ICP Test Report Certification Packet
Company name :
Littelfuse, Inc.
Product Series:
3.6 x 10 mm Axial Leaded Fuse
Product #:
876xxx Series
Issue Date:
May 25, 2012
It is hereby certified by Littelfuse, Inc. that there is neither RoHS (EU Directive
2002/95/EC)-restricted substance nor such use, for materials to be used for unit parts, for
packing/packaging materials, and for additives and the like in the manufacturing processes.
In addition, it is hereby reported to you that the parts and sub-materials, the materials to be used
for unit parts, the packing/packaging materials, and the additives and the like in the manufacturing
processes, are all composed of the following components.
Issued :
<Global EHS Engineer>
(1) Parts, sub-materials and unit parts
This document covers the 3.6 x 10 mm Axial Leaded Fuse, RoHS-Compliant series
products manufactured by Littelfuse, Inc.
＜ Raw Materials Used
Please see Table 1
(2) The ICP data on all measurable substances
Please see appropriate pages as identifed in Table 1
Remarks：
Form 585-047 Rev. A
1
2/21/06
Table 1: List of Raw Materials covered by this report
Total Parts
1
2
3
4
5
6
Raw Material Part Number
909-444
934-065
425672
497xxx-001
082xxx
692481
Raw Material Description
Ceramic Body
Cap/ Lead Assay – base and plating
Black Ink
Sn Plated Wire- Ni42Fe58MCuMSn
Ag Plated Cu-Element
Solder Wire
2
Page(s)
3-13
14-17
18-26
27-33
34-38
39-43
nov'
TESTREPORT
NO.:4002E11121307-2R02
page1of4
Oa!aiDec15,2o11
Customer:SuzhouFuHongElectrcnic
IndustfialCo,
Ltd.
Addrgs8:NO.89WElDUROAD,WANGTING
TOWN,
XTANGCHENG
D|STR|CT,
SUZHOU,
CHTNA
Reporton th6 3ubmittedssmplesaidio be
Samplename:Fusoscoppershell
llodol: /
Material:/
D$cription:/
Buyea:/
supplier:/
Sa|nplerecelveddate:Dec.13,2011
Tcatlngp€riod:FrcmDec.13,2011
to Dec.15,2011
T€tino Reau6ted
As specined
by client,to delermine
theL€ad,Cadmium,
Mercrry& Hexavatent
Chrcmium
contentin thesubmitted
samptein
accordancewilh Direclive2002/95/EC(RoHS).
Tcstindmethod:
Testing llem
[,leasudng
inslrument
MQL
Lead (Pb)
EC 62321:2008,seclion9
ICP-OES
2mglkg
cadmium(Cd)
(Hg)
Mercury
EC62321:2008,sectionI
ICP€ES
2 mg/kg
EC62321r
2008,section7
rcP-oEs
2 mg/kg
(Crl'I)
Chrom'um
EC62321:2008,
AnnexI
0.02mg,a(g'
lsg
-'0.02mg/kgreturs
10lheMQLofsample
extEction
tiquid.
99!s!.c!i9!j
-ffien tesiedas specifred
thesubmitted
sample
complied
withtherequircments
of commission
Decision
of 18Aug2005
amending
Directive
2002l95/EC
nolified
lnderdocument
2005/618/EC
ILS, PLEASEREFERTOTHE FOLLOWINGPAGE(S)'**'
',:,"il:::i"
ryf4
,3ffi::::1,,44
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lffH*"",",We-i
S}'EI{ZN€N AOV TGSTINGT€CHNOlOGY CO.,L'D.KUNSHAN EiANCH
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86-512-551
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6
TESTREPORT
NO.:4002E11121307-2R02
Add the digestionsolution;the
vesselis heatedLrntillhe sampl€
AddHrO,unlilthesampl€is clear
F;;1.-F;;,",..;-1.-
Cooling
thevessel,fllleriwashedand
filledto themarkwithdistilled
water.
