ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: Nano Fuse 1206 Product #: 458DR Series Issue Date: December 10, 2012 It is hereby certified by Littelfuse, Inc. that there is neither RoHS (EU Directive 2002/95/EC, 2011/65/EU)-restricted substance nor such use, for materials to be used for unit parts, for packing/packaging materials, and for additives and the like in the manufacturing processes. In addition, it is hereby reported to you that the parts and sub-materials, the materials to be used for unit parts, the packing/packaging materials, and the additives and the like in the manufacturing processes, are all composed of the following components. Issued by: <Global EHS Engineer> (1) Parts, sub-materials and unit parts This document covers the Nano Fuse-1206 RoHS-Compliant series products manufactured by Littelfuse, Inc. < Raw Materials Used Please see Table 1 (2) The ICP data on all measurable substances Please see appropriate pages as identifed in Table 1 Remarks: Pb (lead) contained in the high temperature melting solder > 85% and is categorized as exempt under section 7a of the RoHS Annex. Form 585-047 Rev. A 1 2/21/06 Table 1: List of Raw Materials covered by this report Total Parts 1 2 3 4 5 Raw Material Part Number 909-443 910-275 082xxx 692321 425809 Raw Material Description Body Cap Element – Ag Plated Cu/Ni Solder Ink 2 Page(s) 3-10 11-16 17-26 27-32 33-41 Test Report Applicant: Number : TWNC00285769 Littelfuse Philippines Inc. LIMA Technology Center, Lipa City, Malvar, Batangas Date : Nov 19, 2012 Sample Description: One (1) group of submitted samples said to be : Part Description : Body Part Number : 909-443 Date Sample Received : Nov 12, 2012 Date Test Started : Nov 13, 2012 Test Conducted : As requested by the applicant, for details please refer to attached pages. Authorized By: On Behalf Of Intertek Testing Services Taiwan Limited K. Y. Liang Director *THJ0285769* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 1 of 8 Number : TWNC00285769 Test Conducted (Ⅰ) Test Result Summary : Result (ppm) Beige Plastic Test Item Heavy Metal Cadmium (Cd) content Lead (Pb) content Mercury (Hg) content Chromium VI (Cr6+) content Polybrominated Biphenyls (PBBs) Monobrominated Biphenyls (MonoBB) Dibrominated Biphenyls (DiBB) Tribrominated Biphenyls (TriBB) Tetrabrominated Biphenyls (TetraBB) Pentabrominated Biphenyls (PentaBB) Hexabrominated Biphenyls (HexaBB) Heptabrominated Biphenyls (HeptaBB) Octabrominated Biphenyls (OctaBB) Nonabrominated Biphenyls (NonaBB) Decabrominated Biphenyl (DecaBB) Polybrominated Diphenyl Ethers (PBDEs) Monobrominated Diphenyl Ethers (MonoBDE) Dibrominated Diphenyl Ethers (DiBDE) Tribrominated Diphenyl Ethers (TriBDE) Tetrabrominated Diphenyl Ethers (TetraBDE) Pentabrominated Diphenyl Ethers (PentaBDE) Hexabrominated Diphenyl Ethers (HexaBDE) Heptabrominated Diphenyl Ethers (HeptaBDE) Octabrominated Diphenyl Ethers (OctaBDE) Nonabrominated Diphenyl Ethers (NonaBDE) Decabrominated Diphenyl Ether (DecaBDE) ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND *THJ0285769* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 2 of 8 Number : TWNC00285769 Test Conducted (Ⅰ) Test Result Summary : Result (ppm) Beige Plastic Test Item Halogen Content Fluorine (F) Chlorine (Cl) Bromine (Br) Iodine (I) ND ND ND ND Remarks: ppm = Parts per million based on weight of tested sample = mg/kg ND = Not detected Responsibility of Chemist : Irene Chiou / Kevin Liu / Cathy Chen Date Sample Received Test Period : Nov 12, 2012 : Nov 13, 2012 To Nov 15, 2012 (Ⅱ) RoHS Limits: Restricted Substances Cadmium (Cd) Content Lead (Pb) Content Mercury (Hg) Content Chromium VI (Cr6+) Content Polybrominated Biphenyls (PBBs) Polybrominated Diphenyl Ehters (PBDEs) Limits 0.01% (100ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) The above limits were quoted from Annex II of 2011/65/EU for homogeneous material. *THJ0285769* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 3 of 8 Number : TWNC00285769 Test Conducted (Ⅲ) Test Method: Test Item Cadmium (Cd) content Lead (Pb) content Mercury (Hg) content Chromium VI (Cr6+) content Polybrominated Biphenyls (PBBs) Polybrominated Diphenyl Ethers (PBDEs) Halogen Content Test Method With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in clause 7, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in annex C, by alkaline digestion and determined by UV-Vis spectrophotometer. With reference to IEC 62321 edition 