ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: Compact 3.6 x 10 mm Single Pigtail Fuse Product #: 877xxx Series Issue Date: June 03, 2013 It is hereby certified by Littelfuse, Inc. that there is neither RoHS (EU Directive 2002/95/EC, 2011/65/EU)-restricted substance nor such use, for materials to be used for unit parts, for packing/packaging materials, and for additives and the like in the manufacturing processes. In addition, it is hereby reported to you that the parts and sub-materials, the materials to be used for unit parts, the packing/packaging materials, and the additives and the like in the manufacturing processes, are all composed of the following components. Issued : <Global EHS Specialist > (1) Parts, sub-materials and unit parts This document covers the Compact 3.6 x 10 mm Single Pigtail Fuse, RoHS-Compliant series products manufactured by Littelfuse, Inc. < Raw Materials Used Please see Table 1 (2) The ICP data on all measurable substances Please see appropriate pages as identifed in Table 1 Remarks: Form 585-047 Rev. A 1 2/21/06 Table 1: List of Raw Materials covered by this report Total Parts 1 2 3 4 5 6 Raw Material Part Number YJ50/YJM (909-444) 692481 934-065 7132 (425672) DRAG**** 648112-001 Raw Material Description Ceramic Base - Body Solder Cap & Lead wire (base & plating) Ink-Black Element - Wire-Sn Plated Ag/Cu Ceramic Yarn 2 Page(s) 3-9 10-15 16-19 20-29 30-34 35-42 Test Report Applicant: Littelfuse Philippines Inc. LIMA Technology Center, Lipa City, Malvar, Batangas Number : TWNC00304282 Date : Mar 29, 2013 Sample Description: One (1) group of submitted samples said to be : Part Description : Ceramic Body Part Number : 909-444_909-157_909-438 Date Sample Received : Mar 21, 2013 Date Test Started : Mar 22, 2013 Test Conducted : As requested by the applicant, for details please refer to attached pages. Authorized by: On Behalf of Intertek Testing Services Taiwan Limited K. Y. Liang Director *THJ0304282* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C. 全國公證檢驗股份有限公司 11492 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 1 of 7 Number Test Conducted : TWNC00304282 (Ⅰ) Test Result Summary: Test Item Result White ceramic RL ND 2 ND 2 ND 2 ND 1 ppm ND 5 ppm ND 5 ppm ND 5 ND 5 ND 5 ND 5 ND 5 ppm ND 5 ppm ND 5 ppm ND 5 Unit Test Method Heavy Metal Cadmium (Cd) Content ppm Lead (Pb) Content ppm Mercury (Hg) Content ppm Chromium VI (Cr6+) Content ppm Polybrominated Biphenyls (PBBs) Monobrominated Biphenyls (MonoBB) Dibrominated Biphenyls (DiBB) Tribrominated Biphenyls (TriBB) Tetrabrominated Biphenyls (TetraBB) Pentabrominated Biphenyls (PentaBB) Hexabrominated Biphenyls (HexaBB) Heptabrominated Biphenyls (HeptaBB) Octabrominated Biphenyls (OctaBB) Nonabrominated Biphenyls (NonaBB) Decabrominated Biphenyl (DecaBB) ppm ppm ppm ppm With reference to IEC 62321: 2008, by microwave digestion and determined by ICP-OES. With reference to IEC 62321: 2008, by microwave digestion and determined by ICP-OES. With reference to IEC 62321: 2008, by microwave digestion and determined by ICP-OES. With reference to IEC 62321: 2008, by alkaline digestion and determined by UV-Vis Spectrophotometer. With reference to IEC 62321: 2008, by solvent extraction and determined by GC-MS and further HPLC-DAD confirmation when necessary. *THJ0304282* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C. 全國公證檢驗股份有限公司 11492 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 2 of 7 Number Test Conducted Test Item Unit Polybrominated Diphenyl Ethers (PBDEs) Monobrominated Diphenyl Ethers ppm (MonoBDE) Dibrominated Diphenyl Ethers ppm (DiBDE) Tribrominated Diphenyl Ethers ppm (TriBDE) Tetrabrominated Diphenyl ppm Ethers (TetraBDE) Pentabrominated Diphenyl ppm Ethers (PentaBDE) Hexabrominated Diphenyl Ethers ppm (HexaBDE) Heptabrominated Diphenyl ppm Ethers (HeptaBDE) Octabrominated Diphenyl Ethers ppm (OctaBDE) Nonabrominated Diphenyl Ethers ppm (NonaBDE) Decabrominated Diphenyl Ether ppm (DecaBDE) Halogen Content Fluorine (F) ppm Chlorine (Cl) ppm Bromine (Br) ppm Iodine (I) ppm Remarks: ppm ND RL : TWNC00304282 Test Method With reference to IEC 62321: 2008, by solvent extraction and determined by GC-MS and further HPLC-DAD confirmation when necessary. With reference to EN 14582:2007 by calorimetric bomb with oxygen and determined by Ion Chromatograph. Result White ceramic RL ND 5 ND 5 ND 5 ND 5 ND 5 ND 5 ND 5 ND 5 ND 5 ND 5 ND ND ND ND 50 50 50 50 = parts per million based on weight of tested sample = mg/kg = Not detected = Reporting Limit, Quantitation limit of analyte in sample Responsibility of Chemist: Date Sample Received Test Period Kevin Liu/ Irene Chiou/ Vico Lin : Mar 21, 2013 : Mar 22, 2013 To Mar 29, 2013 *THJ0304282* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C. 