ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: NANO Fuse Product #: 462 SERIES Issue Date: May 7, 2012 It is hereby certified by Littelfuse, Inc. that there is neither RoHS (EU Directive 2002/95/EC)-restricted substance nor such use, for materials to be used for unit parts, for packing/packaging materials, and for additives and the like in the manufacturing processes. In addition, it is hereby reported to you that the parts and sub-materials, the materials to be used for unit parts, the packing/packaging materials, and the additives and the like in the manufacturing processes, are all composed of the following components. Issued by: <Global EHS Engineer> (1) Parts, sub-materials and unit parts This document covers the 462--Nano RoHS-Compliant series products manufactured by Littelfuse, Inc. < Raw Materials Used Please see Table 1 (2) The ICP data on all measurable substances Please see appropriate pages as identifed in Table 1 Remarks: 1 Table 1: List of Raw Materials covered by this report Total Parts 1 2 3 4 5 6 Form 585-047 Rev. A Raw Material Part Number 910-280 909-438 901-311 901-310 DRFE-001,2,3,5 (497303-001) DRAG (082719-001) 2 Raw Material Description Cap Plastic Tube Silicon Square Profile Silicon Round Profile Wire-Sn Plated NiFeMCu Wire-Sn Plated AgCu Page(s) 3-7 8-18 19-27 28-36 37-43 44-48 2/21/06 Test Report Applicant: Number : TWNC00233551 Littelfuse Philippines Inc. LIMA Technology Center, Lipa City, Malvar, Batangas Date : Nov 28, 2011 Sample Description: One (1) group of submitted samples said to be : Part Description : Cap Part Number : 910-280 Date Sample Received : Nov 21, 2011 Date Test Started : Nov 23, 2011 Test Conducted : As requested by the applicant, for details please refer to attached pages. Authorized By: On Behalf Of Intertek Testing Services Taiwan Limited K. Y. Liang Director This report shall not be reproduced except in full, without the written approval of the laboratory. Page 1 of 5 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401 Number : TWNC00233551 Test Conducted (Ⅰ) Test Result Summary : Test Item Heavy Metal Cadmium (Cd) content Lead (Pb) content Mercury (Hg) content Chromium VI (Cr6+) content (mg/kg with 50cm2) Result (ppm) (1) (2) 8 15 ND Negative (< 0.02) ND 195 ND Negative (< 0.02) Remarks: ppm = Parts per million based on weight of tested sample = mg/kg ND = Not detected < = Less than mg/kg with 50cm2 = milligram per kilogram with 50 square centimetre Negative = A negative test result indicated positive observation was not found at the time of Test. Tested Components (1) Coppery Metal Base Material (2) Silvery Plating Layer Responsibility of Chemist : Irene Chiou / Kevin Liu Date Sample Received Test Period : Nov 21, 2011 : Nov 23, 2011 To Nov 25, 2011 (Ⅱ) RoHS Requirement: Restricted Substances Cadmium (Cd) Content Lead (Pb) Content Mercury (Hg) Content Chromium VI (Cr6+) Content Limits 0.01% (100ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for homogeneous material. Page 2 of 5 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401 Number : TWNC00233551 Test Conducted (Ⅲ) Test Method: Test Item Cadmium (Cd) content Lead (Pb) content Mercury (Hg) content Chromium VI (Cr6+) content Test Method With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in clause 7, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in annex B, by boiling water extraction and determined by UV-Vis spectrophotometer. Reporting Limit 2 ppm 2 ppm 2 ppm 0.02 mg/kg with 50cm2 Remark: Reporting limit = Quantitation limit of analyte in sample Page 3 