1.0:2008 in annex A, by solvent extraction and determined by GC-MS and further HPLC-DAD confirmation when necessary. With reference to IEC 62321 edition 1.0:2008 in annex A, by solvent extraction and determined by GC-MS and further HPLC-DAD confirmation when necessary. With reference to EN 14582:2007 by calorimetric bomb with oxygen and determined by Ion Chromatograph. Reporting Limit 2 ppm 2 ppm 2 ppm 1 ppm 5 ppm 5 ppm 50 ppm Remark: Reporting limit = Quantitation limit of analyte in sample *THJ0285769* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 4 of 8 Number : TWNC00285769 Test Conducted (Ⅳ) Measurement Flowchart: Test for Cd/Pb/Hg/Chromium (VI)/PBBS/PBDES Contents Reference Standard: IEC 62321 edition 1.0:2008 Sample preparation For non-metal part For metal part Take sample and immerse into Aqua Regia, start to strip plating layer Stop the stripping procedure upon color change completely Take the Aqua solution as plating component and stripped body as substrate component PBBs/PBDEs Weigh sample and add organic solvent By Soxhlet extraction or Solvent extraction Concentrate the extract and make up with organic solvent Analyzed by GC-MSD Cr 6+ Substrate Cd/Pb/Hg Weigh sample and add alkaline solution For different material, digest the sample with *1 appropriate acid Plating Cr 6+ By spot test Definite temp. extraction Cool and filter the extract Confirm the tested samples are totally dissolved Negative *2 Get 50cm2 sample Make up with deionized water By boiling water extraction Analyzed by ICP-OES Make up with deionized water and add diphenyl-carbazide solution Analyzed by UV-VIS *THJ0285769* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 5 of 8 Number : TWNC00285769 Test Conducted (Ⅳ) Measurement Flowchart: Remarks: *1: List of Appropriate Acid: Material Polymers Metals Electronics Acid Added for Digestion HNO3,HCl,HF,H2O2,H3BO3 HNO3,HCl,HF HNO3,HCl,H2O2,HBF4 *2: If the result of spot test is positive, Chromium VI would be determined as detected. *THJ0285769* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 6 of 8 Number : TWNC00285769 Test Conducted (Ⅳ) Measurement Flowchart: Test for Halogen Content Reference Standard:EN 14582 Sampling/grinding or cutting Add absorbent in a combustion flask & place weighed sample in equipment Fill oxygen into calorimetric bomb Ignite then leave the bomb at room temperature Transfer the absorbent into a volumetric flask Make up with deionized water Analyzed by ion chromatography End of Report This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a recommendation for any particular course of action. Intertek does not accept a duty of care or any other responsibility to any person other than the Client in respect of this report and only accepts liability to the Client insofar as is expressly contained in the terms and conditions governing Intertek's provision of services to you. Intertek makes no warranties or representations either express or implied with respect to this report save as provided for in those terms and conditions. We have aimed to conduct the Review on a diligent and careful basis and we do not accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by statute or otherwise, except in the event of our gross negligence or wilful misconduct. *THJ0285769* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 7 of 8 Number : TWNC00285769 Test Conducted Photo *THJ0285769* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 8 of 8 Test Report Applicant: Number : TWNC00285774 Littelfuse Philippines Inc. LIMA Technology Center, Lipa City, Malvar, Batangas Date : Nov 19, 2012 Sample Description: One (1) group of submitted samples said to be : Part Description : Cap Part Number : 910-275 Date Sample Received : Nov 12, 2012 Date Test Started : Nov 13, 2012 Test Conducted : As requested by the applicant, for details please refer to attached pages. Authorized By: On Behalf Of Intertek Testing Services Taiwan Limited K. Y. Liang Director *THJ0285774* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 1 of 6 Number : TWNC00285774 Test Conducted (Ⅰ) Test Result Summary : Result (ppm) (1) (2) Test Item Heavy Metal Cadmium (Cd) content Lead (Pb) content Mercury (Hg) content Chromium VI (Cr6+) content (mg/kg with 50cm2) ND ND ND Negative (< 0.02) (#) ND ND ND Negative (< 0.02) (#) Remarks: ppm = Parts per million based on weight of tested sample = mg/kg ND = Not detected < = Less than mg/kg with 50cm2 = milligram per kilogram