{Melalsubslrat€)
Add lhe digestionsolution,clos€
The sampleis digestedin the
the macrowavevess€|.
micrcwave oven following a specific
program.
decomposilion
Coolingthe vessel,filter washedand
filled to the mark with distilled water.
Remove
thesample,
andcool
lhe beakerlo rcomtempefalure,
anddo1ie colorreaction
Heal50 mL ofDlwaterin lhe
beakertoboilingfor 10 min
Testthesamplesolution
andlhe 0.02
mg/kgstandard
solution
by UV-VIS.
To Detemine
(Praring)
andl\rercury
Content:
coor,ns.
nrr",
*""n"0 r"o
_____-l
""0 |
I
tothemark
withDtwater
I
,l o*o
-ill_.;*--;-l
I r*r.r*t
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TESTREPORT
NO.:
4002E11121
307-2R02
Date:Dec.15,2011
Page3 ol4
5. ToDetemineHexavalent
Chromium
Contentln
colorless
andcolored
ctlromate
coalingon metals: (Plating)
'' ',.'1
re$eoovr I r
s.t sw-resi (M&
lflhe lest resullis positive,
the sampleis considered
1o
havehexavalenlchromium
Boiling- waieF extraction
procedure
shallbe usedto
and the 0.02 mg/kg
lfthe€ isrnterference
orI rshardto decide*terhel
lhesamplehavethehexavalent
chrcmium
5 2 BoilingwEter-en€ction
Takethe (5015)cm'z
samplein thebeaker.
Heat50 mlof Olwaterin the
beaker
lo boilingfor 10min
Remove
he sample,
andcool
lhe beaker
1oroomtemperature,
anddo thecolorreaction
Testthe samplesolutionand the 0.02
mg/kgstandardsolutionby UV-VIS.
Srmple d93cription:
Coppershellsubslrate
Leadwle Platrng
Unil
24
CoppershellPlaling
RoHS
Limit
2-3
24"
Lead(Pb)
mg/Kg
1000
N.D.
2.5
40.0
N.D.
Cadmium
{Cd)
mg/kg
100
N,D.
N.D.
N.D.
N.D.
(Hs)
Msrorry
(Crvl)
Chromium
mg/kg
1000
N.D,
N.D,
N.D.
N.D.
mg/Kg
1000
Negative Negative Negalive
Negative
SH!NZHEN AOV TESTINGTCCTNOIqGY CO.,L}D,KUNSHAN BFANCH
n
Hotline
86'512^551
80 0 0
nov.
TESTREPORT
NO.rA002E11121307-2R02
Dat€iOec15,2011
-The new RoHSdi.ective2011/65/EU,
on Jul 21, 2011comeinto force,on Jan.03, 2013the fomat imotementation.
Dircctive
2002l95/ECshallbe reoealedsimultaneouslv.
Sp€cim€ns,wnicnrequestedto determineLead,Cadmiumand l4ercuryConlent,havebeendissotvedcomptetety.
-mg/kg=ppm
-N.D.=notdetected(<tVoL)
-MQL=l'rethodOuaniilationLimit
-Negalive=Abs€nce of Cr (VI);
Posilive=Prcs€nce
of Cr (VI)i
Uncedain=c€n noi ve fy whetherthe samplehaveHexavat€nt
Chrcmium by spoliesl.
(The tested s€mple should be furlher venfed by boiling-waterextradion
method if the spol test result is uncertainor
-'The test is basedon the followingassumption:Thesampteptatingis a singtetayerandeach pad is unifom. The test resutt
maybecannolslandior rhe physicartruthof sampleplating.
Photog.aphofSample
"'End of Repod"'
S'iE'!ZH€N AOVT€STING TECXNO!OGYCO..lIO,KUNSHAN ABANCH
Hh,:/fuloi6n
n
Hotline
86-512-551
80 0 0
Number : TWNC00256916
Test Report
Applicant:
Littelfuse Philippines Inc.
