ICPTest_216XEP_08 13 2012 pdf

ICP Test Report Certification Packet
Company name :
Littelfuse, Inc.
Product Series:
216 series Axial Leaded Fuse
Product #:
216XEP
Issue Date:
August 13, 2012
It is hereby certified by Littelfuse, Inc. that there is neither RoHS (EU Directive 2002/95/EC,
2011/65/EU)-restricted substance nor such use, for materials to be used for unit parts, for
packing/packaging materials, and for additives and the like in the manufacturing processes.
In addition, it is hereby reported to you that the parts and sub-materials, the materials to be used
for unit parts, the packing/packaging materials, and the additives and the like in the manufacturing
processes, are all composed of the following components.
Issued by:
<Global EHS Engineer >
(1) Parts, sub-materials and unit parts
This document covers the 5x20 Fuse RoHS-Compliant series products manufactured by
Littelfuse, Inc.
< Raw Materials Used
Please see Table 1
(2) The ICP data on all measurable substances
Please see appropriate pages as identifed in Table 1
Remarks:
Form 585-047 Rev. A
1
2/21/06
Table 1: List of Raw Materials covered by this report
Total Parts
1
2
3
4
5
6
7
Raw Material Part Number
910-005
692539-002
909-455
091251
082xxx
C030210
C030210
Raw Material Description
Cap
Solder
Body
Sand Filler (RoHs & Halogens)
Wire-AgCu
Overcap (Cap base & plating)
Overcap (Wire base & plating)
2
Page(s)
3-6
7-11
12-22
23-28
29-38
39-42
39-42
nov^
TESTREPORT
NO.4002R12050740-1R02
Daie:May.09,2012
Cu8tomer:SuzhouFuHongElectrcnic
IndustrialCo.,
Ltd.
AddT€€3:NO,69\ryEIDUROAD,WANGTING
TO\M{,XIANGCHENG
OISTRICISUZHOU.
CHINA
R€pot on the submitt€d sample sald to b€
Samplenah€: Copp€rsh€ll
Supplier:/
Samplerocolv€ddate:lvlay.07, 2012
T6tf ng pedod: Frcmluay.07,29l2toMay.A9,2012
T€€tino R€ou€6tod
As specifiedby clienl,lo delerminethe Lead,Cadmium,
l\,telcury
& Hexavalent
Chrcmiummntentin the submitledsamplein
.ccodancewilh Dircctive200295/EC(RoHS).
T€stino method:
I\l1QL
IEC62321:2008,seclionI
cadmium(Cd)
IEC62321:2008,seclion9
Mercury(Hs)
(CrVI)
chrcmium
IEC62321 2008,s€ction7
tcP-oEs
rcP-oEs
tcP-oEs
IEC62321i200EAnn€xB
2mg/kg
2 mg/kg
2 mSeS
0.02mg/kg'
Ieq
r 0.02mgl(g efers to the MQLofsampbenractiontiquid.
Concll|3ion:
-Whenlestedas specifiedlhe submitledsampl€€ompliedwith the requircments
of commission
Decisionof 18 Aug 2005
amendingDirecnve
2002r95/Ecnotifiedunderdocument
2005/61E/Ec.
*'*FOR FURTHERDETAILS.
PLEASEREFERTOTHEFOLLOWING
PAGE{S).*'"
Sigmdior andon behalfof
Shenzhen
AOVTeslingTechnology
Co.,Lld,KunshanBranch
/uI?'
,.r.ou.o.,,
oro.'n,44.
Li nngtng, lMaggie
Ch€micalTestDi€ctor
S}I€I\IZIIENAOV TESTINGTECHNOLOGY
CO.,ITD.(UI{SHAN ERANCH
ol:9Jllis,.*""
nov'
TESTREPORT
NO. A002R12050740-1R02
Add lhe digeslion€olution;lhe
vesselis heal€dunlilthe sample
f*;;1.,-
Coolinglhe vessel,fiteri washedand
T6st€dby tCP-OEs
filledto the man(withdislilledwater
Th8sampleis digesredin the
micrcwave
ov€niollowinga specific
decompositionprogram
Coolinglhevessol,filtsr;wasi€d and
filledlo lhe markwilhdistilled
water.
