnedby ICP-AES.
to IEC62321:2008and
mg/Kg \{/ittrreference
Mercury(Hg)
performed
by ICP-AES.
m9Kg Wttr referenceto IEC02321: 2008and
Cr(Vl)bY
Chromium
Hexav€lent
perfomedby W-VIS.
alkalineextraction
Biphenyls(PCBS) mg/Kg Wih referenceto US EPA3#0C method
Polychlorinated
AnalysiswasperfomedbYGC/MS
(CAS No.i 001336-36-3)
mg/Kg Wittr referenceto US EPA3*0C method
Naphthalone
Polychlorinated
AnalysiswasperformedbYGC/MS.
(PcNs)
mg/Kg With referenceto US EPA3540Cmethod
Terphenyls
Folychlorinated
AnalysiswasperformedbYGC/MS.
(PCTs)
Vvitfrrlferenceto US EPA3540Cmethod
Alkanes,
C10-13,chloro(Short
bYGC/MSwEsperformed
Analysis
(CAS
Paraffins)
ChainChlorinated
No.:085535-84-8)
(CASNo.:000050- mg/kg with ieterenceto ISO 1722d1(2oo8\.
Formaldehyde
Analysis,.vasperformedby HPLC/DAD
00-0)
AnalysiswasperformedbYFTIRand
PVC
FIAMETest.
to USEPA3540C:1996
mg/kg Wittrreference
Peduorooctanesulfonates
was
Analysi6
methodfor PFOSContent.
(PFOS)
p€rfomedby LC/MS.
PFOS- Acid
PFoS- MetalSalt
PFOS-Amide
to USEPA3540C:1996
mg/kg Withreferance
PFOA(CASNo.r000335€71)
(Cd)
Cadmium
Analysiswas
forPFOAContent.
method
pertomedbyLC/[,S.
MDL
Re9ult
No.1
Limit
2
n.d.
100
2
n.d.
'1000
2
n.d.
1000
n.d.
1000
0.5
n.d.
n.d.
0.5
n.d.
0.01
n,o-
3
n.o.
Negative
10
n.d.
10
n.d.
Test Report
No.: CA2fi1121775 Dale:201110222 Page: 3 of 23
|l][ttr
CERAIVTECGIVBH
mg/Kg Wittrreferenceto uS EPA8270Dmethod.
0.5
Result
No.1
n.o,
to Us epn 8270Dmethod
wittr reterence
bYGC/MS.
wasperlormed
Analysis
0.5
n.d.
m9Kg wttr referenceto 0S EPA8270Dmethod.
Analysis
wasperfomedby GC/MS.
0.5
n.d.
Analvsis
to DIN38407-13.
mgKg Withreference
performed
by GC/FPD.
wa6
to
mg/Kg Vvithreference DIN38407-13. Analvsis
wasperformedby GC/FPD.
0.03
n.d.
0.03
n.o.
Unit
T€at ltem (s):
Monomethyl
dibromodiPhenyl
methane(DBBT)
dichlorodiPhenYl
Monomethyl
methane(Ugilec12l)
Monomethyltetrachlorodiphenyl
methane(Ugilec14'1)
Organic-tlncompounda
TributylTinC[BT)(CASNo.:
000688-73-3)
(tphT) (CAsNo.i
TriphenylTin
0006683H)
Halons
Halon-1211
(CAS No.: 000353-59-3)
H€lon-1301
(CAS No.: 00007ffi3-8)
Method
MDL
m!/Kg
n.d.
mg/Kg With referenceto US EPA5021method
Halogen
(F)(CASNo.:
Halogen-Fluorine
014762-94€)
(Cl)(CASNo.:
Halogen4hlorine
022537-15-1](Br)(CASNo.:
Halogen-Bromine
010097-32-2)
(l) (CAS No.i
Halogen-lodine
0 14362.44-8)
Limit
Analysis,.!asperformedby GC/lrS.
AnalysiswasperformedbYGC/MS.
mg/Kg With referenceto US EPA5021rnethod.
bYGC/MS.
Analysis
wBsperformed
mg/kg Wittrreierenceto US EPA5021method.
Analysiswasperfomedby GC/MS.
Halon-2402
(CASNo.:000124-73-2)
m ]l
mg/Kg With referenceto BS EN 14582.2007.
bYlC.
wasp€rformed
Analysis
mg/Kg Withfeferenceto Bs EN 14582:2007.
wa6perfomedby lc.
Analysis
mg/kg Withreferenceto BS EN 14582:2007.
Analysisw€sperformedbYlC.
.
mg/kg f',tithreferenceto BS EN 1458212007
performed
lC.
by
uras
Analysis
n.d.
n.d-
50
n.d.
50
n.d.
50
n.d.
50
n.o.
'r;Fgi:'xffi+lii[i1931ffii1lr:,:i:11:-l':*l'IrTli"r"""*'u""e''*':*llllll.i:"**
u'fi:s",s1;Iif
$i1r#:t;.:nb#xtr:il'U.:aqq'*!."*
6$"#?ngffi#i#"ffi*iffiTfi"#ng"ffi"#
-ii *0
. ei"
";t;t"c"'.
s--.
ao.
^-
TestReport
No. : CE12011121775Oale. 2O11102122 page : 4 ol 23
CERAMTECGI\4BH
ltl|[tat][tttttl
T€6tltem (s):
Unit
Asbestoa
(CASNo.:077536$6-4)
Actinolite
Amosite(CASNo.:012172-73-5)
Anthophyllite
(CASNo.:077536%
67-5)
(CASNo.:012001-29-5 o/o
Chrysotile
Crocidolite
(CASNo.:012001-28-
%
4)
(CASNo.:0253e68€)
Tremolite
Phthalatos
BBP(Benzylbutylphthalare)(CAS
No.i00008568-7)
DEHP(Di-(2-ethylhexyD
phthalate)
(CASNo.:000117-81-71
phthalate)
DIDP(Di-isodecyl
(CAS
No.:02676140-0)
phthalate)
(CAS
DINP(Di-isononyl
No.:028553-12-0)
phthalate)
DNOP(Di-n-oc{yl
(CAS
No.:000117-84-0)
DBP (Dibutylphthalate)(CAS No.:
oooou-74-2')
%
%
%
%
%
Method
MDL
Withreference
to NIOSH9000method.
Analysis\ras performedby XRD.
With referenc€to NIOSH9000methodAnalysisvrrasperformedby XRD.
Withreference
to NIOSH9000method.
Analysis
wasperformed
by XRD.
Withreference
to NIOSH9000method.
Analysiswasperformedby XRD.
Withreference
to NIOSH9000method.
Analysis
\ €s performed
by XRD.
Withreferenceto NIOSH9000method.
Analysis,,,rasperformedby XRD.
Result
No.l
1
Negativg
'I
Negative
'I
Negative
1
Negative
1
Negative
1
Negative
Withreference
to EN 14372.Analysiswas 0.003
pedormed
by GC/MS.
Withreference
to EN 14372.
Analysiswas 0.003
performedby GC/MS.
Withreference
to EN14372.Analysiswas 0.01
pedormedby GC/[/|S.
Withreference
to EN 14372.
Analysis
was
0.01
Derfomed
bv GC/MS.
Withreference
to EN 14372.Analysiswas 0.003
performedby GC/MS.
With referenceto EN 14372.Analysiswa6
0.003
pe.formedby GC/MS.
com@iy+r r rr ]r r: rt-+3: rl,{:ltunL i,i;rll n ]'!hLlii
e(s)bsd rh s Es €p.n cid
{,r .*!1irrr . i:r-.ri,:ii:
& rc
ysub]dbkc3fficoidlomdss
itun'idh.
4d iuigldo 6s!6 @
6|yaddwh'.h.]msolcl'6t3.sM
h * i g n a a n d o b ] i g a l o i s h e b e h i s f @ l d c d 6 r c o p 1 m ] !
s €i3ds rE comFny s iid ^$ d rhe
n,o.
n.d.
n.d.
n.d.
n.d.
n.d.
Llmit
TestReport
No.I CEn011n1775 Oale: 2011t02t22 pageI 5of 23
CERAMTECGMBH
lt
T€atltern(s):
Unit
M6thod
MDL
Sumof PBBa
Monobromobiphenyl
Dibromobiphenyl
Tribromobiphenyl
Telrabromobiphenyl
Pent€bomobiphenyl
Hexabomobiphenyl
Heptabromobiphenyl
Oclabromobiphenyl
Nonabromobiphenyl
Decabromobiphenyl
Result
with reference
to IEC62321:2008and
mg/Kg
performedby GC/IUS.
l\Ionobromodiphenyl
€ther
Dibromodiphenyl
ether
f ribromodiphenyl
ether
fetrabromodiphenyl
ether
Pentabromodiphenyl
ether
Hexabromodiphenyl
ether
Heptabromodiphenyl
ether
Octabromodiphenyl
ether
Nonabromodiphenyl
ether
Decabromodiphenyl
ether
AZO
1): 4-AMINODIPHENYL
(CAS No.l
000092€7-1)
5
n.d.
5
5
n.d.
n.d.
n.d-
5
5
5
5
5
Limit
1000
n.o.
n.d.
n.d.
n.d.
n.d.
mg/kg Withreference
to LFGB82.02-2.
Analysis
5
5
5
5
5
5
5
n.d.
n.o.
n.o.
3
n.d.
3
n.d.
3
n.d.
3
n.d.
3
n.d.
compsy Fjf,irirqr,
;.i.'r
arrilir:irlkr.ai
'ii.xa
rrr
rh r d@iM1€ sd
by $e hFiy
sublodb c c8nffi cotoronsd s€
b f . . c t s a b m 4 d 6 u n r 4 s u ' J d l M e . l h l n A t e i l d i 3 d l ' w i l o l h d ' m l d s d l a b ] 1 y
id q s b e cLsd andstr dsmed
6e r6i
n.d.
n-d.
wasperformedby GC/[,S.
2):BENZIDINE
(CASNo.:00092- mg/Kg Withreference
to LFGB82.02-2.
Analysis
87-5)
was p€rformedby cC/iIS.
3)i 4-CHLORO-O-TOLUIDINE
mg/Kg Withreference
to LFGB82.02-2.
Analysis
(CASNo.: 000095€9-2)
wasperformedby cc/lis.
4):2-MPHTHYLAI,IIlNE
(CAS
mg/Kg Withreference
to LFGB82.02-2.
Analysis
No.:000091-59-8)
wasperformedby cC/[4S.
5): O-AMTNOAZOTOLUENE
(CAS mg/Kg Withreference
to LFGBE2.02-2.
Analysis
No.: 000097-56-3)
wasDerformed
bv GC/l\rS.
ad obitsl ons !.&
No.'l
n-d.
n.d.
Sum of PBDES
N. iob
[II]lltttt!
d
n.d.
n.o.
n.d.
n.d.
n.d.
1000
SGS
Test Report
No.-.CEl2011t21VSDate:21t1to2n2 page:6of 23
CEMMTECGMBH
|l]t|u[r|||Nlltll
Testltem(s):
Unit
Irethod
I'DL
6):2-AMINO-4-NITROTOLUENE
mg/Kg Withreferenc€
to LFGB82.02-2.
An€tysis
(CASNo.:000099-55-8)
wasperformedby GC/MS
7): P-CHLOROANILINE
(CAStioj mg/Kg Withreference
lo LFGB82.02. Anatysis
00010647€)
wEsperformedby GC/MS.
d)rz,4-utAMtNOANtsoLE
(cAs
mg/Kg Withreference
to LFGB82.02-2.
Anttsis
No.:000615-054)
'/t/asp€r{omedbyGC/[IS.
9).4,4'mg/Kg Withreference
to LFGB82-2-li;tG
DIAMINODIPHENYLMETHANE
was pe.tormed by GC/MS_
(CASNo.i000101-7/-9)
'l0):3,3'-DICHLOROBENZIDINE
mgfts Withreference
to LFGB82.02-2.
Analysis
(CASNo.:000091-94-'1)
n€s performedby GC/LilS.
