ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: 1206 Sub-Assembly Fuse - Low rating Product #: 440xxx Series (0.25A – 1.5A) Issue Date: July 13, 2011 It is hereby certified by Littelfuse, Inc. that there is neither RoHS (EU Directive 2002/95/EC)-restricted substance nor such use, for materials to be used for unit parts, for packing/packaging materials, and for additives and the like in the manufacturing processes. In addition, it is hereby reported to you that the parts and sub-materials, the materials to be used for unit parts, the packing/packaging materials, and the additives and the like in the manufacturing processes, are all composed of the following components. Issued by: <Global EHS Engineer> (1) Parts, sub-materials and unit parts This document covers the 1206 Sub-Assembly Fuse RoHS-Compliant series products manufactured by Littelfuse, Inc. < Raw Materials Used Please see Table 1 (2) The ICP data on all measurable substances Please see appropriate pages as identifed in Table 1 Remarks: Form 585-047 Rev. A 1 2/21/06 Table 1: List of Raw Materials covered by this report Total Parts 1 Raw Material Part Number 039643 011004 2 3 4 011001 011003 5 6 7 011005 010118 010119 Raw Material Description Ceramic Subsrate Page(s) 3-8 Underglaze Paste -Dielectric Paste Ag End Termination Paste Cover Glass-Overglaze Paste Conductor Paste – Sintered Resinate Paste Nickel Anode Tin Anode 9-15 16-22 23-28 2 29-34 35-39 40-44 Test Report Applicant: Number : TWNC00186567 Littelfuse, Philippines Inc. LIMA Technology Center, Lipa City, Malvar, Batangas Date : Dec 29, 2010 Sample Description: One (1) group of submitted samples said to be : Part Description : Ceramic Substrate Part Number : 039643 Date Sample Received : Dec 24, 2010 Date Test Started : Dec 24, 2010 Test Conducted : As requested by the applicant, for details please refer to attached pages. Authorized By: On Behalf Of Intertek Testing Services Taiwan Limited K. Y. Liang Director This report shall not be reproduced except in full, without the written approval of the laboratory. Page 1 Of 6 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401 Number : TWNC00186567 Test Conducted (Ⅰ) Test Result Summary : Testing Item Result (ppm) White Material Heavy Metal Cadmium (Cd) content Lead (Pb) content Mercury (Hg) content Chromium VI (Cr6+) content Polybrominated Biphenyls (PBBs) Monobrominated Biphenyls (MonoBB) Dibrominated Biphenyls (DiBB) Tribrominated Biphenyls (TriBB) Tetrabrominated Biphenyls (TetraBB) Pentabrominated Biphenyls (PentaBB) Hexabrominated Biphenyls (HexaBB) Heptabrominated Biphenyls (HeptaBB) Octabrominated Biphenyls (OctaBB) Nonabrominated Biphenyls (NonaBB) Decabrominated Biphenyl (DecaBB) Polybrominated Diphenyl Ethers (PBDEs) Monobrominated Diphenyl Ethers (MonoBDE) Dibrominated Diphenyl Ethers (DiBDE) Tribrominated Diphenyl Ethers (TriBDE) Tetrabrominated Diphenyl Ethers (TetraBDE) Pentabrominated Diphenyl Ethers (PentaBDE) Hexabrominated Diphenyl Ethers (HexaBDE) Heptabrominated Diphenyl Ethers (HeptaBDE) Octabrominated Diphenyl Ethers (OctaBDE) Nonabrominated Diphenyl Ethers (NonaBDE) Decabrominated Diphenyl Ether (DecaBDE) Halogen Content Fluorine (F) Chlorine (Cl) Bromine (Br) Iodine (I) ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND Remarks: ppm = Parts per million based on weight of tested sample = mg/kg ND = Not detected Responsibility Of Chemist : Irene Chiou / Kevin Liu / Cathy Chen Date Sample Received Testing Period : Dec 24, 2010 : Dec 24, 2010 To Dec 28, 2010 Page 2 Of 6 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401 Number : TWNC00186567 Test Conducted (Ⅱ) RoHS Requirement: Restricted Substances Cadmium (Cd) Content Lead (Pb) Content Mercury (Hg) Content Chromium VI (Cr6+) Content Polybrominated Biphenyls (PBBs) Polybrominated Diphenyl Ehters (PBDEs) Limits 0.01% (100ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for homogeneous material. (Ⅲ) Test Method: Testing Item Cadmium (Cd) content Lead (Pb) content Mercury (Hg) content Chromium VI (Cr6+) content Polybrominated Biphenyls (PBBs) Polybrominated Diphenyl Ethers (PBDEs) Halogen Content Testing Method With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in clause 7, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in annex C, by alkaline digestion and determined by UV-Vis spectrophotometer. With reference to IEC 62321 edition 1.0:2008 in annex A, by solvent extraction and determined by GC-MSD and further HPLC confirmation when necessary. With reference