(boitingChromium
Content
warerext€crion)r
subsrrare)
{Mstat
Removetnesample,snd cool
Heal50 mL ofDlwalerin the
beakerto boilingfor 'l 0 min
-j.f*--*
lhe beakerto rcomtemp€€turc,
anddo the colorr€action
Testlhe samplesolutionandlhe 0.02
mg/kgstandardsolutionby W-VIS.
ToDsbmine d,C4lmiumandMercury
Conbnt(Plating)
Cooling,filter;washed
andfjll€d
lo lhe markwithDl water.
-------------l
-r€st€d by
________'
l__rl nupo,r I
Instumenl |
SHENZHEI\I
AOV T€STII{OTECHI{OLOGY
CO.,!TO.XUNSTIA BNA CH
|
|
Hotllne
nov'
TESTREPORT
NO
Dats:iray 09,2012
Page3ot4
5. To DetemineH€xavalent
Ch.omiumContenlin colorlessand coloredchromatecoalingon metals:(Plaling)
",ffii'Q*a*
lf lh€ tast r€sult is positive,
lhe samplels considered
lo
hav€hexavalenl
chromium
lfthe l€st tesull
and lhe 0.0?mg/kg
Boiling- waler- enraclion
proc€dureshall be used to
lfthe|eis interierence
oritis hardlodecidewhether
the samplehavelhe ho(avalent
chromium
5.2 Boiling-waleFexlraclion
Takethe (5015)cm'z
Remov€lhe sample,andcool
Heats0 mloforwalerin lhe
beaker
!o boiling
for10min
the b€akorlo roomtsmp€ralute,
anddo the colorreaction
Teslthe samplesolution
andthe 0.02
mg/kgslandaritsolutionby UV-VIS.
Pl€ring
Lead(Pb)
(cd)
cadmium
(Hg)
Mercury
(Cr\,I)
chromium
Unil
RoHSLimil
mg/xg
1000
100
1000
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
1000
Negalive
Negalive
mg/Kg
mg/xg
mg/xg
SHENZHENAOV TISTII{G IECHNOfOGYCO.,!TO.XUNSIIATINA CH
Hotline
36.512-55100000
novTESTREPORT
NO.:4002R12050740-1R02
-Tnen€w RoHSdi€ctive2011/65/EU,
on Jul.21, 2011 com€inloiorce,on Jan 03,2013 thefomat imptemenlaton,
Dircctrve
2002/95/EC
sh.ll be rcp€aledsimultaneousty.
-Specimens,
whichrequesred
to detemineLead,Cadmiumand MercuryConrent,
haveboendissotved
compt€r€ty.
-N.D.=not
detecGd(<rUaL)
]\,lQL=lvlethod
Quantilation
Limit
-Negative=Absene
or cr (VI):
'Positive=Presence
of Cr (VI)l
Uncedain=
can nolv€dfywhetherthe samplehav€Hexavalent
Chromium
by spot-test.
(The lerled sampleshouldbe tunherveified by boiting,wal€r+xtraclion
methodif lhe spot test resuttis uncedainol
sThe tesl is basedon the followi.gassumplion:
The sampteptaringis a singlelayerandeachpa( is unifom The testresult
maybecannotsrandior lh€ physicalttuth
ofsampteptating.
Photographof Sample
SHINZIIENAOVTESIINGTFCHNOLOGYCO.,LTO-KUNSHABRAI{CH
Ollo.tll.?,.""""
TestR€port
No.SHAEC1116009839
Date:14 Ocl2011
Page1of 5
ZHEJIANGASIA GENERALSOLDERING& BRAZINGMATERIALCO,,LTD
XIHU INDUSTRIALPARK,SANDUN,HANGZHOU
CITY,ZHEJIANG
PROVINCE,CHINA
Thefollowing
sample(s)
was^/vere
submitted
andidentified
on behalfof thecrients
as : LEAD-FREE
soLDER
WIRE
SGSJobNo.:
ModelNo.:
Composition:
Dateof SampleReceived
:
TestingPedod:
Test Requested:
- SH
sP11-030781
YTW102(692539-002)
Sn2.ocuRE
09 Oct2011
09Oct2011- 13Oct2011
Selectedtest(s)as requestedby client.
Test Method:
Pleasereferto nextpage(s).
Test Results;
Pleasereferto nextpage(s).
