ICPTest_259 pdf

ICP Test Report Certification Packet
Company name :
Littelfuse, Inc.
Product Series:
Sate T-Plus Fuse
Product #:
259xxx Series
Issue Date:
September 5, 2011
It is hereby certified by Littelfuse, Inc. that there is neither RoHS (EU Directive
2002/95/EC)-restricted substance nor such use, for materials to be used for unit parts, for
packing/packaging materials, and for additives and the like in the manufacturing processes.
In addition, it is hereby reported to you that the parts and sub-materials, the materials to be used
for unit parts, the packing/packaging materials, and the additives and the like in the manufacturing
processes, are all composed of the following components.
Issued by:
<Global EHS Engineer>
(1) Parts, sub-materials and unit parts
This document covers the Sate T-Plus Fuse RoHS-Compliant series products
manufactured by Littelfuse, Inc.
< Raw Materials Used
Please see Table 1
(2) The ICP data on all measurable substances
Please see appropriate pages as identifed in Table 1
Remarks:
Pb (lead) contained in the high temperature melting solder > 85% and is categorized as
exempt under section 7a of the RoHS Annex.
Form 585-047 Rev. A
1
2/21/06
Table 1: List of Raw Materials covered by this report
Total Parts
1
2
3
4
5
6
7
Raw Material Part Number
910-263
909-144
497xxx (497238)
057895
275001-1
692320
425826
Raw Material Description
Cap
Body
Filament
Moulding Compound
Sleeve
Solder
Ink-Black
2
Page(s)
3-7
8-13
14-20
21-27
28-34
35-39
40-45
Test Report
Applicant:
Number : TWNC00191797
Littelfuse, Philippines Inc.
LIMA Technology Center, Lipa City,
Malvar, Batangas
Date
: Feb 22, 2011
Sample Description:
One (1) group of submitted samples said to be :
Part Description
: Cap and Lead Assay
Part Number
: 910-023/910-263(910XXX)
Date Sample Received
: Feb 16, 2011
Date Test Started
: Feb 17, 2011
Test Conducted :
As requested by the applicant, for details please refer to attached pages.
Authorized By:
On Behalf Of Intertek Testing Services
Taiwan Limited
K. Y. Liang
Director
This report shall not be reproduced
except in full, without the written
approval of the laboratory.
Page 1 Of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Number : TWNC00191797
Test Conducted
(Ⅰ) Test Result Summary :
Testing Item
(1)
Result (ppm)
(2)
(3)
(4)
Heavy Metal
Cadmium (Cd) content
Lead (Pb) content
Mercury (Hg) content
ND
ND
ND
ND
ND
85
ND
89
ND
ND
ND
ND
Negative
Negative
Negative
Negative
Chromium VI (Cr6+) content (mg/kg with 50cm2)
(< 0.02) (< 0.02) (< 0.02) (< 0.02)
Remarks: ppm = Parts per million based on weight of tested sample = mg/kg
ND = Not detected
<
= Less than
mg/kg with 50cm2 = milligram per kilogram with 50 square centimetre
Negative = A negative test result indicated positive observation
was not found at the time of testing.
Tested Components
(1) Beige Substrate (Body)
(2) Silvery Plating (Body)
(3) Coppery Substrate (Pin)
(4) Silvery Plating (Pin)
Responsibility Of Chemist : Irene Chiou / Kevin Liu / Cathy Chen
Date Sample Received
Testing Period
: Feb 16, 2011
: Feb 17, 2011 To Feb 22, 2011
(Ⅱ) RoHS Requirement:
Restricted Substances
Cadmium (Cd) Content
Lead (Pb) Content
Mercury (Hg) Content
Chromium VI (Cr6+) Content
Limits
0.01% (100ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for
homogeneous material.
Page 2 Of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Number : TWNC00191797
Test Conducted
(Ⅲ) Test Method:
Testing Item
Cadmium (Cd)
content
Lead (Pb) content
Mercury (Hg)
content
Chromium VI (Cr6+)
content
Testing Method
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 7, by microwave
digestion until the tested samples are
totally dissolved and determined by
ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in annex B, by boiling water
extraction and determined by UV-Vis
spectrophotometer.
Reporting Limit
2 ppm
2 ppm
2 ppm
0.02
mg/kg with 50cm2
Remark: Reporting limit = Quantitation limit of analyte in sample
Page 3 Of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Number : TWNC00191797
Test Conducted
(Ⅳ) Measurement Flowchart:
Test For Cd/Pb/Hg/Chromium (VI)
Reference Standard:IEC 62321 edition 1.0:2008
Sample preparation
Take sample and immerse into Aqua Regia, start to strip plating layer
Stop the stripping procedure upon color change completely
Take the Aqua solution as plating component and stripped body as substrate component
Cd/Pb/Hg
Cr
Polymers /
electronics
Metal
For different
material, digest
the sample with
*1
appropriate acid
By spot test
Negative
Confirm the tested
samples are
totally dissolved
Make up with
deionized water
6+
*2
Weigh sample
and add
alkaline
solution
Get 50cm2 sample
Definite temp.
extraction
By boiling water
extraction
Cool and filter
the extract
Analyzed by ICP-OES
Make up with deionized water and add
diphenyl-carbazide solution
Remarks:
*1: List Of Appropriate Acid:
Material
Polymers
Metals
Electronics
Analyzed by UV-VIS
Acid Added For Digestion
HNO3,HCl,HF,H2O2,H3BO3
HNO3,HCl,HF
HNO3,HCl,H2O2,HBF4
*2: If the result of spot test is positive, Chromium VI would be determined as detected.
End Of Report
Page 4 Of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Number : TWNC00191797
Test Conducted
Photo
Page 5 Of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Test Report
Applicant:
Number : TWNC00182413
Littelfuse, Philippines Inc.