of 5 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401 Number : TWNC00233551 Test Conducted (Ⅳ) Measurement Flowchart: Test for Cd/Pb/Hg/Chromium (VI) Reference Standard:IEC 62321 edition 1.0:2008 Sample preparation Take sample and immerse into Aqua Regia, start to strip plating layer Stop the stripping procedure upon color change completely Take the Aqua solution as plating component and stripped body as substrate component Cd/Pb/Hg Cr Polymers / electronics Metal For different material, digest the sample with *1 appropriate acid By spot test Negative Confirm the tested samples are totally dissolved Make up with deionized water 6+ *2 Weigh sample and add alkaline solution Get 50cm2 sample Definite temp. extraction By boiling water extraction Cool and filter the extract Analyzed by ICP-OES Make up with deionized water and add diphenyl-carbazide solution Remarks: *1: List of Appropriate Acid: Material Polymers Metals Electronics Analyzed by UV-VIS Acid Added for Digestion HNO3,HCl,HF,H2O2,H3BO3 HNO3,HCl,HF HNO3,HCl,H2O2,HBF4 *2: If the result of spot test is positive, Chromium VI would be determined as detected. End of Report Page 4 of 5 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401 Number : TWNC00233551 Test Conducted Photo Page 5 of 5 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401 Number : TWNC00233531 Test Report Applicant: Littelfuse Philippines Inc. LIMA Technology Center, Lipa City, Malvar, Batangas Date : Nov 25, 2011 Sample Description: One (1) group of submitted samples said to be : Part Description : Silicon Round Part Number : 910-311 Date Sample Received : Nov 21, 2011 Date Test Started : Nov 22, 2011 Test Conducted : As requested by the applicant, for details please refer to attached pages. Authorized By: On Behalf Of Intertek Testing Services Taiwan Limited K. Y. Liang Director This report shall not be reproduced except in full, without the written approval of the laboratory. Page 1 of 9 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401 Number : TWNC00233531 Test Conducted (Ⅰ) Test Result Summary : Test Item Result (ppm) Brown Material Heavy Metal Cadmium (Cd) content Lead (Pb) content Mercury (Hg) content Chromium VI (Cr6+) content Polybrominated Biphenyls (PBBs) Monobrominated Biphenyls (MonoBB) Dibrominated Biphenyls (DiBB) Tribrominated Biphenyls (TriBB) Tetrabrominated Biphenyls (TetraBB) Pentabrominated Biphenyls (PentaBB) Hexabrominated Biphenyls (HexaBB) Heptabrominated Biphenyls (HeptaBB) Octabrominated Biphenyls (OctaBB) Nonabrominated Biphenyls (NonaBB) Decabrominated Biphenyl (DecaBB) Polybrominated Diphenyl Ethers (PBDEs) Monobrominated Diphenyl Ethers (MonoBDE) Dibrominated Diphenyl Ethers (DiBDE) Tribrominated Diphenyl Ethers (TriBDE) Tetrabrominated Diphenyl Ethers (TetraBDE) Pentabrominated Diphenyl Ethers (PentaBDE) Hexabrominated Diphenyl Ethers (HexaBDE) Heptabrominated Diphenyl Ethers (HeptaBDE) Octabrominated Diphenyl Ethers (OctaBDE) Nonabrominated Diphenyl Ethers (NonaBDE) Decabrominated Diphenyl Ether (DecaBDE) Halogen Content Fluorine (F) Chlorine (Cl) Bromine (Br) Iodine (I) Phthalates Di(2-ethylhexyl) Phthalate (DEHP) Dibutyl Phthalate (DBP) Benzyl Butyl Phthalate (BBP) Others Hexabromocyclododecane (HBCDD) ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 209 ND ND ND ND ND ND Remarks: ppm = Parts per million based on weight of tested sample = mg/kg ND = Not detected Responsibility of Chemist : Irene Chiou / Kevin Liu / Cathy Chen Date Sample Received Test Period : Nov 21, 2011 : Nov 22, 2011 To Nov 24, 2011 Page 2 of 