Basedontheperformed
testson submitted
samples,
theresultsof Lead,
Mercury,
Cadmium,
Hexavalent
chromium,
Polybrominated
(pBB),
biphenyls
Polybrominated
diphenylethers
(PBDE)complywith
thetimitsas setby RoHS
Directive
20'11/65/EU
Annexll; recasting
2002/95/EC.
Condusion
:
Signedforandon behalfof
SGS-CSTC
Ltd.
7Qv
Fan Jingjie,JJ
Approved
Signatory
rd adlrN
h.csFry-+dbnctqLo6&d..lSrnFrituori.d,e|ilhdqu.r&*asbrn^@J/{*.r!..@tu
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dffi
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hrri.rry
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nL(H1J61{&504H!(d-21)tl6d!lll . q3.drr€rt-@n
M6nboror$€ 69S Oroop(SGSa )
TestReport
No.SHAECl116009839
Date:14 Oc12011
Page2 of 5
TestResults:
Test PartDescdotion:
SpodrnonNo.
SGSSamptotD
DosoriBlon
I
SHA11_160098.034Si|very
metalwhe
Rem€rks:
(1)1 mg/kg= 1 PPm=0.0001%
= MethodDetection
(2) IVIDL
Limit
=
(3) ND NotDetected
( < MDL)
(4)"-" = NotRegulated
RoHSDl€dive 2011r'65/EU
TestMethod: Withreference
to IEC62321:2008
(1)Determination
of Cadmium
by ICP-OES.
(2)Determination
of Leadby ICP-OES.
(3)Determination
of Mercury
by lCP-OES.
(4)Determination
of Hexavalent
Chromilmby Spottest/ Colodmetric
MethodusingUV-Vis.
(5)Deterfiination
of PBBS/ PBDES
by GC-IrS.
Test ltem{s)
Cadmium(Cd)
Lead(Pb)
Mercury(Hg)
Hexavalent
Chromium(Cr(Vl))
Sumol PBBS
Monobromobiphenyl
Dibromobiphenyl
Tribromobiphenyl
Tetrabrcmobiphonyl
Pentabromobiphenyl
Hexabromobiphenyl
Heptabromobiphenyl
Odabromobiphenyl
Nonabromobiphenyl
Decabromobiphenyl
thi!
ud!
10O
1,000
mg/kg
mgikg
1,0_00mslks
1,000
-
mg/kg
mg/Kg
mg/Kg
mdks
mwKs
mgKg
mg/Kg
ms,Ks
mg/kg
_
mgKg
mgiKg
1,000 ms/ks
-
l\ronobromodiphenyl
ether
mg/Kg
MD!
034
2
2
2
O
-
N
D
165
N
D
Negative
N
D
5
5
5
5
5
5
5
5
5
5
,
N
N
N
N
N
N
N
N
N
N
N
D
D
D
D
D
D
D
D
D
D
D
5
N
D
, bYrb cdtsnr $$.r b rr sd{
tu
'tootud&qd
b lmr u
3'a-Eberrrto
d&tuaudrglol|
2o@go
tl..t,|.*JE6il|ll33et3*t
ll@t
IE €16-2i)61@63 lE€ pea)eFCfig
H!(S-Z)6 q04
Hjl6-AF.a)Br
w.6,t!.@
. qFd'aroF.o
Momhcrorihe 8CSOroup(sGA8l)
TestReport
No.SHAEC1116009839
Test ltem{s)
Dibromodiphenyl
ether
Tribromodiphenyl
ether
Tetrabromodiphenyl
ether
Pentabromodiphenyl
ether
Hexabromodiphenyl
elher
Heptabromodiphenyl
ether
Oc€bromodiph€nyl
ether
Nonabromodiphenyl
ether
Decabromodiphenyl
ether
Date:14 Oct 2011
ud!
tiEil
ng/Kg
mg/Kg
mgKg
mgKg
mg/Kg
mg/Kg
mg/(g
mg/kg
mg/kg
MDt
034
5
5
5
5
5
5
5
5
5
ND
ND
ND
ND
ND
ND
ND
ND
ND
Page 3 of 5
Notes:
(1)Themaximum
permissible
limitis quotedfromdirective
2011/65/EU,
Annexll
(2)o spot-test:
= AbsenceofCrVlcoating,
= presence
Negative
Positive
of CrVtcoating;
Thetestedsampleshouldbefurtherverifiedby boiting-waterextraction
methodifthe spottestresultis
Negative
or cannotbeconfirmed.