11): 3,3'-Dl[4ETHOXYBENZTDINE
mg/Kg With referenceto LFGB82.02-2.Analysi6
(CASNo.:000119-904)
was performed by GC/MS.
12):3,3'-DIMETHYLBENZ|DtNEmg/Kg With referenceto LFGB8r-r-. Anatysis
(CASNo.:000119-93-7)
wEsperformedby GC/MS.
13):3,3'-DIMETHYL-4,4'mg/kg With referenceto LFGB8i.02-zlAna!dsDIAI\4INODIPHENYLMETHANE
wEsperfomedby GC/MS.
(CASNo.:000838J8-0)
14):P-CRESIDINE
(2-METHOXY-mg/Kg Withreference
to LFGB82.02-2.
Anatysis
,,,/asperformedby cC/[rS.
s-METHYLANILINE)
(CASNo.:
00012G71{)
15):4,4'-METHYLENE-B|S(2mg/Rg Withreference
to LFGB82.02-2.
Analts.is
(CASNo.:
',,€sperformedby GC/[rS.
CHLOROANILINE)
000101-144)
16):4,4'-OXYDIANILINE
(CAS
mg/Kg Withreference
to LFGB82.02-2.
Analysi6
',,rasperformedby cC/lVS.
No.:000101-80-4)
17):4,4'-THIODIANILINE
(CAS
m9Kg with ref€rence
to LFGB82.02-2.
Anatysis
No.:000139€5-1)
wEsperfomedby GC/MS.
18):O-TOLUIDINE
(CASNo.l
mSikS Withreference
to LFGB82.02-2.
Analysis
000095-5!4)
wasperfomedby GC/MS.
19):2,+TOLUYLENEDLqITINE mSikS Withreference
to LFGB82.02-2.
Analysis
(CASNo.:00009$80-7)
wasperformedby GC/MS.
20):2,4,tTRl[TETHYLANILINE mSikS Withreference
to LFGB82.02-2.
Analysis
(CASNo.:000137-17-4
wasperformedby GC/MS.
Result
3
No.1
n.d.
3
n.d.
3
n.d.
3
n.d.
3
n.d.
3
n.d.
3
n.d.
3
n.o.
n.d.
n.d.
3
n.d.
n.d.
3
n,o,
3
n.o.
n.o.
ysub]edbkc6E.dcoidl06ol$
-erd:
mtdwhdberfrbdcrsrs
ndd
nh t sro Gc€daidsadaffird
b. r€prdu€d 8:c€d ntu.wtbdptu
s d.f.t.s
a:.m
o,r,b a
Limit
sc$
I
Test Report
No. '. CE12011121775De1.e
| 2O11tO2t22 page:7of2g
CERAMTEC
GMBH
lllfl||at]ruu
Test ltem (s):
Unit
21):O-ANISIDINE
(CASNo000090{4{)
22):P-AMINOAZOBENZENE
{CASNo.r000060-09-3)
23):2,4-XYLIDINE
(CASNo.:
000095€6-1)
24):2,SXYLIDINE
(CASNo.:
00008762-7)
method
iiDL
Retult
No.l
mg/Kg Withreference
to LFGB82.02-2.
Anatysis
wasperformedby cC/[rS.
mg/Kg Withreference
to LFGB82.02-2.
Anaty6is
wasper{omedby GC/MS_
mg(g Withreference
to LFGB82.02-2.
AnalysiswEsperfomedby GC/MS.
3
n.d.
3
n.d.
3
n.d.
mg/kg Withreference
to LFGB82n2.2-rAnalysrs
'aasperformed
byGC/lrS.
3
n.d.
(Chlorofl
CFC'S
uorocarbonst
GroupI
Chlorof
luoroca6on-1
1 (CASNo.I
000075€94)
Chlorofluorocarbon-12
(CASNo,
-8)
00007s-71
Chlorofluorocarbon-1
13(CASNo.
000076-1
3-1)
uhtorottuoroca$on-l
14(CASNo_:
000076-1+2)
Chlorofluorocarbon-l
15 (CAS No.l
00007&15-3)
mg/Kg With referenceto US EPA5021m€thod
Analysis
wasperformed
by GC/MS.
mg/Kg Wath
reference
to USEPA502'1method.
Analysis
wasperformed
by GC/MS.
mSikg Withreferenceto US EpA 502.1method
qnary6is
wasperfomedby GC/MSmgKg Withreference
to USEPA5021method.
Analysis
wasperfomedby GC/MS.
mg/Kg Withreference
to USEPA5021method.
Analysis
wEsperformed
by GC/MS.
Grouplll
Chlorofluorocarbon-1
3 (CASNo.: mg/Kg Withreference
to USEPA5021method.
000075-72-9)
Analysi6
w€sperformed
by GC/MS.
chtorottuorocarbon111(CASNo.: mg/Kg Withreference
to uS EPA5021method.
000354-56-3)
AnalysiswEsperformedby GC/MS.
L;htorottuorocarbon-112
(CAS No.: mg/Kg Withreference
to LJSEPA5021method.
000076.12-0)
Analysis
wEsperfomedby GC/MS.
Chlorof
luorocarbon-2l
1 (CASNo.: m9Kg With r€ferenceto US EPA5021method.
000422-784t
Analysis
wasperfomedby GC/MS.
(CASNo.i mSikS Withreference
Chlorofl
uorocarbon-212
to USEPA5021method.
003182-26-1)
Analysis
wasperformed
by GC/MS.
Chlorof
luorocabon-2'1
3 (CASNo.: mg/Kg Withreference
to USEPA502'tmethod.
',,,ias
performed
Analysis
byGC/lllS.
002354-06-5)
(CASNo.:
luoroca6on-214
Chlorof
029255-31-0)
c.npary ts'i r,1ri[]t
bresdoctoma
'-rx-i
dumdq
'l]tfiiHil
mg/Kg With referenceto US EPA5021method.
Analysis,r/asperformedby GC/[,S.
n6t q E
.ilf.+f.+rv_rljr:
e6) leied Ths bd €pd
t r-l irrr.i\
subd
b e r n g h b a M o b g a o i s h d ' l i h . l c i e @ d m d o r c o p I m i u
n-d.
n.d.
n.o.
n.d.
n.d.
n.d.
n.d.
n.d.
n.d.
n.d.
n.d.
n.d.
€nnor b3 ,4
tuie
hm Areiloi
s drewi lo rha ,mrar6 ot bb tt
Limit
t
TestReport
No.I CEl2011l21nSDale 2o1jt12n2 page:Bof23
CERAMTECGMBH
t[tttl|||tttltl
Testltem (s):
Chlorofluorocarbon-21S
(CASNol
004,25943-2)
Unit
Method
mg/Kg Withreference
to USEPA502liEi66E.
Analysis
wasperformed
bycC/l\IS.
Chlorof
luorocarbon16lcAsN6l mgikg Withreterenceto uS EPA5021mrethod
-97-2)
000661
Analysis
wEsperfomedby GC/MS.
Chlorof
luorocarbon-2f
leASNo.:- mg/Kg Withreferenc€to US EpA 5021met]iod.
000422-86€)
Analysis
wasperformed
by GC/MS.
CHCa(Chlo.inatehydrocarbon)
1,1,1,2-Tet.achloroethane
(CAS
mg/Kg with reference
to LJsEPA5021method.
No.:000630-20-6)
Analysisw€sperformedby GC/MS.
1,1,'t-trichloroethane
mg/Kg Withreference
ICAS|{o:
to USEpAs02amethod
000071-55€)
Analy6is
wasperformed
byGC/MS.
1,1,2,2-Tetrachloroe'thane
(CAS
mg/Kg Withreference
tJS
to EpA 5d2l6EfdlNo.: 0000793,f5)
Analysis
wasperformed
byGC/MS.
'1,1,2-Trichloroahane
ICASNo.:
000079{0-5)
Result
MDL
mgKg With referenceto LJSEPA5021method
Analysis
wEsperformed
by GC/MS.
mg/K9 With referenceto US EPA5021method
Analysis
wasperformed
by GC/tltS.
mg/Kg Wilhreferenceto US EPA5021method.
Analysis
wasperform€d
by GC/MS.
mSikS Withreference
to USEPA5021method.
qnalysis
wasperfomedby GC/MS.
mdkg Withreferenceto US EPA502'1method.
qnaly6i6
wasperfomedby GC/MS.
mgKg 6,/ithreferenceto US EPA5021method.
Analysiswasperfomedby GC/MS_
mdkg Withreference
to USEPA5021method.
qnarysiswasperformedby GC/MS.
mgikg Withreference
to USEPA5021method.
Analysis
wasperformed
by GC/MS.
mg/Kg Withrefer€nceto US EPA502'1method.
Analysislr,iasperformedby cC/[rS.
mg/Kg Withreference
to Us EPA5021method.
1
No.{
n.d.
1
n.d.
1
n.d.
1
n.d.
1
n.d-
1
n.o,
1
n.d.
1,1-Dichloroethane
(CASNo000075-34-3)
1, 1-Dichloroethene
(CASNo.:
000075-354)
1,l-Dichloropropene
(CASNo.:
000563-585)
1,2,3-Trichloropropane
(CASNo.:
000096-1
8-4)
'1,2-Dichloroethane
(CASNo.:
000107-06-2)
1,2-Drchtoropropane
(CASNo.:
000078€7-s)
l,}Dichloropropane
(CASNo.:
000142-28-9)
(CASNo.:
2,2-Dichloropropane
000594-20-7)
(CASNo.:
Calbontetrachloride
',,€sperformed
000056-23-s)
Analysis
bycc/lls.
(CASNo.:000075- mg/Kg With referenceto US EPA5021method.
Chloroethane
00-3)
Analysis
wEsperfomedby GC/MS.
-'-n::: l,$t: u:1f nri!.t
rh6 @n9d
3 $ued by lb cmFny
bredmrharduffib
suqd
Limit
n.d.
n.d.
n.d,
n.o.
n.d.
n.d.
n.o,
n-d.
n.d.
n.d.
dud'eepl'ifu
ru I Lr, t1\ _1i!:_ia r {,r dt9i
qmdhh
.rr
ii
Aedon
s&awnrobe
m6tro,
radLiy
I r!r rrj/..ri46e!rsf
Men&,ofhascsc,4pr%se)
TestReport
No.: Cel2011l21TI5 Date:2011t0i]22 page: 9 of 23
CERAMTECGMBH
trlN|||ta!] ttlt|l
Testltem (3):
Unft
Method
Chloroform(CASNo.:000067€J- mg/Kg With referenc€to US EPA5021method
3)
Analysiswasperformedby GC/LlS.
Chloromethane
(CASNo.:
mg/Kg With referenceto US EPA502'1method.
000074-87-3)
Analysis
waspeformedby cc/l\rs.
cis-1,2-Dichloroethene
(CASNo.l mg/xg Withreference
to US EPA5021method.
000156-59-2)
Analysiswaspertormedby GC/MS.
cis-1,3-Dichloropropene
(CASNo.: mgikg Withreferenceto US EPA5021method.
010061-01-5)
Analysis
wasperformed
by GC/MS.
Hexachlorobutadiene
(CASNo_:
mg/kS Withreference
to USEPA5021method.
00008768-3)
Analysiswasperformedby GC/MS.
Methylene
Chloride(CASNo.l
mgKg Withreferenceto US EPA5021 method.
000075{9-2)
Analysiswasperfomedby GC/MS.
Tetrachloroethene
(CASNo.:
mgKg Withreference
to LJSEPA5021method.
000127-18,4)
Analysis
wE6perfomedby GC/MS.
(CAS
trans-l,2-Dichloroethene
mg/Kg Withr€ference
to uS EPA5021method.
No.i000156-60-5)
Analysis
wEsperfomedby GC/MS.
(CAS
trans-1,3-Dichloropropene
mg/Kg Withreference
to USEPA5021method.
No.:010061{2-6)
Analysis
w€sperformed
by GC/MS.
Trichloroethylene
(CASNo.:
mlyKg Withreferenc€
to USEPA5021 method.