全國公證檢驗股份有限公司 11492 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 3 of 7 Number Test Conducted (Ⅱ) Limit: RoHS Limit Restricted Substances Cadmium (Cd) content Lead (Pb) content Mercury (Hg) content Chromium VI (Cr6+) content Polybrominated Biphenyls (PBBs) Polybrominated Diphenyl Ehters (PBDEs) : TWNC00304282 Limits 0.01% (100ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) The above limits were quoted from Annex II of 2011/65/EU for homogeneous material. *THJ0304282* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C. 全國公證檢驗股份有限公司 11492 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 4 of 7 Number Test Conducted : TWNC00304282 (Ⅲ) Measurement Flowchart: Test for Cd/Pb/Hg/Chromium (VI)/PBBS/PBDES Contents Reference Standard: IEC 62321 edition 1.0:2008 Sample preparation For non-metal part For metal part Take sample and immerse into Aqua Regia, start to strip plating layer Stop the stripping procedure upon color change completely Take the Aqua solution as plating component and stripped body as substrate component PBBs/PBDEs Weigh sample and add organic solvent By Soxhlet extraction or Solvent extraction Concentrate the extract and make up with organic solvent Cr 6+ Substrate Cd/Pb/Hg Weigh sample and add alkaline solution For different material, digest the sample with *1 appropriate acid Plating Cr 6+ By spot test Definite temp. extraction Cool and filter the extract Confirm the tested samples are totally dissolved Negative Get 50cm2 sample Make up with deionized water By boiling water extraction Analyzed by ICP-OES Analyzed by GC-MSD Remarks: *1: List of Appropriate Acid: Material Polymers Metals Electronics *2 Make up with deionized water and add diphenyl-carbazide solution Analyzed by UV-VIS Acid Added for Digestion HNO3,HCl,HF,H2O2,H3BO3 HNO3,HCl,HF HNO3,HCl,H2O2,HBF4 *2: If the result of spot test is positive, Chromium VI would be determined as detected. *THJ0304282* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C. 全國公證檢驗股份有限公司 11492 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 5 of 7 Number Test Conducted : TWNC00304282 Test for Halogen Content Reference Standard:EN 14582 Sampling/grinding or cutting Add absorbent in a combustion flask & place weighed sample in equipment Fill oxygen into calorimetric bomb Ignite then leave the bomb at room temperature Transfer the absorbent into a volumetric flask Make up with deionized water Analyzed by ion chromatography End of Report This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a recommendation for any particular course of action. Intertek does not accept a duty of care or any other responsibility to any person other than the Client in respect of this report and only accepts liability to the Client insofar as is expressly contained in the terms and conditions governing Intertek's provision of services to you. Intertek makes no warranties or representations either express or implied with respect to this report save as provided for in those terms and conditions. We have aimed to conduct the Review on a diligent and careful basis and we do not accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by statute or otherwise, except in the event of our gross negligence or wilful misconduct. *THJ0304282* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C. 全國公證檢驗股份有限公司 11492 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 6 of 7 Number Test Conducted : TWNC00304282 Photo *THJ0304282* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C. 全國公證檢驗股份有限公司 11492 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 7 of 7 Test Report Applicant: Number : TWNC00289673 Littelfuse Philippines Inc. LIMA Technology Center, Lipa City, Malvar, Batangas Date : Dec 13, 2012 Sample Description: One (1) group of submitted samples said to be : Part Description : Solder Part Number : 692481 Date Sample Received : Dec 06, 2012 Date Test Started : Dec 07, 2012 Test Conducted : As requested by the applicant, for details please refer to attached pages. Authorized By: On Behalf Of Intertek Testing Services Taiwan Limited K. Y. Liang Director *THJ0289673* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C. 全國公證檢驗股份有限公司 11492 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 1 of 6 Number : TWNC00289673 Test Conducted (Ⅰ) Test Result Summary : Result (ppm) Silvery metal Test Item Heavy Metal Cadmium (Cd) content Lead (Pb) content Mercury (Hg) content Chromium VI (Cr6+) content (mg/kg with 50cm2) ND 260 ND Negative (< 0.02) Remarks: ppm = Parts per million based on weight of tested sample = mg/kg ND = Not detected < = Less than mg/kg with 50cm2 = milligram per kilogram with 50 square centimetre Negative = A negative test result indicated positive observation was not found at the time of Test. Responsibility of Chemist : Irene Chiou / Kevin Liu Date Sample Received Test Period : Dec 06, 2012 : Dec 07, 2012 To Dec 12, 2012 (Ⅱ) RoHS Limits: Restricted Substances Cadmium (Cd) Content Lead (Pb) Content Mercury (Hg) Content Chromium VI (Cr6+) Content Limits 0.01% (100ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) The above limits were quoted from Annex II of 2011/65/EU for homogeneous material. *THJ0289673* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C. 