ICP Test Report Certification Packet
Company name :
Littelfuse, Inc.
Product Series:
3AB Fuse
Product #:
505xxxP
Issue Date:
August 9, 2012
It is hereby certified by Littelfuse, Inc. that there is neither RoHS (EU Directive
2002/95/EC)-restricted substance nor such use, for materials to be used for unit parts, for
packing/packaging materials, and for additives and the like in the manufacturing processes.
In addition, it is hereby reported to you that the parts and sub-materials, the materials to be used
for unit parts, the packing/packaging materials, and the additives and the like in the manufacturing
processes, are all composed of the following components.
Issued by:
<Global EHS Coordinator>
(1) Parts, sub-materials and unit parts
This document covers the 505P 3AB Fuse RoHS-Compliant series products manufactured
by Littelfuse, Inc.
＜ Raw Materials Used
Please see Table 1
(2) The ICP data on all measurable substances
Please see appropriate pages as identifed in Table 1
Remarks：.
Form 585-047 Rev. A
1
2/21/06
Table 1: List of Raw Materials covered by this report
Total Parts
1
2
3
4
5
6
7
8
Raw Material Part Number
910-005
C610 (909-162/909-532)
YTW102 (692535-003)
3M 3779-PG (087244)
091251
082xxx
920-481-00x
934-054/934-055
Raw Material Description
Cap – Fuse copper shell
Ceramic tube - Body
Solder
HMA
Sand
Wire- Ag Plated Cu
Pure Silver Sheet Argentine
Overcap
2
Page(s)
3-6
7-30
31-35
36-44
45-50
51-60
61-64
65-68
nov'
TESTREPORT
NO.jA002E11121307'1R02
page1of4
DaG:Dec.t5,2Oi1
Custom6iSuzhouFuHongEteclronic
IndustialCo.,
L6.
AddT€sg:
NO.89WEIDUROAD,WANGTINGTOWN.
XIANGCHENG
oIsTRIcT.sUzHoU.CHINA
Reporton tie subnitiedsamptes.idto be
Samplename:Coppershell
Modsl:/
Materlal:/
D€cripiion:/
Buyer:/
Supplier:/
SamPlercceiwd date:Elec.'13,2011
T€dng poriod:FromDec.13,2011
lo Dec.15,2o.l1
T€lino Reou6ted
As sp€cified
by client,to deteminethe L€ad,Cadmium,
Mercury
& Hexavat€nt
Chromilmcontentantheslbmifiedsamptein
accordancewilh Dircctive200295/EC(RoHS).
Te.Unomethod:
T€slingliem
Lead(Pb)
IEC62321:2008,
sectionI
IEC62321:20t,3,
s€clion9
cadmium(cd)
llercury(Hg)
(Crl'1)
Chromrum
IEC62321:2008,
section7
IEC62321:2008,
AnnexB
Measuring
instrument MQL
rcP-oEs
2mg/kg
tcPoEs
lcPoEs
2 mg/kg
2 mg/kg
0 o2mgkg'
leg
-' 0.02mg/kgreGrclo theMQLof sampte
extraction
tiquid.
99!9!cis!i
-When
tesledas specined
thesubmi(ed
sample
compli€d
wilhthercquirements
of commission
Decision
of 18Aug2005
amendingDirective2002/95/ECnotiliedundefdocument2005/618/EC.
---FOR
Pro,ect
Leader
(Engine€r)
FURTHERDETAILS,PLEASEREFERTOTHEFOLLOWNGPAGE(ST**'
/{bjA-L
J4
,ffi:::j:,,44
lnsoected
bv
,**'*''*,n-, [,[rlg-,iti-Y\
BRANCIi
SHENZHEnlAOVTESTINC TECHNO!OGY CO..L.TD,KUI\ISIIAI\I
Holline
8 6 . 5 1 2 . 5 5 1800 0 0
nov.
TESTREPORT
NO,:A002E11121307-1
R02
Weighthesampleinto
Add the digestionsotutionithe
vesselis healeduntilthe sampl€
hasb€€ndissolved
F*_-lTo
Tesledby ICP-OES
Content(MelalsubstEle)
Add the digeslionsolutjon,ctose
The sampleis digesredin the
the micfowaveves:€|.
mrcrowave
oveniollowinga sp€citic
program.
decomposilion
+
Coolingthe vessel,fltet washedand
filled to the ma* with distilled wat€r.
To Detenn
exavalenl
Chromium
(bojtingContent
(Metatsubstrate)
wateFextraction):
Heat50 mL of Dl walerin the
samplein the beaker.
beakerto boilingior 10 min
F;;1.To Delemine
Remove
thesample,
andcool
thebeakerto roomlemperature,
anddothecolorleadion
Tesllh€s€mplesolution
andthe0.02
mg/kgstandardsolutionby UV-VIS.
andl\Iercury
Content(Plaling)
andlilled
___+l coorins.rirteiwashed
l_-_----|lresteo oy l+fl_*l
t ot h em a * w i tD
ht w a t e r .
l r n " r , u r n " nI , l " * '
I
I
SHENZHsN AOV TG6TINGICCHITOI"OGYCO.,L'O.KUNAHAN BRANCH
a
I
Hotline
86-512-551
80 0 0
nov'
TESTREPORT
NO.i4002E11121307-rR02
oste:oec15,2011
5. ToO€temineHexavalent
Chromium
Contentincolorlessand cotorcdcnromaEcoatingon metats(Plaljng)
,':"j":::i
v^02
lf the tesl rcsultis posilive,
the sampleis considercdto
havehexavalenl
chromilm
Place
1-5
Compare
the
Eoiling- wateF ext€ctjon
prccedurcshall be usedto
andlhe 0.02mg/(q
standa.d
solution
lfthereis int€rference
or it is hardto decidewhether
thesampl€havetie h€xavatent
chromium
5 2 Eoilingwat6Fextraction
Tako the (50+5) cm'?
Heat50 mlof Dlwaier in the
samplein the beaker.
beakerlo boilingfor 10 min
Removetie sample,and cool
lhe beaksrto roomtempeEture,
and do the colorreaolion
Testthesamplesolution
andthe0.02
mg/kgstandard
solution
by UV,VIS.
T€t Re6ult3:
Unit
Limil
Substrate
Plating'
N.O.
N.O.
N.D.
Negalive
Lead(Pb)
(cd)
Cadmium
mg/Kg
(Hg)
lvercury
mgn(]s
1000
100
1000
chromium(Crl'I)
mg/Kg
1000
mg/Kg
Result
RoHS
N.D,
N.D.
N.D.
Negative
S!IENZHENAOV'CSTING IECIINOIOGY CO..ITD,KUNSHAN gNANCH
Hotline
a6-512-551
80 0 0
novTESTREPORT
NO 4002E11121307.rR02
'The new RoHSdirective2011/65/EU,on Jul. 21 2011 comeintolorce
,
on Jan.03, 2013 the fomat imptementation.
Direclive
2002,95/ECshallbe rcpeatedsimuttaneousty.
-specimens,whichrequestedto determineLead,cadmiumand l,rercury
conteni,havebeendissorvedcomprererv
-N.D.=notdetected(<tltoL)
-MOL=ntethodOuantitation
Limit
-Negative=Absenceof Cr (VIir
PositivFPresenceofCr (\ll)i
Unc€rlain=can not verifywhetlerthe samptehaveHexavatent
Chromiumby spoltest.
(The test€d sample should be fufthet verifiedby boiling-waler-€nraction
method if the spot test resutt |s uncertainor
negalive.)
-'The tesl is basedon lhe followingassumption:Thesampteptatingis a singtetayefand
each paft is uniform.The tesr resutt
maybecannotslandbr lhe physicaltruthofsampteptating.
Photograph
ofSample
Coppershell
ARANCTI
SHENZHEN
AOVT€STINGTECHNOLOGYCO.,IID,XUNSHAN
e!:-"Jllls,.*
Validi
ForQ
Please
Test Report
own
SGS
No. : CE/2012I14843ADare.2O12J02104Pagel.1o124
tll||Ill
CERAIVTEC
GIVBH
MULTIFUNCTIONAL
CERAI/IICSLUITPOLDSTMSSE
15 D.91207LAUF,GERMANY
ltltt]r
The following sample(s)was/u,€resubmiltsd and identifiedby/on behalfof the client as:
Sample Description
Stle/ltem No.
SampleReceivingDate
TestingPerjod
CERAMIC
c610
2012,01t30
2012J01| 30 TO 201Z 02t04
Te3tRe.ult(s)
: Pleasereferlo nextpage(s).
Conclu6ion
Lead,
: Bas€dontheperformed
testsonsubmitted
samples,
thetestresults
of Cadmium,
lvlercury,
Hexavalent
Cf(Vl),PBBS
andPBDES
comply
withthelimit6assetby
Ch.omium
RoHSDireclive
Annexll; recasting
200295/EC.
2011/65/EU
Sg|rad for||d
Cltorlcd Lborlbry-
T.Fd
comDafrAilB6;RE ,tRd-LXlAllHll lftlCt
!IAIA|
lq"1 )19{
"SFiAE
Th3dodm6dE6ebyfuconMy&bjedbi6Gengg|cddfooi3ds.s6pii6oveis43Eisb.on4wd
aadrsd tui i'no
t'lnld d6 kru6 doinoddroEi Adyhoderot hB tuhed
mt and
f sr rrE comp.nr'EE r.rspombrl'
"ih
comFry Atu sadoEs
. rodon torcsryor rslff€ton d rhe6ibd or sD
nd ofl.id.6 m.y e p,@dk
ih6 r ft or rtsiftmton
.*n, ;S-:HJ'Y
I iH::::gj;t.*t;:,$;;
'-;*,t^--
"
ro s. rd
r !6!a {Brts
***'*
Test Report
No.: CEJ2012/14843ADale| 201Z0ZM
Page: 2 o f 2 4
t]r||lrrfl||fllllt
CERAI\,ITEC
GMBH
MULTIFUNCTIOML
CERAITIICS
LUITPOLDSTMSSE
15 D.91207LAUF,GERIJANY
IeclBecc$GL
PARTNAMENo.l
Test ltem(s)
I
WHITECERAIVIC
lJnit
MDL
Method
R€ult
Limit
l{o.t
2
n,o,
100
2
178
1000
2
n.o.
1000
2
n.d.
1000
0.5
n.d.
mS/kS Withfeference
to USEPA3540C
0.5
n.d.
method.
Analysis
waspedormed
by
GC/MS.
mg/Kg Withreference
to uS EPA3540C
method.
Analysis
wasperformed
by
GC/|VS.
5
n.d.
0.01
n.d.
10
n.d.
Cadmium(Cd)
mS/kS With referenceto IEC 62321:2008 and
perfomed by ICP-AES.
Lead (Pb)
mg/Kg With referenceto IEC62321:2008 and
performedby ICP-AES.
lrercury(Hg)
mg&g Withreferenceto IEC62321:2008and
performedby ICP-AES.
Hexavalent
ChromiumCr(Vl)
mgikg Withreference
to IEC62321:2008and
pedormedby UV-VIS.
Polychlorinated
Biphenyls(PCBS) mgikg Withreference
to USEPA3g0C
(cAS No.:1336-3G3)
method.
Analysis
wasperformed
by
GC/rrs.
Polychlodnated
Terphenyls
(PCTs)
Polychlofi
natedNaphthalene
(PCNs)
oa
Alkanes,C1Gl3, chloro(Shoft
With referenc€to US EPA 3540C
ChainChlodnated
Paraffins)(CAS
method.Analysiswasperformed
by
No.:8553t0a-8)
GC/MS.
Pe|fluoroodanesulfonates
mgKs With referenceto US EPA 3540C:
(PFOS-Acid,
MetalSalt,Amide)
1996 methodfor PFOSContent.
Analysiswasperformed
by LC/MS.
PFOA(CASNo.:335{7-1)
m9Kg With referenceto US EPA 3540C:
1996methodfor PFOACont€nt.
Analysiswasperformed
by LC/MS(CASNo.:50{0-0) mg/kg With referenceto ISO 17226-11200$.
Formaldehyde
Analysiswas perfomed by HPLC/DAD.
Analysiswasperformed
by FTIRand
FLAMETest.
cmEm6, REest hElEielifidizliLbq.6fi-{s6-"
! . ? -" q r ' i
Er,]t&
fttrerdEE$dbyTconp'
I ohF d r.rr'r, 'n&nre'r
a{r]'d'do1's.!
e -.d w's'1 ary -016' d dBderuddad!e
tan*don ft6 a.B no ai h.r dod
comEry ary un&ibai srbEron bM
ori'iBrelon d b6 onbnr d.F
alnnr+nuunar-iI
q
10
3
n.d.