00007941$)
Analysis
w€sperformed
by GC/MS.
HCFCs
(Hydrochlorof
luorocarbohs)
(CASNo.:000075.43-4)mdkg Withreference
HCFC-21
to LJSEPA5021method.
Analysis
wE6perfomedby GC/MS.
HCFC-22
{CASNo.:000075-45€) mS/kg Withreference
to USEPA5021method.
Analysis
wasperfomedby GC/MS.
HCFC-31
{CASNo.:000593-70-4)mS/kS Withreterence
to USEPA5021method.
Analysis
wasperform€d
by GC/MS.
(CASNo.:00035+14- mg/Kg With.efe.enceto US EPA5021method.
HCFC-'121
3)
Analysis,,vasperformedby GC/[/|S.
(CASNo.:000354-21- mg/Kg With referenceto uS EPA5021method.
HCFC-122
,\
Analysis
wasperfomedby GC/MS.
(CASNo.:000306-89 m!/Kg Withreference
HCFC-123
to USEPA5021method.
2)
Analysiswasperformedby GC/MS.
t rt u r i , l r ! ! jr; G ' 1 n \
.4ri{ra:r.\:frtjr.rr::r'ijl
ysu']ed6bG6fficoidionsds€
mryadwbnturmbdcrsnndd
ua. iots ad obrFr oB uner ha ra
b ! ! s r ob c ' e d a i d h s @ m n r d o
MDL
'1
Re€ult
No.1
n.d.
1
n.d-
1
n.d.
'I
n.o.
'I
n.o.
1
n,d,
1
n.d.
1
n.d.
I
n.d.
1
n.d.
1
n.d.
1
n.o.
1
n,o,
I
n.d.
1
n.d.
1
n.d.
Limit
TestReport
No.: CE12011n1775Date: 2011t0i,22 page: lOof 23
CERAMTECGMBH
ll|l
Teat ltem (s):
Unit
Method
MDL
(CASNo.r002837-89- mgKg With referenceto US EPA5021method
HCFC-124
0)
Analysis
wEsperfomedby GC/MS.
HCFC-131
(CASNo.ro0O35S2& mg/kg With refercnceto LJSEPA5021method.
4)
Analysiswasperformedby GC/[,IS.
HCFC-132b
(CASNo.:001649-08. mg/Kg Withreferenceto US EPA8021marhod
7)
Analysiswasperformedby GC/MS.
(CASNo.:000075-88.mgkg Withreference
HCFC-133a
to USEPA5021method
7l
Analysis
wEsperfonned
by GC/MS.
(CASNo.:001717-00-mg/Kg With referenceto US EPA502t method
HCFC-'|41b
6)
Analysiswasperformedby GC/MS.
HCFC-142b
(CASNo.:000075$8- mg/Kg With referenceto US EpA 5021method.
3)
Analysis
wasperformed
by GC/I,S.
i|qFo-221 (CAS No.: 000422-26- mg/Kg Wathrefer€ncelo US EPA502.1method.
4)
Analysis
wa6performed
by GC/MS.
(CAS
HCFC-222
No.:00042249- mgikg Withreforence
to USEPA5021method.
1)
Analysis
wasperfomedby GC/MS.
HCFC-223
(CASNo.:000422-52- mg/kg Withreference
to USEPA5021method.
6)
Analysis
wEsperfomedby GC/MS.
HCFC-224
(CASNo.:000422-5+ mg/kg Withreference
to USEPA5021method
8)
Analysis,r€s performedby cC/[rS.
(CASNo.:000422- mg/K9 With referenceto US EPA5021method.
HCFC-225ca
s6-0)
Analysis
wasperformed
by co/lrs.
HCFC-22scb
(CASNo.:000507- mg/kg With referenceto US EPA502.1method.
55-1)
Analysis
wasperformed
by GC/MS.
(CASNo.:000431-87- mg/kg Wilh eferenceto uS EPA5021ma]iod
HCFC-226
8)
Analysis
waspertormed
by GC/MS.
(CASNo.:000421-94- mg/xg Withreference
HCFC-231
to uS EPA5021method.
3)
Analysis
wasperformed
by GC/MS.
HCFC-232
(CASNo.:000460-69- mg/Kg With referenceto US EPA5021method.
Analysis',/asperformedby GC/[,S.
(CASNo.:00712$84- mg/Kg Wth referenceto US EPA5021method.
HCFC-233
0)
Analysis
wasperformed
by GC/lrS.
(CASNo.:00042t94- mg/Kg Withreference
HCFC-234
to us EPA5021method.
Analysis
wasperformed
by GC/I,S.
.'lffturri!n
rhar iehb ato oder ons!.er he ran
r
iif
||t
Result
No.{
1
n,ct.
1
n.d.
1
n.d.
1
n.d.
1
n.d.
1
n.d.
'I
n.d.
1
n.o.
|||ll[]ll
Limit
n.d.
1
n.d.
'I
n.d.
1
n.d.
1
n.d.
1
n.d.
1
n.d.
1
n.d.
'I
n.d.
r1.
,h t 3ro cc,smaidsatumdd€
4duiLrzwN4iirper.'rLq/r,r,1rti,,ri
dds
..€ o: ohJ tr
ab m d '-b,,,
r. comFry s id,as arrM he d 6 ^Etost;i
autunzd db6nn
r.1 .-rrs6orrsrT
Menbaoihe565Grolp6cssA)
Test Report
No.: CE12O11121775
Dale| 201110i,22 Page: 11of 23
CEMMTECGMBH
Test ltem (s):
n!./Fu-zJc(uAu No.: 000460_92_
4)
HCFC-241
(CASNo.| 000666-22
3)
I||t!tt]
Unlt
Method
MOL
mdks Withreference
to LJSEpA502iiEE6E.
Analysas
wasperformed
byGC/MS.
mg/kg With referenceto US EpA 502i methori
Analysis
wasperformed
by GC/MS.
HUFU-Z4Z(9AS No.: 000460€3- msikg With referenceto US EpA 50tl rnelhod
s)
Analysis
w€sperfomedby GC/MS.
HcFc-243(CASNo.r000,{6G69- mg/Kg Withreference
to uS EPe-SDlTEihod-
Analysis
wasperformed
byGC/MS.
HCFC-244
msikg With referenceto LJSEPASO21method
Analysis\4€sperformedby GC/MS.
riL;FC-251
(CASNo.:000421-41- mg/Kg wirhreferenc€
tous EFASozi;;ifr;i-0)
An€lysis,,!asperformedby GC/ltS.
(CASNo.:OOO819-0Gmg/Kg Withreferenceto US EPA50-1 method
HCFC-252
1)
Analysiswasperformedby GC/MS.
HCFC-253
(CASNo.:000460-3t mg./Kg Withreference
to USEPA5021methodAnalysiswEsperformedby GC/MS.
HCFC-261
(CASNo.:00042G97- mg/Kg With referenceto US EPA5021method
3)
Analysiswasperformedby GC/[,S.
HCFC-262
(CASNo.:000421-02- mg/Kg With referenceto US EpA-O216ethod03)
Analysis
waspertormed
by GC/MS.
HCFC-271
(CASNo.:000430-55- mSikS Withreferenceto US EPA5021method
qnalysis
7)
wasperformed
by GC/MS.
Result
No.l
n.d.
1
n.d.
1
n.o.
1
n.d.
I
n.d.
1
n.d.
1
n,d.
1
n.d.
1
n.d.
1
n.d.
1
n.o.
Note:
'1.
mg/kg= ppm i 0.1M%= lOOOppm
2. n.d.= NotDetecled
3. MDL= MethodDetection
Limit
4."-"=NotRegulated
5. - = Qualitative
(NoUnit)
analysis
6. Negative= Undetectable
/ Positive= Detectabte
=
7. Asbestos: Negative "< 1.0%",Positive='> 1.0%,,
c o m F nryr " ? i r i : p : r . L + a i r ! 1 : 1 i L r 1 t : * ' r F i , r . * t r r l " . r r r . ,
y3ubjdbhcsm6coioioBdss
f u e e ' o n c l . m d d e l h e d q s b r d m s t h m A d s b i s d f u i l o f u ] m b l m d | d r ' ! .
nfui@ldsndld*'d'M3fu6deli
mLl atu ''b. ha rmh d crsr 'Bid
b'{y sro bcffr6d$E@mddc!
ndotudeB na b. qosdd
b lh! tu
tutf,
Limit
TestReport
No. : CE12O11121775O ale:201110i,22 Page:12ot 23
CEMMTECGMBH
l
[ill
ll[I[|l
PFOSR€ferenceInformation: Directive2006/I2ZEC
(l) Maynotbg placedonthe marketor us€das a substance
orconstituent
of preparations
in a concentration
equaltoor
higherthan0.005o/oby mas6.
(2) Maynotbe placedonthema*et in semi-finished
products
or€rticle6,
or partsthereof,if theconcenlration
of PFOS
i6equ€lto or higherthan0.1% by masscalculated
withreference
to thema6sof structurally
or microstructura
y
di6tinctpartsthatcontainPFos or,fortextires
orothercoatedmateriars,
if theamountof pFos is equartoor hlgher
than 1pg/m' of the coatedmaterial.
pbdud.repl'fu1
comFny irl r;1rrti:.ltii!:
rl,ii.jir!,*N:qa
'-i[]ri,
rir lr':
s6idb
6 Gd€d c.ddom or sou
j
rr;.!llll
bacFdda€plifu|w6o(pnor
Menbsots€5GsG,o!p66ssAl
TestReport
No.: CEl28lnlns
Dde | 20111O2J22
P age: 13of 23
CERAMTECGMBH
ul|[flrr|||||tt
1) Thes€samples
weredissolved
totallyby pr+conditioning
methodaccording
to belowflowcnan.
r Cf' teslmethodexctuded
)
2) Nameof thepeFonwhomademeasurement
yang
Climbgroat
3) Nameofthe personin chargeof measurement:
TroyChang
Acid digestionby suitableacid
depended on different sample
material(as belowtiable)
l\ricrowEve
digestionwith
HNO3/HCyHF
Addappropiateamountof
digestion
reagent
Heatto appropriate
temperature
to extract
Cool,filterdigestate
1) AlkaliFu6ion
2) HClto dissolve
ICP.AES
Adddiphenylcarbazide
for
SampleMaterial
Steel,copper,aluminum,
solde.
DigestionAcid
colordevelopment
Aquaregia,HNO3,HCl,HF,HrOz
measurelhe absorbance
Glass
HNO3/HF
palladium,
Gold,platinum,
c€ramic Aquaregia
at 540nm by UV-VIS
Silver
HNO3
Plastic
HrSO1,HrOr,HNO3,HCI
Others
Anyacidto totaldige6lion
!til:::
throughfilter
l!rii:rii1!E;lqi
]'**ir
4:\-.r:t;'|.
!6'dbtG.mdcod,orods3tr
ri:{'iE':l
s|yldub'nha|frbdc|skndd
ba Gpdu€d
ffid
i tu r. w hod pffi
Md.d$!i65c6!p66s3^)
TestReport
No. I CE12011121775Date.2011lOZ22Page:14of 23
CERAMTECGMBH
ltNl t]|l|||ltl!|l
ChlorinatedFlameretardantanalyticalflow chart
1) Nameofthepersonwhomademeasuremenl
BanyTseng
2) Nameof thep€rsonin chargeof measurement:
TroyChang
I
r
Reference
method:
USEpA8270D,USEpA3540
Testltems:PCRS,
PCNS,pCTs,Mir€x.Cp MCCP
Data
k1s) bdd
rh6 6sr epd
cmd
re €pbdud,
eEpr
n tu
rfud6!n6d5$uedb,[email protected]
n.
"@.
oi
"o"r.,td.