9 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401 Number : TWNC00233531 Test Conducted (Ⅱ) RoHS Requirement: Restricted Substances Cadmium (Cd) Content Lead (Pb) Content Mercury (Hg) Content Chromium VI (Cr6+) Content Polybrominated Biphenyls (PBBs) Polybrominated Diphenyl Ehters (PBDEs) Limits 0.01% (100ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for homogeneous material. (Ⅲ) Test Method: Test Item Test Method With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by Cadmium (Cd) content microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by Lead (Pb) content microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in clause 7, by microwave Mercury (Hg) content digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition Chromium VI (Cr6+) 1.0:2008 in annex C, by alkaline content digestion and determined by UV-Vis spectrophotometer. With reference to IEC 62321 edition 1.0:2008 in annex A, by solvent Polybrominated extraction and determined by GC-MSD Biphenyls (PBBs) and further HPLC confirmation when necessary. Reporting Limit 2 ppm 2 ppm 2 ppm 1 ppm 5 ppm Page 3 of 9 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401 Number : TWNC00233531 Test Conducted (Ⅲ) Test Method: Test Item Test Method With reference to IEC 62321 edition 1.0:2008 in annex A, by solvent Polybrominated Diphenyl Ethers extraction and determined by GC-MSD (PBDEs) and further HPLC confirmation when necessary. With reference to EN 14582:2007 by Halogen Content calorimetric bomb with oxygen and determined by ion chromatography With reference to EN 14372: 2004, by Phthalates solvent extraction and determined by GC-MSD With reference to USEPA 3540C, by Hexabromocyclododecane solvent extraction and determined by (HBCDD) GC-MSD Reporting Limit 5 ppm 50 ppm 50 ppm 10 ppm Remark: Reporting limit = Quantitation limit of analyte in sample Page 4 of 9 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401 Number : TWNC00233531 Test Conducted (Ⅳ) Measurement Flowchart: Test for Cd/Pb/Hg/Chromium (VI)/PBBS/PBDES Contents Reference Standard: IEC 62321 edition 1.0:2008 Sample preparation For non-metal part For metal part Take sample and immerse into Aqua Regia, start to strip plating layer Stop the stripping procedure upon color change completely Take the Aqua solution as plating component and stripped body as substrate component Cd/Pb/Hg Cr Confirm the tested samples are totally dissolved Make up with deionized water PBBs/PBDEs Polymers / electronics Metal For different material, digest the sample with *1 appropriate acid 6+ Weigh sample and add organic solvent By spot test Negative Get 50cm2 sample By boiling water extraction *2 Weigh sample and add alkaline solution By Soxhlet extraction or Solvent extraction Definite temp. extraction Cool and filter the extract Analyzed by ICP-OES Concentrate the extract and make up with organic solvent Analyzed by GC-MSD Make up with deionized water and add diphenylcarbazide solution Analyzed by UV-VIS Remarks: *1: List of Appropriate Acid: Material Polymers Metals Electronics Acid Added for Digestion HNO3,HCl,HF,H2O2,H3BO3 HNO3,HCl,HF HNO3,HCl,H2O2,HBF4 *2: If the result of spot test is positive, Chromium VI would be determined as detected. Page 5 of 9 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401 Number : TWNC00233531 Test Conducted (Ⅳ) Measurement Flowchart: Test for Halogen Content Reference Standard:EN 14582 Sampling/grinding or cutting Add absorbent in a combustion flask & place weighed sample in equipment Fill oxygen into calorimetric bomb Ignite then