ICPTest_FLQ pdf

ICP Test Report Certification Packet
Company name :
Littelfuse, Inc.
Product Series:
FLQ Series
Product #:
FLQ Series
Issue Date:
March 20, 2012
It is hereby certified by Littelfuse, Inc. that there is neither RoHS (EU Directive
2002/95/EC)-restricted substance nor such use, for materials to be used for unit parts, for
packing/packaging materials, and for additives and the like in the manufacturing processes.
In addition, it is hereby reported to you that the parts and sub-materials, the materials to be used
for unit parts, the packing/packaging materials, and the additives and the like in the manufacturing
processes, are all composed of the following components.
Issued by:
<Global EHS Engineer>
(1) Parts, sub-materials and unit parts
This document covers the FLQ RoHS-Compliant series products manufactured by
Littelfuse, Inc.
＜ Raw Materials Used
Please see Table 1
(2) The ICP data on all measurable substances
Please see appropriate pages as identifed in Table 1
Remarks：
Form 585-047 Rev. A
1
2/21/06
Table 1: List of Raw Materials covered by this report
Total Parts
1
2
3
4
5
6
7
8
9
10
11
Raw Material Part Number
648102
082xxx (082384)
079xxx
685xxx
923-001
692532
927-027
909-410
09018x
425723/425721
087293
Raw Material Description
Yarn
Wire-Copper Nickel Alloy
Wire-Cu 110 Strip w/center Sn Overlay
Pure Ag (685406)
Fuse cap
Wire Solder
Solder Pellet
Midget Paper Body
Sand filler
Ribbon
Adhesive
2
Page(s)
3-11
12-21
22-25
26-30
31-35
36-40
41-45
46-52
53-61
62-67
68-76
Intertek Testing Services Ltd., Shanghai
TFH Division
Block B, Jinling Business Square,No.801 Yi Shan Road,
Shanghai, China, 200233
Tel: +86 21 6120 6565
Fax: +86 21 6127 9740
www.intertek.com
www.intertek.com.cn
China Toll-Free: 800 999 1338
TEST REPORT
APPLICANT: LITTELFUSE,INC.
800 E. NORTHWEST HWY
ATTN: A. CESISTA/ K. BACILA
NUMBER: SHAH00276230
DATE: AUG 24, 2011
SAMPLE DESCRIPTION:
One(1) submitted sample said to be :White yarn.
Part Description
: Yarn.
Part Number
: 648102.
Date Sample Received
: Aug.18, 2011.
Date Test Started
: Aug.18, 2011.
***********************************************************************
TESTS CONDUCTED:
AS REQUESTED BY THE APPLICANT, FOR DETAILS REFER TO ATTACHED PAGE(S)
***********************************************************************
TO BE CONTINUED
PREPARED AND CHECKED BY:
FOR INTERTEK TESTING SERVICES
LTD., SHANGHAI
AUTHORIZED BY:
FOR INTERTEK TESTING SERVICES
LTD., SHANGHAI
MYRA LV
CHEMICAL LAB SENIOR MANAGER
STEPHEN TSANG
GENERAL MANAGER
PAGE 1 OF 9
Intertek Testing Services Ltd., Shanghai
TFH Division
Block B, Jinling Business Square,No.801 Yi Shan Road,
Shanghai, China, 200233
Tel: +86 21 6120 6565
Fax: +86 21 6127 9740
www.intertek.com
www.intertek.com.cn
China Toll-Free: 800 999 1338
TEST REPORT
NUMBER: SHAH00276230
TESTS CONDUCTED
1
(I) Test Result Summary :
Testing Item
Halogen Content
Fluorine (F)
Chlorine (Cl)
Bromine (Br)
Iodine (I)
Result (ppm)
ND
ND
ND
ND
Remarks: ppm = Parts per million = mg/kg
ND = Not detected
Responsibility Of Chemist : Ken He
(II) Test Method:
Testing Item
Testing Method
With reference to EN 14582:2007 by
Halogen
combustion flask with oxygen and
Content
determined by ion chromatography
Reporting Limit
50 ppm
Remark: Reporting limit = Quantitation limit of analyte in sample
***********************************************************************
TO BE CONTINUED
PAGE 2 OF 9
Intertek Testing Services Ltd., Shanghai
TFH Division
Block B, Jinling Business Square,No.801 Yi Shan Road,
Shanghai, China, 200233
Tel: +86 21 6120 6565
Fax: +86 21 6127 9740
www.intertek.com
www.intertek.com.cn
China Toll-Free: 800 999 1338
TEST REPORT
NUMBER: SHAH00276230
TESTS CONDUCTED
(III) Measurement Flowchart:
Test For Halogen Content
Reference Standard： EN 14582
sampling/grinding or
cutting
add absorbent in a
combustion flask &
place weighed sample in
equipment
fill the combustion
flask with oxygen
ignite then leave the
flask at room
temperature
transfer the absorbent
into a volumetric flask
make up with deionized
water
analyzed by ion
chromatography
***********************************************************************
TO BE CONTINUED
PAGE 3 OF 9
Intertek Testing Services Ltd., Shanghai
TFH Division
Block B, Jinling Business Square,No.801 Yi Shan Road,
Shanghai, China, 200233
Tel: +86 21 6120 6565
Fax: +86 21 6127 9740
www.intertek.com
www.intertek.com.cn
China Toll-Free: 800 999 1338
TEST REPORT
NUMBER: SHAH00276230
TESTS CONDUCTED
2
(I) Test Result Summary :
Testing Item
Heavy Metal
Cadmium (Cd) content
Lead (Pb) content
Mercury (Hg) content
Chromium VI (Cr6+) content
Polybrominated Biphenyls (PBBs)
Monobrominated Biphenyls (MonoBB)
Dibrominated Biphenyls (DiBB)
Tribrominated Biphenyls (TriBB)
Tetrabrominated Biphenyls (TetraBB)
Pentabrominated Biphenyls (PentaBB)
Hexabrominated Biphenyls (HexaBB)
Heptabrominated Biphenyls (HeptaBB)
Octabrominated Biphenyls (OctaBB)
Nonabrominated Biphenyls (NonaBB)
Decabrominated Biphenyl (DecaBB)
Polybrominated Diphenyl Ethers (PBDEs)
Monobrominated Diphenyl Ethers (MonoBDE)
Dibrominated Diphenyl Ethers (DiBDE)
Tribrominated Diphenyl Ethers (TriBDE)
Tetrabrominated Diphenyl Ethers (TetraBDE)
Pentabrominated Diphenyl Ethers (PentaBDE)
Hexabrominated Diphenyl Ethers (HexaBDE)
Heptabrominated Diphenyl Ethers (HeptaBDE)
Octabrominated Diphenyl Ethers (OctaBDE)
Nonabrominated Diphenyl Ethers (NonaBDE)
Decabrominated Diphenyl Ether (DecaBDE)
Result (ppm)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Remarks: ppm = Parts per million = mg/kg
ND = Not detected
Responsibility Of Chemist : Dent Fang / Ken He
***********************************************************************
TO BE CONTINUED
PAGE 4 OF 9
Intertek Testing Services Ltd., Shanghai
TFH Division
Block B, Jinling Business Square,No.801 Yi Shan Road,
Shanghai, China, 200233
Tel: +86 21 6120 6565
Fax: +86 21 6127 9740
www.intertek.com
www.intertek.com.cn
China Toll-Free: 800 999 1338
TEST REPORT
NUMBER: SHAH00276230
TESTS CONDUCTED
(II) RoHS Requirement:
Restricted Substances
Cadmium (Cd) Content
Lead (Pb) Content
Mercury (Hg) Content
Chromium VI (Cr6+) Content
Polybrominated Biphenyls (PBBs)
Polybrominated Diphenyl Ehters (PBDEs)
Limits
0.01% (100ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
The above limits were quoted from 2002/95/EC and amendment
2005/618/EC for homogeneous material.
(III) Test Method:
Testing Item
Testing Method
Reporting
Limit
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
Cadmium (Cd)
microwave digestion until the
2 ppm
content
tested samples are totally
dissolved and determined by ICPOES.
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the
Lead (Pb) content
2 ppm
tested samples are totally
dissolved and determined by ICPOES.
