ICPTest_SP1003_01ETG_SP3030_01ETG_SP3031_01ETG__pdf

ICP Test Report Certification Packet
Company name :
Littelfuse, Inc.
Product Series:
TVS Diode for ESD Protection
Product #:
SP1003-01ETG, SP3030-01ETG & SP3031-01ETG
Issue Date:
August 22, 2011
It is hereby certified by Littelfuse, Inc. that there is neither RoHS (EU Directive
2002/95/EC)-restricted substance nor such use, for materials to be used for unit parts, for
packing/packaging materials, and for additives and the like in the manufacturing processes.
In addition, it is hereby reported to you that the parts and sub-materials, the materials to be used
for unit parts, the packing/packaging materials, and the additives and the like in the manufacturing
processes, are all composed of the following components.
Issued by:
<Global EHS Engineer>
(1) Parts, sub-materials and unit parts
This document covers the
TVS Diode for ESD Protection - Package Type
RoHS-Compliant series products manufactured by Littelfuse, Inc.
＜ Raw Materials Used
Please see Table 1
(2) The ICP data on all measurable substances
Please see appropriate pages as identifed in Table 1
Remarks：.
1
Table 1: List of Raw Materials covered by this report
Total Parts
1
2
3
4
5
6
Form 585-047 Rev. A
Raw Material Part
Number
N/A
N/A
84-1LMlSR
CEL-922O
N/A
N/A
Raw Material Description
Leadframe
Gold Bonding Wire
Adhesive
Epoxy Molding Compound
Tin
Wafer
2
Page(s)
3-11
12-24
25-50
51-58
59-63
64
2/21/06
TestReport
No.:GZ1101010693CHEM
Date:FEB09,2oil
Page1 ot I
QPL LI[.4ITED
NO.1,PINZHI ROAD,XINAN INDUSTBIAL
PARK,CHANGAN TOWN,DONGGUAN,
GUANGDONG,
CHINA
The followingsample(s)was/weresubmittedand identified
on behatfot the appticantas C194
SGSJob No.
s212959189
SGS InlernalReferenceNo.
25.8
ClientReferenceInformalion
Samplemaycover QFN,DFN,SOp, HD,BU,SBp, SO|C,DUAL,
OFP,PLCC,PDIP,TOFP
Dateof SampleReceived
JAN 26, 20t 1
TeslingPeriod
JAN 26, 20'11TO FEB09, 2011
Tesl Requested
Selectedtest(s) as requestedby client.
TestMelhod
Pleasereferto nextpage(s).
TestResult(s)
Pleasereferto nextpage(s).
Conclusion
A: Basedontheperformed
testsonsubmitted
sampte(s),
thereslltscomply
withtheRoHSDirective
2002/95/EC
anditssubsequent
amendmenls.
Signedfor andon behalfof
scs-csTcLtd.
Manson
Yang
ApprovedSignatory
,trbkarlldef.(hdrcr"rbfr
rdelfure!|.rbtn-
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Test
I eSI Report
nePOIl
No.:czi 10j0j 0693/CHE|,,
Date:FEB09,2011
pago2 ot
TeslResults:
Description
forspecimen
1 : Coppercolored
surfaced
melalsheet
A: RoHSDlrectiv. 2002/95/EC
Test ltem(s)
Cadmium(Cd)
Lead (Pb)
Mercury(Hg)
HexavalentChromium(CrVl)by
boilingwaterextraction
Sumol PBBS
Monobromobiphenyl
Dibromobiphenyl
Tribromobiphenyl
Telrabromobaphenyl
Pontabromobiphenyl
Hexabromobiphenyl
Heplabromobiphenyl
Octabromotiphenyl
Nonabromobiphenyl
Decabromobiphenyl
Sumof PBDES
Monobromodiphenyl
ether
Dibromodiphenylether
Tdbromodiphenyl
ether
Tetrabromodiphenyl
ether
Pentabromodiphenyl
ether
Hexabromodiphenyl
ether
Heptabromodiphenyl
ether
Oclabromodiphenyl
ether
Nonabromodiphenyl
ether
Decabromodiphenyl
ether
Unii
Tesl Method(Reference)
mg/Kg
MEKg
mgKg
lEc 62321:2008,|CP-OES
IEC62321:2008,ICP-OES
IEC62321:2008,ICP-OES
IEC62321:2008,UV-Vis
mqikg
mg/kg
mg/kg
MEKg
mg/Kg
mgKg
MEKg
mgKg
mgKg
mgKg
mqKg
m9Kg
ms/Kg
ms/xs
me/kg
m9xg
MEKg
msI(s
mg/kg
mgn(g
mgas
msftg
[4DL Limit
N-D.
2
100
N.D,
2
1000
N.D.
2
1000
Negalive
o
#
N.D,
1000
N.D.
5
N.D.
5
Resull
IEC62321:2008,
GC-MS
tEc 62321:2008,
GC-MS
IEC62321r2008,GC-MS
tEc 62321:2008,GC-MS
tEc 62321:2008,GC-MS
IEC62321:2008,GC-MS
IEC62321:2008,GC-MS
IEC62321:2008,GC-[4S
IEC62321:2008,GC-l,,rS
IEC62321r2008,GC-IVS
N.D.
N.D.
N.D.
N,D.
N,D.
N,D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D,
N.D,
N.D.
N.D.
N.D.
N.D,
N.D,
N.D.
IEC62321:2008.GC-l'rS
IEC62321:2008,
GC-MS
IEC62321:2008,
GC-MS
IEC62321: 2008,GC-l',lS
lEc 62321:2008,GC-[,|S
IEC62321:2008,
GC-MS
IEC62321:2008,
GC-MS
IEC62321:2008,GC-I,I|S
IEC62321:2008,GC-lllS
IEC62321:2008,
GC-MS
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Test Report
No.:GZl 101010693CHEi,/l
Date:FEB09,2011
Page3 of I
Note:
1. mg/kg= ppm
2. N.D.= NotDetected
l< MDL)
3. MDL= MethodDelection
Limit
4. O = Soottest:
= Absence
Negalive
= presence
ol CrVtcoating.
Positive
ot CrVtcoating:
(Thetestedsampl€shouldbefurlherveifiedby boiling
walerextraclion;ethod
it thespottestresultis negative
or cannotbeconfirmed.)
Boiling
walerexlraction:
= Absenc€
Negalive
ol CrVlcoatinq
Posilive.=
Presence
of CrV.I
coating-i
thedetected
concenlration
in boilingwaterextraction
solution
is eqlalor
grealerthan0.02mg,/kg
with50cm'sampte
surface
area.
Storageronditions
andp.oduction
dateofthetestedsample
areunavailabte
andthusresultsol C(Vl) repres€nt
statusof thesampleatlhetkneol testing.
5. # = Positiveindicalesthe presenceof CrVlonthe testedarea.
Negativeindicatesthe absenceof CrVtonthetestedarea.
6. "-"= Notregulated
Br PFOA& PFOS(P€rtluorooctanotc
acid & porftuorooct.nosu[onates)
Testltem(s)
Perfluorooctanoicacid(PFOA)
Perfluorooctane
sultonates(PFOS)
PFOS- Acid
PFos - Metatsatt
PFOS-Amide
Unit
tdm'
Test Method{Reference)
EPA3550C:2007,LC-I,S
Result
N.D.
MDL
1
!g/m
EPA3550C:2007,LC-MS
N.D,
1
Nole:
1. mg/kg= ppm
2. N.D.= Nol Delected(< MDL)
3. MDL = lrethod DeleclionLimit
For reference:Enlry53 of Regulation
(EC)No 55Z2OO9
(EC)No
amendingAnnexXV ot REACHRequlation
1907/2006(prsviously
restricledunderDir€ctive2OO6|12ZEC)|
{1) lray not be daced on the markeloausedas a substanceor conslituent
of preparalions
in a crncentrationequallo
or higherthan0,005% by mass.
(2) May not be daced on the rharkelin semi-linished
productsor anicles,or partsthereof,il the concentration
ot PFOS
is equalto or higherthan 0,1%by masscalculated
with reference
to the massof structurally
or micrcstructuratty
distinci
partsthat containPFOSor, for textilesor othercoaiedmaterials,iflhe amountof PFOSis equalto or higherlhan.tpg
/m'?ofthe coatedmate al.
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SGS
Test Report
No.:G21101010693/CHEI
Date:FEB09, 2011
Page4 o{ 9
C: Halooen
Test llern(s)
Fluorine(F)
Chlorine(Cl)
Bromine(Br)
lodine(l)
LJnit
mg/K9
MEKg
m9r(g
Tesl Method(Reference)
BS EN 14582:2007,
lC
BS EN 14582:2007,
lC
BS EN 14582:2007,
lC
BS EN 14582:2007,
lC
Result
N.D.
N.D,
N.D,
N,D.
MDL
50
50
50
50
Unit
m9xg
Testl\rethod(Reterence)
EPA30508:1996,ICP-OES
Result
N.D.
lllDL
10
ms'4<s
Nol€:
1. mg/kg= ppm
2. N.D.= Not Del€cled(< [,tDL)
3. MDL= MethodDetectionLimit
Dr ElementaavAnalvsls
Tesl ltem(s)
Anlimony(Sb)
Notel
1. mgr'kg= ppm
2. N.D.= Not Detected(< tuDL)
3. MDL= MelhodDetectionLimit
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scs
TestReport
No.:GZ11010106931/CHE[.,1
D ate:FEB09,2011
page5 of
ATTACHMENTS
BoHSTes ng FtowChad
1)Nameot thepersonwhomadetesting:
BellaWang/ Cuteyyu / RossZhan
2) Nameol thepersonin chargeol tesling:
Adamsyu / Ryanyang
J) | nesesamptes
weredissolved
lotallybypre_condilioning
method
according
to belowflowchan
(Cr6+andPBBsi/PBDEs
testmelhodexcludeo).
Pb/Cd/H9
PBBS,/PBDEs
Concentration/
Dilltionof exlraction
s0luton
Negalive
Heatang
to
90-95'Cfor
exlraclion
1)AlkaliFusion/
DryAshing
2) Acid lo
dissolve
Adding1,5diphenylcalbazide
Adding1,t
diphenylcarbazide
indical€sthe
presence of crer. lf
t ', tubr|'
r.d.e'soqcbt
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d
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Test Report
No.:GZl 101010693/CHEM Date:FEB09,2011
Page 6 of I
ATTACHMENTS
PFOA/ PFOSTaningFtowChart
1)Nameof thepersonwbo madetesting:CindyHliang
2) Nameof thepersonin chargeol testing:RyanYang
Samplecutting/ preparation
SampleMeasuremenl
Solventextraction
Concentration/Dilulioh
Fillfation
LC-MS
DATA
bd&l!gM.bu@
idt/tD,F|a|[email protected]|6hhllec
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'I
Test Report
No.:czi 101010693CHEM Date:FEB09, 20i l
Page 7 ol I
ATTACHMENTS
HalogenTestingFlowChart
1) Nameof the personwho madelestingrLiangWang
2) Nameof the personin chargeof testing:Michette
Song
Samplecutling/ preparation
Samplel\,leasurement
Combustion
in orygenbomb
Dissolvedin an absorplionsolution
Analyzedby ion clromatography.
Doubleconfim by other
instruments,
if necessary
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TestReport
No.:czl 101010693CHEI, Date:FEB09, 2011
page8 of
ATTACHMENTS
Elementary
TestingFlowCharl
1)Nameof thepersonwho madetesting:BellaWang
2) Nameof thepersonin chargeof testing:AdamsYu
Sampiecuting/ preparation
SampleMeasuremeni
Aciddigestion
Filtration
Solution
lcP-oEs/Ms
DATA
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scs
TestReport
No.:GZl 101010693l/CHEM
Dale:FEB09,2011
PageI of I
Samplephoto:
SGS authenticate
Ihe photoon originalrepononty
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TestReport
No.SHAEC1100514403
Date:18Jan2011
Page1 of 13
Horaeus
(Zhaoyuan
Co.,Ltd/He€eus
)l\IelatMatedals
Zhaoyuan
(Changshu)
Electronic
Materiats
Co.,Ltd.
M 238-Linglong
Roadzhaoyuan
shandong/Huangpujiang
Road,changshusoutheast
Economic
Deveropmenr
Zone,Changshu,
Jiangsu
Thefollowing
s€mpre(s)
was^/vere
submitted
andidentified
onbehalfof theclientsas : coLD BONDTNG
wlRE
HD
SGS Job No. :
- sH
sP11-000807
DateofSampfeReceived.
12 Jan2011
TestingPeriod:
TestRequested:
12Jen2011- 18Jan2011
Selectedtest(s)as requestedby ctient.
TestMethod:
Pleasereferto nextpage(s).
Pleasereferto nextpage(s).
TestResults:
Basedon the performedtestson submittedsamples,lhe resultscomplywiththe
RoHSDireciive
200295/EC
anditssubsequent
amendments.
Conclusion
:
Signedfor and on behalfof
sc$csTc Ltd.
,.Qr,-
Fan Jingjie,JJ
Approved Signatory
nrd@tud
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TestReport
No. SHAEC1100514403
Date:18Jan2011
Page2 of 13
TestResultsI
TestPartDescriotion:
Sp€dm€.1No. SGSSamplslD
De6qipdon
1
SHA11-005.144.002
Gotdenmetatwire
Remafts:
(1)1 mg/kg=1 ppm=0.000i%
(2)lrDL = MethodDetection
Limit
=
(3) ND NotDetected( < ttDL )
(4) "-" = NotRegulated
RoHSDir€.lh€ 2002105iEC
TestMethod: Wth reference
to IEC62321:2OOB
( 1) Determination
of Cadmium
by tCp-OES.
(2)Detemination
of Leadby tCp-OES.
(3)Determination
of Mercury
by tCp"OES.
