ICPTest_263HF pdf

ICP Test Report Certification Packet
Company name :
Littelfuse, Inc.
Product Series:
Pico
Product #:
263xxxHF Series
Issue Date:
April 11, 2011
It is hereby certified by Littelfuse, Inc. that there is neither RoHS (EU Directive
2002/95/EC)-restricted substance nor such use, for materials to be used for unit parts, for
packing/packaging materials, and for additives and the like in the manufacturing processes.
In addition, it is hereby reported to you that the parts and sub-materials, the materials to be used
for unit parts, the packing/packaging materials, and the additives and the like in the manufacturing
processes, are all composed of the following components.
Issued by:
<Global EHS Engineer>
(1) Parts, sub-materials and unit parts
This document covers the Pico RoHS-Compliant series products manufactured by
Littelfuse, Inc.
< Raw Materials Used
Please see Table 1
(2) The ICP data on all measurable substances
Please see appropriate pages as identifed in Table 1
Remarks:
Pb (lead) contained in the high temperature melting solder > 85% and is categorized as
exempt under section 7a of the RoHS Annex.
Form 585-047 Rev. A
1
2/21/06
Table 1: List of Raw Materials covered by this report
Total Parts
1
2
3
4
5
6
Raw Material Part Number
909-448
497xxx-001
082xxx
692321
910-272
087341
Raw Material Description
Body-Ceramic
Element – Ni42Fe58MCuMSn
Element – 5% by weight Ag Clad Cu
Solder
Cap & Lead Assembly
Epoxy Powder ( HF Green)
2
Page(s)
3-9
10-16
17-25
26-30
31-35
36-42
Test Report
Applicant:
Number : TWNC00176946
Littelfuse, Philippines Inc.
LIMA Technology Center, Lipa City,
Malvar, Batangas
Date
: Oct 08, 2010
Sample Description:
One (1) group of submitted samples said to be :
Part Description
: Body
Part Number
: 909-448
Date Sample Received
: Oct 04, 2010
Date Test Started
: Oct 05, 2010
Test Conducted :
As requested by the applicant, for details please refer to attached pages.
Authorized By:
On Behalf Of Intertek Testing Services
Taiwan Limited
K. Y. Liang
Director
This report shall not be reproduced
except in full, without the written
approval of the laboratory.
Page 1 Of 7
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Number : TWNC00176946
Test Conducted
(Ⅰ) Test Result Summary :
Testing Item
Result (ppm)
White Material
Heavy Metal
Cadmium (Cd) content
Lead (Pb) content
Mercury (Hg) content
Chromium VI (Cr6+) content
Polybrominated Biphenyls (PBBs)
Monobrominated Biphenyls (MonoBB)
Dibrominated Biphenyls (DiBB)
Tribrominated Biphenyls (TriBB)
Tetrabrominated Biphenyls (TetraBB)
Pentabrominated Biphenyls (PentaBB)
Hexabrominated Biphenyls (HexaBB)
Heptabrominated Biphenyls (HeptaBB)
Octabrominated Biphenyls (OctaBB)
Nonabrominated Biphenyls (NonaBB)
Decabrominated Biphenyl (DecaBB)
Polybrominated Diphenyl Ethers (PBDEs)
Monobrominated Diphenyl Ethers (MonoBDE)
Dibrominated Diphenyl Ethers (DiBDE)
Tribrominated Diphenyl Ethers (TriBDE)
Tetrabrominated Diphenyl Ethers (TetraBDE)
Pentabrominated Diphenyl Ethers (PentaBDE)
Hexabrominated Diphenyl Ethers (HexaBDE)
Heptabrominated Diphenyl Ethers (HeptaBDE)
Octabrominated Diphenyl Ethers (OctaBDE)
Nonabrominated Diphenyl Ethers (NonaBDE)
Decabrominated Diphenyl Ether (DecaBDE)
Halogen Content
Fluorine (F)
Chlorine (Cl)
Bromine (Br)
Iodine (I)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Remarks: ppm = Parts per million based on weight of tested sample = mg/kg
ND = Not detected
Responsibility Of Chemist : Irene Chiou / Kevin Liu / Cathy Chen
Date Sample Received
Testing Period
: Oct 04, 2010
: Oct 05, 2010 To Oct 07, 2010
Page 2 Of 7
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Number : TWNC00176946
Test Conducted
(Ⅱ) RoHS Requirement:
Restricted Substances
Cadmium (Cd) Content
Lead (Pb) Content
Mercury (Hg) Content
Chromium VI (Cr6+) Content
Polybrominated Biphenyls (PBBs)
Polybrominated Diphenyl Ehters (PBDEs)
Limits
0.01% (100ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for
homogeneous material.
(Ⅲ) Test Method:
Testing Item
Cadmium (Cd)
content
Lead (Pb) content
Mercury (Hg)
content
Chromium VI (Cr6+)
content
Testing Method
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 7, by microwave
digestion until the tested samples are
totally dissolved and determined by
ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in annex C, by alkaline
digestion and determined by UV-Vis
spectrophotometer.
Reporting Limit
2 ppm
2 ppm
2 ppm
1 ppm
Page 3 Of 7
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Number : TWNC00176946
Test Conducted
(Ⅲ) Test Method:
Testing Item
Polybrominated
Biphenyls (PBBs)
Polybrominated
Diphenyl Ethers
(PBDEs)
Halogen Content
Testing Method
With reference to IEC 62321 edition
1.0:2008 in annex A, by solvent
extraction and determined by GC-MSD
and further HPLC confirmation when
necessary.
With reference to IEC 62321 edition
1.0:2008 in annex A, by solvent
extraction and determined by GC-MSD
and further HPLC confirmation when
necessary.