With reference to IEC 62321 edition
1.0:2008 in clause 7, by microwave
Mercury (Hg)
digestion until the tested samples
2 ppm
content
are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
Chromium VI (Cr6+) 1.0:2008 in annex C, by alkaline
1 ppm
content
digestion and determined by UV-Vis
spectrophotometer.
***********************************************************************
TO BE CONTINUED
PAGE 5 OF 9
Intertek Testing Services Ltd., Shanghai
TFH Division
Block B, Jinling Business Square,No.801 Yi Shan Road,
Shanghai, China, 200233
Tel: +86 21 6120 6565
Fax: +86 21 6127 9740
www.intertek.com
www.intertek.com.cn
China Toll-Free: 800 999 1338
TEST REPORT
NUMBER: SHAH00276230
TESTS CONDUCTED
Testing Item
Polybrominated
Biphenyls (PBBs)
Polybrominated
Diphenyl Ethers
(PBDEs)
Testing Method
With reference to IEC 62321 edition
1.0:2008 in annex A, by solvent
extraction and determined by GC-MSD
and further HPLC confirmation when
necessary.
With reference to IEC 62321 edition
1.0:2008 in annex A, by solvent
extraction and determined by GC-MSD
and further HPLC confirmation when
necessary.
Reporting
Limit
5 ppm
5 ppm
Remark: Reporting limit = Quantitation limit of analyte in sample
Date Sample Received : AUG.18, 2011
Testing Period : AUG.18, 2011 TO AUG.23, 2011
***********************************************************************
TO BE CONTINUED
PAGE 6 OF 9
Intertek Testing Services Ltd., Shanghai
TFH Division
Block B, Jinling Business Square,No.801 Yi Shan Road,
Shanghai, China, 200233
Tel: +86 21 6120 6565
Fax: +86 21 6127 9740
www.intertek.com
www.intertek.com.cn
China Toll-Free: 800 999 1338
TEST REPORT
NUMBER: SHAH00276230
TESTS CONDUCTED
(IV) Measurement Flowchart:
Test For Cd/Pb/Hg/Chromium (VI)/PBBs/PBDEs Contents
Reference Standard: IEC 62321 edition 1.0:2008
sampling/grinding or cutting
Cr6+
Cd/Pb/Hg
metal
weigh sample and
for different
material, digest
the sample with
confirm the tested
samples are totally
dissolved
spot test
negative*2
No
polymers /
electronics
weigh sample
and add
alkaline
solution
get 50cm2
samples
definite
temp.
boiling water
extraction
cool and
filter the
extract
PBBs/PBDEs
weigh sample
and add
organic
soxhlet
extraction or
solvent
extraction
make up with
deionized water
analyzed by ICP-OES
make up with deionized
water and add diphenylcarbazide solution
concentrate
the extract
and make up
with organic
analyzed by GCMSD
analyzed by UV-VIS
***********************************************************************
TO BE CONTINUED
PAGE 7 OF 9
Intertek Testing Services Ltd., Shanghai
TFH Division
Block B, Jinling Business Square,No.801 Yi Shan Road,
Shanghai, China, 200233
Tel: +86 21 6120 6565
Fax: +86 21 6127 9740
www.intertek.com
www.intertek.com.cn
China Toll-Free: 800 999 1338
TEST REPORT
NUMBER: SHAH00276230
TESTS CONDUCTED
REMARKS:
*1: List of appropriate acid：
Material
Acid added for digestion
Polymers
HNO3,HCl,HF,H2O2,H3BO3
Metals
HNO3,HCl,HF
Electronics
HNO3,HCl,H2O2,HBF4
*2: If the result of spot test is positive, Chromium VI would be
determined as detected.
***********************************************************************
TO BE CONTINUED
PAGE 8 OF 9
Intertek Testing Services Ltd., Shanghai
TFH Division
Block B, Jinling Business Square,No.801 Yi Shan Road,
Shanghai, China, 200233
Tel: +86 21 6120 6565
Fax: +86 21 6127 9740
www.intertek.com
www.intertek.com.cn
China Toll-Free: 800 999 1338
TEST REPORT
NUMBER: SHAH00276230
TESTS CONDUCTED
***********************************************************************
END OF REPORT
PAGE 9 OF 9
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""..o..o-.,..o".o"
rFlil,*E+
Test Report
i t 4 ( N " . ) , cE/20t2/taa3?
$\Date) : 2012/0r/r\
F*(pzse)
ET.SCHUXOM
ELEKTROSCHUTZKOMPONENTENBAU
GMBH
GEWERBES]IASSE
8?, D-98669 WII-SDORF, GBMA\Y
t[] [ttt]
*[S4it(styr€/rten No.)
( D - 1 ) 1 0 1- - 2 2 8 . 0 ' - t u n g s t e n- t i n n e d E i . e t V ,S n
( D - 2) r 0 1 . 0 1 2 6 . -0 qr, Ni
tungsten purity, nickel pLatedrire
( D - 3 ) r 0 1 . 0 1 2 t . 0- _
corp€f - nickel {1 anoy (cotrsranran) sire
cuNi.tl
( D - 4 )r 0 r . 0 1 2 4 . 0 - - copp€r-!ickel zinc-attoy
vire (NSl8) - CuNi18Zn20
( D - 5 )1 0 r . 0 1 2 7 . 0 - - -_
copper - nickel -alLoy sire
cuNi 2
( D - 6 )l 0 l . 0 1 2 90. - - - copper - nickel -alloy
rire
ClNi 12
( D - 7 )1 0 1 . 0 1 7 4 .- 0 - coppe. - nrcket -a]]oy
wire
CuNi 6
( D - 8 )1 0 1 . 0 r 7 5 . 0 - copper - nickel -attoy
wire
CuNi 22
( D - 9 )r 0 r . 0 r 7 8 . 0- - - iron - nickel -attoy sire
FeNi36(rivar)
( D - 1 0 r) 0 r . 0 1 ? 5 . 0- - - copper - nanganese- nickel -alloy
vire
CuMnt2Ni
compada
yil
1/ !r.
rr.l':,ri,'l:l;nr'i
I
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: s of r0
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TestReport
IILSCIiIKOIi IIEKTROsCHUTZKOIIPONENTENBAU
GMBH
GEWERBESTMSSE
87, D 98669 VEII.SDoRF, GIRUANry
1l
#iq,x T 6t*,reI:r'6+
, |ls e,eljg*
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ll][t[]t
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2) i.Jt{.^ I : it41* / Nameof the personwrD mademeasu€menl:Ctimbs@tyang
3) jrl{ I ir'. : *4rr+ / Narneortle p€€on in .hargeof medurernern:T.oychang
f *,' gli*s
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/Culting.P€pararion
/ samolei,leasuMent
&447:n*.e h d q a|^at $!a{4lifi tri+ T t
rf+) /Aciddigeslion
bysuirabte
aciddepended
on
(asb€tow
difierenr
sampre
maledat
tabt€)
.g&/E rn/{ n*irr&)tti lh /
Microuave
dig$tionsilh HNorHct/HF
,"*5.1{*a,t4ti,Alt+
18'/ Heatto apprcpdate
liftlgfl
/ Hcl to dissolE
/ lcP-AEs
6E*+tt,F+d+it*d'
N[,?itf /sampleMaEnd
,AlC.{,rtltfr / Diqeslion
Acd
r*, I{*, I.n, n*.*, tnn /
S€el.copp€r,
aluminum,
solder
I:1i' r i,r,'j:lirl,i
: r.r
/rdd
r/* ,f *, a l,ra/..,t$.,t
,4*'.sAkAs0 nmr!'{
4i{ q{.'t {&, i* / H:so.,H,o,,HNotr.
Hcl
/ any acid1ototaldigBtion
,!^l+ttrt4taa*
tu
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ldua reoia.HNo..Hct.HF.H,o,
4re.! R* / HNO,1-iF
Gold.dalinum.oalladium.
