ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: 250V UMF FA Product #: 464xxx Series Issue Date: October 19, 2011 It is hereby certified by Littelfuse, Inc. that there is neither RoHS (EU Directive 2002/95/EC)-restricted substance nor such use, for materials to be used for unit parts, for packing/packaging materials, and for additives and the like in the manufacturing processes. In addition, it is hereby reported to you that the parts and sub-materials, the materials to be used for unit parts, the packing/packaging materials, and the additives and the like in the manufacturing processes, are all composed of the following components. Issued by: <Global EHS Engineer> (1) Parts, sub-materials and unit parts This document covers the 250V UMF FA RoHS-Compliant series products manufactured by Littelfuse, Inc. < Raw Materials Used Please see Table 1 (2) The ICP data on all measurable substances Please see appropriate pages as identifed in Table 1 Remarks: Pb (lead) contained in the high temperature melting solder > 85% and is categorized as exempt under section 7a of the RoHS Annex. Form 585-047 Rev. A 1 2/21/06 Table 1: List of Raw Materials covered by this report Total Parts 1 2 3 4 5 6 7 Raw Material Part Number 910-261 909-423 497xxx 082xxx 082xxx 692323 425809 Raw Material Description Cap Body Cu Clad Fe5842NiAg by weight Wire 5% by weight Ag Clad Cu Wire 2% by weight Ag Clad Cu Wire Solder Ink 2 Page(s) 3-7 8-13 14-20 21-25 26-30 31-35 36-41 Test Report Applicant: Number : TWNC00183566 Littelfuse, Philippines Inc. LIMA Technology Center, Lipa City, Malvar, Batangas Date : Dec 03, 2010 Sample Description: One (1) group of submitted samples said to be : Part Description : Cap Part Number : 910-261 Date Sample Received : Nov 25, 2010 Date Test Started : Nov 30, 2010 Test Conducted : As requested by the applicant, for details please refer to attached pages. Authorized By: On Behalf Of Intertek Testing Services Taiwan Limited K. Y. Liang Director This report shall not be reproduced except in full, without the written approval of the laboratory. Page 1 Of 5 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401 Number : TWNC00183566 Test Conducted (Ⅰ) Test Result Summary : Testing Item Heavy Metal Cadmium (Cd) content Lead (Pb) content Mercury (Hg) content Chromium VI (Cr6+) content (mg/kg with 50cm2) Result (ppm) (1) (2) ND ND ND Negative (< 0.02) ND ND ND Negative (< 0.02) Remarks: ppm = Parts per million based on weight of tested sample = mg/kg ND = Not detected < = Less than mg/kg with 50cm2 = milligram per kilogram with 50 square centimetre Negative = A negative test result indicated positive observation was not found at the time of testing. Tested Components (1) Coppery Substrate (2) Silvery Plating Responsibility Of Chemist : Irene Chiou / Kevin Liu / Cathy Chen Date Sample Received Testing Period : Nov 25, 2010 : Nov 30, 2010 To Dec 03, 2010 (Ⅱ) RoHS Requirement: Restricted Substances Cadmium (Cd) Content Lead (Pb) Content Mercury (Hg) Content Chromium VI (Cr6+) Content Limits 0.01% (100ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for homogeneous material. Page 2 Of 5 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401 Number : TWNC00183566 Test Conducted (Ⅲ) Test Method: Testing Item Cadmium (Cd) content Lead (Pb) content Mercury (Hg) content Chromium VI (Cr6+) content Testing Method With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in clause 7, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in annex B, by boiling water extraction and determined by UV-Vis spectrophotometer. Reporting Limit 2 ppm 2 ppm 2 ppm 0.02 mg/kg with 50cm2 Remark: Reporting limit = Quantitation limit of analyte in sample Page 3 Of 5 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401 Number : TWNC00183566 Test Conducted (Ⅳ) Measurement Flowchart: Test For Cd/Pb/Hg/Chromium (VI) Reference Standard:IEC 62321 edition 1.0:2008 Sample preparation Take sample and immerse into Aqua Regia, start to strip plating layer Stop the stripping procedure upon color change completely Take the Aqua solution as plating component and