leave the flask at room temperature Transfer the absorbent into a volumetric flask Make up with deionized water Analyzed by ion chromatography Page 6 of 9 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401 Number : TWNC00233531 Test Conducted (Ⅳ) Measurement Flowchart: Test For Phthalates Contents Reference Method: EN 14372: 2004 Sampling/grinding or cutting Weigh sample and add organic solvent By solvent extraction Concentrate the extract and make up with organic solvent Analyzed by GC-MSD Page 7 of 9 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401 Number : TWNC00233531 Test Conducted (Ⅳ) Measurement Flowchart: Test For Hexabromocyclododecane (HBCDD) Reference Standard:USEPA 3540C Sampling/grinding or cutting Weigh sample and add organic solvent By soxhlet extraction Concentrate the extract and make up with organic solvent Analyzed by GC-MSD End of Report Page 8 of 9 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401 Number : TWNC00233531 Test Conducted Photo Page 9 of 9 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401 Number : TWNC00233532 Test Report Applicant: Littelfuse Philippines Inc. LIMA Technology Center, Lipa City, Malvar, Batangas Date : Nov 25, 2011 Sample Description: One (1) group of submitted samples said to be : Part Description : Silicon Square Part Number : 910-310 Date Sample Received : Nov 21, 2011 Date Test Started : Nov 22, 2011 Test Conducted : As requested by the applicant, for details please refer to attached pages. Authorized By: On Behalf Of Intertek Testing Services Taiwan Limited K. Y. Liang Director This report shall not be reproduced except in full, without the written approval of the laboratory. Page 1 of 9 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401 Number : TWNC00233532 Test Conducted (Ⅰ) Test Result Summary : Test Item Result (ppm) Brown Material Heavy Metal Cadmium (Cd) content Lead (Pb) content Mercury (Hg) content Chromium VI (Cr6+) content Polybrominated Biphenyls (PBBs) Monobrominated Biphenyls (MonoBB) Dibrominated Biphenyls (DiBB) Tribrominated Biphenyls (TriBB) Tetrabrominated Biphenyls (TetraBB) Pentabrominated Biphenyls (PentaBB) Hexabrominated Biphenyls (HexaBB) Heptabrominated Biphenyls (HeptaBB) Octabrominated Biphenyls (OctaBB) Nonabrominated Biphenyls (NonaBB) Decabrominated Biphenyl (DecaBB) Polybrominated Diphenyl Ethers (PBDEs) Monobrominated Diphenyl Ethers (MonoBDE) Dibrominated Diphenyl Ethers (DiBDE) Tribrominated Diphenyl Ethers (TriBDE) Tetrabrominated Diphenyl Ethers (TetraBDE) Pentabrominated Diphenyl Ethers (PentaBDE) Hexabrominated Diphenyl Ethers (HexaBDE) Heptabrominated Diphenyl Ethers (HeptaBDE) Octabrominated Diphenyl Ethers (OctaBDE) Nonabrominated Diphenyl Ethers (NonaBDE) Decabrominated Diphenyl Ether (DecaBDE) Halogen Content Fluorine (F) Chlorine (Cl) Bromine (Br) Iodine (I) Phthalates Di(2-ethylhexyl) Phthalate (DEHP) Dibutyl Phthalate (DBP) Benzyl Butyl Phthalate (BBP) Others Hexabromocyclododecane (HBCDD) ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 385 ND ND ND ND ND ND Remarks: ppm = Parts per million based on weight of tested sample = mg/kg ND = Not detected Responsibility of Chemist : Irene Chiou / Kevin Liu / Cathy Chen Date Sample Received Test Period : Nov 21, 2011 : Nov 22, 2011 To Nov 24, 2011 Page 2 of 9 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401 Number : TWNC00233532 Test Conducted (Ⅱ) RoHS Requirement: Restricted Substances Cadmium (Cd) Content Lead (Pb) Content Mercury (Hg) Content Chromium VI (Cr6+) Content Polybrominated Biphenyls (PBBs) Polybrominated Diphenyl Ehters (PBDEs) Limits 0.01% (100ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for homogeneous material. (Ⅲ) Test Method: Test Item Test Method With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by Cadmium (Cd) content microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by Lead (Pb) content microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in clause 7, by microwave Mercury (Hg) content digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition Chromium VI (Cr6+) 1.0:2008 in annex C, by alkaline content digestion and determined by UV-Vis spectrophotometer. With reference to IEC 62321 edition 1.0:2008 in annex A, by solvent Polybrominated extraction and determined by GC-MSD Biphenyls (PBBs) and further HPLC confirmation when necessary. Reporting Limit 2 ppm 2 ppm 2 ppm 1 ppm 5 ppm Page 3 of 9 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401 Number : TWNC00233532 Test Conducted (Ⅲ) Test Method: Test Item Test Method With reference to IEC 62321 edition 1.0:2008 in annex A, by solvent Polybrominated Diphenyl Ethers extraction and determined by GC-MSD (PBDEs) and further HPLC confirmation when necessary. With reference to EN 14582:2007 by Halogen Content calorimetric bomb with oxygen and determined by ion chromatography With reference to EN 14372: 2004, by Phthalates solvent extraction and determined by GC-MSD With reference to USEPA 3540C, by Hexabromocyclododecane solvent extraction and determined by (HBCDD) GC-MSD Reporting Limit 5 ppm 50 ppm 50 ppm 10 ppm Remark: Reporting limit = Quantitation limit of analyte in sample Page 4 of 9 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401 Number : TWNC00233532 Test Conducted (Ⅳ) Measurement Flowchart: Test for Cd/Pb/Hg/Chromium (VI)/PBBS/PBDES Contents Reference Standard: IEC 62321 edition 1.0:2008 Sample preparation For non-metal part For metal part Take sample and immerse into Aqua Regia, start to strip plating layer Stop the stripping procedure upon color change completely Take the Aqua solution as plating component and stripped body as substrate component Cd/Pb/Hg Cr Confirm the tested samples are totally dissolved Make up with deionized water PBBs/PBDEs Polymers / electronics Metal For different material, digest the sample with *1 appropriate acid 6+ Weigh sample and add organic solvent By spot test Negative Get 50cm2 sample By boiling water extraction *2 Weigh sample and add alkaline solution By Soxhlet extraction or Solvent extraction Definite temp. extraction Cool and filter the extract Analyzed by ICP-OES Concentrate the extract and make up with organic solvent Analyzed by GC-MSD Make up with deionized water and add diphenylcarbazide solution Analyzed by UV-VIS Remarks: *1: List of Appropriate Acid: Material Polymers Metals Electronics Acid Added for Digestion HNO3,HCl,HF,H2O2,H3BO3 HNO3,HCl,HF HNO3,HCl,H2O2,HBF4 *2: If the result of spot test is positive, Chromium VI would be determined as detected. Page 5 of 9 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401 Number : TWNC00233532 Test Conducted (Ⅳ) Measurement Flowchart: Test for Halogen Content Reference Standard:EN 14582 Sampling/grinding or cutting Add absorbent in a combustion flask & place weighed sample in equipment Fill oxygen into calorimetric bomb Ignite then leave the flask at room temperature Transfer the absorbent into a volumetric flask Make up with deionized water Analyzed by ion chromatography Page 6 of 9 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401 Number : TWNC00233532 Test Conducted (Ⅳ) Measurement