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abEolbanceat 5)40nm bY
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TestReport
*(Date) : 2012101/11 q*(p,s")
ETSCHUKOM
ELE(TROSCHUI'ZXONPONENTENBAU
GVBH
CEIERBESTRASSE
87, D-98669 VEILSDORF,GERVJ}.IY
t *d*/
||ll[tutflru ||[rl
r *4+&+&jft,'E||
/ PBB/PBDE
anatyticat
FLowCHART
.
il]li/-F r Aqry / Nameotthe peEon \ifro mad€measurementRomanWono
r
,Q;{ A t \ r tACq / Nameofthe peEon rl cha€e ofmeasurcmentT.oy Cha;g
t rtrl3ttr+ / FirsttBling proc6s ------t
/ Optimalscreenpocess----....
4#t1Slta,l
pro@ss-. -.t
&At:rt / Confmatjon
Scrcenanalysis/t{Srf
I
I
t 7 0 t L 0
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{ltr;++J
soxhrer
method*{+qqi
I
I
concentrate/Dilute
Extractedsotution
+clRri*/it6
Filter/ +f.t{i&&
Analysis
byGC/[4S
/ {rtB&fi.{*d.+tr
p31stbsrad rh6 rad GPon €f ml be
rysub]dlobGe^e6cdidsonsds
l:,]'i+..:ir&l0rl2sr
,fl-d,#+
Test Report
lE6(No.) : cEl2012lr0837 E * ( D a t e ) : 2 0 1 2 l o r / 1 1 F * ( p , e " )
EI,SCHU(OM ELE(IROSCHIITZKOMPONENTEN&{U
GVBH
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87,
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tt+fi*#f
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GEL\LAI{Y
/ Analyticalflow
chartof hatogon
content
I
jllt[LF : *.S,* /Nameoftheperson
whomademeasurement
RitaChen
I
jllt\, F l-l. : tits4 / Nameof thepeFonin chargeof measurcment:
TroyChang
e+8fr16,ifr t
Analysis
wasperformed
by lC
||||l[![]|ll
fi{s,+E+
Test Report
!t4(No.)
: cD/2012l10837
ES(Date) : 2012l01/11 Ftk(p,s") : 9 of to
ELSCHU(OM
ELEKTROSCHTITZKOMA)NENTENBAU
CMBH
GETERBESTRASSE
87, D-98669 T'EILSDORF,CER\LA\Y
lt]
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Analytical flow chart of Soxhletextraction(LC/ltS) procedure
r
r
;{:t/-F : .-i-!9d / Narneof the personwhomademeasurement:
Rofian Wong .
x{fi I l',,i' : ,i,*R / Nameof thepersonin chargeof measurement:
TroyChang
( d,t E: A;.+ti,4rUAE+&(*) ' *&:4t{bA&
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comp.i,fj: irl,!iii
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lE6(No.) : CEl2012lr0S37 E * ( D a r e ) : 2 0 r 2 l 0 1 / 1 1 F j k ( p a s e ) : r 0 o f l 0
EIICI1UKOMELEXTRqSCHIT'TZKOIIPONENTEN&qU
CMBH
GEIERBESTRASSE
8?, D-98669 VEITSDORF,
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is oarked !y
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PENY
PonyTcstingInaernalional
Group
T€atReport
NO.: W020320112MD
Ddet 2012.02.07
Page1 of4
Applicant:
Address:
SUZHOUXINWUOPTRONICTTECHNOLOGY
CO,.LTD
368 YOUYIRD,YOUYIDEVELOPMENT
AREA,SONGLING
TOWNWUJIANG
SUZHOU,CHINA
Thefollowingsample(s)
waslderesubmittedandidentified
on behalfof the clientas:
SampleName:
BRASS
i/lanufacfurer,
SUZHOU
XINWUOPTRONICTTECHNOLOGY
CO.,LTD
SampleDescription, SOLDER
COATING
ONCu
Testing
PadDescription:l\4lxTESTED
SampleReceived
Date: 2012.O2.03
TestPeriod:
2012.02.03 Io 2012.02.07
TestRequested
.
ln accordance
withthe RoHSDirective2011/65/EU
AnnexII
TestMethod:
Withreference
to 1EC62321
Edition1.0:2008method: RegulatedSubstances
Contentof testprooesswithElectrical
& Electronic
Products
(1) LeadAnalysis
performed
is
byMS
(2) CadmiumAnalysisis performed
byAAS
(3) MercuryAnalysis
is performed
by ICP-OES
(4) Hexavalent
Chromium
Analysisis performedBy Spot-test/Boiling-waterextractionMethod
(5) PBBSand PBDESAnalysis
is performedby GC-|\4S
TestResult:
Pleasereferto nextpage(s)
Approvedby:
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NO.: W020320.11204D
Datet 2012.02.07
Page2 ol 4
TestResult(Unit:
Test lHn
I\4DL
Lead (Pb)
'|
Cadmium(Cd)
1
TestResult
N.D.
N.D.
(Hg)
Mercury
1
See Note (6)
Negative
Hexavalent
Chromium(Cr6*)
RoHSLimit
N,D,
1000
PBBs
5
N.D.
N.D.
5
5
N,D,
Pentabromobiphenyl
Hexabromobiphenyl
Heptabromobiphenyl
5
Octabromobiphenyl
Nonabromobiphenyl
Decabromobiphenyl
N.D.
N.D,
N,D.
N,DN.D.
N-DN.D.
PBDEs
1000
Bromodiphenyl
ether
Dibromodiphenyl
ether
Tribromodiphenyl
ether
Tetrabromodiphenyl
ether
Pentabromodiphenyl
ether
Hexabromodiohenvl
ether
Heptabromodiphenyl
ether
Octabromodiphenyl
ether
5
N.D.
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5
5
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100
1000
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Dibromobiphenyl
Tribromobiphenyl
Tetrabromobiphenyl
mNv slE
1000
N.D.
N.D.
N.D.
N.D.
N,D,
N.D,
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Croup
TestReport
Note:
NO.,W02032011204D
Da|e,2012.02.07
Page3 of 4
= ppm
(1)mgr'kg
(2) '-" = Do6 not stipulate
(3)N.D.= NorDeteded(<MDL)
(a) MDL= MethodD€teclonUmit
(5)Themostallowable
limit valuereference
to RoHSDirecli\€2011/6tEUAnnexII
(6)Spot-tst,
Negative= NotDetectedof CrVlcoatrng,Po€iti!€= Presenceof CrVlcoatingl
(Thetestedsarnpleshouldbs furth€rveifi€d by boilingFwateFextracljon
methodif the spottest resultcannotbe
confimedor negatjve)
j
Boiling-wAeFextraclion
N€gative= NotOet€ct€dof CrVlcraijng
Positi\,€: Presenceof CrVlcoatingithe detecledconcentmtion
in boiling-wateGextraction
solutionis equal
or g€atd thanO.O2mgy'kg
with soon'?samplesudac€areaused.
pedomedas clionfsrequ€st.
The
mixing
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te€t
was
Resultobtained
onlygive€infomalityvalu€anddoe6
{7)
notreDresent
individual
samDle
male al.
Photo:
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the photoon originalreportonly
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PonyTesting
Intemationnl
Ctoup
TestReport
NO.: W02032011204D
Date,2012.02.07
Measurement
Flo /-chart
Page4 of 4
Testedby' XuYing
Checkedby: Walter
Personin chargeofthe lab: Zhangdaiqin
TheseSamplesWere DissolvedToblly By Pre-conditioning
MethodAccordingTo BetowFlowChart.(Cf*
And PBBS,/PBDES
TestMethodExcluded)
Samplel\reasurement
Acid digestionwith
microrave/hotplate
Nonmetallic
materi€l
Filtration
andpH
Adding1,5diphenylcarbazi
deforcolor
development
AAS/tCP-OES
**End of Report"'
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Int nrtiond
Grcup
l!€at
Nuniber
R€polt
ApplicanE:
r i rf6l
f"qa
Dhirinnino<
Jatf, 20, 2072
Tr-
LTMA Technology Cent.er., Lipa
Malvai,
Batangas
c:nnl6
n6c^ri^fi
of suLfi\itted
samples said
'
Part
Nurber
h.F6
<.1161
6
Da^6i
q,76
TesE conducted :
As requested by the applicanE,
ctTi^
for
deEails
please
refer
!o aEEached pages.