. Boiling-water-extraction:
= Abs€nceof CrVlcoating;Positive
= Presenc€
Negative
of CrVlcoating
Thedetected
concenhation
in boiling-water-extraction
solutionis equalor greaterthan0.02mg/kgwith5C
cmzsamolesurfacearea.
protection
Forcorrosion
coatings
on metals:Information
onstorageconditions
andproduction
dateofthe
testedsampleis un€vaibble
andthusresultsof Cr(Vl)represent
stratus
of thesampteat thetimeof
testing
nrdmd
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TestReport
No.SHAEC1116009839
Date:14 Oct 2011
Page4 of 5
ATTACHMENTS
RoHSTestingFtowChart
'1)Nameof the pe6onwhomade
testing:
JanShi/yoyo
Wangy'Allen
Xiao/Gary
Xu
2) Nameof the personin chargeof testing:
JeffZhanglceorge
Xu/EtimLin
3) Thesesamples
weredissolved
totallyby preconditioning
methodaccordlng
to belowflowcnan.
(Cr6+andPBBS/PBDEStest
methodexctuded)
SamplePreparation
SampleMeasurement
Pb/Cd/Hg
PBBs/PBDES
Heatingto 90-9511
for extraclion
1)AlkaliFusion/
DryAshing
2) Acidto dissolve
Filtrationand pH
adjustment
Adding1,5diphenylcarbazide
forcolor
development
rh!@d
b b.!d br rh. Od4.ny uqd b r| Or.ra C.d{!.
ol6.ri6 lnN o{'Li...r.1.
ffi
d.di.raiq. r.@ r$ c.d{rd
E
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t4q4
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20023
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indicates
the
presence
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necessary,
d i@l&4:$!4!!4!@I4
tui.nrd*
! |o b cn.d rd fir tutuid'r
| E!EFeA)6!(EA
tr{6-2t611@5aa
Adding1,S
diphenylcarbazide
for color
development
i.6'nerr'.
id .rbm!
lE!E(S-al)6tFSt9
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TestReport
No.SHAECIl16009839
Date:14 Oct2011
Page 5 of 5
Samplephoto:
sHAl 1-160098.034
SGSauthenticate
the photoon originalreporlonly
'** Endof Report'"
'-6.hk
ht'rH
-Fdrr'
drybr[
rmpr.{.) hdi
3'ltEr5&ltn&.d)0hr!sBtrE[drt
*r'I|.$,E8tl!l689rw+ll
20@3
tl:M
IEtE&4r)fl{lr6r
rEiEFa)6{srt
tllj (6-2t61a@Sa H.:F-a)s5dB65
Mc,nturoltlo SOSOrcu9IAGS&1)
Number : TWNC00233073
Test Report
Applicant:
Littelfuse Philippines Inc.
LIMA Technology Center, Lipa City,
Malvar, Batangas
Date
: Nov 23, 2011
Sample Description:
One (1) group of submitted samples said to be :
Part Description
: Sand Filler
Part Number
: 091251
Date Sample Received
: Nov 17, 2011
Date Test Started
: Nov 18, 2011
Test Conducted :
As requested by the applicant, for details please refer to attached pages.
Authorized By:
On Behalf Of Intertek Testing Services
Taiwan Limited
K. Y. Liang
Director
This report shall not be reproduced
except in full, without the written
approval of the laboratory.