LIMA Technology Center, Lipa City,
Malvar, Batangas
Date
: Nov 24, 2010
Sample Description:
One (1) group of submitted samples said to be :
Part Description
: Ceramic Body
Part Number
: 909-144
Date Sample Received
: Nov 16, 2010
Date Test Started
: Nov 17, 2010
Test Conducted :
As requested by the applicant, for details please refer to attached pages.
Authorized By:
On Behalf Of Intertek Testing Services
Taiwan Limited
K. Y. Liang
Director
This report shall not be reproduced
except in full, without the written
approval of the laboratory.
Page 1 Of 6
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Number : TWNC00182413
Test Conducted
(Ⅰ) Test Result Summary :
Testing Item
Result (ppm)
Cream Plastic
Heavy Metal
Cadmium (Cd) content
Lead (Pb) content
Mercury (Hg) content
Chromium VI (Cr6+) content
Polybrominated Biphenyls (PBBs)
Monobrominated Biphenyls (MonoBB)
Dibrominated Biphenyls (DiBB)
Tribrominated Biphenyls (TriBB)
Tetrabrominated Biphenyls (TetraBB)
Pentabrominated Biphenyls (PentaBB)
Hexabrominated Biphenyls (HexaBB)
Heptabrominated Biphenyls (HeptaBB)
Octabrominated Biphenyls (OctaBB)
Nonabrominated Biphenyls (NonaBB)
Decabrominated Biphenyl (DecaBB)
Polybrominated Diphenyl Ethers (PBDEs)
Monobrominated Diphenyl Ethers (MonoBDE)
Dibrominated Diphenyl Ethers (DiBDE)
Tribrominated Diphenyl Ethers (TriBDE)
Tetrabrominated Diphenyl Ethers (TetraBDE)
Pentabrominated Diphenyl Ethers (PentaBDE)
Hexabrominated Diphenyl Ethers (HexaBDE)
Heptabrominated Diphenyl Ethers (HeptaBDE)
Octabrominated Diphenyl Ethers (OctaBDE)
Nonabrominated Diphenyl Ethers (NonaBDE)
Decabrominated Diphenyl Ether (DecaBDE)
Halogen Content
Fluorine (F)
Chlorine (Cl)
Bromine (Br)
Iodine (I)
ND
98
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Remarks: ppm = Parts per million based on weight of tested sample = mg/kg
ND = Not detected
Responsibility Of Chemist : Irene Chiou / Kevin Liu / Cathy Chen
Date Sample Received
Testing Period
: Nov 16, 2010
: Nov 17, 2010 To Nov 24, 2010
Page 2 Of 6
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Number : TWNC00182413
Test Conducted
(Ⅱ) RoHS Requirement:
Restricted Substances
Cadmium (Cd) Content
Lead (Pb) Content
Mercury (Hg) Content
Chromium VI (Cr6+) Content
Polybrominated Biphenyls (PBBs)
Polybrominated Diphenyl Ehters (PBDEs)
Limits
0.01% (100ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for
homogeneous material.
(Ⅲ) Test Method:
Testing Item
Cadmium (Cd)
content
Lead (Pb) content
Mercury (Hg)
content
Chromium VI (Cr6+)
content
Polybrominated
Biphenyls (PBBs)
Polybrominated
Diphenyl Ethers
(PBDEs)
Halogen Content
Testing Method
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 7, by microwave
digestion until the tested samples are
totally dissolved and determined by
ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in annex C, by alkaline
digestion and determined by UV-Vis
spectrophotometer.
With reference to IEC 62321 edition
1.0:2008 in annex A, by solvent
extraction and determined by GC-MSD
and further HPLC confirmation when
necessary.
With reference to IEC 62321 edition
1.0:2008 in annex A, by solvent
extraction and determined by GC-MSD
and further HPLC confirmation when
necessary.
With reference to EN 14582:2007 by
calorimetric bomb with oxygen and
determined by ion chromatography
Reporting Limit
2 ppm
2 ppm
2 ppm
1 ppm
5 ppm
5 ppm
50 ppm
Remark: Reporting limit = Quantitation limit of analyte in sample
Page 3 Of 6
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Number : TWNC00182413
Test Conducted
(Ⅳ) Measurement Flowchart:
Test For Cd/Pb/Hg/Chromium (VI)/PBBS/PBDES Contents
Reference Standard: IEC 62321 edition 1.0:2008
Sampling/grinding or cutting
Cd/Pb/Hg
Cr
Weigh sample and
add organic solvent
By spot test
Negative
Confirm the tested
samples are
totally dissolved
Make up with
deionized water
PBBs/PBDEs
Polymers /
electronics
Metal
For different
material, digest
the sample with
*1
appropriate acid
6+
Get 50cm2 sample
By boiling water
extraction
*2
Weigh sample
and add
alkaline
solution
By Soxhlet
extraction or
Solvent extraction
Definite temp.
extraction
Cool and filter
the extract
Concentrate the
extract and make up
with organic
solvent
Analyzed by ICP-OES
Analyzed by GC-MSD
Make up with deionized
water and add diphenylcarbazide solution
Remarks:
*1: List Of Appropriate Acid:
Material
Polymers
Metals
Electronics
Analyzed by UV-VIS
Acid Added For Digestion
HNO3,HCl,HF,H2O2,H3BO3
HNO3,HCl,HF
HNO3,HCl,H2O2,HBF4
*2: If the result of spot test is positive, Chromium VI would be determined as detected.