to IEC 62321 edition 1.0:2008 in annex A, by solvent extraction and determined by GC-MSD and further HPLC confirmation when necessary. With reference to EN 14582:2007 by calorimetric bomb with oxygen and determined by ion chromatography Reporting Limit 2 ppm 2 ppm 2 ppm 1 ppm 5 ppm 5 ppm 50 ppm Remark: Reporting limit = Quantitation limit of analyte in sample Page 3 Of 6 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401 Number : TWNC00186567 Test Conducted (Ⅳ) Measurement Flowchart: Test For Cd/Pb/Hg/Chromium (VI)/PBBS/PBDES Contents Reference Standard: IEC 62321 edition 1.0:2008 Sample preparation For non-metal part For metal part Take sample and immerse into Aqua Regia, start to strip plating layer Stop the stripping procedure upon color change completely Take the Aqua solution as plating component and stripped body as substrate component Cd/Pb/Hg Cr Weigh sample and add organic solvent By spot test Negative Confirm the tested samples are totally dissolved Make up with deionized water PBBs/PBDEs Polymers / electronics Metal For different material, digest the sample with *1 appropriate acid 6+ Get 50cm2 sample By boiling water extraction *2 Weigh sample and add alkaline solution By Soxhlet extraction or Solvent extraction Definite temp. extraction Cool and filter the extract Analyzed by ICP-OES Concentrate the extract and make up with organic solvent Analyzed by GC-MSD Make up with deionized water and add diphenylcarbazide solution Remarks: *1: List Of Appropriate Acid: Material Polymers Metals Electronics Analyzed by UV-VIS Acid Added For Digestion HNO3,HCl,HF,H2O2,H3BO3 HNO3,HCl,HF HNO3,HCl,H2O2,HBF4 *2: If the result of spot test is positive, Chromium VI would be determined as detected. Page 4 Of 6 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401 Number : TWNC00186567 Test Conducted (Ⅳ) Measurement Flowchart: Test For Halogen Content Reference Standard:EN 14582 Sampling/grinding or cutting Add absorbent in a calorimetric bomb & place weighed sample in equipment Fill oxygen into calorimetric bomb Ignite then leave the flask at room temperature Transfer the absorbent into a volumetric flask Make up with deionized water Analyzed by ion chromatography End Of Report Page 5 Of 6 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401 Number : TWNC00186567 Test Conducted Photo Page 6 Of 6 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401 Test Report Applicant: Number : TWNC00215224 Littelfuse Philippines Inc. LIMA Technology Center, Lipa City, Malvar, Batangas Date : Jul 12, 2011 Sample Description: One (1) group of submitted samples said to be : Part Description : Sintered (Underglaze Paste) Dielectric Paste Part Number : 011004 Date Sample Received : Jul 07, 2011 Date Test Started : Jul 07, 2011 Test Conducted : As requested by the applicant, for details please refer to attached pages. Authorized By: On Behalf Of Intertek Testing Services Taiwan Limited K. Y. Liang Director This report shall not be reproduced except in full, without the written approval of the laboratory. Page 1 Of 7 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401 Number : TWNC00215224 Test Conducted (Ⅰ) Test Result Summary : Test Item Heavy Metal Cadmium (Cd) content Lead (Pb) content Mercury (Hg) content Chromium VI (Cr6+) content Polybrominated Biphenyls (PBBs) Monobrominated Biphenyls (MonoBB) Dibrominated Biphenyls (DiBB) Tribrominated Biphenyls (TriBB) Tetrabrominated Biphenyls (TetraBB) Pentabrominated Biphenyls (PentaBB) Hexabrominated Biphenyls (HexaBB) Heptabrominated Biphenyls (HeptaBB) Octabrominated Biphenyls (OctaBB) Nonabrominated Biphenyls (NonaBB) Decabrominated Biphenyl (DecaBB) Polybrominated Diphenyl Ethers (PBDEs) Monobrominated Diphenyl Ethers (MonoBDE) Dibrominated Diphenyl Ethers (DiBDE) Tribrominated Diphenyl Ethers (TriBDE) Tetrabrominated Diphenyl Ethers (TetraBDE) Pentabrominated Diphenyl Ethers (PentaBDE) Hexabrominated Diphenyl Ethers (HexaBDE) Heptabrominated Diphenyl Ethers (HeptaBDE) Octabrominated Diphenyl Ethers (OctaBDE) Nonabrominated Diphenyl Ethers (NonaBDE) Decabrominated Diphenyl Ether (DecaBDE) Result (ppm) White/Blue Material ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND Page 2 Of 7 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401 Number : TWNC00215224 Test Conducted (Ⅰ) Test Result Summary : Test Item Result (ppm) White/Blue Material Halogen Content Fluorine (F) Chlorine (Cl) Bromine (Br) Iodine (I) ND ND ND ND Remarks: ppm = Parts per million based on weight of