LIMA Technology Center, Lipa City,
Malvar, Batangas
Date
: May 16, 2012
Sample Description:
One (1) group of submitted samples said to be :
Part Description
: Ink
Part Number
: 425672
Date Sample Received
: May 10, 2012
Date Test Started
: May 10, 2012
Test Conducted :
As requested by the applicant, for details please refer to attached pages.
Authorized By:
On Behalf Of Intertek Testing Services
Taiwan Limited
K. Y. Liang
Director
This report shall not be reproduced
except in full, without the written
approval of the laboratory.
Page 1 of 9
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00256916
Test Conducted
(Ⅰ) Test Result Summary :
Test Item
Heavy Metal
Cadmium (Cd) content
Lead (Pb) content
Mercury (Hg) content
Chromium VI (Cr6+) content
Polybrominated Biphenyls (PBBs)
Monobrominated Biphenyls (MonoBB)
Dibrominated Biphenyls (DiBB)
Tribrominated Biphenyls (TriBB)
Tetrabrominated Biphenyls (TetraBB)
Pentabrominated Biphenyls (PentaBB)
Hexabrominated Biphenyls (HexaBB)
Heptabrominated Biphenyls (HeptaBB)
Octabrominated Biphenyls (OctaBB)
Nonabrominated Biphenyls (NonaBB)
Decabrominated Biphenyl (DecaBB)
Polybrominated Diphenyl Ethers (PBDEs)
Monobrominated Diphenyl Ethers (MonoBDE)
Dibrominated Diphenyl Ethers (DiBDE)
Tribrominated Diphenyl Ethers (TriBDE)
Tetrabrominated Diphenyl Ethers (TetraBDE)
Pentabrominated Diphenyl Ethers (PentaBDE)
Hexabrominated Diphenyl Ethers (HexaBDE)
Heptabrominated Diphenyl Ethers (HeptaBDE)
Octabrominated Diphenyl Ethers (OctaBDE)
Nonabrominated Diphenyl Ethers (NonaBDE)
Decabrominated Diphenyl Ether (DecaBDE)
Halogen Content
Fluorine (F)
Chlorine (Cl)
Bromine (Br)
Iodine (I)
Result (ppm)
Black Paste
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Page 2 of 9
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00256916
Test Conducted
(Ⅰ) Test Result Summary :
Test Item
Result (ppm)
Black Paste
Phthalates
Di(2-ethylhexyl) Phthalate (DEHP)
Dibutyl Phthalate (DBP)
Benzyl Butyl Phthalate (BBP)
Others
Hexabromocyclododecane (HBCDD)
ND
ND
ND
ND
Remarks: ppm = Parts per million based on wet weight of tested sample =
mg/kg
ND = Not detected
Responsibility of Chemist : Irene Chiou / Kevin Liu / Cathy Chen
Date Sample Received
Test Period
: May 10, 2012
: May 10, 2012 To May 16, 2012
(Ⅱ) RoHS Requirement:
Restricted Substances
Cadmium (Cd) Content
Lead (Pb) Content
Mercury (Hg) Content
Chromium VI (Cr6+) Content
Polybrominated Biphenyls (PBBs)
Polybrominated Diphenyl Ehters (PBDEs)
Limits
0.01% (100ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for
homogeneous material.
Page 3 of 9
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00256916
Test Conducted
(Ⅲ) Test Method:
Test Item
Test Method
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
Cadmium (Cd)
microwave digestion until the tested
content
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
Lead (Pb) content
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 7, by microwave
Mercury (Hg)
digestion until the tested samples are
content
totally dissolved and determined by
ICP-OES.
With reference to IEC 62321 edition
6+
Chromium VI (Cr ) 1.0:2008 in annex C, by alkaline
content
digestion and determined by UV-Vis
spectrophotometer.
With reference to IEC 62321 edition
1.0:2008 in annex A, by solvent
Polybrominated
extraction and determined by GC-MS and
Biphenyls (PBBs)
further HPLC-DAD confirmation when
necessary.
With reference to IEC 62321 edition
Polybrominated
1.0:2008 in annex A, by solvent
Diphenyl Ethers
extraction and determined by GC-MS and
(PBDEs)
further HPLC-DAD confirmation when
necessary.