(4) Determination
of HexavalenlChromiumby Spottest/ Colodmetric
MethodusingLIV_Vis.
(5)Determination
of PBBS/ pBDEsby GC_MS.
Test ltem{s)
Cadmium(Cd)
Lead(Pb)
Mercury(Hg)
Hexavalent
Chromium(CrVl)
Sumof PBBS
Monobromobiphenyl
Dibromobiphenyl
Tribromobiphenyl
Tetrabromobiphenyl
Pentabromobiphenyl
He/€bromobiphenyl
Heptabromobiphenyl
Octabromobiphenyl
Nonabrcmobiphenyl
Decabrcmobiphenyl
Sumof PBOES
Monobronodiphenyl
elher
, !r rb orrdr
ui!
uot
100
1,000
1,000
mg/kg
1,000
mg/Kg
mg/Kg
mg/Kg
m9Kg
mg/Kg
m9Kg
mg/Kg
mgKs
ms/Ks
mg/Ks
ms/Ks
mg/Ks
mg/xg
2
2
2
O
-
N
D
N
D
N
D
Negative
N
D
5
5
5
5
5
5
5
5
5
5
-
N
N
N
N
N
N
N
N
N
N
N
O
D
D
D
D
D
D
D
D
D
D
5
N
D
tbi!
1,000
mg/rg
'n:*
ap2
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h cmn/.
[r rE || cr.d sd Nr emd
dql id s;;r
.nc on.{.6
rfr ,.(.tB.c
3'drnon!.syrFto dlilet4ll'dioft
$l '!l .*[grdra€lei€tt
l|:
ao@39
2@e
hry h hncuad
ro th. turdri rd.d d rh. rs
IEE[6-e1)61160lElEFqFd9S'tg
m.s4]s
..F.d'|Or.@
HJF46l{dzna
illiid-alFael
M.nber ol |noSOSg|!Up (9gg SA)
TestReport
No. SHAECl100514403
Test ltem(s)
Dibromodiphenyl
elher
Tribromodiphenylelher
Telrabromodiphenyl
ether
Penlabromodiphenyl
ether
Hexabromodiphenyl
ether
Heptabrornodiphonyt
ether
Octabromodiphenyl
elher
Nonabrcmodiphenyl
ether
Decabromodiphenyl
ether
Date:18Jan2011
!rni!
Udt
_
-
uDt
aa
mg/Kg
mgKg
mg/Kg
mg/xg
mg/Kg
mgKS
mgKg
ngKg
mgKg
5
5
5
5
5
5
5
5
5
ND
ND
ND
ND
ND
ND
ND
ND
ND
-
Page3 of 13
Notes:
(1)Themaximum
permissibre
rimitasquotedfromthedoorment
2oot618/Ecamending
RoHsdirective
2002t95tEC
(2) SPot'test:
"
Negative= Absenceof CrVlcoating,positive= pres€nc€of CrVlcoating;
Thetestedsampleshourdbe furtherverifedby boiring-water-extraction
methodif the spottest resurtis
Negative
or cannotbeconfirmed.
o Boiling-water-exfaction:
Negative= Absenceof CrVtcoatingi positive= presenceof CrVtcoating
Thedetectedconcentration
in boiling-wateFextraclion
solutionis equalo. greaterthan0.02mg/kgwith
50 cfir' s€mplesurfacearea.
For@nodonprotectioncoalingson melals:Information
on storageconditionsandproductiondateof
the testedsampleis unavailabte
andthusrcsuttsof Cr(Vt)representstatusof the sampteat the timeof
testing
Helooon
TestMethod:Wth reference
to EN 14582:2007,analysis
wasperfomedby tonChromatograph
(lC).
Test ltem(s)
Fluorine(F)
Chlorine(Cl)
Brcmine(Br)
lodine(l)
ud!
MDt
50
mg/Kg
mg/Kg
mg/Ks
mg/(g
50
50
50
0!2
ND
ND
ND
ND
Ebm€a 8)
Test l\,lethod: With r€ferenceto US EPA l,I€thod 30508:1996,analysiswas performedby lCp-OES.
tnLdodb.&-brirrcdF
*ilffi
rrr{.dbhorrJcq!ct{..rrjyk
rdda@&rr{lltrdrcu.dq
.Hiffi1.ilsf.H:*3ffit-ffi,i:,?ffi
h.!ubF. rB.
I|4!1l.9!!F*q!ntf!dqd
dld.i'
!D.c-r!
! qlw|r.m
d!.',4
Df ulI||'!E..ERr,
riffihddlrdrnf
n c{nll
drbb|mr|n.)rnhd.
t-ttlrnarrblbdpnr$4trEtt'dl|
+!.t1.*rqtdrl@|'3ttl
g
:,flffi
d. ruB{'rv.cdc{ds
&.lm{[email protected]
2@3
al.2@3
rn.brhdM
d.tr m., r. pnrgb.!.ri.tui.ii.
rEl€F+r)31l02A tErE{6-AF466r9
ft.o4.6
Hlj(&-?116r/t(e5D(
. {.drrcrs.s
HL|s-2r)5|606
Monb.r oiin. SOS9lo!1 (soA al)
T€stR€port
No.SHAEC1100514403
Testltem(s)
Anlimony(Sb)
sb,o:.
(P)
Phosphorus
Date:18Jan2011
ud!
uot
mgKs
10
12
20
ms/xs
mS/kg
Page4 of 13
@
ND
ND
ND
Notes:
(1). Calculatedconcentraljon
of Sb,O. is basedon the identifedSb
HeEbomocrdododecanefi BCDDI
TestMethod: Wth referenceto EpA8270D:20o7.Analysis
wasperformed
by GC-MS.
Testltem(s)
Hexabromocyclododecane
(HBCDD)
!d!
mS/kS
ust
'10
a@
ND
Ph0|elat€6
Test[,!ethod: Withreferenceto EN14372:2004,analysiswas
performed
byGGlrS.
Testltem(s)
Dibutyl
Phthalate
(DBP)
aenzylbutyl
(BBP)
Phthalate
Bis-(2-ethylhexyl)
Phthatare
(DEHP)
!d!
%
%
%
MpL
0.003
0.003
0.003
0@
ND
ND
ND
Notes :
(1) DBP,BBP,DEHP
Referenceinformation:
Entry51 of Regutation
(EC)No SS2J2OO9
amendingAnnex
XVll of REACHRegulation(EC)No 1907/2006(previousty
reshictedunderDir€clive200584/EC):
i) Shallnot be usedas substancesor in mixtures,in concentrations
greaterthan 0,1 % by weightof
the plasticisedmaterial,in toys and childcareartides.
ii) Toys and childcarearticlescontainingthesephthalatesin a concenfatongreaterthan0.1 % by
weight of the plasticisedmatedatshatl not be ptacedon the market.
Please refer to Regulatjon(EC) No 552i2009to get more detail information
T€feb|l,n|ot isph€.lol A fiBBPdI
Test Method : With referenceto t-JSEPA 3550C: 2007, anatysiswas pertormedby GC-MS.
rybtu'h.r.&)6nd
3.Ettl(afi0tudxrrurt{i.Ciorr
+l..tl.*E[lr!i€€o!s
r
l*@
20@3|
lE!E{6-q)611@ lE!€(iaF.95S'r!
tu|6-A)6|.@,44 iu{E-?lFaffi
ffq4|..{.n
. l.d'do'te
(scs8A)
.|n!orotth€soscmuD
TestReport
No.SHAEC1
100514403
Testltem{s)
Telrabromobisphenol
A OBBP-A)
u!!!
mdkS
Date:18Jan2011
MpL
a02
10
ND
Page5 of 13
PFOSlPertuoroodan6Sutbnat 6l
TestMethod: With.eferenceto US EpA 35SOC:
2007,anatysiswesperformedby HPLC_|VS.
Testltem(s)
Perfluorooclane
Sulfonales
(PFOS)andretatod
Acid,Melal
SaltandAmide
ud!
Mot
002
mgkS
10
ND
Notes :
(1) PFOSReferenceInformation:
Entry53 of Regulation
(EC)No 552/2009afiendingAnnexXV of
REACH Regutation(EC) No 1907/2006(previoustyrestrictedunder Dheclive 2OO6/12ZEC)
(i) May not be placed on the ma*et or us€d as a substan@of constituentof preDaratonsIn
a
concentrataon
equattoor higherthan0.005% by mass.
(ii) May not be ptacedon the ma*et in semi-fnished productsor articles. or parts thereof, if the
concentration
of PFOSis equalto or hjgherthan0.1 % by massc€tcutated
with referenceto the
mass of struc*urallyor microstrucluraltydistinct parts that cont€in PFOS or, for textiles or other
coatedmaterials,if the amountof PFOSis equalto or higherthan 1Ug/m2of the coatedmaterial.
Please refer to Regutation(EC) No 5522009 to get more detail information
t\E!,b.Gllrbdetuqi9l5rtiorr
$l .-tl.iE8ldrt€@lrrl
20@
l*
2o@s
rE!€{s-sr)6t461 tElE(6{rFggD
irr (6-2r)!r4@!aa&{ft-a[.{r!a
ffq-.0.6
. rFdir€{.@
r&Ir$or ol ti! SGSGrou!(3gg SA)
TestReport
No.SHAEC1100514403
Date:18Jan2011
Page6 of 13
ATTACHMENTS
RoHSTestingFtowChart
t) N€meof thepersonwhomadelesting:AltenXiao/WesleyWei/ AndyZhao/EhmLin
z, Nameorthe.person
Inchaage
oftesling:JeffZhang/George
XdTracyyue
r) | nese_sampes
weredissotved
totallyby precanditioning
methodaccording
to belowflowchart.(Cr5*
andPBBdPBDES
testmethodexctuded)
Pb/Cd/Hg
PBBs/PBDEs
Acid digestion with
microwave/ hotplate
Concenkation/
Dilution
of extraction
solUtion
'1)AlkaliFusion
/
DryAshing
2) Acid to dissolve
Adding
1,s
diphenylc€rbazjde
forcolor
development
Db dod
b -!@ d,ib!4!hb
br h cqFr,
hx
dM,rucd
!q.d
dtnritu.s*xhM
lltEri.dtsturucrhhffi
ll!. r6t..yd*hdb
hN
rJll nub.i.s
b h Gild
c.idrd.
b rhr
N c4i@
d I
k
E
&r icdr.r h tuh.d
dircd
dnrde
r.ded
mr .&.!m*ni6_
Mii6tuaiEffiiii.iffiiiE
Addingl,S
diphenylc€rb€zide
for@lor
development
A .edcolor
indicatesthe
presenceof cr6'. ff
necessary,
confirmwith
Ai-6r_I-t'l-
F-6FEMi
' | l 8 ' r r l c . | b y r E | . I . B s n d g d | n L d e ' b . h r d o
tu.rturdn.co4{iy
,.jd.^dd.id..
nr, b. F-cqi..b'i.tu|;i.dh'd
tbJEgrbtrrre.dIrnLI4trlritotr
+t.rjl.*Eat&l€3ol3tt
2@39
tr:M3
rEl€6?r)6l02rs3 lE!€{6-21r/|l56'l
HL{s-2ll6fie!41 hlj{6-a)6ffi4
h. Lt
n6.&.m
.{rd*r€S6
vonberotih€sos GouP(sgs aA)
TestReport
No. SHAEC1100514403
Page7 of '13
Date:18Jan2011
HalogenTestingFlowChart
1) Nameof the personwhomadetesting:
DaisyGong
2) Nameof the personin chargeoftesting:Alex
Jiang
Samplemeasuremenl
Combustion
in oxyg€nbomb
Dissolved
in anabsorption
solution
Analyzed
by ion
chromalography.
Doubleconfirm
by otherinstruments,
if
dbr rb 6rFit r'lqd b r. o-"
c.nd{s. or&rn6 Dniw ov.rr.r, .
k|fu'
d|flr do6r4r{dbrd.
6a@r{dbrdr
rr
Fr
fr.{.4bhr...dihi,
fr.s.dbhr..oMitiir-Affidr-hr
rd ludre
!.qd.hd
rxs, Ad r.lrde
]|.gfr,r h *{d
hrirb.idd
r'.hr.doD. r@. nio.lluyr
ni6o''uyl
!b sM.5
sr6.5ut r lrb
!|nrhhhrr.rllr6rr
oco.llo.rd.ltlt0Nn
ordbna@itslr,ft1.lbdmrn{iiotb.
Id
d6
rhh r'r'bb.
nrd -rr flrt b tu 3.hpr.t) brbd
tttg|leYdntod)Ori0al4strriorr
+! .-tl .*E8ltft89lotl
20@39
al. 2Mo
6dldc
or.io.tr
h..{
'ad
r.r o. mteid
Affi4-dan,
ft
t-Flffir'fot
d.r' r |bmdib.hEdd
ibre-b.rflEdd
|n(rDDB.Iolh.connny
b 'i. rlrbi .fur d h. rn
lalEls-sl)dt46ll€18163F.05$'n
H!(&-21)et@!4. Hlr{I6-aF1@a
lw6..o.m
..F.diro4Am
M.nDofolfi€SOSGoup(SGSS )
TestReport
No.SHAEC1100514403
Date:18Jan2011
Page8 of 13
ElementaryTestingFlowChart
1) Nameof the personwhomadetesting:Wesley
Wei/ AllenXiao
2) Nameofthe personin chargeof testing:
JeffZhang
Samplecutting/prepa€tion
'^rffFEHff,?H*"sffi
*-,.#,ruffi
.r'#ilf
#*#mffi
!fi s,6i$ff
d!!F$.q!
h !'1|n
FrtFn!"
etud
i bud
n'lEfl4ru!.wnndd
EW!!'tf,F.'r-"
br 'b 6EFrr
r4.d
qd
b r.dr
$r c.i.'@
k tu
!. ht. rr.dm{{iir't
t br[..h.r.i.,
I'A/tn9beY|qicd&ni|lt1sirfi
Sl .-tl . *trAlddl689+r9!
bhr
Orr 20@33
ll
2@3
b. DEdad
tffi
i
n'./hF!,aidbh.rrrbifrtdfrr,tu
tElE{&-gl)61.6
Hj(a+ll6!10211
tEl€l6-aba95$1!