With reference to EN 14582:2007 by
calorimetric bomb with oxygen and
determined by ion chromatography
Reporting Limit
5 ppm
5 ppm
50 ppm
Remark: Reporting limit = Quantitation limit of analyte in sample
Page 4 Of 7
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Number : TWNC00176946
Test Conducted
(Ⅳ) Measurement Flowchart:
Test For Cd/Pb/Hg/Chromium (VI)/PBBS/PBDES Contents
Reference Standard: IEC 62321 edition 1.0:2008
Sampling/grinding or cutting
Cd/Pb/Hg
Cr
Weigh sample and
add organic solvent
By spot test
Negative
Confirm the tested
samples are
totally dissolved
Make up with
deionized water
PBBs/PBDEs
Polymers /
electronics
Metal
For different
material, digest
the sample with
*1
appropriate acid
6+
Get 50cm2 sample
By boiling water
extraction
*2
Weigh sample
and add
alkaline
solution
By Soxhlet
extraction or
Solvent extraction
Definite temp.
extraction
Cool and filter
the extract
Concentrate the
extract and make up
with organic
solvent
Analyzed by ICP-OES
Analyzed by GC-MSD
Make up with deionized
water and add diphenylcarbazide solution
Remarks:
*1: List Of Appropriate Acid:
Material
Polymers
Metals
Electronics
Analyzed by UV-VIS
Acid Added For Digestion
HNO3,HCl,HF,H2O2,H3BO3
HNO3,HCl,HF
HNO3,HCl,H2O2,HBF4
*2: If the result of spot test is positive, Chromium VI would be determined as detected.
Page 5 Of 7
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Number : TWNC00176946
Test Conducted
(Ⅳ) Measurement Flowchart:
Test For Halogen Content
Reference Standard: EN 14582
Sampling/grinding or
cutting
Add absorbent in a
calorimetric bomb &
place weighed sample in
equipment
Fill the calorimetric
bomb with oxygen
Ignite then leave the
flask at room
temperature
Transfer the absorbent
into a volumetric flask
Make up with deionized
water
Analyzed by ion
chromatography
End Of Report
Page 6 Of 7
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Number : TWNC00176946
Test Conducted
Photo
Page 7 Of 7
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Validi
FOr QUe$l
PleaseCo
TestReport
No.: CE20'10/C0095Oale| 2010112108Paoe: 1 of 7
POLYFILAG
OBERALLMENDSTRASSE
2OA,CH€3OOZUG / SWITZERLAND
Thofollowingaamplda)was/weresubmilted and id6ntifi6d by/on behalf of the cliont as:
Ni42FeSSMCuMSn
10-0914
2010t12t01
201011?,01
ro 2010t12na
SampleDescription
Buyer/OrderNo.
SampleReceiving
Date
TestingPeriod
Pleasereferto nextpage(s)
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paget2 of 7
No.: CE/201OC0095Datet2O10/121OA
POLYFILAG
OBERALLMENDSTRASSE
2OA,CH43OO
ZUG/ SWITZERLAND
tr]
tttl|ltl|l|l
Ta€t Resultls|
PARTI{AMENo.1
Test ltem (s):
Cadmium(Cd)
SILVERCOLORED
ITETAL
WIRE
Unlt
Method
MDL
R€6ult
No.l
mg/Kg Withref€rence
to IEC62321:2008and
n.o.
p€rfomedby ICP-AES.
Lead(Pb)
mg/Kg Withref€rence
to IEC62321:2008and
n.d,
perfodned
by ICP-AES.
(Hg)
Mercury
mg/kg Withreference
to IEC62321:2008and
n.d.
perfomedby ICP-AES.
Hexavalent
Chromium
Cr(Vl)by
Withreference
to IEC62321:2008end 0.02mgr'kgNegative
Spottest / boilingwaterextraction
perfofinedby Spottest / boiling,,,€ter with50cm'z
extraclionMethod.(SeeNote6)
surface
Halogsn
(F)
Halogen-Fluorine
(CASNo.:014762-94€)
(Cl)
Halogen-Chlorine
(CASNo.:022537-15-1)
(Br)
Halogon-Bromine
(CASNo.:010097-32-2)
(l)
Halogen-lodine
(CASNo.:014362-4€)
Sumof PBBa
Monobromobiphenyl
Dibromobiphenyl
Tribromobiphenyl
Tetrabromobiphenyl
Pentabromobiphenyl
Hexabromobiphenyl
With referenceto BS EN 14582t2007.
mg/Kg
AnalysiswE6perfomedby lC.
50
n.d.
50
n.d.
50
n.d.
50
n-d.
n.d-
mg/Kg
Withreference
to IEC62321:2008and
oerfomedbv GC/MS.
Hepiabromobiphenyl
5
5
5
5
5
5
n.d.
n.d.
n.o.
n.o.
n,d,
n.d.
n.d.
n.d,
n.d.