stripped body as substrate component Cd/Pb/Hg Cr Polymers / electronics Metal For different material, digest the sample with *1 appropriate acid By spot test Negative Confirm the tested samples are totally dissolved Make up with deionized water Analyzed by ICP-OES Remarks: *1: List Of Appropriate Acid: Material Polymers Metals Electronics 6+ *2 Weigh sample and add alkaline solution Get 50cm2 sample Definite temp. extraction By boiling water extraction Cool and filter the extract Make up with deionized water and add diphenyl-carbazide solution Analyzed by UV-VIS Acid Added For Digestion HNO3,HCl,HF,H2O2,H3BO3 HNO3,HCl,HF HNO3,HCl,H2O2,HBF4 *2: If the result of spot test is positive, Chromium VI would be determined as detected. End Of Report Page 4 Of 5 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401 Number : TWNC00183566 Test Conducted Photo Page 5 Of 5 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401 Test Report Applicant: Number : TWNC00183567 Littelfuse, Philippines Inc. LIMA Technology Center, Lipa City, Malvar, Batangas Date : Nov 30, 2010 Sample Description: One (1) group of submitted samples said to be : Part Description : Body Part Number : 909-423 Date Sample Received : Nov 25, 2010 Date Test Started : Nov 25, 2010 Test Conducted : As requested by the applicant, for details please refer to attached pages. Authorized By: On Behalf Of Intertek Testing Services Taiwan Limited K. Y. Liang Director This report shall not be reproduced except in full, without the written approval of the laboratory. Page 1 Of 6 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401 Number : TWNC00183567 Test Conducted (Ⅰ) Test Result Summary : Testing Item Result (ppm) Cream Material Heavy Metal Cadmium (Cd) content Lead (Pb) content Mercury (Hg) content Chromium VI (Cr6+) content Polybrominated Biphenyls (PBBs) Monobrominated Biphenyls (MonoBB) Dibrominated Biphenyls (DiBB) Tribrominated Biphenyls (TriBB) Tetrabrominated Biphenyls (TetraBB) Pentabrominated Biphenyls (PentaBB) Hexabrominated Biphenyls (HexaBB) Heptabrominated Biphenyls (HeptaBB) Octabrominated Biphenyls (OctaBB) Nonabrominated Biphenyls (NonaBB) Decabrominated Biphenyl (DecaBB) Polybrominated Diphenyl Ethers (PBDEs) Monobrominated Diphenyl Ethers (MonoBDE) Dibrominated Diphenyl Ethers (DiBDE) Tribrominated Diphenyl Ethers (TriBDE) Tetrabrominated Diphenyl Ethers (TetraBDE) Pentabrominated Diphenyl Ethers (PentaBDE) Hexabrominated Diphenyl Ethers (HexaBDE) Heptabrominated Diphenyl Ethers (HeptaBDE) Octabrominated Diphenyl Ethers (OctaBDE) Nonabrominated Diphenyl Ethers (NonaBDE) Decabrominated Diphenyl Ether (DecaBDE) Halogen Content Fluorine (F) Chlorine (Cl) Bromine (Br) Iodine (I) ND 34 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND Remarks: ppm = Parts per million based on weight of tested sample = mg/kg ND = Not detected Responsibility Of Chemist : Irene Chiou / Kevin Liu / Cathy Chen Date Sample Received Testing Period : Nov 25, 2010 : Nov 25, 2010 To Nov 30, 2010 Page 2 Of 6 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401 Test Conducted (Ⅱ) RoHS Requirement: Restricted Substances Cadmium (Cd) Content Lead (Pb) Content Mercury (Hg) Content Chromium VI (Cr6+) Content Polybrominated Biphenyls (PBBs) Polybrominated Diphenyl Ehters (PBDEs) Number : TWNC00183567 Limits 0.01% (100ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for homogeneous material. (Ⅲ) Test Method: Testing Item Cadmium (Cd) content Lead (Pb) content Mercury (Hg) content Chromium VI (Cr6+) content Polybrominated Biphenyls (PBBs) Polybrominated Diphenyl Ethers (PBDEs) Halogen Content Testing Method With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in clause 7, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in annex C, by alkaline digestion and determined by UV-Vis spectrophotometer. With reference to IEC 62321 edition 1.0:2008 in annex A, by solvent extraction and determined by GC-MSD and further HPLC confirmation when necessary. With reference to IEC 62321 edition 1.0:2008 in annex A, by solvent extraction and determined by GC-MSD and further HPLC