-,Brd d
adq
Test Report
No. I CE12O11121775 Date'.2011tO?,22P a g e : 1 5 o f 2 3
CERA['TECGMBH
I[| ||tt
Analysisflow chartfor determinationof pVCin material
1) Nameofthepersonwhomademeasufemeft:
EvaChao
2) Nameofthepe6onin chargeof measurement
ShinjyhChen
Samplepre{reatment
Sampl€analfzedby FTIR
Checkwavsnumber
of C-Clbonding
resd rh 3bsrcp.d €^id be€
n mrhs rdd€pd €re,oi y b se samprels)
rr'rrl
rii!:!- rj!:F '(rri"lli f-i[A+ rrr":sitit.r]:
ysubjdbGG.n€ccnidloBds6rusgifuodd3€adaonreq@
isb t sro cc
sdaidsa@isl
*ibdgdmtsspp6€oilhacmp
|lttt||l
TestReport
No.: CE12O11121775
Dale:2011102j22 Page: 16of 23
CERAMTECGMBH
rt fltu [ttttl!
Analytical flow chart of Soxhlet extraction (LC/MS)procedure
1) Nameof thepersonwhomademeasurementt
LydiaFu
2) Nameof thepersonin chargeof measurement
Shinjyh
Chen
. Benzotiazote
rTest ltems:PFOSiFFOA
SamplepreueatmenUseparation
Data
r nr.:;. l,{li.t;.lrfi
F.
lhsdmsnsgedbylbcmFry9sFdlobcs.klGdi6so'sfr
;,rtjl:n.{r\
3(s) r€d€d rhs bi
r lIr.i|]
_lxjf,t
rePd eindr & rc
bgrcFdudssplniu|dodpnol
Test Report
No.: CA2U1121775 Dale:2011102.22Page 17ol 23
CERAMTECGMBH
t||m||!l] t!l!ll
Analltical flow chartof Soxhletextraction(GC/MS)procedure
1) Naneof lhe pe6onwhomademeasurement:
LydiaFu
2) Nameof thepersonin chargeof measurem€nt:
ShinjyhChen
, Benzoldazole
, HBCDD, Np DBBT.
I Testltems:Phth€late
Organicphosphorus
compounds
Data
,rn::::
ftEdmem3ssledbyh€comFry
l,{t: ai1!nr;tlin'
r}!,,,ti!.{r
€G) rdsd rhs bn €pd
- r i.iir.
_ar:_,j
€fid
be fe'
TestReport
No.: CE12011/21n5 Daie:2O11lO2n2Pagei18of23
CEMMTECGMBH
lltfl
lt
||tlt|l
Analytcal flow chartof Organic-Tincontent
1) Nameofthe pe6on whomademeasurement:
GinnyChen
2) Nameoflhe per6onin chargeof measurement:
TroyChang
Conc€ntrate/Dilute
Extracted
solution
Analysis
wasperfomedby GC/FPD
Data
; - + = r ! , Y ; 1 ; n J i r : i r " R {' [ e i i - a ] r . E d r i l , 1 . r . i ; r i , ! x
ior.Ldro(,omd dduffib 3uqd
tuemn idron
ad lmsd d oi ssu6 ei
cunedhmAtetuoisdwf ldrhaimrarsdrob'rr
Test Report
No.: CEl2011l21TI5
Date: 201|1|
tO2nZ page : 19of 23
CERAMTECGMBH
|l][
] tfttlll
Analytical flow chart of halogen content
1) Name
oftheperson
whomademeasurement:
RitaChen
2) Nameoftheperson
incharge
ofmeasuremer{:
TroyChang
Samplepretreatment
/ SeDaration
Weighting
andputtingsamptejn cetl
OrygenBombCombustion
/ AbsorDtion
Dilution
to fxed volume
Analysis
wasperformed
by lC
l:::::r
'rI:jJr(ilt.lqji
rri-Ili
r,;hA*
ysubjdbbGsi66coidloi3d$
j:j
7.r
.r'!:l
mL}diowbih.Iobdc|sk'ndd
batsFdd
sspr
niur whod',o,"dena@od
,ri:
i rrfiii.
dhs c!mM!
rrrs6lrrs14
k!
lBddzm
rF€ibn
Test Report
No.: CEl201'1121775
Date:2O11|OZ22 Page: 20of 23
CERAMTEC
GMBH
ll n|llrl[
Analysisflow chartfor determinationof Asbestos
1) Nameof thepersonwhomademeasuremer*:
VictorKao
2) Nameof thepe6onin chargeof mea6urement:
WendyWei
Diffractionpeakof
asbestosi5 absent
Asbestosidentificationby
opticalmicro€copy
Asbestos
fiberis pre6ent
Containing
Asbesios/
Positive
Asbesto6
fiberis absent
Notcontaining
Asbestos/
Negative
eG) r8s€d rhs bn €pod Bfid
b.3dMrcbs'dum$b
suqd
be le'
tumdhrn
Arbdon stuwiroo.,middor
rabt,
Iecpd|d€K.plnju|vlhdplo
.,^ l
..r*--".
ePmer orhe 5Gscrtua t$5 ra)
l[|r
TestReport
No. I CEl2011l21Tl5 Dale| 2011102122Page:21cf.23
CERAMTECGMBH
l[t[][1[]||[I|
Analyticalflow chart
1) Nameof thepersonwhomademeasurement:
RomanWong
2) Nameof thepersonin chargeof measurement
TroyChang
r TestItems:PBB/PBDE,
TBBP-A.bis
Firsll€slingproc€ss-+
Optionaiscreen
process---.
Screenanalysis
SamDle
extraction
method
J
@
V
F ler
AnalysisbyGC/I,S
t
lssueRepod
baeFdud8spli'd|w|hodplo'
process-.>
Contimation
Test Report
No. : CEl2011
121775 Dale : 2O11102122 paoe | 22 ot 23
CERAMTEC
GMBH
llt
Analytical flow chart of volatile organic compounds (VOCS)
1) Reference
method: USEPA5021
2) Nameof thepersonwhomademeasurement
: D€lkiYen
3) Nameof thepe6onin cha.geof measurement
: Shinjyh
Chen
Samplepretreatment
Takesampleandputit into
glasswale.
headspace
Bakelhesamplein theoven
Analysiswas perfomedby GC/IiS
cons^!|",]..i]].l|.71]n]'!rii.:i-1]]!r|1ji''{
subjdbcGei6dcoidtomdsefo
Fsh t sro tc€daidbsdotumn
||[][]|lt|r
TestReport
No.: CE12011/21n5Dale: 2011102n2 Page: 23of 23
CERA[/ITECGl,ilBH
tt][]tI|
21775
*. Endof Report *'
i-:.-:
nf oo*oc
!r:ll-tnllr*qi
toma d@uMds tubrdl
r+i':i,
{-rrliriil
e(st€sd th s red €p5. eiiot e re
i. . i-.c irt!
.rnenhm Aretuoi sdGwiiorhe 'mbrsd!€b'9
] m1!
Test Report
Applicant:
Number : TWNC00194906
Littelfuse, Philippines Inc.
LIMA Technology Center, Lipa City,
Malvar, Batangas
Date
: Mar 17, 2011
Sample Description:
One (1) group of submitted samples said to be :
Part Description
: Silver Clad Cu wire with 2 mass % Ag
Part Number
: 082684
Date Sample Received
: Mar 14, 2011
Date Test Started
: Mar 15, 2011
Test Conducted :
As requested by the applicant, for details please refer to attached pages.
Authorized By:
On Behalf Of Intertek Testing Services
Taiwan Limited
K. Y. Liang
Director
This report shall not be reproduced
except in full, without the written
approval of the laboratory.
Page 1 Of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00194906
Test Conducted
(Ⅰ) Test Result Summary :
Test Item
Heavy Metal
Cadmium (Cd) content
Lead (Pb) content
Mercury (Hg) content
Chromium VI (Cr6+) content (mg/kg with 50cm2)
Result (ppm)
Silvery Metal
ND
ND
ND
Negative (< 0.02)
Remarks: ppm = Parts per million based on weight of tested sample = mg/kg
ND = Not detected
<
= Less than
mg/kg with 50cm2 = milligram per kilogram with 50 square centimetre
Negative = A negative test result indicated positive observation
was not found at the time of Test.
Responsibility Of Chemist : Irene Chiou / Kevin Liu / Cathy Chen
Date Sample Received
Test Period
: Mar 14, 2011
: Mar 15, 2011 To Mar 17, 2011
(Ⅱ) RoHS Requirement:
Restricted Substances
Cadmium (Cd) Content
Lead (Pb) Content
Mercury (Hg) Content
Chromium VI (Cr6+) Content
Limits
0.01% (100ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for
homogeneous material.
Page 2 Of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00194906
Test Conducted
(Ⅲ) Test Method:
Test Item
Cadmium (Cd)
content
Lead (Pb) content
Mercury (Hg)
content
Chromium VI (Cr6+)
content
Test Method
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 7, by microwave
digestion until the tested samples are
totally dissolved and determined by
ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in annex B, by boiling water
extraction and determined by UV-Vis
spectrophotometer.
Reporting Limit
2 ppm
2 ppm
2 ppm
0.02
mg/kg with 50cm2
Remark: Reporting limit = Quantitation limit of analyte in sample
Page 3 Of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00194906
Test Conducted
(Ⅳ) Measurement Flowchart:
Test For Cd/Pb/Hg/Chromium (VI)
Reference Standard：IEC 62321 edition 1.0:2008
Sampling/grinding or cutting
Cd/Pb/Hg
Cr
Polymers /
Electronics
Metal
For different
material, digest
the sample with
*1
appropriate acid
By spot test
Negative
Confirm the tested
samples are
totally dissolved
Make up with
deionized water
6+
*2
Weigh sample
and add
alkaline
solution
Get 50cm2 sample
Definite temp.
extraction
Boiling water
extraction
Cool and filter
the extract
Analyzed by ICP-OES
Make up with deionized
water and add diphenylcarbazide solution
Remarks:
*1: List Of Appropriate Acid：
Material
Polymers
Metals
Electronics
Analyzed by UV-VIS
Acid Added For Digestion
HNO3,HCl,HF,H2O2,H3BO3
HNO3,HCl,HF
HNO3,HCl,H2O2,HBF4
*2: If the result of spot test is positive, Chromium VI would be determined as detected.
End Of Report
Page 4 Of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00194906
Test Conducted
Photo
Page 5 Of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Test Report
Applicant:
Number : TWNC00194902
Littelfuse, Philippines Inc.
LIMA Technology Center, Lipa City,
Malvar, Batangas
Date
: Mar 17, 2011
Sample Description:
One (1) group of submitted samples said to be :
Part Description
: Silver Clad Cu wire with 5 mass % Ag
Part Number
: 082375
Date Sample Received
: Mar 14, 2011
Date Test Started
: Mar 15, 2011
Test Conducted :
As requested by the applicant, for details please refer to attached pages.
Authorized By:
On Behalf Of Intertek Testing Services
Taiwan Limited
K. Y. Liang
Director
This report shall not be reproduced
except in full, without the written
approval of the laboratory.
Page 1 Of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00194902
Test Conducted
(Ⅰ) Test Result Summary :
Test Item
Heavy Metal
Cadmium (Cd) content
Lead (Pb) content
Mercury (Hg) content
Chromium VI (Cr6+) content (mg/kg with 50cm2)
Result (ppm)
Silvery Metal
ND
ND
ND
Negative (< 0.02)
Remarks: ppm = Parts per million based on weight of tested sample = mg/kg
ND = Not detected
<
= Less than
mg/kg with 50cm2 = milligram per kilogram with 50 square centimetre
Negative = A negative test result indicated positive observation
was not found at the time of Test.
Responsibility Of Chemist : Irene Chiou / Kevin Liu / Cathy Chen
Date Sample Received
Test Period
: Mar 14, 2011
: Mar 15, 2011 To Mar 17, 2011
(Ⅱ) RoHS Requirement:
Restricted Substances
Cadmium (Cd) Content
Lead (Pb) Content
Mercury (Hg) Content
Chromium VI (Cr6+) Content
Limits
0.01% (100ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for
homogeneous material.