Page 4 Of 6
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Number : TWNC00182413
Test Conducted
(Ⅳ) Measurement Flowchart:
Test For Halogen Content
Reference Standard: EN 14582
Sampling/grinding or
cutting
Add absorbent in a
calorimetric bomb &
place weighed sample in
equipment
Fill the calorimetric
bomb with oxygen
Ignite then leave the
flask at room
temperature
Transfer the absorbent
into a volumetric flask
Make up with deionized
water
Analyzed by ion
chromatography
End Of Report
Page 5 Of 6
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Number : TWNC00182413
Test Conducted
Photo
Page 6 Of 6
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Validi
For Q
Please
Test Report
sGs
No. : CE2010/C0094 Dale | 2O1Oh2tO8 page : 1of 7
POLYFIL
AG
OBERALLMENDSTRASSE
2OA,CH€3OO
ZUG/ SWITZERLAND
Th6followingsample(s)wa3/weresubmitted and identified by/on behalfoftha client as:
SampleDescription
Buyer/Order
No.
SampleReceiving
Date
TeslingPeriod
Ni42Fe58MCuirAg5%
94462
2010t1?,01
20t0t1zo110 2010t1208
Te6t Rosult(s)
Pleasereferto nextpage(s).
(NWO
ilha1d6Ftde.onyblbgnplels)l6sdThs|69@d€ndb€
c d € r y r r r , l l , l r J l .r r . l l t + i 4 r r r l i l *
ft8 d@nd
for.sdmr
own
6 gEd hy b6 c.mp.
fomar donds
slq
rk'ons
i i. t]li, l&rl\
.:' -' l'
1.1rJts!!.
i any ft6cmP4tsso6r.
fttrngB.ind[946!un&rlh16
1 r .+ r { r r { i * : r t r r s { o z r r r e e
|llt [lrr]||rltttt
TestReport
No. CE2010/C0094 Date| 2010/'12y08Page: 2 ot 7
POLYFIL
AG
OBERALLMENDSTRASSE
2OA,CH€3OO
ZUG/ SWITZERLAND
|r [tll||lI|tl|t
Test Resultlsl
PARTNAIVENo,1
SILVERCOLORED
i'ETALWIRE
Test ltem (8):
Unit
Cadmium(Cd)
Method
Result
MDL
mg/Kg Withreference
to IEC62321:2008and
2
No.1
n.d.
5o
n.d.
50
n.d.
50
n.d.
50
n.d.
pedormedby ICP-AES.
mgls Withreferenc€
to IEC62321:2008€nd
2
n.d.
pertomedby lCPdES.
Mercury(Hg)
mdkg With referencelo IEC62321:2008and
2
n,d,
perfomedby ICP-AES.
Hexavalent
ChrcmiumCr(Vl)by
Withreference
to IEC62321:2008and 0.02m9/kg Negative
Spottest / boiling\,r€terextraction
perfomedby Spottest/ boilingwEter with50cm,
extradtionlrethod.(SeeNote6)
sudace
Lead (Pb)
Halogen
Halogen-Fluorine
(F)
(CASNo.:014762-94-8)
Halogen-Chlorine
(Cl)
(CASNo.:022537-15-1)
Halogen-Bromine
(Br)
(CASNo.:010097-32-2)
(l)
Halogen-lodine
(CASNo.:01436244-8)
With referenceto BS EN 14582t2007
.
mg/Kg
Analysiswasperformedby lC-
Sum of PBB6
n.d-
Monobromobiphenyl
Dibromobiphenyl
Tribromobiphenyl
Tetrabromobipheny
Pentabromobiphenyl
mgikg
Hexabromobiph€nyl
Heptabromobiphenyl
Ociabromobiphenyl
Nonabromobiphenyl
Decabromobiphenyl
cm€ry r.r r|,;i:r} , ..rti'Ji: + i4!rj.,ijlt " ei.
n6tud
l d 6
Wth reference
to IEC62321t2008and
perfomedby GC/MS.
5
5
5
5
n.dn.d.
n.d.
n.d.
5
5
n.d,
5
5
5
5
n.o.
n.o.
n.d.
n.d.
n.d.
p3G)rssdrh3rd.@n€ndb
i:+::r 'J. i r'r"llt}rl.
rn'1,1.J{7:1l
3 sdbyh6m@nyshdroisc*'dcmdibBd
6 d M E l o m a l d .
@
n
h
.
d
ontandwrhrh€rmborcrds,.ddons'lary.ft8csrt3sobEspBbrt
3
o
l
b
h
e
]
i
m
i
b
l
d
d
'
a
b
L
t
y
srobcltrrandrhsdEs
u hdsrkr 2orcrapo cooirrriiwio/f ttti f lr: :r,rrit:il
lt r is6orpDerD,re0rr2arrT
ww+.on
TestReport
paqe:3of7
No.: CE/2010/C0094Date:2O1O/12!OB
POLYFILAG
OBERALLMENDSTMSSE2OA,CHS3OOZUG / SWITZERLAND
Te3t ltem (s):
unit
Method
rr] ttrr[it|lt
MDL
Sumof PBDES
Monobromodiphenyl
eth€r
Oibromodiphenyl
ether
No.1
n.d.
n.d.
n.d.
fnbomodiphenyl
eth€r
Tetrabromodiphenyl
ether
Pentabromodiphenyl
ether
Hexabromodiphenyl
ether
Heptabrornodiphenyl
ethe.
Oclabromodiphenyl
ether
Nonabromodiphenyl
ether
Decabomodiphenyl
ether
Result
n.o,
mgxg
Withreference
to IEC62321:2008and
perfomedby GC/MS.
5
5
5
5
n.ct.
n.d.
n.d.
n.d.
n.d.
5
n.o,
n.o.
Note:
1. mg/kg= ppm; 0.1M%= 100oppm
2- n.d. = Not Detected
3. MDL= MethodDeteclionLimit
4."-"=NotRegulated
5. " = Qualitative
(NoUnit)
analysis
6. SDot-te.st:
N€gative= Absenceof Cr(Vl)coating/ surfacelayer;positive= presencoof Cr(Vt)coating/ surtacetayer;
(Thetestedsampleshouldbe furthervedfiedby boiling-water-extraction
methodif the spottest resuttcannot
beconfimed.)