confirmation when necessary. With reference to EN 14582:2007 by calorimetric bomb with oxygen and determined by ion chromatography Reporting Limit 2 ppm 2 ppm 2 ppm 1 ppm 5 ppm 5 ppm 50 ppm Remark: Reporting limit = Quantitation limit of analyte in sample Page 3 Of 6 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401 Number : TWNC00183567 Test Conducted (Ⅳ) Measurement Flowchart: Test For Cd/Pb/Hg/Chromium (VI)/PBBS/PBDES Contents Reference Standard: IEC 62321 edition 1.0:2008 Sample preparation For non-metal part For metal part Take sample and immerse into Aqua Regia, start to strip plating layer Stop the stripping procedure upon color change completely Take the Aqua solution as plating component and stripped body as substrate component Cd/Pb/Hg Cr Confirm the tested samples are totally dissolved Make up with deionized water PBBs/PBDEs Polymers / electronics Metal For different material, digest the sample with *1 appropriate acid 6+ Weigh sample and add organic solvent By spot test Negative Get 50cm2 sample By boiling water extraction *2 Weigh sample and add alkaline solution By Soxhlet extraction or Solvent extraction Definite temp. extraction Cool and filter the extract Analyzed by ICP-OES Concentrate the extract and make up with organic solvent Analyzed by GC-MSD Make up with deionized water and add diphenylcarbazide solution Analyzed by UV-VIS Remarks: *1: List Of Appropriate Acid: Material Polymers Metals Electronics Acid Added For Digestion HNO3,HCl,HF,H2O2,H3BO3 HNO3,HCl,HF HNO3,HCl,H2O2,HBF4 *2: If the result of spot test is positive, Chromium VI would be determined as detected. Page 4 Of 6 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401 Number : TWNC00183567 Test Conducted (Ⅳ) Measurement Flowchart: Test For Halogen Content Reference Standard:EN 14582 Sampling/grinding or cutting Add absorbent in a calorimetric bomb & place weighed sample in equipment Fill oxygen into calorimetric bomb Ignite then leave the flask at room temperature Transfer the absorbent into a volumetric flask Make up with deionized water Analyzed by ion chromatography End Of Report Page 5 Of 6 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401 Number : TWNC00183567 Test Conducted Photo Page 6 Of 6 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401 Validi For Q Please Test Report sGs No. : CE2010/C0094 Dale | 2O1Oh2tO8 page : 1of 7 POLYFIL AG OBERALLMENDSTRASSE 2OA,CH€3OO ZUG/ SWITZERLAND Th6followingsample(s)wa3/weresubmitted and identified by/on behalfoftha client as: SampleDescription Buyer/Order No. SampleReceiving Date TeslingPeriod Ni42Fe58MCuirAg5% 94462 2010t1?,01 20t0t1zo110 2010t1208 Te6t Rosult(s) Pleasereferto nextpage(s). (NWO ilha1d6Ftde.onyblbgnplels)l6sdThs|69@d€ndb€ c d € r y r r r , l l , l r J l .r r . l l t + i 4 r r r l i l * ft8 d@nd for.sdmr own 6 gEd hy b6 c.mp. fomar donds slq rk'ons i i. t]li, l&rl\ .:' -' l' 1.1rJts!!. i any ft6cmP4tsso6r. fttrngB.ind[946!un&rlh16 1 r .+ r { r r { i * : r t r r s { o z r r r e e |llt [lrr]||rltttt TestReport No. CE2010/C0094 Date| 2010/'12y08Page: 2 ot 7 POLYFIL AG OBERALLMENDSTRASSE 2OA,CH€3OO ZUG/ SWITZERLAND |r [tll||lI|tl|t Test Resultlsl PARTNAIVENo,1 SILVERCOLORED i'ETALWIRE Test ltem (8): Unit Cadmium(Cd) Method Result MDL mg/Kg Withreference to IEC62321:2008and 2 No.1 n.d. 5o n.d. 50 n.d. 50 n.d. 50 n.d. pedormedby ICP-AES. mgls Withreferenc€ to IEC62321:2008€nd 2 n.d. pertomedby lCPdES. Mercury(Hg) mdkg With referencelo IEC62321:2008and 2 n,d, perfomedby ICP-AES. Hexavalent ChrcmiumCr(Vl)by Withreference to IEC62321:2008and 0.02m9/kg Negative Spottest / boiling\,r€terextraction perfomedby Spottest/ boilingwEter with50cm, extradtionlrethod.(SeeNote6) sudace Lead (Pb) Halogen Halogen-Fluorine (F) (CASNo.:014762-94-8) Halogen-Chlorine (Cl) (CASNo.:022537-15-1) Halogen-Bromine (Br) (CASNo.:010097-32-2) (l) Halogen-lodine (CASNo.:01436244-8) With referenceto BS EN 14582t2007 . mg/Kg Analysiswasperformedby lC- Sum of PBB6 n.d- Monobromobiphenyl Dibromobiphenyl Tribromobiphenyl Tetrabromobipheny Pentabromobiphenyl mgikg Hexabromobiph€nyl Heptabromobiphenyl Ociabromobiphenyl Nonabromobiphenyl Decabromobiphenyl cm€ry r.r r|,;i:r} , ..rti'Ji: + i4!rj.,ijlt " ei. n6tud l d 6 Wth reference to IEC62321t2008and perfomedby GC/MS. 5 5 5 5 n.dn.d. n.d. n.d. 5 5 n.d, 5 5 5 5 n.o. n.o. n.d. n.d. n.d. p3G)rssdrh3rd.