tested sample = mg/kg ND = Not detected Responsibility Of Chemist : Irene Chiou / Kevin Liu / Cathy Chen Date Sample Received Test Period : Jul 07, 2011 : Jul 07, 2011 To Jul 11, 2011 (Ⅱ) RoHS Requirement: Restricted Substances Cadmium (Cd) Content Lead (Pb) Content Mercury (Hg) Content Chromium VI (Cr6+) Content Polybrominated Biphenyls (PBBs) Polybrominated Diphenyl Ehters (PBDEs) Limits 0.01% (100ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for homogeneous material. Page 3 Of 7 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401 Number : TWNC00215224 Test Conducted (Ⅲ) Test Method: Test Item Cadmium (Cd) content Lead (Pb) content Mercury (Hg) content Chromium VI (Cr6+) content Polybrominated Biphenyls (PBBs) Polybrominated Diphenyl Ethers (PBDEs) Halogen Content Test Method Reporting Limit With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested 2 ppm samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested 2 ppm samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in clause 7, by microwave digestion until the tested samples are 2 ppm totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in annex C, by alkaline 1 ppm digestion and determined by UV-Vis spectrophotometer. With reference to IEC 62321 edition 1.0:2008 in annex A, by solvent extraction and determined by GC-MSD 5 ppm and further HPLC confirmation when necessary. With reference to IEC 62321 edition 1.0:2008 in annex A, by solvent extraction and determined by GC-MSD 5 ppm and further HPLC confirmation when necessary. With reference to EN 14582:2007 by calorimetric bomb with oxygen and 50 ppm determined by ion chromatography Remark: Reporting limit = Quantitation limit of analyte in sample Page 4 Of 7 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401 Number : TWNC00215224 Test Conducted (Ⅳ) Measurement Flowchart: Test For Cd/Pb/Hg/Chromium (VI)/PBBS/PBDES Contents Reference Standard: IEC 62321 edition 1.0:2008 Sample preparation For non-metal part For metal part Take sample and immerse into Aqua Regia, start to strip plating layer Stop the stripping procedure upon color change completely Take the Aqua solution as plating component and stripped body as substrate component Cd/Pb/Hg Cr Weigh sample and add organic solvent By spot test Negative Confirm the tested samples are totally dissolved Make up with deionized water PBBs/PBDEs Polymers / electronics Metal For different material, digest the sample with *1 appropriate acid 6+ Get 50cm2 sample By boiling water extraction *2 Weigh sample and add alkaline solution By Soxhlet extraction or Solvent extraction Definite temp. extraction Cool and filter the extract Analyzed by ICP-OES Concentrate the extract and make up with organic solvent Analyzed by GC-MSD Make up with deionized water and add diphenylcarbazide solution Analyzed by UV-VIS Remarks: *1: List Of Appropriate Acid: Acid Added For Digestion Material Polymers HNO3,HCl,HF,H2O2,H3BO3 Metals HNO3,HCl,HF Electronics HNO3,HCl,H2O2,HBF4 *2: If the result of spot test is positive, Chromium VI would be determined as detected. Page 5 Of 7 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401 Number : TWNC00215224 Test Conducted (Ⅳ) Measurement Flowchart: Test For Halogen Content Reference Standard:EN 14582 Sampling/grinding or cutting Add absorbent in a combustion flask & place weighed sample in equipment Fill oxygen into calorimetric bomb Ignite then leave the flask at room temperature Transfer the absorbent into a volumetric flask Make up with deionized water Analyzed by ion chromatography End Of Report Page 6 Of 7 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401 Number : TWNC00215224 Test Conducted Photo Page 7 Of 7 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401 Test Report Applicant: Number : TWNC00182419 Littelfuse, Philippines Inc. LIMA Technology Center, Lipa City, Malvar, Batangas Date : Nov 22, 2010 Sample Description: One (1) group of submitted samples said to be : Part Description : End Termination Paste Part Number : 011001 Date Sample Received : Nov 16, 2010 Date Test Started : Nov 17, 2010 Test Conducted : As requested by the applicant, for details please refer to attached pages. Authorized By: On Behalf Of Intertek Testing Services Taiwan Limited K. Y. Liang Director This report shall not be reproduced except in full, without the written approval of the laboratory. Page 1 Of 7 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401 Number : TWNC00182419 Test Conducted (Ⅰ) Test Result Summary : Testing