P\/.
on Behalf of hEerEek
Taiwan Limited
K. Y. liang
Director
tso be :
ei l var
:685>oo(
| Jan 16, 2012
I Jan 16, 2012
t,aA
Date Teslr SEarEed
z6a
Citsy,
^h.
One (1) group
r,, Fh^7i
TWNC00240910
Testing
Services
This reports shal1 not be reproduced
witshouts the writsten
excepts in full,
approval of the laboral:ory.
IntertekTesting S€wlcesTaisranLtd.
8F., No.423, RuiguangRd., NeihuDi6t ci, Taipei 114, Taiwan,R.O c
A E a\S+*r*xq6t fRa\;l
114g JLt '9:lEE* i€te423ft 8 +l
. 2797{885 Fax (+886-2)
6602.24006602_2401
Teli{+08e2)6602-2848
Nuricer
Test
: T!,1NC00240910
Conductsed
( I ) Test
Result
Summary :
Result
{ppm)
silvery
Metal
lilelal
Eeavy
Cadmium (Cd) content
(Pb)
l,ead
ND
ND
ND
content
Mercury (ltg ) contsent
Chromiun VI (Crh+) conlent
(ms/kg witsh 50cm')
Nesative
(< 0.02 )
based on weight of tested sample = mg/kg
Remarks: ppm = Parts per million
ND = Nots detectsed
= Less tshan
<
mg/kg with 5ocm'z= milLigram per kilogram wiEh 50 square centimetsre
observation
tesL result
indicaEed positive
NegaEive = A negative
was not found at the time of Test.
Responsibility
Date
Test
(ul
of ChemisL
: Irene
Chiou / Kevin Liu
: ,Ja \6, 2012
| 'Jan 16, 2412 To JaI] 20, 2OI2
Sa$p1e Received
Period
KoHs KequrremenE:
Limitss
0.01t (10oppm)
0 . 1 t ( 1 00 o p p m )
0 18 (100oppm)
0 1* ( 100oppn)
Restsrictsed Substances
Cad,nium (Cd) Contenl
Lead
(Pb)
Mercury
ConLent
(Hg) ConEen!
ChromiLrm vI
(cr6t)
Content
were quotsed from 2002/95/EC and amendments2005/6IAlEC
The above limirs
homooeneous natseria1.
for
Page 2 of
Intert€kTesting Se.vlcesTaiwanLtd.
Taiwan,
R o C.
Taipei114,
Rd.,NeihuDistrlct.
No.423,
Ruiguang
8F.,
4 g a\':Si*r&11.1'
tr IEa\61
1 1 46 i L t ] ^ { E x i j L r * 4 2 3* 8 *
@02-288a2?97-8885Fa: (+88G2)6602-2'1006602-2401
Teti(+886-2)
5
Nurnber : TWNCo0240910
Tests Conduct.ed
(lll)
Tests Method:
Test Ilem
Tesl
Method
Repo]:ting
With reference Lo IEC 62321 editsion
1.0:2008 in clause 8/9/10, by
admium (Cd)
microwave digest.ion until
Lhe tsested
samples are totally
dissolved and
deternined by ICP-OES.
wirh reference to TEc 62321 editsion
1.0:2008 in clause 8/9/10, by
Lead (Pb) contenE
microwave digrestion until
the rested
samples are totally
dissolved and
determined by ICP OES.
With reference to IEC 62321 editsion
1.0:2008 in clause 7, by microwave
l4ercury (Eg)
digest.ion until
the tsestsedsamples are
tsotally dissolved and detsermined by
ICP OES.
t{ith reference to IEC 62321 editsion
1.0:2008 in armex B, by boiling water
(ms/ks witsh s0cm'?) extractsion and detsermined by W-Vis
SpecLrophotomeLer .
Remark:
Reporting
limit
= QuantiLation
limiE
of analyte
in
IntertekT$ting Servic€sT.iwan Ltd.
Rd.,NeihuOislricl,
Taipei114.Taiwan,R.O.C
8F.,No.423,Ruiguang
A Ela\lir*ft&?} tr rEa\5l
ret: (+&2)
1146 jhF E i! 6S /i,!| 423!l I *
6@2-2aB 2n7{885
Fa* (+88F2)6602-2400 6602-2401
I,imit
2 ppm
2 ppm
2 ppm
o,a2
mg/kg with
sample
5ocm'?
Number : TWNCo0240910
Test ConducLed
( IV) ueasurenent Flowchart :
Test Eor Cd/ Pb/HSlchromium (VI)
R e f e r e n c e S t a n d a r d : I E C 6 2 3 2 1 -e d i t i o n
sanPli.g/glindins
confim
1.0:2008
or cutting
Ehe tesred
Amlyzed by rcP ols
l,take up with deionized
wa!e! ald add dipnenyl
calbazid€
solution
Analyzed b, rrv vrs
11: Lisl
Of Appropriale
Acid
added
Fo!
pigestion
l o l o r . H c l , H F ,H : O , , H ] B O 3
taNor.Hcl,tlF
:lNOr HCL H,O, HBF!
*2:
If
Ehe lesu1t
of
spot tes!
is posltiwe,
chroniN
vI
would be deternined
as detected.
End of
Reports
Page
Int€n€kT$ting ServlcesTaiwanLid.
8F., No. !r23, RoiguangRd., NeihuDisfici, Taipei 114, Taiwan,R.o.c
its a\:e,*&is&'* fE'a\A
1143 JLt rsr{3E* tt} 423!i I *
rel: (+33e2)6602-28882797€aAS Fd: (AAG2!6602-24O0664,-2401
4 of
5
Nunlcer
: T!,1NC00240910
Tests Conducted
Photo
IntertekTestlng Sedices Taiu,anLtd.
Rd.,NeihuDisiricl,Taipei114 Taiwan,R O C
SF.,No.,t23,Ruiguang
A tsa\:6?h&&4)a R a\ ;l
114 e t lF ri|;146JS it& 423 li 3 i+
Tel: (€a6-2) 6602-2884 2797_8885 Fd: (+8562) 6602-2400 6602_2401
Test Report
Applicant:
Number : TWNC00213348
Littelfuse, S.A. de C.V.
Blvd. Fausto Z. Martinez #1800
Col. Magisterio Seccion 38 C.P.
26070 Piedra Negras, Coahuila,
Mexico
Date
: Jul 01, 2011
Sample Description:
One (1) group of submitted samples said to be :
Part Description
: FUSE CAP-Plated
Part Number
: 923-001
Date Sample Received
: Jun 28, 2011
Date Test Started
: Jun 28, 2011
Test Conducted :
As requested by the applicant, for details please refer to attached pages.
Authorized By:
On Behalf Of Intertek Testing Services
Taiwan Limited
K. Y. Liang
Director
This report shall not be reproduced
except in full, without the written
approval of the laboratory.
Page 1 Of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00213348
Test Conducted
(Ⅰ) Test Result Summary :
Result (ppm)
(1)
(2)
Test Item
Heavy Metal
Cadmium (Cd) content
Lead (Pb) content
Mercury (Hg) content
Chromium VI (Cr6+) content (mg/kg with 50cm2)
ND
ND
ND
Negative (<
0.02)(#)
ND
ND
ND
Negative (<
0.02)(#)
Remarks: ppm = Parts per million based on weight of tested sample = mg/kg
ND = Not detected
<
= Less than
mg/kg with 50cm2 = milligram per kilogram with 50 square centimetre
Negative = A negative test result indicated positive observation
was not found at the time of Test.
#
= Due to the insufficient sample area, reduced total sample
surface of 10 cm2 was used and the dilution factor was
adjusted accordingly.
Tested Components
(1) Silvery Plating Layer
(2) Silvery Metal Base Material
Responsibility Of Chemist : Irene Chiou / Kevin Liu / Cathy Chen
Date Sample Received
Test Period
: Jun 28, 2011
: Jun 28, 2011 To Jul 01, 2011
(Ⅱ) RoHS Requirement:
Restricted Substances
Cadmium (Cd) Content
Lead (Pb) Content
Mercury (Hg) Content
Chromium VI (Cr6+) Content
Limits
0.01% (100ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for
homogeneous material.