@n€ndb i:+::r 'J. i r'r"llt}rl. rn'1,1.J{7:1l 3 sdbyh6m@nyshdroisc*'dcmdibBd 6 d M E l o m a l d . @ n h . d ontandwrhrh€rmborcrds,.ddons'lary.ft8csrt3sobEspBbrt 3 o l b h e ] i m i b l d d ' a b L t y srobcltrrandrhsdEs u hdsrkr 2orcrapo cooirrriiwio/f ttti f lr: :r,rrit:il lt r is6orpDerD,re0rr2arrT ww+.on TestReport paqe:3of7 No.: CE/2010/C0094Date:2O1O/12!OB POLYFILAG OBERALLMENDSTMSSE2OA,CHS3OOZUG / SWITZERLAND Te3t ltem (s): unit Method rr] ttrr[it|lt MDL Sumof PBDES Monobromodiphenyl eth€r Oibromodiphenyl ether No.1 n.d. n.d. n.d. fnbomodiphenyl eth€r Tetrabromodiphenyl ether Pentabromodiphenyl ether Hexabromodiphenyl ether Heptabrornodiphenyl ethe. Oclabromodiphenyl ether Nonabromodiphenyl ether Decabomodiphenyl ether Result n.o, mgxg Withreference to IEC62321:2008and perfomedby GC/MS. 5 5 5 5 n.ct. n.d. n.d. n.d. n.d. 5 n.o, n.o. Note: 1. mg/kg= ppm; 0.1M%= 100oppm 2- n.d. = Not Detected 3. MDL= MethodDeteclionLimit 4."-"=NotRegulated 5. " = Qualitative (NoUnit) analysis 6. SDot-te.st: N€gative= Absenceof Cr(Vl)coating/ surfacelayer;positive= presencoof Cr(Vt)coating/ surtacetayer; (Thetestedsampleshouldbe furthervedfiedby boiling-water-extraction methodif the spottest resuttcannot beconfimed.) Boiling-wEter-exlraclion: Negative= Absenc€of Cr(Vl)coating/ surtacelayer; Positive= Pres€nceof Cr(Vl)coating/ surtacelayer; Th6 detec{edconcentrationin boiling-water-ext.action solutionis equalor greaterthan0.02mg/kgwith SOcm. samDlesurfacearea. npsGlrsdd th316r@nendb cmponyrill4l.;i.!.illi'r.lrF,fl::tr)li"ei.nU'i.1:]S:11;:=:i:.J.1.11JF1". th6ddh€fr 3 sd by tu c.mp3iy srqd b tu GmmrcmdtuB d ss r@€.d6rc romar [email protected] 3!q sFBb|ly9locc'.d.ndlh!d6u h r n ' h s a d d ! € d b s u e h c n n d b a 4 d f d € ! € , l i f u l w i d h. imeloi or €b ry Test Report No-: CE/201UC0094Date:2OiOt12tOepaoe,4of7 POLYFILAG OBEMLLMENDSTMSSE 2OA,CH€3OOZUG / SWITZERLAND rtlt tIll|||||lllttt '1) Thesesarples w€Ie dissotr€dtoblfy by pre-conditioning rEthod accordingto belowflow chart ( Cf' test nethod e)cluded) 2) flanE of the personwho mademeasurefiEnl:Climbgreatyang 3) tlarE ofthe pe6on in charg€of r€asurenEnt TroyChang Cutting / Preparation Aciddigestion by suitable 6cid dependedon difierentsarble nEterial(asbelowtable) Microwavedigestionwith Addappropdate anbuntof digeslion reagent HNo3/rcUHF Healto appropdate tefiperatureto extEct Cool.filterdigeotae through fiher AlkaliFusion F|cIto dissolve Add diphedyl-carb€zidefor colordeveloprnent Safiple Material cNFry DigestbnAcid S'teel, copper,aluninun\solder Aqua regia,HNO3,HCl,HF,HrO, Gl€ss palladium, Gold,platinum, ceraric HNO3/HF Aquaregia Sitver HNO3 Plastic l-lrsOi, HrOr,HNO3,HCI Oh€rs Anyacidto trctaldigestion lilltt;!r; id adM'cromd nrturerGe.drorso^ryb6.smpo13)@rod Ihs'61,6p.nenddb' ,lr'!lt !;.::l!ll.l!!L.\;:+tr] .Lili:!'Ii!lJi J rrl rttrrll. ^y elttod b iE ce66rcond r onsot s @n* 3uq me€suaethe ab6orbance at 540 nmby UV-VIS he 'n,@id d iab t onryaidwih'nkhisdCr€db ndtudds iany tuCmparyss&6Fnsbriy srohC,6niadhsdmum Ihelf0hbandob]Ed6munddl|l.vs.*1.6prclud6tc€p1nfu||*ihfulffd LU:],: *-r,\:l rrl r 1s6orrrsrru r 1s610rr2arr wws<on TestReport No.: CE/2010/C0094Oale| 201U12t08 paae:Sof7 POLYFIL AG OBEMLLMENDSTRASSE 2OA, CH€3OO ZUG/ SWITZERLAND |lll/[atl|l|lt|llrr Analytical flow chart of halogen content 1) NanEoftheperson whorEdefiEasurery€nt: RitaChen 2) Naneof thepersoninchargeof neasu.eBentt TroyChang Samplepretreatment / Separation Weighlingand puttingsanple in cell Oryg€nBombCo.rbustion / Absorption Dilution lo fixedvolurE Analysis wasperfomEdby lC 6G) Gnd ft6 r€' '@n 1.r'llll!. cdhF.y;1.r1f;nr..ll{r:,+rF:1i:-1:irl*ir;..J11i l.}!}1,-r:."r,r ny s6jed b G Gse6rcod ' o^s d s tu ekmic bmd @msnb suq €nnd b , ndb..qdudgcaplnfunwibd ! idsntrzongrdF.oloe.rdwdil ::hi Fr' frr lir:,,i4 r rMrorrs TestReport No.: CE/2010/C0094Datet2O1U1Z08 Page: 6of 7 POLYFILAG OBERALLMENDSTRASSE 2OA,CH63OOZUG/ SWITZERLAND tr]flttt!]