Odabromobiphenyl
Nonabromobiphenyl
Dec6bromobiphenyl
5
n.d.
p6G)r€$adIh t B1r6f.d dnnd b
l l'1ti'l'
c m E f r t i ! 1 1; i I . I l i l r l : ? r s l . . ; , \ j r l t 1 : n r l L l . t r l l l : + . i ' ' l
T.sd@hd
s *u€d by t€ compsnyebled ro B Gm,dc4dd 06 d s
ror.edmr fomd @d6tu
eq
r.@nr@!m andjudsdidtr ssB d
sponrbr{ystobc 3n{af,!rh6d@
dnLyandwrhLi$€h'lsdcr€ds Bl
pM w b^ 4!6va drho companvAnvu
s r€groduc€d
*..pi 'nru |
rbr r otu ad dEdds undd rh. vdc&r
"{hod
! rdsorzoe,raiFcolivrdwd/:
rll:r,1r
rlrr IFf,-rf r+s610r)rstTef 1d{02)22e07
w!$.om
Test Report
No.: CE/201oC0095 Odl€:2010h?J(]f P a g e : 3 o f 7
POLYFIL
AG
OBERALLMENDSTMSSE
2OA,CH.63OO
ZUG/ SWITZERLAND
T€t ltem (s):
Sumof PBDES
lllonobromodiphenyl
ether
Dibromodiphenyl
ether
f ribromodiphenyl
ether
fetrabromodiphenyl
ether
Pentabromodiphenyl
ether
Hexabrcmodiphenyl
ether
Hoptabromodiphenyl
ether
Octabromodiphenyl
ether
Nonabromodiphenyl
ether
Decabromodiphenyl
ether
Unit
r
l||t||t
Roault
method
"DL
Withreferenc€
to IEC62321:2008and
pedormed
by GC/[,S.
No.l
n.d.
n.o,
5
mg/Kg
[tll
n.o,
n.d.
5
5
5
n.d.
n.d.
n.d.
5
5
5
n.d.
n.d.
n.d.
n.d.
Note :
1. mg/kg= ppm : 0.1we/6
= 1000ppm
2. n.d.= NotDetected
3. MOL= MethodDot€ction
Limit
4."-"=NotRegulated
(NoUnit)
5. " = Qualitative
analysis
6. Spot-test:
Negative= Absenceof Cr(Vl)coating/ surfacelayer;Positive= presenceof Cr(Vt)coating/ surfacetayer;
Cfhetestedsampleshouldbefuftherverifiedby boiling-wEter-€xtraclion
methodif the spottest esult cannot
be confirmed.)
BoiIing-water-extraclion:
Negative= Absenceof Cr(Vl)coating/ surfacelayer; Positive= Presenc€of Cr(Vl)coating/ surfacel€yer;
The detectedconcentrationin boiling-water+xhaction
solutionis €quator greaterthan0.02mg/kgwith 50 cm,
samplesurfacearea.
c o m F r yi ' : l l i r r ; i t
.tiil-!'rFlln;;-1111*-ir;.rlll-r.{l:-r,l
ny sdted b 6 G*Ercdd
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b e
turetr €ids
be compa0ysr drnss a
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.-$r i
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Msber dr(he5G56@p r5C5sA)
Test Report
No.: CE/2010/C0095D€['e 2O.\O|1ZOApaget4ofz
POLYFIL
AG
OBERALLMENDSTRASSE
2OA,CH€3OO
ZUG/ SWITZERLAND
lll[lrr
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1) Thesesarples weredissoh€dtotallyby preronditioningfiEthodaccordingto betowflowchat
( Cft bst rEthod e)(ctuded
)
2) llarne of the personwho rtsde nEasurerEnttClimbgreatyarE
3) Mrne of the personin chargeof dEasurernent:
TroyChang
A.id digestion
by suitable
acid
dependedon differentsarple
rnaterial(as belowtable)
Add appropdate anDunt of
digestionre€gent
Fleatto appropriate
ternperature
to extract
Cool,frlterdigestate
throughfilter
1) AlkaliFusion
2) HCltodissotue
Adddipheny
l-carbazide
for
colordeveloprEnt
SanpleMaterial
DigestionAcid
So9l, copper,alufiinum,solder
Aquaregia,HNO3,HCl,HF,l-lro,
rEasure the abGorbanc€
Glass
HNO3/HF
at 540 nmby UV-VIS
Gold,platinun\palhdium,ceranic
Aqua€gia
Silver
HNos
Plastic
l-ISOr, HrOr,HNOg,t-tCl
Othe|s
Anyacidto tctraldig€stion
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romal d@mdds s6j
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Test Report
No. I CE/2010/C0095 D&e: 201U1210EPage: 5of 7
POLYFILAG
OBERALLMENOSTRASSE
2OA,CH$3OO
ZUG/ SWITZERLAND
Analytical flow chart of halogen content
1) t,lanpoftheperson
whonEdenEa6urcd€nt:
RitaChen
2) l.lanEofthepersonin chargeof fiFasurerEnt:
TroyChang
Sanplepretreatient / Separation
Weighting
andputtingsarple in cell
OxygenBombConbustion
/Ab€oDtion
Dilution
to fixedvolurp
Analysiswas perfonrEdby lC
nnihsi6|cpdld&onybihegndsG]isndThsbsi@dendb
!'raz!,.
cmFiyni;rlltr!;.rri:l,r:+df::r.n\t(,1:iia.r1l1.tr.l!rr-\lrl!iil,1.
fts dum6l6 's*d bybecmr
r6ionq f 3ry ftscmrys
bnghsandob|Ea|trss6'blE
so3€s@b'
t€ro 6crsrandbsdn
I]|||tu
l|tItIl
Test Report
No.: CE/2010/C0095Dale:2O1U121O8Page: 6 of 7
POLYFILAG
OBERALLMENDSTRASSE
2OA,CH$3OO
ZUG/ SWITZERLAND
PBB/PBDEanalyticatFLOWCHART
1) Narneofthe pe6on who fiECbnEasuler€nt: Rornanwong
2) Narneofthe personin chargeof rEasurerent: Troy Chang
Firstt€stingprocess-.--+
Optionalscreenprocess---,
proce6s - .>
ConfirnEtion
Scaeen
analysis
"""""'1"""""'
56rple ext€ctiorV
SoxhletflFthod
I
ConcentratdDih.rte
Extracted
solution
Filter
Analysis
by GC/lrS
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|l]tI|t||fiIltln
TestReport
No.: CE2010/C0095 Dale 21iOh2JOa Page 7 ol7
POLYFIL
AG
OBEMLLMENDSTRASSE
2OA,CH63OO
ZUG/ SWITZERLAND
ll]flt!t]ll|Itll
c009s
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TestReport
No.: CE12011/10410A
Oale: 2O11t0'Ii1 P a g e : 1 o f g
ELSCHUKOM
ELEKTROSCHUTZKOMPONENTENBAU
GI\.TBH
GEWERBESTRASSE
87,D.98669
VEILSDORF,
GERMANY
tl][ttt][littltt
Thefollowingsample(s)waa/weresubmittedand identifiedby/onbehaltofthe cliontas :
SampleDescription
Style/ltem
No.