With reference to EN 14582:2007 by
Halogen Content
calorimetric bomb with oxygen and
determined by Ion Chromatograph.
With reference to EN 14372: 2004, by
Phthalates
solvent extraction and determined by
GC-MS.
With reference to USEPA 3540C, by
Hexabromocyclodode
solvent extraction and determined by
cane (HBCDD)
GC-MSD.
Reporting Limit
2 ppm
2 ppm
2 ppm
1 ppm
5 ppm
5 ppm
50 ppm
10 ppm
10 ppm
Remark: Reporting limit = Quantitation limit of analyte in sample
Page 4 of 9
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00256916
Test Conducted
(Ⅳ) Measurement Flowchart:
Test for Cd/Pb/Hg/Chromium (VI)/PBBS/PBDES Contents
Reference Standard: IEC 62321 edition 1.0:2008
Sample preparation
For non-metal part
For metal part
Take sample and immerse into Aqua Regia, start to strip plating layer
Stop the stripping procedure upon color change completely
Take the Aqua solution as plating component and stripped body as substrate component
Cd/Pb/Hg
Cr
Weigh sample and
add organic solvent
By spot test
Negative
Confirm the tested
samples are
totally dissolved
Make up with
deionized water
PBBs/PBDEs
Polymers /
electronics
Metal
For different
material, digest
the sample with
*1
appropriate acid
6+
Get 50cm2 sample
By boiling water
extraction
*2
Weigh sample
and add
alkaline
solution
By Soxhlet
extraction or
Solvent extraction
Definite temp.
extraction
Cool and filter
the extract
Analyzed by ICP-OES
Concentrate the
extract and make up
with organic
solvent
Analyzed by GC-MSD
Make up with deionized
water and add diphenylcarbazide solution
Analyzed by UV-VIS
Remarks:
*1: List of Appropriate Acid：
Acid Added for Digestion
Material
Polymers
HNO3,HCl,HF,H2O2,H3BO3
Metals
HNO3,HCl,HF
Electronics
HNO3,HCl,H2O2,HBF4
*2: If the result of spot test is positive, Chromium VI would be determined as detected.
Page 5 of 9
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00256916
Test Conducted
(Ⅳ) Measurement Flowchart:
Test for Halogen Content
Reference Standard：EN 14582
Sampling/grinding or
cutting
Add absorbent in a
combustion flask &
place weighed sample in
equipment
Fill oxygen into
calorimetric bomb
Ignite then leave the
bomb at room
temperature
Transfer the absorbent
into a volumetric flask
Make up with deionized
water
Analyzed by ion
chromatography
Page 6 of 9
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00256916
Test Conducted
(Ⅳ) Measurement Flowchart:
Test For Phthalates Contents
Reference Method: EN 14372: 2004
Sampling/grinding or
cutting
Weigh sample and add
organic solvent
By solvent extraction
Concentrate the extract
and make up with
organic solvent
Analyzed by GC-MSD
Page 7 of 9
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00256916
Test Conducted
(Ⅳ) Measurement Flowchart:
Test For Hexabromocyclododecane (HBCDD)
Reference Standard：USEPA 3540C
Sampling/grinding or cutting
Weigh sample and add organic
solvent
By soxhlet extraction
Concentrate the extract and
make up with organic solvent
Analyzed by GC-MSD
End of Report
Page 8 of 9
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00256916
Test Conducted
Photo
Page 9 of 9
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Validi
nown
ForQues
P|easeU
TestReport
No.: CE/2011i84956
l
Th€followingsampl€(s)was/w6resubmitt€d and identified by/on b€halfofthe client as:
SampleDescdption
Buyer/Order
No.
SampleReceiving
Date
TesiingPeriod
Ni42Fe5SMCuMSn
'10-1185
2011t11t25
2011| 11n5 10 2011t12tol
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Dale:2O11|1ZO1
POLYFIL
AG
OBERALLMENDSTMSSE
2OA.CH$3OO
ZUG/ SWITZERLAND
L l Il?