全國公證檢驗股份有限公司 11492 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 2 of 6 Number : TWNC00289673 Test Conducted (Ⅲ) Test Method: Test Item Cadmium (Cd) content Lead (Pb) content Mercury (Hg) content Chromium VI (Cr6+) content Test Method With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in clause 7, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in annex B, by boiling water extraction and determined by UV-Vis Spectrophotometer. Reporting Limit 2 ppm 2 ppm 2 ppm 0.02 mg/kg with 50cm2 Remark: Reporting limit = Quantitation limit of analyte in sample *THJ0289673* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C. 全國公證檢驗股份有限公司 11492 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 3 of 6 Number : TWNC00289673 Test Conducted (Ⅳ) Measurement Flowchart: Test For Cd/Pb/Hg/Chromium (VI) Reference Standard:IEC 62321 edition 1.0:2008 Sampling/grinding or cutting Cd/Pb/Hg Cr 6+ Polymers / Electronics Metal For different material, digest the sample with *1 appropriate acid By spot test Negative Confirm the tested samples are totally dissolved Make up with deionized water *2 Weigh sample and add alkaline solution Get 50cm2 sample Definite temp. extraction Boiling water extraction Cool and filter the extract Analyzed by ICP-OES Make up with deionized water and add diphenylcarbazide solution Analyzed by UV-VIS *THJ0289673* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C. 全國公證檢驗股份有限公司 11492 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 4 of 6 Number : TWNC00289673 Test Conducted Remarks: *1: List of Appropriate Acid: Material Acid Added for Digestion Polymers HNO3,HCl,HF,H2O2,H3BO3 Metals HNO3,HCl,HF Electronics HNO3,HCl,H2O2,HBF4 *2: If the result of spot test is positive, Chromium VI would be determined as detected. End of Report This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a recommendation for any particular course of action. Intertek does not accept a duty of care or any other responsibility to any person other than the Client in respect of this report and only accepts liability to the Client insofar as is expressly contained in the terms and conditions governing Intertek's provision of services to you. Intertek makes no warranties or representations either express or implied with respect to this report save as provided for in those terms and conditions. We have aimed to conduct the Review on a diligent and careful basis and we do not accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by statute or otherwise, except in the event of our gross negligence or wilful misconduct. *THJ0289673* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C. 全國公證檢驗股份有限公司 11492 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 5 of 6 Number : TWNC00289673 Test Conducted Photo *THJ0289673* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C. 全國公證檢驗股份有限公司 11492 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 6 of 6 AOV"BPFS,U TESTREPORT R02 NO.:4002R12100802+1 Dare:ocr.10,2012 Customer:SuzhouFuHongElectronjc InduslrialCo., Lld. XIANGCHENG DlsTRlCT, SUZHOU, CHINA Addres!:NO.89WEIDUROAD,WANGTINGTOWN, to be Reporton ths submitreds.mplesald S.mplename:CoppeJ,shell Mod€h/ Item/LoiNo.:/ Metarlal:/, Buyer: / , Suppli€r:/ Samplorecaivsdd.te: Ocl.08.2012 1o'O4r'10, 2012 Testinsperiod:Ffomoct os,20!€ '\l ' . . ,, E9S!.s-Ecs!ed9!f samplein Chrcmium contentin thesubmitled & Hexavalent As specifiedby dient, to determineihe Lead,cadmlun, Mercury accordancewith Dircctive2002/95/EC{RoHS). Ec!!!s-ee$9!.: instrumeni I\4QL Measunng Testingltem (cd) Cadmium (Hg) [4ercury IEC62321:2008,s€ction9 |EC62321: 2008,seclionI 7 lEc 623212008,seclron Chromum(Cr\rl) IEC623212008AnnexB Lead(Pb) ICP€ES 2-'nglkg ICP-OES 2 mg/kg tcP-oEs 2 mg/kg 0.02m9/k9' Ieq r 0.02mg/kgreE|sto theMQLofsampleextfaction liquid SsElcge!: Decision ol 18 Aug 2005 of commission withthe requirements -whentesledas speci{i€d samplecomplied the submitted 2005/618/Ec noiiliedunderdocument 2002/95/Ec Directjve amending ILS,PLEASEREFERTOTHE FOLLOWNGPAGE(S)*** signedlor andon behalfof Brcncn Co.,Ltd,Kunshan Technology Shenzhen AOVTesling We-r k] n **n*"oor, /blfil caeateaaer: LiTingting,Maggie ooo,',*or44. Ylan Qi, lrickey Chemic€lTestDirecror S I t E N 2 H E NA O V T f S I I N G T € C H N O I , O 6 YC O . , I " T O . K U N S N ABNR A N C T I , /// \ Noll ne Ja,t 7tt) 9€'t'o AOV'*F#S,[ TESTREPORT NO.:4002R121008024-1 R02 Oate:Od.10,2012 1. To Determiney'.ead, C€dmium Contenli(Metalsubslrate) I*redby (y'a04* Weighihe sampleinto Add ihe digestionsolulionithe vesselis heatedunlilthe sample AddHrOruntilthe sampleis clear nlter;washed and Cooling thevess€|, Rlled wat€r. 10themarkwithdistill€d To Dete sulit€le) Content i|retb.r . \ . The sampleis digestedin the Weighihe sample microwaveovenfollowinga specific decomposrlonprogram Tested by lcP-oES Coolingthe vessel,tiltei washedand filledlothe maiKwilh dislilledwater. ChromiumContenl(boiling-wat€F€xtlaclion):([4etalEubstrate) Takethe (50i5) cm, samplein the beaker. Heat50 mLof Olwaterin thebe6ker to boilingfor 1o F;;1.