SILVERPLATED& PURESILVERWIRES
(1)101.014-.---EWN02.01.-SILVER
PLATEDCOPPER
W|RE- Cu,Ag - - %
(2)101.0131.---EWN02.01.-PURE
SILVERWtRE-Ag1000
(3)101.0123.0--EWN01,03.. SILVERPLATEDPURESTNICKELWIRENi99.98%,
Agl0/6
( 4 )1 0 1 . 0 1 8 -2-.-0
EWN03-07,. SILVER-COPPER
ALLOYPLATEDCOPPER
CLADWIRE-ELCON
D,Agcus%
(5)101.0120.0--SILVERPLATEDCONSTANTAN
WIRE-CuNi,t4,
Ag5%
Countryof Origin
SampleR€ceiving
Date
TestingPerjod
GERMANY
2011tO1t04
2011tO|tU
TO2U1n1t11
Test R€ault(s)
Pleasereferto nextpag€(s)-
NW4)
Sgn d 6rltd
Ctrdr{.d t&rtrt-TS.l
comFryr.irf,jnii!.-r
€lt ie$d h s r6d ,eFd €ind b" tr
ri '!,rn1l l'lrli.,'ra: /.iii-i!rr.1,::l:L Jii . I ,ritrrr
nysub]sd|obc5e6]codlbnso,s
suq3dro r€ms ad cdms
tu €
Test Report
No.: CE2011l10410ADate: 2011to1t.l
l Page:2ofg
ELSCHUKOM
ELEKTROSCHUTZKOMPONENTENBAU
GMBH
GEWERBESTRASSE
87,D.98669
VEILSDORF,
GERMANY
f,]tIlt||
ttttttl
Test Result{s)
PARTNAMENo.1
Te8tltem (s):
Cadmium(Cd)
Lead (Pb)
(Hg)
[4ercury
Hexavaler{
Chromium
Cr(Vl)by
Spottest / boilingwater
e)dractaon
Peduorooclanesulfonates
(PFOS)
PFOS-Acid
PFOS- MetalSalt
PFOS-Amide
PFOA(CASNo.:000335$7-1)
MIXEDALL COLORMETALWIREONCLUDING
THE
PLATING
LAYER)(5 KINDS)
Unit
Method
MDL
Result
No.l
n.o.
mg/Kg Withreferenc€
to IEC62321:
2
2008€ndperfomedby ICP.AES.
mg/Kg With referenceto tEC62321:
n.d.
2008andperfomedby ICP-AES.
mg/Kg With referenceto IEC62321:
2
n.d.
2008andperform€d
by lCPdES.
With referenceto IEC62321:
0.02mgr'kgNegative
2008and perfornedby Spottest / with50cm'z
boiling,,raater
ext€ctionMethod.
suface
(SeeNote5)
mg/xg With refer€ncelo US EPA3540C:
10
n.d.
1996methodfor PFOSContent.
Anaiysiswaspertormedby
LC/MS.
mg/ks With referenceto Us EPA3540C:
'10
n.d.
50
n.d.
50
n.d-
50
n.d.
50
n.o.
1996methodfor PFOAContent.
Analysiswasp€rformedby
LC/MS.
Halogen
(F) (CASNo.:
Halogen-Fluorine
014762-94€)
(Cl)(CASNo.:
Halogen-Chlorine
022537-1s-1)
(Br)(CASNo.:
Halogen-Bromine
010097-32-2)
With referenceto gS EN
mg/Kg 14582:2007.
Analysis
w€s
pefformed
by lC.
(l) (CASNo.:
Halogen-lodine
014362-44-8)
oldEd6i.4inlu
.r!r!1 ;:r!rrllt::11t i.bF.9,,.1.r!,:ii',,
comDary!::lrit'rJ:.-ri1;.
D6tuad
s ss6d by the cohpsny 3u&d b a GssBicod lionso, s
suq€d b rems ad codrms ro, E
l
rrlllill
nsibi'y6loiscLen':db"@men
nolb6fopfoduc€.ot@pl'nltrr.s|MU|
Memb4,
orthe56s6 o!p 6GssAJ
TestReport
No.: CE2011l10410A Date| 2O11tO
lti1
Page:3ofg
ELSCHUKOM
ELEKTROSCHUTZKOMPONENTENBAU
GMBH
GEWERBESTMSSE
87,D-98669
VEILSDORF,
GERIT'ANY
Test ltom (s):
Sum of PBB6
Monobromobiphenyl
Dibromobiphenyl
Tribromobiphenyl
Tetrabromobiphenyl
Pentabromobiphenyl
Hexabrcmobiphenyl
H€ptabrornobiphenyl
Octabromobiphenyl
Nonabromobiphenyl
Decabromobiphenyl
Sumot PBDES
lVonobromodiphenyl
ether
Dibromodiphenyl
ether
Tribromodiphenyl
elher
Tetrabromodiphenyl
ether
Pentabromodiphenyl
ether
Hexabromodiphenyl
ether
Heptabromodiphenyl
ether
Octabromodiphenyl
ether
Nonabromodiphenyl
ether
Decabromodiphenyl
ether
unlt
tl][Ilr|I|
Method
TIDL
5
5
5
Re3ult
No.1
n.d.
n.d.
n.d.
n.o,
n.d.