Boiling-wEter-exlraclion:
Negative= Absenc€of Cr(Vl)coating/ surtacelayer; Positive= Pres€nceof Cr(Vl)coating/ surtacelayer;
Th6 detec{edconcentrationin boiling-water-ext.action
solutionis equalor greaterthan0.02mg/kgwith SOcm.
samDlesurfacearea.
npsGlrsdd th316r@nendb
cmponyrill4l.;i.!.illi'r.lrF,fl::tr)li"ei.nU'i.1:]S:11;:=:i:.J.1.11JF1".
th6ddh€fr
3 sd by tu c.mp3iy srqd b tu GmmrcmdtuB d ss
r@€.d6rc romar [email protected] 3!q
sFBb|ly9locc'.d.ndlh!d6u
h r n ' h s a d d ! € d b s u e h c n n d b a 4 d f d € ! € , l i f u l w i d
h. imeloi
or €b ry
Test Report
No-: CE/201UC0094Date:2OiOt12tOepaoe,4of7
POLYFILAG
OBEMLLMENDSTMSSE 2OA,CH€3OOZUG / SWITZERLAND
rtlt tIll|||||lllttt
'1) Thesesarples w€Ie
dissotr€dtoblfy by pre-conditioning
rEthod accordingto belowflow chart
( Cf' test nethod e)cluded)
2) flanE of the personwho mademeasurefiEnl:Climbgreatyang
3) tlarE ofthe pe6on in charg€of r€asurenEnt TroyChang
Cutting
/ Preparation
Aciddigestion
by suitable
6cid
dependedon difierentsarble
nEterial(asbelowtable)
Microwavedigestionwith
Addappropdate
anbuntof
digeslion
reagent
HNo3/rcUHF
Healto appropdate
tefiperatureto extEct
Cool.filterdigeotae
through
fiher
AlkaliFusion
F|cIto dissolve
Add diphedyl-carb€zidefor
colordeveloprnent
Safiple Material
cNFry
DigestbnAcid
S'teel,
copper,aluninun\solder
Aqua regia,HNO3,HCl,HF,HrO,
Gl€ss
palladium,
Gold,platinum,
ceraric
HNO3/HF
Aquaregia
Sitver
HNO3
Plastic
l-lrsOi, HrOr,HNO3,HCI
Oh€rs
Anyacidto trctaldigestion
lilltt;!r;
id adM'cromd
nrturerGe.drorso^ryb6.smpo13)@rod Ihs'61,6p.nenddb'
,lr'!lt !;.::l!ll.l!!L.\;:+tr]
.Lili:!'Ii!lJi
J rrl rttrrll.
^y elttod b iE ce66rcond r onsot s
@n*
3uq
me€suaethe ab6orbance
at 540 nmby UV-VIS
he 'n,@id d iab t
onryaidwih'nkhisdCr€db
ndtudds iany tuCmparyss&6Fnsbriy
srohC,6niadhsdmum
Ihelf0hbandob]Ed6munddl|l.vs.*1.6prclud6tc€p1nfu||*ihfulffd
LU:],: *-r,\:l
rrl r 1s6orrrsrru r 1s610rr2arr wws<on
TestReport
No.: CE/2010/C0094Oale| 201U12t08 paae:Sof7
POLYFIL
AG
OBEMLLMENDSTRASSE
2OA,
CH€3OO
ZUG/ SWITZERLAND
|lll/[atl|l|lt|llrr
Analytical flow chart of halogen content
1) NanEoftheperson
whorEdefiEasurery€nt:
RitaChen
2) Naneof thepersoninchargeof neasu.eBentt
TroyChang
Samplepretreatment
/ Separation
Weighlingand puttingsanple in cell
Oryg€nBombCo.rbustion
/ Absorption
Dilution
lo fixedvolurE
Analysis
wasperfomEdby lC
6G) Gnd ft6 r€' '@n
1.r'llll!.
cdhF.y;1.r1f;nr..ll{r:,+rF:1i:-1:irl*ir;..J11i
l.}!}1,-r:."r,r
ny s6jed b G Gse6rcod ' o^s d s
tu ekmic
bmd @msnb
suq
€nnd
b ,
ndb..qdudgcaplnfunwibd
! idsntrzongrdF.oloe.rdwdil
::hi Fr' frr
lir:,,i4 r rMrorrs
TestReport
No.: CE/2010/C0094Datet2O1U1Z08 Page: 6of 7
POLYFILAG
OBERALLMENDSTRASSE
2OA,CH63OOZUG/ SWITZERLAND
tr]flttt!]||I|tIt]
PBB/PBDE
analyticalFLOWCHART
1) l.lanEof the personwho rEde dFasurefi€nt:RolIEnWong
2) t{afiE of the personin chargeof ryEasuaed€nt:
T.oy Chang
Firsttestingprocess-----'
Optional
screenprocess.--CodfinrEtionprocess - .>
Screenamlysis
V
Sanpleextraction/
SoxhletfiEthod
v
ConcenlratdDilute
E lrac€d solution
Filter
Analysisby GC/MS
cdp.nyiJ,:r,i!
l;ii ! rlftll::..ir;i
rh3fuum*ttsE3uadb!lheconF
rbr.otsadd€doi3u^6,bor.
;!n-1n
/.!|.rJ,
pr4t ladd Dc r6d rstsd cainor 6
rri,t.'
r:1,]t!11i.
ndbe.4ducdqcBpl
nrlr
iod
Test Report
No.: CE/2010C0094 Da'.e'.2O1042OAP a g e : 7 o f 7
POLYFILAG
OBERALLMENDSTRASSE
2OA,CH€3OO
ZUG/ SWITZERLANO
I
[tl
|l|lt[t
c0094
- Endof Repon"
c @ p a i yi r t , l r i t
iri
r.rl,,tif;i';rl
Th36umdts6suedbylhecdmp,
: n . { : : l ' r l . P . . : - t\ ! r i
/:,.:1iihf.
cisdsbecmtsiysrnd'Bsa66|[email protected]
.:I^ ri
t:rkf,!
| (,@rorze*
r r s6orrDrr
ww$!rm
Test Report
Applicant:
Number : TWNC00176939
Littelfuse, Philippines Inc.