HL{n-al)5adldl!
ff6.0.6
..(rdtrrer$m
ir.rilcr oflnsSOSOmup(SGS8A)
TestReoort
No.SHAEC1100514403
Date:18Jan2011
PageI of 13
HBCDDTestingFlowChart
1) Nameof thepersonwhomadetesting:BillZhong
2) Nameof the personin chargeof testing:
SusanLiu
Concentration/Dilution
nbdod
|&.qbyibco{@
rbd.b..dyF*;x
!!t
d b !r osd
d;ffii.;;ii{;i;;;fta;ie&
c.dd.d6.ndo
ad,s,. ooa*i d,*&.-*m.tu'idffiffii#,!ft##ffi
tuif
'rrfr
dMn-|fu-Ftfi
Non
dfulhtrbdtdnPdd.*
tbng|5iollDto
SI 'It.
dxlhllst1llldoir
*ir8l tft8ef3€t
2rq33
ltr2Mg
i6F;iu
hc4../.
idhF
dbhd
{.6n.rrrnE*a.rcrh.Mkindbn'ds.rh.
t EIE(s-al)611@5a
lEa€(&-A)649Stg
m.o.!.@
rL{&.21J6ra0Zn4irL{6-t)5a@
..9sdiE€r.6
MonUofrh€so3ooup(sossA)
TestReport
No.SHAEC1100514403
Date:18 Jan 2O1t
Page10of 13
PhthalatesTestingFlowChan
1)Nameof the personwhomadetesting:
VickeyGui
pe6on
2) Nameof the
in chargeoftesting:Susan
Liu
Samplecutting/prepa€tion
Samplemeasurement
rt
6
dumd.
dlg!!!g'd
tud
b, tb c.nF
-.t
wd
edBu,lqd
d b t o-ar
cdtlJorr dlwl
i bd. $t coiordF rr
.hJ.t
E. f a.
hr .<ddtfr,
I6nni-idnEiFFlffi.n
oi
.iM|.dldh|o.dd6d/m.h.M
nr conryt
b
iy b rb 'hFr.{.t
drr
t'AanE|n.OYlstodhtud!4siCrCl.t
+! .l,|.ltrArdt!€€o||e.}t
l*
nr*dry
dn oiic
r@90
ea
r.b b cr.d 6d B d4Mrds
b. FrE |lda .^ap! h nljdnE4
nd noirab drd.!_b. h-6d
ra iftr
&DMd or m. con{N
rElE{6-a)0s02563
rE!E&-4tr{6$',D
Hlj{E+1)614@!,aHl{ft-2rFaaEt
ff !n..!!..!,n
.rFdi€s@
(sGgs)
frrnboroffE
soseouc
TestReport
No.SHAEC1100514403
Date:18Jan2011
Page11of 13
TBBP-ATestingFtowChart
1) Nameof the personwhomadelesting:Garyxu
2) Nameof thepersonin chargeof testing:
TracyYue
Samplecutting/preparation
Samplemea6urement
Liquidliquid
exraction
r br rb hpvrq.d
.id n'd.!rd-
b I ohnr
kslbn'.i
c.dusr
or!rn6
rft
.Eh''
dr.Eri.
Bd.dh.odds.c4.l'
rrbrb..n.r.(r)u.bi
3'Ettrbngl|sto
dtll|l're4g,iirort
$t .-t,| . *JEAltftretsBl
lli
2qnag
2M3
tElrF2l)6la@lElE(fi-n)04S3qtg
Mo..!.@
.l$inir€Erd
t{j{b-21)6la02l{ ill{S-A)5a&@
ilomlarol lnsScSOrcup(SOSSA)
T€stReport
No.SHAEC1100514403
Date:18 Jan 2011
Page12 of 13
PFOSTestingFtowChart
1) Nameof the personwhomadetesting:
JudyLi
2) Nameof thepersonin chargeof testing:NanryDu
Concentration/Ditution
lrtd
b tr csar
oord{s.
or$d6
[email protected]
dd|$huld'uf,'.6tc'{
'e'r,4ltdd|oid!\.d,i
ElbrimhEbdnpdDrrdrrbib
slt$5lcr96icdxlhti$4grtlioh
+l.Il.ltrEltl88g+st$
.dfr
r.hr.(.)bbc
20(493
ll:a@3!
a!.ntr.rh
m.Rad
rorh. Mknd.n'd
l$€66-al)61a60
lE!E(6-5)64€!!dt9
t(6-21161402514 lt(FzlFl5llllll
6. rtu.
md..!.ff
..9tdir€.*6
Momlolof |ns sG3 GrouoISGSSA)
T€stReport
No.SHAECl100514403
Date:18Jan2011
Page13 of 13
Samplephoto:
sHA1l-0051,t4.002
SGSauthenticate
thephotoonoriginal
reportonly
"' Endof Report*-
Iftdoftdl.buntn
tb r'4,n, ,lFrll!
c.n!..t rrld
bmd @i|d,n!ld
b l. CrElod$q.
d!.
b
brmr
rmr ''rt coi.fte
Lr
'y b tu rhPL(r,
t'it$|5,tor|ue.dnirrhilshdaorr
'il'.t,|.liEAtdrl€setttl
o.*Mb
r tu
dhd
i [email protected]
r,qtrhmr.{oetuidi',
.-doetu|ffi,
hEffi
iF6ffi
iiiF;da-h
rffi'
rE 'i r. cd6 tr b lffir.n
c@ jri
nBd
{ h h
c
c
.
2O@O
l|:zolag
rEIEF{r)6ra@ laf (&aFas6D
RJ{6.r1)6r4029a'i!{6-?l)5adK
fficr.{r.!n
.rydn€$@
M.nlor ol tn€SGSOmup(SGsSA)
TestReport
:2O10h1115 P a g e : 1 o f 2 6
No.: CEl2010/82266Dar'.e
rlllllllulllll|lr]l
HENKELCORPORATIOp
IRVINE
CALIFORNIA'
ROAD,
14000
JAMBOREE
MAIN
OFFICE:
HENKEL
ADHESIVES-ELECTRONICS
92606U.S.A
Thefollowingsample(s)was/weresubmlttedand identlfiedby/onbehalfofthe cliontas:
SampleDescription
No.
Style/ltem
Date
SampleReceiving
TestingPerjod
ADHESIVE
84-1LMlSR4
2010t11t11
11115
2010t1 l | 1I r o 20101
TestRosult(s)
Pleasgreferto nextpage(s).
Sfnad fo. .||d
OrdiLJ
Lhorrbay
conDany !t
ft"4'1.*,
i!
Frl.
g,s*
-TdFd
L rl'
til.'+?:li
;ti,l,!
jr i
1ri
:i;lrlr.
byo" c-'a
.d".^r*r-."d!*dd-'*63i
,i",i-a *r r" i." a o*. *rtud6", -y
r'i,,s'r -a" o e'o* -d., u" *"
o,s"d. r,bnd;" a o. .nd .
. c"hpa^vs sd",*
per3lrsd6d frs b$ repod6oior be
li ::r:,1'!!t
lr r
"
TestReport
No.: CE/2010/82266Dale| 2010111115Page.2ot26
lllllllltlllllllllll
HENKEL
CORPORATTON
ROAD,
lRVlNE,
CALIFORNIA,
14000
JAMBOREE
MAINOFFICE:
ADHESIVES-ELECTRONICS
HENKEL
92606U.S.A
Test Result(sl
GRAYPASTE
PARTNAMENo.1
Testltem (s):
Unit
Method
Withreference
to IEC62321:2008and
p€rtormed
by ICP-AES.
mg/Kg Withreference
to IEC62321:2008and
perfomedby lCPdES.
mS/kS Withreferenceto IEC62321: 2008and
performed
by ICP-AES.
to IEC62321:2008and
mg./Kg Withreference
performedby UV-VIS.
mg/Kg With referenc€to US EPAlrethod
Analysis
Content.
30508for Beryllium
wasperfomedby ICP-AES.
mgikS with referonceto US EPAMethod3052
tor Antimonycontent.Anaiysiswas
perfomedby ICP-AES.
mgftg With referenceto US EPA3g0C
wEsperformed
by
method.
Analysis
GC/MS.
mdks With ref€renceto US EPA3g0C
wasperformEd
bY
method.
Analysis
GC/MS.
toL
R€6ult
2
n.d.
2
n-d.
2
n.d.
2
n.d.
2
n.o.
mgikg
Cadmium(Cd)
Lead (Pb)
Mercury(Hg)
Cr(Vl)by
Hexevalent
Chromium
alkalineextraction
(Be)
Beryllium
(Sb)
Antimony
(PcBs)
Biphenyls
Polychlorinated
(CASNo.:001336-36-3)
Naphthalene
Polychlorinated
(PCNs)
to us EPA31oc
(PCTs) mgKg withref€rence
Teryh€nyls
Polychlorinated
tlo.l
n.o.
n.o.
n.d.
0.5
n.d.
bY
Analysis
waspertormed
method.
GC/MS.
Alkanes,
C10-13,chloro(Short
(CAS
Paraffins)
ChainChlodnated
No.:085535-84-8)
PVC
(SF6)(CAS
SulfurHexafluoride
No.:002551€24)
cdoany ;rt,l11rJi.;.Ii]'1:rrillr:l,irrli"+a
0.01
With referenceto US EPA3540C
method.Analy6iswasperformedbY
GC/MS.
Analysiswasperformedby FTIRand
FLAMETest.
1
mg/Kg With referenc€to US EPA5021method.
wasperformed
bYGC/MS.
Analysis
r'ni l:!trii;f:
e(3)r$bd rhG Gd rspodeiidl
r'i:lnilrll!'
+.
iiiJli",l.!'ii ;"!,"jq ;; c*e
.|i'"iiii-"i.*Jiin.*t*!d'oi"*"-dc-dt-"b,€bd-"o;,'*6d*a"-'^
s' 5dv$dsdnemdn
,io'J*rii,"ir"*oa*,**;
-L-.*h...i.bdc,s,s
;i.l';;;;;";;;i".1,";;'i*,
i.;;;,;;,;;;;;
B,
;;"".,;"*"."d*;-6
".
rh';d;.d
-
pdsb 'ri*b
be r€
@d'i&
bcrad"drrsdodm
Jrr t 12:n!
t r+s61tr2!
n.d.
Negative
n.d.
TestReport
No.: CE/2010/82266Date: 2010/11115Page:3 of26
llllllltltlllrlrlll
HENKELCORPORATION
,14OOO
ROAD'
IRVINE'
CALIFORNIA,
JAITBOREE
MAIN
OFFICE:
ADHESIVES.ELECTRONICS
HENKEL
92606U.S.A
T63tltom (s):
Perfluorooclane
sultonates(PFOS)
PFOS- Acid
PFOS- MetalSalt
PFOS- Amide
PFOA(CASNo.:000335€7-1)
Unlt
I'IDL
Method
mg/Kg With reforenceto US EPA3540C:1996
was
Analysis
methodfor PFOSContent.
perfomedby LC/luS.
mg/Kg With referenceto US EPA3540C:1996
wEs
methodfor PFOAcontent.Analysis
perfonnedby LC/MS.
mg/Kg With referenceto US EPA3540C
2-(3,tui-ten-butyl-2method.Analysiswasp€rformedby
hydoryphenyl)-2H+enzotriazole
GC/MS.
(cAs No.:003846-71-7)
(CASNo.:000074- mg/Kg With referenceto US EPA5021method.
Bromomethane
Analysiswasperformedby GC/MS.
83-9)
to USEPA5021method.
(CASNo.:
mlyK9 Withreference
B.omochloromethane
Analysiswasperformedby GC/MS.
000074-97-5)
A9bestos
(CASNo.:077536$6-4)
Ac,tinolite
(CAs
No.:012'172-73-5)
Amodte
(CASNo.:07753647Anthophyllite
%
000688-73-3)
(TphT)(CASNo.:
TriphenylTin
oo0668-34-E)
10
No.1
n.d.
10
n.d.
n.d.
1
n.d.
1
n.o.
Negative
Negative
Negative
to NIOSH9000method.
Withreference
pertormed
by XRD.
Analysiswa6
(CASNo.:0'12001-29-5)
Chrysotile
(CASNo.:01200'1-28-4)
Crocidolite
(CAS
No.:0253668€)
Tremolite
Halogen
(F) (CAsNo.i
Halogen-Fluodne
014762-94-8)
(Cl)(CASNo.l
Halogen4hlorine
022537-1r't\
to Bs EN1458212007.
with reference
mgKg
performed
was
bylC.
Anatysis
(Br)(CASNo.:
Halogen-Bromine
-32-2')
010097
(l) (CAsNo.:
Halogen-lodine
014362-44-8)
O|!anic-tincompounds
to DIN38407-13.
mgKg Withreference
(IBT)(CASNo.:
TributylTin
Result
Negative
Negative
Negatave
50
n.d.
50
173
50
n.o.
50
n.d.
0.03
n.d.
0.03
n.d.
byGC/FPD.
wasperformed
Analysis
to DIN38407-13.
mg/Kg with reference
bYGC/FPD.
Analysis
wasperformed
'tj?j ri i!r
tliI
I trs6lor)'!'