1iI' ItrlII'l+46lo?)'ee
ithscs
[t[[l[ttl]l
Test Report
No.: CE/201
1/84956
Dale:2011t1201
Page:2 of 7
POLYFIL
AG
OBEMLLMENDSTMSSE
2OA,CH63OO
ZUG/ SWITZERLAND
ll]ttutflflttl
T€at Resultls)
PARTl.lAMENo.1
T6st ltem(s)
uaomrum(qd)
Lead (Pb)
Mercury
(Hg)
Hexavalent
Chrornium
Cr(Vl)
Sum ot PBBS
Monobromobiphenyl
Dibromobrphenyl
Triblomobiphenyl
Tetrabromobiphenyl
Pentabromobiphenyl
Hexabromobiphenyl
Heptabromobiphenyl
Octabromobiphenyl
Nonabromobiphenyl
Decabromobiphenyl
Sumof PBOEa
Monobromodiphenyl
ether
Dibromodiphonyl
ether
Tribromodiphenyl
ether
Tetrabromodiphenyl
ether
Pentabromodiphenyl
ether
Hexabromodiphenyl
ether
Heptabromodiphenyl
ether
SILVERCOLORED
IJETALWIRE(NCLUDING
THEPLATING
LAYER)
Unit
Method
IIIDL
mg/Kg Withreference
to tEC62321:zl08 and-
Result
No.l
pedonned
by ICP-AES.
mgikS Withreference
to tEC62321:2008€nd
perfomedby ICP-AES_
2
n.o.
2
62
mg/kg With referenc€to IEC 62321: 2008 and
performedby ICP-AES.
2
n.d.
Wilhreference
to IEC62321:2008and
performedby Boilingwaterextrection
Method.#
Negative
5
5
5
5
With referenceto IEC62321: 2008and
mg/Kg p€rformed
by GC/[,S.
5
5
n.o,
n.d.
n,d,
n.d.
n.d.
n.d.
n.d.
n.dn.d.
n.d.
n.o.
n.d.
5
5
5
n,o,
5
n.d.
5
5
5
n.d.
n.d.
Octabromodiphenyl
elher
5
NonabromodiDhenvl
ether
Decabromodiphenyl
ether
n.d.
5
n.d.
n.d.
5
cffip.dy hr | 1 lr'rf;ri
r,1'riiilt,itJ.r
rt,..t]i
*1{J1i
Tb€doons'csFbysecdnPanysuqedbcoseE|cdndloi3olsefuepinbdovsdeat6V6ibdeo.€q
iidbol€p.du€dercplmigl.wbou
Lfi!-*. rir i: rk!, i,,t + s6 t0r)rre
n.d.
n.d.
n.d.
Test Report
No. : CE/2011/84956
Page: 3 of 7
Ode :2O114ZO1
POLYFILAG
OBEMLLMENDSTRASSE2OA,CH€3OOZUG / SWITZERLAND
Tost ltem(s)
Halogen
Halogen-Fluorine
(F)
(CASNo.r14762-94-8)
Halogen-Chlorine
(Cl)
(CASNo.:22537-15-1)
Halogen-Bromine
(Bt
(CASNo.:10097-32-2)
Unit
[[||||l|||m|lrll]l
Method
MDL
With referenceto BS EN 14582..2007.
mg/Kg
Analysis
wasperfomedby lC.
Halogenlodine
(l)
(CASNo.:14362-44-8)
Result
No.1
50
n.d.
50
n.d.
50
n.d.
50
n.d.