Page 2 Of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00213348
Test Conducted
(Ⅲ) Test Method:
Test Item
Cadmium (Cd)
content
Lead (Pb) content
Mercury (Hg)
content
Chromium VI (Cr6+)
content
Test Method
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 7, by microwave
digestion until the tested samples are
totally dissolved and determined by
ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in annex B, by boiling water
extraction and determined by UV-Vis
spectrophotometer.
Reporting Limit
2 ppm
2 ppm
2 ppm
0.02
mg/kg with 50cm2
Remark: Reporting limit = Quantitation limit of analyte in sample
Page 3 Of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00213348
Test Conducted
(Ⅳ) Measurement Flowchart:
Test For Cd/Pb/Hg/Chromium (VI)
Reference Standard：IEC 62321 edition 1.0:2008
Sample preparation
Take sample and immerse into Aqua Regia, start to strip plating layer
Stop the stripping procedure upon color change completely
Take the Aqua solution as plating component and stripped body as substrate component
Cd/Pb/Hg
Cr
Polymers /
electronics
Metal
For different
material, digest
the sample with
*1
appropriate acid
By spot test
Negative
Confirm the tested
samples are
totally dissolved
Make up with
deionized water
6+
*2
Weigh sample
and add
alkaline
solution
Get 50cm2 sample
Definite temp.
extraction
By boiling water
extraction
Cool and filter
the extract
Analyzed by ICP-OES
Make up with deionized water and add
diphenyl-carbazide solution
Remarks:
*1: List Of Appropriate Acid：
Material
Polymers
Metals
Electronics
Analyzed by UV-VIS
Acid Added For Digestion
HNO3,HCl,HF,H2O2,H3BO3
HNO3,HCl,HF
HNO3,HCl,H2O2,HBF4
*2: If the result of spot test is positive, Chromium VI would be determined as detected.
End Of Report
Page 4 Of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00213348
Test Conducted
Photo
Page 5 Of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Test Report
Applicant:
Number : TWNC00213351
Littelfuse, S.A. de C.V.
Blvd. Fausto Z. Martinez #1800
Col. Magisterio Seccion 38 C.P.
26070 Piedra Negras, Coahuila,
Mexico
Date
: Jul 01, 2011
Sample Description:
One (1) group of submitted samples said to be :
Part Description
: WIRE SOLDER .100 DIA - ROHS
Part Number
: 692532
Date Sample Received
: Jun 28, 2011
Date Test Started
: Jun 28, 2011
Test Conducted :
As requested by the applicant, for details please refer to attached pages.
Authorized By:
On Behalf Of Intertek Testing Services
Taiwan Limited
K. Y. Liang
Director
This report shall not be reproduced
except in full, without the written
approval of the laboratory.
Page 1 Of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00213351
Test Conducted
(Ⅰ) Test Result Summary :
Result (ppm)
Silvery Metal
Test Item
Heavy Metal
Cadmium (Cd) content
Lead (Pb) content
Mercury (Hg) content
Chromium VI (Cr6+) content (mg/kg with 50cm2)
ND
221
ND
Negative (< 0.02)
Remarks: ppm = Parts per million based on weight of tested sample = mg/kg
ND = Not detected
<
= Less than
mg/kg with 50cm2 = milligram per kilogram with 50 square centimetre
Negative = A negative test result indicated positive observation
was not found at the time of Test.
Responsibility Of Chemist : Irene Chiou / Kevin Liu / Cathy Chen
Date Sample Received
Test Period
: Jun 28, 2011
: Jun 28, 2011 To Jul 01, 2011
(Ⅱ) RoHS Requirement:
Restricted Substances
Cadmium (Cd) Content
Lead (Pb) Content
Mercury (Hg) Content
Chromium VI (Cr6+) Content
Limits
0.01% (100ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for
homogeneous material.
Page 2 Of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00213351
Test Conducted
(Ⅲ) Test Method:
Test Item
Cadmium (Cd)
content
Lead (Pb) content
Mercury (Hg)
content
Chromium VI (Cr6+)
content
Test Method
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 7, by microwave
digestion until the tested samples are
totally dissolved and determined by
ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in annex B, by boiling water
extraction and determined by UV-Vis
spectrophotometer.
Reporting Limit
2 ppm
2 ppm
2 ppm
0.02
mg/kg with 50cm2
Remark: Reporting limit = Quantitation limit of analyte in sample
Page 3 Of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00213351
Test Conducted
(Ⅳ) Measurement Flowchart:
Test For Cd/Pb/Hg/Chromium (VI)
Reference Standard：IEC 62321 edition 1.0:2008
Sample preparation
Take sample and immerse into Aqua Regia, start to strip plating layer
Stop the stripping procedure upon color change completely
Take the Aqua solution as plating component and stripped body as substrate component
Cd/Pb/Hg
Cr
Polymers /
electronics
Metal
For different
material, digest
the sample with
*1
appropriate acid
By spot test
Negative
Confirm the tested
samples are
totally dissolved
Make up with
deionized water
6+
*2
Weigh sample
and add
alkaline
solution
Get 50cm2 sample
Definite temp.
extraction
By boiling water
extraction
Cool and filter
the extract
Analyzed by ICP-OES
Make up with deionized water and add
diphenyl-carbazide solution
Remarks:
*1: List Of Appropriate Acid：
Material
Polymers
Metals
Electronics
Analyzed by UV-VIS
Acid Added For Digestion
HNO3,HCl,HF,H2O2,H3BO3
HNO3,HCl,HF
HNO3,HCl,H2O2,HBF4
*2: If the result of spot test is positive, Chromium VI would be determined as detected.
End Of Report
Page 4 Of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00213351
Test Conducted
Photo
Page 5 Of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Test Report
Applicant:
Number : TWNC00213353
Littelfuse, S.A. de C.V.
Blvd. Fausto Z. Martinez #1800
Col. Magisterio Seccion 38 C.P.
26070 Piedra Negras, Coahuila,
Mexico
Date
: Jul 01, 2011
Sample Description:
One (1) group of submitted samples said to be :
Part Description
: SOLDER PELLET
Part Number
: 927-027
Date Sample Received
: Jun 28, 2011
Date Test Started
: Jun 28, 2011
Test Conducted :
As requested by the applicant, for details please refer to attached pages.
Authorized By:
On Behalf Of Intertek Testing Services
Taiwan Limited
K. Y. Liang
Director
This report shall not be reproduced
except in full, without the written
approval of the laboratory.
Page 1 Of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00213353
Test Conducted
(Ⅰ) Test Result Summary :
Result (ppm)
Silvery Metal
Test Item
Heavy Metal
Cadmium (Cd) content
Lead (Pb) content
Mercury (Hg) content
Chromium VI (Cr6+) content (mg/kg with 50cm2)
ND
335
ND
Negative (< 0.02)
Remarks: ppm = Parts per million based on weight of tested sample = mg/kg
ND = Not detected
<
= Less than
mg/kg with 50cm2 = milligram per kilogram with 50 square centimetre
Negative = A negative test result indicated positive observation
was not found at the time of Test.
Responsibility Of Chemist : Irene Chiou / Kevin Liu / Cathy Chen
Date Sample Received
Test Period
: Jun 28, 2011
: Jun 28, 2011 To Jul 01, 2011
(Ⅱ) RoHS Requirement:
Restricted Substances
Cadmium (Cd) Content
Lead (Pb) Content
Mercury (Hg) Content
Chromium VI (Cr6+) Content
Limits
0.01% (100ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for
homogeneous material.
Page 2 Of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00213353
Test Conducted
(Ⅲ) Test Method:
Test Item
Cadmium (Cd)
content
Lead (Pb) content
Mercury (Hg)
content
Chromium VI (Cr6+)
content
Test Method
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 7, by microwave
digestion until the tested samples are
totally dissolved and determined by
ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in annex B, by boiling water
extraction and determined by UV-Vis
spectrophotometer.