Item Heavy Metal Cadmium (Cd) content Lead (Pb) content Mercury (Hg) content Chromium VI (Cr6+) content Polybrominated Biphenyls (PBBs) Monobrominated Biphenyls (MonoBB) Dibrominated Biphenyls (DiBB) Tribrominated Biphenyls (TriBB) Tetrabrominated Biphenyls (TetraBB) Pentabrominated Biphenyls (PentaBB) Hexabrominated Biphenyls (HexaBB) Heptabrominated Biphenyls (HeptaBB) Octabrominated Biphenyls (OctaBB) Nonabrominated Biphenyls (NonaBB) Decabrominated Biphenyl (DecaBB) Polybrominated Diphenyl Ethers (PBDEs) Monobrominated Diphenyl Ethers (MonoBDE) Dibrominated Diphenyl Ethers (DiBDE) Tribrominated Diphenyl Ethers (TriBDE) Tetrabrominated Diphenyl Ethers (TetraBDE) Pentabrominated Diphenyl Ethers (PentaBDE) Hexabrominated Diphenyl Ethers (HexaBDE) Heptabrominated Diphenyl Ethers (HeptaBDE) Octabrominated Diphenyl Ethers (OctaBDE) Nonabrominated Diphenyl Ethers (NonaBDE) Decabrominated Diphenyl Ether (DecaBDE) Result (ppm) Grey Paste ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND Page 2 Of 7 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401 Number : TWNC00182419 Test Conducted (Ⅰ) Test Result Summary : Testing Item Result (ppm) Grey Paste Halogen Content Fluorine (F) Chlorine (Cl) Bromine (Br) Iodine (I) ND ND ND ND Remarks: ppm = Parts per million based on wet weight of tested sample = mg/kg ND = Not detected Responsibility Of Chemist : Irene Chiou / Kevin Liu / Cathy Chen Date Sample Received Testing Period : Nov 16, 2010 : Nov 17, 2010 To Nov 19, 2010 (Ⅱ) RoHS Requirement: Restricted Substances Cadmium (Cd) Content Lead (Pb) Content Mercury (Hg) Content Chromium VI (Cr6+) Content Polybrominated Biphenyls (PBBs) Polybrominated Diphenyl Ehters (PBDEs) Limits 0.01% (100ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for homogeneous material. Page 3 Of 7 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401 Number : TWNC00182419 Test Conducted (Ⅲ) Test Method: Testing Item Cadmium (Cd) content Lead (Pb) content Mercury (Hg) content Chromium VI (Cr6+) content Polybrominated Biphenyls (PBBs) Polybrominated Diphenyl Ethers (PBDEs) Halogen Content Testing Method With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in clause 7, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in annex C, by alkaline digestion and determined by UV-Vis spectrophotometer. With reference to IEC 62321 edition 1.0:2008 in annex A, by solvent extraction and determined by GC-MSD and further HPLC confirmation when necessary. With reference to IEC 62321 edition 1.0:2008 in annex A, by solvent extraction and determined by GC-MSD and further HPLC confirmation when necessary. With reference to EN 14582:2007 by calorimetric bomb with oxygen and determined by ion chromatography Reporting Limit 2 ppm 2 ppm 2 ppm 1 ppm 5 ppm 5 ppm 50 ppm Remark: Reporting limit = Quantitation limit of analyte in sample Page 4 Of 7 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401 Number : TWNC00182419 Test Conducted (Ⅳ) Measurement Flowchart: Test For Cd/Pb/Hg/Chromium (VI)/PBBS/PBDES Contents Reference Standard: IEC 62321 edition 1.0:2008 Sampling/grinding or cutting Cd/Pb/Hg Cr Weigh sample and add organic solvent By spot test Negative Confirm the tested samples are totally dissolved Make up with deionized water PBBs/PBDEs Polymers / electronics Metal For different material, digest the sample with *1 appropriate acid 6+ Get 50cm2 sample By boiling water extraction *2 Weigh sample and add alkaline solution By Soxhlet extraction or Solvent extraction Definite temp. extraction Cool and filter the extract Concentrate the extract and make up with organic solvent Analyzed by ICP-OES Analyzed by GC-MSD Make up with deionized water and add diphenylcarbazide solution Analyzed by UV-VIS Remarks: *1: List Of Appropriate Acid: Material Polymers Metals Electronics Acid Added For Digestion HNO3,HCl,HF,H2O2,H3BO3 HNO3,HCl,HF HNO3,HCl,H2O2,HBF4 *2: If the result of spot test is positive, Chromium VI would be determined as detected. Page 5 Of 7 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401 Number : TWNC00182419 Test Conducted (Ⅳ) Measurement Flowchart: Test For Halogen Content Reference Standard: EN 14582 Sampling/grinding or cutting Add absorbent in a calorimetric bomb & place weighed sample in equipment Fill the calorimetric bomb with oxygen Ignite then leave the flask at room temperature Transfer the absorbent into a volumetric flask Make up with deionized water Analyzed by ion chromatography End Of Report Page 6 Of 7 