LIMA Technology Center, Lipa City,
Malvar, Batangas
Date
: Oct 08, 2010
Sample Description:
One (1) group of submitted samples said to be :
Part Description
: Compound
Part Number
: 057895
Date Sample Received
: Oct 04, 2010
Date Test Started
: Oct 05, 2010
Test Conducted :
As requested by the applicant, for details please refer to attached pages.
Authorized By:
On Behalf Of Intertek Testing Services
Taiwan Limited
K. Y. Liang
Director
This report shall not be reproduced
except in full, without the written
approval of the laboratory.
Page 1 Of 7
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Number : TWNC00176939
Test Conducted
(Ⅰ) Test Result Summary :
Testing Item
Result (ppm)
Yellow Material
Heavy Metal
Cadmium (Cd) content
Lead (Pb) content
Mercury (Hg) content
Chromium VI (Cr6+) content
Polybrominated Biphenyls (PBBs)
Monobrominated Biphenyls (MonoBB)
Dibrominated Biphenyls (DiBB)
Tribrominated Biphenyls (TriBB)
Tetrabrominated Biphenyls (TetraBB)
Pentabrominated Biphenyls (PentaBB)
Hexabrominated Biphenyls (HexaBB)
Heptabrominated Biphenyls (HeptaBB)
Octabrominated Biphenyls (OctaBB)
Nonabrominated Biphenyls (NonaBB)
Decabrominated Biphenyl (DecaBB)
Polybrominated Diphenyl Ethers (PBDEs)
Monobrominated Diphenyl Ethers (MonoBDE)
Dibrominated Diphenyl Ethers (DiBDE)
Tribrominated Diphenyl Ethers (TriBDE)
Tetrabrominated Diphenyl Ethers (TetraBDE)
Pentabrominated Diphenyl Ethers (PentaBDE)
Hexabrominated Diphenyl Ethers (HexaBDE)
Heptabrominated Diphenyl Ethers (HeptaBDE)
Octabrominated Diphenyl Ethers (OctaBDE)
Nonabrominated Diphenyl Ethers (NonaBDE)
Decabrominated Diphenyl Ether (DecaBDE)
Halogen Content
Fluorine (F)
Chlorine (Cl)
Bromine (Br)
Iodine (I)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Remarks: ppm = Parts per million based on weight of tested sample = mg/kg
ND = Not detected
Responsibility Of Chemist : Irene Chiou / Kevin Liu / Cathy Chen
Date Sample Received
Testing Period
: Oct 04, 2010
: Oct 05, 2010 To Oct 07, 2010
Page 2 Of 7
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Number : TWNC00176939
Test Conducted
(Ⅱ) RoHS Requirement:
Restricted Substances
Cadmium (Cd) Content
Lead (Pb) Content
Mercury (Hg) Content
Chromium VI (Cr6+) Content
Polybrominated Biphenyls (PBBs)
Polybrominated Diphenyl Ehters (PBDEs)
Limits
0.01% (100ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for
homogeneous material.
(Ⅲ) Test Method:
Testing Item
Cadmium (Cd)
content
Lead (Pb) content
Mercury (Hg)
content
Chromium VI (Cr6+)
content
Testing Method
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 7, by microwave
digestion until the tested samples are
totally dissolved and determined by
ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in annex C, by alkaline
digestion and determined by UV-Vis
spectrophotometer.
Reporting Limit
2 ppm
2 ppm
2 ppm
1 ppm
Page 3 Of 7
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Number : TWNC00176939
Test Conducted
(Ⅲ) Test Method:
Testing Item
Polybrominated
Biphenyls (PBBs)
Polybrominated
Diphenyl Ethers
(PBDEs)
Halogen Content
Testing Method
With reference to IEC 62321 edition
1.0:2008 in annex A, by solvent
extraction and determined by GC-MSD
and further HPLC confirmation when
necessary.
With reference to IEC 62321 edition
1.0:2008 in annex A, by solvent
extraction and determined by GC-MSD
and further HPLC confirmation when
necessary.
With reference to EN 14582:2007 by
calorimetric bomb with oxygen and
determined by ion chromatography
Reporting Limit
5 ppm
5 ppm
50 ppm
Remark: Reporting limit = Quantitation limit of analyte in sample
Page 4 Of 7
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Number : TWNC00176939
Test Conducted
(Ⅳ) Measurement Flowchart:
Test For Cd/Pb/Hg/Chromium (VI)/PBBS/PBDES Contents
Reference Standard: IEC 62321 edition 1.0:2008
Sampling/grinding or cutting
Cd/Pb/Hg
Cr
Weigh sample and
add organic solvent
By spot test
Negative
Confirm the tested
samples are
totally dissolved
Make up with
deionized water
PBBs/PBDEs
Polymers /
electronics
Metal
For different
material, digest
the sample with
*1
appropriate acid
6+
Get 50cm2 sample
By boiling water
extraction
*2
Weigh sample
and add
alkaline
solution
By Soxhlet
extraction or
Solvent extraction
Definite temp.
extraction
Cool and filter
the extract
Concentrate the
extract and make up
with organic
solvent
Analyzed by ICP-OES
Analyzed by GC-MSD
Make up with deionized
water and add diphenylcarbazide solution
Remarks:
*1: List Of Appropriate Acid:
Material
Polymers
Metals
Electronics
Analyzed by UV-VIS
Acid Added For Digestion
HNO3,HCl,HF,H2O2,H3BO3
HNO3,HCl,HF
HNO3,HCl,H2O2,HBF4
*2: If the result of spot test is positive, Chromium VI would be determined as detected.