- lhe sample, andcool Remove thebeak€rto roomtemperature, anddo thecolorreaction Testthe samplesolutionand lhe 0.02 ng/kg standardsolltion by uv-vls. BSANCH lCCINOLOGYCO.,LTD.KUNSIIAN SH€NZH€NAOVTESTITIG (: Hotlrne 'tL)0700 8600 nov'Bpf,F,il TESTREPORT NO.: 4002R121008024-1R02 Daie:Ocl.10, 2012 5. TooetemineHexavalenl Chromium Contonlin colorlessand coloredchromatecoatingon metats:iPtating) _ .. -i\ : va'hu't' lfthe lest resultis positive, the sample is consideredto havehexavalent chmmium Place 1-5 Boiling- water- extraotion procedu€shallbe usedto and the 0.02 mg/kg lflhee is interference or it is hardto decide whetherlhesamplehavelhe hexavalent 5.2Boiling-wateF enradion Remove thesample, andcool thebeaker lo roomtemperalure, anddolhe colorreaction Heat50 mlof Dlwaier in the samplein thebeaker. beakerto boilingfor 10 min Testtnesamplesolution andlhe0.02 mg/kgstandadsolulion by UV-VIS. SampleDelcriptlon: Code 1-1 SampleDescndion Substrate Plating Te3tR63ulb: Unit RoHSLimit Lead(Pb) msfts 1000 N.D. 10 (Cd) Cadmium Merorry(Hg) mg/K9 N.D. ms/Kg 100 1000 N.D, N.O. N.D. Chromium {Crl,ll) m9/kg 1000 Negative Negative s8€NZh€N AOVT€SrtNGTECHNOlOSYCO,,tTD,TUNSHAI! ARANCH ,.r Ho t l i ne .100700B6a0 nov'F"Ff"qn TESTREPORT No.:A002R1210o602:L1 R02 -ThenewRoHSdircclive 2011/6tEU,on Jul.21,2011comeintoforc€,onJan.03,2013lheformalimplementation, Direclive repealed 2002r'95/EC simultaneously. ahallbe Sp€cimens, whichr€Slested lo detemineLead,Cadmium havebeendissolved andMercury Content, completely, -mg/kg=ppm , -N.D.=not i",,,,,, ( The iested sample resultis uncertain or neoatve., -"The te8t is bas€d on lhe followins d!!{mplifi: maybe cannot stand lor the physical lrdh 6t s€r Coppershell SH€NZII AFANCH AOVTIST|n|GTECHNOIOCVCO.,ITD.KUNSHAN Ho t l i ne 400 /00 8600 Test Report Applicant: Littelfuse Philippines Inc. LIMA Technology Center, Lipa City, Malvar, Batangas Number : TWNC00304280 Date : Mar 29, 2013 Sample Description: One (1) group of submitted samples said to be : Part Description : Black Ink Part Number : 425672 Date Sample Received : Mar 21, 2013 Date Test Started : Mar 22, 2013 Test Conducted : As requested by the applicant, for details please refer to attached pages. Authorized by: On Behalf of Intertek Testing Services Taiwan Limited K. Y. Liang Director *THJ0304280* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C. 全國公證檢驗股份有限公司 11492 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 1 of 10 Number : TWNC00304280 Test Conducted (Ⅰ) Test Result Summary: Test Item Result Submitted samples RL ND 2 ND 2 ND 2 ND 1 ppm ND 5 ppm ND 5 ppm ND 5 ND 5 ND 5 ND 5 ND 5 ppm ND 5 ppm ND 5 ppm ND 5 Unit Test Method Heavy Metal Cadmium (Cd) Content ppm Lead (Pb) Content ppm Mercury (Hg) Content ppm Chromium VI (Cr6+) Content ppm Polybrominated Biphenyls (PBBs) Monobrominated Biphenyls (MonoBB) Dibrominated Biphenyls (DiBB) Tribrominated Biphenyls (TriBB) Tetrabrominated Biphenyls (TetraBB) Pentabrominated Biphenyls (PentaBB) Hexabrominated Biphenyls (HexaBB) Heptabrominated Biphenyls (HeptaBB) Octabrominated Biphenyls (OctaBB) Nonabrominated Biphenyls (NonaBB) Decabrominated Biphenyl (DecaBB) ppm ppm ppm ppm With reference to IEC 62321: 2008, by microwave digestion and determined by ICP-OES. With reference to IEC 62321: 2008, by microwave digestion and determined by ICP-OES. With reference to IEC 62321: 2008, by microwave digestion and determined by ICP-OES. With reference to IEC 62321: 2008, by alkaline digestion and determined by UV-Vis Spectrophotometer. With reference to IEC 62321: 2008, by solvent extraction and determined by GC-MS and further HPLC-DAD confirmation when necessary. *THJ0304280* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C. 