5
n.d-
n.d.
n.d.
mgkg
Withreference
to IEC62321:
2008andperformed
by GC/MS.
5
n.d.
n.d.
5
n.o.
n.d.
5
5
5
5
5
5
5
in rh' 16r cpd dar6ry rorb smprslr rsdd ft sree @n €nid b.qd
,l-.1+,ildll: :--r.:,?.
c@Fiy,r:rrri.iN
r i - t r r : r : l l i t i l rr , l i ! t r r A i
rl{'1
Thseumrt[Esuadb'lhecomMysUb]dbbGsffi:condlffids
r!r,ttr
rlrs6rc?2rr&ras
n.d.
n.o.
n.d.
n.o,
n.o,
n.o,
n,d,
n.d.
n.o.
ll
TestReport
paoe:4of9
No.: CEi2011l1MlOADed;e2011101t11
ELSCHUKOM
ELEKTROSCHUTZKOMPONENTENBAU
GMBH
GEWERBESTMSSE
87,}.98669VEILSDORF,
GERMANY
[l
lllrr||||l
Note: 1. mg/kg= ppm;o.1$olo=1000ppm
2. n.d.= NotDetected
3. MDL= MethodDetection
Limit
4."-"=NotRegulated
5. Spot-test:
Negative= Absenceof Cr(Vt)coating/ surfacetayer,
Positive= Presenceof Cr(Vl)coating/ sudacelaye.;
(Thetestedsampleshouldbe furtherverifiedby boiting-water-extraction
methodif the
spoltestresultcannotbecontimed.)
Boiling-water-extraction
:
Negative= Absenceof Cr(Vl)coating/ surfacelayer.
Positive= Presenceof Cr(Vl)coating/ surfacelayer;
the detectedconceftrationin boiling-&ater-extraclion
solutionis €quator greater
than 0.02mg/kgwjth 50 cm2safiple surfacearea.
(NoUnit)
6. " = Qualitative
analysis
7. Thesample(s)
wadlvereanalyzed
on beh€lfof theapplicant
as mixingsamplein onetesting.
Theaboveresult(s)Mras/were
onlygivenas the informalityvalue.
PFOSRefer€nceInformation : Directlve2006/{2ZEC
('t) Maynotbe placedonthe marketor us€das a substance
or constituent
of preparations
In a
0/6
concentration
equaltoor higherthan
0.005 by masr.
(2)Maynol be placedon themarketin 6emi-finished
products
or adicte6,
or partsthereof,if the
concentrationof PFOSis equalto or higherthan0. 1% by masscalculatedwith refercnceto the
massof skucturallyor microstruclurally
distinctpartsthat containPFOSor, for textilesor omer
coatedmaterials,
if theamountof PFOSis equaltoor higherthan'1pg/m,
of thecoatedm€terial.
c@Fryr
fttrd@md.
rir;;'..:iitsrr:rfii.:;llrrlrl:.:ir
np6Glb{d rhs bsrr@d €.nd e
r-rr+liFxafJltr?:.I. r.t-:,'tl'l
sdby'fuc.mpa
36lsd6T.ms4dcmdiloBdE
rL-: ,: :!r 1i', i,s6orrrt
l|l
TestReport
No.:CE/2011/1M10A Date| 2011t01t11 P a g e : 5 o f g
ELSCHUKOM
ELEKTROSCHUTZKOMPONENTENBAU
GMBH
GEWERBESTRASSE
87,D.98669
VEILSDORF,
GERMANY
Thesesamplesweredi66ovedtotallyby pre-conditioning
methodaccordingto belowflo^/chart.
( Cf' testmethodexcluded
)
yang
Nameof theper6onwhomademeasurementt
Climbgreal
3) Nameof the pe6on in chargeof measurementTroyChang
1)
Cutting/ Preparation
Aciddigestion
by suitable
acid
dependedon difierenlsampl€
material(as belowtable)
Add appropriateamountof
digestionreagent
Heatto appropriate
temperatureto exhact
Cool,filterdigestate
throughfiller
1) AlkaliFusion
2) HCltodissolve
Add diphenyl-carbazide
for
colordevelopmerf
SampleMaterial
DigestionAcid
S1eel,
copper.aluminum,
bolder
Aqua regia,HNO3,HCl,HF,HrO,
Glass
HNO3/HF
palladium,
Gold,platinum,
ceramic Aqua regia
Silver
HNO3
Plastic
Others
HrSO4,
HrOr,HNO3,
HCt
Anyacidto totaldigestion
'd th s rsr r€pd f€1arsry ro tb smpblt redd h s 16r re@d€inor 6 r6p
, t r,,i!ir.