||I|tIt] PBB/PBDE analyticalFLOWCHART 1) l.lanEof the personwho rEde dFasurefi€nt:RolIEnWong 2) t{afiE of the personin chargeof ryEasuaed€nt: T.oy Chang Firsttestingprocess-----' Optional screenprocess.--CodfinrEtionprocess - .> Screenamlysis V Sanpleextraction/ SoxhletfiEthod v ConcenlratdDilute E lrac€d solution Filter Analysisby GC/MS cdp.nyiJ,:r,i! l;ii ! rlftll::..ir;i rh3fuum*ttsE3uadb!lheconF rbr.otsadd€doi3u^6,bor. ;!n-1n /.!|.rJ, pr4t ladd Dc r6d rstsd cainor 6 rri,t.' r:1,]t!11i. ndbe.4ducdqcBpl nrlr iod Test Report No.: CE/2010C0094 Da'.e'.2O1042OAP a g e : 7 o f 7 POLYFILAG OBERALLMENDSTRASSE 2OA,CH€3OO ZUG/ SWITZERLANO I [tl |l|lt[t c0094 - Endof Repon" c @ p a i yi r t , l r i t iri r.rl,,tif;i';rl Th36umdts6suedbylhecdmp, : n . { : : l ' r l . P . . : - t\ ! r i /:,.:1iihf. cisdsbecmtsiysrnd'Bsa66|[email protected] .:I^ ri t:rkf,! | (,@rorze* r r s6orrDrr ww$!rm Test Report Applicant: Number : TWNC00194902 Littelfuse, Philippines Inc. LIMA Technology Center, Lipa City, Malvar, Batangas Date : Mar 17, 2011 Sample Description: One (1) group of submitted samples said to be : Part Description : Silver Clad Cu wire with 5 mass % Ag Part Number : 082375 Date Sample Received : Mar 14, 2011 Date Test Started : Mar 15, 2011 Test Conducted : As requested by the applicant, for details please refer to attached pages. Authorized By: On Behalf Of Intertek Testing Services Taiwan Limited K. Y. Liang Director This report shall not be reproduced except in full, without the written approval of the laboratory. Page 1 Of 5 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401 Number : TWNC00194902 Test Conducted (Ⅰ) Test Result Summary : Test Item Heavy Metal Cadmium (Cd) content Lead (Pb) content Mercury (Hg) content Chromium VI (Cr6+) content (mg/kg with 50cm2) Result (ppm) Silvery Metal ND ND ND Negative (< 0.02) Remarks: ppm = Parts per million based on weight of tested sample = mg/kg ND = Not detected < = Less than mg/kg with 50cm2 = milligram per kilogram with 50 square centimetre Negative = A negative test result indicated positive observation was not found at the time of Test. Responsibility Of Chemist : Irene Chiou / Kevin Liu / Cathy Chen Date Sample Received Test Period : Mar 14, 2011 : Mar 15, 2011 To Mar 17, 2011 (Ⅱ) RoHS Requirement: Restricted Substances Cadmium (Cd) Content Lead (Pb) Content Mercury (Hg) Content Chromium VI (Cr6+) Content Limits 0.01% (100ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for homogeneous material. Page 2 Of 5 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401 Number : TWNC00194902 Test Conducted (Ⅲ) Test Method: Test Item Cadmium (Cd) content Lead (Pb) content Mercury (Hg) content Chromium VI (Cr6+) content Test Method With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in clause 7, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in annex B, by boiling water extraction and determined by UV-Vis spectrophotometer. Reporting Limit 2 ppm 2 ppm 2 ppm 0.02 mg/kg with 50cm2 Remark: Reporting limit = Quantitation limit of analyte in sample Page 3 Of 5 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401 Number : TWNC00194902 Test Conducted (Ⅳ) Measurement Flowchart: Test For Cd/Pb/Hg/Chromium (VI) Reference Standard:IEC 62321 edition 1.0:2008 Sampling/grinding or cutting Cd/Pb/Hg Cr Polymers / Electronics Metal For different material, digest the sample with *1 appropriate acid By spot test Negative Confirm the tested samples are totally dissolved Make up with deionized water 6+ *2 Weigh sample and add alkaline solution Get 50cm2 sample Definite temp. extraction Boiling water extraction Cool and filter the extract Analyzed by ICP-OES Make up with deionized water and add diphenylcarbazide solution Analyzed by UV-VIS Remarks: *1: List Of Appropriate Acid: Material Polymers Metals Electronics Acid Added For Digestion HNO3,HCl,HF,H2O2,H3BO3 HNO3,HCl,HF HNO3,HCl,H2O2,HBF4 *2: If the result of spot test is positive, Chromium VI would be determined as detected. End Of Report Page 4 Of 5 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401 