Negative
hr .
oodn.da Ti e oo@nofl @nd F sd
arapdciiv'rawd/firtd'rirr**Hmn:fiE
G
TestReport
Page:3 of 24
D e:2012102104
No.:CE/2012I14843A
Result
Test ltem(s)
Unit
Melhod
MDL
(CAS
BBP(Benzylbutylphthalate)
No-:85-68-7)
DEHP(Di-(2-€thylhexyl)
phthalate)
(CASNo.: 1'17-81-7)
DIDP(Di-isodecylphthalate)(CAS
No.:26761-40-0)
phthalate)
(CAS
DINP(Di-isononyl
No.:2855312-0)
phthalate)
(CAS
DNOP(Di-n-ociyl
No.:117"84-0)
(CASNo.:
DBP(Dibutylphthalate)
%
Withreference
to EN 14372.Analygs
was performedby GC/lVlS.
Withrofefenceto EN 14372.Analysis
wBspedormedby GC/lVlS.
With referenceto EN 14372.Analysis
wBspedormedby GC/IVS.
Withreference
to EN 14372.Analysis
rvasperformedby GC/MS.
Withreference
to EN 14372.Analysis
was perlomed by GC/MS.
0.003
n.d.
0.003
n.d.
0.01
n.d.
0.01
n.d.
0.003
n.d.
0.003
n.o.
0.5
n.d.
0.5
n.d.
0.5
n.d.
0.03
n-d.
0.03
n.d.
%
oa
y'Vith
Analysis
reference
to EN14372.
/vasperfomedby GC/MSl\Ionomethyl
dibromodiphenyl
mg/Kg Withreference
to USEPA8270D
methane(DBBT)
method.Analysiswasperformed
by
Go/tlls.
l\ronomethyl
mgikg Withrefefence
to USEPA8270D
dichlorodiphenyl
method.
Analysis
w€sperfomed
by
methane(Ugilec121)
GC/ttIS.
Monomethyl
tetrachlorodiphenyl mgikg Withrefefenceto USEPA8270D
(Ugilecl41)
methane
method.
Analysis
w6spefomedby
Go/tlls.
llll
|l]|||tllllll
CERAITTEC
GltlBH
MULTIFUNCTIONAL
LUITPOLDSTRASSE
15 D.91207LAUF,GERMANY
CERAI\/IICS
No.l
Limlt
u-74-2)
Organic-tincompounds
IributylTin (TBT)
IriphenylTin (TphT)
Halons
(CASNo.:353-59-3)
Halon-12'11
Halon-13o1
(CASNo.:75-63-8)
(CASNo.:124-73-2)
Halon-2402
mgikg Withrefefenceto DIN38407-13.
Analysiswas performed
by GC/FPD.
mgKs With reference
to DIN3840713.
AnalysiswEsperformed
by GC/FPD.
n.d.
mg/Kg with referenceto US EPA 5021
melhod.Analysiswas performedby
GC/MS.
mg/Kg With referenceto US EPA 5021
by
method-Analysiswas pertormed
Gc/tlls.
mg^g with refercnce
to us EPA5021
waspedormed
by
method.
Analysis
GC/tis.
redu€d..sdntur
comEfr [}ll B E$3! nE-L1l{91:!l:dzttfla
'mEn
a3 ndmsa
! 6_sd 4 bs
E
l Hd- lH4
-
l*lEii9 E
!.r dd*
<Bd4€
h.rr
i-*f,r
b r d or ib 'ftiwdo1
oits so {rhi
'dnffioi
tum ssEsm aii,ffi' nohbaiodcrm!
-ne b6rtuedori
comp.ny er mr6od&
a radoi
ta.ry o, tal6h6doi d rb 6ibd
or s
i "I f, I ft{.
d tE oodafl
n.d.
wLhdl rior k6
pomE! on d t6
;Bousd r.r 'do
a hrF. r Lbai /iurfi#JtE*$6nd4sct
TestReport
Pege: 4 d 24
Dale:2012102104
No.: CE/2012/14843A
rt|| tt]l
CERAIVTEC
GIVBH
LAUF,GERMANY
LUITPOLDSTRASSE
15D-91207
MULTIFUNCTIONAL
CERAI\/IICS
Test ltem(s)
Unit
Halog€n
(F) (CASNo.:
Halogen-Fluorine
14762-94-a)
(cl) (cAs No.:
Halosen-chlorine
22537-15-1)
(Br)(CASNo.:
Halogen-Bromine
10097-32-2)
(l) (CASNo.:
Halogen-lodine
14 24+81
MDL
Method
with ref€renc€
to BS EN 14582:2007Analysiswas performedby lC.
mS/kS Withreference
to BS EN 14582:2007.
Analysis
was performed
by lc.
mgKs With referenceto BS EN 14582:2007.
Analysiswaspedormedby lC.
mgKs r'Vithreference
to BS EN 14582:2007.
qnalysiswasperformed
by lC.
mg/kS
Result
No.l
50
50
n.d.
50
n,d.
50
n.o.
A3b€Bto3
AclinoliteICASNo.:77536-664)
Amosite(CASNo.:12172-73-5)
%
(CASNo.:77536-67Anthophyllite
5)
(CASNo.:12001-29-5)
Chry6otile
%
(CASNo.:12001-284)
Crocidolite
%
Tremolite{CASNo.:7753&686)
%
comD.frKJ AF.fl8n d H:8Rl{6,!
^i-ttlg(
t E-{R
Withreference
to EPA600/R-93/116
method.Analysiswas performedby
SM, PLMandXRD.
With referenceto EPA 600/R-93/116
method.Analysiswas performed
by
SM, PLMandXRD.
with refeence to EPA600/R-93/116
method.AnalysiswEsperformed
by
S[4,PL[4andXRD.
Negatave
Withreference
to EPA600/R'93/116
method.
Analysis
wasperformed
by
S[,],PL[,]andXRD.
Withreference
to EPA600/R-93/116
method.Analysis$raspedormedby
SM,PL[,]andXRD.
Negative
Withreference
to EPA600/R-93/116
method.AnalysiswEsperfomed by
SNl,PLNIandXRD.
Negative
l_" rE/r:
Negative
Negative
Negative
l"rJ n E{.
M€'rbqod.al'.€.b.d1qu
'miirnon or I rii ly. knnnfr€ron
end inld cds r$u6 dornd 6eF n Ad ho der or his dodmd
d.lftdi!'fti@lonf|rad#i
Fnldonbm.^esnoaida'
ndtr and od'G.tr3 ida, bs.6ieddi
a1 ruuroda-d a Fdoi,o$ry
.mFry
o.Elserol
d rhs @-6a o' I
effinr+Irror/rs|laa%|
tded
that into
' q!!g1ryr!:: ! li ll!'l5!:l?! NqrdF c! r'E{ / rirlrnsirL**FErn}t'n
l]l
Limlt
Test
Report
24
Pase:5of
No.: cE/2012/14843A
Date-2o1zo2to4
|ll
CEMMTEC GMBH
15 D.gl207LAUF,GERMANY
I\4ULTIFUNCTIONAL
CEMMICS LUITPOLDSTMSSE
Test liem(s)
Sumof PBBs
Monobromobiphenyl
Dibromobiphenyl
Tribromobiphenyl
Tetrabromobiphenyl
Pentabromobiphenyl
Hexabromobiphenyl
Heptabromobiphenyl
Oclabromobiphenyl
Nonabromobiphenyl
Decabromobiphenyl
Sum of PBDE3
Monobromodiphenyl
ether
Dibromodiphenyl
ether
Tribromodiphenyl
ether
Tetrabromodiphenylether
Pentabromodiphenyl
ether
Hexabromodiphenylether
Unit
MDL
lllethod
5
With referenceto IEC6232112008and
mg/Kg perfofined
by GC/MS.
5
5
5
5
5
5
5
5
|llt
R€sult
No.{
n.d.
n.d.
n.d.
n.d.
n.d.
n.d.
n.d.
n.d.
n.d.
n-d.
n.d.
5
5
5
5
5
5
n.d.
Heptabromodiphenyl
ether
5
n.o.
Octabromodiphenyl
ether
Nonabrcmodiphenyl
ether
5
5
Decabrcmodiphenyl
ether
5
n.d.
n.d.
n.d.
3
n.d.
AZO
to LFGB82.02-2.
1):4AIIINODIPHENYL(CASNo.l mg/kg Withreference
Analysiswasp€rfomedby GC/MS.
92-67-1)
m9/K9 With referenceto LFGB82.02-2.
2)i BENZIDINE(CAS No.: 92-87by GC/lvlS.
Analysiswasperformed
5)
3): +CHLORO-O-TOLUIDINE mg/Kg /Vith referenceto LFGB82.02-2.
Analysiswas performedby GC/MS.
(CASNo.:95692)
(CAS
4):2-MPHTHYLAIIINE
No.:91-59-8)
to LFGB82.02-2.
msftg with reference
Analysiswas perfo.medby GC/l/lS.
to LFGB82.02-2.
(CAS mg/kg with reference
5): O-AIVINOMOToLUENE
Analysis\ /as performedby GC/MS.
No.:97-5&3)
a;;;;hi
rtErca Di'-t+4r{.4-6HEc
(4d-r8..".:'-}
n,o,
n.d.
n.d.
n.d.
n.d.
3
3
n.d.
3
n.d.
3
n.d,
ro r)rl&"
inhel!lEI.'*i.d*d.dno'-*""d."**dcoturd;s
irii6iim-"j"in-inii*ij'iiilb''bnF.''.'[email protected]|fma.Doi!as1g{ws!sods4€i!g
]ii;;'6iifoidhnic!!aidiiirnidoili$@dmdMdn:ii;h;bl's];di{'md,i'ddmdi
ii
bs In !d c.a.n6rcr;i
i , i i , l i n d r,;"
,nii"e-- -r *"".i
;1;;
;-o
d, r*' "qtu ro d, odotu Ln6 h. t'nsdoi ooer.ma
baea d b 3'* * d ' r d;;:;;;';;;;l;
.o.oan, ay ..arho-a ,! s d-
-6{0''esb6d*w43@n|f!-!j'dgldg::ll
6cFaf,do.o!*rcdd6.dd
ni s [email protected] @nr b' €
doan"i4,"; ad a.o ot
llllll
Limit
1000
'1000
TestReport
No. ICE/2012114843ADaie:2O1Z0ZO4 Paoe:6 ot 24
tl]tI|tt
CERAIVTEC
GITIBH
MULTIFUNCTIOML
CERAIIIICSLUITPOLDSTMSSE
15 D-91207LAUF,GERIVANY
Testltem(s)
Unit
6)i 2'AMINO-4-NITROTOLUENEmgftg
(CASNo.:99-55.8)
7): P-CHLOROANILINE
(CASNo.: mdks
10647-8)
8): 2,4-DIAMINOANISOLE
(cAS
m9Kg
No.:615-05-4)
mg/Kg
9): 4,4L
DIAIIIINODIPHENYLMETHANE
(CASNo.:101-77-9)
10)r3,3'-DICHLOROBENZIDINEmg/kS
(CASNo.:91-9+1)
11): 3,3'-DIMETHOX/BENZIDINEmgikg
(CASNo.:11990-4)
12):3,3!DIMETHYLBENZIDINE mg/kg
(CASNo.:11993-7)
MDL
Method
With refercnceto LFGB82.02-2.
Analysiswas performed
by GC/MS.
With reference
to LFGB82.02-2.
Analysisw€sperfomedby GC/lVlS.
With reference
to LFGB82.02-2.
Analysiswasp€rformed
by GC/|\IS.
With reference
LFGB
to
82.02-2.
Analysiswas performedby GC/I\IS.
3
No.1
3
n.d.
3
n-d.
3
n.d.
Withreference
to LFGB82.02-2.
Analysiswasperformedby GC/MS.
3
n.d.
With relerenceto LFGB82.02-2.
Analysis\ /as performedby GC/MS.
3
n,o,
3
n.o.
3
n.d.
3
n.d.
3
n.d.
mgftg Withrcfercnceto LFGB82.02-2.
Analysiswasperformed
by GC/MS-
3
n.d.
mgKg With reference
to LFGB82.02-2.
by Gc/lvls.
Analysiswas performed
3
n.d.
3
n.d.
3
n.d.
3
n.d.
3
n,d.
Withreference
to LFGB82.02-2.
Analy6iswasperfomedby GC/MS.
'|3):3,3-DlMETl-lYL-4,4'msfts With referenceto LFGB82.02-2.
DIAMINODIPHEI.IYLIIIETHANE
Analysiswaspertormed
by GC/lVlS.
(CASNo.:838-8&0)
(2]!IETHOXY- mg/Kg A/ithreference
14):P-CRESIDINE
to LFGB82.02-2.