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401 Number : TWNC00182419 Test Conducted Photo Page 7 Of 7 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401 Test Report Applicant: Number : TWNC00182415 Littelfuse, Philippines Inc. LIMA Technology Center, Lipa City, Malvar, Batangas Date : Nov 22, 2010 Sample Description: One (1) group of submitted samples said to be : Part Description : Coverglass Paste Part Number : 011003 Date Sample Received : Nov 16, 2010 Date Test Started : Nov 17, 2010 Test Conducted : As requested by the applicant, for details please refer to attached pages. Authorized By: On Behalf Of Intertek Testing Services Taiwan Limited K. Y. Liang Director This report shall not be reproduced except in full, without the written approval of the laboratory. Page 1 Of 6 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401 Number : TWNC00182415 Test Conducted (Ⅰ) Test Result Summary : Testing Item Result (ppm) Light Green Paste Heavy Metal Cadmium (Cd) content Lead (Pb) content Mercury (Hg) content Chromium VI (Cr6+) content Polybrominated Biphenyls (PBBs) Monobrominated Biphenyls (MonoBB) Dibrominated Biphenyls (DiBB) Tribrominated Biphenyls (TriBB) Tetrabrominated Biphenyls (TetraBB) Pentabrominated Biphenyls (PentaBB) Hexabrominated Biphenyls (HexaBB) Heptabrominated Biphenyls (HeptaBB) Octabrominated Biphenyls (OctaBB) Nonabrominated Biphenyls (NonaBB) Decabrominated Biphenyl (DecaBB) Polybrominated Diphenyl Ethers (PBDEs) Monobrominated Diphenyl Ethers (MonoBDE) Dibrominated Diphenyl Ethers (DiBDE) Tribrominated Diphenyl Ethers (TriBDE) Tetrabrominated Diphenyl Ethers (TetraBDE) Pentabrominated Diphenyl Ethers (PentaBDE) Hexabrominated Diphenyl Ethers (HexaBDE) Heptabrominated Diphenyl Ethers (HeptaBDE) Octabrominated Diphenyl Ethers (OctaBDE) Nonabrominated Diphenyl Ethers (NonaBDE) Decabrominated Diphenyl Ether (DecaBDE) Halogen Content Fluorine (F) Chlorine (Cl) Bromine (Br) Iodine (I) ND 27 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND Remarks: ppm = Parts per million based on wet weight of tested sample = mg/kg ND = Not detected Responsibility Of Chemist : Irene Chiou / Kevin Liu / Cathy Chen Date Sample Received Testing Period : Nov 16, 2010 : Nov 17, 2010 To Nov 22, 2010 Page 2 Of 6 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401 Number : TWNC00182415 Test Conducted (Ⅱ) RoHS Requirement: Restricted Substances Cadmium (Cd) Content Lead (Pb) Content Mercury (Hg) Content Chromium VI (Cr6+) Content Polybrominated Biphenyls (PBBs) Polybrominated Diphenyl Ehters (PBDEs) Limits 0.01% (100ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for homogeneous material. (Ⅲ) Test Method: Testing Item Cadmium (Cd) content Lead (Pb) content Mercury (Hg) content Chromium VI (Cr6+) content Polybrominated Biphenyls (PBBs) Polybrominated Diphenyl Ethers (PBDEs) Halogen Content Testing Method With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in clause 7, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in annex C, by alkaline digestion and determined by UV-Vis spectrophotometer. With reference to IEC 62321 edition 1.0:2008 in annex A, by solvent extraction and determined by GC-MSD and further HPLC confirmation when necessary. With reference to IEC 62321 edition 1.0:2008 in annex A, by solvent extraction and determined by GC-MSD and further HPLC confirmation when necessary. With reference to EN 14582:2007 by calorimetric bomb with oxygen and determined by ion chromatography Reporting Limit 2 ppm 2 ppm 2 ppm 1 ppm 5 ppm 5 ppm 50 ppm Remark: Reporting limit = Quantitation limit of analyte in sample Page 3 Of 6 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401 Number : TWNC00182415 Test Conducted (Ⅳ) Measurement Flowchart: Test For Cd/Pb/Hg/Chromium (VI)/PBBS/PBDES Contents Reference Standard: IEC 62321 edition 1.0:2008 Sampling/grinding or cutting Cd/Pb/Hg Cr Weigh sample and add organic solvent By spot test Negative Confirm the tested samples are totally dissolved Make up with deionized water PBBs/PBDEs Polymers / electronics Metal For different material, digest the sample with *1 appropriate acid 6+ Get 50cm2 sample By boiling water extraction *2 Weigh sample and add alkaline solution By Soxhlet extraction or Solvent extraction Definite temp. extraction Cool and filter the extract Concentrate the extract and make up with organic solvent Analyzed by ICP-OES Analyzed by GC-MSD Make up with deionized water and add diphenylcarbazide solution Remarks: *1: List Of Appropriate Acid: Material Polymers