Note :
1. mg/kg= ppm; 0.1M%= lOOOppm
2. n.d. = Not Detected
3. MDL= MethodDetection
Limit
4."-"=NotRegulated
5. " = Qualitative
(NoUnit)
analysas
=
6. # a. Positivemeansthe presenceof CA/l on the testedareas
b. Negativemeansthe absenceof CrVlon the testedareas
Thedetected
concentration
in boiling-water-€xt€ction
sorrition
is equaror greaterthan
o.02mg/kgwith50cm,
testedareas,
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on beharfof theappric€nt
as mixingsamprein onetesting.Theaboveresurt(s)
wEsl^/ere
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Test Report
No. : CE/201'1/84956
Page: 4 of 7
Da1e| 2O1112JO1
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dissolved
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methodaccorcling
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by suitable
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dependedon diferent samole
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throughfilter
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for
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No.: CE/2011/84956
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No.: CE/2011/84956
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Test Report
Applicant:
Number : TWNC00249179
Littelfuse Philippines Inc.
LIMA Technology Center, Lipa City,
Malvar, Batangas
Date
: Mar 28, 2012
Sample Description:
One (1) group of submitted samples said to be :
Part Description
: Silver plated Wire
Part Number
: DRAGxxx
Date Sample Received
: Mar 22, 2012
Date Test Started
: Mar 22, 2012
Test Conducted :
As requested by the applicant, for details please refer to attached pages.
Authorized By:
On Behalf Of Intertek Testing Services
Taiwan Limited
K. Y. Liang
Director
This report shall not be reproduced
except in full, without the written
approval of the laboratory.
Page 1 of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00249179
Test Conducted
(Ⅰ) Test Result Summary :
Test Item
Heavy Metal
Cadmium (Cd) content
Lead (Pb) content
Mercury (Hg) content
Chromium VI (Cr6+) content (mg/kg with 50cm2)
Result (ppm)
Submitted Samples
ND
ND
ND
Negative (< 0.02)
Remarks: ppm = Parts per million based on weight of tested sample = mg/kg
ND = Not detected
<
= Less than
mg/kg with 50cm2 = milligram per kilogram with 50 square centimetre
Negative = A negative test result indicated positive observation
was not found at the time of Test.
Responsibility of Chemist : Irene Chiou / Kevin Liu / Cathy Chen
Date Sample Received
Test Period
: Mar 22, 2012
: Mar 22, 2012 To Mar 27, 2012
(Ⅱ) RoHS Requirement:
Restricted Substances
Cadmium (Cd) Content
Lead (Pb) Content
Mercury (Hg) Content
Chromium VI (Cr6+) Content
Limits
0.01% (100ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for
homogeneous material.
Page 2 of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00249179
Test Conducted
(Ⅲ) Test Method:
Test Item
Cadmium (Cd)
content
Lead (Pb) content
Mercury (Hg)
content
Chromium VI (Cr6+)
content
Test Method
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 7, by microwave
digestion until the tested samples are
totally dissolved and determined by
ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in annex B, by boiling water
extraction and determined by UV-Vis
Spectrophotometer.
Reporting Limit
2 ppm
2 ppm
2 ppm
0.02
mg/kg with 50cm2
Remark: Reporting limit = Quantitation limit of analyte in sample
Page 3 of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00249179
Test Conducted
(Ⅳ) Measurement Flowchart:
Test For Cd/Pb/Hg/Chromium (VI)
Reference Standard：IEC 62321 edition 1.0:2008
Sampling/grinding or cutting
Cd/Pb/Hg
Cr
Polymers /
Electronics
Metal
For different
material, digest
the sample with
*1
appropriate acid
By spot test
Negative
Confirm the tested
samples are
totally dissolved
Make up with
deionized water
6+
*2
Weigh sample
and add
alkaline
solution
Get 50cm2 sample
Definite temp.
extraction
Boiling water
extraction
Cool and filter
the extract
Analyzed by ICP-OES
Make up with deionized
water and add diphenylcarbazide solution
Analyzed by UV-VIS
Remarks:
*1: List Of Appropriate Acid：
Material
Polymers
Metals
Electronics
Acid Added For Digestion
HNO3,HCl,HF,H2O2,H3BO3
HNO3,HCl,HF
HNO3,HCl,H2O2,HBF4
*2: If the result of spot test is positive, Chromium VI would be determined as detected.