Page 1 of 6
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Number : TWNC00233073
Test Conducted
(Ⅰ) Test Result Summary :
Test Item
Result (ppm)
Light Grey Powder
Heavy Metal
Cadmium (Cd) content
Lead (Pb) content
Mercury (Hg) content
Chromium VI (Cr6+) content
Polybrominated Biphenyls (PBBs)
Monobrominated Biphenyls (MonoBB)
Dibrominated Biphenyls (DiBB)
Tribrominated Biphenyls (TriBB)
Tetrabrominated Biphenyls (TetraBB)
Pentabrominated Biphenyls (PentaBB)
Hexabrominated Biphenyls (HexaBB)
Heptabrominated Biphenyls (HeptaBB)
Octabrominated Biphenyls (OctaBB)
Nonabrominated Biphenyls (NonaBB)
Decabrominated Biphenyl (DecaBB)
Polybrominated Diphenyl Ethers (PBDEs)
Monobrominated Diphenyl Ethers (MonoBDE)
Dibrominated Diphenyl Ethers (DiBDE)
Tribrominated Diphenyl Ethers (TriBDE)
Tetrabrominated Diphenyl Ethers (TetraBDE)
Pentabrominated Diphenyl Ethers (PentaBDE)
Hexabrominated Diphenyl Ethers (HexaBDE)
Heptabrominated Diphenyl Ethers (HeptaBDE)
Octabrominated Diphenyl Ethers (OctaBDE)
Nonabrominated Diphenyl Ethers (NonaBDE)
Decabrominated Diphenyl Ether (DecaBDE)
Halogen Content
Fluorine (F)
Chlorine (Cl)
Bromine (Br)
Iodine (I)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Remarks: ppm = Parts per million based on weight of tested sample = mg/kg
ND = Not detected
Responsibility of Chemist : Irene Chiou / Kevin Liu / Cathy Chen
Date Sample Received
Test Period
: Nov 17, 2011
: Nov 18, 2011 To Nov 22, 2011
Page 2 of 6
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Number : TWNC00233073
Test Conducted
(Ⅱ) RoHS Requirement:
Restricted Substances
Cadmium (Cd) Content
Lead (Pb) Content
Mercury (Hg) Content
Chromium VI (Cr6+) Content
Polybrominated Biphenyls (PBBs)
Polybrominated Diphenyl Ehters (PBDEs)
Limits
0.01% (100ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for
homogeneous material.
(Ⅲ) Test Method:
Test Item
Cadmium (Cd)
content
Lead (Pb) content
Mercury (Hg)
content
Chromium VI (Cr6+)
content
Polybrominated
Biphenyls (PBBs)
Polybrominated
Diphenyl Ethers
(PBDEs)
Halogen Content
Test Method
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 7, by microwave
digestion until the tested samples are
totally dissolved and determined by
ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in annex C, by alkaline
digestion and determined by UV-Vis
spectrophotometer.
With reference to IEC 62321 edition
1.0:2008 in annex A, by solvent
extraction and determined by GC-MSD
and further HPLC confirmation when
necessary.
With reference to IEC 62321 edition
1.0:2008 in annex A, by solvent
extraction and determined by GC-MSD
and further HPLC confirmation when
necessary.
With reference to EN 14582:2007 by
calorimetric bomb with oxygen and
determined by ion chromatography
Reporting Limit
2 ppm
2 ppm
2 ppm
1 ppm
5 ppm
5 ppm
50 ppm
Remark: Reporting limit = Quantitation limit of analyte in sample
Page 3 of 6
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Number : TWNC00233073
Test Conducted
(Ⅳ) Measurement Flowchart:
Test for Cd/Pb/Hg/Chromium (VI)/PBBS/PBDES Contents
Reference Standard: IEC 62321 edition 1.0:2008
Sample preparation
For non-metal part
For metal part
Take sample and immerse into Aqua Regia, start to strip plating layer
Stop the stripping procedure upon color change completely
Take the Aqua solution as plating component and stripped body as substrate component
Cd/Pb/Hg
Cr
Weigh sample and
add organic solvent
By spot test
Negative
Confirm the tested
samples are
totally dissolved
Make up with
deionized water
PBBs/PBDEs
Polymers /
electronics
Metal
For different
material, digest
the sample with
*1
appropriate acid
6+
Get 50cm2 sample
By boiling water
extraction
*2
Weigh sample
and add
alkaline
solution
By Soxhlet
extraction or
Solvent extraction
Definite temp.
extraction
Cool and filter
the extract
Analyzed by ICP-OES
Concentrate the
extract and make up
with organic
solvent
Analyzed by GC-MSD
Make up with deionized
water and add diphenylcarbazide solution
Remarks:
*1: List of Appropriate Acid:
Material
Polymers
Metals
Electronics
Analyzed by UV-VIS
Acid Added for Digestion
HNO3,HCl,HF,H2O2,H3BO3
HNO3,HCl,HF
HNO3,HCl,H2O2,HBF4
*2: If the result of spot test is positive, Chromium VI would be determined as detected.