Reporting Limit
2 ppm
2 ppm
2 ppm
0.02
mg/kg with 50cm2
Remark: Reporting limit = Quantitation limit of analyte in sample
Page 3 Of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00213353
Test Conducted
(Ⅳ) Measurement Flowchart:
Test For Cd/Pb/Hg/Chromium (VI)
Reference Standard：IEC 62321 edition 1.0:2008
Sample preparation
Take sample and immerse into Aqua Regia, start to strip plating layer
Stop the stripping procedure upon color change completely
Take the Aqua solution as plating component and stripped body as substrate component
Cd/Pb/Hg
Cr
Polymers /
electronics
Metal
For different
material, digest
the sample with
*1
appropriate acid
By spot test
Negative
Confirm the tested
samples are
totally dissolved
Make up with
deionized water
6+
*2
Weigh sample
and add
alkaline
solution
Get 50cm2 sample
Definite temp.
extraction
By boiling water
extraction
Cool and filter
the extract
Analyzed by ICP-OES
Make up with deionized water and add
diphenyl-carbazide solution
Remarks:
*1: List Of Appropriate Acid：
Material
Polymers
Metals
Electronics
Analyzed by UV-VIS
Acid Added For Digestion
HNO3,HCl,HF,H2O2,H3BO3
HNO3,HCl,HF
HNO3,HCl,H2O2,HBF4
*2: If the result of spot test is positive, Chromium VI would be determined as detected
End Of Report
Page 4 Of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00213353
Test Conducted
Photo
Page 5 Of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Test Report
Applicant:
Number : TWNC00213350
Littelfuse, S.A. de C.V.
Blvd. Fausto Z. Martinez #1800
Col. Magisterio Seccion 38 C.P.
26070 Piedra Negras, Coahuila,
Mexico
Date
: Jun 30, 2011
Sample Description:
One (1) group of submitted samples said to be :
Part Description
: MIDGET PAPER BODY
Part Number
: 909-410
Date Sample Received
: Jun 28, 2011
Date Test Started
: Jun 28, 2011
Test Conducted :
As requested by the applicant, for details please refer to attached pages.
Authorized By:
On Behalf Of Intertek Testing Services
Taiwan Limited
K. Y. Liang
Director
This report shall not be reproduced
except in full, without the written
approval of the laboratory.
Page 1 Of 7
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00213350
Test Conducted
(Ⅰ) Test Result Summary :
Test Item
Result (ppm)
Black Material
Heavy Metal
Cadmium (Cd) content
Lead (Pb) content
Mercury (Hg) content
Chromium VI (Cr6+) content
Polybrominated Biphenyls (PBBs)
Monobrominated Biphenyls (MonoBB)
Dibrominated Biphenyls (DiBB)
Tribrominated Biphenyls (TriBB)
Tetrabrominated Biphenyls (TetraBB)
Pentabrominated Biphenyls (PentaBB)
Hexabrominated Biphenyls (HexaBB)
Heptabrominated Biphenyls (HeptaBB)
Octabrominated Biphenyls (OctaBB)
Nonabrominated Biphenyls (NonaBB)
Decabrominated Biphenyl (DecaBB)
Polybrominated Diphenyl Ethers (PBDEs)
Monobrominated Diphenyl Ethers (MonoBDE)
Dibrominated Diphenyl Ethers (DiBDE)
Tribrominated Diphenyl Ethers (TriBDE)
Tetrabrominated Diphenyl Ethers (TetraBDE)
Pentabrominated Diphenyl Ethers (PentaBDE)
Hexabrominated Diphenyl Ethers (HexaBDE)
Heptabrominated Diphenyl Ethers (HeptaBDE)
Octabrominated Diphenyl Ethers (OctaBDE)
Nonabrominated Diphenyl Ethers (NonaBDE)
Decabrominated Diphenyl Ether (DecaBDE)
Halogen Content
Fluorine (F)
Chlorine (Cl)
Bromine (Br)
Iodine (I)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Remarks: ppm = Parts per million based on weight of tested sample = mg/kg
ND = Not detected
Responsibility Of Chemist : Irene Chiou / Kevin Liu / Cathy Chen
Date Sample Received
Test Period
: Jun 28, 2011
: Jun 28, 2011 to Jun 30, 2011
Page 2 Of 7
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Test Conducted
(Ⅱ) RoHS Requirement:
Restricted Substances
Cadmium (Cd) Content
Lead (Pb) Content
Mercury (Hg) Content
Chromium VI (Cr6+) Content
Polybrominated Biphenyls (PBBs)
Polybrominated Diphenyl Ehters (PBDEs)
Number : TWNC00213350
Limits
0.01% (100ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for
homogeneous material.
(Ⅲ) Test Method:
Test Item
Cadmium (Cd)
content
Lead (Pb) content
Mercury (Hg)
content
Chromium VI (Cr6+)
content
Test Method
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 7, by microwave
digestion until the tested samples are
totally dissolved and determined by
ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in annex C, by alkaline
digestion and determined by UV-Vis
spectrophotometer.
Reporting Limit
2 ppm
2 ppm
2 ppm
1 ppm
Page 3 Of 7
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Test Conducted
(Ⅲ) Test Method:
Test Item
Polybrominated
Biphenyls (PBBs)
Polybrominated
Diphenyl Ethers
(PBDEs)
Halogen Content
Number : TWNC00213350
Test Method
With reference to IEC 62321 edition
1.0:2008 in annex A, by solvent
extraction and determined by GC-MSD
and further HPLC confirmation when
necessary.
With reference to IEC 62321 edition
1.0:2008 in annex A, by solvent
extraction and determined by GC-MSD
and further HPLC confirmation when
necessary.
With reference to EN 14582:2007 by
calorimetric bomb with oxygen and
determined by ion chromatography
Reporting Limit
5 ppm
5 ppm
50 ppm
Remark: Reporting limit = Quantitation limit of analyte in sample
Page 4 Of 7
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00213350
Test Conducted
(Ⅳ) Measurement Flowchart:
Test For Cd/Pb/Hg/Chromium (VI)/PBBS/PBDES Contents
Reference Standard: IEC 62321 edition 1.0:2008
Sample preparation
For non-metal part
For metal part
Take sample and immerse into Aqua Regia, start to strip plating layer
Stop the stripping procedure upon color change completely
Take the Aqua solution as plating component and stripped body as substrate component
Cd/Pb/Hg
Cr
Confirm the tested
samples are
totally dissolved
Make up with
deionized water
PBBs/PBDEs
Polymers /
electronics
Metal
For different
material, digest
the sample with
*1
appropriate acid
6+
Weigh sample and
add organic solvent
By spot test
Negative
Get 50cm2 sample
By boiling water
extraction
*2
Weigh sample
and add
alkaline
solution
By Soxhlet
extraction or
Solvent extraction
Definite temp.
extraction
Cool and filter
the extract
Analyzed by ICP-OES
Concentrate the
extract and make up
with organic
solvent
Analyzed by GC-MSD
Make up with deionized
water and add diphenylcarbazide solution
Remarks:
*1: List Of Appropriate Acid：
Material
Polymers
Metals
Electronics
Analyzed by UV-VIS
Acid Added For Digestion
HNO3,HCl,HF,H2O2,H3BO3
HNO3,HCl,HF
HNO3,HCl,H2O2,HBF4
*2: If the result of spot test is positive, Chromium VI would be determined as detected.
Page 5 Of 7
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00213350
Test Conducted
(Ⅳ) Measurement Flowchart:
Test For Halogen Content
Reference Standard：EN 14582
Sampling/grinding or
cutting
Add absorbent in a
combustion flask &
place weighed sample in
equipment
Fill oxygen into
calorimetric bomb
Ignite then leave the
flask at room
temperature
Transfer the absorbent
into a volumetric flask
Make up with deionized
water
Analyzed by ion
chromatography
End Of Report
Page 6 Of 7
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00213350
Test Conducted
Photo
Page 7 Of 7
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Intertek Testing Services Ltd., Shanghai
TFH Division
Block B, Jinling Business Square,No.801 Yi Shan Road,
Shanghai, China, 200233
Tel: +86 21 6120 6565
Fax: +86 21 6127 9740
www.intertek.com
www.intertek.com.cn
China Toll-Free: 800 999 1338
TEST REPORT
APPLICANT: LITTELFUSE,INC.
800 E. NORTHWEST HWY
ATTN: A. CESISTA/ K. BACILA
NUMBER: SHAH00296144
DATE: DEC 20, 2011
SAMPLE DESCRIPTION:
One(1) submitted sample said to be White powder.
Part Description
: Snow white filler.
Part Number
: 090184.
Date Sample Received
: Dec.14, 2011.