(CASNo.:
5-METHYLANILINE)
Analysis
waspedomedbyGC/l\Is.
120-71-8)
(215):4,4'-[,IETHYLENE-BIS(CASNo.:
CHLOROANILINE)
101-14-4)
(CAS
16):4,4LOXYDIANILINE
No.:101-80-4)
(CAS
17):4,4'-THIODIANILINE
No.:13965-1)
(CASNo.:9$
18):O-TOLUIDINE
Result
mg&g With referenceto LFGB82.02-2.
||ttll!t
Limit
Analysiswas performedby GC/MS.
mg/Kg
5s)
Withreference
to LFGB82.02-2.
Analysiswasperfomedby GC/IVS.
19):2,4-TOLUYLENEDIAMINEmg/kg With .eferenceto LFGB82.02-2.
(CASNo.:95-80-7)
Analysiswas perfonnedby GC/MS.
20):2,4,5-TRIItIETHYLANILINE mg/Kg
(CASNo.:137-17-7)
(CAs No.:9G
mg/kg
2'l): O-ANISIDINE
04-0)
With referenceto LFGB82.02-2.
Analysiswasperfomedby GC/lVlS.
y]/ith.eferenceto LFGB82.02-2.
Analysiswas performedby GC/MS.
inALF,{rr!-i-Eeaa
tdd- iMt, lg6"+_I T lil:' u?
fi;6d,n;dB;;;'iti;@ind]li'ibd.o'i..fgeicsdnf.,*rn6qrbilode,'6|.d.o'Gqus
ed io,asdtr'ctud6.r.n!
*tidri,Tds.{cdmiomb-6d
;i;bn;]ni'i;;.ii'nd6'ilnijii'nd;fusd.mn60DDnAilhdde.dFEoodnaa''.oIsdF,''ft
-€conFnvt{ts@o13b"t'
-mdor
ary
hs m' d tr! 'nbii$ron 6k and*'rin h 'redlrsrtr
adb.cpdLddrcpl|1tr|
Jiii'i''neton a L* ontoni;ii,pp*Eme t 'h s [email protected] k mrdd sna or*dare mai bo prcedd
ii;i'inil;lii;dn;;a;G;;;1iiiriiry
];i1ira&eD6ri^;i
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iiij;j;;:;;;t
'l;idD;;;t
i;;J;
d3rcE
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1.p.n6-bs
Test Report
No. : CE/2012/14843A Dele : 201210204 Page | 7 of 24
l]|||lll
CERAMTEC
GI/lBH
15 D.91207LAUF,GERMANY
I\4ULTIFUNCTIONAL
CERAMICSLUITPOLDSTRASSE
unit
T€st ltem(s)
22):P-A[,IINOAZOBENZENE
(CASNo.:60-09-3)
(CASNo.:9$
23):2,4-XYLIDINE
68-1)
(CASNo.:8724):2,6-XYLIDINE
62-n
CFC's(Chlorofluorocarbons)
Group I
luorccabonl 1 (CASNo.:
Chlorof
75-694)
(CASNo.:
Chlorofluorocarbon-12
7171-8)
3
ReBult
No.1
n.d.
3
n.d,
MDL
Method
msfts With referenceto LFGB82.02-2.
by GC/lVlS.
Analysis
was performed
to LFGB82-02-2.
mg/Kg /Vithreference
Analysiswas p€rformedby GC/MS.
mdks Withref€renceto LFGB82.02-2.
by GC/MS.
Analysiswas performed
ll
llll
Limlt
3
mg/kg With referenceto US EPA 5021
method.Analysiswas performedby
GC/MS,
to USEPA5021
mg/Kg Wth reference
n.d.
method.Analysiswasperformedby
Gc/rlls.
to uS EPA5021
13 (CASNo.: MEKg with reference
Chlorofluorocalbonl
wasperformed
by
method.
Analysis
76-13-1)
GCiMS.
n.d.
luoroca|bon-1
14 (CASNo.: mgikg With referenceto US EPA 502'1
Chlorof
method.AnalysiswaspedormedbY
76-14-2)
GC/MS.
to Us EPA5021
115 (CASNo.: mg/Kg Withreference
Chlorofluorocarbon-
'|
n.d.
1
n.d.
1
n.d.
1
n.d.
1
n.d.
bY
Analysis
wasPertormed
method.
6C/MS.
7&'ts-3)
Grouplll
3 (CASNo.:
Chlorof
luorocarbon-l
7U72-9)
mg/kg With .eferenceto US EPA 5021
method.Analysiswas performedbY
GC/MS.
(CAS
m9Kg
with referenceto us EPA 5021
I1
No.:
Chlorofluorocarbon-1
method.Analysisvrasperformedby
354-56-3)
GC/|\,IS.
to IJSEPA5021
Chlorofluoroca6on-112 (CAS No.: mgKg Withreference
mehod.Analysis\o?sperfomedbY
GC/tVlS.
7B-12-0)
Chlorofluorocarbon-2l1 (CAS No.
422-784)
n,o.
mg/kg Wilh feferenceto US EPA 5021
method.Analysiswas PerformedbY
GC/t\4S.
r5!E?;':r"
YisfPlT
?':;'il*'Tl"il]lli*:::]]:il :"*'"-**-'"-"-"
"f::Fri
;:li";iy*T
B#;rftETtisi4u
?ilrl",il
ffffi**;"lu*:ffir*"ieB,:.mr""*r*:[''*'inmv""r*irf#ilfi€sitr;:t$ijii"{s#xpa#
**.s's*-"'frvi i ' i i i n n n i i i l i i w t i t i " * r r - " * o" :"'*r,*cl '-" a L ' " r , * r . " - . i i ' ' i ' ; ; t ; d n . ! . € d s d r o | d t r b
i;6;;:!,;uft
d; r;,oi'"
t . . . u , g . . * " ' ' o ' r . r ' g . ; ; 6 ; ; d n ' " d * r g d * " ' b . 6r;;;"n;;id'ialia
a * -'.j;:;;;;;
s",r ri'tdo'
"
oird*
ra b p6eo*d 6 n'
4riiFiciv,r
TrtiJLinSl[&*6EE
st!fi
TestReport
No.: CE/201214843ADale:2o1Z0AU Page:8 or24
l:]
CERAMTEC
GIVBH
't5 D-91207LAUF,GERMANY
ItIULTIFUNCTIONAL
CERAlrlcS LUITPOLDSTMSSE
Test ltem(6)
(CASNo.:
luoroca6on-212
Chlorof
3182- -1)
Unit
MDL
ll/lethod
to uS EPA5021
mdks Withreference
lrn
Result
No.l
n,d,
tllllll
Limit
Analysis
wasperfomed
by
method.
GC/MS.
3 (CASNo.: mg/Kg With referenceto US EPA 5021
Chlorofluorocarbon-21
method-Analysiswas performedby
235,L0e5)
GC/ttIS.
(CASNo.: mgKg With referenceto uS EPA 5021
Chlorofl
uorocarbon-2'l4
method.Analysiswas performedby
292sr31-0)
GC/MS.
luorocarbon-2l
5 (CASNo.: mgikg With referenceto L,SEPA 502'l
Chlorof
method.AnalysiswaspedormedbY
425943-2)
GC/MS.
to uS EPA5021
Chlorof
luorocarbon-21
6 (CASNo.: mg/Kg Withreference
method.Analysiswasp€rformedby
661-97-2)
n.d.
n.d.
1
n.d.
mgKs With referenceto uS EPA 5021
method.Analysiswas perfomed by
GC/MS.
1
n.d.
With feferenceto uS EPA 5021
method.AnalysiswEsperformedby
GC/t\4S.
mdks With refeence to US EPA 5021
method.Analysiswas performedbY
GC/MS,
1
n.d.
1
n,o,
mg'ks with referenceto us EPA5021
1
n.d.
1
n.d.
GC/l\rs.
7 (CAS No.:
Chlorofluorocarbon-21
422-86-6)
CHCa(Chlorinalehydroca.bon)
(CAS
1,1,1,2-Tetrachloro€thane
No.r630-20-6)
(CASNo.:
1,1,1-Trichloro€thane
71-556)
(CAS
1,1,2,2-Tetrachloroethane
No.:79-3+5)
(CASNo.:
1,1,2-Trichlorcethane
7900-5)
mgKg
bY
waspedormed
method.
Analysis
GC/MS.
to USEPA5021
mg/kg Withreference
method.AnalysiswasperfomedbY
GC/MS.
to USEPA5021
Withreference
bY
wasPerformed
Analysis
method.
(CASNo.:751,1-Diclloroethane
mg/Kg
(CASNo.:751,1-Dichloroethene
GC/|VS.
mg/Kg With referenceto IJS EPA 5021
s+3)
3s)
n.d.
method.Analysiswas PerformedbY
GC/|VS.
""" *- *"*'*
?.gT+:ex;1:FdT6l.f
8"*affirli;sffr':!t'i?+riFs.t'li::E?'"iri:'13i:
ib::T::a:":1:
::,T"
.morr;dti
r*bFbGq€E
'#.?n"i*inni#noi*i*t*b]66d'.tcodm!b,Ei.:i;;'d;;;6iw4.;'.''n
il"i].i,i.ii"ni.ii'i.ini"ii'i&tona"ai"d@,$6dd"*b.1";.;;;;;b';mda'1'''e"9dFai'
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Test Report
Paqe:9of24
No. : CE/201214843A Date:2012,0i,M
rrrfirnl||
CERAIVTEC
GIlIBH
15 D-91207LAUF,GERMANY
MULTIFUNCTIONAL
CERAIVICSLUITPOLDSTMSSE
Testltem(s)
Unit
(CASNo.:
1,1-Dichloropropene
563-5&6)
'1,2,3-Tridlloropropane
(CASNo.:
9618-4)
(CASNo.:
1,2-Dichloroethane
1O7-06-2)
MOL
ilethod
Result
No.l
mg/kg Withreference
to USEPA5021
n.o.
Analysis
wasperformed
by
method.
GC/MS,
MEKq Wiihreference
to uS EPA5021
method.Analysiswasperfomedby
GC/MS.
n.d.
mg/Kg With referenceto US EPA 5021
n.d.
method.Analysis\ rasperfomed by
Gc/ltlS.
(CASNo.:
1,2-Dichloropropane
msr'(g With refefenceto US EPA 5021
method.Analysiswasperformed
by
78-87-5)
GC/MS.
(CASNo.:
l,SDichtoropropane
mg/Kg With referenceto US EPA 5021
method.Analysis\oasperformedby
142-28-3)
GC/MS.
(CASNo.:
2,2-Dichloropropane
mg,Kg Wth referenceto US EPA 5021
method.Analysjswas performedby
594-20-7)
GC/MS.
Carbontetrachlonde(CAS No.:
mg/kg With referenceto US EPA 5021
56-235)
method.Analysis$/asp€rformedby
GC/ltlS.
(CASNo-:75-00-3) mgikg With .eferenceto US EPA 5021
Chloroethane
method.AnalysiswEsperformed
by
GC/|VS.
(CASNo.:67-66-3)
Chloroform
m9K9 With referenceto US EPA 5021
method.Analysiswasperformed
by
GC/MS.
(CASNo-:74-87- m9KS With referenceto US EPA 5021
Chloromethane
3)
method,Analysiswas performeclby
GCiMS.
(CASNo.: mg/Kg Withreference
cis-1,2-Dichloroethene
to USEPA5021
n.d.
n.d-
n.d.
n.d.
n.d.
n.d,
n.d.
method.Analysiswasperformedby
GC/MS.
15G59-2)
(CASNo.: mg/Kg With referenceto US EPA 5021
cis-1,3-Dichloropropene
10061-01-5)
melhod.Analysiswes performedby
GC/t\4S.
n.d.
pdued&€pl'nfujmhodpndd
i-h'.on
cohpaa
^iy !i'6od;j
Bsddh?n
o b,6r 6i toaery tr hrsheb
d h6 trhr
*ydeddroo*readlq{std
o
or apts
qrdF
.M ta wd / ii:lld,|ilt**FmliEffitri
:]l
Limit
Test Report
No.:CU2O1Z14U3A Dale 201210i,04 Page: 10 of 24
t]|lrr
CERAI/ITEC
GIlIBH
LUITPOLDSTMSSE
15 D-91207LAUF,GERIJANY
MULTIFUNCTIONALCERAI\'ICS
Tost ltem(s)
(CASNo.:
Hexachlorobutadiene
8748-3)
unit
MDL
llethod
mgKg Withrefercnce
to uS EPA5021
by
method.Analysiswasperfo{med
GCiMS.
to Lls EPA5021
lMethylene
Chloride(CASNo.:7+ mg/kg Withreference
by
method.Analysiswaspertormed
0$.2)
GC/l\rs.