Flowchart: Test For Phthalates Contents Reference Method: EN 14372: 2004 Sampling/grinding or cutting Weigh sample and add organic solvent By solvent extraction Concentrate the extract and make up with organic solvent Analyzed by GC-MSD Page 7 of 9 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401 Number : TWNC00233532 Test Conducted (Ⅳ) Measurement Flowchart: Test For Hexabromocyclododecane (HBCDD) Reference Standard:USEPA 3540C Sampling/grinding or cutting Weigh sample and add organic solvent By soxhlet extraction Concentrate the extract and make up with organic solvent Analyzed by GC-MSD End of Report Page 8 of 9 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401 Number : TWNC00233532 Test Conducted Photo Page 9 of 9 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401 Validi nown ForQues P|easeU TestReport No.: CE/2011i84956 l Th€followingsampl€(s)was/w6resubmitt€d and identified by/on b€halfofthe client as: SampleDescdption Buyer/Order No. SampleReceiving Date TesiingPeriod Ni42Fe5SMCuMSn '10-1185 2011t11t25 2011| 11n5 10 2011t12tol Pleasereferto nextpage(s). T€atR€ault(s) Efn d fe.rd Ct rdcJ L.bor.tory- rupd r,rllj"ili!nrl.i f i lR 11{.11 cdoaiy 1l r1irr!.f-li ii,"iJ"1.!'ji!*';Jul;"c".p"nysgb]edbbcsi*dcdndi6i3ds aao conoro* o aa so,eit o i"-" iii.aonc ro*a ai'-s. ,a*i.in*r -,t e"sa* rec)rosbdft€G{ctod€ndber I!l 4n'!rtn,{ **"; "r'i, i ' r iisft . o m*o . u "o,,"-. l i ' t o c " '**,,h" " . " t , d " *B d a ' ' y T i . " c " ' p . r y 3 $ b 6 i" o te o^cn reeri o' a "r*r Page:'1of7 Dale:2O11|1ZO1 POLYFIL AG OBERALLMENDSTMSSE 2OA.CH$3OO ZUG/ SWITZERLAND L l Il? 1iI' ItrlII'l+46lo?)'ee ithscs [t[[l[ttl]l Test Report No.: CE/201 1/84956 Dale:2011t1201 Page:2 of 7 POLYFIL AG OBEMLLMENDSTMSSE 2OA,CH63OO ZUG/ SWITZERLAND ll]ttutflflttl T€at Resultls) PARTl.lAMENo.1 T6st ltem(s) uaomrum(qd) Lead (Pb) Mercury (Hg) Hexavalent Chrornium Cr(Vl) Sum ot PBBS Monobromobiphenyl Dibromobrphenyl Triblomobiphenyl Tetrabromobiphenyl Pentabromobiphenyl Hexabromobiphenyl Heptabromobiphenyl Octabromobiphenyl Nonabromobiphenyl Decabromobiphenyl Sumof PBOEa Monobromodiphenyl ether Dibromodiphonyl ether Tribromodiphenyl ether Tetrabromodiphenyl ether Pentabromodiphenyl ether Hexabromodiphenyl ether Heptabromodiphenyl ether SILVERCOLORED IJETALWIRE(NCLUDING THEPLATING LAYER) Unit Method IIIDL mg/Kg Withreference to tEC62321:zl08 and- Result No.l pedonned by ICP-AES. mgikS Withreference to tEC62321:2008€nd perfomedby ICP-AES_ 2 n.o. 2 62 mg/kg With referenc€to IEC 62321: 2008 and performedby ICP-AES. 2 n.d. Wilhreference to IEC62321:2008and performedby Boilingwaterextrection Method.# Negative 5 5 5 5 With referenceto IEC62321: 2008and mg/Kg p€rformed by GC/[,S. 5 5 n.o, n.d. n,d, n.d. n.d. n.d. n.d. n.dn.d. n.d. n.o. n.d. 5 5 5 n,o, 5 n.d. 5 5 5 n.d. n.d. Octabromodiphenyl elher 5 NonabromodiDhenvl ether Decabromodiphenyl ether n.d. 5 n.d. n.d. 5 cffip.dy hr | 1 lr'rf;ri r,1'riiilt,itJ.r rt,..t]i *1{J1i Tb€doons'csFbysecdnPanysuqedbcoseE|cdndloi3olsefuepinbdovsdeat6V6ibdeo.€q iidbol€p.du€dercplmigl.wbou Lfi!-*. rir i: rk!, i,,t + s6 t0r)rre n.d. n.d. n.d. Test Report No. : CE/2011/84956 Page: 3 of 7 Ode :2O114ZO1 POLYFILAG OBEMLLMENDSTRASSE2OA,CH€3OOZUG / SWITZERLAND Tost ltem(s) Halogen Halogen-Fluorine (F) (CASNo.r14762-94-8) Halogen-Chlorine (Cl) (CASNo.:22537-15-1) Halogen-Bromine (Bt (CASNo.:10097-32-2) Unit [[||||l|||m|lrll]l Method MDL With referenceto BS EN 14582..2007. mg/Kg Analysis wasperfomedby lC. Halogenlodine (l) (CASNo.:14362-44-8) Result No.1 50 n.d. 50 n.d. 50 n.d. 50 n.d. Note : 1. mg/kg= ppm; 0.1M%= lOOOppm 2. n.d. = Not Detected 3. MDL= MethodDetection Limit 4."