with 50 square centimetre Negative = A negative test result indicated positive observation was not found at the time of Test. # = Due to the insufficient sample area, reduced total sample surface of 25 cm2 was used and the dilution factor was adjusted accordingly. Tested Components (1) Coppery metal base material (2) Golden plating layer Responsibility of Chemist : Irene Chiou / Kevin Liu Date Sample Received Test Period : Nov 12, 2012 : Nov 13, 2012 to Nov 16, 2012 (Ⅱ) RoHS Limits: Restricted Substances Cadmium (Cd) Content Lead (Pb) Content Mercury (Hg) Content Chromium VI (Cr6+) Content Limits 0.01% (100ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) The above limits were quoted from Annex II of 2011/65/EU for homogeneous material. *THJ0285774* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 2 of 6 Number : TWNC00285774 Test Conducted (Ⅲ) Test Method: Test Item Cadmium (Cd) content Lead (Pb) content Mercury (Hg) content Chromium VI (Cr6+) content Test Method With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in clause 7, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in annex B, by boiling water extraction and determined by UV-Vis Spectrophotometer. Reporting Limit 2 ppm 2 ppm 2 ppm 0.02 mg/kg with 50cm2 Remark: Reporting limit = Quantitation limit of analyte in sample *THJ0285774* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 3 of 6 Number : TWNC00285774 Test Conducted (Ⅳ) Measurement Flowchart: Test For Cd/Pb/Hg/Chromium (VI) Reference Standard:IEC 62321 edition 1.0:2008 Sample preparation Take sample and immerse into Aqua Regia, start to strip plating layer Stop the stripping procedure upon color change completely Take the Aqua solution as plating component and stripped body as substrate component Cd/Pb/Hg Substrate For different material, digest the sample with *1 appropriate acid Cr 6+ By spot test Confirm the tested samples are totally dissolved Make up with deionized water Plating Negative *2 Get 50cm2 sample By boiling water extraction Analyzed by ICP-OES Make up with deionized water and add diphenyl-carbazide solution Analyzed by UV-VIS *THJ0285774* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 4 of 6 Number : TWNC00285774 Test Conducted Remarks: *1: List Of Appropriate Acid: Material Polymers Metals Electronics Acid Added For Digestion HNO3,HCl,HF,H2O2,H3BO3 HNO3,HCl,HF HNO3,HCl,H2O2,HBF4 *2: If the result of spot test is positive, Chromium VI would be determined as detected. End of Report This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a recommendation for any particular course of action. Intertek does not accept a duty of care or any other responsibility to any person other than the Client in respect of this report and only accepts liability to the Client insofar as is expressly contained in the terms and conditions governing Intertek's provision of services to you. Intertek makes no warranties or representations either express or implied with respect to this report save as provided for in those terms and conditions. We have aimed to conduct the Review on a diligent and careful basis and we do not accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by statute or otherwise, except in the event of our gross negligence or wilful misconduct. *THJ0285774* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 5 of 6 Number : TWNC00285774 Test Conducted Photo *THJ0285774* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 6 of 6 ,fl.d,+E+ TestReport trTxlt*.5G nown ForOue5ll PleaseCo ithscs f i , S ( N " . ) , c E / 2 0 1 2 / ] 0 8 3 5 E 4 ( D a t e ) : 2 0 r 2 l 0 1 / 1 1 F & ( P a 8 e ): r o f r o ELSCHUrcMELEKTROSCHUTZI{OMPONENTENBAU GIIBH CEI'ERBESTR,ASSE 87, D-98669 \EIISDORF, GE&UA\Y ideltified Validit 68P 't&, -R& *,P +*&lf*P hylon behatf of rle client iiSZ,f*(s.'pl" D€s.ripr ion) if gd&(style/I r€b N".) 4 , & . E ( c o u n t i y" f o r i s i n ) {t4 A S (s.'!1" Rec€ivingDate) ,tlHS&l(Tesrihc P€.i od) ji,t,+ jR(rest Resrlts ) ' |l] *AnT (The folloeins saDples ra./rcre srbeittcd t|| fl m and as): SILIER PIATED & PURE SILVM $'IRES ',tr+*sR (PLEASEREFERTo PAGEs) (GERI4A\"Y) {EE 2012/0t/04 2 0 1 2 / 0 t / 0 4 ' f o2 a t 2 /a t / t l 5 + X .F - F { P r e a , e r e f p - r o r e x r ! a s c ! r (Alw4?\ C$Fdft.