(CASNo.:127- mgKg Withrefercnce
to USEPA5021
Tetrachloroethene
method.Analysiswasperfomedby
184)
GC/MS.
msikg With referenceto L,S EPA 5021
ttang1,2-Dichloro6thene
{CAS
No.:15G60-5)
(CAS
trans-l,3-Dichloropropene
No.:10061-02-6)
(CASNo.:79Trichloroethylene
014)
method.Analysiswaspedormedby
GC/MS.
mg/Kg With referenceto US EPA 5021
method.Analysiswas performedbY
Go/tlls.
mgKg With rcferenceto IJS EPA 5021
method.Analysiswas perfomed bY
GC/rVlS.
Result
No.l
n.d.
|ll|rlr
Limit
n.d.
n.d.
n,d.
n.d,
1
n.d.
1
n.d.
1
n.d.
1
n.d.
1
n.o,
HCFcs
(llydrochlorofiuorocarbom)
HCFC-21(CASNo.:75-43-4)
HcFc-22(cAs No.: 7545{)
HCFG3l (CASNo.:593-7G4)
mg/Kg With referenceto IJS EPA 5021
method-Analysiswas performedbY
Gc/lrlS.
mg/Kg With rcferenceto uS EPA 5021
melhod.Analysiswas perfomed bY
Go/tlls.
to lJs EPA5021
mgKg with rcference
melhod.AnalysiswasperfomedbY
GC/l\,IS.
(cAs No.:35,4-14-3) msn(gWithrcfef€nc€to USEPA5021
HCFo12'1
bY
method.Analysiswasperformed
GC/tus.
(CAsNo.:3*21-2)
HCFG122
mgrs
to USEPA5021
Withreference
bY
wasPedomed
Analysis
method.
GC/MS.
n.d.
*-"f
stf,i"S"13::89';'.i:'rs,":g"r",F:'r'..i:iEr8ffintr8yq;HlErTftf
ill1:-:1"::--':,::"'""***'*'*
'i,?i;d,r.a !;dbyb6hE
y*b@bbk..
c-d *.d;
i lti;it
ds'bcorim!'0,e6ft
iA;;
:i,itn,iar'Jniii.innft-m"*oi"ao"-*"a"-to-.*"'i'nd;;'F,;-..-''*d*drd";;:;;;;;;i;;
d n ; ; : ; ; ; ; i ; ; : ; ; a ; F ' i i i . , . 6 d c | f l s ' M d m . , a " y € c d n s n Y ' ! d . l . : p o 1 6 b ' i t } -ir err'
@;.;3
. -"....
tr. 8a...0
i;sd m 'n o.€r,i
o n d t . @ +"-*n
{dr4
_a'6
a @ n l D m a . , T a l d b E t o ' i b w d ' 5"o,s*"
n ir
6-d b trpq"-ed
"h113fr.{;*'""".HT:iS X
"€er
I lLmfrtE*FffinfiRtfi
TestReport
No.: C9201214843A OaIe:201210204 Page:11of 24
llfir
CERAIVTEC
GIlIBH
15 D-91207LAUF,GERMANY
MULTIFUNCTIONAL
CERAIIIICSLUITPOLDSTMSSE
Te3t lt€m(s)
(CASNo.:30G83-2)
HCFG123
Unit
MDL
ilethod
Result
No.{
n.d.
to uS EPA5021
mgKg Withreference
method.Analysiswasperformedby
GC/tMS.
(CAS
to USEPA5021
HCFC-124
No.i2837-89-0) mg/kg Withreference
by
method.
Analysis
wasperformed
GC/MS.
n.d.
mgKg With referenceto US EPA 5021
method.Analysiswas perfomed by
GC/l\,1S.
(CASNo.:1649-0&n mg/kg With refe.enc€to US EPA 5021
HCFC-132b
by
method.Analysiswasperformed
GC/MS,
to USEPA5021
(CASNo.:75-88-7)
mg/Kg Withreference
HCFC-133a
n.d.
(CASNo.:1717-006) mg/Kg with referenceto US EPA 5021
HCFC-141b
method.Analysis\Nasperfomod bY
GC/MS.
mdts With referenceto US EPA 5021
HCFG142b(CASNo.:7568-3)
by
method.AnalysiswEsperfoamed
GC/MS.
HcFc-221(cASNo.:422-26-4) mg/kg With referenceto US EPA 502'l
bY
m€thod.Analysiswas performed
GC/t S.
(CASNo.r42249-1)
mg/Kg With referenceto US EPA 5021
HCFC-222
melhod-Analysiswas performedbY
n.d.
HCFG131(CASNo.r35$28-4)
n.d.
method.Analysiswasp6rformedby
GC/tS.
1
n.d.
'I
n,d,
I
n.d.
1
n.d.
1
n.d.
Gc/rlls.
(CASNo.r422-526)
HCFC-223
mgKg
With referenceto IJS EPA 5021
melhod.Analysis\ /as performedby
GC/|\,IS.
(CASNo.:422-54-8) mgKg Withfeference
to USEPA5021
HCFG224
bY
method.Analysiswasperformed
GC/tVlS.
to USEPA5021
(CASNo.:422-56-0) msftg Withreference
HCFG22sca
bY
wasperformed
Analysis
method.
GC/MS.
n.d.
iilit f&iFi#riE:ii:E8fdJrjie'€BlYs"'r,Fi:*r51':*dI'sEi':'or:nrF6::i-::1::l
l"*^'*-*-"*
asq.dregL6n.?!omsd..66e1ado!..adaI'!b€olELg'
;;;;;H.;.;t-d"*..ft!'.idhr"-.-dc*d'6-b#;i;6;,n'i's*4!or,sf.m
; i ; ; d ; n ; i * d - - | v * " * h 1 " " r . " e c . l .".n* .r -' a. i-i -] r- y* ei d. .; "c*o"a, i;''i;"!.do.6€dsdf gs od |E, vt dl b, i a d s o ' ft'"*r'nrrc'b'Fru
'"
*;"iihr;tui
r" or s,r *' *s
ldr
':;"@i':ri;in
- * ". -;:E;;;;
md ftnds
fuY b Pm
a rred. vr.dii
/ ttitirfiJ|x*mBndst6t
l
lllll
Limit
TeSt
RepOft
No.:cs201214843ADare:2o1zozo4Pasetl2ot24
tl
CERAIIITEC
GITIBH
MULTIFUNCTIONAL
CERAIVIICS
LUITPOLDSTMSSE
15 D-91207LAUF.GERITIANY
Test ltem(s)
Unit
MDL
Method
(CASNo.:507"55-1) mgKg Withreference
HCFC-22scb
to USEPA5021
method.Analysis\oasperfomedby
GC/t\4S.
-87-8)
(CAS
HCFC-226
No.:431
mg/kg Withreference
to USEPA5021
wasperformed
by
method.
Analysis
Go/tlls.
HCFG231(CASNo.:421-94-3)
m(/kg Withrefercnce
to uS EPA5021
method.Analysiswasperformed
by
GCiMS.
(CASNo.:460-89-9)
HCFC-232
mg/Kg Withreference
to USEPA5021
melhod.Analysiswasperformedby
GC/t\4S.
HCFG233(CASNo.:7125-84-0) m9ks Withrefercnceto US EPA5021
(CASNo.;666-27-3)
HCFC-241
by
method.Analysiswasperformed
GC/MS.
mg/Kg With referenceto US EPA 5021
method-Analysiswas performedby
GC/t S.
mgKg With rcferenceto US EPA 5021
method.Analysiswas performedby
GCA4S.
to USEPA502t
mg/kg Withreference
(CASNo.:460-63-9)
HCFC-242
mgKg
HCFC-234
{CASNo.:425-94-5)
HCFG235(CASNo.:46G92-4)
HCFS243(CASNo.:46G69-5)
Resull
t{o.'l
r mrrll|l
Limlt
n.d.
n.d.
n,d.
1
n.d-
1
n.d.
1
n.d.
1
n,d.
1
n,d,
1
n.d.
wasperformed
by
method,
Analysis
GC/MS.
With rsfefenceto US EPA 5021
method.Analysiswas perfomed bY
GC/MS.
mgfts With rcfefenceto US EPA 5021
method.Analysiswas performedbY
1
GC/tVrS.
HCFG244
(CASNo.:42141-0)
HCFC-251
msas Withreferenceto uS EPA5021
n.d.
by
Analysis
wasperformed
method.
GC/MS.
to USEPA5021
mg/kg Withreference
bY
method.Analysiswasper{ormed
GC/MS.
n.d.
":1::: - ll-:"'*-***""*
H#n#Hyqgg1:iffdf
+rsfi;T,.ffi8flq;i:"r."fi-tq"r'
jrj"er***:n*,f*njtru"rln*:."sltr,s:sr.".1x-rffrf*rrlgirsi"",Lrx$;"'trili:'#*tr"'r#ii**'".o*;
EUs o.rne t6c' 'ii; hod.'d rF .oor.a teied rar 'r'io
i"iu'.,i,i mnrii
oo iiddr
t i , i i i . ' . . g ' n r o - ."i'i#i-m^
* - ' - o . r i n ' h . ' n | E d c | 5 1 s , d d o T : ; i ' ; i . i ' " " J i " d . g p o * b ' . ' o -' ti s' oco| €d nn hi ' d6 '110- ', B
. d ' m o a m 4 m . 6 @ p rn a l
aad'ed
€maffqoo.e_'
r;;;;n';;ou_od
rs ns.
bilru;ad
36rdu 4d on ideB rut b p@ork
bs'ry d dr ier m d b.6nbdi;;F-;;at
cam;ry Ary-.dtu;.dEErm.
b he tuhd 'ns( d b' a*
ryrr+! crr ri wd / firlfisrlE+FmnERt*
TeSt
RepOft
Date.2o1zozo4
Pase:13or24
No.rcE/201214843A
|l] ||ttl[Ilrt]r
CEMMTEC GMBH
IVIULTIFUNCTIONAL
CERAMICSLUITPOLDSTMSSE
15 D-91207LAUF.GERMANY
Teetltem(s)
(CASNo.:819-0t!1)
HCFC-252
HCFC-253
{CASNo.:460-35-5)
Unit
Resull
MDL
Mothod
mgikg with refefenceto US EPA 5021
method.Analysiswaspedormedby
GC/MS.
mgKg Withreference
to USEPA5021
No.l
1
n.d.
1
n.d.
method.Analysiswasperfomedby
GC/MS.
(CASNo.:420-97-3)
HCFC-261
mg/kg Withreference
to USEPA5021
method.
Analysis
waspedormed
by
GC/|VS.
(CASNo.:421-02-03) m9Kg Withreference
HCFG262
to USEPA5021
method.Analysiswasperfotmedby
GCiMS.
(CASNo.:430-55-7)
HCFC-271
Limit
n.o.
n,d,
n.d.
mg/Kg With referenceto US EPA 5021
method.Analysiswas perfomed by
GC/MS.
= 1000ppm
1. mg/kg= ppm : 0.1wro,6
2. n.d.= NotDetected
3. MDL= llethod DetectionLimit
4."-"=NotRegulated
5- * = Qualitative
analysis(No Unit)
6. Negative= lJndeteclable/ Positive= Detectable
7. Asbestos: Negative= "< 1.0%", Positive= "> 1.0%"
PFOS Reterence Information : POPS- (EU) 757/20'10
productsor
above0.001%(10ppm),in s€mi-finished
or preparations
in conc€ntrations
OutlawingPFOSas substances
in textilesor othercoatedmatedalsabove1ug/m2
adiclesor partsat a levelabove0.1%(1000ppm),
'ntrBb3l€Fntt'01ylo.h.qd
cdmdi!kJr
El *qs { HlElllltflr'llH2Efi 61 " 4H& l Iti :)"lBd ldil l s _]ta'
_i;;n.1
mrud oi.^tr *dbds r @
Ed.d o d; cmFni aoF b tu crs6 coo'm; dlrc
A;;;i#';€!s;;;'atii"d
brd dntr+b &d@ b-!-' {d c"-ft-, h' ii;;;;
am.ro.ortu
i;;ft;d;
rbtilt'. hdanMata'iii"d i'iir;liai(n ''is ddlrei iDrein it; i'di* t h€ demi, 'isd{si ba iro
ftled'B'fumdmfxflo*o:1l€|fi.3dL.dlBl1ffgi!nyD.!mpa1yss€ceo'3'b|i,Gb
ft6 d*rsd e..d ba F
re
h6 Endon @ritu
migoo. rt""*go"|*'
ohb ro d{.r@
or $h edm$r ts m r[{ur sd
. i.dbi; hosry d h]!'idi
orih€ obi;i;iF,Ae
.mpanr tur d.dodd
crdido-lr'T€
o-6trs
abnb'306*roh'
ompaivi ird ie3d
4 hlts .lq,rawd / FirLrrirrd*Erdrifrffirs
Test Report
paoe: 14 of 24
No.: CE/201214843A Date:201i,02t}4
CERAMTEC
GMBH
MULTIFUNCTIONAL
CERAIJICSLUITPOLDSTMSSE
15 D-91207LAUF,GERIJANY
t]
tl| [ttttlrl
1 ) Thes€sampiesweredissolved
totallyby pre-conditioning
meihodaccording
to betowttowchart.