Metals Electronics Analyzed by UV-VIS Acid Added For Digestion HNO3,HCl,HF,H2O2,H3BO3 HNO3,HCl,HF HNO3,HCl,H2O2,HBF4 *2: If the result of spot test is positive, Chromium VI would be determined as detected. Page 4 Of 6 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401 Number : TWNC00182415 Test Conducted (Ⅳ) Measurement Flowchart: Test For Halogen Content Reference Standard: EN 14582 Sampling/grinding or cutting Add absorbent in a calorimetric bomb & place weighed sample in equipment Fill the calorimetric bomb with oxygen Ignite then leave the flask at room temperature Transfer the absorbent into a volumetric flask Make up with deionized water Analyzed by ion chromatography End Of Report Page 5 Of 6 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401 Number : TWNC00182415 Test Conducted Photo Page 6 Of 6 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401 Toat Applicants: RaDoat Lit.tel.fuse, Inc. 800 E. Northnest. Hw]t Desplaines IL 60016 Salnple Description: One (1) group of suhnitted Part Nurnlcer Datse Sanple Received Date Tests Started K. Y. Liang Director Tescing TWNC00172370 Date Sep 03, 2010 samples said to be : Sintered Resinatse Pasle 0 1 1 0 05 Aug 31, 2010 Sep 01, 2010 Test Conducted : As requested by the applicant, Autshorized By: on Behalf Of Intsertek Taiwan Liriited Nunber for details please iefer !o attached paqes Services This reporc sha11 nots be repr:oduced except in fu1l, wilhout the wriEcen approval of tshe laboratory. lnte.t€k Te8tng Servic€sTai{,an Ltd. 8F.,No.423, Ruiguang Rd.,NeliuDietricl, Taip6ill:r,tsiwan,R.O.C. A Eta\Siirh&?i f, fE.a\ 4 114brt,tA{E**r}423 * 8* . 2797{885Fd: (+6€&2) . 6602,2a01 T€r:(+88e2) 6602-2888 6602-24!0 Nurnber : TWNCo0172370 Tes! Conducted ( I Test Result ResulE (ppm) Testing colden/whiEe Tt.en Material E€rvy U.t.l Cadmium (Cd) content Lead (Pb) conlent Mercury lHq ) contents Chromilrm VI { C r " ' ) c o n L e n E ND ND ND ND (PBB.) Po].ybrcGiDAt.fl BiDih.Eyk Monobrominated BiDhenvls {MonoBB) ND ND i\'D DibromioaEed Biohenvls {DiBB Tribrominated Biphenyls (TriBB) (TetraBB) ?etrabrominatsed Biphenvls Pentsabrominatsed Biphenyls ND (PenEaBB) ND ND ND ND I\'D I\'D Hexabrom.inaLed B.iphenvLs (HexaBB) HeoLabrom.inaLed BiDhenvls (HeoLaBB) OcLabrominaLed Biphenvls {OcLaBB) Nonabrominared BiDhenvls {NonaBB) Decabrominared Biphenvl {DecaBB) (PBDES) DlDhaDvl Etharr 9olvbacoiDltcfl Monobroninaled DiDhenvl EEbers (MonoBDE) Dibrominated DiDhenvl Ethers (DiBDE) Tribrominated Diphenvl Erbers ( Tr i BDE) TeErabrominatsed DiDhenvl Etshers (TecraBDE Penrabrominaled Diphenvl E Lhe.rs (PenEaBDE Hexabrominated Diphenvl EEhers (HexaBDE) HeDtabrominaEed DiDhenvl Ethers (HeptaBDE) Oclabrominated Diphenvf Ethers (OCEaBDE) NonabrominaEed DiDhenvl Ethers {NonaBDE) DecabrominaEed Diphenyl Ether (DecaBDE) Ealogqn Coot€ll chlorine Bromine ND ND ND ND I\D N'D ND ND ND ND ND ND ND (cl) {Br) ND Remarks: ppm = Parts per million ND = Not detecEed Responsibility Of Chemists : Irene Date Sample Received Testing Period based on ireight Chiou / Kevin of Liu tested / Cathy sample = mg/kg Chen : Aug 3 1 , 2 0 1 0 : sep 0 1 , 2 0 1 0 T o S e p 0 2 , 2 0 1 0 Pagre 2 Of 6 Interbk T€sting SewicesTaiwar Ltd. R.O.C. Rd.,NeihuOi{nd,Tsip€l114,Taiwsn, 8F.,No.423, Ruiguang +E a\*ldrh&6t f&a';1 11,rg4f ASG*,t,r+423lt IE Iel: (+88G2)6002'2888 2797{885 Fax (+8€8'2)6602-2,|006602-2401 Nunber : 1wNc00172370 Test Conducted (tr Restricted Limtta u.u.Lt (luuppm 10 0 0ppm u . 1 t 10 0 0oonr 100oppm 100000m 0 . 1 t 100oDDm Substances Cd) Content (Pb IJead contenE ltlercurv Hq) conEenE Chromium VI ( C ! ' - l C o n t e n l Polvblominaled Pofvb.rominaEed Brphenv.Ls { PBBS) (PBDES) DiDhenvl Ehters The above limits were quoLed from 2OA2/95/EC and amendment 2005/678/EC tor nomogeneous macerlal. (m Tests MeEhod: Test.ing ltem Testing Cadmium (cd) Lead (Pb) Mercury content {Hg) chromiur vr (Cr6') Polybrominatsed ( PBBS) Biphenyls Polybrominated Diphenyl Ethers (PBDES) flalogen Method WiEh reterence to IEC 62321 editlon 1.0:2008 in clause 8/9/10, by nicrowave digesEion until the tesEed sampfes are totsa]]y dissolved and Conlent idith reference t.o rEC 62321 edit.ion 1.0:2008 in clause 8/9/10, by dcrowave digesEion untl1 the tested samples are tsotsa11y dissolved and Xetermined bv ICP-OES. with reterence to IEc 62321 editsion 1.0:2008 in clause ?, by microlrave digestsion untsil the tesled samples are tolally dissolved and determined by TCP-OES. ivith r.eference to IEC 62321 edition 1.0:2008 in annex C, by alkaline Cigestsion