Page 5 Of 7
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Number : TWNC00176939
Test Conducted
(Ⅳ) Measurement Flowchart:
Test For Halogen Content
Reference Standard: EN 14582
Sampling/grinding or
cutting
Add absorbent in a
calorimetric bomb &
place weighed sample in
equipment
Fill the calorimetric
bomb with oxygen
Ignite then leave the
flask at room
temperature
Transfer the absorbent
into a volumetric flask
Make up with deionized
water
Analyzed by ion
chromatography
End Of Report
Page 6 Of 7
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Number : TWNC00176939
Test Conducted
Photo
Page 7 Of 7
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Test Report
Applicant:
Number : TWNC00176944
Littelfuse, Philippines Inc.
LIMA Technology Center, Lipa City,
Malvar, Batangas
Date
: Oct 08, 2010
Sample Description:
One (1) group of submitted samples said to be :
Part Description
: Sleeve
Part Number
: 275000-1
Date Sample Received
: Oct 04, 2010
Date Test Started
: Oct 05, 2010
Test Conducted :
As requested by the applicant, for details please refer to attached pages.
Authorized By:
On Behalf Of Intertek Testing Services
Taiwan Limited
K. Y. Liang
Director
This report shall not be reproduced
except in full, without the written
approval of the laboratory.
Page 1 Of 7
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Number : TWNC00176944
Test Conducted
(Ⅰ) Test Result Summary :
Testing Item
Heavy Metal
Cadmium (Cd) content
Lead (Pb) content
Mercury (Hg) content
Chromium VI (Cr6+) content
Polybrominated Biphenyls (PBBs)
Monobrominated Biphenyls (MonoBB)
Dibrominated Biphenyls (DiBB)
Tribrominated Biphenyls (TriBB)
Tetrabrominated Biphenyls (TetraBB)
Pentabrominated Biphenyls (PentaBB)
Hexabrominated Biphenyls (HexaBB)
Heptabrominated Biphenyls (HeptaBB)
Octabrominated Biphenyls (OctaBB)
Nonabrominated Biphenyls (NonaBB)
Decabrominated Biphenyl (DecaBB)
Polybrominated Diphenyl Ethers (PBDEs)
Monobrominated Diphenyl Ethers (MonoBDE)
Dibrominated Diphenyl Ethers (DiBDE)
Tribrominated Diphenyl Ethers (TriBDE)
Tetrabrominated Diphenyl Ethers (TetraBDE)
Pentabrominated Diphenyl Ethers (PentaBDE)
Hexabrominated Diphenyl Ethers (HexaBDE)
Heptabrominated Diphenyl Ethers (HeptaBDE)
Octabrominated Diphenyl Ethers (OctaBDE)
Nonabrominated Diphenyl Ethers (NonaBDE)
Decabrominated Diphenyl Ether (DecaBDE)
Halogen Content
Fluorine (F)
Chlorine (Cl)
Bromine (Br)
Iodine (I)
Result (ppm)
Transparent Plastic
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
272696
260
ND
ND
Remarks: ppm = Parts per million based on weight of tested sample = mg/kg
ND = Not detected
Responsibility Of Chemist : Irene Chiou / Kevin Liu / Cathy Chen
Date Sample Received
Testing Period
: Oct 04, 2010
: Oct 05, 2010 To Oct 07, 2010
Page 2 Of 7
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Number : TWNC00176944
Test Conducted
(Ⅱ) RoHS Requirement:
Restricted Substances
Cadmium (Cd) Content
Lead (Pb) Content
Mercury (Hg) Content
Chromium VI (Cr6+) Content
Polybrominated Biphenyls (PBBs)
Polybrominated Diphenyl Ehters (PBDEs)
Limits
0.01% (100ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for
homogeneous material.
(Ⅲ) Test Method:
Testing Item
Cadmium (Cd)
content
Lead (Pb) content
Mercury (Hg)
content
Chromium VI (Cr6+)
content
Testing Method
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 7, by microwave
digestion until the tested samples are
totally dissolved and determined by
ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in annex C, by alkaline
digestion and determined by UV-Vis
spectrophotometer.
Reporting Limit
2 ppm
2 ppm
2 ppm
1 ppm
Page 3 Of 7
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Number : TWNC00176944
Test Conducted
(Ⅲ) Test Method:
Testing Item
Polybrominated
Biphenyls (PBBs)
Polybrominated
Diphenyl Ethers
(PBDEs)
Halogen Content
Testing Method
With reference to IEC 62321 edition
1.0:2008 in annex A, by solvent
extraction and determined by GC-MSD
and further HPLC confirmation when
necessary.
With reference to IEC 62321 edition
1.0:2008 in annex A, by solvent
extraction and determined by GC-MSD
and further HPLC confirmation when
necessary.
With reference to EN 14582:2007 by
calorimetric bomb with oxygen and
determined by ion chromatography
Reporting Limit
5 ppm
5 ppm
50 ppm
Remark: Reporting limit = Quantitation limit of analyte in sample
Page 4 Of 7
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Number : TWNC00176944
Test Conducted
(Ⅳ) Measurement Flowchart:
Test For Cd/Pb/Hg/Chromium (VI)/PBBS/PBDES Contents
Reference Standard: IEC 62321 edition 1.0:2008
Sampling/grinding or cutting
Cd/Pb/Hg
Cr
Weigh sample and
add organic solvent
By spot test
Negative
Confirm the tested
samples are
totally dissolved
Make up with
deionized water
PBBs/PBDEs
Polymers /
electronics
Metal
For different
material, digest
the sample with
*1
appropriate acid
6+
Get 50cm2 sample
By boiling water
extraction
*2
Weigh sample
and add
alkaline
solution
By Soxhlet
extraction or
Solvent extraction
Definite temp.
extraction
Cool and filter
the extract
Concentrate the
extract and make up
with organic
solvent
Analyzed by ICP-OES
Analyzed by GC-MSD
Make up with deionized
water and add diphenylcarbazide solution
Remarks:
*1: List Of Appropriate Acid:
Material
Polymers
Metals
Electronics
Analyzed by UV-VIS
Acid Added For Digestion
HNO3,HCl,HF,H2O2,H3BO3
HNO3,HCl,HF
HNO3,HCl,H2O2,HBF4
*2: If the result of spot test is positive, Chromium VI would be determined as detected.