Date Test Started
: Dec.14, 2011.
***********************************************************************
TESTS CONDUCTED:
AS REQUESTED BY THE APPLICANT, FOR DETAILS REFER TO ATTACHED PAGE(S)
**********************************************************************
TO BE CONTINUED
PREPARED AND CHECKED BY:
FOR INTERTEK TESTING SERVICES
LTD., SHANGHAI
AUTHORIZED BY:
FOR INTERTEK TESTING SERVICES
LTD., SHANGHAI
MYRA LV
CHEMICAL LAB SENIOR MANAGER
STEPHEN TSANG
GENERAL MANAGER
PAGE 1 OF 9
Intertek Testing Services Ltd., Shanghai
TFH Division
Block B, Jinling Business Square,No.801 Yi Shan Road,
Shanghai, China, 200233
Tel: +86 21 6120 6565
Fax: +86 21 6127 9740
www.intertek.com
www.intertek.com.cn
China Toll-Free: 800 999 1338
TEST REPORT
NUMBER: SHAH00296144
TESTS CONDUCTED
1
(I) Test Result Summary :
Testing Item
Halogen Content
Fluorine (F)
Chlorine (Cl)
Bromine (Br)
Iodine (I)
Result (ppm)
ND
ND
ND
ND
Remarks: ppm = Parts per million based on weight of tested sample =
mg/kg
ND = Not detected
Responsibility Of Chemist
(II) Test Method:
Testing Item
Halogen Content
: Ken He
Testing Method
With reference to EN 14582:2007 by
combustion flask with oxygen and
determined by ion chromatography
Reporting Limit
50 ppm
Remark: Reporting limit = Quantitation limit of analyte in sample
**********************************************************************
TO BE CONTINUED
PAGE 2 OF 9
Intertek Testing Services Ltd., Shanghai
TFH Division
Block B, Jinling Business Square,No.801 Yi Shan Road,
Shanghai, China, 200233
Tel: +86 21 6120 6565
Fax: +86 21 6127 9740
www.intertek.com
www.intertek.com.cn
China Toll-Free: 800 999 1338
TEST REPORT
NUMBER: SHAH00296144
TESTS CONDUCTED
(III) Measurement Flowchart:
Test For Halogen Content
Reference Standard： EN 14582
sampling/grinding or
cutting
add absorbent in a
combustion flask &
place weighed sample in
equipment
fill the combustion
flask with oxygen
ignite then leave the
flask at room
temperature
transfer the absorbent
into a volumetric flask
make up with deionized
water
analyzed by ion
chromatography
**********************************************************************
TO BE CONTINUED
PAGE 3 OF 9
Intertek Testing Services Ltd., Shanghai
TFH Division
Block B, Jinling Business Square,No.801 Yi Shan Road,
Shanghai, China, 200233
Tel: +86 21 6120 6565
Fax: +86 21 6127 9740
www.intertek.com
www.intertek.com.cn
China Toll-Free: 800 999 1338
TEST REPORT
NUMBER: SHAH00296144
TESTS CONDUCTED
2
(I) Test Result Summary :
Result (ppm)
Testing Item
Heavy Metal
Cadmium (Cd) content
ND
Lead (Pb) content
ND
Mercury (Hg) content
ND
Chromium VI (Cr6+) content
ND
Polybrominated Biphenyls (PBBs)
Monobrominated Biphenyls (MonoBB)
ND
Dibrominated Biphenyls (DiBB)
ND
Tribrominated Biphenyls (TriBB)
ND
Tetrabrominated Biphenyls (TetraBB)
ND
Pentabrominated Biphenyls (PentaBB)
ND
Hexabrominated Biphenyls (HexaBB)
ND
Heptabrominated Biphenyls (HeptaBB)
ND
Octabrominated Biphenyls (OctaBB)
ND
Nonabrominated Biphenyls (NonaBB)
ND
Decabrominated Biphenyl (DecaBB)
ND
Polybrominated Diphenyl Ethers (PBDEs)
Monobrominated Diphenyl Ethers (MonoBDE)
ND
Dibrominated Diphenyl Ethers (DiBDE)
ND
Tribrominated Diphenyl Ethers (TriBDE)
ND
Tetrabrominated Diphenyl Ethers (TetraBDE)
ND
Pentabrominated Diphenyl Ethers (PentaBDE)
ND
Hexabrominated Diphenyl Ethers (HexaBDE)
ND
Heptabrominated Diphenyl Ethers (HeptaBDE)
ND
Octabrominated Diphenyl Ethers (OctaBDE)
ND
Nonabrominated Diphenyl Ethers (NonaBDE)
ND
Decabrominated Diphenyl Ether (DecaBDE)
ND
**********************************************************************
TO BE CONTINUED
PAGE 4 OF 9
Intertek Testing Services Ltd., Shanghai
TFH Division
Block B, Jinling Business Square,No.801 Yi Shan Road,
Shanghai, China, 200233
Tel: +86 21 6120 6565
Fax: +86 21 6127 9740
www.intertek.com
www.intertek.com.cn
China Toll-Free: 800 999 1338
TEST REPORT
NUMBER: SHAH00296144
TESTS CONDUCTED
Remarks: ppm = Parts per million = mg/kg
ND = Not detected
Responsibility Of Chemist : Dent Fang / Ken He
(II) RoHS Requirement:
Restricted Substances
Cadmium (Cd) Content
Lead (Pb) Content
Mercury (Hg) Content
Chromium VI (Cr6+) Content
Polybrominated Biphenyls (PBBs)
Polybrominated Diphenyl Ehters (PBDEs)
Limits
0.01% (100ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
The above limits were quoted from 2002/95/EC and amendment
2005/618/EC for homogeneous material.
**********************************************************************
TO BE CONTINUED
PAGE 5 OF 9
Intertek Testing Services Ltd., Shanghai
TFH Division
Block B, Jinling Business Square,No.801 Yi Shan Road,
Shanghai, China, 200233
Tel: +86 21 6120 6565
Fax: +86 21 6127 9740
www.intertek.com
www.intertek.com.cn
China Toll-Free: 800 999 1338
TEST REPORT
NUMBER: SHAH00296144
TESTS CONDUCTED
(III) Test Method:
Testing Item
Testing Method
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
Cadmium (Cd)
microwave digestion until the
content
tested samples are totally
dissolved and determined by ICPOES.
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the
Lead (Pb) content
tested samples are totally
dissolved and determined by ICPOES.
With reference to IEC 62321 edition
1.0:2008 in clause 7, by microwave
Mercury (Hg)
digestion until the tested samples
content
are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
Chromium VI (Cr6+) 1.0:2008 in annex C, by alkaline
content
digestion and determined by UV-Vis
spectrophotometer.
With reference to IEC 62321 edition
1.0:2008 in annex A, by solvent
Polybrominated
extraction and determined by GC-MSD
Biphenyls (PBBs)
and further HPLC confirmation when
necessary.
With reference to IEC 62321 edition
Polybrominated
1.0:2008 in annex A, by solvent
Diphenyl Ethers
extraction and determined by GC-MSD
(PBDEs)
and further HPLC confirmation when
necessary.