Page 2 Of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00194902
Test Conducted
(Ⅲ) Test Method:
Test Item
Cadmium (Cd)
content
Lead (Pb) content
Mercury (Hg)
content
Chromium VI (Cr6+)
content
Test Method
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 7, by microwave
digestion until the tested samples are
totally dissolved and determined by
ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in annex B, by boiling water
extraction and determined by UV-Vis
spectrophotometer.
Reporting Limit
2 ppm
2 ppm
2 ppm
0.02
mg/kg with 50cm2
Remark: Reporting limit = Quantitation limit of analyte in sample
Page 3 Of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00194902
Test Conducted
(Ⅳ) Measurement Flowchart:
Test For Cd/Pb/Hg/Chromium (VI)
Reference Standard：IEC 62321 edition 1.0:2008
Sampling/grinding or cutting
Cd/Pb/Hg
Cr
Polymers /
Electronics
Metal
For different
material, digest
the sample with
*1
appropriate acid
By spot test
Negative
Confirm the tested
samples are
totally dissolved
Make up with
deionized water
6+
*2
Weigh sample
and add
alkaline
solution
Get 50cm2 sample
Definite temp.
extraction
Boiling water
extraction
Cool and filter
the extract
Analyzed by ICP-OES
Make up with deionized
water and add diphenylcarbazide solution
Analyzed by UV-VIS
Remarks:
*1: List Of Appropriate Acid：
Material
Polymers
Metals
Electronics
Acid Added For Digestion
HNO3,HCl,HF,H2O2,H3BO3
HNO3,HCl,HF
HNO3,HCl,H2O2,HBF4
*2: If the result of spot test is positive, Chromium VI would be determined as detected.
End Of Report
Page 4 Of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00194902
Test Conducted
Photo
Page 5 Of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Validi
ForQuesll
PleaseCo
Test Report
No.: CE/2011/M953
Dale | 201111?J01
POLYFILAG
OBERALLMENDSTMSSE2OA,CH63OOZUG / SWITZERLAND
Thefollowingsample(s)was/weresubmiltedand identlfiedby/onbehalfoflho clientas:
Ni36Fe64tAg7%o
'114894
2011t11t25
2011I 11t25TO 2011tlzol
SampleD€scription
Buyer/OrderNo.
Date
SampleReceiving
TestingPeriod
Pleasereferto nextp€ge(s).
Test Result(s)
{Nw
, i 1 J jn r ' , ! i i : i . t n
c o m e a ni :y; f r , . .! l r l ! i i ' i . 1
,*,l,a b,ri. c".p"
ir
g,beiro i"-"
" a;.-s
r- "i*i'*r ro,'a
"n&oni(,
,"o-",i
-o"
e*oa * ,**;
"r
*n
oli*aw"n.i.racrn"
b-.;dB,G6nd
ad?
d
{i.ril
aa conam^ t' ea
.
pr'(s) resbd rhs rs3tdpo. dnnd b
:,1 'rLlJiilr!'
nown
ithscs
Page:'l of 7
ilt] l||rt]|llllll
Test Report
No. : CE/2011/84953
Page:2 ol7
Oate.2O11l12lO1
POLYFILAG
OBEMLLMENDSTMSSE 2OA,CH63OO
ZUG/ SWITZERLAND
Ta6t Resultl6)
PART MME No.1
t|||t]||t
tll[l
SILVERCOLOREDIVETALWIRE (|NCLUDINGTHE PLATINGLAYER)
Unlt
T€61 ltem(5)
moL
Method
mg/Kg Withreference
to IEC62321:2008and
Cadmium(Cd)
Lead(Pb)
(Hg)
Mercury
Hexavalent
Chromium
Cr(Vl)
oerfomedbv ICP.AES.
mgKg With referenceto IEC62321.2008and
pedormed
by lCP.qES.
mg/Kg Withreference
to IEC62321:2008and
perfomedby ICP-AES.
Withreference
to IEC62321r2008and
perfomedby Boiling',!aterextraolion
Method.#
2
Result
No,l
n.d.
n.d.
2
n.dNegalive
Sumof PBB5
Monobromobiohenvl
Dibromobiphenvl
n.d.
n.d.
n.o.
Tribromobiphenyl
n.o.
TetrabromobiDhenvl
PentabromobiDhenvl
Hexabromobiohenvl
5
n.d.
Heplabrornobiphenyl
Octabromobiphenyl
Nonabromobiohenvl
Decabromobiohenvl
n-d.
5
5
n.d.
n.d.
5
5
n.o.
n.o.
n.d.
With referenceto IEC 62321:2008 and
Sumof PBDEa
Monobrcmodiohenvl
ether
mg/Kg perfomed
by GC/MS.
n.d.
Dibromodiohenvl
ether
Tribromodiohenvl
ethgr
Tetrabromodiohenvl ether
5
5
n.d.
5
5
n.d.
n.d.
n.d.
n.d.
ether
Octabrornodiphenyl
5
5
5
5
ether
Nonabrcmodiphenyl
Dec€brcmodiohenvl
ether
5
ether
Pentabromodiphenyl
Hexabromodiohenvl
ether
Heptabromodiphenyl
ether
c o m o , ni vi , r l r i l , r i i l i l ' r r - J : ,
rh,s dd,men, s *usd by be cmpa
r ,t l , l i r , j . l F
*it.ll
n.o.
n.d.
n.d.
n.d.
n.d.
ft€ G! epod annd b
PraG)rasbd
't.rltlijt!!!.
hdreonGfracb16 compaf,v3liidhqs
o i | y a i d v ' h ] n l h 6 f i t d c s l s ] n s p s g b ' t } l s b c c { e d a . d l h s d o a m
i.G"t -r.'ieM
oi h" -"bd
r:iIr'r,
i1ldJt,.l'e6(02)2eet,
rre6{o?)zeett
lwasm
TestReport
No.: CE/2011/M953
Page:3 of 7
Oaie| 201111i,01
rtl
POLYFILAG
OBEMLLMENDSTMSSE 2OA,CH$3OOZUG / SWITZERLAND
Test ltem(s)
Unit
ethod
Halogen
(F)
Halogen-Fluorine
(CASNo.:14762-9+8)
(Cl)
Halogen-Chlo.ine
(CAS No.r22537-15-1)
(Br)
Halogen-Bromine
(CASNo.:10097-32-2)
(l)
Halogen-lodine
(CASNo.:14362-4+8)
With referenceto BS EN 1458212007
.
mg/Kg
Analysis
wasperformed
by lC-
MDL
ttttlt
lttr
Result
No.l
50
n-d-
50
n.d.
50
n.d.
50
n.d.
Note:
= 1000ppm
1. mgikg= ppm i 0.1wP/o
2. n.d.= NotDetected
3. [,,lDL= MethodDetectionLimit
4."-"=NotRegulated
(NoUnit)
analysis
5. '" = Qualitative
6. # = a. Positivemeansthe presenceof C l on the testedarcas
b. Negalivemeansthe absenceof CrVl on the testedareas
Thedetected
concent.ation
in boiling-wEter€xtraction
0.02mg/kgwith50cm'
solutionis equalorgreaterthan
testedareas.
7. Thesample(s)
wEsi/vere
analyzed
on behalfofthe applicant
as mixingsamplein onetestingTheaboveresult(s)
was/weeonlygivenas the informality
value.
c o m o afn" v, l r l l r l , r : - r i " i r , r r l l l: :i t r i
rh8 dmenr
s 'sed
i Ix
ddil\
prec)r.s€d rh 3 bi r+dd ennd b
i'r'lnLirnlt'
by he company aqad b b 6s€r.r cddd r di3 br s
suh.d 10 rems aid cotuions tor E
ane on B drawn 10 he rmtaron oi 'ab It
poigbly9btcl.daidlhsdodm
t^
tls6ol?zeett
ww!!.on
sAr
Memb.oiihescscoup1s4s
TestReport
No.I CE/2011/84953
Dale'.2011h201
POLYFIL
AG
OBERALLMENDSTRASSE
2OA,CH6300ZUG/ SWITZERLAND
Page:4 of 7
trtN[[tN tI|tttl
'1) Thes€sampleswercdissolved
totallyby pre-conditioning
methodaccordingto belowflow chart.
( Cr- test methodo(cluded)
2) Nameof theperconwhomademeasurement
Climbgreat
Yang
3) Nameof the personin chargeof measurementTroyChang
Acid digestionby suitableacid
d€pendedon differentsample
material(as belowtable)
Add appropriateamountof
digestion
reagent
Heatto appropriate
temperatureto extract
Cool,filter digestate
1) AlkaliFusion
2) HCltodissolve
ICP-AES
throughfilter
Adddiphenyl-carbazide
for
SampleMaterial
DigestionAcid
colordevelopment
Sleel,copper,aluminum,
solder
Aquaregia,HNO3,HCl,HF,HrO,
Glas6
HNO3/HF
measurethe absodance
Gold,pldinum, pelladium,cerafiic
Aquaregia
at 540 nm by UV-VIS
Silver
HNO3
Plastic
HrSO., HrOr,HNq, HCI
Others
Anyacidto totaldigestion
c m o a d vr : r l ! /
qll,r-nl
tIrrlJr':i::ti..,,
fn
{ti.L\
preG)En6d rh s lsd r4od ennd €
' .rn rrtllll'
&qed b rems aid condrldis ror E
3pssibll}"btcled,ndlh3doo
nD r's6(0r)2eett
*d.a'eh
Test Report
No.: CE/2011/M953
Page:5 of 7
Dale: 2011112J01
POLYFILAG
OBERALLIVENDSTRASSE
2OA,CH€3OO
ZUG/ SWITZERLAND
ll
|l[]tIt]tttl
PBB/PBDEanalyticalFLOWCHART
1) l,larEof thepersonwhomadefieasurenEnt:
RormnWong
2) lhme of thepersonin chargeof nEasurementTroy Chang
Firsttestingprocess-----;
Optiomlscre€nprocess-.-process - .>
ConfiftrEtion
Screenanatsis
Safiple e{raction/
Soxhlet rnethod
ConcentratdDilute
E{racbd solution
Filter
Analysisby GC/[4S
c o m p a dhyi r i , : i r , L i ' i r . , r i l
li:jri
i.tf
l$:li.
mpbG)r63€drhs€d €Fd€iiolb
ir'r.,
ritlt.
abjed ro rems aid coMmonsror E
uhdsqiz6e NturaiFr.'yrirv4/!
Ahedrons dr&n 10th€ n raron or I'ab t'
tnrr:
t
, lel1,,,i+s6orrD
Test Report
No.: CE,2011l84953
Date| 2O1111?J01
POLYFILAG
OBERALLMENDSTMSSE2OA,CH€3OO
ZUG/ SWITZERLAND
Page:6 of 7
llllflI|
Anallticalflow chartof halogencontent
1) t{anEof thepe6onwhorEde rEasurernentt
RitaChen
2) NarE of the personin chargeof nEasurernent:
TroyChang
Safiplepretreatrnent
/ Separation
Weighting
andputtingsafipb in cetl
OxygenBombCodbustion/ Absorption
Dilutionto fiy€dvolunE
Analysis
wasperfornEd
by lC
c o m o a nt rvr i , , l , i r l
id6(s)
rii'ilr,
liirriJli
i:i.tfi
l+4trl
b3r6d rh s r€d 6pd
, I . r . ^ E r, l l r l ! i { .
eniol
b
Th3@mnI5's!.dby6ecom9any$bjedbb6e6|cdnd!oBdse
s l b ] e d I o T e m s a | d e d i o n s f o r E A l b n l o n s & a w . l o h e | f i b l o i d ' a b ' i y '
aspmsb It is b c cred ,id ri s dod
||t[]|l
TestReport
No.: CE/2011/84953
Dalei 20'1111201
Page:7 of 7
POLYFIL
AG
OBEMLLMENDSTMSSE
2OA,CHS3OO
ZUG/ SWTZERLAND
i|||||!tr
fitl|{l
'The testedsample/ part
is ma*ed by an arrowif ifs shownon the Dhoto.,
'* EndofReport..