( Cf'lest methodexcluded)
yang
2) Nameoflhe personwho mademeasuremenl:
Climbgreat
3) Nameoflhe personin chargeof measurement
TroyChang
Samplelvleasurement
Aciddigestionby suitableacid
clepended
on differenlsample
mateial(as belowtable)
Microwave
digeslionwith
HNO/HCI/HF
Heatlo appropriate
temperalurelo exiract
Cool,tilterdigesiate
AlkaliFusion
HCllo dissolve
ICP-AES
SampleIVaterial
throughfilter
Add diphen9-carbazide
for
DigestionAcid
Steel,copper,aluminum,solder
Aquaregia,HNOr,HCl,HF,H,O,
Glass
HNO3/HF
measurethe absorbance
Gold,platinum,palladium,
ceramic
Aquarcgra
at 540nm by UV-VIS
Silver
HN03
Plastic
HrSO4,HrOr,HNO3,HCI
Others
Any acidlo totaldigestion
[email protected]
co.Dar t? / B l ;?!i .rlRA1l Rl6?ldlSt,&AlF? 4E- 1144- "i*EjAl
T lS.nlb!
I d brsd ro 'b c3?d cfdrol - d s.
usd b rmE 'i cond' m3 tu .tu
inturondrdrt idmnfieron,ndluddturrslsd.fn.dh.Dn.Adh
feyTh.comFrybe|'rs4odbity
cmFny tuy uiadoda
du6d.6€0tintur wr$dpdoffrlGnpomsdndb.
abdoii '@dryd h]3fidoi orrh€6L*r oraoFadtu. orlh s dodn.d c ui.['ur.nd on€nds n.i b6pGeMed b ib tu *id;ddb6rtu
*"un,,,i"&1,1ffii*,I
il{,tliiilgtiffI1?lil'"
T-
TestReport
No.: C9201214843A D3l.e:201210?,04Paoe:15 ol24
CERAIIITEC
GITIBH
MULTIFUNCTIOML
CEMI\4lCS LUITPOLDSTMSSE
15 II91207 LAUF.cERltlANY
t][Ilmfirllltl
Analyticalflow chan of Soxhletextracgon(LCIMS)procadure
a
r
Nameoflhe perconwhomademeasurementRomanWong
TroyChang
Nameof lhe perconin chafgeof measurement:
I Test lten3: PFOS/PFOA' Benzotriazole)
pretrcatmenuseparation
Sample
I
Data
comDafr
[r ]l-dFdE nH-LxlAlrrl:L:EtAa
and rq*ftntrmardidm*6
'c,':trr'6n.r.or19
" td;.
{{r"Eifi"4l
i
A..bA
$68
6r6m3ed codhoGbrErtunc
ooomsds.t trw $'@n/ddnE
@!rn a.yrredd!dcmrdad!Hhi
l;-{rrdn <isdd
dir€'
[email protected],
.nd drsdon!
d edon! une
Lnd u.
b. hns.dori
[email protected]
eft.ro
ri
rh s3 ddmed
odn.r
-
ennor
endb b Ep.de
€p.d!E.
r tu
L ulM
wrd
md tu
#,Posg,Ppdgr d ha
ha
sopt
sEp(
sopr n
Jr.
r.
w1M pnor
TeSt
No.:cEt2o12t14843A
24
Date.2o12to2to4
Pase:16of
RepOft
CERAMTEC
GMBH
I\4ULTIFUNCTIONAL
CERAI/IICSLUITPOLDSTMSSE
15 D-91207LAUF.GERMANY
Chlorinated Flamc retardant analytical flow chart
1) Nameoftheperson
whomademeasurcment:
BaryTseng
2) Nameoftheperson
in chaeeof measurenent:
TroyChang
I
r
Refercnce
method:
USEPA8270D,
USEPA3540
Teslltems:PCBS,
PCNS,
PCTS,
ltlkex,Ce MCCP
Data
C o m o a n h lq F e s r ' n E ; g F l { ? , s : i z t s , r E ! .
nbrond16rq'T*rnelonsrd
i
rn-I&
!
pr€13)
'6bd rhk bn @on 6n6r barc
" ilr"q :r' I "rn E{.
rfy
rh comFny6 de 4o$
'bi,v
rdbEpdl€d3cpli1fu|
ll|l|t
[|rrlr|r
Test
No.: cE/201214843A
Date:2o1zo2!o4PasetlTof24
Report
|l][t
CERAMTEC
GMBH
ItIULTIFUNCTIONAL
CERAMICSLUITPOLDSTMSSE
l5 D'91207LAUF,GERMANY
Analysis flow chart for delerminalion of PVC in matorial
r
I
GinnyChen
Nameoflhe personwho mademeasuremenl:
Nameofthe personin charceof m€asurcmentr
TroyChang
Sampleanalyzedby FTIR
Chec* wave-numberof C-Clbonding
i n s s b { D F n ' $ e l o n ] y l o l h € & o p l @ d u d r e p t i f u | , d o d p i d " r i
'nEryrilTEl,&sj
,{HAl"i*l49l1li"E.:&flAE lEd- kl,l1, \.13 til
lq! llCS
rnhd€um$tlaig.dby1h6c0np.ry!ub]6dbbGsmBcodlon6ds
blddbr.-..nd cf d !0.Eb Er*n
-.*".;;i: il:|
:.*:ij;*.)T.i."'"#',H.*-*;*ii"- '
" """-'*','
t!l||r
Test Report
No. : CE/2012l148434 Dai€.2O1ZOZO4 Paoe: 18 of 24
CERAIVTEC
GITIBH
MULTIFUNCTIONAL
CERAMICSLUITPOLDSTMSSE
15 D-91207LAUF,GERIVANY
trfllrI.
tllllll
Analyticalflowcha of Soxhlet€xlraction(GC/MS)procedure
I
r
Nameof lhe personwhomademeasurement
RomanWong
Nameoflhe personin chargeofmeasuremenlTroyChang
(TeEtltems:Phthalate' B€nzotriazole. HBCDD. NP . DBBT.
Oryanicphosphorus
compoundrs)
* ihdr Fiorwins p€m3sond h3
nrh.radGoodcrdontb{i.*nr€{e)l.sd.h6bn@od6nmLsrcpodu€d.€^6prrntur
'"lJl-atv
td&l:ldf-qEFdb
corraaBr. e e@ !BS4Fr*tdj^+-as
ThEood-md tr $&bh6comM
ns4{4oT
on/rsd*0oor.i
andror..dM( rffi dem.nr &t.di,-nr
am codtms w
imibron d rdrt idmnneton l;d ':id doi i$u.s dsfind b.6 i Air io d.r ol rhi3doonenl adu$d hlr 'ft
u.lim.fi1!nEii€ntmd'ands.liin1i.imibo'c||€n|li9rudo6iai,rhconFnybd3r..ponEb''
-@didouMts
-b doLnfr 6
cmFny Ary uruubodair abdon foasry or fsltr€ron or h' @i6d or ap
TestReport
No. : CE/201214843A Date:201i,02104 Page: 19of 24
CERAI/ITEC
GI/tBH
MULTIFUNCTIONAL
CERAIVICSLUITPOLDSTMSSE
15 D-91207LAUF,GERMANY
lll|t|::
l]t
Analyticalflow chart of Organic-Tincontent
I
I
Nameofthe personwhomademeasurement
GinnyChen
Nameoflhe perconin chaee of measurement:
T.oyChang
Concenbate/Dilute
Exkacted
solution
Analysiswas perfomedby GC/FPD
Dala
CmEi!hl
EJ8!
i E ,ERHtlr€ll2ll
l A r " IE"{t{|
i J.,b8l
"4h:n:
,ond oftdSe1uDnftdoER
drrdr.rerdco.ono$6rEr.m
oducdeeplifuldbodp'old
*
iandid on E6
dnd
tudn An' h
rh rh6 dbideiadoi
onrvsnd * ihii h6 rh r d c iad3 insdons
iiry
hneo m rdm .rcEsm dl hq notu so dro.ron! und h. b.n*dod @
compary Ary unadhoruA rE,!r n bqary q bls i€ln
d hs trhr
or ap
n"**.,ffiiu';tl.':ji,;H.Jiil*iilI1n
$ff,991"**tr,i:1.""-,nu*'u***oon*.*
I
Test Report
No.: CE/201214e43ADale: 201210?,04Paoe:20 ot 24
CERAMTEC
GMBH
II,IULTIFUNCTIONAL
CERAMICSLUITPOLDSTMSSE
15 D.91207LAUF,GERMANY
Analyticalflow chart of halogencontent
1) Nameofthe personwho mademeasuremenl:
RitaChen
2) Nameofthe personin chafgeof measurement:
TroyChang
Sampleprelreatment
/ Sepataiion
Weighting
andputtingsamplein cell
OxygenBombCombustion
/ Absorpiion
Dilutbn10fixedvolume
Analysis
wasperformed
by lC
conFl[i]l teS3! -[HiL+liti]13
lliiAA. ldA f Ad .-FditE
rcddm. E s".d d u. cmEn
3d ro dftnrbrddLnfb
&drF16 smEfd cortonsto'Ebtu
i'ln*idm s6
ddd
badn. Anr fd
tErm.d6'miwmononkaowft
ihrmcrC
ads n$trotr3 iin
hiso
m irem &sE,ft
dl h.r iotu eo dr oar on! Lne h. hlnsdort
ecmda
comp'a Any!m6o,ze
dEErm'toEerydbsidbdhstrblorap
i " Eo\tqr'
ms odr6a
6nd
ba Eru
*-,nu"nuo*"*"oo"o
*"*'*ffilil]iio\'3;Il;k,ifig;|ff l"t*$$#gll"*.,lll:]"!k
TestReport
No.: CE|2O1Z14843A.Date: 2O1ZOZO4 Paae: 21 of 24
CEMMTEC GIMBH
MULTIFUNCTIONAL
CERAIJICSLUITPOLDSTMSSE
15 D-91207LAUF,GERIVANY
Analysis flow chart for determinationof Aabestos
1) Nameof the Dersonwho mademea6urcmenl:
VictorKao
2) Nameofthe personin chargeof measuremeni:
WendyWei
l6 )
I Refercncemothod:EPA600/R-93/l
Conlinuewh€nproblem€
a€ encounle€dwithPLlvl
and/orfor qualily assurancepurpo€€s
Inleriercncemahi\ removal
Asbeslos identificationby dispersion
stainingpobnzationlightmicroscopy
A€bestosidentiticationby X-€y
Notconraining
Asbesros/
cnFnyRJ BA&.8 {E: *lRl6flnld -AB Frt IEd-*l{4 \:ltffril
nidhi
d ri'driry. id.mn ieln
rE$don tm d.eno.i
cdmFry Ary u@rb4n
r.JfllSp
@dudrepliful.dodpidfr
'id j
h., nod
sbdon
blw
or raibf€ton
F hnEdon oodn.nri
d b. @ftdtr
@
Tdeoo@r
** f,iFi$l' I ;i*,?1.;r,];'i[il::t;.,]-**u;]'*.,
r ar'eb.,.lr
'**...*.
Test Report
No.: CEi2012l14843A Date: 2O1Z0ZM
Paoe: 22 ol 24
CERAITITEC
GMBH
IJULTIFUNCTIONAL
CERAMICSLUITPOLDSTMSSE
15 I}91207LAUF,GERITIANY
Analyticalflowchart
I
I
Nameof lhe personwho mademeasurcmentRomanWong
Nameof lhe personin chargeofmeasurement
TroyChang
TBBP-A-bb)
I Tesl llem3:PBB/PBDE,
pfoceEs---.
Firsllestingproc€ss-----+ Optionalscrcen
proces€-.>
Confirmation
Screenanalysis
'Li-;iirn-rrn;i;;;i.ii
.i;ii.
Sampleextraclion
method
Concentrale/DiluteExtractedsolulion
Filter
Analysisby GC/lt/S
lssueRepod
c o F o . r a JF H & ! i - { & d E
- l l q U d l nI E E A { . i € b f l 4 d r " - s a , q .