全國公證檢驗股份有限公司 11492 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 2 of 10 Number : TWNC00304280 Test Conducted Test Item Unit Polybrominated Diphenyl Ethers (PBDEs) Monobrominated Diphenyl Ethers ppm (MonoBDE) Dibrominated Diphenyl Ethers ppm (DiBDE) Tribrominated Diphenyl Ethers ppm (TriBDE) Tetrabrominated Diphenyl ppm Ethers (TetraBDE) Pentabrominated Diphenyl ppm Ethers (PentaBDE) Hexabrominated Diphenyl Ethers ppm (HexaBDE) Heptabrominated Diphenyl ppm Ethers (HeptaBDE) Octabrominated Diphenyl Ethers ppm (OctaBDE) Nonabrominated Diphenyl Ethers ppm (NonaBDE) Decabrominated Diphenyl Ether ppm (DecaBDE) Phthalates Di(2-ethylhexyl) Phthalate ppm (DEHP) Dibutyl Phthalate (DBP) ppm Benzyl Butyl Phthalate (BBP) ppm Halogen Content Fluorine (F) ppm Chlorine (Cl) ppm Bromine (Br) ppm Iodine (I) ppm Others Hexabromo cyclododecane (HBCDD) ppm Test Method With reference to IEC 62321: 2008, by solvent extraction and determined by GC-MS and further HPLC-DAD confirmation when necessary. Result Submitted samples RL ND 5 ND 5 ND 5 ND 5 ND 5 ND 5 ND 5 ND 5 ND 5 ND 5 With reference to EN 14372: 2004, by solvent extraction and determined by GC-MS. ND 50 ND ND 50 50 With reference to EN 14582:2007 by calorimetric bomb with oxygen and determined by Ion Chromatograph. ND ND ND ND 50 50 50 50 With reference to USEPA 3540C, by solvent extraction and determined by GC-MS. ND 10 *THJ0304280* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C. 全國公證檢驗股份有限公司 11492 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 3 of 10 Number : TWNC00304280 Test Conducted Remarks: ppm ND RL = parts per million based on wet weight of tested sample = mg/kg = Not detected = Reporting Limit, Quantitation limit of analyte in sample Responsibility of Chemist: Date Sample Received Test Period Kevin Liu/ Irene Chiou/ Vico Lin : Mar 21,2013 : Mar 22,2013 to Mar 26,2013 (Ⅱ) Limit: RoHS Limit Restricted Substances Limits Cadmium (Cd) content 0.01% (100ppm) Lead (Pb) content 0.1% (1000ppm) Mercury (Hg) content 0.1% (1000ppm) Chromium VI (Cr6+) content 0.1% (1000ppm) Polybrominated Biphenyls (PBBs) 0.1% (1000ppm) Polybrominated Diphenyl Ehters (PBDEs) 0.1% (1000ppm) The above limits were quoted from Annex II of 2011/65/EU for homogeneous material. *THJ0304280* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C. 全國公證檢驗股份有限公司 11492 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 4 of 10 Number : TWNC00304280 Test Conducted (Ⅲ) Measurement Flowchart: Test for Cd/Pb/Hg/Chromium (VI)/PBBS/PBDES Contents Reference Standard: IEC 62321 edition 1.0:2008 Sample preparation For non-metal part For metal part Take sample and immerse into Aqua Regia, start to strip plating layer Stop the stripping procedure upon color change completely Take the Aqua solution as plating component and stripped body as substrate component PBBs/PBDEs Weigh sample and add organic solvent By Soxhlet extraction or Solvent extraction Concentrate the extract and make up with organic solvent Analyzed by GC-MSD Cr 6+ Substrate Cd/Pb/Hg Weigh sample and add alkaline solution For different material, digest the sample with *1 appropriate acid Plating Cr 6+ By spot test Definite temp. extraction Cool and filter the extract Confirm the tested samples are totally dissolved Negative *2 Get 50cm2 sample Make up with deionized water By boiling water extraction Analyzed by ICP-OES Make up with deionized water and add diphenyl-carbazide solution Analyzed by UV-VIS *THJ0304280* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C. 全國公證檢驗股份有限公司 11492 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 5 of 10 Number : TWNC00304280 Test Conducted Remarks: *1: List of Appropriate Acid: Material Polymers Metals Electronics Acid Added for Digestion HNO3,HCl,HF,H2O2,H3BO3 HNO3,HCl,HF HNO3,HCl,H2O2,HBF4 *2: If the result of spot test is positive, Chromium VI would be determined as detected. *THJ0304280* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C. 全國公證檢驗股份有限公司 11492 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 6 of 10 Number : TWNC00304280 Test Conducted Test for Halogen Content Reference Standard:EN 14582 Sampling/grinding or cutting Add absorbent in a combustion flask & place weighed sample in equipment Fill oxygen into calorimetric bomb Ignite then leave the bomb at room temperature Transfer the absorbent into a volumetric flask Make up with deionized water Analyzed by ion chromatography *THJ0304280* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C. 全國公證檢驗股份有限公司 11492 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 7 of 10 Number : TWNC00304280 Test Conducted Test For Phthalates Contents Reference Method: EN 14372: 2004 Sampling/grinding or cutting Weigh sample and add organic solvent By solvent extraction Concentrate the extract and make up with organic solvent Analyzed by GC-MSD *THJ0304280* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C. 