TestReport
Date:2010/11/15Page'.4d 26
No.:CE/2010/82266
llllllMllllllllll
HENKELCORPORATTON
ROAD,lRVlNE,CALIFORNIA'
MAINOFFICE:14000JAMBOREE
HENKEL
ADHESIVES-ELECTRONICS
92606U.S.A
Test ltem (s):
TributylTin Oxide(TBTO)"' (CAS
No.:000056-35-9)
Sum of PBBS
Monobromobiphenyl
Dibromobiphenyl
Tribromobiphenyl
Tetrabromobiphenyl
Pentabromobiphenyl
Hexabromobiphenyl
Heptabromobiphenyl
Octabromobiphenyl
Method
Unlt
Sum of PBDES
5
5
5
5
5
and
With referenc€to IEC62321:2OOA
mg/Kg performed
by GC/MS.
ether
Monobromodiphenyl
ether
Dibromodiphenyl
ether
fribromodiphenyl
ether
TetEbromodiphenyl
5
Pentabromodiphenylether
5
ether
Hexabromodiphenyl
Heptabromodiphenyl
ether
ether
Octabromodiphenyl
ether
Nonabromodiphenyl
eth€r
Decabromodiphenyl
AZO
5
'1):4-AMINODIPHENYL
(CAS No.l
00009247-1)
5
c o m p a n;y1 + l . :
5
5
5
a;.a-"
n.d.
n.d.
n-d,
n.d.
n.d.
n.d.
n.d.
n.d.
n.o,
n.d.
n.d.
n,o,
n.d-
to LFGB82.02-2.
mdks Withreference
I rl' r:i rillr .'lrrrl !r1; illi
i:'.1.,1.':iir
:
r
;j,)'r\'
- l - a . t " u " i . ' s o o E n " * r p 6 i 3 b ] ' j s b 6 c l a d , i d l i 3 d o & m
oq-i" *
n.d.
n.d.
n.d.
n.d.
n.d.
n.o.
n-d.
n.d.
n.d.
Analysisw6sperformedby GC/MS.
to LFGB82.02-2.
(CASNo.:0009mgKg Withr€ference
2)rBENZIDINE
Analysiswasperformedby GC/MS.
87-5)
to LFGB82.02-2.
(CAS mg/Kg Withreference
3):4-CHLORoO-TOLUIDINE
wEsperfomedby GC/MS.
Analysis
No.: 00009569-2)
to LFGB62.02-2.
(CASNo.i mgikg Withreference
4): 2-I{APHTHYLAMINE
Analysis'.li€sperformedby GC/MS.
000091-59€)
(CAS mdks Withreference
to LFGB82.02-2.
5):O.AMINOAZOToLUENE
Analysiswaspertormedby GC/IVS.
No.:000097-56-3)
" o r l . r. c*o
r"i*,].-r
""*"ooy
aooj.*s
."bj
i*
. ro'.,r
"r*o" *r i," -a e*au - ,**i:
,m,.^i
Ros!ll
No.l
n.d.
mg/kg Withreferenceto DIN38407-13.
wasperfomedby GC/FPD.
Analysis
Nonabomobiphenyl
Decabromobiphenyl
MOL
3
n.d.
3
n.d.
n.d.
3
n,o,
3
n.d.
TestReport
No. : CE/2010/82266 D?l.e| 2010111115 Paoe:5of26
N|l[I|
HENKELCORPORATION
IIAIN OFFICE: 14OOO
JAMBOREEROAD,IRVINE,CALIFORNIA,
HENKELADHESIVES-ELECTRONICS
92606U.S.A
Test ltem (s):
Unit
MOL
Method
to LFGB82.02-2.
6): 2-AMINO-4-NITROTOLUENEmg/Kg Withreference
Analysis
wasperformed
by Gc/Ms.
{CASNo.: 000099-55-8)
(CAS
to LFGB82.02-2.
7): P-CHLOROANILINE No.: mg/Kg withreference
Analysi6
wa6performed
byGC/[,S.
00010647-8)
(CAS
mg/kg with referenceto LFGB82.02-2.
8):2,4-DIAMINOANISOLE
Analysis
w€sperfomedby GC/MS.
No.:000615-05-4)
to LFGB82.02-2.
mg/Kg Withreference
9):4,4Analysis
wasperformed
by GC/IIS.
DIAI,i!INODIPHENYLMETHANE
(CASNo.:000101-77-9)
'10): 3,3'-DICHLOROBENZIDINEm9/Kg Withreference
to LFGB82.02-2.
(CASNo.:000091-94-1)
Analysis
wasperfomedby GC/MS.
m€yKg Withreference
to LFGB82.02-2.
11):3,3'-DIMETHOXYBENZIDINE
(CASNo.: 000119-904)
Analysiswa6performedby GC/liS.
'12):3,3'-DIMETHYLBENZIDINE mgftg Withreference
to LFGB82.02-2.
performed
by Gc/Ms.
Analysisv/as
{CASNo.r000119-93-7)
mg/Kg Withreference
to LFGB82.02-2.
13):3,3'-DIMETHYL-4,4
Analysis
wEsperformed
by GC/MS.
DIAMINODIPHENYLMETHANE
(CASNo.:000838-88-0)
(2-METHOXY-Smgikg Withrefe.ence
to LFGB82.02-2.
14):P-CRESIDINE
performed
(CAS
Analysis
\r€s
by GC/MS.
I,ETHYLANILINE) No.:
00012G71{)
(2to LFGB82.02-2.
mdkg Withreference
15):4,4-METHYLENE-BIS(CASNo.:
wasperformed
by GC/MS.
Analysis
CHLOROANILINE)
000101-144)
(CASNo.: mlyKg Withreference
to LFGB82.02-2.
16):4,4'-O)(YD|ANILINE
performed
Analysis
was
by Go/[IS.
000101-804)
(CASNo.: mg/l(g Withreference
to LFGB82.02-2.
17):4,4'-THIODIANILINE
wa6performed
by GC/MSAnalysi6
ooo139$!1)
to
LFGB
82.02-2.
(cAs
m9Kg
With
reference
No.i
18):O-TOLUIDINE
Analysiswa6perform€dby GC/MS.
000095-53-4)
to LFGB82.02-2.
19):2,4-TOLUYLENEoIAI\4lNE mg/Kg Withreference
Analysiswasperfomedby GC/MS.
(CASNo.:000095-80-4
20):2,4,s-TRIMETHYLANILINE mg4(g With referenceto LFGB82.02-2.
Analysis
wasperfomedby GC/MS.
(CASNo.:000137-17-7)
to LFGB82.02-2.
(CASNo.:
mgKg Withr€ference
21):O.ANISIDINE
Analysiswasper{orm€dby GC/IVS.
000090-04-o)
II![I|I!
Result
No.1
3
n.d.
3
n.d.
3
n.d,
3
n.d.
3
n-d.
3
n.d.
3
n.o.
3
n.d.
3
n.o.
3
n.d.
3
n.d-
n.o,
n.d.
3
n.d.
3
n.d.
3
n.d.
pels) lesEd htr re$ repode^ior b6
'i:r,lrt9:'
c o m p . n y ; 1 , ! , l r : l j l . tr i ' 4 r r + i l i ; ! . r ) r l " i l F r r d ' r r r ' r i l : i i ; ' : :
irisiro*'*r',*eo uyr,oc.'m
5 dQwi ro rheim{aronor ab't
i- .,""r"" L-d dd*."6
",rr
"
.d"."i.i--de*dd-,**.;
-,ma*"o.i.*acun"*rfud6gl.nyrecompanys6o]6Gs
rei,,gns-a oLq'ore *o, t" m
o $a ond rorse^/'o oHrd;n
:i:r:,i r!:r.\J
i ''s6{or,e
TestReport
No.: CE/2010/82266Datei 2010/11/15 Page: 6 of 26
l[llllllllllllll]r
HENKELCORPORATTON
ROAD,lRVINE,CALIFORNTA'
JAMBOREE
MAINOFFICE:'14000
ADHESIVES-ELECTRONICS
HENKEL
92606U.S.A
Te€t ltem (s):
Unit
MDL
Method
(CAS mg/Kg Withreference
to LFGB82.02-2.
22):P-AMINOAZOBENZENE
Analysis
w€sperfomedby GC/MS.
No.:00006M9-3)
to LFGB82.02-2.
(CASNo.:
mdkg Withreference
23):2,4-XYLIDINE
performed
was
by GC/MS.
Analysis
00009568-1)
to LFGB82.02-2.
(CASNo.:
mg/Kg Withreference
24):2,6-XYLIDINE
by GC/MS.
Analysis
wasperfonned
000087€2-7)
CFC's(Chlorofiuo.ocarbons)
GroupI
to IJSEPA5021method.
mdkg Withreference
1 (CASNo.:
Chlorofluorocarbon-1
performed
by GC/MS.
Analysis
was
000075€9-4)
(CASNo.:
mg/Kg With referenceto US EPA5021method.
luorocarbon-12
Chlorof
Analysis
wasperlomedby GC/MS.
000075-71€)
to US EPA5021method.
(CAS
With
reference
No.: mg/kg
I3
Chlorof
luoroca6on-1
perfomed
by GC/MS.
Analysis
wa6
ooo07+1!1)
to uS EPA5021method.
mgkg Withreference
14(CASNo.I
luorocarbon-1
Chlorof
performed
by GC/MS.
Analysis
was
000076-14-2)
15(CASNo.: mg/Kg With referencato uS EPA5021method.
Chlorofluorocarbon-l
Analysiswasperformedby GC/MS.
5-3)
000076-1
G]ouplll
to USEPA5021method.
mg/Kg Withreferenc€
3 (CASNo.:
Chlorofluorocarbon-1
perfomed
by GC/MS.
Analysiswas
000075-72-9)
to USEPA5021method.
(CAsNo.: m!yK9 Withreference
chlorofluorocarbon-1'11
by GC/MS.
Analysis
wasperformed
000354-56-3)
EPA
5021 method.
(CAS
With
reference
to
US
No.: mg/Kg
12
Chlorofluorccarbon-1
pertormed
by
GC/l\rS.
Analysis
was
000076-12-0)
mg/Kg With referenc€to US EPA5021method.
I (CASNo.:
Chlorofluorocarbon-21
by GC/MS.
Analysis
wasperformed
000422-78$)
Us
EPA
5021method.
(CAS
With
reference
to
No.:
mgftg
luoroca6on-212
Chlorof
performed
by
GC/MS.
Analysis
u/€s
003'182-2&1
)
method
EPA
5021
with
reference
to
Us
(cAs No.: mg/Kg
chlorofluorocalbon-213
performed
by
GC/MS.
was
Analysis
002354-06-s)
mgKg !ryithreferenceto US EPA5021method.
14(CASNo.:
Chlorofluorocarbon-2
Analysiswasperformedby GC/l!lS.
029255-31-0)
15(CASNo.: mg/Kg With referenceto US EPA5021method
Chlorofluorocarbon-2
perfomedby GC/MS.
Analysiswas
0M25943-2)
pq9€sGdrtubsrcpon€mdb
'..::i,rr!
ao;;d ri, ,r:,.'r,:,r'i,.+{J.;.r.',,ri. tLn.1.,,i',.r'.r,;Ji:1
iiii!ii]].!,ir'J":ij!y;"c"^p""iou"aotomeac"rtmots
*.ta.."t*aa".j.*e".jo"'tbTemaidcodlmsb.E€drc
*d thddmd'; -"b'd
t*"" r"v rcsorn
io- *a p"o,a.,**";**o
"a*.*r"d"
"0"'i-o;
*
u" ri'* o c
-,
"" "
".
'.'.."'.
,3s,c';n
o,m{
.a o .
:r1r.t
llir,i ii. t '+$6orre
Result
I'lo.l
3
n.o,
3
n.d.
3
n.d.
I
n.d.
1
n.d.
1
n.o.
n.d.
n.d.
n.d.
n.d.
I
n.d.
'|
n.o.
1
n.d.
,l
n.d.
I
n.d.
1
n.o.
TestReport
Page:7 of 26
Der'Le.2010111115
No.: CE/2O1C|/82266
ll[| |r[llllllllll
HENKELCORPORATION
,14OOO
CALIFORNIA,
IRVINE,
ROAD,
JAI'BOREE
MAINOFFICE:
ADHESIVES-ELECTRONICS
HENKEL
92606U.S.A
Test ltem (5):
(cAS No.:
ohbrofluorocarbon-216
000661-97-2)
(CASNo.:
uorocarbon-217
Chlorofl
000422-866)
Unit
MDL
lrethod
mg/Kg Wlttr referenceto US EPA5021method
AnalysiswasperformedbYGC/MS
mg/Kg Wlth referenc€to US EPA5021method
bYGC/MS
wasperformed
Analysis
n.o.
1
n_o.
n-d.
(CASNo.:000075'434)
HCFC-21
HCFCl42b (CAS No.: 000075S83)
to Us EPA5021method
frg-ilg-ft\littrreference
performed
byGC/l'rS
was
lAnalysis
(CASNo.:000422-26-4) mg/Kg Witlr referenceto US EPA5021method
HCFC-221
AnalysiswaspertormedbYGC/MS
to USEPA502'1method
HCFG222(CASNo.:00042249-1) mgmglwii reierenc€
bYGC/MS
wasperfomed
lAnalysis
(CASNo.:00M22-524) mg/Kg fvith referenceto US EPA5021method
HCFC-223
AnalysiswEsperformedbYGC/MS
1.!!,iili
""
No.t
1
HCFCs
(Hydrochlorofluorccadons)
mg/Kg Wli6 referenceto US EPA5021method
AnalysiswEsperfomedbYGC/MS
HoFG22(CASNo.:000075-45$) mg/Kg W-rthreferenceto Us EPA5021method.
wasperfomedbYGC/MS
Analysis
(CASNo.:000593-70-4) mg/Kg Witlr referenc€to US EPA5021method.
HCFC-31
AnalysiswasperformedbYGC/MS
(CASNo.:000354-1+3) mg/K9 F;i6 referenceto US EPA5021method
HCFC-121
AnalysiswasPerfomedbYGC/MS
(CASNo.:000354-21-2)mg/Kg With referenc€to US EPA5021method
FEFC-122
AnalysiswasperfomedbYGC/MS
(CASNo.:000306-832) mg/Kg Witfrreferenceto LiSEPA5021method.