Number : TWNC00194902 Test Conducted Photo Page 5 Of 5 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401 Test Report Applicant: Number : TWNC00194906 Littelfuse, Philippines Inc. LIMA Technology Center, Lipa City, Malvar, Batangas Date : Mar 17, 2011 Sample Description: One (1) group of submitted samples said to be : Part Description : Silver Clad Cu wire with 2 mass % Ag Part Number : 082684 Date Sample Received : Mar 14, 2011 Date Test Started : Mar 15, 2011 Test Conducted : As requested by the applicant, for details please refer to attached pages. Authorized By: On Behalf Of Intertek Testing Services Taiwan Limited K. Y. Liang Director This report shall not be reproduced except in full, without the written approval of the laboratory. Page 1 Of 5 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401 Number : TWNC00194906 Test Conducted (Ⅰ) Test Result Summary : Test Item Heavy Metal Cadmium (Cd) content Lead (Pb) content Mercury (Hg) content Chromium VI (Cr6+) content (mg/kg with 50cm2) Result (ppm) Silvery Metal ND ND ND Negative (< 0.02) Remarks: ppm = Parts per million based on weight of tested sample = mg/kg ND = Not detected < = Less than mg/kg with 50cm2 = milligram per kilogram with 50 square centimetre Negative = A negative test result indicated positive observation was not found at the time of Test. Responsibility Of Chemist : Irene Chiou / Kevin Liu / Cathy Chen Date Sample Received Test Period : Mar 14, 2011 : Mar 15, 2011 To Mar 17, 2011 (Ⅱ) RoHS Requirement: Restricted Substances Cadmium (Cd) Content Lead (Pb) Content Mercury (Hg) Content Chromium VI (Cr6+) Content Limits 0.01% (100ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for homogeneous material. Page 2 Of 5 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401 Number : TWNC00194906 Test Conducted (Ⅲ) Test Method: Test Item Cadmium (Cd) content Lead (Pb) content Mercury (Hg) content Chromium VI (Cr6+) content Test Method With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in clause 7, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in annex B, by boiling water extraction and determined by UV-Vis spectrophotometer. Reporting Limit 2 ppm 2 ppm 2 ppm 0.02 mg/kg with 50cm2 Remark: Reporting limit = Quantitation limit of analyte in sample Page 3 Of 5 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401 Number : TWNC00194906 Test Conducted (Ⅳ) Measurement Flowchart: Test For Cd/Pb/Hg/Chromium (VI) Reference Standard:IEC 62321 edition 1.0:2008 Sampling/grinding or cutting Cd/Pb/Hg Cr Polymers / Electronics Metal For different material, digest the sample with *1 appropriate acid By spot test Negative Confirm the tested samples are totally dissolved Make up with deionized water 6+ *2 Weigh sample and add alkaline solution Get 50cm2 sample Definite temp. extraction Boiling water extraction Cool and filter the extract Analyzed by ICP-OES Make up with deionized water and add diphenylcarbazide solution Remarks: *1: List Of Appropriate Acid: Material Polymers Metals Electronics Analyzed by UV-VIS Acid Added For Digestion HNO3,HCl,HF,H2O2,H3BO3 HNO3,HCl,HF HNO3,HCl,H2O2,HBF4 *2: If the result of spot test is positive, Chromium VI would be determined as detected. End Of Report Page 4 Of 5 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401 Number : TWNC00194906 Test Conducted Photo Page 5 Of 5 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401 Test Report Applicant: Number : TWNC00183558 Littelfuse, Philippines Inc. LIMA Technology Center, Lipa City, Malvar, Batangas Date : Dec 02, 2010 Sample Description: One (1) group of submitted samples said to be : Part Description : Solder Part Number : 692323 Date Sample Received : Nov 25, 2010 Date Test Started : Nov 29, 2010 Test Conducted : As requested by the applicant, for details please refer to attached pages. Authorized By: On Behalf Of Intertek Testing Services Taiwan Limited K. Y. Liang Director This report shall not be reproduced except in full, without the written approval of the laboratory. Page 1 Of 5 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401 