Page 5 Of 7
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Number : TWNC00176944
Test Conducted
(Ⅳ) Measurement Flowchart:
Test For Halogen Content
Reference Standard: EN 14582
Sampling/grinding or
cutting
Add absorbent in a
calorimetric bomb &
place weighed sample in
equipment
Fill the calorimetric
bomb with oxygen
Ignite then leave the
flask at room
temperature
Transfer the absorbent
into a volumetric flask
Make up with deionized
water
Analyzed by ion
chromatography
End Of Report
Page 6 Of 7
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Number : TWNC00176944
Test Conducted
Photo
Page 7 Of 7
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Test Report
Applicant:
Number : TWNC00182563S1
Littelfuse, Philippines Inc.
LIMA Technology Center, Lipa City,
Malvar, Batangas
Date
: Jan 20, 2011
This is to supersede
report No. TWNC00182563
dated Nov 22, 2010.
Sample Description:
One (1) group of submitted samples said to be :
Part Description
: Solder (metal)
Part Number
: 692320
Date Sample Received
: Nov 17, 2010
Date Test Started
: Nov 17, 2010
Test Conducted :
As requested by the applicant, for details please refer to attached pages.
Authorized By:
On Behalf Of Intertek Testing Services
Taiwan Limited
K. Y. Liang
Director
This report shall not be reproduced
except in full, without the written
approval of the laboratory.
Page 1 Of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Number : TWNC00182563S1
Test Conducted
(Ⅰ) Test Result Summary :
Result (ppm)
Silvery Metal
Testing Item
Heavy Metal
Cadmium (Cd) content
Lead (Pb) content
Mercury (Hg) content
Chromium VI (Cr6+) content (mg/kg with 50cm2)
Remarks: ppm
ND
<
#1
ND
898496(#1)(#2)
ND
Negative (< 0.02)
=
=
=
=
Parts per million based on weight of tested sample = mg/kg
Not detected
Less than
Results were transferred from report No. TWNC00188654 dated
Jan 17, 2011.
#2 = As claimed by the declaration submitted by the client, the
tested component was within the scope of RoHS exception:
lead in high melting temperature type solders (i.e. Leadbased alloys containing 85% by weight or more lead) were
exempted from the prohibition of RoHS directive 2002/95/EC
and amendment 2005/747/EC.
mg/kg with 50cm2 = milligram per kilogram with 50 square centimetre
Negative = A negative test result indicated positive observation
was not found at the time of testing.
Responsibility Of Chemist : Irene Chiou / Kevin Liu / Cathy Chen
Date Sample Received
Testing Period
: Nov 17, 2010
: Nov 17, 2010 To Nov 22, 2010
(Ⅱ) RoHS Requirement:
Restricted Substances
Cadmium (Cd) Content
Lead (Pb) Content
Mercury (Hg) Content
Chromium VI (Cr6+) Content
Limits
0.01% (100ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for
homogeneous material.
Page 2 Of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Number : TWNC00182563S1
Test Conducted
(Ⅲ) Test Method:
Testing Item
Cadmium (Cd)
content
Lead (Pb) content
Mercury (Hg)
content
Chromium VI (Cr6+)
content
Testing Method
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 7, by microwave
digestion until the tested samples are
totally dissolved and determined by
ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in annex B, by boiling water
extraction and determined by UV-Vis
spectrophotometer.
Reporting Limit
2 ppm
2 ppm
2 ppm
0.02
mg/kg with 50cm2
Remark: Reporting limit = Quantitation limit of analyte in sample
Page 3 Of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Number : TWNC00182563S1
Test Conducted
(Ⅳ) Measurement Flowchart:
Test For Cd/Pb/Hg/Chromium (VI)
Reference Standard:IEC 62321 edition 1.0:2008
Sampling/grinding or cutting
Cd/Pb/Hg
Cr
Polymers /
Electronics
Metal
For different
material, digest
the sample with
*1
appropriate acid
By spot test
Negative
Confirm the tested
samples are
totally dissolved
Make up with
deionized water
6+
*2
Weigh sample
and add
alkaline
solution
Get 50cm2 sample
Definite temp.
extraction
Boiling water
extraction
Cool and filter
the extract
Analyzed by ICP-OES
Make up with deionized
water and add diphenylcarbazide solution
Remarks:
*1: List Of Appropriate Acid:
Material
Polymers
Metals
Electronics
Analyzed by UV-VIS
Acid Added For Digestion
HNO3,HCl,HF,H2O2,H3BO3
HNO3,HCl,HF
HNO3,HCl,H2O2,HBF4
*2: If the result of spot test is positive, Chromium VI would be determined as detected.
End Of Report
Page 4 Of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Number : TWNC00182563S1
Test Conducted
Photo
Page 5 Of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Test Report
Applicant:
Number : TWNC00177238
Littelfuse, Philippines Inc.
LIMA Technology Center, Lipa City,
Malvar, Batangas
Date
: Oct 11, 2010
Sample Description:
One (1) group of submitted samples said to be :
Part Description
: Ink
Part Number
: 425826
Date Sample Received
: Oct 06, 2010
Date Test Started
: Oct 06, 2010
Test Conducted :
As requested by the applicant, for details please refer to attached pages.