HCFC-123
AnalysiswEsperformedbYGC/MS
referenceto US EPA502't method
(CASNo.r002837-890) mg/kg Wj-rth
HCFC-124
AnalysiswasPerformedbYGC/MS
(;AS No.:000359-2&4)mg/kg fvith referenceto US EPA5021method
FtcFc-131
AnalysiswasPerformedbYGC/MS
to USEPA5021method
(CASNo.:00164M8- mg/Kg with refere.nce
HCFC-'132b
performed
bYGC/MS.
Analysis
was
7\
EPA
5021method.
to
US
With
reference
m9Kg
(CASNo.:000075-88HCFC-133a
performed
bY
GC/MS.
was
Analysis
7)
HcFc-l41b(CASNo.:0017',17-00-mgKg With referenceto US EPA5021method.
AnalysiswaspedormedbYGC/lllS
6)
Result
n.o,
1
n.o,
1
n.o,
1
n,o,
1
n.o.
1
n.d.
I
n.d.
n.d.
n.dn.d.
1
n.d.
1
n_o.
1
n.o.
,1
n.d.
rs6oan4etre rls
TestReport
No.:CE/2010/82266
Date:2010/11/15Page:8 of 26
ltfllllllllllllnt
HENKEL
coRPoRATloN
ROAo,
lRVlNE,
CALIFORNIA,
MAIN
OFFICE:
14000
JAI,BoREE
HENKEL
ADHESIVES-ELECTRONICS
92606U.S.A
Test ltem (B):
HCFC-224(CASNo.: 000422-*8)
Unit
Method
MOL
1
mg/Kg Withreferenceto US EPA502'! method.
Analysis
wasperfomedby GC/MS.
I
(CASNo.:000422-56- m9Kg With referenceto US EPA5021method.
HCFC-225ca
per{ormed
by
GC/lrS.
Analysis
was
0)
1
(CASNo.:000507-55- mg/Kg With referenceto US EPA5021method.
HCFC-22scb
Analysiswasperformedby GC/MS.
1)
(CASNo.:0Cn431€7-8) mg/Kg Withrcference
to USEPA5021method. 'I
HCFC-226
Analysis$rasperformedby GC/MS.
(CASNo.:000421-94-3) mlyKg With referenceto US EPA502'1method.
HCFC-231
Analy6iswasperformedby Go/lis.
HCFC-232(CASNo.: 000460-899) mg/Kg With referenceto US EPA5021method.
AnalysiswasperformedbYGC/MS.
(CAS
No.:00712$8,{-0) mg/kg Withrefe.enceto US EPA5021method.
HCFC-233
by GC/MS.
wasperformed
Analysis
to USEPA5021method.
(CASNo.:00042$94-5) mgKg Withreference
HCFC-234
by GC/MS.
wasperformed
Analysis
1
EPA
5021 method.
reference
to
US
mg/Kg
ntith
(CAS
No.:
000460-92-4)
HCFC-235
bYGC/lrS.
Analysis
waspertormed
1
(cAS No.:000666-27-3) mg/Kg Withreferenceto US EPA5021method.
HCFC-241
perfomed
by
GC/MS.
wEs
Analysir
to USEPA5021method. 1
mgikg
Withreference
(CAS
No.:
0004606$9)
HCFC-242
Analysiswss performedby GC/MSto USEPA5021method. 1
HCFC-243(CASNo.:00o,16G69-5) mg/Kg Withreference
,Nas
performed
bYGC/MS.
Analysis
to uS EPA5021method. 1
m9Kg with reference
HCFC-244
R€sult
No.l
n.o,
n.dn_0.
n.d.
n.d.
n.d.
n.d.
n.d.
n.d.
n.d.
n.d.
n.d.
n.d.
byGC/iIS.
wasperformed
Analysis
mg/Kg With referenc€to US EPA5021method
Analysiswasp€rformedbYGC/MS.
to USEPA5021method.
m
g/kg
Wittrraference
(CASNo.r000819-oG1)
HcFc-252
(CASNo.:00042141{)
HCFC-251
1
n.o,
1
n.d.
byGC/MS.
w€sperformed
Analysis
(CASNo.:000{6G35-5) mgKg Wiihreference
to USEPA5021methodHCFC-253
performed
bYGC/MS.
Analysis\ras
us
EPA
5021method.
reference
to
mgKg
With
(CASNo.:00042G97-3)
HCFC-261
waspeformedbYGC/MS.
Analysis
to US Epn 5021method
(CASNo.:000421-02- mgKg Wittr refere.nce
HCFC-262
Analy6iswasperformedby GC/l!lS.
03)
n.d.
n.dn.d.
TestReport
No.: CE/2010/82266Datr'e:2010h1/'l5Page: I of26
ltll lllllllllllllll
HENKELCORPORATION
ROAD,lRVlNE,CALIFORNIA,
llAlN OFFICE:14000JAITBOREE
ADHESIVES-ELECTRONICS
HENKEL
92606U.S.A
i,DL
mothod
unit
Test ltem (s):
(CASNo.:00M30-55-7) mg/Kg With referenceto US EPA5021method.
1
HCFC-271
Analysiswasp€rfomedby GC/MS.
Halons
1
mg/Kg Withreferenceto US EPA5021 method.
Halon-1211
performed
Analysis
was
by GC/MS.
(CASNo.:000359593)
1
mg/Kg With referenceto US EPA5021method.
Halon-1301
(CASNo.:00007563-8)
by GC/MS.
Analysis
wasperformed
1
mS/kS With referenceto US EPA5021method.
Halon-2402
(CASNo.:00012,1-73-2)
Analysiswasperformedby GC/MS.
HBFCs
(Hydrobromofl
uorocarbons)
1
mg/kg Withref€renceto US EPA5021method.
HBFC-2182(CHFBi2)(CAS No.:
Analysis
wasperformed
by GC/MS.
001868-53-7)
m9Kg With referenceto US EPA5021method.
HBFC-2281(CHF2Br)(CAS No.:
Analysiswasperformedby GC/l!lS.
001511€2-2)
R€6ult
i.lo.t
n.d.
n.d.
n.d.
n.d.
n.d.
n.d.
HBFC-3181(CH2FBr)(CAS No.:
000373-524)
mg/Kg With referenceto US EPA 5021 method.
AnalysiswE6performedby GC/MS.
n.o.
(C2HFBr4)
HBFC-12184
to uS EPA5021method.
mg/kg Withreference
by GC/MS.
Analysis
wasperformed
mg/Kg With referenceto US EPA5021 method.
wasperlormed
by GC/MS.
Analysis
to US EPA5021method.
mg/kg Withreference
Analysiswasperformedby GC/MS.
mgKg With referenceto uS EPA5021method
Analysiswaspertormedby GC/lrS.
mg/kg Withreferenceto US EPA5021method.
Analysis
wasperfomedby GC/MS.
to uS EPA5021method.
mgKg Withreference
Analysisv/asperformedby GC/MS.
mlyxg With referenceto US EPA5021method.
by GC/l\rS.
Analysis
wasperformed
mg/Kg With referenc€to US EPA5021method.
Analysis
wasperfomedby GC/MS.
mgil(g With referenceto US EPA5021methodby GC/MS.
wasperformed
Analysis
to uS EPA5021method
mg/Kg Wth reference
n.d.
(C2HF2813)
HBFC-12283
(C2HF3812)
HBFC-12382
HBFC-I2481{C2HF4Br)
(C2H2FB13)
HBFC-131B3
2Brz)
HBFc -13282(c2H2F
(C2H2F3Br)
HBFC-13381
(C2H3FB12)
HBFC-14182
(C2H3F2Br)
HBFC-14281
(C2H4FBr)
HBFC-15181
bYGC/lrS.
wasperformed
Analysis
npqg
a;F ,
€sGd rhs bi
rcpo^ emd
b
ii"i"J*n,i";;owt.c"^m.y$bfdbG6enerdcondloi3ofs
oi.e.^"t-*oj'*eE'6rsm9a.dcMdloisb.E*.""o"*'-ta*"q".'a
i*t- *o r"o,a." **. a.
trmy ri,ecmFrys$erc
"a-..* ;,";ut i.
c *,"."r!dD*
J,iri
' .---.
. '" u'n*'-0.
" "
h*"'.
's6a;ndbs
:rxi. r
i,r ! +d, !1.1.$6hlxe
n.o.
n.d.
1
n.d.
1
n.d.
1
n.d.
'I
n.d.
1
n.o.
1
n.d.
,|
n.d.
TestReport
No.: CE/201CyB2266
Date:201Oh1115Page: 10of 26
l[lllllrllllllll]l
HENKELCORPORATION
ROAD,lRVlNE,CALIFORNIA,
MAINOFFICE:14000JAMBOREE
HENKEL
ADHESIVES-ELECTRONICS
92606U.S.A
Test ltem (3):
(C3HFB16)
HBFC-22'186
(C3HF2B15)
HBFC-22285
(C3HF3814)
HBFC-22384
(c3HF4B13)
HBFC-22483
(C3HF5812)
HBFC-22582
HBFC-22681
{C3HF6Br)
(C3H2FB15)
HBFC-23185
HBFC-232B4G3H2F2Bt4)
(C3H2F3Br3)
HBFC-23383
HBFC-23r'BzIC3H2F4Bi2\
(C3H2F5Br)
HBFo-23581
HBFC-24184(C3H3FB14)
HBFC-24283(C3H3F2B13)
unlt
method
i,DL
mg/Kg With referenc€to US EPA5021method.
Analysis
w€sperformed
by GC/MS.
reference
to
US
EPA
5021method.
mgftg With
Analysis\ras performedby GC/MS.
mdks With referenceto US EPA5021method.
Analy6iswasperformedby Gc/Ms.
mg/Kg Withreferenc€to US EPA502t method.
wasperfomedby Go/MS.
Analysis
mgftg With referenceto US EPA5021method.
Analysisw€sperformedby GC/MS.
mgKg With referenceto US EPA5021method.
by GC/l!lS.
wasperlormed
Analysis
mg/Kg With referenceto US EPA5021method.
wasperfomedby GC/MS.
Analysis
mgilg with rcferenceto us EPA502'1method.
Analysiswasperformedby GC/MS.
mgKg uvithreferenceto uS EPA502'1method.
'ras pedormed
by GC/MS.
Analysis
m9Kg With referenc€to US EPA5021 method.
by GC/l!lS.
Analysis
wasperformed
mg/Kg With referenceto US EPA5021method
Analysiswasperfomedby GC/MS.
mg/Kg with referenceto us EPA5021method.
wEsperfomedby GC/MS.
Analysi6
to us EPA5021method
mg/kg wiahreference
R€6ult
I'lo-l
1
n.o,
1
n.d.
1
n.d.
'I
n.o.
1
n.d.
1
n.d.
1
n.o,
n.d.
n.d-
n.d.
n.o.
I
n.d.
1
n.d.
bYGC/MS.
w€sperformed
Analysis
(C3H3F3Br2)
HBFC-24382
mgikS
to USEPA5021method.
Wittrreference
Analysis,.!"s performedby GC/MS.
1
n.d.
HBFC-24481 (C3H3F4Br)
m!/Kg
Wittr reference to US EPA 5021 method.
Analysiswas performedbYGC/MS.
1
n.d.
HBFC25183(CaH4FB13)
to Us EPA5021method.
mdkg WiiFreference
,,,/as
performed
byGC/MS.
Analysis
5021method
US
EPA
to
With
r€ferance
mg/Kg
bYGo/lrs
wasperformed
Analysis
I
n.d.
1
n.d.
HBFC.252B2GAH4F2BQ\
HBFG253Bl(C3H4F3B0
mgKg with referenceto US EPA5021 method.
wasPetormedbYGC/lrS
Analysis
rl*: '!
Jrrnt
i!lstlor'e
n.d.
TestReport
No.ICE/2010/82266Dde 2010111h5 Paoe: '11of 26
HENKELCORPOMTTON
[][ttt!|||tttl|l
HENKEL
ADHESIVES-ELECTRONICS
MAINOFFICE:14000JAITBOREE
ROAD.lRVlNE.CALIFORNIA.
92606U.S.A
Testltom (s):
Unit
method
il|DL
mg/Kg Withreference
to USEPA5021method. 'I
HBFC-26182(C3H5FB12)
Analysiswasperfo.medby GC/l!rS.
mg/kg Withreferenceto US EPA5021method.
Anelvsis
wasDerfofmed
bv GC/MS.
(C3H5F2Br)
HBFC-26281
(C3H6FBr)
HBFC-27181
HFCs(Hydrofluorocarbon)
HFC-23(CHF3)(CAS
No.:00007546-7)
No.:000075HFC32(CH2F2XCAS
1G5)
No.:000593HFC41(CH3FXCAS
53-3)
(C5H2F10)
HFC-43-1omee
HFC-125(C2HF5)
HFC-134|C2H2F4')
No.i
HFC-I34a(CH2FCF3XCAS
1-97-2)
00081
(CH3F3)
HFC-143
Result
No.'l
n.d.
1
n.d.
mg/Kg With refefence to US EPA 5021 method.
Analysiswas perfomed by GC/MS.
1
n.d.
mgftg Withreference
to USEPA5021methodAnalvsiswasDerformedbv GC/l\rS.
mg/Kg Withreforenceto uS EPA5021method.
Analvsis
wasperfomedbv GC/MS.
mg/Kg With referenceto US EPA5021method.
Analysis
wa6perform€d
by GC/MS.
mg/kg Withreference
to US EPA5021method.
Analvsis
waspedormed
bv GC/MS.
mg/Kg With referenceto US EPA5021method.