Number : TWNC00183558 Test Conducted (Ⅰ) Test Result Summary : Result (ppm) Silvery Metal Testing Item Heavy Metal Cadmium (Cd) content Lead (Pb) content Mercury (Hg) content Chromium VI (Cr6+) content (mg/kg with 50cm2) ND 935574 ND Negative (< 0.02)(#) Remarks: ppm = Parts per million based on weight of tested sample = mg/kg ND = Not detected < = Less than mg/kg with 50cm2 = milligram per kilogram with 50 square centimetre Negative = A negative test result indicated positive observation was not found at the time of testing. # = Due to the insufficient sample area, reduced total sample surface of 10 cm2 was used and the dilution factor was adjusted accordingly. Responsibility Of Chemist : Irene Chiou / Kevin Liu / Cathy Chen Date Sample Received Testing Period : Nov 25, 2010 : Nov 29, 2010 To Dec 01, 2010 (Ⅱ) RoHS Requirement: Restricted Substances Cadmium (Cd) Content Lead (Pb) Content Mercury (Hg) Content Chromium VI (Cr6+) Content Limits 0.01% (100ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for homogeneous material. Page 2 Of 5 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401 Number : TWNC00183558 Test Conducted (Ⅲ) Test Method: Testing Item Cadmium (Cd) content Lead (Pb) content Mercury (Hg) content Chromium VI (Cr6+) content Testing Method With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in clause 7, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in annex B, by boiling water extraction and determined by UV-Vis spectrophotometer. Reporting Limit 2 ppm 2 ppm 2 ppm 0.02 mg/kg with 50cm2 Remark: Reporting limit = Quantitation limit of analyte in sample Page 3 Of 5 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401 Number : TWNC00183558 Test Conducted (Ⅳ) Measurement Flowchart: Test For Cd/Pb/Hg/Chromium (VI) Reference Standard:IEC 62321 edition 1.0:2008 Sampling/grinding or cutting Cd/Pb/Hg Cr Polymers / Electronics Metal For different material, digest the sample with *1 appropriate acid By spot test Negative Confirm the tested samples are totally dissolved Make up with deionized water 6+ *2 Weigh sample and add alkaline solution Get 50cm2 sample Definite temp. extraction Boiling water extraction Cool and filter the extract Analyzed by ICP-OES Make up with deionized water and add diphenylcarbazide solution Remarks: *1: List Of Appropriate Acid: Material Polymers Metals Electronics Analyzed by UV-VIS Acid Added For Digestion HNO3,HCl,HF,H2O2,H3BO3 HNO3,HCl,HF HNO3,HCl,H2O2,HBF4 *2: If the result of spot test is positive, Chromium VI would be determined as detected. End Of Report Page 4 Of 5 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401 Number : TWNC00183558 Test Conducted Photo Page 5 Of 5 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401 Test Report Applicant: Number : TWNC00183571 Littelfuse, Philippines Inc. Date LIMA Technology Center, Lipa City, Malvar, Batangas : Nov 30, 2010 Sample Description: One (1) group of submitted samples said to be : Part Description : Ink Part Number : 425809 Date Sample Received : Nov 25, 2010 Date Test Started : Nov 25, 2010 Test Conducted : As requested by the applicant, for details please refer to attached pages. Authorized By: On Behalf Of Intertek Testing Services Taiwan Limited K. Y. Liang Director This report shall not be reproduced except in full, without the written approval of the laboratory. Page 1 Of 6 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401 Number : TWNC00183571 Test Conducted (Ⅰ) Test Result Summary : Testing Item Result (ppm) Black Paste Heavy Metal Cadmium (Cd) content Lead (Pb) content Mercury (Hg) content Chromium VI (Cr6+) content Polybrominated Biphenyls (PBBs) Monobrominated Biphenyls (MonoBB) Dibrominated Biphenyls (DiBB) Tribrominated Biphenyls (TriBB) Tetrabrominated Biphenyls (TetraBB) Pentabrominated Biphenyls (PentaBB) Hexabrominated Biphenyls (HexaBB) Heptabrominated Biphenyls (HeptaBB) Octabrominated Biphenyls (OctaBB) Nonabrominated Biphenyls (NonaBB) Decabrominated Biphenyl (DecaBB) Polybrominated Diphenyl Ethers (PBDEs) Monobrominated Diphenyl Ethers (MonoBDE) Dibrominated Diphenyl