-d6rnh6dolend
irturondrdi
t
sa.ftdn<ifuMonf|ya'od
bjd b rffir
ad codi
r" iid!.
m3 tu E 6dm
b a ' d d i s . f 3 ' r d e . ' 0 . ? 9 d o n p d L e d 4 e p l i l f u |
.r
t]ttllll||Iltt]l
Test Report
No.: CE|2O1Z14A$A Dale:2012102104Paoe:23 of 24
CERAMTEC
GI\,iBH
MULTIFUNCTIONAL
CERAI\/IICS
LUITPOLDSTMSSE
15 D,91207LAUF.GERMANY
Analyticalflow cha(otvolatils oryaniccompounds(VOCS)
I
I
Nameof lhe personwhomademeasuremenl
: ChunWu
Nameof the personin chargeofmeasurement
: ShinjyhChen
I Referencemelhod : US EPA 5021)
Samplepretrealmenl
Takesampleandputil into
glassware.
headspace
o r p a n y u Jt l r ; t 8 r ' { F 1 t : R @ 9 l d l t 4
&-AE
lEl,-{lil
":-"q
. rE&"
nlfltm
lm0trmt
Test Report
No.: CEI2O1Z14U3A, Date 201210?,A4 Page 24 ot 24
CEMMTEC G[/lBH
MULTIFUNCTIONAL
CERAIVICSLUITPOLDSTMSSE
15 D-91207LAUF,GERMANY
r:|| tt]||ln|rr|l
* The tested sample / paft i6 marl(ed by an anow if if,s shown on the photo. .
L4843
** End of Report "
cmF.th/
- t s f u 9 1 3 i gtq$qS
. d b y s o .llmel
ffF
.?l49jii];i -df{R&.,lE:
llt li"
*TA;
I
"! n dlJ.
|edhbdoUm'di3'sdtsdhatdo
h t m d B d s ' e d i o i o n | , a n d d l h f t s c m F r y s s o € E s o i d b l i l y i s b
-_*-***-_*^_1
|
rdF cie ri wd / fittir5:]ijf*Ld6n}f*r*
TestReport
Date:14Oct2011
No. SHAEC1116009838
Page1of 5
ZHEJIANG
ASIAGENERAL
SOLDERING
& BRAZING
MATERIAL
CO.,LTD
XIHUINDUSTRIAL
PARK,SANDUN,HANGZHOU
CITY.ZHEJIANG
PROVINCE.CHINA
The followingsample(s)was/u/eresubmittedand identifedon b€hatfof the clientsas : LEAD-FREESOLDER
WRE
-SH
sP11-030781
SGSJobNo.:
l,IodelNo. I
Composition
:
Dateof SampleReceived:
YTW102(692535-00
t,692535-002,692535-003)
Sn2.0CuRE
09Oct2011
TestingPeriod:
TestRequested:
09Oct2011-13Oct2011
Seleciedtest(s)as requestedby client.
TestMethod:
Pleasereferto nextpage(s).
Pleaseleferlo nextpage(s).
TestResults:
Basedon the performedtestson submittedsamples,the resultsof Lead,
(PBB),
Mercury,
Cadmium,
Hexavalent
Polybrominated
chromium,
biphenyls
(PBDE)
Polybrominated
diphenylethers
comply
wilhthelimitsas setby RoHS
Diredive2011/65/EU
Annexll; recasting
200295/EC.
Condusion
:
Signedfor and on behalfof
SGgCSTC Lrd.
,zQr''
FanJingjie,JJ
Approved Signatory
j hdA/hw er.oiw!!-!44!d!trN
. m q!$' 4 tarrbr.
co'v,uo. ds.dd
rnd .,.,h.r, .nr|
r {.I'-r. i. *oflq
b Edisr
'tu; DA;;F.
DoMFF . !Etl@q!!1!l9s!!!g!@
i*!tEa@r:419!s4!sja!.Eii
I'drie' nhrm'd
adebdd.ih*hd.arhl*r!rd.d.a'.dLdtdrdiffidRhf,i$rrss.c4m"/.
d o9n
,b. rh.c!.lar
rb|bc||fndnui.d..dil6
$.hado'.*.
i'.nvd.d,
rd. '.r.ddDri
cdEd
ar-r
b tu ondr
b tu. ts c.icrba
d;fi;L-;ii;;'tu;a-e-a;fr;;;;
,d;iirrii€
;";;;d;;d;'d
t$aidqiagDi.f
.ntu'nm'it
ad
b FFd,{d.€!r
h tun*'hod F!
sFtbtu6db@h'd
Lun
.hMri*hrntsnhtudrbib.6!i.(r)in!.
fArhthn9l|red&|,a.{9r9roh
lnt.!:.ltral&1830+$
@
lrl2@3
l*.d.aicm
r$EF-?r)04€ryt9
lEt(H1)8'lqA
HLO-el)611@t Hlj(10-21p15@ .sd'lerFq
r .nbdol tr'. SGSGmrP(gGSSA)
T€stReport
No. SHAECl116009838
Date:14 Ocl2011
Page2 of 5
TestResults:
TestPartDescriotion:
Sp€dhen tlo.
1
SGS&mdo lD
Dscridion
SHA11-160098.033Sitverymetatwire
Remarks:
(1) 1 mg/kg= 1 PPm= 0 0001%
(2)MDL= MethodDeteciion
Limit
(3) ND= NotDetected( < tvDL)
(4)"-' = NotRegulated
RoHSDir€div€2011lbs/Eu
TestMethod: Withreference
to IEC62321:2008
(1)Determination
ofCadmium
by ICP-OES.
(2)Determination
of Leadby ICP-OES.
(3)Determination
of Mercury
by ICP-OES.
(4)Determination
of Hexavalent
Chromium
by Spottest/ Colodmetdc
MethodusingIJV-Vis.
(5)Determination
ofPBBS/PBDES
by GC-MS.
T€stltem(s)
(Cd)
Cadmium
Lead (Pb)
Merorry(Hg)
HexavalentChromium(Cr(Vl))
Sumof PBBS
Monobbmobiph€nyl
Dibromobiphenyl
Tribromobiphenyl
T€trabromobiphenyl
Pentabromobiphenyl
Hexabromobiphenyl
Heptabrornobiphenyl
Octabromobiphenyl
Nonabromobiphenyl
Decabromobiphenyl
Sumof PBDES
ether
lllonobromodiphenyl
ti!!t
Ud!
100
1,000
1,000
mg/kg
mg/kg
mg/kg
1,000
-
mg/kg
mgKs
mgKs
mg/Kg
ms/Ks
mdks
1,000
-
ms/KS
ms/Kg
mg/Kg
mgKs
mg/Kg
mg/kg
mg/Kg
MDt
033
2
2
2
O
-
N
D
167
N
D
Negative
N
D
5
5
5
5
5
5
5
5
5
5
.
N
N
N
N
N
N
N
N
N
N
N
D
D
D
D
D
D
D
D
D
D
D
5
N
D
!.'vr6
ry&uEr b r. or-rcdt'|m.l
dh Dcsr{rb.r tGrrr!Ar!!&t!!ll&s0,al@
rdw
detudt..dddMliFd6affih.noi.i'rtbs.c!rt,.
-*rirEt
id&n.h*did.i^dri.ah
dE. n.cMrt
or.o.4lbrlUr6k
c lx{rnuirlh4Mr.6'd-.fi|
b.a-iEiifi*rhntur
rdchdr hdd.!,
rh!dgr'ibb&-t'|h.
dun
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fr.mbor
olU. AOSGoup(8GsS)
TestReport
Test ltem{s)
Dibromodiphenyl
ether
Tdbromodiph€nyl
eiher
Tetrabromodiphenyl
eiher
Pentabromodiphenyl
elher
Hexabromodiphenyl
ether
Heplabromodiphenyl
ether
Octabromodiphenyl
ether
Nonabromodiphenyl
eiher
Decabromodiphenyl
elhe.
No.SHAEC1116009834
Limit
ldr
m9Kg
mdks
mgkg
msn<9
mg/Kg
mg/Ks
mg/Kg
mgK9
mgKs
Date:14Oct2011
MDt
033
5
5
5
5
5
5
5
5
5
NO
ND
ND
ND
ND
ND
ND
ND
ND
Page3 of 5
Notes:
(1)Themaximum
permis,sibte
timjtis quotedfromdireciive
2011/65/EU,
Annexll
(2) o spottest:
Negative= Absenceof C t coating,positive= presenceof CrVlcoating;
Thetestedsampleshoutdb€furthorverifiedby boiting-wateFextraction
methodif the spottest resultis
Negative
or cannotbeconfrmed.
o Boiling-water-extraction:
Negative= Absenceof CrVlcoating;Positive= presenceof CrVtcoating
Thedetectedconcentration
in boiting-waterextraction
solutionis equator greaterthanO.O2mg/kgwithS0
cm2samplesurfacearea.
Forcorrosionprctectioncoatingson metals:Infomationon storageconditionsandproducliondateof the
testedsampleis unavailable
andthusresults
of Cr(Vl)represent
statusof thesampleat thetimeof
testino
fitED&nrhrrhrD.l4LC'ao
Sl.-tt.*fiAldt|€€efl+l
de33
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TestReport
No.SHAEC1116009838 Date:14 Oct2011
Page 4 of 5
ATTACHMENTS
RoHSTestingFlowChart
1) Nameof thepersonwhomadetesling:JanShi/yoyoWang/AenXiao/Gary
Xu
z) Nameorme personin chargeoftesling:Jefizhang/George
xu/ ElimLin
J) | nesesamples
w€redissolved
totaltvbv oreconditioning
methodaccording
lo belowflowchart.
(Cl6+andPBBS/PBDES
testmethod'ex;tuoeo,
SamplePreparation
Samplel\Ieasurcment
Pb/Cd/Hg
PBB9/PBDES
Acid digestionwith
macrowave/hotplate
Nonmetallic
material
Heating
to 90-95C
for extraction
1)AlkaliFusion/
DryAshing
2)Acidto di66olve
Adding1,5diphenylcarbazide
for color
development
brr4f,iki.drrdiehxa&hd
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fr l'trrd
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i{F.bE-yt
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.rbrd
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forcolor
development
A red color
indicatesthe
presence
of Cr6'.
necess€ry,
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TestReport
No.SHAEC1116009838
Date:14Oct20t l
Page 5 of 5
Sample photo:
SGSauthenticate
the photoon originalr€portonly
'- Endof Report"*
br. o.'|'rc.d!{rd
l.d{
[email protected],
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TestReport
No.SHAEC1119525001 Date:07 Dec2011
Page1of 5
3MCHINALII\4ITED
222#T|ANLtNROAD,SHANGHAT
(200233)
Thefollowing
sample(s)
was/were
submjtted
andidentified
on behatfof thectientsas j 3M3779-pc
SGS Job No. :
- SH
sP11-036760
Date of Sample Received :
TestingPedod:
03 Dec2011
03 Dec20'11- 07 Dec2011
Test Requested :
Selectedtest(s)as requestedby ctient.
Test llethod :
Pleasereferto nextpage(s).
Test Rosults :
Pleasereferto nextpage(s).
Signedforandon behalfof
scs-csTcLtd.
,.,1s
,rt*{
*
Fan Jingjie,JJ
ApprovedSignatory
B dud d hr
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H! n1)314&591 Hlr@6-21)646063 . €.!'i'€re.q
Monboroth. SGSgrup (SGgS )
TestReport
No.SH4EC1119525001
Date:07 Dec 201'1
Page 2 of 5
Test Results:
TestPanDescriotion
:
Spodm€nNo.
1
SGSSamplelD
D66cription
1-195250.001
SHA1
Ye ow sotid
Remarks
:
(1)1 mg/kg=I PPm=0.0001o/o
(2)MDL= l,tethodDetection
Limit
(3)ND = NotDetected
( < IIDL )
(4)"-"= NotRegulated
RoHSDir€dive201iA5/EU
Testl\rethod: with referenc€
to tEC62321i2008
(1)Delemination
ofCadmium
by tCP-OES.
(2)Determination
of Leadby tCp-OES.
(3)Determination
of Mercury
by lCp-OES.
(4)Determination
of Hexavatent
Chromium
by Cotodmetric
MethodusingIJV-Vis.
(5)Determination
of PBBS/ PBDES
contentby GC-MS.
Test ltem(s)
Cadmium(Cd)
Lead(Pb)
Mercury(Hg)
Hexavalent
Chrcmium(Cr(Vl))
Sumof PBBS
Monobromobiphenyl
Dibromobiphenyl
Tdbromobiphenyl
Tetrabromobiphenyl
Pentabromobiphenyl
Hexabromobiphenyl
Heptabromobiphenyl
Oclabromobiphenyl
Nonabrohobjphenyl
Decabromobiph6nyl
Sumof PBDES
Monobromodiphenyl
ether
$uB4t6-.Bdk,Hie
'aad*
ud!
udr
Ma!