:rir,
i-*rfii!:l.!c@Fny 4rlr;!i:ir..1.-fi+rrrlrrriir:i!1rf.ir:9!i
Th'deumd6G5uadbylh6cohpanyEubdbbcff€conditrsds
isbi|ys10i9c.d.ndl|6d@fun
_:, r fJ Irr
measurethe absotbance
at 540 nm by uV-VlS
Test Report
No.: CE/2011/10410ADale| 2l11t01ti1 P a g e : 6 o f g
ELSCHUKOMELEKTROSCHUTZKOI/|PONENTENBAU
GMBH
GEWERBESTRASSE
87, D.98669VEILSDORF,GERMANY
ill
||atl[m||]t
Analtticalflow chartof Soxhletextraction(LC/MS)procedure
1) Nameof thepersonwhomademeasurement:
LydiaFu
2) Nameofthe personin chargeof measurement
ShinjyhChen
rTe61ltems:PFOS/PFOA. Benzotriazole
Samplepretreatmenu6eparation
Datra
nrh3r*rr€@1d€ronryrolbsampstrsdd
comFiv f.lr,,;-'
rr ,ir , rlrir i l:!rii
th 3 6umdr tr csusdbyrhsconFny subr€d
b b6effi condrtrsd s
rhdr r $t
a^d ob 0d o^3uid.r th. ta
ft€radrcFd€mdbc
nsb iv 6 io is c ed.d h6 dne.
iiot be €pdud
ace|' 'n ,u r,khtu
f! r,rirr:i,,i
i +s6 orrer!
r+88
TestReport
No.I CE/2011/'104104Date: 2011|t11t1|1page: 7 of I
ELSCHUKOM
ELEKTROSCHUTZKOMPONENTENBAU
GMBH
GEWERBESTRASSE
87, D-98669
VEILSDORF,
GERMANY
[fffitf,IltIlttttII
Analyticalflow chartof hatogancontent
1) Nameofthepersonwhomademeasurement:
RitaChen
2) Nameof thepe6onin chargeof measuaement:
TroyChang
Samplepretre€tment
/ Separation
Weighting
€ndputtingsamplein cell
OrygenBombCo.nbustion
/ Absorption
Dilution
to fixedvolume
Analysas
wasperfomedby lC
6G) raGd rhs Gn €p.n 6^d
- J ,ltbi!
u.i-il.ial4rr
r:i;''].
1i:
ny suqed b {s Gm6brcdr
ons oi s
compary l:if,i!J.
6.€8dq€bmd
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6 d
@Batu
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|h6/rohb.dd|ad'oisuehsk
rt',
,: :!
rrr i
r $6 ozrlerru
t 'e
otjrr@tt
ldw{!(h
TestReport
No.: CEl2011l10410ADale: 2011t01t11 P a g e : 8 o f 9
ELSCHUKOMELEKTROSCHUTZKOI/|PONENTENBAU
GMBH
GEWERBESTRASSE
87, D-S8669VEJLSDORF,
GERMANY
iul |ltt][n|l!ll
PBB/PBDEanalyticatFLOWCHART
1) lbfiE of the personwho fiEde nEasurel|Ent RonBn Wong
2) MrE of the personin chargeof nEasurerEnt:TnoyChang
Firsttestingprocess---+
process
.--Optional
screen
process- .>
ConfirrEtion
Screenanalysis
Sanple extractiod
Soxhlet nEthod
V
ConcentlatdDilute
Extracted
solution
Ft|ler
Analysisby GC/MS
I
' !,f
ftsdmumd6*dbylfucwF
1:
:irrri
if,
,-iriif1,.
\
preG) re$d rh 3 r6n @d
- :: rr!!:
i, r'
€Dno1 b'
",
\,'"''d'&d'.";
Ll's6r0r Drr
r r *6@ r@rr
syw{!@o
Test Report
No.: CE/2011/10410ADate| 2011t01t11 P a g e r 9 o f g
ELSCHUKOMELEKTROSCHUTZKOMPONENTENBAU
GIUBH
GEWERBESTRASSE
87, D-98669VEILSDORF,
GERMANY
" Endof Report
Epslslrsdd Ths r€i r@n €nnorb
c d p . r y r r r j l . i , , . " ri i l f l : i + : :i : \ , r l l r i - . . j r 1 . d r , : t , . i : i : I - t . " r n _ i
Th6domeftssdby'bc6mp,ny9qadb8Gmlalcmdionsds
g!b].db'msTdcmdhoBb.E
tl||[l[Il[ttttltl
Test Report
Number : TWNC00183554
Applicant: Littelfuse, Philippines Inc.
LIMA Technology Center, Lipa City,
Malvar, Batangas
Date
: Nov 29, 2010
Sample Description:
One (1) group of submitted samples said to be :
Part Description
: Solder
Part Number
: 692321
Date Sample Received
: Nov 25, 2010
Date Test Started
: Nov 25, 2010
Test Conducted :
As requested by the applicant, for details please refer to attached pages.
Authorized By:
On Behalf Of Intertek Testing Services
Taiwan Limited
K. Y. Liang
Director
This report shall not be reproduced
except in full, without the written
approval of the laboratory.
Page 1 Of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Number : TWNC00183554
Test Conducted
(Ⅰ) Test Result Summary :
Testing Item
Heavy Metal
Cadmium (Cd) content
Lead (Pb) content
Mercury (Hg) content
Chromium VI (Cr6+) content (mg/kg with 50cm2)
Result (ppm)
Silvery Metal
ND
961722
ND
Negative
(< 0.02)(#)
Remarks: ppm = Parts per million based on weight of tested sample = mg/kg
ND = Not detected
<
= Less than
mg/kg with 50cm2 = milligram per kilogram with 50 square centimetre
Negative = A negative test result indicated positive observation
was not found at the time of testing.
#
= Due to the insufficient sample area, reduced total sample
surface of 10 cm2 was used and the dilution factor was
adjusted accordingly.
Responsibility Of Chemist : Irene Chiou / Kevin Liu / Cathy Chen
Date Sample Received
Testing Period
: Nov 25, 2010
: Nov 25, 2010 To Nov 29, 2010
(Ⅱ) RoHS Requirement:
Restricted Substances
Cadmium (Cd) Content
Lead (Pb) Content
Mercury (Hg) Content
Chromium VI (Cr6+) Content
Limits
0.01% (100ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for
homogeneous material.