|nd chrnLd lrbor.tlry - Trlpd ? r'-;.!liiri i .: i ).:!tli p3G)6rad rb s rad Gpon€n'orF ir. r.r rl!tul. McmbForfie !69 Gouo6c! Sr,.r ,fla,+E+ TestReport ! t 4 5 ( N o .) : c E / 2 0 I 2 l l o d J s E q ( D a r " ) : 2 0 1 20 I / l l E*{pase) ,2 oi l0 ELSCHUKOM ELU(TRqSCHUTZXOMPONENTENMU GVBH GENERBESTI{ASSE 87, D-98669'IIEIISDORF,CE!.T{Ar\Y It**(T.st ]||lt[ttl||||fiml|! R e 6 u lt s ) jrl:i *r'.i (PARTNAME)No.l : ie;qma&ein& (6{t,r) (Jt6t ) (MTXED ALLmLoRtltErArNrm ( INCLUDINGTIiE PLATINC LA\'ER) (6 TYPES)) r|iiit E ttt.ttrl Etl{N *ittri +lt (Urit) ,fr / cadniun (cd) (rDL) +arEc 623zLt2oo8r;i, 4&,S*{ 6€*.F+&4t*.*d,h;Fl. / q'ith refe.ence perforfted S / Lead (Pb) to IFC 62327t 2008 anl 6y ICP-AFS. ++IEc 6232rt2008ti1, rr t$A*t +t*fr+**i*,;*d&;il. / {i ih .eference to IEC 62321: 2008 and by ICP-,ES. terforaed *- / vercury (Hs) : 2008t&,'r€E*4 ++ lEx.62321 +€ {/F + **t rt ;* d,*birl. / $i r1' reference to IEC 62321: ?008 and perforned by tCP-r{XS, ,i.flJ' / Heaav,lent chroni!n c.(vI) ++ \F: 62321.2OO8li*, t)a.,fr *+ / with fefe.€n€e ro IEc RliAtll. 6 2 3 2 1 . 2 i A B a n d p e r f o r m e db y B o iI i n s s a t e r e x t . a c t i o n M € t h o d . # }fr.+B** sulfonates / Perrruo.oocrane nglka (PF!S-Acid. Uetal salt t+us EPA3540C:1996tii, 'lil IO iE,9*f1[-r*&}f,4 an+,t,4*69' / t r i t h r e f e r e n c e t o u s E P A3 5 4 0 c 1 9 9 6n € t h o d f o r P F o SC o . l e . l . Analysis was perlorned by tClMS. an+6.(J+) / PFoA(cAsNo.: 3356? r) ++US EPA3540c:l996tt!, ,Xtl &Eif 1{r*{,*fl an+d(n) }f / w i t h r e f e t e n c € t o U S E P A3 5 4 0 C 1 9 9 6e e t h o d f o r P F O AC o n t e n t . Analysis was perfofned by rc/MS. i j :i :r l , ]. r : . a i i . ; ; r t i ] c o n o a .t y r r , : 1 r 1 , ri!' _, r r l - J n iy $qd rob cene6cdidroc d s onlysndwibinlh.imlsoic€nls'ns pelsr reded rhE bd rcpod Enid be 1, . r, rjr,!*. l0 s* (Resql t) No,1 rfla+E+ ft4(No.) : cE/20I2lr0835 Test Report E J q ( D a r :e2)0 t 2 l 0 t E * . t e , B " ,/ 3 . r ELSCHUKOM ELEKTROSCHUTZKONPONENTENBAU CMBq GMERBESTRASSE 87, D-98669 !'EIISDORF, GERMAIr\ d{t E lll +4o ,{fi,t* ( U n it ) ( R e s u1 t ) (IDL) No.l / uonobronobiphenyt :;Ad* qA#tri / Dib.onobipltenyl / T r i b r o n o b ip h e n y l / T e t r a b r 6 n o bLo h e n v l I*#Xi / P e n t a b r o n o br o h e n ! I / Hexabronobiphenyl ?!4$it +iASf / H e p r a b . o n o bpi h e . y 1 ^itrfi A / o.rabronobipheDyl / Nonabromobipheryt 4)qS* / D e c a b r o n o bpih e n y t +;ASf *trEc / suo of PBDES t*AS.t&t" -;ASf!{ / M o n o b r o n o dD i hehvl ether =-r[#*e :;A#+a{ / D i b r o n o d ip h e n y l e t h e r / ' l r i b r o d o d i p } e n v l er h e . B,*SiFa* / Tet ra6.onodi phe.vl erher i;*Sxad 'r*S*a* / P e . r a b r o m o dDi h € " v l e t h e r / H e a a b r o n o dpih e r v t e r h e r -k;A#Xa{ / H e p t a b r o m o d iD h € n v l e t h e r ,\;*SXa{ / o c r a b r o n o dD i he.vl ether ,L;i#*e i henvl etler i N o n a b r o m o dD +&#ii4 / D € c a b r o n o d i D h e n velt h e r 623211 zoo$iiF, ,tfu|aE +8dlf :*d,&jrl. / $ith rererence ro IEC 62321:?008 and perforned by rc/MS. 5 5 5 5 5 5 5 5 5 5 5 5 5 5 a* / s"l.s." (fr.) / Halogen-Floo.ine(F) (c{s 6* No.: 14?6?_94-8) (5.) / Haloeen-chlo.ine (cl) (cAs 6* ! o . : 2 2 5 3 71- 5 - r ) & * ( * ) / H a l o r e n - B r o n i n e( B r ) ( c A S l{o.: 10097-32-2) 50 ng/18 vx&+8fr ltBs vt r4s82:2007, 50 / sirh reference to Bs EN {r}*t. I 4 5 8 2 r 2 0 0 7A. n a l y si s v a s 50 (I) (cAS 6fr (dU / Halocen-lodine No.: 14362-44-8) conFiv;" r 1 llu.,[r'r, l: i/irr.r I i.tl lt!,lr'i oyglbredbb6ai.'alcondloisds 50 hrr.(s) rssbd rh s resr €pon ennd lLr Lt[]!. iq 3pdJb't}6lobc€da^dhsdocu b r** ,illt,rl EIE{I / su! of PBtss t*t**'ts :14#* :i*#f' (Iethod) ro l ]tl| ]t ,F{a+E+ ff6(No.) Test Report : CE/2012l10835 aBlJzr.) . 20L2/ot/71 Ftk(pare) : 1 of r0 EI-SCHIrXOI1I ELEKTROSCHUTZ(oVPO|iENTU\]BAU GttBH GEI/ERBE.STT.ASSE 87, D,98669 VEITSDORF.GERVIIY []tl||t][]tI| fiii(N.t.): l . m g l k g: p p m ;0 . | w t %= l o o o p p n 2 _ n _ d . = N o r D e t e c t e d( * . t A r r ) 3 - M D L: M e t l o d D e t e c t i o n L i r i i ( r l t l A ; { t s 1 8 1 6 ) 4. '- = Not R"sulated (Sli,+&.6) 5 . r ' = Q u a t i t a t i v e a n a L y s i s( N o u n i t ) _ € , B r ) * f ( * + & ) 6. #: a . P o s i t i v e b e a ! s t l e p . e s e n c eo f C r V t o n t h e r € s t e d a r e a s (po s i t i ve *,F rq,lit E q.tF jq r{ ,r{l rS) b . N e g a t i v e n e a n s t h e a b s e n c eo f C i V I o n r h € r e s t e d a . e a s ( Nesat i ve i nr::tl*, E 4 t.tA ).14 'r1l1g ) T h e d e t e c t e dc o h c e n r r a t i o ni n b o i l ] n a - e a r € r - e x r r a c t i o sno l u t i o n i s € q u a l o r g r € a r e r t h a b 0 . 