100
1,000
1,000
1,000
1,000
-
mS/kS
mg/kg
mg/kg
mg/kg
mg/kg
mg/Kg
ng/Kg
mg/kg
mg/Kg
mgfl(g
mg/kg
mg/Kg
mgKg
mgKg
mg/Kg
mg/kg
mg/kg
2
2
2
2
-
N
N
N
N
N
D
D
D
D
D
5
5
5
5
5
5
5
5
5
5
,
N
N
N
N
N
N
N
N
N
N
N
D
D
D
D
D
D
D
D
D
D
D
5
N
D
1,000
-
b hr
rmr
hd
com'rk
'.
h. c@
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l*o3e3.h
.t5.diE€F9{q
Membfi ol h6 SGS G.o{p (SqS S,A)
TestReport
No.SHAEC1119525001
Test ltemls)
Dibromodiphenyl
ether
Tribrcmodiphenyl
ether
Tetrabromodiphenylether
Pentabromodiphenyl
elh€r
Hexabromodiphenyl
ether
Heptabromodiphenyl
ether
Oclabromodiphenyl
elher
Nonabromodiphenyl
ether
Decabromodiphenyl
elher
tuni.!
Ulit
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mdkS
mg/kg
mdkS
Date:07 Dec 2011
Mgt
Page3 ofs
@l
5
5
5
5
5
5
5
5
5
ND
ND
ND
ND
ND
ND
ND
ND
ND
Notes:
(1)Themaximum
permissible
limitis quotedfromdirective
2011/65/EU,
Annexll
lhrid@'i.n
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Membsrol tlraSGSGrolp (6GSSA)
TestReport
No.SHAEC1119525001 Date:07 Dec2011
Page4 of 5
ATTACIII,|ENTS
Rol-lsTestingFlo\ r Chart
1) Nameof the p€rsonwho madetesting:Jan S hi/yolo Wangr'Aen Xiaocary Xu
2) Nameofthe p€r6onin charg€ofteging: JeffZhang/George
Xu/ Etim Lin
3) Thesesamples wered issolvedt otatty by pre-cond
itioning methodacDordi
ng to betow ffow chan.
(Cr6+and PABs/PBDEst6st
methodexdudeO
SamplePreparalion
SampleMeasuremenl
Pb/Cd/Hg
PBBs/PBDES
Acid digestionwith
micrDwa\€/hohlate
Metallic
matedal
Concentratio
n/
Dilutaon
ofodradion
solution
Heatingto 90-95C
for extraclion
1)AlkaliFudon
/
OryAshing
2) Acjdtodissol\E
Filtrationand pH
adiustnent
Adding1,S
diphenY€arbazide
Adding'l,$
diphentcarbazide
de\elopment
indicatesthe
iro -drll!!tub
bd
&!m.tr6
Ebld
b thr
md cdhffi
6
[email protected]
ry b rb ..FPr.(.)
Er. r.@idb
rr BiorqcldhdN'elndd'rid.
hrbd
3'hidterdre.d&n
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ll:2o@3
rErE6-?)0110?653
lElE&"rF4o$tg
md..!.cm
HL(A-2',)01'&Cr r.iL{e-21)s.6dEE3 . rg5ftnD9d
M3mb6rot rheSGSGroup(SGSSA)
TestReport
No.SHAECI'l19s25001
Date:07Dec2011
Page 5 of 5
Samplepholo:
sHA11n9s250.001
SGS authenticate
the photoon originalreportonly
""' Endof Report"*
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HL@-21)61{@e1 rt{6-21}516u853
Msnb€iol dt6SGSGble {SqSs,q)
TastReport
No. SHAEC1119525002
Date:07 Dec 2011
Page 1 of4
3MCHINALIIVITED
222#T|ANLtNROAD,SHANGHAT
(200233)
Thefollowing
sample(6)
wasi/vere
submitted
andidentified
on behalfofthectientsas :3M 3779-pc
- SH
SGSJobNo.:
sP11-036760
Dateof SampleReceived 03Dec2011
TestingPedod:
03Dec2011-07Dec2O11
Tesl Requested:
Selectedtest(s)as requestedby client.
Test Method:
Pleasereferto nextpage(s).
TestResults:
Pleasereferto nextpage(s).
Signedfor and on behalfof
scs-csTcLtd.
.--),-
,/t*(
Y*
Fan Jingjie,JJ
Approved Signatory
tiu dud
irdd.qlqs*
'r .sd
br rh c.6Fn &b!.r b r! o-nr c.i.dEr.r
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t!'tl.*iEEt
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{orol
atr.ci.43im
..s..hnc&!.d,
(SGSaA)
lrombor
otth€SCSCloup
TestReport
No.SHAEC1119525002
Date:07Dec2011
Page2 of 4
Test Results:
T€st PartDescriotion:
Sp€dm6nNo.
SGSSamplolO
D€6cfiption
1
SHA1l-195250.001Yellowsolid
Remarks:
(1) 1 mg/kg=1 ppm=0.0001%
(2) MDL = MethodDetectionLimit
(3) ND = Not Detected( < MDL )
(4) "-" = Not Regulated
Haloo€n
Test lrethod : With reference
to EN 14582:2007,analysis
wasperformed
(lC).
by lonChromatograph
Testltem{s)
(F)
Fluorine
(Cl)
Chlorine
(Br)
Bromine
lodine(l)
Unit
mg/kg
mg/kg
mg/kg
mg/kg
ftldemd
b &.d by rh. c.rtse &q-i
hd
@,.,gEo*
d..4d,r4d
tudnc
l+ltffill{eq!l.dlgr9
t3ltzEnastql/l!l{i!.'gq
P|q-T5^46N@htuhtr
b h. ofmrc&dlnld
!d
b rlm.ir
o6idri6 k EMor.
h'h
aryi"k.lhb
&ffitL
MDL
50
50
50
50
D.eMr
d mcoMrB.-dM'
rdrd!E
ffi;Eifiaii'*-iiiaii
OA
ND
ND
ND
ND
tu- abdli
d.trtr,rD.cmk_qL.
rEtetlgfdritud&rrirE
$I.5f.h[AlttStots+ll
dnfi.$aoh 2o@3
!l:2@o3
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tErE€6+l)el4!55! taE6-al)t405$?9
Bci.t{.com
r€sdirorF.@
!r!(6-rjl611@o4 H!lt6-zt)sa6K0
MehbrrotlheSGSOlouD(SGSSA)
TestReport
No.SHAEC1'119525002
Date:07 Dec201'1
Page3 of 4
ATTACHMENTS
HalogenTestingFlowChart
1) Nameof thepersonwhomadetesting:
DaisyGong
2) Nameof thepersonin chargeofte6ting:Alex
Jiang
Samplemeasurement
Combustion
in oxygenboftb
Dissolved
in an absorption
solution
Analyzed
by ion
chromatography.
Doubleconfkm
byotherinstruments,
if
rhbdtuiff
| 6rd !r rh conFry rhtd b dr oddr ftrdds3 ar5
hn
daclhublr 4- b r.nr tn! codfr
!l! rd,,!!!!r'*
b ddo.
|.sd.nndbrdi.^ryh&'dls
ddroit, tur. . rn.c@ryr
rn.c@rvr
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rdlon
Doo|Eb
trqld & |d|#
!t ,N
ffis.c.fr4.!4!d!hn
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t'etEl$&lbrsto dxniudtd,gt$aflonr 2@33
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.r idt.'@rj!I!4!rt!!!!r!!_s'q!!!r!
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lwcr.3s"co6
. .ssd'mO69q
(SGgsr)
M6mb6rollheaqsGbup
T€st Report
No.SHAEC1119525002
Date:07Dec2011
Page4 ol4
Samplephoto:
sHA11-195250.001
SGS authenticate
the photoon odginatreportonty
"* End of Report'*'
tTr.t:ry::.
i:?aq!Ke.n:
D-? I'gT.
j!L
1cbj
*nrbr .prdd orb. comr.iy.
hrw.iMridrndnldrhrnrrr.ih..F
l'Dt!.It6eY.l.iicdunosJdshdtorr
tl..ti,*iE8lurt|8ogli3qt
r.(.)r..bd.
200233
lrl:2M3
rEtEl&2r)d14653 lElE6?lje€$da
Hli(s-zll6t@ol &ls-?l)se$
ffi .i..!.cm
..s.dr&F.6
(scssa)
Mlmb€|
olrh.scsGoup
Number : TWNC00233073
Test Report
Applicant:
Littelfuse Philippines Inc.
LIMA Technology Center, Lipa City,
Malvar, Batangas
Date
: Nov 23, 2011
Sample Description:
One (1) group of submitted samples said to be :
Part Description
: Sand Filler
Part Number
: 091251
Date Sample Received
: Nov 17, 2011
Date Test Started
: Nov 18, 2011
Test Conducted :
As requested by the applicant, for details please refer to attached pages.
Authorized By:
On Behalf Of Intertek Testing Services
Taiwan Limited
K. Y. Liang
Director
This report shall not be reproduced
except in full, without the written
approval of the laboratory.
Page 1 of 6
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00233073
Test Conducted
(Ⅰ) Test Result Summary :
Test Item
Result (ppm)
Light Grey Powder
Heavy Metal
Cadmium (Cd) content
Lead (Pb) content
Mercury (Hg) content
Chromium VI (Cr6+) content
Polybrominated Biphenyls (PBBs)
Monobrominated Biphenyls (MonoBB)
Dibrominated Biphenyls (DiBB)
Tribrominated Biphenyls (TriBB)
Tetrabrominated Biphenyls (TetraBB)
Pentabrominated Biphenyls (PentaBB)
Hexabrominated Biphenyls (HexaBB)
Heptabrominated Biphenyls (HeptaBB)
Octabrominated Biphenyls (OctaBB)
Nonabrominated Biphenyls (NonaBB)
Decabrominated Biphenyl (DecaBB)
Polybrominated Diphenyl Ethers (PBDEs)
Monobrominated Diphenyl Ethers (MonoBDE)
Dibrominated Diphenyl Ethers (DiBDE)
Tribrominated Diphenyl Ethers (TriBDE)
Tetrabrominated Diphenyl Ethers (TetraBDE)
Pentabrominated Diphenyl Ethers (PentaBDE)
Hexabrominated Diphenyl Ethers (HexaBDE)
Heptabrominated Diphenyl Ethers (HeptaBDE)
Octabrominated Diphenyl Ethers (OctaBDE)
Nonabrominated Diphenyl Ethers (NonaBDE)
Decabrominated Diphenyl Ether (DecaBDE)
Halogen Content
Fluorine (F)
Chlorine (Cl)
Bromine (Br)
Iodine (I)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Remarks: ppm = Parts per million based on weight of tested sample = mg/kg
ND = Not detected
Responsibility of Chemist : Irene Chiou / Kevin Liu / Cathy Chen
Date Sample Received
Test Period
: Nov 17, 2011
: Nov 18, 2011 To Nov 22, 2011
Page 2 of 6
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00233073
Test Conducted
(Ⅱ) RoHS Requirement:
Restricted Substances
Cadmium (Cd) Content
Lead (Pb) Content
Mercury (Hg) Content
Chromium VI (Cr6+) Content
Polybrominated Biphenyls (PBBs)
Polybrominated Diphenyl Ehters (PBDEs)
Limits
0.01% (100ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for
homogeneous material.
(Ⅲ) Test Method:
Test Item
Cadmium (Cd)
content
Lead (Pb) content
Mercury (Hg)
content
Chromium VI (Cr6+)
content
Polybrominated
Biphenyls (PBBs)
Polybrominated
Diphenyl Ethers
(PBDEs)
Halogen Content
Test Method
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 7, by microwave
digestion until the tested samples are
totally dissolved and determined by
ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in annex C, by alkaline
digestion and determined by UV-Vis
spectrophotometer.
With reference to IEC 62321 edition
1.0:2008 in annex A, by solvent
extraction and determined by GC-MSD
and further HPLC confirmation when
necessary.
With reference to IEC 62321 edition
1.0:2008 in annex A, by solvent
extraction and determined by GC-MSD
and further HPLC confirmation when
necessary.