Reporting
Limit
2 ppm
2 ppm
2 ppm
1 ppm
5 ppm
5 ppm
Remark: Reporting limit = Quantitation limit of analyte in sample
DATE SAMPLE RECEIVED : DEC.14, 2011
TESTING PERIOD : DEC.14, 2011 TO DEC.19, 2011
**********************************************************************
TO BE CONTINUED
PAGE 6 OF 9
Intertek Testing Services Ltd., Shanghai
TFH Division
Block B, Jinling Business Square,No.801 Yi Shan Road,
Shanghai, China, 200233
Tel: +86 21 6120 6565
Fax: +86 21 6127 9740
www.intertek.com
www.intertek.com.cn
China Toll-Free: 800 999 1338
TEST REPORT
NUMBER: SHAH00296144
TESTS CONDUCTED
(IV) Measurement Flowchart:
Test For Cd/Pb/Hg/Chromium (VI)/PBBs/PBDEs Contents
Reference Standard: IEC 62321 edition 1.0:2008
sampling/grinding or cutting
Cr6+
Cd/Pb/Hg
metal
weigh sample and
for different
material, digest
the sample with
confirm the tested
samples are totally
dissolved
spot test
negative*2
No
polymers /
electronics
weigh sample
and add
alkaline
solution
get 50cm2
samples
definite
temp.
boiling water
extraction
cool and
filter the
extract
PBBs/PBDEs
weigh sample
and add
organic
soxhlet
extraction or
solvent
extraction
make up with
deionized water
analyzed by ICP-OES
make up with deionized
water and add diphenylcarbazide solution
concentrate
the extract
and make up
with organic
analyzed by GCMSD
analyzed by UV-VIS
**********************************************************************
TO BE CONTINUED
PAGE 7 OF 9
Intertek Testing Services Ltd., Shanghai
TFH Division
Block B, Jinling Business Square,No.801 Yi Shan Road,
Shanghai, China, 200233
Tel: +86 21 6120 6565
Fax: +86 21 6127 9740
www.intertek.com
www.intertek.com.cn
China Toll-Free: 800 999 1338
TEST REPORT
NUMBER: SHAH00296144
TESTS CONDUCTED
REMARKS:
*1: List of appropriate acid：
Material
Acid added for digestion
Polymers
HNO3,HCl,HF,H2O2,H3BO3
Metals
HNO3,HCl,HF
Electronics
HNO3,HCl,H2O2,HBF4
*2: If the result of spot test is positive, Chromium VI would be
determined as detected.
**********************************************************************
TO BE CONTINUED
PAGE 8 OF 9
Intertek Testing Services Ltd., Shanghai
TFH Division
Block B, Jinling Business Square,No.801 Yi Shan Road,
Shanghai, China, 200233
Tel: +86 21 6120 6565
Fax: +86 21 6127 9740
www.intertek.com
www.intertek.com.cn
China Toll-Free: 800 999 1338
TEST REPORT
NUMBER: SHAH00296144
TESTS CONDUCTED
**********************************************************************
END OF REPORT
PAGE 9 OF 9
Test Report
Applicant:
Number : TWNC00222563
Littelfuse, S.A. de C.V.
Blvd. Fausto Z. Martinez #1800
Col. Magisterio Seccion 38 C.P.
26070 Piedra Negras, Coahuila,
Mexico
Date
: Sep 07, 2011
Sample Description:
One (1) group of submitted samples said to be :
Part Description
: Ribbon black
Part Number
: 425723
Date Sample Received
: Sep 05, 2011
Date Test Started
: Sep 05, 2011
Test Conducted :
As requested by the applicant, for details please refer to attached pages.
Authorized By:
On Behalf Of Intertek Testing Services
Taiwan Limited
K. Y. Liang
Director
This report shall not be reproduced
except in full, without the written
approval of the laboratory.
Page 1 of 6
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00222563
Test Conducted
(Ⅰ) Test Result Summary :
Test Item
Result (ppm)
Black Plastic Film
Heavy Metal
Cadmium (Cd) content
Lead (Pb) content
Mercury (Hg) content
Chromium VI (Cr6+) content
Polybrominated Biphenyls (PBBs)
Monobrominated Biphenyls (MonoBB)
Dibrominated Biphenyls (DiBB)
Tribrominated Biphenyls (TriBB)
Tetrabrominated Biphenyls (TetraBB)
Pentabrominated Biphenyls (PentaBB)
Hexabrominated Biphenyls (HexaBB)
Heptabrominated Biphenyls (HeptaBB)
Octabrominated Biphenyls (OctaBB)
Nonabrominated Biphenyls (NonaBB)
Decabrominated Biphenyl (DecaBB)
Polybrominated Diphenyl Ethers (PBDEs)
Monobrominated Diphenyl Ethers (MonoBDE)
Dibrominated Diphenyl Ethers (DiBDE)
Tribrominated Diphenyl Ethers (TriBDE)
Tetrabrominated Diphenyl Ethers (TetraBDE)
Pentabrominated Diphenyl Ethers (PentaBDE)
Hexabrominated Diphenyl Ethers (HexaBDE)
Heptabrominated Diphenyl Ethers (HeptaBDE)
Octabrominated Diphenyl Ethers (OctaBDE)
Nonabrominated Diphenyl Ethers (NonaBDE)
Decabrominated Diphenyl Ether (DecaBDE)
Halogen Content
Fluorine (F)
Chlorine (Cl)
Bromine (Br)
Iodine (I)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Remarks: ppm = Parts per million based on weight of tested sample = mg/kg
ND = Not detected
Responsibility of Chemist : Irene Chiou / Kevin Liu / Cathy Chen
Date Sample Received
Test Period
: Sep 05, 2011
: Sep 05, 2011 To Sep 07, 2011
Page 2 of 6
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Test Conducted
(Ⅱ) RoHS Requirement:
Restricted Substances
Cadmium (Cd) Content
Lead (Pb) Content
Mercury (Hg) Content
Chromium VI (Cr6+) Content
Polybrominated Biphenyls (PBBs)
Polybrominated Diphenyl Ehters (PBDEs)
Number : TWNC00222563
Limits
0.01% (100ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for
homogeneous material.
(Ⅲ) Test Method:
Test Item
Cadmium (Cd)
content
Lead (Pb) content
Mercury (Hg)
content
Chromium VI (Cr6+)
content
Polybrominated
Biphenyls (PBBs)
Polybrominated
Diphenyl Ethers
(PBDEs)
Halogen Content
Test Method
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 7, by microwave
digestion until the tested samples are
totally dissolved and determined by
ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in annex C, by alkaline
digestion and determined by UV-Vis
spectrophotometer.
With reference to IEC 62321 edition
1.0:2008 in annex A, by solvent
extraction and determined by GC-MSD
and further HPLC confirmation when
necessary.
With reference to IEC 62321 edition
1.0:2008 in annex A, by solvent
extraction and determined by GC-MSD
and further HPLC confirmation when
necessary.
With reference to EN 14582:2007 by
calorimetric bomb with oxygen and
determined by ion chromatography
Reporting Limit
2 ppm
2 ppm
2 ppm
1 ppm
5 ppm
5 ppm
50 ppm
Remark: Reporting limit = Quantitation limit of analyte in sample
Page 3 of 6
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00222563
Test Conducted
(Ⅳ) Measurement Flowchart:
Test for Cd/Pb/Hg/Chromium (VI)/PBBS/PBDES Contents
Reference Standard: IEC 62321 edition 1.0:2008
Sample preparation
For non-metal part
For metal part
Take sample and immerse into Aqua Regia, start to strip plating layer
Stop the stripping procedure upon color change completely
Take the Aqua solution as plating component and stripped body as substrate component
Cd/Pb/Hg
Cr
Confirm the tested
samples are
totally dissolved
Make up with
deionized water
PBBs/PBDEs
Polymers /
electronics
Metal
For different
material, digest
the sample with
*1
appropriate acid
6+
Weigh sample and
add organic solvent
By spot test
Negative
Get 50cm2 sample
By boiling water
extraction
*2
Weigh sample
and add
alkaline
solution
By Soxhlet
extraction or
Solvent extraction
Definite temp.
extraction
Cool and filter
the extract
Analyzed by ICP-OES
Concentrate the
extract and make up
with organic
solvent
Analyzed by GC-MSD
Make up with deionized
water and add diphenylcarbazide solution
Analyzed by UV-VIS
Remarks:
*1: List of Appropriate Acid：
Material
Polymers
Metals
Electronics
Acid Added for Digestion
HNO3,HCl,HF,H2O2,H3BO3
HNO3,HCl,HF
HNO3,HCl,H2O2,HBF4
*2: If the result of spot test is positive, Chromium VI would be determined as detected.
Page 4 of 6
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00222563
Test Conducted
(Ⅳ) Measurement Flowchart:
Test for Halogen Content
Reference Standard：EN 14582
Sampling/grinding or
cutting
Add absorbent in a
combustion flask &
place weighed sample in
equipment
Fill oxygen into
calorimetric bomb
Ignite then leave the
flask at room
temperature
Transfer the absorbent
into a volumetric flask
Make up with deionized
water
Analyzed by ion
chromatography
End of Report
Page 5 of 6
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00222563
Test Conducted
Photo
Page 6 of 6
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401