-"=NotRegulated 5. " = Qualitative (NoUnit) analysas = 6. # a. Positivemeansthe presenceof CA/l on the testedareas b. Negativemeansthe absenceof CrVlon the testedareas Thedetected concentration in boiling-water-€xt€ction sorrition is equaror greaterthan o.02mg/kgwith50cm, testedareas, T Thesample(s) was^rcreanaryzed on beharfof theappric€nt as mixingsamprein onetesting.Theaboveresurt(s) wEsl^/ere onlygivenas the infomalityvatue. c o m p a r yi ! , 1 ,r j r l , ! , i ' i r - r lj i l l j l i f t [email protected]'gedby6ecompa L L . L .t f lt!!L\ mpreG) resbdrh3 b..6odd €ndorb i !r.,.,r rji,,f,.!. o-.ai'edo,n"i - . . ' " ' , o ". d * . ; r s - . . 4 D . a ' . 0 \ Test Report No. : CE/201'1/84956 Page: 4 of 7 Da1e| 2O1112JO1 POLYFILAG OBERALLMENDSTMSSE2OA,CH{3OOZUG / SWITZERLAND rtl |ltt Ltt tt 1) Thesesampleswere dissolved totallyby precondjtjoning methodaccorcling to belowflowcnaft. I Ur tesl methodexctuded) yang 2') Nameof thepersonwhomademeasuremedt: Climbgreat 3) Nameofthe pe6onin chargeof measurement TroyChang SampleI\reasurement Aciddigestion by suitable acid dependedon diferent samole material(as belowtable) Micro,,€vedigestionwith HNOs/HCUHF Addappopriateamountof digestion reagent Heatto appropriate temperatureto extract '1) AlkaliFusion 2) HCltodissolve ICP.AES Cool,filterdigestate throughfilter Add diphenyl-carbazide for SampleMaterial colordevelopment DigeslionAcid Steel,copper, aluminum, solder Aqua regia,HNO3,HCl,HF,H2O, Glass palladium, Gold,platinum, ce€mic HNO3/HF Aqua regia Silver HNO3 Plastic HrSO4,HrOr,HNO3,HCt Others Anyacidtototaldigestion comDa+ n yl , r i r l , r l l irrrtili:ll f;. i,.i.lF *iirrl\ I Ths dmenl s 'ged by 6e c6mpa subj.cl'o t tu $d conddo^sfor F 'j.r measurethe absorbance at 540 nm by UV-VIS :i,l\li. Aibn'onG dRn ro s6 rmid'onof rdrt +onsbi|yslo6cen'ad6Edc! !hdsrizo,qN4!F.vriieaoilf!1r,rjr.fr rt's6(0r)2eer^r+s6(or)rsrr@wa*on Test Report No.: CE/2011/84956 Pager5 of 7 Date:2011t1?/0i POLYFIL AG OBEMLLMENDSTMSSE 2OA,CH63OO ZUG/ SWITZERLAND nl| l||l[]tn PBB/PBDE analytical FLOW CHART 1) Narneofthe personwnonECerEasuerent: RonEnWong 2) NarE of the personin chargeof rEasurernent: TroyCharE Firsttestingprocess---t Odionalscreenprocess--,proc€ss - .> Confiarnation Screenamlysis """""'1""........ Sarpleextraction/ SoxhletdEthod Concentrate/Dilute Extractedsolution Ft|ter Analysis by GC/MS rsG)ras€drh s 16sr.6pod annd b€, .l:. c d n p , i yi , : r ' rl r i r i . : - r i i i l ' l ; i l i J t i i:i.!t i i!r,1!l l!l!l Th5dogrud6gu3dbyb.compan,s!jedb{sG:iemlcofu1disolsedepndddvede,t9v,'3daoncq {qed {o Tems aid coid{o.s ior E 3!d^gb'tyslo'9c€dandh's@ Ane oo r dr&^ ld s6 hrd'odo drty TestReport No.: C92011/84956 Dale: 2Olltiuj,l POLYFILAG OBERALLMENDSTRASSE 2OA,CH63OO ZUG/ SWITZERLANO |l!t][mmfftmfl Analyticalflow chartof halogencontent 1) Narneof thepersonwhonradenEasurenEntt RitaChen 2) Nameof the personin chargeof nEasurenEnt:TroyChang SanplepretreatnEnt/ Separation Weighting andputtings€rptein cetl OrygenBombCombustion / AbsorDtion Dildonto fixed\^clunE Analysis wasperforn€dby lC comtsiy riji,tlr r1rr,. 3' i r1lliitlft r+ Lt,. ! jt .Lti!11_\ Th3dogm.nlE]s!.dbybecon0,n'9qedb€Gd.r.|condloBds. 3G) r6€d rh s €d €pod €iid : r, 4r !rJll!j{- Page: 6 of 7 B re 3p.nsb]itr€b{scl€d3ndlhsd@ _Lirr!?,ri: i.ri:l1rj,t +8610r)r!e Test Report No.: CE/2011/84956 Paget7 ol7 D€l'e:2011112101 POLYFILAG OBERALLMENDSTMSSE 2OA,CH€3OO ZUG/ SWITZERLAND ltN ltlt]fltttltl * Thetestedaample/ part is markod by an anow it ifs shownon the Dhoto., '* Endof Report " cohF0 'ir ! i !!r, rt,{' I rr'ri,lr.r!"t; Ths dddmsl 6 'sd h, 6e c.np' ior sbdonc rom31dodneib abj 1, . 