0 2 m A l k gw i t h 50 cn: tested ar.a". / li6;i{XA>0.02 nslka *iih 50 cm, (tested z. tte.i,tlS{r.'Af ;F./.**isArxl:{,, *E+titi,sA,tt:ri}:+.Tftt 4 +1Erll+-ttlt aiAE. (The sanples sas/were analyzed on behalf of the atfricant ! e s u l t s w a s / w e r eo n l y g i v e n a s r t e i n f o . n a t i t y v a l u e , ) PFos++*d,(R"f Inf orlation)' "'.o"€ (1) riitrrf rTfi.'|tsld.&n,r+r+4rrf, as mixing sanpre in one resrine. The above !A+ 2oo6trzztEa (Di rect iae 2006/t2ztw) d.Ee,Ed,rlE*tla+,i6d.n,+0. 005%. (May not be placed on the market o. used as a sDbstance o. consrituent €qual io or nigh€r than 0.005 % by nass.) of prepararrons (2rtit{ttX4n&*fi&}.ei+d."%d.6s{.*{r1+;1!i*€1+}aX*Jt+ApFosi.4t?J*fi}.e.t&r€t6€};l4pFosEE ,i.&+,i!d.i,ifo.r%,6*r&€d.4{tti.4rf. {,RprrsaAt*f + 6E*;Ad.Ji;Aruc/.,. (Maynot be placed on ihe na.k€t in seni-linisned prodocts or articles, or pa.ts rhereof, if ure c o n c e n t . a t i o n o f P F O Si s e q u a t r o o r h i g h e . t h a n 0 . 1 % b y n a s s c a l c ! l a t e d s i t h r e f e r e n c e t o t l e n a s s o f s t . u c t u r a l i y o . f r i c . o s t r u c r u r a l l y d i s r i n . r p a r r s t ! a i c o n t a i n P F o . so r , f o . r e x r i t e s o r o t h e . c o a r e d naterials, if thc anoun! of PFOSis equal to o. hiahcr than Ug/nr of thc coated nateriat.) c o m p a ityr : ; r , r ; : i r l , , ; - f i t . r l J r . n i r r , . r , , t i i Ltlttr 1i., r".l,r!/,)! ont andub'n ihsh b orc en'3,ns -.4ttr - ! . ! , , : r r i r l l i - I. c i e o a F i -:.r ;::rlnti,,;i+46iDr,ssr7 l ,rla#+ TestReport ft,q(No.) : cE/20r2lr0835 E S ( D a t e ) : 2 0 1 2 1 0 1 / 1 1F * . ( p a s € ) : 5 o r l 0 EI-SCHIXOi,I ELEKTRO€CHUIZKNTPONENTENMU CVBH GEIIERBESTInSSE 87, D 98669 IEIT,SDORF.GERILUY tl&4!t(styl./I [t[t t.' N".) (B-1) 101. 014 -silver plated coFpe.{tre-Cu. Ag - - % (B-2) 101. 0131. - - - - -pure silve. sire-Ag l()()() ( B - 3 ) 1 0 1 . 0 1 2 3 . 0- - - - s i l v e r platcd purest nickct vire-Ni99.98%. AgI% -silve.-copper alloy plated cotpe. clad vire-Elcon D, (B-4) 10r,0182.0 - -silver (B 5) 101.0120.0 p l a t e d c o n s t a n t a nw i i € - C u N i 4 4 , A A S % ( B - 6 ) 1 0 1 . 0 1 5 1 . 0- - - - c o p p e r - n i c k e t 4 4 a l l o y s v e r p l a r e d s i . e - c u N i 4 4 , c o D o a n tv l r I t ! . , r - N ' | , r " l : l , i l l l i :. ! 1 1:;!1,1\ p sG)rssr€drh s€d Gpon€ind e rlllrillrl. ! ont 3nd*ii'n rh. hrs or c €nr s 'ns ri.:l,;l-":Iq:j1 tl| |||ll ,fl-d,#+ Test Report f i { 5 ( N o . ) : C E l 2 0 1 2 l l o s 3 s E S ( D a r e ): 2 o t z l 0 r / t t F # ( p a s € ) : ELSCHUI{OM ELEKTROSCHUTZKOMPONENTENBAU G\!BH GEWERBESTRNSSE 8?, D 98669 WILSDoII, CERMA\Y 6 0 f l 0 [l|[]|l r) ll?cr,-F $,EEn zI*1+ ' *.& aia*t+ . ( *1' j&d *tt *hrl. ) / Thes€samDtes !,€€ d€sotuedrolrrryby p.e-condrumhgmethooaccodinglo betN nowchad. cP re€tmethodexcludeo 2) r.lri^l: yang $e ! / Naheotlneps6onwhomadenEsuremed:ctimbgreal 3) ir'13{I i ^ : tl4* / Nameof the pe6on in chargeormeasu€m€nlrTroychans tr*. {rtt*s /curing. p€galaton iqr{.&,cf ! / sdde MeasuEmenl &lf;F n l*'.g6tt{ f, 6 }xn!trai&it,tirt /LoeTt 4rt/!inlt n.i'la{&,aib / 4,;) /Acid dig€slion by suitabte acid dependedon dtrerenlsahdemaledat{asbetowiable) MiorcMve digestion with HNO3/HC|/HF ,"rl4rOf jit& jt.li,lilt + C( / H€i to appropriate 1) 2) f [*a{*4+*it{rtc / AlkaliF6ion /HCltod$d€ / rcP,aEs f!911L / samdeMatedal 51eel,@pper,allnirum, solder <gti ta{*tt ;filt&AJlfi / DiqesL|onAcd -t+, 4la{,!lt, nn*, el,,k / Aa@ reoia. HNO' HCl. HF. H,O, rra{,Inc / HNoJftF A, J6,€, nit / Gold,olalinum, Dalladium, ceramic ,i(f rf 7h-ir,g t.rLrlf,.' I irl#B*i{Aftrcnm 6id rti!€ /HNOr &E / Plaslic 4?,*i&8tt$ / coot, fherdigestate lhrough liher *d, t{"*, s!t, td / H,so. Ho,. HNorhcl ,! \'efi*1eti*l+ / Anyacldlo lotaldig€Gtion j i i r i r + r i l , i , ! . r 1 r . t p . l i , . 1 , i f i ' ! ! l . rhcdddneiiAs€dbysgcompa^ys!b4d{ob6ai..a|condloi3ds ab6o6anceat a/ronmby UV-VIS t]n]l ,F{a*R+ Test Report iEIS(No.) : cE/2012l10835 E rr?(Dare) : 2012l01/11 F&(P,s") ELSCHUKOMELEI$ROSCHUTZKOIIPONENTENB,qU GMBH CETERBESTRA.SSE87, D-98669 VEIISDORF, CER[{AI\'Y t ttt*/t rtt+4+f l *,aE / PBB/PBDE anatyticat FLOWCHART a }l{,/\l I a_i9*, / Nameoftheperson whomademeasuremenl: RomanWonq r,$Ji( frt ^ : &+le / Nam€of thepersonIn chargeof measurement TrcyCha;g n^ ld,ElF / Firstlestry proce.s------------f ....,---. prccess €*,E&*€F / OptionalscE€n -. -,t *{.