With reference to EN 14582:2007 by
calorimetric bomb with oxygen and
determined by ion chromatography
Reporting Limit
2 ppm
2 ppm
2 ppm
1 ppm
5 ppm
5 ppm
50 ppm
Remark: Reporting limit = Quantitation limit of analyte in sample
Page 3 of 6
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00233073
Test Conducted
(Ⅳ) Measurement Flowchart:
Test for Cd/Pb/Hg/Chromium (VI)/PBBS/PBDES Contents
Reference Standard: IEC 62321 edition 1.0:2008
Sample preparation
For non-metal part
For metal part
Take sample and immerse into Aqua Regia, start to strip plating layer
Stop the stripping procedure upon color change completely
Take the Aqua solution as plating component and stripped body as substrate component
Cd/Pb/Hg
Cr
Weigh sample and
add organic solvent
By spot test
Negative
Confirm the tested
samples are
totally dissolved
Make up with
deionized water
PBBs/PBDEs
Polymers /
electronics
Metal
For different
material, digest
the sample with
*1
appropriate acid
6+
Get 50cm2 sample
By boiling water
extraction
*2
Weigh sample
and add
alkaline
solution
By Soxhlet
extraction or
Solvent extraction
Definite temp.
extraction
Cool and filter
the extract
Analyzed by ICP-OES
Concentrate the
extract and make up
with organic
solvent
Analyzed by GC-MSD
Make up with deionized
water and add diphenylcarbazide solution
Remarks:
*1: List of Appropriate Acid：
Material
Polymers
Metals
Electronics
Analyzed by UV-VIS
Acid Added for Digestion
HNO3,HCl,HF,H2O2,H3BO3
HNO3,HCl,HF
HNO3,HCl,H2O2,HBF4
*2: If the result of spot test is positive, Chromium VI would be determined as detected.
Page 4 of 6
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00233073
Test Conducted
(Ⅳ) Measurement Flowchart:
Test for Halogen Content
Reference Standard：EN 14582
Sampling/grinding or
cutting
Add absorbent in a
combustion flask &
place weighed sample in
equipment
Fill oxygen into
calorimetric bomb
Ignite then leave the
flask at room
temperature
Transfer the absorbent
into a volumetric flask
Make up with deionized
water
Analyzed by ion
chromatography
End of Report
Page 5 of 6
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00233073
Test Conducted
Photo
Page 6 of 6
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
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iEIS(No.) : cE/2012l10835
E rr?(Dare) : 2012l01/11 F&(P,s")
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Pory Testing Inrcmationsl croup
TestReport
NO.: E122020
t4504D
DaIet 2011.12.23
Page1 of4
Applicant,
SUZHOUXINWUOPTRONICT
TECHNOLOGY
CO.,LTD
368YOUYIRD,YOUYI
DEVELOPMENT
AREA,SONGLING
TOWNWUJIANG
SUZHOU,CHINA
The follo,ringsample(6)
waJweresubmitted
and identified
on behalfoftheclientas.
SampleName,
Ag
Manufacturer,
SUZHOUXINWUOPTRONICT
TECHNOLOGY
CO.,LTO
SampleRecejved
Dat€, 2011.12.20
Te6lPerbd,
2011
.12.20
ro m1l j223
TestRequested,
ln accordancewith
theRoHSDirective
2011/6tEU
AnnexII
Testllethod:
Witheferenceto 1EC62321
Edition
1.0:2008
method:Regutated
Subsiances
Contentof testprocesswithElectrical& Electronic
Products
(1)LeadAnalysis
is performed
byAAS
(2)Cadmium
pertodned
Analysis
is
byAAS
(3)Mercury
Analysis
is performed
by ICP-OES
(4)Ho€valentChromium
Analysis
isperformed
BySpoLtesUBoiling-water€)draclion
Method
(5)PBBS
andPBDE6Analysis
is pedormed
byGC-MS
TestResult:
Pleasereferto nen page(s)
4efi^
Code: sg2wg
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Pory Testinglni€marion l Croup
TestReport
NO.: E12202014504D
Test Result (Unit: mg/kg)
Test llErn
Lead (Pb)
Cadmium(Cd)
MDL
1
(Hs)
Mercury
HetEvalentChromium(Cf )
PBBs
Bromobiphenyl
Dibromobiphenyl
Tribromotiphenyl
Dale,2011j223
1
Tesl Result
N.D,
N,D.
I
See Note (6)
N€gative
N-0.
Page2 of 4
RoHSLimil
1000
100
1000
1000
5
Tetrabrom
obiphenyl
Pentabromobipheny
5
5
5
5
N.D,
N.D,
N.D.
N.D.
N.D.
He)€bromobiphenyl
5
N.D,
Heptabrcmobipheny
5
N.D.
Ochbromobiphenvl
Nonabromobiphenyl
Decabromobiphenyl
5
5
5
N-D.
N.D,
Bromodiphenylether
5
Dibromodiphenyl
ether
Tribromodiphenyl
ether
Tetrabromodipheny
ether
5
Pentabromodiphonyl
ether
He)€bromodiDhenvl
ether
Heptabromodiphenyl
ether
Octabromodiphenyl
ether
Nonabromodiphenyl
ether
Decabromodiphenyl
6ther
5
5
N,D.
N.D.
N.D.
N.D.
N,D.
N.D.
N,D.
N.D,
N-D.
1000
5
5
5
5
N.D.
N.D.
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NO.:El2202014s04D
Dere.2011.12.23 Page3 of 4
(1) mg/kg= ppm
(2) "-" = Doesnot $bubl€
(3) N.D.= Nc'tDgt€cbd(<MDL)
(4) MDL= it€thod DetectionLinit
(5) Tle mo6talrowabretimilvahE eferenceto Rotts One€tive2011/6gEUAnnex II
(6) Spot-Gst:
Negative- Not Det€dsdof Cdl coating,Postive- ftes€nce ol Cfft coarilE;
CIhetasled sampleshouldb€ tunherEilEd by boiling{arer€{Edion m€thodif ih€ spottsst rcsuttcannorbe
@.rimsd or n€sali€)
Boiling-lvatr€n6dbn:
Neg.iive = Not D€t€ctodof C t coating
PGiti€ = P€s€ncs of C l coatingiths dot€cted@ncentratbnin boiting.water-extradion
soturionis eqEl
or gr.al€r thano.o2mg/kgwith5o6n2samptesudacoareaused.
Ponyauihenticate
lhe photoon o ginalreportonly
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T€st Report
NO.: T12152015704D Daie: 2010.12.20
Page4 of4
Measurcmenl
Flow'charl
TheseSamplosWgreDissolvedTotallyBy Pre-conditioning
l\IethodAccordingTo BetowFtd,vChart.(Cf*
And PBBS,/PBDES
TestMethodExcluded)
'"End of Reporl'"
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TESTREPORT
NO.:4002E11121307-2R02
page1of4
Oa!aiDec15,2o11
Customer:SuzhouFuHongElectrcnic
IndustfialCo,
Ltd.
Addrgs8:NO.89WElDUROAD,WANGTING
TOWN,
XTANGCHENG
D|STR|CT,
SUZHOU,
CHTNA
Reporton th6 3ubmittedssmplesaidio be
Samplename:Fusoscoppershell
llodol: /
Material:/
D$cription:/
Buyea:/
supplier:/
Sa|nplerecelveddate:Dec.13,2011
Tcatlngp€riod:FrcmDec.13,2011
to Dec.15,2011
T€tino Reau6ted
As specined
by client,to delermine
theL€ad,Cadmium,
Mercrry& Hexavatent
Chrcmium
contentin thesubmitted
samptein
accordancewilh Direclive2002/95/EC(RoHS).
Tcstindmethod:
Testing llem
[,leasudng
inslrument
MQL
Lead (Pb)
EC 62321:2008,seclion9
ICP-OES
2mglkg
cadmium(Cd)
(Hg)
Mercury
EC62321:2008,sectionI
ICP€ES
2 mg/kg
EC62321r
2008,section7
rcP-oEs
2 mg/kg
(Crl'I)
Chrom'um
EC62321:2008,
AnnexI
0.02mg,a(g'
lsg
-'0.02mg/kgreturs
10lheMQLofsample
extEction
tiquid.
99!s!.c!i9!j
-ffien tesiedas specifred
thesubmitted
sample
complied
withtherequircments
of commission
Decision
of 18Aug2005
amending
Directive
2002l95/EC
nolified
lnderdocument
2005/618/EC
ILS, PLEASEREFERTOTHE FOLLOWINGPAGE(S)'**'
',:,"il:::i"
ryf4
,3ffi::::1,,44
hrn
lffH*"",",We-i
S}'EI{ZN€N AOV TGSTINGT€CHNOlOGY CO.,L'D.KUNSHAN EiANCH
Hotllne
86-512-551
80 0 0
nov
6
TESTREPORT
NO.:4002E11121307-2R02
Add the digestionsolution;the
vesselis heatedLrntillhe sampl€
AddHrO,unlilthesampl€is clear
F;;1.-F;;,",..;-1.-
Cooling
thevessel,fllleriwashedand
filledto themarkwithdistilled
water.
{Melalsubslrat€)
Add lhe digestionsolution,clos€
The sampleis digestedin the
the macrowavevess€|.
micrcwave oven following a specific
program.
decomposilion
Coolingthe vessel,filter washedand
filled to the mark with distilled water.
Remove
thesample,
andcool
lhe beakerlo rcomtempefalure,
anddo1ie colorreaction
Heal50 mL ofDlwaterin lhe
beakertoboilingfor 10 min
Testthesamplesolution
andlhe 0.02
mg/kgstandard
solution
by UV-VIS.
To Detemine
(Praring)
andl\rercury
Content:
coor,ns.
nrr",
*""n"0 r"o
_____-l
""0 |
I
tothemark
withDtwater
I
,l o*o
-ill_.;*--;-l
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STIENZH€NAOV TESIING T€CIII{OLOGYCO.,lIO,KUII9HAN BFANCH
Hdpi/j,w.o{,6n
|
-.-
|
Hotline
8 6 - 5 1 2 " s 5 18 0o O 0
nov.
TESTREPORT
NO.:
4002E11121
307-2R02
Date:Dec.15,2011
Page3 ol4
5. ToDetemineHexavalent
Chromium
Contentln
colorless
andcolored
ctlromate
coalingon metals: (Plating)
'' ',.'1
re$eoovr I r
s.t sw-resi (M&
lflhe lest resullis positive,
the sampleis considered
1o
havehexavalenlchromium
Boiling- waieF extraction
procedure
shallbe usedto
and the 0.02 mg/kg
lfthe€ isrnterference
orI rshardto decide*terhel
lhesamplehavethehexavalent
chrcmium
5 2 BoilingwEter-en€ction
Takethe (5015)cm'z
samplein thebeaker.
Heat50 mlof Olwaterin the
beaker
lo boilingfor 10min
Remove
he sample,
andcool
lhe beaker
1oroomtemperature,
anddo thecolorreaction
Testthe samplesolutionand the 0.02
mg/kgstandardsolutionby UV-VIS.
Srmple d93cription:
Coppershellsubslrate
Leadwle Platrng
Unil
24
CoppershellPlaling
RoHS
Limit
2-3
24"
Lead(Pb)
mg/Kg
1000
N.D.
2.5
40.0
N.D.
Cadmium
{Cd)
mg/kg
100
N,D.
N.D.
N.D.
N.D.
(Hs)
Msrorry
(Crvl)
Chromium
mg/kg
1000
N.D,
N.D,
N.D.
N.D.
mg/Kg
1000
Negative Negative Negalive
Negative
SH!NZHEN AOV TESTINGTCCTNOIqGY CO.,L}D,KUNSHAN BFANCH
n
Hotline
86'512^551
80 0 0
nov.
TESTREPORT
NO.rA002E11121307-2R02
Dat€iOec15,2011
-The new RoHSdi.ective2011/65/EU,
on Jul 21, 2011comeinto force,on Jan.03, 2013the fomat imotementation.
Dircctive
2002l95/ECshallbe reoealedsimultaneouslv.
Sp€cim€ns,wnicnrequestedto determineLead,Cadmiumand l4ercuryConlent,havebeendissotvedcomptetety.
-mg/kg=ppm
-N.D.=notdetected(<tVoL)
-MQL=l'rethodOuaniilationLimit
-Negalive=Abs€nce of Cr (VI);
Posilive=Prcs€nce
of Cr (VI)i
Uncedain=c€n noi ve fy whetherthe samplehaveHexavat€nt
Chrcmium by spoliesl.
(The tested s€mple should be furlher venfed by boiling-waterextradion
method if the spol test result is uncertainor
-'The test is basedon the followingassumption:Thesampteptatingis a singtetayerandeach pad is unifom. The test resutt
maybecannolslandior rhe physicartruthof sampleplating.
Photog.aphofSample
"'End of Repod"'
S'iE'!ZH€N AOVT€STING TECXNO!OGYCO..lIO,KUNSHAN ABANCH
Hh,:/fuloi6n
n
Hotline
86-512-551
80 0 0