I h6bd
retsn d'srybhasmp6G)
c o m p a n y , i i /; ;r ,i r l , d l i r U , t ; i t : \ t t i l i l . i . t l i
id6mi idon
adrri&jdion
lL:i"-:llll*ll'::'1111-'
s$s
d
lll:l?ii
it!.t,l\
s'
i'"j
bjsd
rhsbd
ropodemdb€
t n, ^4,1,1rl!!.
sd,sdsddomdo;odand
i;"*
$. c".p.ry
hd
h: ?'pi"t ' $b"*"nsb"v a rors o sd aidh,[email protected],do*
"i.G
"
"s"dr.
NI dme6'; F;$rcs
mB
;turdeeii;he13*
:,:,tl:::ririiru
rtrM{o:)zeerr
Fiy
hs d6rbrd;
Aiy d,,soRd
f re6or)rer,
arsaibi
!,w!!ai
MenF oiihe rs Gdp {s6sr{)
Validi
nown
ForQueEll
PleaseCo
Test Report
No.: CEl2011184955
Datet20'1111201
POLYFILAG
OBERALLMENDSTMSSE2OA,CH€3OOZUG / SWITZERLAND
ithscs
Page:'l of 7
ll]uttfi
[[m
Thefollowingsample(s)wa3/weresubmitledand identitiedby/onbehalfof the clientas:
SampleDesciption
Buyer/OrderNo.
SampleReceiving
Date
TestingPeriod
Ni42Fe58MCuMAgs%
11-0803
2011t11t25
2011t11t25'l O 2011I 1'J01
T€stResult(s)
Pleasereferto nextpage(s).
(NW4E
f,lmdiorrd
Or.rlcd l,.bor|b.t - Trlpd
ps(31i€ded rhs ied rcpod eiior be
cwpanye
!,
rt
rr-ri'f.,ri,il]ilntlli ir ].ri
iiil-:i I
ny tublsd b b Gene6 coideoB d se
1,.
|.lrrrr?!t!:.
dbis r aiy'Iha cohpantssoo r69onsbiI s b r ct'odaddrhs dodm
! hdsrLrzore.N4lrFr .o ri p,i /F L I I|t,
f: lFt
. ,;,i+ @610?)ree
14 | + 8610r)2ee
ry
(w ar.on
TestReport
No.: CE/201
1/84955
Page:2of 7
Dale: 2111/12t01
POLYFILAG
OBERALLI\4ENDSTMSSE
2OA,CH63OO
ZUG/ SWITZERLAND
lm[tmlrltttll
Test Reault{s}
PARTNAMENo.1
SILVERCOLOREDI'ETAL WIRE (INCLUDINGTHE PLATINGLAYER)
T66l ltem(s)
Unit
Cadmium(Cd)
Method
mSikS Witheferenceto tEC62321:2008and
perfom€dby lCPdES.
mgKg Withreference
to IEC62321:2008and
perfomedby ICP-AES.
mg/Kg Withreference
to IEC62321:2008and
pe.formed
by ICP-AES.
Withreferenc€
to IEC6232'1:
2008and
performed
by Boilingwaterextraction
M€thod.#
Lead (Pb)
(Hg)
Mercury
Hexavalent
Chromium
Cr(Vl)
Sumof PBB9
l\4onobromobiphenyl
Dibromobiphenyl
Tribromobiphenyl
Tetrabromobiphenyl
MDL
2
R6sult
No.l
n.o.
2
2
n.d.
Negative
n.d.
n.d.
n.d.
n.d.
n.d.
n.d.
n.d.
n.d.
n,d,
n.o.
5
5
5
Pentabromobiphenyl
Hexabromobiphenyl
Heptabromobiphenyl
Octabromobiphenyl
Nonabromobiphenyl
Decabromobiphenyl
Sumof PBOE3
Monobromodiphenyl
ether
5
mgikg
Withreference
to IEC62321:2008and
per{ormedby GC/lrS.
DibromodiDhenvl
ether
TribromodiDhenvl
ether
Tetrabromodiphenyl
ether
PentabromodiDh9nvl
ether
Hexabromodiohenvl
ether
Heplabro.nodiphenylether
5
5
n.d.
n,o.
5
5
5
n.d.
n.d.
n.d.
n.d.
5
n.o.
n.d.
5
5
5
Octabromodiphenvl
ether
NonabaomodiDhenvl
ether
n.d.
n.d.
n.d.
Decabromodiohenvl
ether
c o m o a n yi r r l ! /
tu.f-]i'
I rlirlltr] ntlrli
n,o,
I
:.i
i
^r!.l;li,
I r.. r.i. rriilA.
L@nnieroi
aidllr edd'on $@3 d
onry3id*ib'.lhormrrsorcenrsnsrld'on.f,'ryth6compaiyssecsponsurrysiobc,enraidhcdm!
iidbe€pduedexeptniur*6oq
!^r+s6(0nreenr
@! a!@n
M€f,be,or 'he 5616,@p (s6sr{)
TestReport
No.: CFJ2011184955
Page:3 of 7
Dale:2O11h21O1
POLYFIL
AG
OBEMLLMENDSTRASSE
2OA,CH-6300ZUG/ SWITZERLAND
Testltem(s)
Halogen
Halogen-Fluorine
(F)
(CASNo.:14762-9+8)
Halogen.chlorine
(Cl)
(CASNo.:22537-15-1)
Halogen-Bromine
(Br)
(CASNo.:10097-32-2)
Unit
lrethod
With refe.enc€to BS EN 14582].2007
.
mg/Kg
Analysis
wasperformod
by lC.
Halogen-lodine
(l)
(CAS No.: 14362-4,4-8)
|l]rl||l]
MDL
t[]||n
Result
No.1
50
n.d.
50
n.d-
50
n.d.
50
n.o.
NoteI
1. mg/kg= ppm; 0.1wt%= 1000ppm
2. n.d.= NotDetected
3. [4DL= MethodDetection
Limit
4."-"=NotRegulated
5. " = Qualitative
(NoUnit)
analysis
=
6. # a. Positivemeansthe presenceof CrVlon the testedareas
b. Negativemeansthe abgenceof CrVlon the testedareas
Thedetected
concentration
in boiling-wEter€xtraction
6olution
is equalor greaterthanO.O2
mg/kgwithS0cm,
testedareas.
7. The6ample(s)
was^rereanalyzed
on behalfoftheapplicant
as mixingsamplein onetesting.Theaboveresult(s)
was^^€re
onlygiv€nas theinformality
vaue.
c m e a i ya r | 1 l l r ' r d 1 1 ' t , r , i i l l , n r 4 L . i . r 1
iirl4li
r3G)rssrd rh I r€d'+on €nnd e '
ir'r'r Nlttll\.
tfi r:li {:/:rFi4,t;r+s6Frtreer7e r}s6Or)xerr
Ewar.on
Test Report
No.: CEl2011/84955
Paget 4 of 7
Dale:2011h2101
POLYFILAG
OBERALLMENDSTMSSE2OA,CH-6300ZUG / SWITZERLAND
t[| tl
rrr ]l
'1) Thesesamples
! €re dissolved
totallyby prcconditioning
methodaccording
to belowflowchart.
( Cf' test methode(cluded)
yang
2) Nameof the personwfiomademeasurement:
Climbgle€t
3) Nameof the personin chargeof measurement:
TroyChang
Cutling/ Preparation
Aciddigestion
by suitable
acid
dependedon differentsample
matedal(as belodtable)
Add appropriateamountof
digestion
reagent
Heatto eppropriate
temp€ratueto extract
Cool, filter digestate
1) AlkaliFusion
2) HCltodissolve
ICP-AES
throughfilter
AdddiphenyFcarbazide
for
SampleMaterial
colordevelopment
DigestionAcid
Steel,copper,aluminum,
solder
Aqua regia,HNO3,HCl,HF,HrO,
Glass
HNO/HF
measure the absorbance
Gold,platinum,palladium,ceramic
Aqua regia
at 540 nm by UV-VIS
Silver
HNOs
Plastic
H,SOI, H'O', HNO3,HCI
Others
Anyacidtototaldigestion
rlrlt
c f f i o . n yB : . 1
t-f
i,l'irl!
!,i
i,.t'l
lii]]irl)
! rd4krzE,
'r
1rItihl-
Nlwri @.ry.tuM{/}i.:
r ;r
+1 r rtLtri,ni+ s6 orrree
Test Report
No.: CE/2011/84955
POLYFILAG
OBEMLLMENDSTRASSE2OA,CH€3OO
ZUG/ SWITZERLAND
|t
PBB/PBDEanalyticalFLOW CHART
1) Name
of theperson
whorEdenEasurer€nt:
RormnWong
2) Mrneof theperson
incharge
of fipasurenEnt:
TroyChang
Firsttestingprocess----+
Optional
screenprocess---process - .>
Confifination
Scfeenanalysis
Sanpleextractiort
So*rlet nEthod
ConcedtratdDilute
Extractedsolution
Filter
Analysisby GCiMS
kriue Relp-l1
c o m p a n yG i ! I
rltl
ri-11'!,liill,lnll].i
tudois
i
.Ir;
riit!-l
]
p3G)!6ied rh s ied €pd eiio,
r'rr.l,ljrll.
rary rh,ComFnys30eGspdisb
r1l6b
Page:5 of 7
Date| 2011h2t01
bddnraidrbsdoem
be
r |l t[]
]l
TestReport
No.: CE/2011/84955
Page:6 of 7
Date 2011,1|:]01
POLYFILAG
OBERALLIVENDSTRASSE
2OA,CH$3OO
ZUG/ SWITZERLAND
rt][]|l
rtl[]ll
Analltical flow chart of halogen content
1) Narneofthe pe6on who rcde fiEasurenEnt:Rita Chen
2) Narneof the person in charge of rEasureient: Troy Chang
SaftplepretreatnEnt/ Separatbn
Weightiryandputting
sanplein cell
OrygenBombConbustion
/ Ahsorption
Dilution
to fixedvolunE
AnalysiswasperforfiEdby lC
cdnp,iy til ,il irl,rlli'i
r l r r r j r J ,n j r l ; .
{i!-rL\
.,, tF
Th s dofuneil 6 'sued h' 6e c onpa
$bjed b tens &d cdidrrois rof E
I
mp31s)rsded nE bd rcpod.aiioi b
r1",1."inr'!.!.
Abnron
nndbaBFdu4detepiilui.whou
6 drtun ro be rmlarioi o, abit
Test Report
No.: CE/2011/84955
Page.7of 7
Dai.e| 2O11112J01
POLYFIL
AG
OBEMLLMENDSTMSSE
2OA,CH{3OOZUG/ SWITZERLAND
][|l
||ttl
' Thetsgtedsample,/pa is ma*ed by an
anow if ifs shownon the photo..
" Endof Repod*'
a o h p a n y, : j f r : | t r j , f _ i '
r , r i r r , , l :i l r l ) : i . . . ! , i
r.{ttLa I
p3(sliseedrhs Gd rcpodeiiolbe
1". ' 1., ijl lt:.
h0r iq6 $d obrrgdioEundartu ra
LnLt:i ,+ = [E?4 ),t+ 86 \a2vee
Mem6edrhe scsGrclp6cssAr
l
Validit
nown
ForQues-ti
PleaseCo
Test Report
No. : CE/2011/84958
l
The following sample(s)was/weresubmitted and id€ntifi€d by/on behalf of the client a6:
SampleDescription
Buyer/OderNo.