全國公證檢驗股份有限公司 11492 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 8 of 10 Number : TWNC00304280 Test Conducted Test For Hexabromocyclododecane (HBCDD) Reference Standard:USEPA 3540C Sampling/grinding or cutting Weigh sample and add organic solvent By soxhlet extraction Concentrate the extract and make up with organic solvent Analyzed by GC-MSD End of Report This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a recommendation for any particular course of action. Intertek does not accept a duty of care or any other responsibility to any person other than the Client in respect of this report and only accepts liability to the Client insofar as is expressly contained in the terms and conditions governing Intertek's provision of services to you. Intertek makes no warranties or representations either express or implied with respect to this report save as provided for in those terms and conditions. We have aimed to conduct the Review on a diligent and careful basis and we do not accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by statute or otherwise, except in the event of our gross negligence or wilful misconduct. *THJ0304280* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C. 全國公證檢驗股份有限公司 11492 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 9 of 10 Number : TWNC00304280 Test Conducted Photo *THJ0304280* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C. 全國公證檢驗股份有限公司 11492 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 10 of 10 Test Report Applicant: Number: ELSCHUKOM ELEKTROSCHUTZKOMPONENTENBAU GMBH GEWERBESTRASSE 87,D-98669 VEILSDORF, GERMANY Date: SHAH0036227401 JAN 18, 2013 Sample Description: Two(2) pieces of submitted samples said to be : (1) Mixed all kinds of metal substrates. (2) Mixed all kinds of plating layers. Item Name : Silver Plated & Pure Silver Wires. Item No. : (B-1) 101.014 -. ---– silver plated copper wire – Cu, Ag--% (B-2) 101.0131.---– pure silver wire – Ag 1000 (B-3) 101.0123.0--– silver plated purest nickel wire – Ni99.98%, Ag1% (B-4) 101.0182.0--– silver-copper alloy plated copper plated iron nickel alloy wire – ElconD, AgCu5% (B-5) 101.0120.0--– silver plated constantan wire – CuNi44, Ag5% (B-6) 101.0151.0--– silver plated copper - nickel 44 alloy wire – CuNi44, Ag10% (B-7) 1050--31.-------– pure silver strips – Ag 1000 pure Country Of Origin : Germany. ************************************************************************************************************************************************************ Tests Conducted: As requested by the applicant, for details refer to attached page(s). ************************************************************************************************************************************************************ To Be Continued Authorized by: For intertek testing services Ltd., Shanghai Jacob Lin General Manager Page 1 Of 5 Intertek Testing Services Ltd., Shanghai Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233 上海天祥質量技術服務有限公司 上海市宜山路 801 號金陵商務廣場 B 座 200233 Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740 www.intertek.com www.intertek.com.cn Test Report Number: SHAH0036227401 Tests Conducted (A) Test result of RoHS Directive: Result Testing item (1) Cadmium (Cd) content (mg/kg) ND Lead (Pb) content (mg/kg) ND Mercury (Hg) content (mg/kg) 6+ Chromium2(VI)(Cr ) result (by boiling water extraction on metal) (mg/kg with 50cm ) ND ND Result Testing item (2) Cadmium (Cd) content (mg/kg) /Plating ND Lead (Pb) content (mg/kg) /Plating ND Mercury (Hg) content (mg/kg) /Plating ND 6+ Chromium2(VI)(Cr ) result (by boiling water extraction on metal) (mg/kg with 50cm ) /Plating ND 2 Remark:mg/kg with 50cm = milligram per kilogram with 50 square centimeter ND = not detected (B) RoHS Requirement: Restricted substances Cadmium (Cd) Lead (Pb) Mercury (Hg) 6+ Chromium (VI) (Cr ) Limits 0.01% (100 mg/kg) 0.1% (1000 mg/kg) 0.1% (1000 mg/kg) 0.1% (1000 mg/kg) The above limits were quoted from RoHS Directive 2011/65/EU for homogeneous material. (C) Test method: Testing item Cadmium (Cd) content Lead (Pb) content Mercury (Hg) content 6+ Chromium (VI) (Cr ) content (for metal) Testing method With reference to IEC 62321 Edition 1.0: 2008, by acid digestion until the tested sample was totally dissolved, and determined by ICP-OES. With reference to IEC 62321 Edition 1.0: 2008, by acid digestion until the tested sample was totally dissolved, and determined by ICP-OES. With reference to IEC 62321 Edition 1.0: 2008, by acid digestion until the tested sample was totally dissolved, and determined by ICP-OES. With reference to IEC 62321 Edition 1.0: 2008, by boiling water extraction and determined by UV-VIS Spectrophotometer. Reporting limit 2 mg/kg 2 mg/kg 2 mg/kg 2 0.02mg/kg with 50cm (in testing solution) Date sample received: Jan.14, 2013 Testing period: Jan.14, 2013 To Jan.17, 2013 ************************************************************************************************************************************************************ To Be Continued Page 2 Of 5 Intertek Testing Services Ltd., Shanghai Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233 上海天祥質量技術服務有限公司 上海市宜山路 801 號金陵商務廣場 B 座 200233 Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740 www.intertek.com www.intertek.com.cn Test Report Number: SHAH0036227401 Tests Conducted (D) Measurement flowchart: Test for