Page 2 Of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Number : TWNC00183554
Test Conducted
(Ⅲ) Test Method:
Testing Item
Cadmium (Cd)
content
Lead (Pb) content
Mercury (Hg)
content
Chromium VI (Cr6+)
content
Reporting Limit
Testing Method
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
2 ppm
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
2 ppm
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 7, by microwave
digestion until the tested samples are
2 ppm
totally dissolved and determined by
ICP-OES.
With reference to IEC 62321 edition
0.02
1.0:2008 in annex B, by boiling water
extraction and determined by UV-Vis mg/kg with 50cm2
spectrophotometer.
Remark: Reporting limit = Quantitation limit of analyte in sample
Page 3 Of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Number : TWNC00183554
Test Conducted
(Ⅳ) Measurement Flowchart:
Test For Cd/Pb/Hg/Chromium (VI)
Reference Standard:IEC 62321 edition 1.0:2008
Sampling/grinding or cutting
Cd/Pb/Hg
Cr
Polymers /
Electronics
Metal
For different
material, digest
the sample with
*1
appropriate acid
By spot test
Negative
Confirm the tested
samples are
totally dissolved
Make up with
deionized water
6+
*2
Weigh sample
and add
alkaline
solution
Get 50cm2 sample
Definite temp.
extraction
Boiling water
extraction
Cool and filter
the extract
Analyzed by ICP-OES
Make up with deionized
water and add diphenylcarbazide solution
Analyzed by UV-VIS
Remarks:
*1: List Of Appropriate Acid:
Material
Polymers
Metals
Electronics
Acid Added For Digestion
HNO3,HCl,HF,H2O2,H3BO3
HNO3,HCl,HF
HNO3,HCl,H2O2,HBF4
*2: If the result of spot test is positive, Chromium VI would be determined as detected.
End Of Report
Page 4 Of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Number : TWNC00183554
Test Conducted
Photo
Page 5 Of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Test Report
Applicant:
Number : TWNC00177120
Littelfuse, Philippines Inc.
LIMA Technology Center, Lipa City,
Malvar, Batangas
Date
: Oct 11, 2010
Sample Description:
One (1) group of submitted samples said to be :
Part Description
: Cap and Lead assembly
Part Number
: 910-272
Date Sample Received
: Oct 05, 2010
Date Test Started
: Oct 06, 2010
Test Conducted :
As requested by the applicant, for details please refer to attached pages.
Authorized By:
On Behalf Of Intertek Testing Services
Taiwan Limited
K. Y. Liang
Director
This report shall not be reproduced
except in full, without the written
approval of the laboratory.
Page 1 Of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Number : TWNC00177120
Test Conducted
(Ⅰ) Test Result Summary :
Testing Item
Heavy Metal
Cadmium (Cd) content
Lead (Pb) content
Mercury (Hg) content
Chromium VI (Cr6+) content (mg/kg with 50cm2)
Result (ppm)
(A)
(B)
ND
ND
ND
Negative
(< 0.02)
ND
ND
ND
Negative
(< 0.02)
Remarks: ppm = Parts per million based on weight of tested sample = mg/kg
ND = Not detected
<
= Less than
mg/kg with 50cm2 = milligram per kilogram with 50 square centimetre
Negative = A negative test result indicated positive observation
was not found at the time of testing.
Test Component
(1) Coppery Metal
(2) Silvery Plating
Responsibility Of Chemist : Irene Chiou / Kevin Liu
Date Sample Received
Testing Period
: Oct 05, 2010
: Oct 06, 2010 To Oct 08, 2010
(Ⅱ ) RoHS Requirement:
Restricted Substances
Cadmium (Cd) Content
Lead (Pb) Content
Mercury (Hg) Content
Chromium VI (Cr6+) Content
Limits
0.01% (100ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for
homogeneous material.
Page 2 Of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Number : TWNC00177120
Test Conducted
(Ⅲ) Test Method:
Testing Item
Cadmium (Cd)
content
Lead (Pb) content
Mercury (Hg)
content
Chromium VI (Cr6+)
content
Testing Method
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 7, by microwave
digestion until the tested samples are
totally dissolved and determined by
ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in annex B, by boiling water
extraction and determined by UV-Vis
spectrophotometer.
Reporting Limit
2 ppm
2 ppm
2 ppm
0.02
mg/kg with 50cm2
Remark: Reporting limit = Quantitation limit of analyte in sample
Page 3 Of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Number : TWNC00177120
Test Conducted
(Ⅳ) Measurement Flowchart:
Test For Cd/Pb/Hg/Chromium (VI)
Reference Standard:IEC 62321 edition 1.0:2008
End Of Report
Page 4 Of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Number : TWNC00177120
Test Conducted
Photo
Page 5 Of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Test Report
Applicant:
Number : TWNC00182410
Littelfuse, Philippines Inc.
LIMA Technology Center, Lipa City,
Malvar, Batangas
Date
: Nov 22, 2010
Sample Description:
One (1) group of submitted samples said to be :
Part Description
: Epoxy Powder (Green-HF)
Part Number
: 087341
Date Sample Received
: Nov 16, 2010
Date Test Started
: Nov 17, 2010
Test Conducted :
As requested by the applicant, for details please refer to attached pages.
Authorized By:
On Behalf Of Intertek Testing Services
Taiwan Limited
K. Y. Liang
Director
This report shall not be reproduced
except in full, without the written
approval of the laboratory.