Page 4 of 6
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Number : TWNC00233073
Test Conducted
(Ⅳ) Measurement Flowchart:
Test for Halogen Content
Reference Standard:EN 14582
Sampling/grinding or
cutting
Add absorbent in a
combustion flask &
place weighed sample in
equipment
Fill oxygen into
calorimetric bomb
Ignite then leave the
flask at room
temperature
Transfer the absorbent
into a volumetric flask
Make up with deionized
water
Analyzed by ion
chromatography
End of Report
Page 5 of 6
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Number : TWNC00233073
Test Conducted
Photo
Page 6 of 6
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
,fl.d,+E+
TestReport
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/ t r i t h r e f e r e n c e t o u s E P A3 5 4 0 c
1 9 9 6n € t h o d f o r P F o SC o . l e . l .
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an+6.(J+) / PFoA(cAsNo.: 3356?
r)
++US EPA3540c:l996tt!,
,Xtl
&Eif 1{r*{,*fl an+d(n) }f
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1 9 9 6e e t h o d f o r P F O AC o n t e n t .
Analysis was perfofned by rc/MS.
i j :i :r l , ]. r : . a i i . ; ; r t i ]
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Test Report
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i;*Sxad
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623211
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ro IEC 62321:?008 and perforned
by rc/MS.
5
5
5
5
5
5
5
5
5
5
5
5
5
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a* / s"l.s."
(fr.) / Halogen-Floo.ine(F) (c{s
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PFos++*d,(R"f
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of prepararrons
(2rtit{ttX4n&*fi&}.ei+d."%d.6s{.*{r1+;1!i*€1+}aX*Jt+ApFosi.4t?J*fi}.e.t&r€t6€};l4pFosEE
,i.&+,i!d.i,ifo.r%,6*r&€d.4{tti.4rf. {,RprrsaAt*f + 6E*;Ad.Ji;Aruc/.,.
(Maynot be placed on ihe na.k€t in seni-linisned prodocts or articles, or pa.ts rhereof, if
ure
c o n c e n t . a t i o n o f P F O Si s e q u a t r o o r h i g h e . t h a n 0 . 1 % b y n a s s c a l c ! l a t e d s i t h r e f e r e n c e t o t l e n a s s o f
s t . u c t u r a l i y o . f r i c . o s t r u c r u r a l l y d i s r i n . r p a r r s t ! a i c o n t a i n P F o . so r , f o . r e x r i t e s o r o t h e . c o a r e d
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4,;) /Acid dig€slion by suitabte acid dependedon
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iEIS(No.) : cE/2012l10835
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n^ ld,ElF / Firstlestry proce.s------------f
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jrl:i,A ll, : #,*e / Nameof thepersonin cbargeof measurement:
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r
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TroyChang
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10835
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TESTREPORT
NO.:4002E11121307-2R02
page1of4
Oa!aiDec15,2o11
Customer:SuzhouFuHongElectrcnic
IndustfialCo,
Ltd.
Addrgs8:NO.89WElDUROAD,WANGTING
TOWN,
XTANGCHENG
D|STR|CT,
SUZHOU,
CHTNA
Reporton th6 3ubmittedssmplesaidio be
Samplename:Fusoscoppershell
llodol: /
Material:/
D$cription:/
Buyea:/
supplier:/
Sa|nplerecelveddate:Dec.13,2011
Tcatlngp€riod:FrcmDec.13,2011
to Dec.15,2011
T€tino Reau6ted
As specined
by client,to delermine
theL€ad,Cadmium,
Mercrry& Hexavatent
Chrcmium
contentin thesubmitted
samptein
accordancewilh Direclive2002/95/EC(RoHS).
Tcstindmethod:
Testing llem
[,leasudng
inslrument
MQL
Lead (Pb)
EC 62321:2008,seclion9
ICP-OES
2mglkg
cadmium(Cd)
(Hg)
Mercury
EC62321:2008,sectionI
ICP€ES
2 mg/kg
EC62321r
2008,section7
rcP-oEs
2 mg/kg
(Crl'I)
Chrom'um
EC62321:2008,
AnnexI
0.02mg,a(g'
lsg
-'0.02mg/kgreturs
10lheMQLofsample
extEction
tiquid.