Cd/Pb/Hg/Cr (VI)/PBBs/PBDEs contents Reference standard: IEC 62321 Edition 1.0: 2008 Sampling/grinding or cutting Cr Cd/Pb/Hg Metal Weigh sample and for different material, digest the sample with *1 appropriate acid Positive No Confirm the tested samples are totally dissolved Yes Polymers / electronics PBBs/PBDEs Weigh sample and add alkaline solution Spot test Get 50cm samples 6+ Weigh sample and add organic solvent *2 Definite temp. Extraction 2 Boiling water extraction Soxhlet extraction or Solvent extraction Cool and filter the extract Concentrate the extract and make up with organic solvent Make up with deionized water Analyzed by ICP-OES Make up with deionized water and add diphenyl-carbazide solution Analyzed by GC-MSD Analyzed by UV-VIS Remarks: *1: list of appropriate acid: Material Polymers Metals Electronics Acid added for digestion HNO3,HCL,HF,H2O2,H3BO3 HNO3,HCL,HF HNO3,HCL,H2O2,HBF4 *2: If the result of spot test is positive, Chromium VI would be determined as detected. ************************************************************************************************************************************************************ To Be Continued Page 3 Of 5 Intertek Testing Services Ltd., Shanghai Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233 上海天祥質量技術服務有限公司 上海市宜山路 801 號金陵商務廣場 B 座 200233 Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740 www.intertek.com www.intertek.com.cn Test Report Number: SHAH0036227401 Tests Conducted ************************************************************************************************************************************************************ To Be Continued Page 4 Of 5 Intertek Testing Services Ltd., Shanghai Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233 上海天祥質量技術服務有限公司 上海市宜山路 801 號金陵商務廣場 B 座 200233 Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740 www.intertek.com www.intertek.com.cn Test Report Number: SHAH0036227401 Tests Conducted ************************************************************************************************************************************************************ End Of Report This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a recommendation for any particular course of action. Intertek does not accept a duty of care or any other responsibility to any person other than the Client in respect of this report and only accepts liability to the Client insofar as is expressly contained in the terms and conditions governing Intertek's provision of services to you. Intertek makes no warranties or representations either express or implied with respect to this report save as provided for in those terms and conditions. We have aimed to conduct the Review on a diligent and careful basis and we do not accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by statute or otherwise, except in the event of our gross negligence or wilful misconduct. Page 5 Of 5 Intertek Testing Services Ltd., Shanghai Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233 上海天祥質量技術服務有限公司 上海市宜山路 801 號金陵商務廣場 B 座 200233 Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740 www.intertek.com www.intertek.com.cn Test Report Applicant: Number : TWNC00285761 Littelfuse Philippines Inc. LIMA Technology Center, Lipa City, Malvar, Batangas Date : Nov 19, 2012 Sample Description: One (1) group of submitted samples said to be : Part Description : Yarn Part Number : 648112-001 Date Sample Received : Nov 12, 2012 Date Test Started : Nov 13, 2012 Test Conducted : As requested by the applicant, for details please refer to attached pages. Authorized By: On Behalf Of Intertek Testing Services Taiwan Limited K. Y. Liang Director *THJ0285761* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 1 of 8 Number : TWNC00285761 Test Conducted (Ⅰ) Test Result Summary : Result (ppm) Submitted Samples Test Item Heavy Metal Cadmium (Cd) content Lead (Pb) content Mercury (Hg) content Chromium VI (Cr6+) content Polybrominated Biphenyls (PBBs) Monobrominated Biphenyls (MonoBB) Dibrominated Biphenyls (DiBB) Tribrominated Biphenyls (TriBB) Tetrabrominated Biphenyls (TetraBB) Pentabrominated Biphenyls (PentaBB) Hexabrominated Biphenyls (HexaBB) Heptabrominated Biphenyls (HeptaBB) Octabrominated Biphenyls (OctaBB) Nonabrominated Biphenyls (NonaBB) Decabrominated Biphenyl (DecaBB) Polybrominated Diphenyl Ethers (PBDEs) Monobrominated Diphenyl Ethers (MonoBDE) Dibrominated Diphenyl Ethers (DiBDE) Tribrominated Diphenyl Ethers (TriBDE) Tetrabrominated Diphenyl Ethers (TetraBDE) Pentabrominated Diphenyl Ethers (PentaBDE) Hexabrominated Diphenyl Ethers (HexaBDE) Heptabrominated Diphenyl Ethers (HeptaBDE) Octabrominated Diphenyl Ethers (OctaBDE) Nonabrominated Diphenyl Ethers (NonaBDE) Decabrominated Diphenyl Ether (DecaBDE) ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND *THJ0285761* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 2 of 8 Number : TWNC00285761 Test Conducted (Ⅰ) Test Result Summary : Result (ppm) Submitted Samples Test Item Halogen Content Fluorine (F) Chlorine (Cl) Bromine (Br) Iodine (I) ND ND ND ND Remarks: ppm = Parts per million based on weight of tested sample = mg/kg ND = Not detected Responsibility of Chemist : Irene Chiou / Kevin Liu / Cathy Chen Date Sample Received Test Period : Nov 12, 2012 : Nov 13, 2012 To Nov 15, 2012 (Ⅱ) RoHS Limits: Restricted Substances Cadmium (Cd) Content Lead (Pb) Content Mercury (Hg) Content Chromium VI (Cr6+) Content Polybrominated Biphenyls (PBBs) Polybrominated Diphenyl Ehters (PBDEs) Limits 0.01% (100ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) The above limits were quoted from Annex II of 2011/65/EU for homogeneous material. *THJ0285761* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 3 of 8 Number : TWNC00285761 Test Conducted (Ⅲ) Test Method: Test Item Cadmium (Cd) content Lead (Pb) content Mercury (Hg) content Chromium VI (Cr6+) content Polybrominated Biphenyls (PBBs) Polybrominated Diphenyl Ethers (PBDEs) Halogen Content Test Method With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in clause 7, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in annex C, by alkaline digestion and determined by UV-Vis spectrophotometer. With reference to IEC 62321 edition 1.0:2008 in annex A, by solvent extraction and determined by GC-MS and further HPLC-DAD confirmation when necessary. With reference to IEC 62321 edition 1.0:2008 in annex A, by solvent extraction and determined by GC-MS and further HPLC-DAD confirmation when necessary. With reference to EN 14582:2007 by calorimetric bomb with oxygen and determined by Ion Chromatograph. Reporting Limit 2 ppm 2 ppm 2 ppm 1 ppm 5 ppm 5 ppm 50 ppm Remark: Reporting limit = Quantitation limit of analyte in sample *THJ0285761* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 4 of 8 Number : TWNC00285761 Test Conducted (Ⅳ) Measurement Flowchart: Test for Cd/Pb/Hg/Chromium (VI)/PBBS/PBDES Contents Reference Standard: IEC 62321 edition 1.0:2008 Sample preparation For non-metal part For metal part Take sample and immerse into Aqua Regia, start to strip plating layer Stop the stripping procedure upon color change completely Take the Aqua solution as plating component and stripped body as substrate component PBBs/PBDEs Weigh sample and add organic solvent By Soxhlet extraction or Solvent extraction Concentrate the extract and make up with organic solvent Analyzed by GC-MSD Cr 6+ Substrate Cd/Pb/Hg Weigh sample and add alkaline solution For different material, digest the sample with *1 appropriate acid Plating Cr 6+ By spot test Definite temp. extraction Cool and filter the extract Confirm the tested samples are totally dissolved Negative *2 Get 50cm2 sample Make up with deionized water By boiling water extraction Analyzed by ICP-OES Make up with deionized water and add diphenyl-carbazide solution Analyzed by UV-VIS *THJ0285761* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 5 of 8 Number : TWNC00285761 Test Conducted (Ⅳ) Measurement Flowchart: Remarks: *1: List of Appropriate Acid: Material Polymers Metals Electronics Acid Added for Digestion HNO3,HCl,HF,H2O2,H3BO3 HNO3,HCl,HF HNO3,HCl,H2O2,HBF4 *2: If the result of spot test is positive, Chromium VI would be determined as detected. *THJ0285761* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 6 of 8 Number : TWNC00285761 Test Conducted (Ⅳ) Measurement Flowchart: Test for Halogen Content Reference Standard:EN 14582 Sampling/grinding or cutting Add absorbent in a combustion flask & place weighed sample in equipment Fill oxygen into calorimetric bomb Ignite then leave the bomb at room temperature Transfer the absorbent into a volumetric flask Make up with deionized water Analyzed by ion chromatography End of Report This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a recommendation for any particular course of action. Intertek does not accept a duty of care or any other responsibility to any person other than the Client in respect of this report and only accepts liability to the Client insofar as is expressly contained in the terms and conditions governing Intertek's provision of services to you. Intertek makes no warranties or representations either express or implied with respect to this report save as provided for in those terms and conditions. We have aimed to conduct the Review on a diligent and careful basis and we do not accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by statute or otherwise, except in the event of our gross negligence or wilful misconduct. *THJ0285761* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 7 of 8 Number : TWNC00285761 Test Conducted Photo *THJ0285761* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 8 of 8