Page 1 Of 7
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Number : TWNC00182410
Test Conducted
(Ⅰ) Test Result Summary :
Testing Item
Heavy Metal
Cadmium (Cd) content
Lead (Pb) content
Mercury (Hg) content
Chromium VI (Cr6+) content
Polybrominated Biphenyls (PBBs)
Monobrominated Biphenyls (MonoBB)
Dibrominated Biphenyls (DiBB)
Tribrominated Biphenyls (TriBB)
Tetrabrominated Biphenyls (TetraBB)
Pentabrominated Biphenyls (PentaBB)
Hexabrominated Biphenyls (HexaBB)
Heptabrominated Biphenyls (HeptaBB)
Octabrominated Biphenyls (OctaBB)
Nonabrominated Biphenyls (NonaBB)
Decabrominated Biphenyl (DecaBB)
Polybrominated Diphenyl Ethers (PBDEs)
Monobrominated Diphenyl Ethers (MonoBDE)
Dibrominated Diphenyl Ethers (DiBDE)
Tribrominated Diphenyl Ethers (TriBDE)
Tetrabrominated Diphenyl Ethers (TetraBDE)
Pentabrominated Diphenyl Ethers (PentaBDE)
Hexabrominated Diphenyl Ethers (HexaBDE)
Heptabrominated Diphenyl Ethers (HeptaBDE)
Octabrominated Diphenyl Ethers (OctaBDE)
Nonabrominated Diphenyl Ethers (NonaBDE)
Decabrominated Diphenyl Ether (DecaBDE)
Result (ppm)
Green Powder
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Page 2 Of 7
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Number : TWNC00182410
Test Conducted
(Ⅰ) Test Result Summary :
Testing Item
Result (ppm)
Green Powder
Halogen Content
Fluorine (F)
Chlorine (Cl)
Bromine (Br)
Iodine (I)
ND
652
ND
ND
Remarks: ppm = Parts per million based on weight of tested sample = mg/kg
ND = Not detected
Responsibility Of Chemist : Irene Chiou / Kevin Liu / Cathy Chen
Date Sample Received
Testing Period
: Nov 16, 2010
: Nov 17, 2010 To Nov 19, 2010
(Ⅱ) RoHS Requirement:
Restricted Substances
Cadmium (Cd) Content
Lead (Pb) Content
Mercury (Hg) Content
Chromium VI (Cr6+) Content
Polybrominated Biphenyls (PBBs)
Polybrominated Diphenyl Ehters (PBDEs)
Limits
0.01% (100ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for
homogeneous material.
Page 3 Of 7
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Number : TWNC00182410
Test Conducted
(Ⅲ) Test Method:
Testing Item
Cadmium (Cd)
content
Lead (Pb) content
Mercury (Hg)
content
Chromium VI (Cr6+)
content
Polybrominated
Biphenyls (PBBs)
Polybrominated
Diphenyl Ethers
(PBDEs)
Halogen Content
Testing Method
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 7, by microwave
digestion until the tested samples are
totally dissolved and determined by
ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in annex C, by alkaline
digestion and determined by UV-Vis
spectrophotometer.
With reference to IEC 62321 edition
1.0:2008 in annex A, by solvent
extraction and determined by GC-MSD
and further HPLC confirmation when
necessary.
With reference to IEC 62321 edition
1.0:2008 in annex A, by solvent
extraction and determined by GC-MSD
and further HPLC confirmation when
necessary.
With reference to EN 14582:2007 by
calorimetric bomb with oxygen and
determined by ion chromatography
Reporting Limit
2 ppm
2 ppm
2 ppm
1 ppm
5 ppm
5 ppm
50 ppm
Remark: Reporting limit = Quantitation limit of analyte in sample
Page 4 Of 7
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Number : TWNC00182410
Test Conducted
(Ⅳ) Measurement Flowchart:
Test For Cd/Pb/Hg/Chromium (VI)/PBBS/PBDES Contents
Reference Standard: IEC 62321 edition 1.0:2008
Sampling/grinding or cutting
Cd/Pb/Hg
Cr
Confirm the tested
samples are
totally dissolved
Make up with
deionized water
PBBs/PBDEs
Polymers /
electronics
Metal
For different
material, digest
the sample with
*1
appropriate acid
6+
Weigh sample and
add organic solvent
By spot test
Negative
Get 50cm2 sample
By boiling water
extraction
*2
Weigh sample
and add
alkaline
solution
By Soxhlet
extraction or
Solvent extraction
Definite temp.
extraction
Cool and filter
the extract
Analyzed by ICP-OES
Concentrate the
extract and make up
with organic
solvent
Analyzed by GC-MSD
Make up with deionized
water and add diphenylcarbazide solution
Analyzed by UV-VIS
Remarks:
*1: List Of Appropriate Acid:
Material
Polymers
Metals
Electronics
Acid Added For Digestion
HNO3,HCl,HF,H2O2,H3BO3
HNO3,HCl,HF
HNO3,HCl,H2O2,HBF4
*2: If the result of spot test is positive, Chromium VI would be determined as detected.
Page 5 Of 7
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Number : TWNC00182410
Test Conducted
(Ⅳ) Measurement Flowchart:
Test For Halogen Content
Reference Standard: EN 14582
Sampling/grinding or
cutting
Add absorbent in a
calorimetric bomb &
place weighed sample in
equipment
Fill the calorimetric
bomb with oxygen
Ignite then leave the
flask at room
temperature
Transfer the absorbent
into a volumetric flask
Make up with deionized
water
Analyzed by ion
chromatography
End Of Report
Page 6 Of 7
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Number : TWNC00182410
Test Conducted
Photo
Page 7 Of 7
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401