Date
SampleReceiving
TestingPeriod
TeEtRoault(a)
Page:1of7
Dale: 201111?,01
POLYFILAG
OBERALLMENDSTMSSE2OA,CH-6300ZUG / SWITZERLAND
Ni99.9
+1357
2011t11t25
201Ih1t2510 201II12t01
Pleasereferto nexlpage(s).
glnaa forrnd
Or..| cd L-or.tory - flhd
mpr.G)r.sbdftr3 b..epdd 6nior b
l:.Lntll il ,.1'fi f.i,i:-\.
com*iyiirilil!,:['irl
i ! , ]. 4 ! r l : 1 , l i r "} l
rhsdodnara sdbyhccompanys!b!3db bcai*rcoddrdi3br se'epi.€doledstsvaiadeoncq
poisb '9 c b b cr ed andrbs doum
q dsnrze.exewDpeicq,rr-r/iL-,,-
r *:r
tiJr4.-i+3361orrr?e
sGs
lfi||| lurrrr
TestReport
No.I CE/201'1/84958
Page:2ol7
Dale:201111201
Il]lIltt]||tttt
POLYFILAG
2OA.CH€3OO
OBERALLMENDSTRASSE
ZUG/ SWITZERLAND
Test R6ult{s)
PARTNAMENo,,1
SILVERCOLOREDMETALWIRE
Tost ltem(8)
tlethod
Unit
(Cd)
Cadmium
mg/Kg With referenceto IEC62321:2008and
perfomedby ICP-AES.
mg/Kg A/ithreferenceto IEC62321: 2008and
cerfomedbv ICP-AESmS/kS Withreference
to IEC62321:2008and
pertormed
by ICP-AES.
and
Withreference
to IEC62321:2008
performedby Boilingwaterexkaction
Method.#
Lead (Pb)
Mercury(Hg)
Hexavalent
Chromium
Cr(Vl)
Sum of PBB6
Monobromobiphenyl
Dibromobiphenyl
Tribrcmobiphenyl
Tetrabromobiphenyl
Pentabromobiohenvl
Hexabromobiphenvl
Heptabromobiphenyl
Oclabromobiphenyl
Nonabromobiphenyl
D€cabromobiohenvl
Sum of PBDE8
Monobromodiohenvl
ether
Dibromodiphenyl
ether
Tribromodiphenyl
ether
MDL
Re8ult
No.1
2
n.d.
2
n.o,
2
n.d.
Negative
5
With referenceto IEC 62321: 2008 and
mg/Kg performed
by GC/MS.
5
5
5
5
5
5
5
n.d.
n.d.
n.d.
n.d.
n.o.
n.d.
n.d.
n.d.
n.d.
n.d.
n.o.
n.d.
5
5
5
n.d.
n.d.
n.d.
Tetrabromodiphenylether
5
5
5
Pentabrcmodiohenvl
ether
Hexabromodiphenyl
ether
HeotabromodiDhenvl
ether
n.d-
n.d.
n.d.
ethgr
Octabromodiphenvl
n.o.
ether
Nonabromodiohenvl
n.d.
5
ether
O€cabromodiphenyl
fililnil*
cmpsiy h,:fr 1 rlt lN'i,rl
rh";;*.,6
**d by,h"c".p,
b.gdrcftcromd dlmm6. iba
-]*d*b'h'inkdc.d"
*
il i
tft
it'rrll
.
n.d.
m.ra(s)radsdst b{ 6pod e^ioi b
iL, "",ar,r;ln'
e mid'onorrsbirv
lpoisb98b bcredsndrrsdoe
. : . l . : 1 1f l r : + i 4 . . , , 1 + e t o r t r e e t r e r r s 6 o a r e e tR
t was<oo
TestReport
No. CE/2011/84958
Page:3 of 7
Dale'.2011112101
:m ItNnt||||r
POLYFILAG
OBERALLIVENDSTMSSE
2OA,CH$3OOZUG / SWITZERLAND
Test ltem(s)
Halogen
(F)
Halogen-Fluorine
(CASNo.:14762-94-a)
Halogen-Chlorine
(Cl)
(CASNo.:22537-15-1)
(Br)
Halogen-Bromine
(CASNo.:10097-32-2)
Unit
mslkg
toL
Mothod
Withreference
to BS ENMSAZ2007.
Analysis
waspefoamed
by lC.
Halogenlodine(l)
(CAS No.: 14362-44-8)
Result
No.l
50
n.o.
50
n.d.
50
n.d.
50
n.d.
Note:
'1.mg/kg= ppm; 0.1wt%= 1000ppm
2. n.d.= NotDetecled
3. [rDL = l,ilethod
Detection
Limit
4."-"=NotRegulated
(NoUnit)
5. " = Qualitative
analysis
6. # = a. Positivemeansthepresence
of CrVlonthetestedareas
b. Negativemeansthe abs€nc€of CrVlon the testedareas
jn boiling-water-extraction
Thedetected
concentration
solutionis equalor greaterthan0.02mg/kgwith50cm'
testedareas.
l:i!z;li
i: i.tt'
r 1lr . "1 il i r.' -r:'1itli
nysled ro 6 &israrcod r oG or s
fors]sdrcnciom.1doem.itssub]
conpsii rir
1,.
1.!.ij'l'!4'
3@gbitr€lo&cl€d,ndh'3('ffi
'.1 , r.Li- ri:,
l
Fn?,,'tle6lor)ze
Test Report
No. : CE/2011/84958
Page:4 of 7
Da,e :2011112,01
POLYFILAG
OBERALLMENDSTMSSE2OA.CH.63OO
ZUG / SWITZERLAND
tt][]|l[[[]
]l
1) Thesesamples
weredissolved
totallyby pre-conditioning
methodaccording
to belowflowchart.
( Cf' test methodexcluded)
2) Nameof the personwhomademeasurement:
Climbgreat
Yang
3) Nameof the pe6on in cha.geof measurementr
TroyChang
Cutting
/ Preparation
Aciddigestion
by suitable
acid
depended
ondifierent
sample
material
las belowtable)
Add appropriateamountof
digestion
reagent
Heatto appropriate
tgnpe€tu€ to ex€ct
'1) AlkaliFusion
2) HClto dissolve
ICP.AES
DigestionAcid
S1eel,
copper,aluminum,
solder
Aquaregia,HNOs,HCl,HF,H,O,
Gla6s
HNO3/HF
p€lladium,
Gold,platinum,
ceramic Aquaregia
Silver
HNO.I
Plastic
HCI
HrSOr,Hroa HNOg,
Others
Anyacidlo tobldige6tion
1.:.ati
i;llri
abjed ro.ems 3id cofdtoG rof E
throughfilter
Add diphenyl-carbazide
for
SampleMaterial
c o m o , i rt t - , i . r i r l L l { i I r . , r l , J i : n i i !
Cool,filterdigestate
colordevelopment
measurethe absobance
at 540 nm by UV-VIS
1r.rrlri}ll.
Atenoi sdrawiroh.rn'bloior
'ab't
TestReport
No.:CEl20'11184958
Dale:201111i,01
POLYFILAG
OBERALLMENDSTRASSE
2OA,CH€3OO
ZUG/ SWITZERLAND
Page: 5 of 7
lU[uIl||t
[t|]l
PBB/PBDEanalyticalFLOWCHART
'1) l{anEofthepersonwholrEderEaru.enEnt:RofiEnWong
2) lhmeoftheperson
incharge
of nEasurerEnt
TroyChang
Firsttestingprocess----+
process-- Optionalscreen
process - .>
Confinmtion
Screen
analysis
Safipleei€ction/
So* et rnethod
concenkate/Dilute
Extractedsolution
Filter
Analysisby GC/IMS
c o m o a nl ivi i l r / t r i , r L r i ' r , - r l , 1 i , ! n i l i ) : i r r ' l j d i
l?q{!.\.
.,
r'.rll'trl'
mdbaGpJdu€dexeplnig].wbou
!hdsrdzoie N.!r:iFcryttrw:orrr:
:r,'
t::Ii+fi,'
's6i0r)2etDr+336(orrstt
ffis'g'.om
TestReport
No.: CE/2011/84958
Dale:2011h2/01
Page:6 of 7
l]m||ufi]ltl|l]
POLYFILAG
OBEMLLMENDSTRASSE2OA,CH-6300
ZUG/ SWITZERLAND
AnaMical flow chart of halogen content
'1) Nafi€ of the oerson who arEderEasurernenl Rita Chen
2) Narneofthe person in charg€ of rEasurerEnt: Troy Chang
Sanplepretreatrnent
/ Separatbn
Weighting
andputting
samplein cell
OrygenBombCombustion
/ Ab€orption
Dilution
lo fixedvolunE
AnalysiswasperfonrEdby lC
c o m p . n yn ; , i r r , l r l , ; ! i ' i l r r j J l l ; ' h
rh s @msnr s 'sred by 6e compa
l,.ljf
,ltirllt
psls)6sbd hb red rcPodanioi bs
i 1 ! . . 1 . " .i , r i ' i j ! .
'ndom^ioroiaidluisdclon $uord
iidbe6pd!€dai6plniu]qho'
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Test Report
Applicant:
Number : TWNC00189732
Littelfuse, Philippines Inc.
LIMA Technology Center, Lipa City,
Malvar, Batangas
Date
: Jan 26, 2011
Sample Description:
One (1) group of submitted samples said to be :
Part Description
: Element (Cu CDA 102 Sn Plated)
Part Number
: 082418-001
Date Sample Received
: Jan 21, 2011
Date Test Started
: Jan 21, 2011
Test Conducted :
As requested by the applicant, for details please refer to attached pages.
Authorized By:
On Behalf Of Intertek Testing Services
Taiwan Limited
K. Y. Liang
Director
This report shall not be reproduced
except in full, without the written
approval of the laboratory.
Page 1 Of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00189732
Test Conducted
(Ⅰ) Test Result Summary :
Testing Item
Heavy Metal
Cadmium (Cd) content
Lead (Pb) content
Mercury (Hg) content
Chromium VI (Cr6+) content (mg/kg with 50cm2)
Result (ppm)
Silvery Metal
Thread
ND
ND
ND
Negative (< 0.02)
Remarks: ppm = Parts per million based on weight of tested sample = mg/kg
ND = Not detected
<
= Less than
mg/kg with 50cm2 = milligram per kilogram with 50 square centimetre
Negative = A negative test result indicated positive observation
was not found at the time of testing.
Responsibility Of Chemist : Irene Chiou / Kevin Liu / Cathy Chen
Date Sample Received
Testing Period
: Jan 21, 2011
: Jan 21, 2011 To Jan 21, 2011
(Ⅱ) RoHS Requirement:
Restricted Substances
Cadmium (Cd) Content
Lead (Pb) Content
Mercury (Hg) Content
Chromium VI (Cr6+) Content
Limits
0.01% (100ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for
homogeneous material.
Page 2 Of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00189732
Test Conducted
(Ⅲ) Test Method:
Testing Item
Cadmium (Cd)
content
Lead (Pb) content
Mercury (Hg)
content
Chromium VI (Cr6+)
content
Testing Method
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 7, by microwave
digestion until the tested samples are
totally dissolved and determined by
ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in annex B, by boiling water
extraction and determined by UV-Vis
spectrophotometer.
Reporting Limit
2 ppm
2 ppm
2 ppm
0.02
mg/kg with 50cm2
Remark: Reporting limit = Quantitation limit of analyte in sample
Page 3 Of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00189732
Test Conducted
(Ⅳ) Measurement Flowchart:
Test For Cd/Pb/Hg/Chromium (VI)
Reference Standard：IEC 62321 edition 1.0:2008
Sampling/grinding or cutting
Cd/Pb/Hg
Cr
Polymers /
Electronics
Metal
For different
material, digest
the sample with
*1
appropriate acid
By spot test
Negative
Confirm the tested
samples are
totally dissolved
Make up with
deionized water
6+
*2
Weigh sample
and add
alkaline
solution
Get 50cm2 sample
Definite temp.
extraction
Boiling water
extraction
Cool and filter
the extract
Analyzed by ICP-OES
Make up with deionized
water and add diphenylcarbazide solution
Analyzed by UV-VIS
Remarks:
*1: List Of Appropriate Acid：
Material
Polymers
Metals
Electronics
Acid Added For Digestion
HNO3,HCl,HF,H2O2,H3BO3
HNO3,HCl,HF
HNO3,HCl,H2O2,HBF4
*2: If the result of spot test is positive, Chromium VI would be determined as detected.
End Of Report
Page 4 Of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00189732
Test Conducted
Photo
Page 5 Of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Test Report
Applicant:
Number : TWNC00233557
Littelfuse Philippines Inc.