€,S / Confimation orccess :l Scre€n analysis / ,, rfi+rt I I sample erlraclion *s+*/ Soxhlet melhod6i,+tx;* Concentrale/Dilute Enractedsoluiion +tri{ rira/ifi# Filter/ +S.i{'E.d Analysis byGC/MS / fr"ian&f ie*,+& *irl+ c o m D a n +! " , I rirr,,: i; r. lJ: ?.lria 1.:-!i -j!,AlrI 3u!,0db'.ms,idcoidsdislolE pslsl bdad h€rad cpod€nnorb3 i.,.-l:r311.! | | t l||tI l rF{-d,+E+ Test Report f t 1 4 ( N o . ) , C E / 2 0 r 2 l 1 0 8 3 5E S ( D a r . ) , 2 o l 2 l l ] t / t t F&{prse) EI.SCHUI(OM ELEI{TROSCHUTZ(OMA)NENTENB,{U GVBIi GE9ERBESTTASSE 87, D 98669 \,'EIT-SDoRF.GEf,Vl}IY it+&fiAn I I Il]tIltt][||||[|! / Analyticalflowchartof halogencontent jtli{,l.F : gi',g* / Naneof thepersonwhomademe€surement: RitaChen jrl:i,A ll, : #,*e / Nameof thepersonin cbargeof measurement: TroyChang *+E &t&.'sl'I Analysis wE6perfomedby lC .Iir Th s ddfuh.il s '$u€d bl ft np61s) rssbd fu bn cpod €nnor b i.'.iiri:llr it Li ii'!r]-l i -1"j! : pa c om 3 l b j e d b ] e m s a i d c o i d l o n s f o r E A t a ^ l o n 6 d d n l o f t ] m l a t o n d s b l t y .;.: r.r- i.1-]ii1 r,r+ s6iorre rD r+ s6 Lo?lrrenr wwslon ilts,#+ TestReport it4(No. ) : cE/2012l10835 AS(Dare) : 201210r/tr F*.(pase) : 9 of lo E-SCHUKOM EI-E(TROSCHUTZKO]\IIONENTEN&{U GMBH GEFERBESTRASSE 87, D-98669 VEIISDORF, CERMA]\ry tI|fll|t][taf, *Ji+n+fin€n / Analyticalflow chartofSoxhtetextraction(LC/MS)procedure r r i A/-F : ij!9*y / Nameofthe personwhomademeesuementRcmanWong t4j:{, q i,\ : tF'.*4 / Nameof the personin chargeof measurement: TroyChang ( rd8,{ a : Afi.+n*.n/Afi.+rt(*) , **.:4i{bA4, Test ltems: PFOS/PFOA. Benzotriazole) *{* cmpanyr:i r , tr 'ri_ll i ,r'"'ll:l ill+ r. r i rtirril: . / Datia p3G)r8sbd rh s rsd,epon €inore -. '.- it!,1 . pdisb ,9 a b b cr ed and ih s dotum / l trl'd,#+ TestReport fi6(N". ) , c-E/2072/10a35 Es(Date) : 2tr2/ar/r1 E*@aEe) : r0 of t0 ELSCHTJKOM ELENROSCHU'\ZKOMPONENTENBAU GMBH GEISRBESTR.ASSE 8?, D.98669 WII-SDOTF,GERVA}Y trlt[tl + ffifi tr'6*t*i ' Fl* ftfrfl*lt,rlz{tsi (The tested sanple / part is narked bt an arror if ir's 1083s 10835 ** lE+344.(E"d of Report) ++ i:. j:r.i | ,.tll itt: I c d h p , i in r . i ' , r , " r i l ' i , , rhsdoarudE 3s!sdbyhe.omp,^yeqedb G6erydcodromor s + *ri.*irr !r. i r,. l6en,a r,p. ' .. . !,r:L!. ${i' t shorn on rhe photo.) fl|||trr Test Report Applicant: Number : TWNC00285771 Littelfuse Philippines Inc. LIMA Technology Center, Lipa City, Malvar, Batangas Date : Nov 16, 2012 Sample Description: One (1) group of submitted samples said to be : Part Description : Solder (Pb is ≥ 90%) Part Number : 692321 Date Sample Received : Nov 12, 2012 Date Test Started : Nov 13, 2012 Test Conducted : As requested by the applicant, for details please refer to attached pages. Authorized By: On Behalf Of Intertek Testing Services Taiwan Limited K. Y. Liang Director *THJ0285771* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 1 of 6 Number : TWNC00285771 Test Conducted (Ⅰ) Test Result Summary : Result (ppm) Silvery metal Test Item Heavy Metal Cadmium (Cd) content Lead (Pb) content Mercury (Hg) content Chromium VI (Cr6+) content (mg/kg with 50cm2) ND 934557 ND Negative (< 0.02) Remarks: ppm = Parts per million based on weight of tested sample = mg/kg ND = Not detected < = Less than mg/kg with 50cm2 = milligram per kilogram with 50 square centimetre Negative = A negative test result indicated positive observation was not found at the time of Test. Responsibility of Chemist : Irene Chiou / Kevin Liu Date Sample Received Test Period : Nov 12, 2012 : Nov 13, 2012 to Nov 16, 2012 (Ⅱ) RoHS Limits: Restricted Substances Cadmium (Cd) Content Lead (Pb) Content Mercury (Hg) Content Chromium VI (Cr6+) Content Limits 0.01% (100ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) The above limits were quoted from Annex II of 2011/65/EU for homogeneous material. *THJ0285771* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 2 of 6 Number : TWNC00285771 Test Conducted (Ⅲ) Test Method: Test Item Cadmium (Cd) content Lead (Pb) content Mercury (Hg) content Chromium VI (Cr6+) content Test Method With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in clause 7, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in annex B, by boiling water extraction and determined by UV-Vis Spectrophotometer. Reporting Limit 2 ppm 2 ppm 2 ppm 0.02 mg/kg with 50cm2 Remark: Reporting limit = Quantitation limit of analyte in sample *THJ0285771* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 3 of 6 Number : TWNC00285771 Test Conducted (Ⅳ) Measurement Flowchart: Test For