Authorized By:
On Behalf Of Intertek Testing Services
Taiwan Limited
K. Y. Liang
Director
This report shall not be reproduced
except in full, without the written
approval of the laboratory.
Page 1 Of 6
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Number : TWNC00177238
Test Conducted
(Ⅰ) Test Result Summary :
Testing Item
Result (ppm)
White Ink
Heavy Metal
Cadmium (Cd) content
Lead (Pb) content
Mercury (Hg) content
Chromium VI (Cr6+) content
Polybrominated Biphenyls (PBBs)
Monobrominated Biphenyls (MonoBB)
Dibrominated Biphenyls (DiBB)
Tribrominated Biphenyls (TriBB)
Tetrabrominated Biphenyls (TetraBB)
Pentabrominated Biphenyls (PentaBB)
Hexabrominated Biphenyls (HexaBB)
Heptabrominated Biphenyls (HeptaBB)
Octabrominated Biphenyls (OctaBB)
Nonabrominated Biphenyls (NonaBB)
Decabrominated Biphenyl (DecaBB)
Polybrominated Diphenyl Ethers (PBDEs)
Monobrominated Diphenyl Ethers (MonoBDE)
Dibrominated Diphenyl Ethers (DiBDE)
Tribrominated Diphenyl Ethers (TriBDE)
Tetrabrominated Diphenyl Ethers (TetraBDE)
Pentabrominated Diphenyl Ethers (PentaBDE)
Hexabrominated Diphenyl Ethers (HexaBDE)
Heptabrominated Diphenyl Ethers (HeptaBDE)
Octabrominated Diphenyl Ethers (OctaBDE)
Nonabrominated Diphenyl Ethers (NonaBDE)
Decabrominated Diphenyl Ether (DecaBDE)
Halogen Content
Fluorine (F)
Chlorine (Cl)
Bromine (Br)
Iodine (I)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
222
ND
ND
Remarks: ppm = Parts per million based on wet weight of tested sample = mg/kg
ND = Not detected
Responsibility Of Chemist : Irene Chiou / Kevin Liu / Cathy Chen
Date Sample Received
Testing Period
: Oct 06, 2010
: Oct 06, 2010 To Oct 11, 2010
Page 2 Of 6
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Number : TWNC00177238
Test Conducted
(Ⅱ) RoHS Requirement:
Restricted Substances
Cadmium (Cd) Content
Lead (Pb) Content
Mercury (Hg) Content
Chromium VI (Cr6+) Content
Polybrominated Biphenyls (PBBs)
Polybrominated Diphenyl Ehters (PBDEs)
Limits
0.01% (100ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for
homogeneous material.
(Ⅲ) Test Method:
Testing Item
Cadmium (Cd)
content
Lead (Pb) content
Mercury (Hg)
content
Chromium VI (Cr6+)
content
Polybrominated
Biphenyls (PBBs)
Polybrominated
Diphenyl Ethers
(PBDEs)
Halogen Content
Testing Method
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 7, by microwave
digestion until the tested samples are
totally dissolved and determined by
ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in annex C, by alkaline
digestion and determined by UV-Vis
spectrophotometer.
With reference to IEC 62321 edition
1.0:2008 in annex A, by solvent
extraction and determined by GC-MSD
and further HPLC confirmation when
necessary.
With reference to IEC 62321 edition
1.0:2008 in annex A, by solvent
extraction and determined by GC-MSD
and further HPLC confirmation when
necessary.
With reference to EN 14582:2007 by
combustion flask with oxygen and
determined by ion chromatography
Reporting Limit
2 ppm
2 ppm
2 ppm
1 ppm
5 ppm
5 ppm
50 ppm
Remark: Reporting limit = Quantitation limit of analyte in sample
Page 3 Of 6
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Number : TWNC00177238
Test Conducted
(Ⅳ) Measurement Flowchart:
Test For Cd/Pb/Hg/Chromium (VI)/PBBS/PBDES Contents
Reference Standard: IEC 62321 edition 1.0:2008
Sampling/grinding or cutting
Cd/Pb/Hg
Cr
Weigh sample and
add organic solvent
By spot test
Negative
Confirm the tested
samples are
totally dissolved
Make up with
deionized water
PBBs/PBDEs
Polymers /
electronics
Metal
For different
material, digest
the sample with
*1
appropriate acid
6+
Get 50cm2 sample
By boiling water
extraction
*2
Weigh sample
and add
alkaline
solution
By Soxhlet
extraction or
Solvent extraction
Definite temp.
extraction
Cool and filter
the extract
Concentrate the
extract and make up
with organic
solvent
Analyzed by ICP-OES
Analyzed by GC-MSD
Make up with deionized
water and add diphenylcarbazide solution
Remarks:
*1: List Of Appropriate Acid:
Material
Polymers
Metals
Electronics
Analyzed by UV-VIS
Acid Added For Digestion
HNO3,HCl,HF,H2O2,H3BO3
HNO3,HCl,HF
HNO3,HCl,H2O2,HBF4
*2: If the result of spot test is positive, Chromium VI would be determined as detected.
Page 4 Of 6
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Number : TWNC00177238
Test Conducted
(Ⅳ) Measurement Flowchart:
Test For Halogen Content
Reference Standard: EN 14582
Sampling/grinding or
cutting
Add absorbent in a
combustion flask &
place weighed sample in
equipment
Fill the combustion
flask with oxygen
Ignite then leave the
flask at room
temperature
Transfer the absorbent
into a volumetric flask
Make up with deionized
water
Analyzed by ion
chromatography
End Of Report
Page 5 Of 6
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Number : TWNC00177238
Test Conducted
Photo
Page 6 Of 6
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401