and delermined by W-Vis 6peccroDhotoneter . i{rEh reterence t.o IEc 62321 eclltion 1.0:2008 in annex A, by solvent extsraction and deEermined by GC-I4SD and further HPLC confirmation when Reporting Limits 2 ppm 2 ppm 2 ppm 1 ppm 5 ppm With reference Eo IEC 62321 edition 1.0:2008 in annex A. bv solvents extractsion and determined by GC.MSD and further HPLC confirnatsion lrhen 5 ppm t/lliEh refelence to EN 14582:2007 by calorinetric boab wiLh o)c/gen and determined bv ion chromatsoqraDhv 50 ppm Ren|alk: Reporting limit = Quantitation limiL of analyte in 6amp1e Page Inte.tek TEting Seryic$ T.iwad Lrd. 8F.,No.423,Ruiguang Rd.,NeihuDistdctTaipei114,Taiwan,R.O.C. ig a\rElh&&.r)A Ra\ 5l 1 1 46 r L f 8 S E * r t n 4 2 3 S 8 * Tel:(+88&2)6602-2888 279ru885 Fax(+88&2)6602-2,100 6602-2401 3 Of 6 Nuniber. : TwNc00172370 Tes! Conducted (W) Measureaeat Flowchart: Tests Fot Cd/Pb/Hglchromium (VI) /PBBS/PBDESConcentss Reference Standard: IEC 62321 edi Lion 1 .0:2008 r.Ilring/grindllg or .{ttils acld andcd Fo! D10€s!10n ftlro3,Hc1 , gF , tl2o' .&Eor Eltor uct, HF tilror ltcl, H,o, HBFI 12. Mh. r$ul! o! spot t€3t 13 pos1tlv., chlolrtum vI eroul,albe alal6riln6d .3 Page 4 of IntertekT6ling S€rvicesTaiwanLtd. 8F.,No.,123, Ruiguang Rd.,NeihuDislricl, Taipei 114,Taiwan, R.O.C. a $ a\Eit&xtt)f, rFa\4 114C Jtt Ed E**,r& 423* I & . 2797-8485Fd: (+88e4 6€02-2/m0 . 6602-2401 Tel (+8E&2)6602-2848 6 Number I T$INCo0172370 TesE Conductsed (IV) Measurenent Flowcltar€ : Test For Halogen Conten! Reference standald : EN 14582 sa&pliner/er!indinar o! add absolb€nt in a caloli&etlic bqib & place weighed sanDLe i! fiLt the calorineilic bonb with oxyqen ignite then leave Ure Eno Lrr ReporE Pase 5 Of 6 Int3rt.k Tetlng Sewice. laiwan Ltd. Taipei114,Taiwan, R,O,C, Rd.,N€ihuDislricl, EF.,No.423,Ruiguang A g a\dlhliIt4) f, nl,a\ a 114Ar!lF4#E*)tAa23*8* . 279ru885Far (+8862) Tel:(+8aGa6602-288a 6602-24m6602-2,10l Nuniber : TWNCo0172370 Test ConducEed Pboto Page 5 of Int€rt€kT6ting ServicesTaiwanLld. 8F.,No.,+23, Rurouano Rd.,NoihuDislricl. Taig€i 114,Taiwan, R.O.C. Ats a\Slh&rt6f, fAa\4 r14 6jt,t 4{ErBjtr+423 tt 8il . '9ru885 Fd (+8€62)6602-2/|00 , 6602-2401 Tel:{+8€G2)6602-288a 5 Test Report Applicant: Number : TWNC00182567 Littelfuse, Philippines Inc. LIMA Technology Center, Lipa City, Malvar, Batangas Date : Nov 19, 2010 Sample Description: One (1) group of submitted samples said to be : Part Description : Nickel (metal) Part Number : 010118 Date Sample Received : Nov 17, 2010 Date Test Started : Nov 17, 2010 Test Conducted : As requested by the applicant, for details please refer to attached pages. Authorized By: On Behalf Of Intertek Testing Services Taiwan Limited K. Y. Liang Director This report shall not be reproduced except in full, without the written approval of the laboratory. Page 1 Of 5 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401 Number : TWNC00182567 Test Conducted (Ⅰ) Test Result Summary : Testing Item Heavy Metal Cadmium (Cd) content Lead (Pb) content Mercury (Hg) content Chromium VI (Cr6+) content (mg/kg with 50cm2) Result (ppm) Silvery Metal ND ND ND Negative (< 0.02)(#) Remarks: ppm = Parts per million based on weight of tested sample = mg/kg ND = Not detected < = Less than mg/kg with 50cm2 = milligram per kilogram with 50 square centimetre Negative = A negative test result indicated positive observation was not found at the time of testing. # = Due to the insufficient sample area, reduced total sample surface of 20 cm2 was used and the dilution factor was adjusted accordingly. Responsibility Of Chemist : Irene Chiou / Kevin Liu / Cathy Chen Date Sample Received Testing Period : Nov 17, 2010 : Nov 17, 2010 to Nov 19, 2010 (Ⅱ) RoHS Requirement: Restricted Substances Cadmium (Cd) Content Lead (Pb) Content Mercury (Hg) Content Chromium VI (Cr6+) Content Limits 0.01% (100ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for homogeneous material. Page 2 Of 5 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401 Number : TWNC00182567 Test Conducted (Ⅲ) Test Method: Testing Item Cadmium (Cd) content Lead (Pb) content Mercury (Hg) content Chromium VI (Cr6+) content Testing Method With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in clause 7, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in annex B, by boiling water extraction and determined by UV-Vis spectrophotometer. Reporting Limit 2 ppm 2 ppm 2 ppm 0.02 mg/kg with 50cm2 Remark: Reporting limit = Quantitation limit of analyte in sample Page 3 Of 5 