Analvsis
wasperfomedbYGC/MS.
mSikS with reference
to USEPA5021method
Analysiswasperformedby GC/MS.
mg/Kg With referenc€to US EPA502'l method.
Analysis
wasperfomedby GC/MS.
1
n.d.
1
n.o,
1
n.d.
1
n.d.
1
n.d.
I
n.d.
1
n.o.
to uS EPA5021method.
msI(s Withreference
n.d.
mg/Kg With referenceto US EPA502'1method.
wtssperfomedby GC/MS.
Analysis
mS/kS Withreference
to USEPA5021method.
Analysiswasperformedby GC/luS.
mg/Kg With referenc€to uS EPA5021method.
wEsperformed
by GC/MS.
Analysis
n.d,
HFC-236fa(C3H2FO)
mgikg With referenceto US EPA 5021method.
Anslysiswas performedby GC/MS.
n.d.
(C3H2FBXCAS
No.:
HFC-236ea
000431€3-0)
mgKg With referenceto US EPA5021method.
Analy6iswasper{ormedby GC/l\rS.
mg/Kg Withreferenc€to US EPA502t method.
Analysis
wasperfomedby GC/MS.
mgftg Withreferenceto US EPA502'1method.
Analysis',!asperformedby GC/MS.
Analysis
wasperformed
byGC/lrS.
(CH3F3)
HFC-143a
No.:
HFCI 52a(C2H4F2)(CAS
00007t37-6)
(C3HFTXCAS
No.:
HFC-227ea
-89-o)
000431
HFC-245ca(C3H3F5)
HFc-245fa(C3H3F5)
r . i P ' ] ;r , i ' r , , ' : ? i i i n l r *
oyrc c".e
" "!"a
**""
,ia""r-,*-"e,.a*
- \ a - * , h " , h . i . t sd c L * ' " *
c;;*yr.
in,"i""i.or
in
n.d.
n.o.
1
n.d.
'I
n.d.
1
n.d.
prsc)r6Gd rh s €sr'3po^6'nd e
','!r,)l!a'
iar ltrrrl:+:;'i
oo"o'tq-r;'o""
Mnb{d!h"scscolp{(c!sAr
TestReport
No.: CE/2010/82266Oale:201U11115 Paae:12ol 26
ITIIIIITI!|II!!ruTT
HENKEL
CORPORATION
MAINOFFICE:14000JAMBOREE
ROAD,lRVlNE,CALIFORNIA,
HENKEL
ADHESIVES-ELECTRONICS
92606U.S.A
Te5tltem (s):
(C4H5F5)
HFC-365mfc
PFCa(P6dluorocarbon)
F14(CASNo.:000075-73-0)
Unit
Method
MDL
Result
No.1
mg/kg Withreference
to US EPA5021method.
Analysiswasperformedby GC/IVS.
n.d.
mg/Kg Withreference
to USEPA5021method.
Analysis
wasperfomedby GC/MS.
mdkg With referenceto US EPA5021method.
Analysi6
wEsperfomedby GC/MS.
n.o.
Fluorocarbon
116(CASNo.:
000076-164)
Freon218(CASNo.r000076-19-7) mg/kS Withreferenceto IJS EPA 5021method.
1
n.d.
,l
n.d.
Withrefe€ncelo US EPA5021method.
Analy6is'ra6 performedby GC/IVS.
FreonC318(CASNo.:000115-2t mg/Kg Withreference
to USEPA5021method.
3)
Analysis
wasperformed
by GC/MS.
PerfluoFl-butene(CAS No.:
mg/Kg With referenceto US EPA5021method.
000357-26$)
Analysis
w€sperfomedby GC/MS.
perfluorisobutene
(CASNo.:
mdkg Withreferenceto US EPA5021method.
000382-21-8)
Analysiswasperformedby GC/MS.
'1,4-dihydrooctafluorobutane (CAS
mSikS Withreference
to USEPA5021method.
No.:000377-36€)
Analy6is
wa6performed
by GC/lllS.
Nonafl
uorr- (trifluoromethyl)
mg/Kg Withreferenceto US EPA5021method.
butane{CASNo.:00059+91-2)
Analysis\ras performedby GC/MS.
(CASNo.:
Perfluoro-n-pentane
mg/Kg With referenceto US EPA5021method.
000678-26-2)
Analysis
wEsperformed
by GC/MS.
(CAS
mg/kg Withreference
2-perfluoromethylpentane
to USEPA5021method.
No.:000355-04-4)
Analysis
wasperformed
by GC/[/|S.
(CASNo.:000355- mg/Kg Withreference
Perfluorohexane
to USEPA5021method.
4241
Analysiswasperformedby GC/MS.
CHCa(Chlo natohydrocarbon)
(CAS
mg/Kg Withreference
to uS EPA5021method.
1,1,1,2-Tetrachloro€thane
Analysis
wasperformed
by GC/MS.
No.:000630-20€)
(CASNo.:
mg/Kg With referenceto US EPA5021method.
1,1,1-Trichloroethane
Analysis
u/€sperformed
by GC/MS.
000071-55€)
'1,1,2,2-Tetrachloroethane
(CAS
m!yKg With referenceto US EPA502'1mothod.
Analysis
wasperfomedby GC/MS.
No.:000079-34-5)
(CAS No.i
to IJSEPA5021method.
mgftg Withreference
1,1,2-Tdchloroethane
Analysis
wasperformed
by GC/[,I]S.
0000794G.5)
1
n.d.
1
n.d.
1
n-o.
1
n.d.
I
n.d.
I
n.d.
'I
n.o.
1
n.d-
1
n.d.
1
n.d.
I
n.d.
1
n.d.
1
n.d-
qnatysiswas pertormedby GC/l\rS.
Decafluoaobutane(CAS No.:
000355-25-9)
mgftg
mpelsrreded rh€ red rcpdd siidlb
cdnoaiYi1l.:]1.:..]].L'l],i!]ll]jl;L!'i-i:i{]i,.,...,.'.'.
Th s bfumsnl s 69u6d oy 66 c ompa
TestReport
No.: CE/20f0/82266 Dale:2010111115Paoe: 13of 26
HENKELCORPORATTON
l
ut
HENKEL
ADHESIVES-ELECTRONICS
MAINOFFICE:14000JAMBOREE
ROAD.lRVlNE.CALIFORNIA.
92606U.S.A
Te6t ltem (s):
Unit
'1,1-Dichloroethane
(CASNo.:
000075-3+3)
(CASNo-:
1,1-Dichloroethene
000075-354)
(CASNo.:
I ,1-Dichloropropene
000563-s86)
'1,2,lTrichloropropane
(CASNo.:
000096-1E4)
'1,2-Dichloroethane
(CASNo.:
000107{6-2)
(CASNo.:
1,2-Dichloropropane
000078€7-5)
(CASNo.:
1,3-Dichloropropane
000142-28-9)
(CASNo.:
2,2-Dichloropropane
000594-20-7)
lethod
mg/Kg Withreference
to USEPA5021method.
Analysis
wasperformed
by GC/MS.
mg/Kg Withrefe€nceto USEPA5021method.
Analysis
wasperfomedby GC/MSmgKg Withreferenceto US EPA5021method.
Analysiswasperlormedby GC/MS.
mSikS Withreference
to USEPA5021method.
Analysis
wa6performed
by GC/lrS.
mg/K{l Withrefer€nce
to US EPA5021method.
Analysis
wasperformed
by GC/MS.
mg/Kg Withreference
to USEPA5021method.
Analysis\ras performedby GC/MS.
mg/Kg With referenceto US EPA5021method.
Analysi6
wa6p€rfomedby GC/MSm9Kg Withreference
to USEPA5021method.
Analysj6wBsperformedby GC/MS.
C€rbontetrachloride(CAS No-:
mdkg Withreference
to USEPA5021method.
000056-23-5)
Analysis
wasperformed
by GC/I/|S.
(CASNo.:000075-00-mg/K(l Withrefer€nce
Chloroethane
to US EPA5021method.
3)
Analysis
\r€sperformed
by GC/MS.
(CAS
Chloroform
No.r000067€6-3) mg/Kg Withreference
to USEPA5021method.
AnalysiswEsperformedby GC/MS.
(CASNo.:000074- mS/kS With reference to IJS EPA 5021 method.
Chloromethane
87-3)
Analysiswas performedby GC/MS.
(CAS
cis-1,2-Dichlo.oethene No.:
mg/Kg Withreference
to US EPA5021m€thod.
Analysiswesperformedby GC/MS.
000156-59-2)
(CASNo.; m9Kg With referenceto US EPA5021method.
cis-1,3-Dichloropropene
Analysis
wasperfomedby GC/MS.
010061-01-5)
(CASNo.:
mg/kg Withrefer€nceto US EPA5021method.
Hexachlorobuladiene
Analysi6wasperformedby GC/MS.
000087$8-3)
mgKg With referenceto US EPA5021method.
Methylene
Chloide(CASNo.:
Analysis
wasperfomedby GC/MS.
000075-09-2)
(cAS
mg/Kg With referenceto US EPA5021method.
Tetrachloroethene No.:
Analysis'r/asperformedby GC/MS.
000127-i84)
(CASNo.: mg/Kg With referenceto US EPA5021method.
trans-1,2-Dichloroethene
wasperfomedby GC/MS.
Analysis
00015s60-5)
c o n o . n yt ,
tt:r'iU.l,i:i,,r:l
ga,*"-a*$"t"
h"i, ' qn" *o
"o
d be mnbd s
ioeet d i. s6€1m
!1i-!rL.i::i. {rri 1.i",.r: ',:l
i
l,rrr)l,r'!.
I/|DL
Reault
1
No.l
n.d.
1
n.d.
1
n.d.
1
n.d.
1
n.d.
1
n.d.
'I
n.o.
'l
n.d.
1
n.d.
'I
n.d.
1
n.o,
1
n.d.
I
n.d.
1
n.o.
1
n.d.
1
n.o,
n.d.
n.o.
||[|]!
TestReport
No.: CEl2010/82266Dal'e:201U11115Paoe: 14of26
ltfl[tf,|l||tttl]l
HENKEL
CORPORATTON
ROAD.lRVlNE.CALIFORNIA.
HENKEL
ADHESIVES-ELECTRONICS
lrAlN OFFICE:'14000
JAITBOREE
92606U.S.A
Testltem(s):
(CAS
trane1,3-Dichloropropene
No.:01006'1-02$)
(CASNo-:
Trichloroethylene
000079-01$)
lrethod
Unit
MDL
Re3ult
No.1
1
n.d.
1
n.o.
mg/kg Withreference
to US EPA5021method.
Analysis
wasperformed
by GC/MS.
mg/Kg With referenceto US EPA5021method.
AnalysiswEsperformedby GC/MS-
Noie i
1. mg/kg= ppm; 0.1wt%= 1000ppm
2. n.d. = Not Detected
Limit
3. MOL= MethodDetection
4."-"=NotRegulated
(NoUnit)
5. " = Oualitative
analysis
= Detectable
/ Po6itive
6. Negative= Undetectable
7. Asbestos: Negative= "< 1.0%",Positive= "> 1.0%"
forTributylTin.
TheMDLwasevaluated
lvascalculated
by thetestre6ults
of TributylTin.
8. *'r Thesubstance
PFOSReferencelnformalion : Directive2006/I2ZEC
in a concentration
equalto
(1) Maynotbe placedon themarketor usedas a substance
or constituent
of preparations
higher
than
0.005
%
by
mass.
or
productsor articles,of partsthereof,if the concentration
of
(2) May not be placedon the ma*et in s€mi-finished
witheferenceto themassof strudtu€llyor
PFOSi6equaltoor higherthanO-10/6by massc€lculated
if theamountof PFOSis
or othercoatedmaterials,
microstructu€lly
distinctpansthatcontainPFOSor,for textile6
material.
higher
than
llg/m'?
of
the
coat€d
equalto or
c o m p a n y , i . .l l r i t
ir
!:ri a:,
i ..,"ar u" c*p.
*i!!.riit.
prels)resGd
rhsEercpon€ond M
I
,lrl\n
.,iq"o oi"-" -o c-4.* t' r
o "i*i,.*, t.", a;'*t
"r*-i-r." -o erooo." **";
,rem",i
o:i-a*t"rei.tacd".'tud6sim'Tirscompaiy3sec
rn"i,,*r -o
*r-"-a*rn"r.
"o o, ,h" -^bd d
ioqe.i - i. 'id;n
,-!:r t
li.rii'|
tr1+s6loa,
TestReport
No.: CE/201C1/82266
Oale:2010h1h5 Page:'15of26
l[lllltrll
HENKEL
CORPOMTTON
ROAD,lRVlNE,CALIFORNIA,
[rAlNOFFICE:14000JAITBOREE
HENKEL
ADHESIVES-ELECTRONICS
92606U.S.A
llllltlll
methodaccording
to b€lowflowchan
dissolved
totallyby pre-conditioning
1) The6esampleswere
acre test melhod€xcluded)
Climbgreat
Yang
2) Nameof thepe6onwhomademea6ufement:
TroyChang
3) Nameof thep€rsonin chargeof measurement:
Cutting/ Preparation
SampleMeasurement
Acid digestionby suitableacid
dependedon difer€nt6ample
material(as belowtable)
Add appropdateamountof
digestion€agent
Heatto appropriate
to extract
temperature
Cool,filterdigestate
AlkaliFu6ion
HClto dissolve
ICP.AES
colordevelopment
solder
Steel,copper,aluminum,
Aquaregia,HNO3,HCl,HF,HrO,
Gla6s
HNO3/HF
measure the absorbance
Gold,platinum,palladium,ceramic
Aquaregia
at 540nm by UV-VIS
Silver
HNO3
Plastic
HrSO. H,O,, HNO3,HCI
Others
Anyacidto totaldigestion
c o n p a n: iy' ; l r . 9 , ; . r ' l ' r : - i : l ' r l l i r n i
g so* q u" c*p,
n" oi.n
rc i.t uc *r...