Cd/Pb/Hg/Chromium (VI) Reference Standard:IEC 62321 edition 1.0:2008 Sampling/grinding or cutting Cd/Pb/Hg Cr 6+ Polymers / Electronics Metal For different material, digest the sample with *1 appropriate acid By spot test Negative Confirm the tested samples are totally dissolved Make up with deionized water *2 Weigh sample and add alkaline solution Get 50cm2 sample Definite temp. extraction Boiling water extraction Cool and filter the extract Analyzed by ICP-OES Make up with deionized water and add diphenylcarbazide solution Analyzed by UV-VIS *THJ0285771* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 4 of 6 Number : TWNC00285771 Test Conducted Remarks: *1: List of Appropriate Acid: Acid Added for Digestion Material Polymers HNO3,HCl,HF,H2O2,H3BO3 Metals HNO3,HCl,HF Electronics HNO3,HCl,H2O2,HBF4 *2: If the result of spot test is positive, Chromium VI would be determined as detected. End of Report This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a recommendation for any particular course of action. Intertek does not accept a duty of care or any other responsibility to any person other than the Client in respect of this report and only accepts liability to the Client insofar as is expressly contained in the terms and conditions governing Intertek's provision of services to you. Intertek makes no warranties or representations either express or implied with respect to this report save as provided for in those terms and conditions. We have aimed to conduct the Review on a diligent and careful basis and we do not accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by statute or otherwise, except in the event of our gross negligence or wilful misconduct. *THJ0285771* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 5 of 6 Number : TWNC00285771 Test Conducted Photo *THJ0285771* Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410 Page 6 of 6 Test Report Applicant: Number : TWNC00253636 Littelfuse Philippines Inc. LIMA Technology Center, Lipa City, Malvar, Batangas Date : Apr 24, 2012 Sample Description: One (1) group of submitted samples said to be : Part Description : Black Ink Part Number : 425809 Date Sample Received : Apr 19, 2012 Date Test Started : Apr 19, 2012 Test Conducted : As requested by the applicant, for details please refer to attached pages. Authorized By: On Behalf Of Intertek Testing Services Taiwan Limited K. Y. Liang Director This report shall not be reproduced except in full, without the written approval of the laboratory. Page 1 of 9 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401 Number : TWNC00253636 Test Conducted (Ⅰ) Test Result Summary : Test Item Heavy Metal Cadmium (Cd) content Lead (Pb) content Mercury (Hg) content Chromium VI (Cr6+) content Polybrominated Biphenyls (PBBs) Monobrominated Biphenyls (MonoBB) Dibrominated Biphenyls (DiBB) Tribrominated Biphenyls (TriBB) Tetrabrominated Biphenyls (TetraBB) Pentabrominated Biphenyls (PentaBB) Hexabrominated Biphenyls (HexaBB) Heptabrominated Biphenyls (HeptaBB) Octabrominated Biphenyls (OctaBB) Nonabrominated Biphenyls (NonaBB) Decabrominated Biphenyl (DecaBB) Polybrominated Diphenyl Ethers (PBDEs) Monobrominated Diphenyl Ethers (MonoBDE) Dibrominated Diphenyl Ethers (DiBDE) Tribrominated Diphenyl Ethers (TriBDE) Tetrabrominated Diphenyl Ethers (TetraBDE) Pentabrominated Diphenyl Ethers (PentaBDE) Hexabrominated Diphenyl Ethers (HexaBDE) Heptabrominated Diphenyl Ethers (HeptaBDE) Octabrominated Diphenyl Ethers (OctaBDE) Nonabrominated Diphenyl Ethers (NonaBDE) Decabrominated Diphenyl Ether (DecaBDE) Result (ppm) Black Paste ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND Page 2 of 9 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401 Number : TWNC00253636 Test Conducted (Ⅰ) Test Result Summary : Test Item Result (ppm) Black Paste Halogen Content Fluorine (F) Chlorine (Cl) Bromine (Br) Iodine (I) Phthalates Di(2-ethylhexyl) Phthalate (DEHP) Dibutyl Phthalate (DBP) Benzyl Butyl Phthalate (BBP) Others Hexabromocyclododecane (HBCDD) ND 610 ND ND ND ND ND ND Remarks: ppm = Parts per million based on wet weight of tested sample = mg/kg ND = Not detected Responsibility of Chemist : Irene Chiou / Kevin Liu / Cathy Chen Date Sample Received Test Period : Apr 19, 2012 : Apr 19, 2012 To Apr 24, 2012 (Ⅱ) RoHS Requirement: Restricted Substances Cadmium (Cd) Content Lead (Pb) Content Mercury (Hg) Content Chromium VI (Cr6+) Content Polybrominated Biphenyls (PBBs) Polybrominated