99!s!.c!i9!j
-ffien tesiedas specifred
thesubmitted
sample
complied
withtherequircments
of commission
Decision
of 18Aug2005
amending
Directive
2002l95/EC
nolified
lnderdocument
2005/618/EC
ILS, PLEASEREFERTOTHE FOLLOWINGPAGE(S)'**'
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S}'EI{ZN€N AOV TGSTINGT€CHNOlOGY CO.,L'D.KUNSHAN EiANCH
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86-512-551
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6
TESTREPORT
NO.:4002E11121307-2R02
Add the digestionsolution;the
vesselis heatedLrntillhe sampl€
AddHrO,unlilthesampl€is clear
F;;1.-F;;,",..;-1.-
Cooling
thevessel,fllleriwashedand
filledto themarkwithdistilled
water.
{Melalsubslrat€)
Add lhe digestionsolution,clos€
The sampleis digestedin the
the macrowavevess€|.
micrcwave oven following a specific
program.
decomposilion
Coolingthe vessel,filter washedand
filled to the mark with distilled water.
Remove
thesample,
andcool
lhe beakerlo rcomtempefalure,
anddo1ie colorreaction
Heal50 mL ofDlwaterin lhe
beakertoboilingfor 10 min
Testthesamplesolution
andlhe 0.02
mg/kgstandard
solution
by UV-VIS.
To Detemine
(Praring)
andl\rercury
Content:
coor,ns.
nrr",
*""n"0 r"o
_____-l
""0 |
I
tothemark
withDtwater
I
,l o*o
-ill_.;*--;-l
I r*r.r*t
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STIENZH€NAOV TESIING T€CIII{OLOGYCO.,lIO,KUII9HAN BFANCH
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nov.
TESTREPORT
NO.:
4002E11121
307-2R02
Date:Dec.15,2011
Page3 ol4
5. ToDetemineHexavalent
Chromium
Contentln
colorless
andcolored
ctlromate
coalingon metals: (Plating)
'' ',.'1
re$eoovr I r
s.t sw-resi (M&
lflhe lest resullis positive,
the sampleis considered
1o
havehexavalenlchromium
Boiling- waieF extraction
procedure
shallbe usedto
and the 0.02 mg/kg
lfthe€ isrnterference
orI rshardto decide*terhel
lhesamplehavethehexavalent
chrcmium
5 2 BoilingwEter-en€ction
Takethe (5015)cm'z
samplein thebeaker.
Heat50 mlof Olwaterin the
beaker
lo boilingfor 10min
Remove
he sample,
andcool
lhe beaker
1oroomtemperature,
anddo thecolorreaction
Testthe samplesolutionand the 0.02
mg/kgstandardsolutionby UV-VIS.
Srmple d93cription:
Coppershellsubslrate
Leadwle Platrng
Unil
24
CoppershellPlaling
RoHS
Limit
2-3
24"
Lead(Pb)
mg/Kg
1000
N.D.
2.5
40.0
N.D.
Cadmium
{Cd)
mg/kg
100
N,D.
N.D.
N.D.
N.D.
(Hs)
Msrorry
(Crvl)
Chromium
mg/kg
1000
N.D,
N.D,
N.D.
N.D.
mg/Kg
1000
Negative Negative Negalive
Negative
SH!NZHEN AOV TESTINGTCCTNOIqGY CO.,L}D,KUNSHAN BFANCH
n
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86'512^551
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TESTREPORT
NO.rA002E11121307-2R02
Dat€iOec15,2011
-The new RoHSdi.ective2011/65/EU,
on Jul 21, 2011comeinto force,on Jan.03, 2013the fomat imotementation.
Dircctive
2002l95/ECshallbe reoealedsimultaneouslv.
Sp€cim€ns,wnicnrequestedto determineLead,Cadmiumand l4ercuryConlent,havebeendissotvedcomptetety.
-mg/kg=ppm
-N.D.=notdetected(<tVoL)
-MQL=l'rethodOuaniilationLimit
-Negalive=Abs€nce of Cr (VI);
Posilive=Prcs€nce
of Cr (VI)i
Uncedain=c€n noi ve fy whetherthe samplehaveHexavat€nt
Chrcmium by spoliesl.
(The tested s€mple should be furlher venfed by boiling-waterextradion
method if the spol test result is uncertainor
-'The test is basedon the followingassumption:Thesampteptatingis a singtetayerandeach pad is unifom. The test resutt
maybecannolslandior rhe physicartruthof sampleplating.
Photog.aphofSample
"'End of Repod"'
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n
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