Ethers (DiBDE) Tribrominated Diphenyl Ethers (TriBDE) Tetrabrominated Diphenyl Ethers (TetraBDE) Pentabrominated Diphenyl Ethers (PentaBDE) Hexabrominated Diphenyl Ethers (HexaBDE) Heptabrominated Diphenyl Ethers (HeptaBDE) Octabrominated Diphenyl Ethers (OctaBDE) Nonabrominated Diphenyl Ethers (NonaBDE) Decabrominated Diphenyl Ether (DecaBDE) Halogen Content Fluorine (F) Chlorine (Cl) Bromine (Br) Iodine (I) ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 336 ND ND Remarks: ppm = Parts per million based on weight of tested sample = mg/kg ND = Not detected Responsibility Of Chemist : Irene Chiou / Kevin Liu / Cathy Chen Date Sample Received Testing Period : Nov 25, 2010 : Nov 25, 2010 To Nov 29, 2010 Page 2 Of 6 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401 Test Conducted (Ⅱ) RoHS Requirement: Restricted Substances Cadmium (Cd) Content Lead (Pb) Content Mercury (Hg) Content Chromium VI (Cr6+) Content Polybrominated Biphenyls (PBBs) Polybrominated Diphenyl Ehters (PBDEs) Number : TWNC00183571 Limits 0.01% (100ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for homogeneous material. (Ⅲ) Test Method: Testing Item Cadmium (Cd) content Lead (Pb) content Mercury (Hg) content Chromium VI (Cr6+) content Polybrominated Biphenyls (PBBs) Polybrominated Diphenyl Ethers (PBDEs) Halogen Content Testing Method With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in clause 7, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in annex C, by alkaline digestion and determined by UV-Vis spectrophotometer. With reference to IEC 62321 edition 1.0:2008 in annex A, by solvent extraction and determined by GC-MSD and further HPLC confirmation when necessary. With reference to IEC 62321 edition 1.0:2008 in annex A, by solvent extraction and determined by GC-MSD and further HPLC confirmation when necessary. With reference to EN 14582:2007 by calorimetric bomb with oxygen and determined by ion chromatography Reporting Limit 2 ppm 2 ppm 2 ppm 1 ppm 5 ppm 5 ppm 50 ppm Remark: Reporting limit = Quantitation limit of analyte in sample Page 3 Of 6 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401 Number : TWNC00183571 Test Conducted (Ⅳ) Measurement Flowchart: Test For Cd/Pb/Hg/Chromium (VI)/PBBS/PBDES Contents Reference Standard: IEC 62321 edition 1.0:2008 Sample preparation For non-metal part For metal part Take sample and immerse into Aqua Regia, start to strip plating layer Stop the stripping procedure upon color change completely Take the Aqua solution as plating component and stripped body as substrate component Cd/Pb/Hg Cr Confirm the tested samples are totally dissolved Make up with deionized water PBBs/PBDEs Polymers / electronics Metal For different material, digest the sample with *1 appropriate acid 6+ Weigh sample and add organic solvent By spot test Negative Get 50cm2 sample By boiling water extraction *2 Weigh sample and add alkaline solution By Soxhlet extraction or Solvent extraction Definite temp. extraction Cool and filter the extract Analyzed by ICP-OES Concentrate the extract and make up with organic solvent Analyzed by GC-MSD Make up with deionized water and add diphenylcarbazide solution Analyzed by UV-VIS Remarks: *1: List Of Appropriate Acid: Material Polymers Metals Electronics Acid Added For Digestion HNO3,HCl,HF,H2O2,H3BO3 HNO3,HCl,HF HNO3,HCl,H2O2,HBF4 *2: If the result of spot test is positive, Chromium VI would be determined as detected. Page 4 Of 6 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401 Number : TWNC00183571 Test Conducted (Ⅳ) Measurement Flowchart: Test For Halogen Content Reference Standard:EN 14582 Sampling/grinding or cutting Add absorbent in a calorimetric bomb & place weighed sample in equipment Fill oxygen into calorimetric bomb Ignite then leave the flask at room temperature Transfer the absorbent into a volumetric flask Make up with deionized water Analyzed by ion chromatography End Of Report Page 5 Of 6 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401 Number : TWNC00183571 Test Conducted Photo Page 6 Of 6 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401