1,3 rii+r-\ I p3(s) t3d.d nEbd rspd€ntu1b3 1. . rr, tr,Jrrl(. r0 rh. rn'brd dr iab't, r:-Irir +:Iri14,.:i+s6loarrerD r+s6oareerr pws5@ Test Report Applicant: Number : TWNC00249179 Littelfuse Philippines Inc. LIMA Technology Center, Lipa City, Malvar, Batangas Date : Mar 28, 2012 Sample Description: One (1) group of submitted samples said to be : Part Description : Silver plated Wire Part Number : DRAGxxx Date Sample Received : Mar 22, 2012 Date Test Started : Mar 22, 2012 Test Conducted : As requested by the applicant, for details please refer to attached pages. Authorized By: On Behalf Of Intertek Testing Services Taiwan Limited K. Y. Liang Director This report shall not be reproduced except in full, without the written approval of the laboratory. Page 1 of 5 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401 Number : TWNC00249179 Test Conducted (Ⅰ) Test Result Summary : Test Item Heavy Metal Cadmium (Cd) content Lead (Pb) content Mercury (Hg) content Chromium VI (Cr6+) content (mg/kg with 50cm2) Result (ppm) Submitted Samples ND ND ND Negative (< 0.02) Remarks: ppm = Parts per million based on weight of tested sample = mg/kg ND = Not detected < = Less than mg/kg with 50cm2 = milligram per kilogram with 50 square centimetre Negative = A negative test result indicated positive observation was not found at the time of Test. Responsibility of Chemist : Irene Chiou / Kevin Liu / Cathy Chen Date Sample Received Test Period : Mar 22, 2012 : Mar 22, 2012 To Mar 27, 2012 (Ⅱ) RoHS Requirement: Restricted Substances Cadmium (Cd) Content Lead (Pb) Content Mercury (Hg) Content Chromium VI (Cr6+) Content Limits 0.01% (100ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for homogeneous material. Page 2 of 5 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401 Number : TWNC00249179 Test Conducted (Ⅲ) Test Method: Test Item Cadmium (Cd) content Lead (Pb) content Mercury (Hg) content Chromium VI (Cr6+) content Test Method With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in clause 7, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in annex B, by boiling water extraction and determined by UV-Vis Spectrophotometer. Reporting Limit 2 ppm 2 ppm 2 ppm 0.02 mg/kg with 50cm2 Remark: Reporting limit = Quantitation limit of analyte in sample Page 3 of 5 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401 Number : TWNC00249179 Test Conducted (Ⅳ) Measurement Flowchart: Test For Cd/Pb/Hg/Chromium (VI) Reference Standard:IEC 62321 edition 1.0:2008 Sampling/grinding or cutting Cd/Pb/Hg Cr Polymers / Electronics Metal For different material, digest the sample with *1 appropriate acid By spot test Negative Confirm the tested samples are totally dissolved Make up with deionized water 6+ *2 Weigh sample and add alkaline solution Get 50cm2 sample Definite temp. extraction Boiling water extraction Cool and filter the extract Analyzed by ICP-OES Make up with deionized water and add diphenylcarbazide solution Analyzed by UV-VIS Remarks: *1: List Of Appropriate Acid: Material Polymers Metals Electronics Acid Added For Digestion HNO3,HCl,HF,H2O2,H3BO3 HNO3,HCl,HF HNO3,HCl,H2O2,HBF4 *2: If the result of spot test is positive, Chromium VI would be determined as detected. End of Report Page 4 of 5 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401 Number : TWNC00249179 Test Conducted Photo Page 5 of 5 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401