Diphenyl Ehters (PBDEs) Limits 0.01% (100ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) 0.1% (1000ppm) The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for homogeneous material. Page 3 of 9 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401 Number : TWNC00253636 Test Conducted (Ⅲ) Test Method: Test Item Test Method With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by Cadmium (Cd) content microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by Lead (Pb) content microwave digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition 1.0:2008 in clause 7, by microwave Mercury (Hg) content digestion until the tested samples are totally dissolved and determined by ICP-OES. With reference to IEC 62321 edition Chromium VI (Cr6+) 1.0:2008 in annex C, by alkaline content digestion and determined by UV-Vis spectrophotometer. With reference to IEC 62321 edition 1.0:2008 in annex A, by solvent Polybrominated extraction and determined by GC-MS Biphenyls (PBBs) and further HPLC-DAD confirmation when necessary. With reference to IEC 62321 edition Polybrominated 1.0:2008 in annex A, by solvent Diphenyl Ethers extraction and determined by GC-MS (PBDEs) and further HPLC-DAD confirmation when necessary. With reference to EN 14582:2007 by Halogen Content calorimetric bomb with oxygen and determined by Ion Chromatograph. With reference to EN 14372: 2004, by Phthalates solvent extraction and determined by GC-MS. With reference to USEPA 3540C, by Hexabromocyclododecane solvent extraction and determined by (HBCDD) GC-MSD. Reporting Limit 2 ppm 2 ppm 2 ppm 1 ppm 5 ppm 5 ppm 50 ppm 10 ppm 10 ppm Remark: Reporting limit = Quantitation limit of analyte in sample Page 4 of 9 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401 Number : TWNC00253636 Test Conducted (Ⅳ) Measurement Flowchart: Test for Cd/Pb/Hg/Chromium (VI)/PBBS/PBDES Contents Reference Standard: IEC 62321 edition 1.0:2008 Sample preparation For non-metal part For metal part Take sample and immerse into Aqua Regia, start to strip plating layer Stop the stripping procedure upon color change completely Take the Aqua solution as plating component and stripped body as substrate component Cd/Pb/Hg Cr Confirm the tested samples are totally dissolved Make up with deionized water PBBs/PBDEs Polymers / electronics Metal For different material, digest the sample with *1 appropriate acid 6+ Weigh sample and add organic solvent By spot test Negative Get 50cm2 sample By boiling water extraction *2 Weigh sample and add alkaline solution By Soxhlet extraction or Solvent extraction Definite temp. extraction Cool and filter the extract Analyzed by ICP-OES Concentrate the extract and make up with organic solvent Analyzed by GC-MSD Make up with deionized water and add diphenylcarbazide solution Analyzed by UV-VIS Remarks: *1: List of Appropriate Acid: Acid Added for Digestion Material Polymers HNO3,HCl,HF,H2O2,H3BO3 Metals HNO3,HCl,HF Electronics HNO3,HCl,H2O2,HBF4 *2: If the result of spot test is positive, Chromium VI would be determined as detected. Page 5 of 9 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401 Number : TWNC00253636 Test Conducted (Ⅳ) Measurement Flowchart: Test for Halogen Content Reference Standard:EN 14582 Sampling/grinding or cutting Add absorbent in a combustion flask & place weighed sample in equipment Fill oxygen into calorimetric bomb Ignite then leave the bomb at room temperature Transfer the absorbent into a volumetric flask Make up with deionized water Analyzed by ion chromatography Page 6 of 9 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401 Number : TWNC00253636 Test Conducted (Ⅳ) Measurement Flowchart: Test For Phthalates Contents Reference Method: EN 14372: 2004 Sampling/grinding or cutting Weigh sample and add organic solvent By solvent extraction Concentrate the extract and make up with organic solvent Analyzed by GC-MSD Page 7 of 9 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401 Number : TWNC00253636 Test Conducted (Ⅳ) Measurement Flowchart: Test For Hexabromocyclododecane (HBCDD) Reference Standard:USEPA 3540C Sampling/grinding or cutting Weigh sample and add organic solvent By soxhlet extraction Concentrate the extract and make up with organic solvent Analyzed by GC-MSD End of Report Page 8 of 9 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401 Number : TWNC00253636 Test Conducted Photo Page 9 of 9 Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401