End of Report
Page 4 of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00249179
Test Conducted
Photo
Page 5 of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Test Report
Applicant:
Number : TWNC00235575
Littelfuse Philippines Inc.
LIMA Technology Center, Lipa City,
Malvar, Batangas
Date
: Dec 08, 2011
Sample Description:
One (1) group of submitted samples said to be :
Part Description
: Solder
Part Number
: 692481
Date Sample Received
: Dec 05, 2011
Date Test Started
: Dec 05, 2011
Test Conducted :
As requested by the applicant, for details please refer to attached pages.
Authorized By:
On Behalf Of Intertek Testing Services
Taiwan Limited
K. Y. Liang
Director
This report shall not be reproduced
except in full, without the written
approval of the laboratory.
Page 1 of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00235575
Test Conducted
(Ⅰ) Test Result Summary :
Test Item
Heavy Metal
Cadmium (Cd) content
Lead (Pb) content
Mercury (Hg) content
Chromium VI (Cr6+) content (mg/kg with 50cm2)
Result (ppm)
Silvery Metal
ND
200
ND
Negative (< 0.02)
Remarks: ppm = Parts per million based on weight of tested sample = mg/kg
ND = Not detected
<
= Less than
mg/kg with 50cm2 = milligram per kilogram with 50 square centimetre
Negative = A negative test result indicated positive observation
was not found at the time of Test.
Responsibility of Chemist : Irene Chiou / Kevin Liu
Date Sample Received
Test Period
: Dec 05, 2011
: Dec 05, 2011 To Dec 08, 2011
(Ⅱ) RoHS Requirement:
Restricted Substances
Cadmium (Cd) Content
Lead (Pb) Content
Mercury (Hg) Content
Chromium VI (Cr6+) Content
Limits
0.01% (100ppm)
0.1% (1000ppm)
0.1% (1000ppm)
0.1% (1000ppm)
The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for
homogeneous material.
Page 2 of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00235575
Test Conducted
(Ⅲ) Test Method:
Test Item
Cadmium (Cd)
content
Lead (Pb) content
Mercury (Hg)
content
Chromium VI (Cr6+)
content
Test Method
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 8/9/10, by
microwave digestion until the tested
samples are totally dissolved and
determined by ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in clause 7, by microwave
digestion until the tested samples are
totally dissolved and determined by
ICP-OES.
With reference to IEC 62321 edition
1.0:2008 in annex B, by boiling water
extraction and determined by UV-Vis
spectrophotometer.
Reporting Limit
2 ppm
2 ppm
2 ppm
0.02
mg/kg with 50cm2
Remark: Reporting limit = Quantitation limit of analyte in sample
Page 3 of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00235575
Test Conducted
(Ⅳ) Measurement Flowchart:
Test for Cd/Pb/Hg/Chromium (VI)
Reference Standard：IEC 62321 edition 1.0:2008
Sample preparation
Take sample and immerse into Aqua Regia, start to strip plating layer
Stop the stripping procedure upon color change completely
Take the Aqua solution as plating component and stripped body as substrate component
Cd/Pb/Hg
Cr
Polymers /
electronics
Metal
For different
material, digest
the sample with
*1
appropriate acid
By spot test
Negative
Confirm the tested
samples are
totally dissolved
Make up with
deionized water
6+
*2
Weigh sample
and add
alkaline
solution
Get 50cm2 sample
Definite temp.
extraction
By boiling water
extraction
Cool and filter
the extract
Analyzed by ICP-OES
Make up with deionized water and add
diphenyl-carbazide solution
Remarks:
*1: List of Appropriate Acid：
Material
Polymers
Metals
Electronics
Analyzed by UV-VIS
Acid Added for Digestion
HNO3,HCl,HF,H2O2,H3BO3
HNO3,HCl,HF
HNO3,HCl,H2O2,HBF4
*2: If the result of spot test is positive, Chromium VI would be determined as detected.
End of Report
Page 4 of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Number : TWNC00235575
Test Conducted
Photo
Page 5 of 5
Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司
114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401