-ly -o
",r.
qa-. -a- 'n. *€d
u.i,,sn"*a"o
io.qei
for
Adddiphenyl-cabazide
DigestionAcid
SampleMaterial
filter
through
tr iabh€,
in oi c6 6dm1
s
rr;
m &d;sc
{'ri *ri1. r. I I I
rh'6dm*Ie
lr!r,rl!1'
TestReport
No.:cE/2010/82266Date:2010/11/15Page:16of26
HENKELCORPORATTON
lflflt
HENKEL
ADHESIVES-ELECTRONICS
MAINOFFICE:14000JAMBOREE
ROAD.lRVlNE.CALIFORNIA.
92606U.S.A
1 ) Thesesamples
weredissolved
totallyby prc-conditioning
methodaccording
to belowflow
2) Nameofthe personwhomademeasurement
ClimhreatYang
person
Name
3)
of the
anchargeof mea6urern
ent:TroyChang
FlowChartof digestionfor lhe elementsanalyslsperfonnedby ICP-AES
1) AlkaliFusion
2) HCltodissolv€
ICP-AES
Steel,copper,
aluminum,
solder
Aqua regia,HNOr, HCl, HF,H,O,
Glass
HNO3/HF
palladium,
Gold,platinum,
ceramic
Aquaregia
Silver
HNO3
Plastic
H,SO1,H'O', HNq, HCI
Others
Anyacidto totaldigestion
mpreG)re$ed rh s Gd @on cid
- rr .i
e
i ri !ii1r ri r+$6onrs
ll|ttlt]l
Test Report
No. : CE/201€ll82266 Date :2O1Oh1115 Page| 17of 26
HENKELCORPORATTON
Utfiltttlfi]t
HENKEL
AoHESIVES-ELECTRONICS
MAINOFFICE:14000JAMBOREE
ROAD,lRVlNE,CALIFORNIA,
92606U.S.A
Analyticalflow chartof Soxhletextraction(GC/ltS)procedure
1) Nameofthepersonwhomademeasurement:
LydiaFu
2) Nameoflhe personin chargeof measurement
ShinjyhChen
!
' Benzotriazole
. HBCDD. NP. DBBT'
T€stltems:Phthalate
phosphorus
Organic
compounds
Data
cmoaiy,i,. lrr Jr; x;l]',+irl!,!trr'1"ii
1rr'
rrec)red:d rh s ied eoodennd b
lu
TestReport
No.: C92010/82266 Datr'e
| 2O1OI11hs Page : 18 of 26
HENKELCORPORATTON
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HENKEL
ADHESIVES-ELECTRONICS
MAINOFFICE:14000JAMBOREE
ROAD.lRVlNE,CALIFORNIA.
92606U.S.A
Analyticalflow chartof Soxhletextraction(LC/iIS)procedure
1 ) Nameof theperson
whomademeasurement
LldiaFu
2) Nameotthe personin chargeofmeasurernent
ShinjyhChen
. Benzotriazole
lTest ltemsPFOS/PFOA
Sampleprelrealrnenvseparation
I
Daia
mpetslre*edrh€ bd repodsinorb
r,
.ll !t4!'
c o m p a n y , 1 ,..' j t , l , r i { l t l r + 1 J !i l r r , i ' i n 1 i i " ; ; ! r l : i r r
pnned ove,eat aroiade o. eq
or
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No.: CE/2010/82266Date: 2010/11115Pagei 19of 26
HENKEL
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ADHESIVES-ELECTRONICS
lrAlN OFFICE:14000JAIVBOREE
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Analysisflow chartfor deteminationof Asbestos
1) Nameof theDeEonwhomademeasurement
VictorKao
2) Nameolthe personin chargeofmeasurement.
WendyWd
XRDQualitativeanalysisby X-raydiftraction
method
Diffractionpeakof
Asbestos
fiberis prcsent
Asbestos
fiberis absent
Nolcontaining
Asbestos/
Negative
c o h p . ^ y? r + l . : , o r j , r r : r ' r : - r i : l l i r t r i r [ " ! ] i . r \ i
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TestReport
No.: CE2010/82266 Dale:2010111,15paqe:20 of 26
HENKELCORPORATTON
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HENKEL
ADHESIVES-ELECTRONICS
liAlN OFFICE:14000JAITBOREE
ROAD,tRV|NE,CAL|FORN|A.
92606U.S.A
[t
Analyticalf,owcha
1) NameofthepeBonwhomademeasurement
RomanWong
2) Nameofthepersonin chargeofmeasurcment
TroyChang
! Teslltems:PBB/PBDE,
TBBP-A-bis
process---)
Filsttesting
pDcess---.
Optionalsc€en
pmcess-,>
Contimation
Sc€e. analysis
Sampleexlraction/Soxhlet
method
t
Conc€ntate/DiluteExlractedsolutjon
I- - - - - - - - - - - - - - - v
Filter
-I - - - - - - - - - - - - . - v
PBB/PBDE
: Analysis
by GC/MS
TBBP{-bis:An.lysEby HPIC/DAD/MS
lssueRepod
c d n a at . t . ' , \ t . : P t l ! . r ' f , i : i l r ! . ! i : r r i
!:1
Irl
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Test Report
No.: CE/2010/82266Dale:201U11h5 Peae:21of 26
||lllllllllllllllll
HENKELCORPORATTON
ROAD,IRVINE,CALIFORNIA,
HENKEL
ADHESIVES.ELECTRONICS
MAINOFFICEI14OOO
JAMBOREE
92606U.S.A
Analyticalflow chartof Organlc-Tincontent
GinnyChen
1) Nameof thepersonwhomademeasurement
pe6on
TroyChang
2) Nameof the
in chargeof measurement:
Concentrate/Dilute
Extractedsolution
by GC/FPD
Analysis
wasperformed
DaE
1.:i,in,
:r I I s6Lrlxeer- flr
Test
p<€e122(f26
No.: cE/2o
10/82266
Date:2010/11/1s
Report
HENKELCORPORATTON
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HENKEL
ADHESIVES-ELECTRONICS
MAINOFFICE:14000JAMBOREE
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ChlorinatedFlameretardantanallticalflow cha
'l) Nameof thepersonwhomademeasurcment
BarryTseng
2) Nameof thepeFonin chargeofmeasurement
TroyChang
a
a
Reference
method:US
EPAE270D.
US EPA3540
Testltems:PCBS,
PCNS,
PCTS,
Mirex,CP,I/ICCP
Data
c o n o a n yr : , r : l ' j i , l . - r i " i r r , : l r : L r - r i ' i : - _ . 1 . 1 1 i , ; r ! ' . ' .
rr r .
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No.: CE/2010/82266Date:2010/11/15 page:23cf 26
HENKEL
CORPORATION
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HENKEL
ADHESIVES.ELECTRONICS
MAINOFFICE:14OOO
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Analyticalflow chartof halogencontent
1) Nameofthepersonwhomademeasurement
RitaChen
2) Nameofthepersonin chargeofmeasurement
TroyChang
pretreatment
Sample
/ Separation
Weighting
andputtingsamplein cetl
OxygenBombCombustion
/ Absorption
Dilution
to fixedvotume
Analysis
wasperfomedby lC
c o m o a i ]r i : , . - l : : : t l . , r r ' i | r : J . , } L r r !
b 6]ectoi c ioma' doeoafu
sub,
i:i.
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s dratr lo lho I mial o. o' 'ab !
Test Report
No. : Cg20'10/82266 Dale :2010111115 Paoe:24 ol 26
HENKELCORPORATION
III IIII|IIIIIITNITI
HENKELADHESIVES-ELECTRONICS
MAIN OFFICE: 14000JAMBOREEROAD,lRVlNE,CALIFORNIA,
92606U.S.A
Analyticalflow chartofvolatileorganiccompounds(VOCS)
1 ) Reference
method: USEPA502'1
: DalkiYen
2) Nameof theDerson
whomademeasurement
: ShinjyhChen
3) Nameof thepersonin chargeof measurement
Takesampleandputit into
glasswafe.
headspace
:r '\,ri i:.i {rr,irr?lr:!.1
-r:'i,
c o n p a i y , :i r i i l
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|
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Test Report
No.: CE/2010/82266Date 211]tl1ttS page: 25 of 26
HENKELCORPORATION
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HENKELADHESIVES-ELECTRONICS
i,tAtNOFFtCEI 14OOO
JAMBOREE
ROAD,IRVINE,CALIFORNIA,
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Analyslsflow chartfor determinationof pVCin material
1) Nameofthepersonwhomademeasurement
EvaChao
2) N€meof thepersonin chargeof mea6urement
ShinjyhChen
pr+treatment
Sample
Sample
analt|zed
by FTIR
Checkwav+numberof C-Clbonding
npe(s)reded rh 3 bd €tor 6.nd
iid
6e rep.dued erced ni!r.qihdd
s
l
Test Report
No.: CE/2010/82266O?i.e
| 2010t11115page 26ot26
HENKEL
CORPORATTON
ll]tIlt||
HENKEL
ADHESIVES-ELECTRONICS
MAINOFFTCE:
14000JAMBOREE
ROAD,tRVtNE,CAL|FORNtA.
92606U.S.A
'- Endof Report "'
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Test Report
ll]tltI|[]
Thefollowingsample(s)wa6/weresubmitted end identified by/on behalfofthe client as:
Test Result(s)
ithscs
No. : CE/2011/42646 Dale | 201110/'t127 Page : 1 of 8
HITACHICHEMICALCO., LTD.
1772-1KAMKUBO YUUKI.SHIIBARAKI,307-0015,JAPAN
SampleDescription
Style/ltemNo.
SampieReceiving
Date
TestingPeriod
nown
EPOXYMOLDING
COIVPOUND
CEL-922OHF
2011t04t14
201I t04t14 TO 201I t04t27
: Pleasereferto nextpage(s).
{Nwa--x
E$rad for rid
cl|.|nicd Laboratory- TdDel
c o m o a n v : l n r lt r : . 1 : a ' : , r ' , " 1 . . / L r r t : ; . :
rt
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rlrt,{'
!dsrdzoiqNa!7dF.&rdwr.ri
:l+46i0lrerr[s610?]rrerr@!ss'rdn
tII|lll
TestReport
No.: CE/2011/42646Daie | 20111c/,127 Page: 2 of 8
HITACHI
CHEMICAL
CO.,LTD.
1772.1KANAKUBO
YUUKI-SHI
IBARAKI,
307-0015,
JAPAN
Ifl[
[[]rr|l
TestResultlsl
PARTNAMENo.1
Testltom (s):
Cadmium(Cd)
Lead (Pb)
Mercury(Hg)
Hexavalent
Chromium
C.(Vl)by
alkalineextraction
(Sb)
Antimony
DARKGRAYLUMP
Unit
Method
mg/Kg Withreference
to tEC62321:2008and
performed
by ICP.AES.
mg/Kg Wilh referenceto IEC62321:2008and
performed
by ICP.AES.
mg/Kg Withreference
to tEC62321:2008and
performed
by ICP-AES.
mg/Kg Wilheferenceto IEC62321:2008and
performedby UV-VIS.
mg/Kg Withfeference
to USEPAMethod
30508forAntimony
Conlent.
Analysis
wasperformed
by ICP-AES.
I'DL
Result
2
n.d.
2
n.d.
2
n.d.
2
n.d.
2
n.d.
50
n.d.
50
n.cl.
50
n.o.
50
n.d.
No-1
Halogen
Halogen-Fluodne
(F) (CASNo-:
14762444\
(Cl)(CASNo.:
Halogen-Chlorine
22537-1+1'
(Bf)(CASNo.:
Halogen-Bromine
10097-32-2)
(l) (CASNo.:
Halogen-lodine
14€6244-8)
Sumof PBBS
llonobromobiphenyl
Dibromobiphenyl
Tribromobiphenyl
Tetrabromobiphenyl
Pentabromobiphenyl
Hexabromobiphenyl
Heptabromobiphenyl
Octabromobiphenyl
Nonabromobiphenyl
Decabromobiphenyl
Withreference
to BS ENU5a22OO7.
m9Kg
Analysis
wasperformed
by lC.
5
5
Withreference
to IEC62321:2008and
mg/kg
Der{ofmed
bv GC/IVS.
c o r o a i y . i : . I r L . l J - l ' r , r i r r l , : 1 r . i :i r i . t l i
n.d.
n.d.
n.d.
n.d.
5
n.o.
5
5
5
5
5
n.d-
n.d.
n.d.
n.d.
n.d.
n.d.
llllr'i
spongblysbbcladsidlh3dod
.: l..r t
i.'iitr:,il+*6o:tDenD ir$6orrrtstt
**!!od
TestReport
No.'.CEl2011l42U6 Daie: 20111c/'n7 Page: 3 of 8
HITACHICHEMICALCO., LTD.
1772.'1KANAKUBOYUUKI-SHIIBARAKI,
307-0015,
JAPAN
Test ltem (s):
Sum of PBDES
lvlonobromodiphenyl
ether
Dibromodiphenyl
ether
fribromodiphenyl
ether
fetrabromodiphenyl
ether
Pentabromodiphenyl
ether
Hexabromodiphenyl
ether
Heptabromodiphenyl
ether
Oclabromodiphenyl
ether
Nonabromodiphenyl
ether
Decabromodiphenyl
ether
Unit
lll
lrlethod
MDL
Withrefe.ence
to IEC62321:2008and
mgftg peformed
by GC/lllS.
5
5
5
5
5
5
5
5
llltI||lu]|l]t
Reault
No,1
n.dn.d.
n.d.
n.d.
n.d.
n.d.
n.o.
n.o.
n.o.
n.o,
5
n.d.