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401 Number : TWNC00182567 Test Conducted (Ⅳ) Measurement Flowchart: Test For Cd/Pb/Hg/Chromium (VI) Reference Standard:IEC 62321 edition 1.0:2008 Sampling/grinding or cutting Cd/Pb/Hg Cr Polymers / Electronics Metal For different material, digest the sample with *1 appropriate acid By spot test Negative Confirm the tested samples are totally dissolved Make up with deionized water 6+ *2 Weigh sample and add alkaline solution Get 50cm2 sample Definite temp. extraction Boiling water extraction Cool and filter the extract Analyzed by ICP-OES Make up with deionized water and add diphenylcarbazide solution Analyzed by UV-VIS Remarks: *1: List Of Appropriate Acid: Acid Added For Digestion Material Polymers HNO3,HCl,HF,H2O2,H3BO3 Metals HNO3,HCl,HF Electronics HNO3,HCl,H2O2,HBF4 *2: If the result of spot test is positive, Chromium VI would be determined as detected. End Of Report Page 4 Of 5 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401 Number : TWNC00182567 Test Conducted Photo Page 5 Of 5 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401 Test Report Applicant: Number : TWNC00182568 Littelfuse, Philippines Inc. LIMA Technology Center, Lipa City, Malvar, Batangas Date : Nov 22, 2010 Sample Description: One (1) group of submitted samples said to be : Part Description : Tin (Sn) Anode (metal) Part Number : 010119 Date Sample Received : Nov 17, 2010 Date Test Started : Nov 17, 2010 Test Conducted : As requested by the applicant, for details please refer to attached pages. Authorized By: On Behalf Of Intertek Testing Services Taiwan Limited K. Y. Liang Director This report shall not be reproduced except in full, without the written approval of the laboratory. Page 1 Of 5 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401 Number : TWNC00182568 Test Conducted Result (ppm) Silvery Metal Testing Item Heavy Metal Cadmium (Cd) content Lead (Pb) content Mercury (Hg) content Chromium VI (Cr6+) content (mg/kg with 50cm2) ND 14 ND Negative (< 0.02)(#) Remarks: ppm = Parts per million based on weight of tested sample = mg/kg ND = Not detected < = Less than mg/kg with 50cm2 = milligram per kilogram with 50 square centimetre Negative = A negative test result indicated positive observation was not found at the time of testing. # = Due to the insufficient sample area, reduced total sample surface of 20 cm2 was used and the dilution factor was adjusted accordingly. Responsibility Of Chemist : Irene Chiou / Kevin Liu / Cathy Chen Date Sample Received Testing Period : Nov 17, 2010 : Nov 17, 2010 To Nov 22, 2010 (Ⅱ) RoHS Requirement: Restricted Substances Cadmium (Cd) Content Lead (Pb) Content Mercury (Hg) Content Chromium VI (Cr6+) Content Limits 0.01% (100ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for homogeneous material. Page 2 Of 5 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401 Number : TWNC00182568 Test Conducted (Ⅲ) Test Method: Testing Item Cadmium (Cd) content Lead (Pb) content Mercury (Hg) content Chromium VI (Cr6+) content Testing Method With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in clause 7, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in annex B, by boiling water extraction and determined by UV-Vis spectrophotometer. Reporting Limit 2 ppm 2 ppm 2 ppm 0.02 mg/kg with 50cm2 Remark: Reporting limit = Quantitation limit of analyte in sample Page 3 Of 5 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401 Number : TWNC00182568 Test Conducted (Ⅳ) Measurement Flowchart: Test For Cd/Pb/Hg/Chromium (VI) Reference Standard:IEC 62321 edition 1.0:2008 Sampling/grinding or cutting Cd/Pb/Hg Cr Polymers / Electronics Metal For different material, digest the sample with *1 appropriate acid By spot test Negative Confirm the tested samples are totally dissolved Make up with deionized water 6+ *2 Weigh sample and add alkaline solution Get 50cm2 sample Definite temp. extraction Boiling water extraction Cool and filter the extract Analyzed by ICP-OES Make up with deionized water and add diphenylcarbazide solution Remarks: *1: List Of Appropriate Acid: Material Polymers Metals Electronics Analyzed by UV-VIS Acid Added For Digestion HNO3,HCl,HF,H2O2,H3BO3 HNO3,HCl,HF HNO3,HCl,H2O2,HBF4 *2: If the result of spot test is positive, Chromium VI would be determined as detected. End Of Report Page 4 Of 5 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401 Number : TWNC00182568 Test Conducted Photo Page 5 Of 5 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401