LIMA Technology Center, Lipa City,
Malvar, Batangas
Date
: Nov 28, 2011
Sample Description:
One (1) group of submitted samples said to be :
Part Description
: BiSb Solder
Part Number
: 927-304
Date Sample Received
: Nov 21, 2011
Date Test Started
: Nov 22, 2011
Test Conducted :
As requested by the applicant, for details please refer to attached pages.
Authorized By:
On Behalf Of Intertek Testing Services
Taiwan Limited
K. Y. Liang
Director
This report shall not be reproduced
except in full, without the written
approval of the laboratory.
Page 1 of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00233557
Test Conducted
(Ⅰ) Test Result Summary :
Test Item
Heavy Metal
Cadmium (Cd) content
Lead (Pb) content
Mercury (Hg) content
Chromium VI (Cr6+) content (mg/kg with 50cm2)
Result (ppm)
Silvery Metal
ND
99
ND
Negative (< 0.02)
Remarks: ppm = Parts per million based on weight of tested sample = mg/kg
ND = Not detected
<
= Less than
mg/kg with 50cm2 = milligram per kilogram with 50 square centimetre
Negative = A negative test result indicated positive observation
was not found at the time of Test.
Responsibility of Chemist : Irene Chiou / Kevin Liu
Date Sample Received
Test Period
: Nov 21, 2011
: Nov 22, 2011 To Nov 25, 2011
(Ⅱ) RoHS Requirement:
Restricted Substances
Cadmium (Cd) Content
Lead (Pb) Content
Mercury (Hg) Content
Chromium VI (Cr6+) Content
Limits
0.01% (100ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for
homogeneous material.
Page 2 of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00233557
Test Conducted
(Ⅲ) Test Method:
Test Item
Cadmium (Cd)
content
Lead (Pb) content
Mercury (Hg)
content
Chromium VI (Cr6+)
content
Test Method
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 7, by microwave
digestion until the tested samples are
totally dissolved and determined by
ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in annex B, by boiling water
extraction and determined by UV-Vis
spectrophotometer.
Reporting Limit
2 ppm
2 ppm
2 ppm
0.02
mg/kg with 50cm2
Remark: Reporting limit = Quantitation limit of analyte in sample
Page 3 of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00233557
Test Conducted
(Ⅳ) Measurement Flowchart:
Test for Cd/Pb/Hg/Chromium (VI)
Reference Standard：IEC 62321 edition 1.0:2008
Sample preparation
Take sample and immerse into Aqua Regia, start to strip plating layer
Stop the stripping procedure upon color change completely
Take the Aqua solution as plating component and stripped body as substrate component
Cd/Pb/Hg
Cr
Polymers /
electronics
Metal
For different
material, digest
the sample with
*1
appropriate acid
By spot test
Negative
Confirm the tested
samples are
totally dissolved
Make up with
deionized water
6+
*2
Weigh sample
and add
alkaline
solution
Get 50cm2 sample
Definite temp.
extraction
By boiling water
extraction
Cool and filter
the extract
Analyzed by ICP-OES
Make up with deionized water and add
diphenyl-carbazide solution
Remarks:
*1: List of Appropriate Acid：
Material
Polymers
Metals
Electronics
Analyzed by UV-VIS
Acid Added for Digestion
HNO3,HCl,HF,H2O2,H3BO3
HNO3,HCl,HF
HNO3,HCl,H2O2,HBF4
*2: If the result of spot test is positive, Chromium VI would be determined as detected.
End of Report
Page 4 of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00233557
Test Conducted
Photo
Page 5 of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00233544
Test Report
Applicant:
Littelfuse Philippines Inc.
LIMA Technology Center, Lipa City,
Malvar, Batangas
Date
: Nov 25, 2011
Sample Description:
One (1) group of submitted samples said to be :
Part Description
: Ink
Part Number
: 425809
Date Sample Received
: Nov 21, 2011
Date Test Started
: Nov 22, 2011
Test Conducted :
As requested by the applicant, for details please refer to attached pages.
Authorized By:
On Behalf Of Intertek Testing Services
Taiwan Limited
K. Y. Liang
Director
This report shall not be reproduced
except in full, without the written
approval of the laboratory.
Page 1 of 6
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00233544
Test Conducted
(Ⅰ) Test Result Summary :
Test Item
Result (ppm)
Black Paste
Heavy Metal
Cadmium (Cd) content
Lead (Pb) content
Mercury (Hg) content
Chromium VI (Cr6+) content
Polybrominated Biphenyls (PBBs)
Monobrominated Biphenyls (MonoBB)
Dibrominated Biphenyls (DiBB)
Tribrominated Biphenyls (TriBB)
Tetrabrominated Biphenyls (TetraBB)
Pentabrominated Biphenyls (PentaBB)
Hexabrominated Biphenyls (HexaBB)
Heptabrominated Biphenyls (HeptaBB)
Octabrominated Biphenyls (OctaBB)
Nonabrominated Biphenyls (NonaBB)
Decabrominated Biphenyl (DecaBB)
Polybrominated Diphenyl Ethers (PBDEs)
Monobrominated Diphenyl Ethers (MonoBDE)
Dibrominated Diphenyl Ethers (DiBDE)
Tribrominated Diphenyl Ethers (TriBDE)
Tetrabrominated Diphenyl Ethers (TetraBDE)
Pentabrominated Diphenyl Ethers (PentaBDE)
Hexabrominated Diphenyl Ethers (HexaBDE)
Heptabrominated Diphenyl Ethers (HeptaBDE)
Octabrominated Diphenyl Ethers (OctaBDE)
Nonabrominated Diphenyl Ethers (NonaBDE)
Decabrominated Diphenyl Ether (DecaBDE)
Halogen Content
Fluorine (F)
Chlorine (Cl)
Bromine (Br)
Iodine (I)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Remarks: ppm = Parts per million based on wet weight of tested sample =
mg/kg
ND = Not detected
Responsibility of Chemist : Irene Chiou / Kevin Liu / Cathy Chen
Date Sample Received
Test Period
: Nov 21, 2011
: Nov 22, 2011 To Nov 25, 2011
Page 2 of 6
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Test Conducted
(Ⅱ) RoHS Requirement:
Restricted Substances
Cadmium (Cd) Content
Lead (Pb) Content
Mercury (Hg) Content
Chromium VI (Cr6+) Content
Polybrominated Biphenyls (PBBs)
Polybrominated Diphenyl Ehters (PBDEs)
Number : TWNC00233544
Limits
0.01% (100ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for
homogeneous material.
(Ⅲ) Test Method:
Test Item
Cadmium (Cd)
content
Lead (Pb) content
Mercury (Hg)
content
Chromium VI (Cr6+)
content
Polybrominated
Biphenyls (PBBs)
Polybrominated
Diphenyl Ethers
(PBDEs)
Halogen Content
Test Method
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 7, by microwave
digestion until the tested samples are
totally dissolved and determined by
ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in annex C, by alkaline
digestion and determined by UV-Vis
spectrophotometer.
With reference to IEC 62321 edition
1.0:2008 in annex A, by solvent
extraction and determined by GC-MSD
and further HPLC confirmation when
necessary.
With reference to IEC 62321 edition
1.0:2008 in annex A, by solvent
extraction and determined by GC-MSD
and further HPLC confirmation when
necessary.
With reference to EN 14582:2007 by
calorimetric bomb with oxygen and
determined by ion chromatography
Reporting Limit
2 ppm
2 ppm
2 ppm
1 ppm
5 ppm
5 ppm
50 ppm
Remark: Reporting limit = Quantitation limit of analyte in sample
Page 3 of 6
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00233544
Test Conducted
(Ⅳ) Measurement Flowchart:
Test for Cd/Pb/Hg/Chromium (VI)/PBBS/PBDES Contents
Reference Standard: IEC 62321 edition 1.0:2008
Sample preparation
For non-metal part
For metal part
Take sample and immerse into Aqua Regia, start to strip plating layer
Stop the stripping procedure upon color change completely
Take the Aqua solution as plating component and stripped body as substrate component
Cd/Pb/Hg
Cr
Confirm the tested
samples are
totally dissolved
Make up with
deionized water
PBBs/PBDEs
Polymers /
electronics
Metal
For different
material, digest
the sample with
*1
appropriate acid
6+
Weigh sample and
add organic solvent
By spot test
Negative
Get 50cm2 sample
By boiling water
extraction
*2
Weigh sample
and add
alkaline
solution
By Soxhlet
extraction or
Solvent extraction
Definite temp.
extraction
Cool and filter
the extract
Analyzed by ICP-OES
Concentrate the
extract and make up
with organic
solvent
Analyzed by GC-MSD
Make up with deionized
water and add diphenylcarbazide solution
Analyzed by UV-VIS
Remarks:
*1: List of Appropriate Acid：
Material
Polymers
Metals
Electronics
Acid Added for Digestion
HNO3,HCl,HF,H2O2,H3BO3
HNO3,HCl,HF
HNO3,HCl,H2O2,HBF4
*2: If the result of spot test is positive, Chromium VI would be determined as detected.
Page 4 of 6
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00233544
Test Conducted
(Ⅳ) Measurement Flowchart:
Test for Halogen Content
Reference Standard：EN 14582
Sampling/grinding or
cutting
Add absorbent in a
combustion flask &
place weighed sample in
equipment
Fill oxygen into
calorimetric bomb
Ignite then leave the
flask at room
temperature
Transfer the absorbent
into a volumetric flask
Make up with deionized
water
Analyzed by ion
chromatography
End of Report
Page 5 of 6
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00233544
Test Conducted
Photo
Page 6 of 6
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Test Report
Applicant:
Number : TWNC00198289
Littelfuse, Philippines Inc.
LIMA Technology Center, Lipa City,
Malvar, Batangas
Date
: Apr 15, 2011
Sample Description:
One (1) group of submitted samples said to be :
Sample Description
: Black Ink
Style / Item No.
: 425809
Date Sample Received
: Apr 13, 2011
Date Test Started
: Apr 13, 2011
Test Conducted:
As requested by the applicant, for details please refer to attached pages.
Authorized By:
On Behalf Of Intertek Testing Services
Taiwan Limited
K. Y. Liang
Director
This report shall not be reproduced
except in full, without the written
approval of the laboratory.
Page 1 Of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00198289
Test Conducted
(Ⅰ) Test Result Summary:
Test Item
Result (ppm)
Black Paste
Phthalates
Di(2-ethylhexyl) Phthalate (DEHP)
Dibutyl Phthalate (DBP)
Benzyl Butyl Phthalate (BBP)
Others
Hexabromocyclododecane (HBCDD)
Remarks :
ppm
ND
ND
= Parts per million based on wet weight of tested sample
= Not detected
Responsibility Of Chemist:
Date Sample Received
Test Period
Irene Chiou / Kevin Liu / Cathy Chen
: Apr 13, 2011
: Apr 13, 2011 To Apr 15, 2011
(Ⅱ) Test Method:
Test Item
Phthalates
Hexabromocyclododecane
(HBCDD)
Remark :
ND
ND
ND
Test method
With reference to ASTM D3421-75,
by solvent extraction and
determined by GC-MSD or GC-FID
With reference to USEPA 3540C, by
solvent extraction and determined
by GC-MSD
Reporting Limit
10 ppm
10 ppm
Reporting Limit = Quantitation limit of analyte in sample
Page 2 Of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00198289
Test Conducted
(Ⅲ) Measurement Flowchart:
Test For Phthalates Contents
Reference Method: ASTM D3421-75
Sampling/grinding or
cutting
Weigh sample and add
organic solvent
By solvent extraction
Concentrate the extract
and make up with
organic solvent
Analyzed by GC-MSD or
GC-FID
Page 3 Of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00198289
Test Conducted
(Ⅲ) Measurement Flowchart:
Test For Hexabromocyclododecane (HBCDD)
Reference Standard：USEPA 3540C
Sampling/grinding or cutting
Weigh sample and add organic
solvent
By soxhlet extraction
Concentrate the extract and
make up with organic solvent
Analyzed by GC-MSD
End Of Report
Page 4 Of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00198289
Test Conducted
Photo
Page 5 Of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401