Note:
1. mg/kg= ppm; 0.lM% = 1000ppm
2. n.d. = Not Detected
3. MDL= MethodDetec{ion
Limit
4."-"=NotRegulated
I l: .rr'.i r:
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ior s sdrod. rom.r dodme^6 slbr
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i
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ro ha mraroo 0r 'ab !t
rn'
!
i
J ri:i1..i;t+s6 tr:ee
Test Report
No. I CE12011/4264€ Date:2011t04t27 paoe:4of8
HITACHI
CHEIVICAL
CO.,LTD.
'1772-1
KANAKUBO
YUUKI.SHI
IBARAKI.
307-OO'15,
JAPAN
fltlt[ttt!
||I|t|l
1) Thesesamples
weredissotved
totallyby pre-conditioning
methodeccording
to betowflowchart.
( Cr"' testmethodexctuded
)
yang
2) Nameof thepe6onwhomademeasurement:
Climbgr€at
3) Nameof thepe6onin chargeof measurement:
TroyChang
Cutling/ Preparaiion
Aciddigestion
by suitable
acid
depended
ondifferent
sample
malerial(asbelowtable)
l\Iicrowavedigestionwih
HNO3/HCUHF
Addappropriate
amountof
digestion
reagent
Heatto appropriate
temperature
to exfact
'1) AlkaliFusion
2) HClto dissolve
ICP.AES
throughfilter
Add diphenyl-carbazide
for
SampleMaterial
DigestionAcid
S-teel,
copper,aluminum,
solder
Aqu€ regia,HNO3,HCl,HF,HrO,
Glass
HNOy'HF
palladium,
Gold,platinum,
ceramic Aquaregra
Silver
HNO3
Plastic
H,SO. H,O,, HNO3,HCI
Others
Anyacidto totaldigestion
c o m o a n v ; "I : : , 1 , r : - i : I r l J i , 1 ' r t i . , : : I t r ' r . r i
asub]adlo'6cenelacoid[omds
Cool,filterdigestate
1:, r':I tr!l{'
colordevelopment
measurethe absorlcance
at g0 nmby UV-VIS
TestReport
No.I CEl2011l42UO Dale 2011t04t27 paoe| 5 of I
HITACHICHEMICALCO., LTD.
1772.1KANAKUBOYUUKI-SHIIBARAKI,307-0015,JAPAN
||fl11 rflr] ||l|
'1) Thesesamples
weredis6olved
totattyby pre-condilioning
methodaccording
to betowflow
cnan.
yang
2) Nameof thepersonwhomademeasurement
Ctimbgreat
3) Nameof thepersonin chargeof measurement:
TroyChang
FlowChaftof digestlonfor the etemenbanatystspertormodby tCp-AES
Aciddigestion
by suitable
aciddepended
on
different
samplematerial(a6
belowtable)
1) AlkaliFusion
2) HClto dissolve
Steel,copper,aluminum,
solder
Aquaregia,HNO3,HCl,HF,HrO,
Glass
HNO3/HF
Gold,platinum,palladium,cefamic
Aqua fegia
Silver
HNO3
Plastic
HrSO4,HrO?,HNO3,HCI
Others
Any acidto totaldigestion
tiir,rr_ii,:,., 1J.1,I-ri L:.ri
c o m o a n; iv, r
rhsad,mm, sc&d byb.cmpa
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rh sbd Gpon€nidb
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tld,ois I any rhs companyssoac
lL
'-:r i l, lili.alru6r0:rre
TestReport
No.I CU2011l42646 Date:2011104127Page:6 ot A
HITACHI
CHEMICAL
CO.,LTD,
1772.1KAMKUEOYUUKI-sHIIBARAKI,
307-0015,
JAPAN
[ffI
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ll
Analyticalf,ow chartof halogencontent
1) Nameofthepersonwhomademeasufement
RitaChen
2) Nameof thepeEonin chargeof measurement
TroyChang
$mple pretreaiment
/ Separ€tion
Weighting
andputtingsamplein cell
OxygenBombCombustion
/ Absorpton
Dilution
to nxedvolume
Analysis
wasperfomedby lC
c o h @ i yr i . . I
i: i tli lili,li
il,..r('r,r,iii:ii,i
oyeqedb G 6ercrcond r ois oi s
s u b ] e d l o T e m s a n d c o d l o i 6 ' o l E A t € d o i s d r o r . l o h e l m L b l o i o i ' a b l J
Mlmbe,orrhe%!crcupiscssal
Test Report
No.: CEl2011l42U6 Dale:2O11lMn7 Pagei 7 of 8
HITACHICHEMICALCO-, LTD,
1772-1KANAKUBOYUUKI-SHIIBARAKI,
307-0015,
JAPAN
|r||[]||
Analyticalflow chart
1) Nameof thepersonwhomademeasurement:
RomanWong
2) Nameof thepersonin chargeof meaaurement
TroyChang
r Test|tems:PBB/PBDE,
TBBP.A-bis
Firsttestingprccess-----f OplionatscEen
process--...
proc€ss-.>
Confi.malion
:ji!!r
Screenanalysis
1' ' ' ' ' ' . . . . . . . . . . . .
SamDle
extactionmethod
Concentrate/Drlute
Extractedsolution
t
Filter
V
Analysis
by GC/MS
lssueReport
r_ ri i ,1, :: i,:rrtr i:
.yslqedb
. r. { .l.i;,.:l
c Gener,rcd.d r dis di s
poisb]ly€locc|3dandlh3ddfum
1_n,:i
l:: r ';;1..ii+s6olxe
|lfltt!
Test Report
No. : CE12011142646Date:2011104127Page: 8 of 8
HITACHICHEMICALCO,, LTD.
1772.,IKAMKUBO YUUKI-SHIIBARAKI,
307-0015,
JAPAN
'. End of Report *'
c o m p . n+yj i ! r
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TestReport
No.CANEC1003736601 Date:01 Sep2010
Page1 of 5
GEJIUZlLl l\,llNlNG&S|\rEL
TINGCO.,LTD
HUOGUDU,JIJIE
TOWN,GEJIUCIry,HONGHEZHOU,YUNNAN
PROVINCE
CHINA
The following sample(s)was/w€re submittedand identifiedon behalf of the clients as
TIN
SGSJobNo.
SGSInternal
Reference
No.
Dateof SampleReceived
TestingPedod
127M6A9- cZ
4.1
30Aug2010
30Aug2010- 01Sep2010
TestRequested
Selecledtest(s)as requestedby client.
TestMethod
Pleasereferto nextpage(s).
TestResulb
Pleaserefefto nextpage(s).
Conclusion
Ba6edonthe performedtestson submitledsample(s),the results conply
wlththe RoHSDireciive200295/ECandits subsequent
amendments.
Signedfor and on behalfof
scs-csTcLtd.
'4
)
(r,rk
TrophyZhang
Sr.Engineer
idocum.i6 rit doclm.nr{nnor b.
ryroh..rmpr!(tr.d.d.
l$xdlRa4sdrPtrolllEdllnildrt&0tiFutoi$dolpurorr
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I (F20)82015119 s cn!F.@n
510€63I (8&?0)&155555
. !$..lrE€A.ff
t!!I:510363 r e2qe2155sssr {6-20)3207sr13
M6mb6/olrhsSGSGrcuD
ISGSSA)
TestReport
No.CANEC1003736601 Date:01Sep2010
Page2 of 5
Test R€sults:
lD for specimen1
Desoriptionfor specimen '1
cAN10-037366.001
Silvefymetal
Rol{S Di€di'r6 2@2/95/EC
Test ltem(s)
Cadmium(Cd)
Lead (Pb)
Mercury(Hs)
(CrVl)by
Heravalent
Chromium
boilingwaterextraction
Sumof PBBS
Monobrcmobiphenyl
Dibromobiphenyl
Tribromobiphenyl
Tetrabromobiphenyl
Pentabromobiphenyl
Herabromobiphenyl
Heptabromobiphenyl
Octabromobiphenyl
Nonabromobiphenyl
Decabromobiphenyl
Monobrcmodiphenyl
eth€r
Dibromodaphenyl
ether
Tdbrcmodiphenyl
elher
Tetrabromodiphenyl
ether
Pentabromodiphenyl
ether
Hexabromodiphenyl
ether
Heptabromodiphenyl
ether
Octabromodiphenyl
ether
Nonabromodiphenyl
ether
Decabromodiphenyl
ether
Unit
msiks
mgfts
msr(g
ms/}(g
msikg
mgikg
msfts
msikg
mg/Kg
mg/Kg
mg/Kg
mdks
mgna
msfts
msfts
msr(g
msiks
msr(g
mg/kg
mdkg
mgkg
mdks
mg-fts
mgKs
ms&s
yabl.drorsc.i.,.
'B.r &un.d. t.utl.d
.utl.d b trr.nd
trr.nd
rid iuidlei
isu.; d.ii.d s.dn
Test Method(Reference)
IEC62321:2m8,ICPOES
IEC62321:2m8,ICP-OES
IEC62321:2008,ICP-OES
IEC62321:2008,
UV-Vis
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
IEC62321:2008.
GC-MS
IEC62321:2008,
GC-IIS
IEC62321:2008,
GC-MS
IEC62321:2008,
GC-MS
IEC62321:2008,
GGMS
IEC62321:2008,
GGMS
IEC62321::D08,
GGMS
IEC62321:2008,
GGMS
IEC62321:2008,
GC-MS
IEC62321:2008,
GC-MS
o6h.tu
ontsnyb e.
Limit
100
1000
1000
Negative
1EC62321:2008,
GC-MS
1EC62321:2008,
GC-MS
IEC62321:2008,
GC-MS
IEC62321:2008,
GC-MS
IEC62321:2008,GC-IIS
IEC62321:2008,
GC-MS
1EC62321:2008,
GC-MS
IEC62321:2008,
GGMS
IEC62321:2008,
GC-MS
IEC62321:2008,GC-IIS
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TestReport
No.CANEC1003736601
Date:01Sep2010
Page3 of 5
Note:
1. mg/kg= ppm
2-N.D.= NotDeteded(< MDL)
3. MDL= lrethodDeteclion
Limit
4. o = Spot-Test:
Negative= Absenceof CrVlcoating,Positive= Presenceof CrVlcoating;
(Thetestedsampleshouldbefurthervedfiedby boiling-wateFextraction
methodif the spottest result
is negativeor cannotbe confirmed.)
Boiling-wateFextr€ction:
Negative= Ab6€nceof CrVlco€ting
Positive= Presenceof CrVlcoating;the detectedconcent€tjonin boiling-water-extraction
sotutionis
equalor greaterthan0.02mgikgwith50 cm. samplesurfa@area.
Storageconditions
andproduction
dateof thetestedsampleareunavailabte
andthusresultsof Cr(Vl)
representstratusof the sampleat thetimeof testing.
5. # = Positiveindicatesthe presenceof CrVlon thetestedareas.
Negativeindicatesthe absenceof CrVlonthe testedareas.
6. "-" = Notregulated
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TestReport
No.C4NECl003736601
Date:0'1Sep 20'10
Page4 of 5
ATTAC*I I'ENTS
RoHST.rt|tg Ftor Chrt
1) Nameofthepersonv{honadetestng:Betta\ ang / cLreyyu / Rosszhan
yu / Ryanyang
2) Naneofthepersmin chargedtestng:Adams
3) TtEsesemples
*e€ dissokBdtotall/
bypra-conditionhg
me&odaccording
- to belowflowch*t
(C€+ andPBBS/PBDES
t€lt method
€xctud€d.
Sample
Meagurement
Pb/cd/Hg
PBB'PBDE.
Aciddigestonwfth
nicrorav€r'hdplate
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Positive
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16agEnt
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egativ€
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ertlaction
1) Alkali Fugion/
DryAshing
2) Acidto
Adding1,5diphenylca|bazide
for color
clevelopmEnt
dissohve
Adding1.5diphBrMcatbazide
for color
development
y.u!hd roir.o.i.. cddrdorots.
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A red color
indicatesthe
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lf necessary,
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TestReDort
No.CANEC
1003736601
Date:01Sep20'10
Page5 of 5
Samplephoto:
cANEC1003736601
cAN10-037366.001
SGSauthenticate
thephotoonoriginat
reportonly
"* Endof Report"'
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M0mb€rolthoSGSGroup(SGSSA)
Littelfuse, Inc.
Data No.: AD120-ICP-1
Date :
2010/12/3
Result of ICP test
Product No.： WF001003
Customer Type No.： RC109A
We report the results of the tests about this product as below.
Name of the part
chip
Result（Detection Limit）　Unit：ppm
Substance
Name of the Maker
Name of the material
Items
silicon
Result
SANYO-CH
Pre-conditioning
SANYO_A1
Method
Measurement Date
Report No.
Measurement Institute
Cd
Pb
Hg
Cr+6
PBBs
<2
<2
<2
<2
<5
PBDEs
<5
acid digestion
acid digestion
Microwave decompos
Alkali fusion
Soxhlet method
Soxhlet method
ICP-AES
ICP-AES
ICP-AES
UV/VIS
GC/MS
GC/MS
2010/08/24
2010/08/24
2010/08/24
2010/08/24
2010/08/24
2010/08/24
CE/2010/84322
CE/2010/84322
CE/2010/84322
CE/2010/84322
CE/2010/84322
CE/2010/84322
SGS Taiwan Ltd.
SGS Taiwan Ltd.
SGS Taiwan Ltd.
SGS Taiwan Ltd.
SGS Taiwan Ltd.
SGS Taiwan Ltd.
Akira.Nishiguchi
General Manager
Environment, Health & Safety Promotion Dept
Quality , Environment & CS Division,
SANYO Semiconductor Co.,Ltd.
Contact Window
Mitsumasa Takano
e-Mail：[email protected]
Address ： 1-1-1 Sakata, Oizumi-machi, Ora-gun, Gunnma-ken, 370-0596 Japan
1/1